#------------------------------------------------------------------------------ #$Date: 2022-10-10 16:50:38 +0300 (Mon, 10 Oct 2022) $ #$Revision: 278508 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/3/50/01/3500131.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_3500131 _cell_angle_alpha 90.000 _cell_angle_beta 103.573 _cell_angle_gamma 90.000 _cell_length_a 7.3431 _cell_length_b 14.0371 _cell_length_c 11.8160 _exptl_crystal_F_000 568.00 _reflns_d_resolution_high 0.8234 _cod_data_source_file jiw751.fcf _cod_data_source_block jiw751 _shelx_title ' Jiw751 in C2/c' _shelx_refln_list_code 4 _shelx_f_calc_maximum 208.27 _shelx_f_squared_multiplier 1.000 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 542.59 642.25 15.35 o 4 0 0 428.72 427.45 21.67 o 6 0 0 92.00 114.90 8.35 o 8 0 0 4.49 3.43 1.79 o 1 1 0 578.37 618.83 12.82 o 3 1 0 639.19 613.02 16.91 o 5 1 0 1469.41 1581.85 27.98 o 7 1 0 0.28 1.15 1.23 o 0 2 0 8.20 7.67 0.35 o 2 2 0 4208.03 4874.18 99.19 o 4 2 0 1155.81 1267.08 27.61 o 6 2 0 640.09 662.60 18.60 o 8 2 0 23.58 25.78 2.23 o 1 3 0 17071.44 16394.62 402.08 o 3 3 0 878.09 891.32 41.65 o 5 3 0 35.73 36.06 1.31 o 7 3 0 66.26 72.99 3.65 o 0 4 0 1640.08 1665.72 43.95 o 2 4 0 1103.34 1023.93 24.84 o 4 4 0 217.80 238.04 6.97 o 6 4 0 82.76 84.54 3.28 o 8 4 0 6.63 6.26 1.34 o 1 5 0 20.22 16.00 0.70 o 3 5 0 18.91 27.09 1.21 o 5 5 0 11.83 7.87 0.75 o 7 5 0 3.38 6.95 1.24 o 0 6 0 2874.79 3049.84 147.16 o 2 6 0 49.78 41.77 1.29 o 4 6 0 314.72 341.84 6.10 o 6 6 0 12.46 14.67 1.78 o 1 7 0 180.73 198.81 4.58 o 3 7 0 444.52 457.05 10.17 o 5 7 0 299.44 274.29 6.88 o 7 7 0 0.02 0.43 0.87 o 0 8 0 2715.93 2360.51 94.48 o 2 8 0 1259.66 1134.49 46.12 o 4 8 0 123.73 113.94 2.50 o 6 8 0 206.23 162.02 6.52 o 1 9 0 66.78 76.77 2.80 o 3 9 0 1749.34 1671.66 25.79 o 5 9 0 115.65 118.18 5.02 o 7 9 0 42.98 47.28 4.20 o 0 10 0 8.89 10.68 1.04 o 2 10 0 207.70 191.92 4.27 o 4 10 0 6.40 6.27 0.93 o 6 10 0 72.10 76.37 5.04 o 1 11 0 691.49 703.61 13.24 o 3 11 0 0.84 0.68 0.76 o 5 11 0 31.11 29.52 2.79 o 0 12 0 570.97 593.18 37.99 o 2 12 0 493.05 518.61 13.34 o 4 12 0 208.67 201.81 10.02 o 6 12 0 6.00 5.66 1.16 o 1 13 0 401.99 382.25 10.38 o 3 13 0 2.56 3.22 0.90 o 5 13 0 7.78 10.51 1.15 o 0 14 0 9.70 12.26 3.81 o 2 14 0 15.22 