#------------------------------------------------------------------------------ #$Date: 2016-03-21 05:35:49 +0200 (Mon, 21 Mar 2016) $ #$Revision: 178486 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/03/07/4030775.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4030775 loop_ _publ_author_name 'Evans, W. J.' 'McClelland, W. G.' 'Greci, M. A.' 'Ziller, J. W.' _publ_section_title ; The utility of aryloxide ligands as bridging ligands for europium and calcium- containing compounds ; _journal_name_full 'European Journal of Solid State and Inorganic Chemistry' _journal_page_first 145 _journal_page_last 156 _journal_volume 33 _journal_year 1996 _chemical_formula_sum 'C44 H66 Eu2 O10' _chemical_formula_weight 1058.91 _space_group_IT_number 19 _symmetry_cell_setting orthorhombic _symmetry_Int_Tables_number 19 _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.271(2) _cell_length_b 19.526(3) _cell_length_c 20.822(4) _cell_volume 4582.5(14) _diffrn_ambient_temperature 163 _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _exptl_absorpt_coefficient_mu 2.765 _exptl_crystal_density_diffrn 1.535 _refine_ls_number_parameters 506 _refine_ls_number_reflns 4182 _refine_ls_R_factor_gt 0.028 _refine_ls_wR_factor_gt 0.033 _cod_data_source_file EJSSIC-1996-33-145-156-1.cif _cod_data_source_block C44H66O10Eu2 _cod_depositor_comments ; No atomic coordinates in the paper ; _cod_original_cell_volume 4582.3(13) _cod_database_code 4030775 loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 x,y,z 2 1/2-x,-y,1/2+z 3 1/2+x,1/2-y,-z 4 -x,1/2+y,1/2-z loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv ? ? ? ? ? ?