#------------------------------------------------------------------------------ #$Date: 2019-11-26 02:53:48 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242446 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/24/4132473.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132473 loop_ _publ_author_name 'Liu, Wenqi' 'Oliver, Allen G.' 'Smith, Bradley D.' _publ_section_title ; Macrocyclic Receptor for Precious Gold, Platinum, or Palladium Coordination Complexes. ; _journal_issue 22 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 6810 _journal_page_last 6813 _journal_paper_doi 10.1021/jacs.8b04155 _journal_volume 140 _journal_year 2018 _chemical_formula_moiety 'C56 H52 N4 O4, Au Cl4, 2(C H Cl3), H5 O2' _chemical_formula_sum 'C58 H59 Au Cl10 N4 O6' _chemical_formula_weight 1459.55 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 83.563(2) _cell_angle_beta 83.050(2) _cell_angle_gamma 80.654(2) _cell_formula_units_Z 1 _cell_length_a 9.4815(13) _cell_length_b 11.0063(15) _cell_length_c 14.5690(19) _cell_measurement_reflns_used 8826 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 26.89 _cell_measurement_theta_min 2.46 _cell_volume 1482.5(3) _computing_cell_refinement 'Bruker SAINT (Bruker, 2015)' _computing_data_collection 'Bruker APEX-3 (Bruker, 2015)' _computing_data_reduction 'Bruker SAINT (Bruker, 2015)' _computing_molecular_graphics 'Bruker XP (Bruker, 2015)' _computing_publication_material 'CIFTAB (Sheldrick, 2008)' _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT-2014/2 (Sheldrick, 2015)' _diffrn_ambient_temperature 120(2) _diffrn_detector_area_resol_mean 8.33 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II' _diffrn_measurement_method 'combination of \w and \f-scans ' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0442 _diffrn_reflns_av_unetI/netI 0.0421 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 18 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 27621 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.188 _diffrn_reflns_theta_min 1.414 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 2.985 _exptl_absorpt_correction_T_max 0.9299 _exptl_absorpt_correction_T_min 0.8649 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details 'SADABS (Krause et al., 2015)' _exptl_crystal_colour 'blue / gold dichroic' _exptl_crystal_density_diffrn 1.635 _exptl_crystal_description rod _exptl_crystal_F_000 732 _exptl_crystal_size_max 0.091 _exptl_crystal_size_mid 0.063 _exptl_crystal_size_min 0.055 _refine_diff_density_max 1.829 _refine_diff_density_min -1.355 _refine_diff_density_rms 0.130 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.035 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 378 _refine_ls_number_reflns 6555 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.035 _refine_ls_R_factor_all 0.0377 _refine_ls_R_factor_gt 0.0350 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0558P)^2^+0.9511P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0856 _refine_ls_wR_factor_ref 0.0871 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6310 _reflns_number_total 6555 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b04155_si_002.cif _cod_data_source_block nd1710 _cod_database_code 4132473 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.773 _shelx_estimated_absorpt_t_max 0.853 _diffrn_source_monochromator 'Bruker TRIUMPH curved-graphite' _shelx_res_file ; TITL nd1710_a.res in P-1 nd1710.res created by SHELXL-2016/6 at 12:39:53 on 03-Oct-2017 REM Old TITL nd1710 in P1 REM SHELXT solution in P-1 REM R1 0.084, Rweak 0.061, Alpha 0.064, Orientation as input REM Formula found by SHELXT: C58 N6 O6 Cl8 Au CELL 0.71073 9.4815 11.0063 14.5690 83.563 83.050 80.654 ZERR 1.000 0.0013 0.0015 0.0019 0.002 0.002 0.002 LATT 1 SFAC C H N O CL AU UNIT 58 59 4 6 10 1 TEMP -153.150 SIZE 0.055 0.063 0.091 L.S. 10 BOND $H FMAP 2 PLAN 20 HTAB N1 Cl1 EQIV $1 -x, -y+1, -z+2 HTAB N2 Cl2_$1 EQIV $2 x, y+1, z HTAB O1W O2_$2 HTAB O1W O1 EQIV $3 -x, -y+2, -z+1 HTAB O1W O1W_$3 CONF ACTA WGHT 0.055800 0.951100 FVAR 0.11289 AU1 6 0.000000 0.500000 1.000000 10.50000 0.01936 0.01084 = 0.01437 -0.00300 -0.00041 -0.00267 CL1 5 0.191624 0.448084 0.893912 11.00000 0.02232 0.02388 = 0.01902 -0.00324 0.00147 0.00045 CL2 5 0.144903 0.466678 1.117514 11.00000 0.02351 0.02399 = 0.01893 -0.00457 -0.00416 -0.00046 O1 4 0.158828 0.757802 0.569001 11.00000 0.04327 0.01614 = 0.01529 -0.00142 0.00393 -0.00491 O2 4 0.051004 0.127316 0.672650 11.00000 0.06078 0.01886 = 0.02085 -0.00992 0.00844 -0.01560 N1 3 0.123373 0.690337 0.720264 11.00000 0.03317 0.01272 = 0.01380 -0.00137 -0.00006 -0.00596 H1N 2 0.121169 0.639004 0.759750 11.00000 0.01697 N2 3 -0.008063 0.252707 0.784637 11.00000 0.04280 0.01189 = 0.01920 -0.00702 0.00567 -0.01162 H2N 2 -0.000906 0.309611 0.802460 11.00000 0.02668 C1 1 0.112988 0.813296 0.751495 11.00000 0.03242 0.01676 = 0.01848 -0.00387 -0.00074 -0.00358 AFIX 23 H1A 2 0.029402 0.867677 0.727005 11.00000 -1.20000 H1B 2 0.200568 0.849246 0.726474 11.00000 -1.20000 AFIX 0 C2 1 0.144920 0.672103 0.630345 11.00000 0.01866 0.01829 = 0.01814 -0.00472 0.00050 -0.00166 C3 1 0.154589 0.542634 0.605000 11.00000 0.01996 0.01693 = 0.01380 -0.00390 -0.00156 -0.00307 C4 1 0.093181 0.452408 0.663612 11.00000 0.02268 0.01825 = 0.01041 -0.00456 0.00008 -0.00188 AFIX 43 H4 2 0.041122 0.472243 0.721261 11.00000 -1.20000 AFIX 0 C5 1 0.108389 0.332890 0.637373 11.00000 0.02196 0.01653 = 0.01398 -0.00563 0.00001 -0.00306 C6 1 0.183562 0.305312 0.551931 11.00000 0.02748 0.01777 = 0.01700 -0.00671 0.00084 -0.00482 AFIX 43 H6 2 0.192957 0.223634 0.534281 11.00000 -1.20000 AFIX 0 C7 1 0.245198 0.394666 0.491852 11.00000 0.02265 0.02381 = 0.01887 -0.00843 0.00111 -0.00596 C8 1 0.227770 0.514012 0.519284 11.00000 0.02133 0.02227 = 0.01559 -0.00163 0.00155 -0.00673 AFIX 43 H8 2 0.266469 0.577088 0.478837 11.00000 -1.20000 AFIX 0 C9 1 0.047706 0.231105 0.699180 11.00000 0.02598 0.02036 = 