18.37 1.64 o 4 14 0 9.62 8.10 1.28 o 1 15 0 22.57 28.27 3.23 o 3 15 0 0.18 -0.38 0.78 o 0 16 0 39.96 36.64 4.56 o 2 16 0 43.19 49.77 2.81 o -7 1 1 103.91 96.53 11.87 o -5 1 1 842.22 853.74 15.97 o -3 1 1 3167.25 3249.35 71.84 o -1 1 1 2093.96 2411.71 44.80 o 1 1 1 400.65 428.93 8.21 o 3 1 1 368.19 330.96 9.36 o 5 1 1 249.98 265.76 5.49 o 7 1 1 0.05 0.05 1.11 o -8 2 1 0.03 1.17 1.05 o -6 2 1 5.38 4.45 1.10 o -4 2 1 51.27 53.90 1.44 o -2 2 1 13326.02 15118.24 401.39 o 0 2 1 67.15 63.69 1.25 o 2 2 1 274.50 286.71 8.15 o 4 2 1 14.38 13.26 0.98 o 6 2 1 178.16 198.03 6.77 o 8 2 1 13.10 16.67 1.76 o -7 3 1 0.13 0.06 0.91 o -5 3 1 2.00 1.22 0.51 o -3 3 1 108.86 109.74 3.23 o -1 3 1 2254.99 2711.74 53.84 o 1 3 1 13984.43 14298.94 289.38 o 3 3 1 6927.22 6748.42 204.88 o 5 3 1 79.87 80.89 1.97 o 7 3 1 60.08 63.72 12.52 o -8 4 1 88.62 107.06 7.03 o -6 4 1 117.52 127.08 4.34 o -4 4 1 164.04 168.04 4.53 o -2 4 1 700.85 681.84 18.26 o 0 4 1 12.87 15.97 0.49 o 2 4 1 1782.48 1679.26 41.25 o 4 4 1 860.19 866.20 18.11 o 6 4 1 80.21 84.77 3.06 o 8 4 1 7.45 5.72 1.24 o -7 5 1 16.73 9.51 1.89 o -5 5 1 686.74 704.24 12.43 o -3 5 1 4013.76 4508.28 99.45 o -1 5 1 344.23 394.76 9.74 o 1 5 1 1167.68 1074.58 43.89 o 3 5 1 150.02 123.75 4.34 o 5 5 1 0.99 0.53 0.52 o 7 5 1 63.34 68.14 3.77 o -8 6 1 13.46 15.54 2.17 o -6 6 1 0.75 1.30 0.98 o -4 6 1 738.23 724.69 12.04 o -2 6 1 483.45 395.36 13.01 o 0 6 1 3037.68 3192.23 65.13 o 2 6 1 899.52 771.36 43.43 o 4 6 1 816.18 839.09 14.29 o 6 6 1 33.79 34.65 2.12 o -7 7 1 0.17 0.50 0.89 o -5 7 1 498.94 511.55 11.73 o -3 7 1 962.07 1045.25 23.89 o -1 7 1 5.14 13.54 0.99 o 1 7 1 509.86 560.09 20.47 o 3 7 1 487.17 472.70 8.96 o 5 7 1 98.31 103.46 3.34 o 7 7 1 9.69 9.67 1.17 o -6 8 1 0.44 0.90 1.01 o -4 8 1 826.99 840.90 13.92 o -2 8 1 126.99 135.76 5.65 o 0 8 1 78.65 56.43 3.98 o 2 8 1 533.51 510.23 13.06 o 4 8 1 59.82 63.92 2.40 o 6 8 1 3.40 2.05 0.91 o -7 9 1 6.87 6.41 1.36 o -5 9 1 78.33 82.61 3.00 o -3 9 1 1.35 1.48 0.47 o -1 9 1 3.97 5.37 0.73 o 1 9 1 1440.37 1522.77 33.69 o 3 9 1 1011.56 954.24 15.63 o 5 9 1 109.23 101.02 4.36 o 7 9 1 0.05 -0.37 0.91 o -6 10 1 5.37 7.02 1.04 o -4 10 1 341.74 330.04 7.56 o -2 10 1 12.85 13.51 0.86 o 0 10 1 249.12 237.84 4.45 o 2 10 1 614.84 630.02 12.65 o 4 10 1 22.72 25.58 1.51 o 6 10 1 32.00 26.92 1.74 o -5 11 1 0.00 0.02 0.66 o -3 11 1 874.39 869.46 17.93 o -1 11 1 3.39 3.04 0.60 o 1 11 1 324.06 324.06 6.60 o 3 11 1 264.27 280.02 7.09 o 5 11 1 22.75 28.35 1.92 o -6 12 1 2.62 2.65 0.94 o -4 12 1 2.40 2.69 0.80 o -2 12 1 172.02 170.63 7.35 o 0 12 1 102.64 100.84 4.92 o 2 12 1 392.12 402.83 10.73 o 4 12 1 70.68 69.39 4.81 o -5 13 1 65.33 83.08 3.14 o -3 13 1 49.69 50.66 2.30 o -1 13 1 171.14 170.19 5.17 o 1 13 1 12.97 14.43 1.62 o 3 13 1 0.13 0.34 0.75 o 5 13 1 8.28 9.57 1.23 o -4 14 1 1.03 0.39 0.75 o -2 14 1 45.96 46.52 4.08 o 0 14 1 128.16 123.15 7.31 o 2 14 1 82.55 97.31 3.87 o 4 14 1 35.47 40.15 2.23 o -3 15 1 30.13 34.29 1.95 o -1 15 1 129.13 131.23 21.35 o 1 15 1 28.99 27.59 3.00 o 3 15 1 86.70 98.48 3.77 o -2 16 1 35.90 36.64 2.93 o 0 16 1 11.39 13.41 2.45 o 2 16 1 121.00 117.38 6.96 o -8 0 2 85.41 74.19 5.87 o -6 0 2 606.06 600.10 23.18 o -4 0 2 55.85 64.32 3.53 o -2 0 2 3631.15 4173.51 110.67 o 0 0 2 4543.63 4935.68 153.35 o 2 0 2 1764.80 2035.19 61.95 o 4 0 2 4029.42 4458.71 136.04 o 6 0 2 202.79 186.09 15.28 o 8 0 2 131.87 175.36 10.12 o -7 1 2 165.61 141.84 7.59 o -5 1 2 24.87 20.53 0.97 o -3 1 2 234.16 253.04 6.74 o -1 1 2 23920.28 19197.25 340.27 o 1 1 2 9.23 7.61 0.36 o 3 1 2 265.90 269.17 7.11 o 5 1 2 331.47 328.46 6.62 o 7 1 2 122.60 123.86 9.73 o -8 2 2 31.75 37.26 3.63 o -6 2 2 1.06 0.73 0.88 o -4 2 2 165.00 147.32 3.54 o -2 2 2 43376.73 35332.05 838.76 o 0 2 2 4576.92 5387.18 101.67 o 2 2 2 12.90 24.71 1.01 o 4 2 2 488.72 511.93 10.98 o 6 2 2 1.85 1.07 1.04 o 8 2 2 3.86 4.61 1.52 o -7 3 2 231.71 229.66 8.98 o -5 3 2 21.11 20.54 1.01 o -3 3 2 135.69 159.87 10.54 o -1 3 2 74.63 77.71 1.59 o 1 3 2 3747.57 4293.55 103.00 o 3 3 2 1760.23 1796.26 69.16 o 5 3 2 1.32 2.33 0.54 o 7 3 2 136.70 136.10 9.64 o -8 4 2 20.95 21.60 3.15 o -6 4 2 4.41 3.78 1.05 o -4 4 2 996.50 1116.59 31.67 o -2 4 2 2648.58 2699.36 102.70 o 0 4 2 1374.83 1563.91 27.67 o 2 4 2 385.40 365.87 15.94 o 4 4 2 10.47 5.51 0.55 o 6 4 2 166.10 152.61 8.53 o 8 4 2 6.60 7.62 1.59 o -7 5 2 132.26 117.47 6.33 o -5 5 2 122.39 124.07 2.71 o -3 5 2 3053.41 2843.17 77.18 o -1 5 2 379.04 440.70 9.12 o 1 5 2 4678.18 5285.71 125.80 o 3 5 2 106.01 97.97 2.64 o 5 5 2 153.37 135.81 4.55 o 7 5 2 1.30 0.99 0.92 o -8 6 2 