0.01496 -0.00602 -0.00095 -0.00393 C10 1 -0.064586 0.154923 0.848025 11.00000 0.04681 0.01961 = 0.01848 -0.00546 0.00546 -0.01485 AFIX 23 H10A 2 -0.001608 0.075232 0.838959 11.00000 -1.20000 H10B 2 -0.161455 0.147247 0.832653 11.00000 -1.20000 AFIX 0 C11 1 -0.074115 0.179885 0.948779 11.00000 0.03454 0.01463 = 0.01461 -0.00358 0.00441 -0.01163 C12 1 -0.206794 0.225112 0.995672 11.00000 0.02535 0.01672 = 0.02001 -0.00098 -0.00065 -0.01009 C13 1 -0.332106 0.269356 0.949524 11.00000 0.03279 0.03060 = 0.02496 0.00032 -0.00948 -0.01298 AFIX 43 H13 2 -0.326087 0.268693 0.884013 11.00000 -1.20000 AFIX 0 C14 1 -0.459505 0.312312 0.996342 11.00000 0.02592 0.03707 = 0.04457 -0.00013 -0.01101 -0.00709 AFIX 43 H14 2 -0.541083 0.341451 0.963638 11.00000 -1.20000 AFIX 0 C15 1 -0.471065 0.313767 1.094351 11.00000 0.02132 0.03852 = 0.04495 -0.00567 0.00120 -0.00494 AFIX 43 H15 2 -0.560722 0.343888 1.126809 11.00000 -1.20000 AFIX 0 C16 1 -0.356075 0.272824 1.142006 11.00000 0.02520 0.02402 = 0.02695 -0.00756 0.00639 -0.00712 AFIX 43 H16 2 -0.366709 0.273329 1.207650 11.00000 -1.20000 AFIX 0 C17 1 -0.218405 0.228661 1.095399 11.00000 0.02101 0.01465 = 0.02244 -0.00357 0.00102 -0.00751 C18 1 -0.096261 0.191673 1.142872 11.00000 0.02574 0.00931 = 0.01725 -0.00435 0.00040 -0.00519 C19 1 0.039006 0.158391 1.094504 11.00000 0.02414 0.01038 = 0.02315 -0.00097 -0.00152 -0.00565 C20 1 0.168419 0.131220 1.139114 11.00000 0.02931 0.01731 = 0.03527 -0.00129 -0.00724 -0.00672 AFIX 43 H20 2 0.164130 0.137166 1.203972 11.00000 -1.20000 AFIX 0 C21 1 0.297964 0.096876 1.089820 11.00000 0.02401 0.02427 = 0.06107 0.00446 -0.00576 -0.00283 AFIX 43 H21 2 0.382811 0.079572 1.120571 11.00000 -1.20000 AFIX 0 C22 1 0.306712 0.086889 0.993370 11.00000 0.02717 0.02727 = 0.05390 0.00463 0.00982 0.00142 AFIX 43 H22 2 0.397485 0.062313 0.960031 11.00000 -1.20000 AFIX 0 C23 1 0.188182 0.111723 0.948080 11.00000 0.03296 0.01789 = 0.03233 0.00010 0.01259 -0.00235 AFIX 43 H23 2 0.196732 0.103919 0.883284 11.00000 -1.20000 AFIX 0 C24 1 0.048745 0.149866 0.995903 11.00000 0.02662 0.00871 = 0.02240 -0.00174 0.00412 -0.00508 C25 1 0.334943 0.358879 0.401360 11.00000 0.03255 0.02842 = 0.01856 -0.01029 0.00676 -0.01156 C26 1 0.376028 0.470764 0.339098 11.00000 0.10857 0.04628 = 0.02921 -0.01747 0.03963 -0.03885 AFIX 137 H26A 2 0.288839 0.527625 0.325162 11.00000 -1.50000 H26B 2 0.429132 0.443740 0.281114 11.00000 -1.50000 H26C 2 0.436600 0.513055 0.370880 11.00000 -1.50000 AFIX 0 C27 1 0.474042 0.273955 0.426766 11.00000 0.02484 0.08539 = 0.03575 -0.02468 0.00150 0.00046 AFIX 137 H27A 2 0.529142 0.318999 0.460457 11.00000 -1.50000 H27B 2 0.532024 0.248388 0.369865 11.00000 -1.50000 H27C 2 0.449132 0.200646 0.466079 11.00000 -1.50000 AFIX 0 C28 1 0.253245 0.286738 0.347135 11.00000 0.03587 0.04148 = 0.01713 -0.01304 0.00272 -0.00894 AFIX 137 H28A 2 0.164229 0.338825 0.330565 11.00000 -1.50000 H28B 2 0.230011 0.212307 0.385671 11.00000 -1.50000 H28C 2 0.313188 0.262895 0.290453 11.00000 -1.50000 AFIX 0 C1S 1 0.502418 0.161951 0.679006 11.00000 0.06932 0.08564 = 0.07052 -0.02083 -0.00413 0.00559 AFIX 13 H1S 2 0.463973 0.198608 0.619402 11.00000 -1.20000 AFIX 0 CL3 5 0.429206 0.259356 0.760770 11.00000 0.04331 0.06948 = 0.06949 -0.03104 0.00327 -0.00611 CL4 5 0.688059 0.149243 0.659336 11.00000 0.04988 0.09212 = 0.06439 -0.01398 0.01612 0.00388 CL5 5 0.444471 0.018833 0.705266 11.00000 0.07825 0.06659 = 0.27015 -0.07465 -0.03787 -0.01498 O1W 4 0.112220 0.995392 0.533979 11.00000 0.07594 0.01873 = 0.02024 -0.00581 0.00239 -0.00662 H1WA 2 0.093032 1.043738 0.581580 11.00000 0.05365 H1WB 2 0.137145 0.908415 0.558229 11.00000 0.10482 H1WC 2 0.000000 1.000000 0.500000 10.50000 0.11260 HKLF 4 REM nd1710_a.res in P-1 REM R1 = 0.0350 for 6310 Fo > 4sig(Fo) and 0.0377 for all 6555 data REM 378 parameters refined using 0 restraints END WGHT 0.0558 0.9511 REM Highest difference peak 1.829, deepest hole -1.355, 1-sigma level 0.130 Q1 1 0.5439 0.1348 0.7382 11.00000 0.05 1.83 Q2 1 0.0921 0.4776 0.9761 11.00000 0.05 1.69 Q3 1 0.0003 0.4531 1.0584 11.00000 0.05 1.61 Q4 1 0.4399 -0.0034 0.7304 11.00000 0.05 1.09 Q5 1 0.4730 0.0275 0.6385 11.00000 0.05 0.86 Q6 1 0.6646 0.0845 0.6254 11.00000 0.05 0.78 Q7 1 0.1928 0.4165 0.9624 11.00000 0.05 0.65 Q8 1 0.4450 0.2980 0.7005 11.00000 0.05 0.62 Q9 1 0.4692 0.1823 0.7853 11.00000 0.05 0.54 Q10 1 0.5180 0.2416 0.7165 11.00000 0.05 0.51 Q11 1 0.4589 0.3595 0.4027 11.00000 0.05 0.50 Q12 1 0.1714 0.5030 0.8542 11.00000 0.05 0.49 Q13 1 0.0593 0.4616 1.1768 11.00000 0.05 0.49 Q14 1 0.1139 0.8197 0.8006 11.00000 0.05 0.48 Q15 1 0.0531 0.1743 1.0416 11.00000 0.05 0.48 Q16 1 0.2670 0.4657 0.8468 11.00000 0.05 0.45 Q17 1 -0.2078 0.2258 1.0455 11.00000 0.05 0.45 Q18 1 0.0735 0.3805 1.0813 11.00000 0.05 0.43 Q19 1 0.4888 0.3786 0.4139 11.00000 0.05 0.43 Q20 1 0.1193 0.5830 0.8475 11.00000 0.05 0.43 ; _shelx_res_checksum 13071 _shelx_hkl_file ; -1 0 0 254.55 7.30 -1 0 0 258.82 7.30 -1 0 0 256.05 7.31 -1 0 0 260.84 7.29 1 0 0 257.54 7.32 1 0 0 254.10 7.29 1 0 0 266.34 7.29 -2 0 0 64.80 2.08 -2 0 0 64.10 2.12 -2 0 0 67.22 2.07 2 0 0 66.28 2.12 2 0 0 65.08 2.05 -3 0 0 4.71 0.66 -3 0 0 5.30 0.60 -3 0 0 6.12 0.68 -3 0 0 5.56 0.67 3 0 0 4.54 0.65 3 0 0 5.27 0.35 3 0 0 5.10 0.35 3 0 0 4.83 0.58 -4 0 0 15.50 1.11 -4 0 0 14.32 1.13 -4 0 0 14.88 1.02 -4 0 0 15.16 1.10 4 0 0 14.56 0.59 4 0 0 13.91 0.59 4 0 0 15.11 1.02 4 0 0 13.45 1.14 -5 0 0 27.04 1.43 -5 0 0 26.83 1.50 -5 0 0 27.72 1.47 -5 0 0 24.63 1.35 5 0 0 27.30 1.36 5 0 0 26.70 0.94 5 0 0 27.35 1.50 5 0 0 27.70 0.94 -6 0 0 67.44 2.45 -6 0 0 66.54 2.51 -6 0 0 68.18 2.59 -6 0 0 67.63 2.59 6 0 0 64.76 2.58 6 0 0 67.47 2.04 6 0 0 67.09 2.46 6 0 0 66.15 2.05 -7 0 0 35.88 1.99 -7 0 0 41.49 2.05 -7 0 0 39.48 1.97 -7 0 0 41.40 1.91 7 0 0 40.76 1.37 7 0 0 40.21 2.05 7 0 0 39.62 1.85 7 0 0 40.02 1.37 -8 0 0 1.92 0.98 -8 0 0 1.93 0.97 -8 0 0 2.17 0.93 8 0 0 1.70 0.82 8 0 0 1.76 0.97 8 0 0 1.08 0.41 8 0 0 1.42 0.40 -9 0 0 21.88 