4.98 5.91 1.03 o -6 6 2 290.67 309.62 9.61 o -4 6 2 178.74 195.72 3.48 o -2 6 2 869.32 781.58 24.36 o 0 6 2 77.09 89.00 2.21 o 2 6 2 1019.05 1161.26 33.27 o 4 6 2 324.77 363.24 6.21 o 6 6 2 0.17 0.65 0.88 o -7 7 2 67.87 75.10 3.94 o -5 7 2 872.20 947.21 20.60 o -3 7 2 23.71 27.57 1.24 o -1 7 2 358.86 405.93 23.54 o 1 7 2 336.08 333.90 7.93 o 3 7 2 1.57 2.58 0.49 o 5 7 2 244.19 226.39 9.61 o 7 7 2 14.02 16.79 1.40 o -6 8 2 0.18 -0.14 0.94 o -4 8 2 44.21 45.53 1.29 o -2 8 2 94.70 80.15 4.51 o 0 8 2 16.38 11.19 0.90 o 2 8 2 1095.44 1108.21 21.31 o 4 8 2 21.22 22.18 1.50 o 6 8 2 12.25 13.97 1.36 o -7 9 2 0.20 -0.20 1.00 o -5 9 2 45.66 45.21 2.02 o -3 9 2 310.48 302.08 5.30 o -1 9 2 1088.98 1150.23 24.33 o 1 9 2 531.89 554.77 10.57 o 3 9 2 31.53 24.50 1.16 o 5 9 2 248.69 252.44 13.34 o -6 10 2 67.80 73.26 4.55 o -4 10 2 404.16 437.59 9.40 o -2 10 2 1027.61 1005.32 19.57 o 0 10 2 604.24 537.12 9.71 o 2 10 2 225.27 247.82 5.01 o 4 10 2 148.53 161.71 8.22 o 6 10 2 66.36 71.27 3.61 o -5 11 2 102.35 90.66 3.78 o -3 11 2 31.55 33.21 1.83 o -1 11 2 259.77 228.27 4.68 o 1 11 2 1054.63 1028.90 28.42 o 3 11 2 98.80 90.18 3.40 o 5 11 2 38.59 38.71 2.23 o -6 12 2 2.30 2.80 0.76 o -4 12 2 0.56 0.20 0.62 o -2 12 2 18.52 16.97 1.41 o 0 12 2 145.75 158.69 5.12 o 2 12 2 53.27 54.92 2.83 o 4 12 2 247.00 223.13 18.48 o -5 13 2 41.87 41.13 1.86 o -3 13 2 49.47 46.56 2.38 o -1 13 2 158.83 153.16 4.76 o 1 13 2 12.12 13.85 1.85 o 3 13 2 46.56 43.18 2.92 o 5 13 2 192.44 214.95 10.01 o -4 14 2 13.98 24.08 1.90 o -2 14 2 37.73 31.56 3.41 o 2 14 2 54.58 61.36 3.05 o 4 14 2 8.66 9.43 1.25 o -3 15 2 35.56 40.23 2.10 o -1 15 2 108.71 110.34 8.75 o 1 15 2 8.38 5.99 1.54 o 3 15 2 3.48 5.48 1.12 o -2 16 2 5.65 4.89 1.25 o 0 16 2 8.08 6.06 2.80 o 2 16 2 17.85 19.71 3.09 o -7 1 3 51.57 39.92 3.12 o -5 1 3 131.07 122.35 2.78 o -3 1 3 1271.08 1507.44 33.12 o -1 1 3 2418.84 2588.63 51.71 o 1 1 3 3724.18 3868.83 105.33 o 3 1 3 447.69 401.06 15.69 o 5 1 3 193.47 193.16 4.15 o 7 1 3 24.50 28.94 2.10 o -8 2 3 38.54 33.90 2.62 o -6 2 3 51.87 55.89 2.71 o -4 2 3 58.15 67.83 3.33 o -2 2 3 1561.55 1868.96 35.22 o 2 2 3 7859.88 8443.08 184.40 o 4 2 3 37.12 29.65 1.06 o 6 2 3 0.40 0.07 0.98 o -7 3 3 151.97 169.89 5.56 o -5 3 3 321.90 336.26 6.37 o -3 3 3 855.63 859.51 29.95 o -1 3 3 82.95 85.67 1.65 o 1 3 3 1.98 2.09 0.27 o 3 3 3 470.23 541.03 12.11 o 5 3 3 84.25 77.14 3.19 o 7 3 3 76.92 79.36 9.42 o -8 4 3 71.73 78.83 8.68 o -6 4 3 47.66 52.10 2.32 o -4 4 3 4202.88 4687.79 111.77 o -2 4 3 2835.84 2669.62 81.35 o 0 4 3 235.35 203.70 3.85 o 2 4 3 959.02 1020.16 24.73 o 4 4 3 31.15 27.89 1.10 o 6 4 3 67.75 59.42 3.72 o -7 5 3 86.92 99.29 4.45 o -5 5 3 132.56 139.91 3.03 o -3 5 3 1122.22 1312.66 31.49 o -1 5 3 2511.54 2589.95 60.63 o 1 5 3 5850.91 6584.85 199.92 o 3 5 3 1737.63 1859.30 38.10 o 5 5 3 190.12 176.82 5.59 o 7 5 3 2.60 4.35 1.06 o -8 6 3 3.45 2.51 1.11 o -6 6 3 119.19 138.94 7.15 o -4 6 3 312.61 338.61 5.34 o -2 6 3 493.99 481.76 27.71 o 0 6 3 1178.70 1179.04 53.38 o 2 6 3 900.12 824.65 18.65 o 4 6 3 239.00 211.19 3.99 o 6 6 3 0.37 1.25 0.83 o -7 7 3 24.90 23.03 6.56 o -5 7 3 723.34 758.92 15.41 o -3 7 3 154.90 156.49 3.45 o -1 7 3 1456.97 1398.01 77.52 o 1 7 3 290.27 298.92 7.17 o 3 7 3 461.19 477.93 8.24 o 5 7 3 39.03 39.54 2.24 o 7 7 3 54.82 52.87 2.50 o -6 8 3 111.59 106.80 4.58 o -4 8 3 67.68 66.37 1.67 o -2 8 3 23.91 17.95 1.00 o 0 8 3 1932.73 2152.51 48.63 o 2 8 3 382.72 379.28 7.40 o 4 8 3 271.29 238.32 6.18 o 6 8 3 9.31 8.07 1.13 o -7 9 3 1.89 0.53 1.11 o -5 9 3 462.06 506.45 11.73 o -3 9 3 59.81 55.17 1.60 o -1 9 3 70.74 74.35 1.90 o 1 9 3 14.13 12.96 0.79 o 3 9 3 1.66 0.46 0.85 o 5 9 3 32.80 27.56 1.70 o -6 10 3 24.48 21.21 1.33 o -4 10 3 1.92 1.90 0.71 o -2 10 3 0.15 0.40 0.49 o 0 10 3 32.90 35.25 1.35 o 2 10 3 5.73 6.55 1.07 o 4 10 3 0.48 0.79 0.86 o 6 10 3 0.54 3.11 0.90 o -5 11 3 8.33 8.31 0.92 o -3 11 3 59.00 57.08 2.41 o -1 11 3 3.92 1.30 0.81 o 1 11 3 727.11 701.09 20.01 o 3 11 3 239.89 254.68 8.49 o 5 11 3 0.00 0.00 0.75 o -6 12 3 5.65 4.25 0.84 o -4 12 3 8.20 9.69 0.95 o -2 12 3 7.91 8.63 1.20 o 0 12 3 0.07 0.09 0.85 o 2 12 3 64.93 58.75 6.53 o 4 12 3 10.04 12.11 1.36 o -5 13 3 38.77 36.42 2.05 o -3 13 3 13.60 12.78 1.31 o -1 13 3 201.83 190.89 6.07 o 1 13 3 256.10 210.15 13.64 o 3 13 3 75.81 68.86 3.31 o -4 14 3 49.90 52.17 2.63 o -2 14 3 40.69 38.01 3.43 o 0 14 3 0.43 0.22 2.03 o 2 14 3 126.72 116.91 5.37 o 4 14 3 0.13 1.20 1.10 o -3 15 3 118.90 133.78 3.98 o -1 15 3 11.25 6.22 1.67 o 1 15 3 48.15 49.20 7.39 o 3 15 3 11.23 9.70 1.57 o -2 16 3 141.64 