1.71 -9 0 0 22.49 1.85 -9 0 0 24.16 1.95 9 0 0 22.17 1.03 9 0 0 23.56 1.99 9 0 0 23.53 1.70 -10 0 0 7.73 1.30 -10 0 0 3.15 1.28 -10 0 0 8.50 1.46 10 0 0 7.98 1.36 10 0 0 8.66 1.43 10 0 0 6.76 0.60 -11 0 0 3.39 1.50 11 0 0 5.26 1.46 11 0 0 4.27 0.55 11 0 0 3.07 1.44 11 -1 0 11.15 1.69 11 -1 0 10.86 1.76 11 -1 0 12.50 0.89 -11 1 0 12.87 1.79 10 -1 0 8.08 0.74 10 -1 0 10.95 1.53 10 -1 0 3.91 1.34 -10 1 0 9.03 1.53 -10 1 0 5.80 1.32 9 -1 0 20.52 1.71 9 -1 0 15.77 1.02 -9 1 0 14.45 1.58 -9 1 0 14.19 1.46 8 -1 0 16.04 1.05 8 -1 0 16.18 1.00 8 -1 0 16.02 1.48 8 -1 0 17.84 1.39 -8 1 0 18.19 1.44 -8 1 0 18.56 1.58 7 -1 0 17.90 1.51 7 -1 0 15.63 0.90 7 -1 0 16.51 1.14 7 -1 0 13.87 0.91 -7 1 0 13.85 1.28 -7 1 0 16.63 1.43 -7 1 0 16.62 1.36 6 -1 0 26.25 1.14 6 -1 0 27.80 1.14 6 -1 0 30.81 1.64 6 -1 0 28.08 1.43 -6 1 0 31.36 1.62 -6 1 0 31.02 1.71 -6 1 0 25.51 1.69 5 -1 0 20.80 0.95 5 -1 0 20.48 1.40 5 -1 0 22.69 1.19 5 -1 0 21.73 0.94 -5 1 0 21.60 1.46 -5 1 0 21.79 1.43 -5 1 0 24.34 1.35 4 -1 0 44.45 1.51 4 -1 0 45.86 1.51 4 -1 0 46.85 1.84 4 -1 0 47.14 1.67 -4 1 0 42.97 1.93 -4 1 0 47.30 1.87 -4 1 0 46.77 1.88 3 -1 0 0.53 0.56 3 -1 0 1.15 0.35 3 -1 0 1.22 0.35 3 -1 0 0.95 0.44 -3 1 0 1.69 0.63 -3 1 0 0.04 0.58 -3 1 0 1.20 0.66 2 -1 0 8.44 0.62 2 -1 0 9.28 0.63 2 -1 0 7.43 0.62 -2 1 0 8.57 0.69 -2 1 0 6.55 0.68 1 -1 0 127.55 3.63 1 -1 0 122.92 3.63 1 -1 0 121.33 3.57 -1 1 0 126.39 3.62 -1 1 0 128.48 3.57 -1 1 0 128.70 3.70 -1 1 0 125.32 3.68 0 -1 0 101.68 2.70 0 -1 0 83.74 2.68 0 -1 0 88.94 2.65 0 -1 0 96.53 2.66 0 -1 0 88.95 2.70 0 1 0 100.96 2.69 0 1 0 96.51 2.66 0 1 0 93.73 2.65 0 1 0 85.22 2.69 -1 -1 0 94.34 2.88 -1 -1 0 95.42 2.97 -1 -1 0 99.22 2.96 -1 -1 0 107.97 2.88 1 1 0 112.48 2.88 1 1 0 104.91 2.89 1 1 0 96.42 2.92 1 1 0 95.10 2.89 -2 -1 0 1.20 0.49 -2 -1 0 2.15 0.55 -2 -1 0 0.87 0.46 -2 -1 0 1.80 0.42 2 1 0 1.18 0.19 2 1 0 1.35 0.18 2 1 0 0.27 0.43 -3 -1 0 1.37 0.51 -3 -1 0 0.93 0.53 -3 -1 0 1.57 0.56 -3 -1 0 0.99 0.56 -4 -1 0 2.89 0.66 -4 -1 0 2.59 0.63 -4 -1 0 2.95 0.59 -4 -1 0 3.17 0.66 4 1 0 1.79 0.60 -5 -1 0 178.41 5.37 -5 -1 0 177.50 5.39 -5 -1 0 179.78 5.42 -5 -1 0 170.02 5.40 5 1 0 177.96 5.40 -6 -1 0 81.70 2.84 -6 -1 0 80.69 2.88 -6 -1 0 83.67 2.88 -6 -1 0 77.95 2.89 6 1 0 82.61 2.88 6 1 0 76.44 2.90 -7 -1 0 34.41 1.85 -7 -1 0 31.32 1.72 -7 -1 0 32.43 1.71 -7 -1 0 31.45 1.89 7 1 0 32.25 1.82 7 1 0 32.63 1.76 -8 -1 0 76.40 2.96 -8 -1 0 76.07 3.11 -8 -1 0 72.49 3.02 -8 -1 0 78.58 2.96 8 1 0 76.77 3.06 8 1 0 72.97 2.29 8 1 0 77.00 2.96 -9 -1 0 8.99 1.32 -9 -1 0 9.82 1.29 -9 -1 0 9.76 1.19 9 1 0 9.38 1.34 9 1 0 7.80 1.16 9 1 0 10.17 1.17 -10 -1 0 3.63 1.25 -10 -1 0 4.87 1.25 10 1 0 8.82 1.47 10 1 0 4.78 1.22 10 1 0 6.76 1.19 -11 -1 0 5.12 1.37 -11 -1 0 4.27 1.38 11 1 0 4.37 1.46 11 1 0 4.80 1.37 -12 -1 0 14.22 1.86 -12 -1 0 13.62 1.82 11 -2 0 8.55 1.68 11 -2 0 6.48 0.85 11 -2 0 8.58 1.74 -11 2 0 5.37 1.63 10 -2 0 8.76 1.55 10 -2 0 8.58 1.60 10 -2 0 7.48 0.83 -10 2 0 8.00 1.57 -10 2 0 6.70 1.37 9 -2 0 17.71 1.18 9 -2 0 18.57 1.68 -9 2 0 16.40 1.56 -9 2 0 13.71 1.64 8 -2 0 30.55 1.46 8 -2 0 34.93 2.14 -8 2 0 34.89 2.18 -8 2 0 33.56 2.10 7 -2 0 42.33 2.19 7 -2 0 43.67 1.82 7 -2 0 41.88 1.64 7 -2 0 38.60 1.64 -7 2 0 41.86 2.23 -7 2 0 45.51 2.21 6 -2 0 35.44 1.53 6 -2 0 32.53 1.41 6 -2 0 39.11 1.95 6 -2 0 35.09 1.44 -6 2 0 39.44 1.86 -6 2 0 32.75 1.92 5 -2 0 61.85 2.42 5 -2 0 60.46 2.08 5 -2 0 62.38 2.08 5 -2 0 64.34 2.13 -5 2 0 63.61 2.42 -5 2 0 61.87 2.48 4 -2 0 16.67 1.21 4 -2 0 14.28 0.87 4 -2 0 14.61 0.87 4 -2 0 15.42 0.88 -4 2 0 15.57 1.20 -4 2 0 11.67 1.01 3 -2 0 30.72 1.18 3 -2 0 27.02 1.08 3 -2 0 28.00 1.41 3 -2 0 29.06 1.20 -3 2 0 28.94 1.48 -3 2 0 28.71 1.46 2 -2 0 3.28 0.48 2 -2 0 4.74 0.53 2 -2 0 4.08 0.36 2 -2 0 5.50 0.72 -2 2 0 3.03 0.63 -2 2 0 4.50 0.50 -2 2 0 3.62 0.65 1 -2 0 21.35 1.04 1 -2 0 24.38 0.80 1 -2 0 24.93 1.16 1 -2 0 20.39 1.07 -1 2 0 21.13 0.83 -1 2 0 21.10 1.16 -1 2 0 23.53 1.02 -1 2 0 21.38 1.07 0 -2 0 1.42 0.36 0 -2 0 1.02 0.45 0 -2 0 0.80 0.48 0 2 0 1.76 0.54 0 2 0 1.41 0.32 0 2 0 1.08 0.41 -1 -2 0 162.34 5.34 -1 -2 0 195.16 5.41 -1 -2 0 181.83 5.41 1 2 0 184.58 5.39 1 2 0 185.74 5.36 1 2 0 208.91 5.37 -2 -2 0 19.66 1.13 -2 -2 0 18.75 1.07 -2 -2 0 20.08 0.80 2 2 0 20.32 0.99 2 2 0 19.16 0.85 2 2 0 20.08 0.85 -3 -2 0 7.74 0.78 -3 -2 0 5.87 0.54 -3 -2 0 6.41 0.72 -3 -2 0 6.68 0.65 3 2 0 6.19 0.42 3 2 0 6.07 0.60 3 2 0 6.31 0.41 -4 -2 0 24.79 1.24 -4 -2 0 24.51 1.16 -4 -2 0 22.90 1.31 -4 -2 0 23.66 1.35 4 2 0 23.97 1.17 4 2 0 23.62 0.83 4 2 0 23.08 0.85 -5 -2 0 28.98 1.52 -5 -2 0 28.26 1.53 -5 -2 0 26.96 1.36 -5 -2 0 27.26 1.36 5 2 0 26.32 0.91 5 2 0 25.78 0.90 5 2 0 27.48 1.30 5 2 0 24.61 1.45 -6 -2 0 31.22 1.66 -6 -2 0 30.21 1.70 -6 -2 0 30.94 1.59 -6 -2 0 31.27 1.56 6 2 0 30.94 1.66 6 2 0 33.22 1.52 -7 -2 0 17.02 1.46 -7 -2 0 20.20 1.49 -7 -2 0 18.67 1.45 -7 -2 0 16.09 1.35 7 2 0 20.93 1.34 7 2 0 19.01 1.54 -8 -2 0 8.49 1.16 -8 -2 0 8.85 1.09 -8 -2 0 9.30 1.07 -8 -2 0 8.56 1.16 8 2 0 6.95 0.97 8 2 0 8.30 1.13 8 2 0 6.98 1.14 -9 -2 0 1.78 0.99 -9 -2 0 0.14 1.01 -9 -2 0 1.12 0.91 -9 -2 0 1.21 0.99 9 2 0 1.17 1.10 9 2 0 0.73 0.85 9 2 0 1.64 1.00 -10 -2 0 12.92 1.44 -10 -2 0 13.85 1.47 -10 -2 0 14.18 1.56 10 2 0 13.82 1.46 10 2 0 14.05 1.66 10 2 0 8.78 1.33 -11 -2 0 8.86 1.47 -11 -2 0 5.36 1.41 11 2 0 6.80 1.38 11 2 0 7.43 1.35 11 2 0 11.66 1.72 -12 -2 0 8.56 1.60 -12 -2 0 6.03 1.57 12 2 0 9.42 1.71 11 -3 0 0.29 1.44 11 -3 0 0.49 0.78 11 -3 0 2.45 1.53 -11 3 0 0.81 1.46 10 -3 0 13.55 1.73 10 -3 0 15.50 1.92 10 -3 0 16.53 1.18 -10 3 0 15.89 1.70 -10 3 0 14.16 1.92 9 -3 0 3.34 1.29 9 -3 0 3.50 0.75 -9 3 0 3.71 1.34 -9 3 0 4.64 1.23 8 -3 0 8.75 1.36 8 -3 0 7.52 0.84 -8 3 0 5.66 1.29 -8 3 0 9.66 1.31 7 -3 0 3.02 1.05 7 -3 0 4.37 0.70 -7 3 0 2.34 1.00 -7 3 0 3.30 1.02 6 -3 0 27.26 1.49 6 -3 0 25.61 1.34 6 -3 0 27.58 1.73 6 -3 0 24.50 1.24 -6 3 0 27.17 1.79 -6 3 0 27.49 1.80 5 -3 0 82.59 2.67 5 -3 0 78.20 2.96 5 -3 0 80.37 2.67 5 -3 0 79.56 2.55 -5 3 0 85.86 3.01 -5 3 0 77.78 3.00 4 -3 0 42.18 1.47 4 -3 0 40.73 1.92 4 -3 0 43.74 1.64 4 -3 0 42.59 1.65 -4 3 0 45.99 1.94 -4 3 0 42.59 1.93 3 -3 0 67.88 2.28 3 -3 0 68.86 2.08 3 -3 0 68.73 2.47 3 -3 0 65.79 2.29 -3 3 0 69.77 2.51 -3 3 0 69.03 2.46 2 -3 0 3.49 0.71 2 -3 0 3.00 0.35 2 -3 0 3.17 0.53 2 -3 0 4.43 0.60 -2 3 0 3.06 0.77 -2 3 0 2.91 0.63 1 -3 0 52.64 1.66 1 -3 0 52.44 1.90 1 -3 0 56.63 1.97 -1 3 0 54.14 1.90 -1 3 0 51.82 1.94 -1 3 0 51.26 1.82 0 -3 0 245.00 7.08 0 -3 0 256.68 7.05 0 -3 0 230.91 7.18 0 -3 0 260.97 7.17 0 3 0 248.74 7.05 0 3 0 239.54 7.20 0 3 0 247.06 7.16 -1 -3 0 982.16 26.53 -1 -3 0 1000.00 26.55 -1 -3 0 872.15 26.42 -1 -3 0 947.90 26.39 -1 -3 0 912.79 26.57 1 3 0 990.71 26.54 1 3 0 960.06 26.53 1 3 0 876.70 26.55 -2 -3 0 92.18 2.86 -2 -3 0 98.03 2.68 -2 -3 0 89.19 2.97 -2 -3 0 87.69 2.99 2 3 0 93.70 2.95 2 3 0 96.88 2.87 2 3 0 95.07 2.68 2 3 0 91.78 2.87 -3 -3 0 64.07 2.35 -3 -3 0 68.45 2.06 -3 -3 0 66.91 2.37 3 3 0 69.04 2.25 3 3 0 66.71 2.13 3 3 0 65.00 2.12 -4 -3 0 31.41 1.58 -4 -3 0 30.40 1.58 -4 -3 0 31.59 1.25 4 3 0 31.70 1.15 4 3 0 29.89 1.35 4 3 0 31.57 1.18 -5 -3 0 10.56 1.01 -5 -3 0 12.07 0.97 -5 -3 0 14.36 1.21 5 3 0 12.25 0.70 5 3 0 12.20 0.69 5 3 0 11.86 0.98 -6 -3 0 63.37 2.31 -6 -3 0 65.81 2.58 -6 -3 0 65.89 2.38 -6 -3 0 60.59 2.46 6 3 0 57.24 2.51 6 3 0 63.34 1.97 6 3 0 64.60 2.35 6 3 0 64.24 1.99 -7 -3 0 25.35 1.70 -7 -3 0 23.26 1.62 -7 -3 0 27.28 1.57 -7 -3 0 23.35 1.49 7 3 0 23.66 0.96 7 3 0 23.33 1.42 7 3 0 21.99 1.66 7 3 0 23.75 0.95 -8 -3 0 1.98 0.94 -8 -3 0 3.18 1.03 -8 -3 0 2.01 0.82 -8 -3 0 3.62 0.92 8 3 0 2.06 0.79 8 3 0 2.61 0.38 8 3 0 2.53 0.38 8 3 0 2.34 0.96 -9 -3 0 2.65 0.98 -9 -3 0 3.41 0.99 -9 -3 0 2.50 1.07 -9 -3 0 2.86 1.10 9 3 0 3.41 0.95 9 3 0 1.98 1.08 -10 -3 0 14.60 1.56 -10 -3 0 11.74 1.53 -10 -3 0 14.26 1.46 10 3 0 12.50 1.37 10 3 0 13.40 1.64 10 3 0 14.78 1.55 -11 -3 0 7.34 1.44 -11 -3 0 4.08 1.41 11 3 0 5.50 1.51 11 3 0 8.32 1.44 -12 -3 0 8.26 1.67 10 -4 0 5.67 1.62 10 -4 0 5.83 0.96 10 -4 0 5.50 1.65 -10 4 0 8.27 1.71 -10 4 0 5.63 1.47 9 -4 0 9.07 1.59 9 -4 0 7.49 0.97 9 -4 0 7.50 1.57 -9 4 0 5.90 1.47 -9 4 0 7.92 1.47 8 -4 0 14.98 1.11 8 -4 0 14.28 1.60 -8 4 0 10.77 1.52 -8 4 0 14.57 1.54 7 -4 0 17.82 1.36 7 -4 0 19.21 1.61 -7 4 0 22.83 1.90 -7 4 0 17.57 1.55 6 -4 0 7.12 0.82 6 -4 0 5.97 1.11 -6 4 0 8.80 1.15 -6 4 0 6.10 1.09 5 -4 0 98.43 2.93 5 -4 0 95.62 3.19 5 -4 0 95.85 3.46 -5 4 0 95.40 3.48 -5 4 0 93.13 3.46 4 -4 0 42.57 1.37 4 -4 0 42.07 1.94 4 -4 0 38.51 1.69 4 -4 0 41.41 1.70 -4 4 0 39.94 1.98 -4 4 0 38.74 1.92 3 -4 0 0.74 0.61 3 -4 0 0.89 0.55 3 -4 0 0.27 0.72 3 -4 0 0.62 0.32 -3 4 0 -0.04 0.78 -3 4 0 1.37 0.71 -3 4 0 1.62 0.59 2 -4 0 33.45 1.49 2 -4 0 30.66 1.10 2 -4 0 31.54 1.57 -2 4 0 29.84 1.64 -2 4 0 30.83 1.42 -2 4 0 31.93 1.50 1 -4 0 29.72 1.48 1 -4 0 29.65 1.15 1 -4 0 29.56 1.46 -1 4 0 30.27 1.39 -1 4 0 29.03 1.53 -1 4 0 27.59 1.28 0 -4 0 208.57 6.09 0 -4 0 199.17 6.23 0 -4 0 217.25 6.05 0 -4 0 225.44 6.22 0 4 0 202.63 6.18 0 4 0 193.27 6.23 0 4 0 217.33 6.06 -1 -4 0 14.20 1.15 -1 -4 0 13.51 0.66 -1 -4 0 13.51 0.99 -1 -4 0 13.30 0.84 1 4 0 15.04 1.09 1 4 0 13.90 1.11 -2 -4 0 127.48 3.87 -2 -4 0 126.43 3.99 -2 -4 0 127.80 3.98 2 4 0 129.47 3.89 2 4 0 125.42 3.94 2 4 0 126.84 3.87 -3 -4 0 6.75 0.82 -3 -4 0 6.01 0.46 -3 -4 0 6.41 0.81 3 4 0 7.34 0.65 3 4 0 7.49 0.75 3 4 0 7.02 0.61 -4 -4 0 4.89 0.85 -4 -4 0 4.68 0.80 -4 -4 0 6.02 0.49 4 4 0 4.63 0.57 4 4 0 5.29 0.53 4 4 0 5.35 0.70 -5 -4 0 55.00 2.25 -5 -4 0 54.98 2.29 -5 -4 0 53.37 1.88 5 4 0 55.41 1.83 5 4 0 51.62 1.84 5 4 0 53.36 2.06 -6 -4 0 34.66 1.85 -6 -4 0 34.10 1.49 -6 -4 0 33.45 1.84 6 4 0 33.70 1.32 6 4 0 35.16 1.31 6 4 0 33.70 1.59 6 4 0 31.27 1.86 -7 -4 0 55.05 2.48 -7 -4 0 53.04 2.49 -7 -4 0 57.97 2.17 7 4 0 55.16 2.53 7 4 0 55.37 1.86 7 4 0 55.73 1.85 7 4 0 50.45 2.20 -8 -4 0 35.03 2.20 -8 -4 0 36.09 1.82 -8 -4 0 37.59 2.16 8 4 0 35.19 1.36 8 4 0 32.10 2.13 8 4 0 34.17 1.84 8 4 0 35.95 1.35 -9 -4 0 53.76 2.79 -9 -4 0 54.21 2.45 -9 -4 0 54.35 2.69 9 4 0 55.57 2.48 9 4 0 54.42 1.86 9 4 0 56.41 2.87 9 4 0 61.46 2.45 -10 -4 0 3.96 1.25 -10 -4 0 5.46 1.26 10 4 0 4.58 0.48 10 4 0 5.21 1.31 -11 -4 0 10.69 1.62 -11 -4 0 11.57 1.63 11 4 0 5.70 1.58 11 4 0 10.82 1.57 10 -5 0 2.55 1.61 10 -5 0 5.31 1.09 10 -5 0 7.22 1.76 -10 5 0 4.85 1.66 -10 5 0 5.68 1.56 9 -5 0 16.83 1.96 9 -5 0 13.20 1.28 9 -5 0 17.32 1.90 -9 5 0 13.74 1.69 -9 5 0 14.67 1.80 8 -5 0 12.46 1.63 8 -5 0 12.29 1.15 8 -5 0 10.47 1.54 -8 5 0 8.50 1.46 -8 5 0 10.31 1.55 7 -5 0 24.73 1.86 7 -5 0 21.14 1.57 -7 5 0 18.80 1.67 -7 5 0 20.72 1.76 6 -5 0 86.24 3.10 6 -5 0 86.31 3.51 -6 5 0 89.28 3.47 -6 5 0 87.75 3.47 5 -5 0 18.76 1.37 5 -5 0 19.48 1.48 -5 5 0 19.77 1.63 -5 5 0 16.26 1.44 4 -5 0 47.55 1.46 4 -5 0 42.13 1.89 4 -5 0 44.00 2.13 -4 5 0 45.36 2.07 -4 5 0 43.50 2.18 3 -5 0 9.58 1.06 3 -5 0 8.46 0.60 3 -5 0 7.03 0.82 -3 5 0 9.35 0.95 -3 5 0 10.79 1.17 2 -5 0 24.65 1.03 2 -5 0 25.29 1.56 2 -5 0 25.38 1.41 -2 5 0 24.44 1.39 -2 5 0 24.16 1.36 -2 5 0 25.48 1.58 1 -5 0 6.53 0.77 1 -5 0 6.60 0.59 1 -5 0 6.90 0.71 1 -5 0 6.94 0.92 -1 5 0 6.84 0.79 -1 5 0 8.12 0.91 -1 5 0 6.33 0.69 0 -5 0 125.09 3.87 0 -5 0 136.33 4.05 0 -5 0 127.32 4.08 0 -5 0 126.43 3.81 0 5 0 122.62 4.09 0 5 0 128.07 3.83 0 5 0 123.38 4.01 -1 -5 0 74.14 2.48 -1 -5 0 70.52 2.20 -1 -5 0 70.00 2.48 -1 -5 0 69.23 2.61 1 5 0 73.19 2.51 1 5 0 75.80 2.63 -2 -5 0 13.37 0.97 -2 -5 0 12.20 1.00 -2 -5 0 14.77 1.24 2 5 0 12.98 1.27 2 5 0 14.97 1.14 2 5 0 14.36 1.05 -3 -5 0 86.77 3.04 -3 -5 0 89.33 3.08 3 5 0 90.58 3.02 3 5 0 91.76 2.91 3 5 0 82.91 2.85 -4 -5 0 7.14 0.51 -4 -5 0 8.39 0.99 -4 -5 0 7.80 0.94 4 5 0 6.85 0.66 4 5 0 5.99 0.69 4 5 0 8.44 0.86 -5 -5 0 43.64 1.51 -5 -5 0 39.79 2.04 -5 -5 0 42.52 2.05 5 5 0 42.20 1.68 5 5 0 43.07 1.65 5 5 0 47.06 1.85 -6 -5 0 21.95 1.13 -6 -5 0 22.74 1.71 -6 -5 0 20.77 1.65 6 5 0 22.81 1.39 6 5 0 20.68 1.14 6 5 0 23.51 1.14 -7 -5 0 39.80 2.16 -7 -5 0 41.17 2.24 -7 -5 0 42.80 1.75 7 5 0 40.56 2.35 7 5 0 41.72 1.60 7 5 0 41.43 1.92 7 5 0 41.77 1.65 -8 -5 0 17.63 