167.33 21.68 o -8 0 4 0.52 -0.24 1.35 o -6 0 4 1.43 -1.00 1.14 o -4 0 4 4928.46 5123.51 154.54 o -2 0 4 1880.66 1875.51 57.99 o 0 0 4 4210.66 4238.17 129.07 o 2 0 4 1314.80 1350.92 50.36 o 4 0 4 101.85 99.42 2.89 o 6 0 4 123.29 135.51 14.75 o -7 1 4 2.85 1.27 1.15 o -5 1 4 6.28 4.31 0.59 o -3 1 4 1094.46 1137.24 35.63 o -1 1 4 5070.64 5229.94 112.72 o 1 1 4 25.18 18.20 1.18 o 3 1 4 362.43 362.35 14.77 o 5 1 4 872.80 901.69 19.82 o 7 1 4 5.60 4.80 1.09 o -8 2 4 37.06 33.89 5.96 o -6 2 4 5.37 4.24 0.89 o -4 2 4 0.66 1.78 0.49 o -2 2 4 494.33 531.65 14.21 o 0 2 4 1978.21 2071.85 55.63 o 2 2 4 217.35 206.01 9.84 o 4 2 4 748.67 707.59 10.17 o 6 2 4 661.08 679.31 33.12 o -7 3 4 0.79 2.11 0.98 o -5 3 4 27.12 26.31 1.22 o -3 3 4 2657.07 2698.48 70.31 o -1 3 4 1828.04 1959.97 46.68 o 1 3 4 364.94 392.84 7.34 o 3 3 4 795.96 790.18 16.60 o 5 3 4 127.35 122.13 4.33 o 7 3 4 75.94 79.86 6.18 o -8 4 4 60.08 68.93 3.74 o -6 4 4 0.65 2.00 0.81 o -4 4 4 864.86 909.54 25.04 o -2 4 4 703.65 732.42 17.66 o 0 4 4 86.18 87.82 2.26 o 2 4 4 1.52 2.81 0.43 o 4 4 4 1.03 2.69 0.57 o 6 4 4 95.09 85.94 7.18 o -7 5 4 17.83 15.25 1.31 o -5 5 4 264.24 282.13 5.83 o -3 5 4 154.11 161.95 6.67 o -1 5 4 684.92 692.22 22.22 o 1 5 4 2717.38 2731.10 84.65 o 3 5 4 859.44 907.40 15.00 o 5 5 4 83.03 60.53 2.79 o 7 5 4 19.61 24.21 2.12 o -8 6 4 2.25 1.50 1.07 o -6 6 4 286.32 315.39 8.18 o -4 6 4 171.71 182.95 3.29 o -2 6 4 1.51 0.12 0.31 o 0 6 4 693.48 801.23 19.57 o 2 6 4 137.67 146.04 3.72 o 4 6 4 68.62 66.39 2.66 o 6 6 4 40.92 30.37 2.26 o -7 7 4 28.47 28.19 2.42 o -5 7 4 313.71 317.82 7.47 o -3 7 4 292.72 299.14 5.29 o -1 7 4 2144.44 2207.66 69.52 o 1 7 4 94.51 81.10 2.60 o 3 7 4 228.41 261.45 4.95 o 5 7 4 1.68 0.19 0.86 o -6 8 4 119.94 124.17 3.85 o -4 8 4 322.26 320.84 5.73 o -2 8 4 108.44 95.69 2.20 o 0 8 4 31.25 50.48 1.87 o 2 8 4 800.92 739.61 12.91 o 4 8 4 63.33 81.36 2.99 o 6 8 4 0.09 0.09 0.75 o -7 9 4 186.43 218.32 18.72 o -5 9 4 3.39 5.90 0.85 o -3 9 4 192.37 164.56 3.38 o -1 9 4 247.72 214.50 4.13 o 1 9 4 7.47 4.91 0.69 o 3 9 4 43.20 42.29 2.18 o 5 9 4 110.52 100.04 5.53 o -6 10 4 1.25 -0.54 0.64 o -4 10 4 15.08 15.71 1.14 o -2 10 4 240.49 234.74 5.23 o 0 10 4 180.29 159.17 4.14 o 2 10 4 314.50 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