1.53 -8 -5 0 21.00 1.69 8 5 0 19.30 1.51 8 5 0 20.28 1.70 8 5 0 20.12 1.11 -9 -5 0 1.44 1.16 -9 -5 0 3.26 1.12 9 5 0 2.27 0.56 9 5 0 2.11 1.23 -10 -5 0 5.70 1.41 -10 -5 0 5.18 1.31 10 5 0 4.86 0.61 10 5 0 4.22 1.41 -11 -5 0 8.18 1.52 -11 -5 0 5.94 1.45 11 5 0 7.22 1.57 10 -6 0 5.71 1.21 -10 6 0 5.83 1.76 9 -6 0 21.13 2.20 9 -6 0 18.19 2.06 9 -6 0 16.94 1.49 -9 6 0 15.90 1.99 -9 6 0 18.61 1.93 8 -6 0 9.25 1.18 8 -6 0 15.52 1.79 8 -6 0 12.13 1.66 -8 6 0 8.69 1.57 -8 6 0 11.86 1.65 7 -6 0 11.44 1.19 7 -6 0 12.16 1.54 7 -6 0 12.35 1.59 -7 6 0 7.80 1.44 -7 6 0 14.38 1.62 6 -6 0 7.01 1.30 6 -6 0 3.94 1.13 6 -6 0 6.87 1.01 -6 6 0 5.15 1.24 -6 6 0 6.25 1.26 5 -6 0 3.11 0.88 5 -6 0 5.93 1.17 -5 6 0 6.21 1.22 -5 6 0 6.14 1.17 4 -6 0 31.65 1.75 4 -6 0 34.38 2.00 -4 6 0 31.10 1.94 -4 6 0 31.97 2.01 3 -6 0 13.43 0.76 3 -6 0 12.56 1.06 3 -6 0 10.96 1.17 -3 6 0 11.82 1.13 -3 6 0 13.21 1.28 2 -6 0 4.99 0.55 2 -6 0 4.57 0.93 2 -6 0 4.65 0.75 2 -6 0 4.57 0.81 -2 6 0 6.15 0.83 -2 6 0 3.21 0.86 -2 6 0 3.64 0.78 1 -6 0 18.93 1.44 1 -6 0 17.27 1.14 1 -6 0 18.22 1.04 1 -6 0 18.67 1.29 -1 6 0 16.46 1.35 -1 6 0 17.00 1.29 -1 6 0 18.64 1.22 0 -6 0 89.10 2.97 0 -6 0 82.67 2.75 0 -6 0 80.57 2.99 0 -6 0 83.41 2.67 0 6 0 81.38 2.68 0 6 0 81.44 3.02 0 6 0 85.77 2.94 -1 -6 0 170.75 5.23 -1 -6 0 163.04 4.92 -1 -6 0 173.25 5.18 -1 -6 0 165.68 5.34 1 6 0 176.72 5.27 1 6 0 169.07 5.33 -2 -6 0 289.02 8.50 -2 -6 0 289.03 8.58 -2 -6 0 289.30 8.46 2 6 0 287.74 8.48 2 6 0 280.91 8.56 -3 -6 0 18.65 1.42 -3 -6 0 20.29 1.26 -3 -6 0 20.43 1.41 3 6 0 18.68 1.35 3 6 0 19.70 1.31 3 6 0 19.65 1.23 -4 -6 0 0.93 0.79 -4 -6 0 1.75 0.83 4 6 0 1.98 0.79 4 6 0 1.93 0.62 4 6 0 1.79 0.58 -5 -6 0 0.92 0.93 -5 -6 0 0.30 0.85 5 6 0 0.64 0.78 5 6 0 0.69 0.57 -6 -6 0 33.28 2.02 -6 -6 0 33.65 1.91 6 6 0 32.74 1.77 6 6 0 32.62 1.52 -7 -6 0 20.57 1.55 -7 -6 0 16.87 1.52 7 6 0 19.60 1.27 7 6 0 17.63 1.57 7 6 0 21.96 1.53 -8 -6 0 31.53 2.29 -8 -6 0 37.27 2.22 8 6 0 32.55 1.56 8 6 0 35.20 2.34 8 6 0 34.29 1.88 -9 -6 0 3.91 1.24 -9 -6 0 4.49 1.35 9 6 0 3.29 0.68 9 6 0 3.81 1.34 -10 -6 0 0.64 1.27 -10 -6 0 0.55 1.21 10 6 0 2.32 0.64 10 6 0 1.37 1.38 -11 -6 0 7.80 1.55 -11 -6 0 6.06 1.60 11 6 0 8.00 0.75 11 6 0 10.03 1.76 9 -7 0 8.77 1.84 9 -7 0 10.80 1.90 9 -7 0 8.89 1.38 -9 7 0 10.33 1.73 -9 7 0 10.72 1.81 8 -7 0 17.34 1.96 8 -7 0 15.08 1.50 8 -7 0 18.82 2.03 -8 7 0 13.28 1.77 -8 7 0 18.21 1.92 7 -7 0 7.87 1.54 7 -7 0 10.32 1.29 7 -7 0 8.01 1.56 -7 7 0 5.16 1.44 -7 7 0 8.12 1.51 6 -7 0 5.48 1.08 6 -7 0 4.13 1.33 6 -7 0 5.02 1.24 -6 7 0 3.02 1.27 -6 7 0 3.35 1.31 5 -7 0 37.12 2.46 5 -7 0 37.94 2.13 5 -7 0 40.41 2.34 -5 7 0 39.67 2.35 -5 7 0 40.64 2.40 4 -7 0 40.73 2.30 4 -7 0 37.78 2.14 4 -7 0 38.78 2.10 -4 7 0 40.10 2.20 -4 7 0 39.24 2.33 3 -7 0 37.95 1.98 3 -7 0 37.71 2.15 3 -7 0 39.19 2.01 -3 7 0 36.47 2.23 -3 7 0 37.74 1.92 2 -7 0 6.74 0.95 2 -7 0 4.63 1.05 2 -7 0 6.98 0.90 2 -7 0 7.44 0.65 -2 7 0 7.14 0.96 -2 7 0 7.15 0.93 -2 7 0 5.72 1.05 1 -7 0 27.99 1.30 1 -7 0 26.00 1.82 1 -7 0 24.17 1.35 1 -7 0 26.03 1.72 -1 7 0 24.88 1.74 -1 7 0 24.08 1.44 -1 7 0 26.21 1.62 0 -7 0 0.56 0.53 0 -7 0 1.86 0.89 0 -7 0 1.24 0.63 0 -7 0 0.34 0.75 0 7 0 1.49 0.78 0 7 0 0.81 0.54 0 7 0 1.95 0.89 -1 -7 0 39.05 1.90 -1 -7 0 36.66 1.99 -1 -7 0 37.70 1.41 -1 -7 0 37.43 1.72 1 7 0 38.43 1.89 1 7 0 40.77 2.00 -2 -7 0 21.42 1.47 -2 -7 0 22.61 1.62 -2 -7 0 21.25 1.48 2 7 0 22.88 1.53 2 7 0 20.66 1.58 -3 -7 0 24.89 1.66 -3 -7 0 27.11 1.69 3 7 0 26.87 1.58 3 7 0 26.86 1.65 -4 -7 0 7.06 1.02 -4 -7 0 7.70 1.09 4 7 0 8.28 1.02 4 7 0 10.13 0.96 -5 -7 0 5.00 1.08 -5 -7 0 6.31 1.12 5 7 0 4.88 0.79 5 7 0 5.23 0.98 -6 -7 0 30.80 1.98 -6 -7 0 31.37 2.07 6 7 0 32.61 1.94 6 7 0 30.72 1.64 -7 -7 0 19.91 1.65 -7 -7 0 24.57 1.92 7 7 0 21.96 1.79 7 7 0 22.77 1.46 7 7 0 23.79 1.76 -8 -7 0 33.01 2.24 -8 -7 0 34.53 2.40 8 7 0 28.56 1.62 8 7 0 33.74 2.46 8 7 0 31.45 1.95 -9 -7 0 22.28 1.97 -9 -7 0 19.02 1.78 9 7 0 20.86 1.41 9 7 0 23.00 2.07 -10 -7 0 13.90 1.67 -10 -7 0 12.11 1.75 10 7 0 11.74 1.80 10 7 0 14.08 1.04 -11 -7 0 4.14 1.55 -11 -7 0 6.17 1.53 11 7 0 6.52 1.69 11 7 0 4.44 0.78 8 -8 0 8.96 1.80 8 -8 0 6.31 1.34 8 -8 0 5.16 1.68 -8 8 0 7.45 1.68 -8 8 0 7.51 1.66 7 -8 0 9.53 1.69 7 -8 0 8.41 1.66 7 -8 0 10.50 1.38 -7 8 0 10.92 1.63 -7 8 0 12.33 1.79 6 -8 0 21.37 1.85 6 -8 0 19.90 1.98 6 -8 0 18.35 1.61 -6 8 0 17.32 1.71 -6 8 0 20.94 1.97 5 -8 0 62.71 2.99 5 -8 0 57.91 2.81 5 -8 0 63.20 3.16 -5 8 0 60.80 2.87 -5 8 0 60.70 3.08 4 -8 0 10.66 1.23 4 -8 0 10.06 1.28 4 -8 0 10.54 1.42 -4 8 0 11.68 1.33 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0 10.45 1.62 -8 -8 0 10.49 1.46 8 8 0 9.84 1.57 8 8 0 9.64 1.02 -9 -8 0 7.95 1.64 -9 -8 0 7.44 1.40 9 8 0 8.93 1.03 9 8 0 4.79 1.61 -10 -8 0 0.72 1.34 -10 -8 0 2.87 1.34 10 8 0 1.57 1.41 10 8 0 1.10 0.81 -8 9 0 12.14 2.04 7 -9 0 7.59 1.75 7 -9 0 11.55 1.69 7 -9 0 7.21 1.38 -7 9 0 8.41 1.74 -7 9 0 8.07 1.68 6 -9 0 7.23 1.60 6 -9 0 7.94 1.37 6 -9 0 8.76 1.55 -6 9 0 7.38 1.50 -6 9 0 10.72 1.71 5 -9 0 3.98 1.28 5 -9 0 6.64 1.30 5 -9 0 6.13 1.41 -5 9 0 6.21 1.33 -5 9 0 6.88 1.57 4 -9 0 34.86 2.63 4 -9 0 39.34 2.37 4 -9 0 36.43 2.26 -4 9 0 39.11 2.31 -4 9 0 37.57 2.61 3 -9 0 12.71 1.51 3 -9 0 17.86 1.42 3 -9 0 12.50 1.33 -3 9 0 16.82 1.39 -3 9 0 17.39 1.77 2 -9 0 19.48 1.52 2 -9 0 22.68 1.63 2 -9 0 14.11 1.57 -2 9 0 18.20 1.72 -2 9 0 17.00 1.34 1 -9 0 2.54 1.01 1 -9 0 4.01 1.12 1 -9 0 2.95 0.77 -1 9 0 3.95 1.16 -1 9 0 2.40 0.79 0 -9 0 4.57 1.12 0 -9 0 4.22 0.82 0 9 0 3.23 1.22 0 9 0 5.24 1.01 -1 -9 0 14.84 1.20 -1 -9 0 16.67 1.54 1 9 0 17.13 1.57 1 9 0 14.06 1.32 -2 -9 0 62.46 2.60 -2 -9 0 64.92 2.96 2 9 0 61.40 2.71 2 9 0 66.44 2.95 -3 -9 0 184.44 6.12 -3 -9 0 182.86 5.93 3 9 0 187.48 6.08 3 9 0 182.64 5.91 -4 -9 0 24.44 1.81 -4 -9 0 23.90 1.93 4 9 0 22.31 1.82 4 9 0 22.93 1.73 -5 -9 0 12.83 1.47 -5 -9 0 12.56 1.45 5 9 0 15.45 1.28 5 9 0 14.94 1.46 -6 -9 0 3.89 1.23 -6 -9 0 2.71 1.17 6 9 0 2.08 0.91 6 9 0 2.98 1.12 -7 -9 0 12.71 1.55 -7 -9 0 10.44 1.51 7 9 0 12.34 1.40 7 9 0 9.31 1.51 7 9 0 7.52 1.09 -8 -9 0 18.51 1.81 -8 -9 0 22.01 2.03 8 9 0 17.78 1.39 8 9 0 20.52 1.95 -9 -9 0 15.57 1.96 -9 -9 0 16.51 1.75 9 9 0 14.53 1.94 9 9 0 12.06 1.23 -10 -9 0 3.75 1.44 -10 -9 0 2.55 1.52 10 9 0 4.42 0.98 10 9 0 2.85 1.58 7 -10 0 5.42 1.70 7 -10 0 8.18 1.54 -7 10 0 6.46 1.60 -7 10 0 6.10 1.77 6 -10 0 12.10 1.72 6 -10 0 7.11 1.47 6 -10 0 8.08 1.78 -6 10 0 7.41 1.75 -6 10 0 8.00 1.56 5 -10 0 5.13 1.57 5 -10 0 6.09 1.36 5 -10 0 7.04 1.40 -5 10 0 9.02 1.74 -5 10 0 6.78 1.44 4 -10 0 28.16 2.17 4 -10 0 30.62 2.37 4 -10 0 31.11 2.56 -4 10 0 29.68 2.14 -4 10 0 24.06 2.18 3 -10 0 15.47 1.76 3 -10 0 19.22 1.53 3 -10 0 22.83 1.80 -3 10 0 21.68 1.85 -3 10 0 20.75 2.02 2 -10 0 14.66 1.48 2 -10 0 15.26 1.35 2 -10 0 13.51 1.59 -2 10 0 13.01 1.69 -2 10 0 14.36 1.29 1 -10 0 5.24 1.36 -1 10 0 6.68 1.36 0 -10 0 3.36 1.24 0 -10 0 4.24 1.08 0 10 0 2.06 1.28 -1 -10 0 11.46 1.45 -1 -10 0 14.62 1.21 1 10 0 9.68 1.27 1 10 0 15.07 1.64 -2 -10 0 15.51 1.34 -2 -10 0 13.95 1.54 2 10 0 16.35 1.62 2 10 0 13.33 1.33 -3 -10 0 12.27 1.31 -3 -10 0 13.36 1.50 3 10 0 12.56 1.47 3 10 0 10.07 1.20 -4 -10 0 12.09 1.40 -4 -10 0 10.18 1.46 4 10 0 9.02 1.24 4 10 0 12.17 1.50 -5 -10 0 2.48 1.18 -5 -10 0 3.00 1.23 5 10 0 3.20 1.01 5 10 0 3.75 1.21 -6 -10 0 0.35 1.17 -6 -10 0 0.59 1.23 6 10 0 -0.07 0.94 6 10 0 1.27 1.11 -7 -10 0 10.68 1.59 -7 -10 0 8.17 1.51 7 10 0 7.74 1.16 7 10 0 8.12 1.52 7 10 0 9.38 1.45 -8 -10 0 26.71 2.29 -8 -10 0 25.27 2.09 8 10 0 28.57 2.33 8 10 0 28.99 1.99 -9 -10 0 23.88 2.12 -9 -10 0 22.92 2.23 9 10 0 23.28 2.24 9 10 0 20.03 1.58 -6 11 0 7.18 1.69 5 -11 0 18.57 1.85 5 -11 0 19.47 2.08 5 -11 0 22.56 2.00 -5 11 0 16.91 1.80 -5 11 0 20.06 2.23 4 -11 0 27.45 2.33 4 -11 0 31.95 2.26 -4 11 0 29.55 2.52 3 -11 0 20.13 2.05 -3 11 0 20.78 2.14 2 -11 0 16.03 1.82 -2 11 0 16.09 1.99 1 -11 0 12.05 1.65 -1 11 0 12.55 1.76 0 -11 0 4.60 1.37 0 11 0 5.06 1.52 -1 -11 0 24.82 2.01 -1 -11 0 28.10 2.03 1 11 0 31.38 2.45 -2 -11 0 22.42 1.83 -2 -11 0 25.11 1.97 2 11 0 23.59 1.95 2 11 0 24.98 1.88 -3 -11 0 13.18 1.43 -3 -11 0 13.46 1.61 3 11 0 13.61 1.52 3 11 0 12.92 1.62 -4 -11 0 26.56 2.06 -4 -11 0 27.91 2.21 4 11 0 24.63 1.88 4 11 0 26.22 2.03 -5 -11 0 16.36 1.80 -5 -11 0 17.29 1.76 5 11 0 16.32 1.54 5 11 0 13.60 1.69 -6 -11 0 7.67 1.54 -6 -11 0 5.15 1.45 6 11 0 5.61 1.40 6 11 0 7.00 1.51 6 11 0 7.04 1.23 -7 -11 0 10.21 1.73 -7 -11 0 11.74 1.71 7 11 0 9.45 1.71 7 11 0 11.38 1.38 -8 -11 0 19.87 2.12 -8 -11 0 17.18 1.93 8 11 0 16.86 1.56 8 11 0 17.81 1.95 4 -12 0 3.29 1.65 -4 12 0 3.17 1.69 3 -12 0 12.25 1.86 -3 12 0 18.61 2.19 2 -12 0 16.91 1.94 -2 12 0 14.47 2.02 1 -12 0 14.93 1.90 -1 12 0 16.63 1.96 0 -12 0 11.90 1.71 0 12 0 15.14 1.91 -1 -12 0 5.92 1.51 1 12 0 4.87 1.54 -2 -12 0 34.28 2.71 2 12 0 39.49 2.95 -3 -12 0 43.28 2.57 -3 -12 0 44.83 2.95 3 12 0 47.12 2.74 3 12 0 44.26 2.93 -4 -12 0 44.67 3.00 -4 -12 0 41.99 2.66 4 12 0 45.79 2.92 4 12 0 42.60 2.65 -5 -12 0 3.37 1.35 -5 -12 0 3.97 1.50 5 12 0 2.09 1.37 5 12 0 3.25 1.24 -6 -12 0 10.05 1.78 -6 -12 0 12.20 1.72 6 12 0 7.34 1.57 6 12 0 8.96 1.69 6 12 0 10.08 1.43 -7 -12 0 5.54 1.61 -7 -12 0 7.58 1.68 7 12 0 8.53 1.75 7 12 0 5.62 1.29 2 -13 0 22.57 2.20 -2 13 0 25.22 2.51 1 -13 0 8.53 1.77 -1 13 0 4.33 1.84 0 -13 0 0.75 1.48 0 13 0 2.73 1.61 -1 -13 0 3.18 1.51 1 13 0 2.61 1.64 -2 -13 0 6.07 1.57 2 13 0 3.01 1.59 -3 -13 0 23.42 2.18 3 13 0 22.27 2.25 -4 -13 0 10.52 1.58 -4 -13 0 13.63 1.94 4 13 0 11.35 1.84 4 13 0 11.73 1.62 4 13 0 10.75 1.66 -5 -13 0 6.29 1.53 -5 -13 0 12.10 1.85 5 13 0 9.25 1.72 5 13 0 7.24 1.62 5 13 0 9.86 1.58 -6 -13 0 2.49 1.46 -6 -13 0 4.51 1.73 6 13 0 1.75 1.26 -1 -14 0 1.83 1.63 -2 -14 0 5.26 1.71 5 13 -1 4.89 1.66 5 13 -1 2.61 1.31 -5 -13 1 6.27 1.60 -5 -13 1 4.58 1.65 4 13 -1 8.73 1.77 4 13 -1 6.89 1.45 -4 -13 1 8.96 1.57 -4 -13 1 10.70 1.80 3 13 -1 8.18 1.76 -3 -13 1 10.53 1.74 -3 -13 1 10.33 1.60 2 13 -1 15.93 2.05 -2 -13 1 11.60 1.79 1 13 -1 7.67 1.79 -1 -13 1 8.70 1.63 0 13 -1 7.05 1.78 0 -13 1 4.74 1.58 -1 13 -1 6.10 1.81 1 -13 1 4.30 1.64 -2 13 -1 14.16 2.14 2 -13 1 7.41 1.81 7 12 -1 5.18 1.26 7 12 -1 3.65 1.58 -7 -12 1 4.81 1.59 -7 -12 1 8.00 1.67 6 12 -1 6.75 1.56 6 12 -1 8.91 1.39 -6 -12 1 5.39 1.60 -6 -12 1 7.19 1.68 5 12 -1 4.99 1.27 5 12 -1 4.45 1.53 -5 -12 1 4.00 1.53 -5 -12 1 1.56 1.35 4 12 -1 48.98 2.77 4 12 -1 51.38 3.11 -4 -12 1 52.03 3.15 -4 -12 1 48.72 2.81 3 12 -1 68.62 3.29 3 12 -1 75.47 3.68 -3 -12 1 77.51 3.60 -3 -12 1 65.03 3.18 2 12 -1 27.03 2.20 -2 -12 1 30.86 2.30 -2 -12 1 26.19 2.11 1 12 -1 12.31 1.84 -1 -12 1 6.65 1.57 0 12 -1 3.85 1.52 0 -12 1 3.36 1.44 -1 12 -1 14.70 2.02 1 -12 1 10.42 1.69 -2 12 -1 18.58 2.19 2 -12 1 20.55 2.08 -3 12 -1 33.81 2.71 3 -12 1 26.65 2.39 -4 12 -1 3.98 1.75 4 -12 1 5.67 1.70 8 11 -1 6.51 1.20 8 11 -1 1.14 1.48 -8 -11 1 7.90 1.61 -8 -11 1 2.08 1.54 7 11 -1 2.56 1.11 7 11 -1 2.89 1.41 -7 -11 1 2.77 1.46 -7 -11 1 3.81 1.42 6 11 -1 4.80 1.14 6 11 -1 5.46 1.47 -6 -11 1 4.87 1.45 -6 -11 1 5.40 1.45 5 11 -1 10.36 1.58 5 11 -1 10.19 1.33 -5 -11 1 7.36 1.45 -5 -11 1 8.47 1.56 4 11 -1 20.42 1.66 4 11 -1 16.66 1.83 -4 -11 1 17.30 1.81 -4 -11 1 17.76 1.67 3 11 -1 16.21 1.57 3 11 -1 16.49 1.77 -3 -11 1 15.16 1.69 -3 -11 1 14.12 1.49 2 11 -1 26.53 2.13 2 11 -1 28.23 2.16 -2 -11 1 26.84 1.98 -2 -11 1 28.08 2.29 1 11 -1 7.03 1.56 -1 -11 1 5.98 1.46 -1 -11 1 6.55 1.11 0 11 -1 1.20 1.37 0 -11 1 -0.71 1.22 -1 11 -1 7.24 1.61 1 -11 1 6.04 1.49 -2 11 -1 28.08 2.30 2 -11 1 23.81 2.05 -3 11 -1 11.85 1.87 3 -11 1 18.35 2.01 -4 11 -1 24.62 2.33 4 -11 1 24.97 2.22 -5 11 -1 15.56 1.75 -5 11 -1 16.10 2.13 5 -11 1 15.70 1.83 5 -11 1 17.24 1.84 5 -11 1 13.99 1.92 9 10 -1 6.11 1.65 9 10 -1 6.23 1.11 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-17 23.22 2.23 -1 -1 17 19.75 2.04 0 1 -17 12.19 2.41 0 1 -17 9.93 1.76 0 -1 17 14.55 1.91 -1 1 -17 3.95 1.50 1 -1 17 3.18 1.46 -2 1 -17 5.40 1.57 2 -1 17 4.15 1.58 -3 1 -17 4.37 1.58 3 -1 17 1.12 1.46 -4 1 -17 8.77 1.73 4 -1 17 6.79 1.65 -5 1 -17 6.57 1.73 5 -1 17 8.64 1.74 3 0 -17 1.86 1.37 3 0 -17 1.77 1.46 3 0 -17 2.35 1.70 -3 0 17 1.39 1.35 2 0 -17 13.68 2.01 2 0 -17 9.83 1.56 2 0 -17 13.89 1.76 -2 0 17 9.17 1.66 1 0 -17 11.18 1.83 1 0 -17 11.03 1.64 1 0 -17 13.80 1.72 -1 0 17 11.44 1.74 0 0 -17 16.70 2.03 0 0 17 17.88 1.96 -1 0 -17 9.16 1.73 1 0 17 10.34 1.69 -2 0 -17 1.05 1.43 2 0 17 1.19 1.44 -3 0 -17 8.26 1.63 3 0 17 7.15 1.60 -4 0 -17 19.08 2.05 4 0 17 16.22 1.99 -5 0 -17 7.78 1.74 5 0 17 8.84 1.74 3 -1 -17 2.97 1.64 3 -1 -17 1.02 1.42 3 -1 -17 1.74 1.30 -3 1 17 2.38 1.40 2 -1 -17 15.02 1.83 2 -1 -17 13.00 2.00 2 -1 -17 13.25 1.69 -2 1 17 14.10 1.75 1 -1 -17 15.13 1.76 1 -1 -17 18.57 2.11 1 -1 -17 17.63 1.81 -1 1 17 19.04 1.92 0 -1 -17 35.97 2.94 0 1 17 31.04 2.37 -1 -1 -17 13.37 1.91 1 1 17 13.28 1.78 -2 -1 -17 6.28 1.62 2 1 17 3.46 1.45 -3 -1 -17 11.75 1.79 3 1 17 4.77 1.54 -4 -1 -17 2.11 1.51 4 1 17 5.99 1.58 -5 -1 -17 10.25 1.78 5 1 17 8.11 1.74 -6 -1 -17 12.41 1.96 6 1 17 13.62 2.03 3 -2 -17 2.10 1.37 3 -2 -17 2.37 1.75 3 -2 -17 5.99 1.56 -3 2 17 2.73 1.57 2 -2 -17 9.69 1.61 2 -2 -17 12.11 1.99 2 -2 -17 9.14 1.62 -2 2 17 11.86 1.64 -2 2 17 8.87 1.67 1 -2 -17 30.01 2.59 1 -2 -17 27.15 2.18 1 -2 -17 28.49 2.38 -1 2 17 26.91 2.16 0 -2 -17 14.94 2.05 0 2 17 15.01 1.81 -1 -2 -17 14.38 1.98 1 2 17 15.30 1.82 -2 -2 -17 3.00 1.55 2 2 17 3.45 1.45 -3 -2 -17 2.71 1.48 3 2 17 1.90 1.39 -4 -2 -17 4.19 1.62 4 2 17 7.96 1.68 -5 -2 -17 14.34 1.92 5 2 17 15.40 2.02 -6 -2 -17 12.90 1.95 6 2 17 12.78 1.94 3 -3 -17 1.46 1.30 3 -3 -17 2.16 1.79 -3 3 17 2.33 1.61 2 -3 -17 0.95 1.28 2 -3 -17 0.99 1.66 2 -3 -17 -0.42 1.26 -2 3 17 0.87 1.41 1 -3 -17 13.05 2.04 -1 3 17 13.73 1.66 0 -3 -17 12.61 1.97 0 3 17 16.54 1.82 -1 -3 -17 16.62 1.99 1 3 17 18.72 1.91 -2 -3 -17 6.22 1.68 2 3 17 4.84 1.48 -3 -3 -17 5.08 1.60 3 3 17 2.59 1.47 -4 -3 -17 11.39 1.84 4 3 17 12.70 1.84 -5 -3 -17 19.13 2.16 5 3 17 17.27 2.06 -6 -3 -17 5.08 1.68 6 3 17 3.65 1.66 2 -4 -17 1.96 1.38 2 -4 -17 3.86 1.47 2 -4 -17 1.67 1.76 -2 4 17 1.44 1.42 1 -4 -17 17.56 2.11 0 -4 -17 37.02 3.16 0 4 17 42.96 2.75 -1 -4 -17 21.58 2.23 1 4 17 21.27 2.00 -2 -4 -17 13.94 1.99 2 4 17 14.44 1.79 -3 -4 -17 4.24 1.59 3 4 17 4.13 1.58 -4 -4 -17 3.36 1.54 4 4 17 5.84 1.58 -5 -4 -17 3.74 1.59 5 4 17 4.16 1.64 -6 -4 -17 3.20 1.64 6 4 17 2.96 1.66 1 -5 -17 3.59 1.79 0 -5 -17 15.38 2.15 -1 -5 -17 21.05 2.32 1 5 17 20.41 1.95 -2 -5 -17 7.84 1.84 2 5 17 9.63 1.63 -3 -5 -17 5.15 1.70 -4 -5 -17 2.91 1.60 4 5 17 8.32 1.73 -5 -5 -17 13.16 1.94 5 5 17 8.05 1.78 0 -6 -17 16.41 2.29 -1 -6 -17 40.29 3.27 -2 -6 -17 13.27 2.04 2 6 17 11.79 1.75 -3 -6 -17 6.68 1.75 3 6 17 7.87 1.63 -4 -6 -17 7.25 1.68 4 6 17 5.82 1.66 -1 -7 -17 27.83 2.62 -2 -7 -17 28.55 2.52 -3 -7 -17 9.84 1.88 3 7 17 12.66 1.86 -1 2 -18 6.60 1.66 1 -2 18 4.15 1.63 1 1 -18 25.35 2.33 -1 -1 18 23.49 2.30 0 1 -18 27.91 2.41 0 -1 18 27.57 2.42 -1 1 -18 5.67 1.64 1 -1 18 7.17 1.66 -2 1 -18 1.08 1.52 2 -1 18 3.45 1.55 -3 1 -18 -0.12 1.43 3 -1 18 0.51 1.50 1 0 -18 29.12 2.44 -1 0 18 23.70 2.21 0 0 -18 28.08 2.40 0 0 18 27.65 2.30 -1 0 -18 6.20 1.61 1 0 18 3.68 1.55 -2 0 -18 3.34 1.59 2 0 18 1.49 1.50 -3 0 -18 10.96 1.78 3 0 18 5.12 1.63 -4 0 -18 13.28 1.97 4 0 18 16.33 2.12 1 -1 -18 23.58 2.30 -1 1 18 22.99 2.15 0 -1 -18 15.09 2.07 0 1 18 15.38 1.93 -1 -1 -18 11.41 1.93 1 1 18 11.10 1.79 -2 -1 -18 3.62 1.64 2 1 18 3.78 1.53 -3 -1 -18 2.85 1.53 3 1 18 4.20 1.60 -4 -1 -18 3.93 1.59 4 1 18 0.86 1.48 1 -2 -18 9.20 2.02 -1 2 18 8.61 1.63 0 -2 -18 22.60 2.30 0 2 18 24.32 2.19 -1 -2 -18 22.25 2.24 1 2 18 16.82 1.98 -2 -2 -18 5.39 1.73 2 2 18 5.75 1.57 -3 -2 -18 1.40 1.53 3 2 18 2.39 1.49 -4 -2 -18 2.92 1.61 4 2 18 3.25 1.50 1 -3 -18 11.34 2.01 -1 3 18 9.98 1.92 0 -3 -18 40.41 3.35 0 3 18 37.83 2.82 -1 -3 -18 18.66 2.23 1 3 18 18.09 1.97 -2 -3 -18 9.70 1.91 2 3 18 10.37 1.77 -3 -3 -18 4.34 1.68 3 3 18 5.06 1.58 -4 -3 -18 7.11 1.78 4 3 18 3.05 1.57 0 -4 -18 16.37 2.26 0 4 18 14.38 1.88 -1 -4 -18 13.30 2.03 1 4 18 11.70 1.78 -2 -4 -18 10.92 1.94 2 4 18 12.57 1.84 -3 -4 -18 3.84 1.61 3 4 18 7.10 1.67 -4 -4 -18 4.49 1.72 4 4 18 5.23 1.67 1 5 18 27.33 2.27 -2 -5 -18 5.93 1.90 2 5 18 9.19 1.68 0 0 0 0.00 0.00 ; _shelx_hkl_checksum 14181 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy Au1 Au 0.000000 0.500000 1.000000 0.01478(7) Uani 1 2 d S . P Cl1 Cl 0.19162(9) 0.44808(9) 0.89391(6) 0.02239(19) Uani 1 1 d . . . Cl2 Cl 0.14490(9) 0.46668(8) 1.11751(6) 0.02214(19) Uani 1 1 d . . . O1 O 0.1588(3) 0.7578(2) 0.56900(18) 0.0254(6) Uani 1 1 d . . . O2 O 0.0510(4) 0.1273(3) 0.6726(2) 0.0329(7) Uani 1 1 d . . . N1 N 0.1234(3) 0.6903(3) 0.7203(2) 0.0198(6) Uani 1 1 d . . . H1N H 0.121(4) 0.639(4) 0.760(3) 0.017(11) Uiso 1 1 d . . . N2 N -0.0081(4) 0.2527(3) 0.7846(2) 0.0241(7) Uani 1 1 d . . . H2N H -0.001(5) 0.310(5) 0.802(3) 0.027(13) Uiso 1 1 d . . . C1 C 0.1130(4) 0.8133(3) 0.7515(3) 0.0226(8) Uani 1 1 d . . . H1A H 0.029402 0.867677 0.727005 0.027 Uiso 1 1 calc R U . H1B H 0.200568 0.849246 0.726474 0.027 Uiso 1 1 calc R U . C2 C 0.1449(4) 0.6721(3) 0.6303(3) 0.0185(7) Uani 1 1 d . . . C3 C 0.1546(4) 0.5426(3) 0.6050(2) 0.0167(7) Uani 1 1 d . . . C4 C 0.0932(4) 0.4524(3) 0.6636(2) 0.0172(7) Uani 1 1 d . . . H4 H 0.041122 0.472243 0.721261 0.021 Uiso 1 1 calc R U . C5 C 0.1084(4) 0.3329(3) 0.6374(2) 0.0173(7) Uani 1 1 d . . . C6 C 0.1836(4) 0.3053(3) 0.5519(3) 0.0205(7) Uani 1 1 d . . . H6 H 0.192957 0.223634 0.534281 0.025 Uiso 1 1 calc R U . C7 C 0.2452(4) 0.3947(4) 0.4919(3) 0.0213(8) Uani 1 1 d . . . C8 C 0.2278(4) 0.5140(3) 0.5193(3) 0.0196(7) Uani 1 1 d . . . H8 H 0.266469 0.577088 0.478837 0.024 Uiso 1 1 calc R U . C9 C 0.0477(4) 0.2311(3) 0.6992(3) 0.0202(7) Uani 1 1 d . . . C10 C -0.0646(5) 0.1549(4) 0.8480(3) 0.0277(9) Uani 1 1 d . . . H10A H -0.001608 0.075232 0.838959 0.033 Uiso 1 1 calc R U . H10B H -0.161455 0.147247 0.832653 0.033 Uiso 1 1 calc R U . C11 C -0.0741(4) 0.1799(3) 0.9488(3) 0.0208(8) Uani 1 1 d . . . C12 C -0.2068(4) 0.2251(3) 0.9957(3) 0.0201(7) Uani 1 1 d . . . C13 C -0.3321(4) 0.2694(4) 0.9495(3) 0.0282(9) Uani 1 1 d . . . H13 H -0.326087 0.268693 0.884013 0.034 Uiso 1 1 calc R U . C14 C -0.4595(5) 0.3123(4) 0.9963(3) 0.0353(10) Uani 1 1 d . . . H14 H -0.541083 0.341451 0.963638 0.042 Uiso 1 1 calc R U . C15 C -0.4711(4) 0.3138(4) 1.0944(3) 0.0351(10) Uani 1 1 d . . . H15 H -0.560722 0.343888 1.126809 0.042 Uiso 1 1 calc R U . C16 C -0.3561(4) 0.2728(4) 1.1420(3) 0.0254(8) Uani 1 1 d . . . H16 H -0.366709 0.273329 1.207650 0.030 Uiso 1 1 calc R U . C17 C -0.2184(4) 0.2287(3) 1.0954(3) 0.0190(7) Uani 1 1 d . . . C18 C -0.0963(4) 0.1917(3) 1.1429(2) 0.0171(7) Uani 1 1 d . . . C19 C 0.0390(4) 0.1584(3) 1.0945(3) 0.0190(7) Uani 1 1 d . . . C20 C 0.1684(4) 0.1312(4) 1.1391(3) 0.0267(8) Uani 1 1 d . . . H20 H 0.164130 0.137166 1.203972 0.032 Uiso 1 1 calc R U . C21 C 0.2980(5) 0.0969(4) 1.0898(4) 0.0371(11) Uani 1 1 d . . . H21 H 0.382811 0.079572 1.120571 0.045 Uiso 1 1 calc R U . C22 C 0.3067(5) 0.0869(4) 0.9934(4) 0.0386(11) Uani 1 1 d . . . H22 H 0.397485 0.062313 0.960031 0.046 Uiso 1 1 calc R U . C23 C 0.1882(4) 0.1117(4) 0.9481(3) 0.0294(9) Uani 1 1 d . . . H23 H 0.196732 0.103919 0.883284 0.035 Uiso 1 1 calc R U . C24 C 0.0487(4) 0.1499(3) 0.9959(3) 0.0195(7) Uani 1 1 d . . . C25 C 0.3349(4) 0.3589(4) 0.4014(3) 0.0259(8) Uani 1 1 d . . . C26 C 0.3760(8) 0.4708(5) 0.3391(4) 0.0611(19) Uani 1 1 d . . . H26A H 0.288839 0.527625 0.325162 0.092 Uiso 1 1 calc R U . H26B H 0.429132 0.443740 0.281114 0.092 Uiso 1 1 calc R U . H26C H 0.436600 0.513055 0.370880 0.092 Uiso 1 1 calc R U . C27 C 0.4740(5) 0.2740(6) 0.4268(4) 0.0486(14) Uani 1 1 d . . . H27A H 0.529142 0.318999 0.460457 0.073 Uiso 1 1 calc R U . H27B H 0.532024 0.248388 0.369865 0.073 Uiso 1 1 calc R U . H27C H 0.449132 0.200646 0.466079 0.073 Uiso 1 1 calc R U . C28 C 0.2532(5) 0.2867(4) 0.3471(3) 0.0308(9) Uani 1 1 d . . . H28A H 0.164229 0.338825 0.330565 0.046 Uiso 1 1 calc R U . H28B H 0.230011 0.212307 0.385671 0.046 Uiso 1 1 calc R U . H28C H 0.313188 0.262895 0.290453 0.046 Uiso 1 1 calc R U . C1S C 0.5024(8) 0.1620(7) 0.6790(5) 0.076(2) Uani 1 1 d . . . H1S H 0.463973 0.198608 0.619402 0.092 Uiso 1 1 calc R U . Cl3 Cl 0.42921(15) 0.25936(15) 0.76077(12) 0.0599(4) Uani 1 1 d . . . Cl4 Cl 0.68806(17) 0.14924(18) 0.65934(12) 0.0718(5) Uani 1 1 d . . . Cl5 Cl 0.4445(2) 0.0188(2) 0.7053(3) 0.1317(12) Uani 1 1 d . . . O1W O 0.1122(4) 0.9954(3) 0.5340(2) 0.0387(8) Uani 1 1 d . . . H1WA H 0.093(6) 1.044(6) 0.582(4) 0.054(17) Uiso 1 1 d . . . H1WB H 0.137(9) 0.908(8) 0.558(6) 0.10(3) Uiso 1 1 d . . . H1WC H 0.000000 1.000000 0.500000 0.11(4) Uiso 1 2 d S . P loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Au1 0.01936(10) 0.01084(10) 0.01437(11) -0.00300(7) -0.00041(7) -0.00267(6) Cl1 0.0223(4) 0.0239(5) 0.0190(4) -0.0032(4) 0.0015(3) 0.0005(3) Cl2 0.0235(4) 0.0240(5) 0.0189(4) -0.0046(4) -0.0042(3) -0.0005(3) O1 0.0433(16) 0.0161(13) 0.0153(13) -0.0014(11) 0.0039(11) -0.0049(11) O2 0.061(2) 0.0189(14) 0.0209(15) -0.0099(12) 0.0084(13) -0.0156(13) N1 0.0332(17) 0.0127(15) 0.0138(15) -0.0014(13) -0.0001(13) -0.0060(13) N2 0.043(2) 0.0119(16) 0.0192(17) -0.0070(13) 0.0057(14) -0.0116(14) C1 0.032(2) 0.0168(18) 0.0185(19) -0.0039(15) -0.0007(15) -0.0036(15) C2 0.0187(16) 0.0183(18) 0.0181(18) -0.0047(14) 0.0005(13) -0.0017(13) C3 0.0200(16) 0.0169(18) 0.0138(17) -0.0039(14) -0.0016(13) -0.0031(13) C4 0.0227(17) 0.0182(18) 0.0104(16) -0.0046(14) 0.0001(13) -0.0019(13) C5 0.0220(16) 0.0165(18) 0.0140(17) -0.0056(14) 0.0000(13) -0.0031(13) C6 0.0275(18) 0.0178(18) 0.0170(18) -0.0067(14) 0.0008(14) -0.0048(14) C7 0.0226(17) 0.024(2) 0.0189(18) -0.0084(15) 0.0011(14) -0.0060(14) C8 0.0213(17) 0.0223(19) 0.0156(18) -0.0016(15) 0.0015(13) -0.0067(14) C9 0.0260(18) 0.0204(19) 0.0150(17) -0.0060(15) -0.0010(14) -0.0039(14) C10 0.047(2) 0.020(2) 0.0185(19) -0.0055(16) 0.0055(17) -0.0148(17) C11 0.035(2) 0.0146(17) 0.0146(18) -0.0036(14) 0.0044(15) -0.0116(15) C12 0.0254(18) 0.0167(18) 0.0200(18) -0.0010(14) -0.0007(14) -0.0101(14) C13 0.033(2) 0.031(2) 0.025(2) 0.0003(17) -0.0095(17) -0.0130(17) C14 0.026(2) 0.037(3) 0.045(3) 0.000(2) -0.0110(19) -0.0071(18) C15 0.0213(19) 0.039(3) 0.045(3) -0.006(2) 0.0012(18) -0.0049(17) C16 0.0252(18) 0.024(2) 0.027(2) -0.0076(16) 0.0064(16) -0.0071(15) C17 0.0210(17) 0.0146(17) 0.0224(19) -0.0036(14) 0.0010(14) -0.0075(13) C18 0.0257(17) 0.0093(16) 0.0172(18) -0.0043(13) 0.0004(14) -0.0052(13) C19 0.0241(17) 0.0104(16) 0.0231(19) -0.0010(14) -0.0015(14) -0.0057(13) C20 0.029(2) 0.0173(19) 0.035(2) -0.0013(17) -0.0072(17) -0.0067(15) C21 0.024(2) 0.024(2) 0.061(3) 0.004(2) -0.006(2) -0.0028(16) C22 0.027(2) 0.027(2) 0.054(3) 0.005(2) 0.010(2) 0.0014(17) C23 0.033(2) 0.0179(19) 0.032(2) 0.0001(17) 0.0126(18) -0.0024(16) C24 0.0266(18) 0.0087(16) 0.0224(19) -0.0017(14) 0.0041(14) -0.0051(13) C25 0.033(2) 0.028(2) 0.0186(19) -0.0103(16) 0.0068(16) -0.0116(17) C26 0.109(5) 0.046(3) 0.029(3) -0.017(2) 0.040(3) -0.039(3) C27 0.025(2) 0.085(4) 0.036(3) -0.025(3) 0.0015(19) 0.000(2) C28 0.036(2) 0.041(3) 0.0171(19) -0.0130(18) 0.0027(16) -0.0089(19) C1S 0.069(4) 0.086(5) 0.071(5) -0.021(4) -0.004(4) 0.006(4) Cl3 0.0433(7) 0.0695(10) 0.0695(10) -0.0310(8) 0.0033(6) -0.0061(6) Cl4 0.0499(8) 0.0921(13) 0.0644(10) -0.0140(9) 0.0161(7) 0.0039(8) Cl5 0.0782(13) 0.0666(13) 0.270(4) -0.0747(18) -0.0379(18) -0.0150(10) O1W 0.076(2) 0.0187(16) 0.0202(15) -0.0058(13) 0.0024(15) -0.0066(15) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 Cl1 Au1 Cl1 180.00(3) . 2_567 Cl1 Au1 Cl2 91.13(3) . . Cl1 Au1 Cl2 88.87(3) 2_567 . Cl1 Au1 Cl2 88.87(3) . 2_567 Cl1 Au1 Cl2 91.13(3) 2_567 2_567 Cl2 Au1 Cl2 180.0 . 2_567 C2 N1 C1 121.6(3) . . C2 N1 H1N 125(3) . . C1 N1 H1N 114(3) . . C9 N2 C10 120.5(3) . . C9 N2 H2N 120(4) . . C10 N2 H2N 119(4) . . N1 C1 C18 111.4(3) . 2_567 N1 C1 H1A 109.3 . . C18 C1 H1A 109.3 2_567 . N1 C1 H1B 109.3 . . C18 C1 H1B 109.3 2_567 . H1A C1 H1B 108.0 . . O1 C2 N1 122.0(3) . . O1 C2 C3 120.2(3) . . N1 C2 C3 117.8(3) . . C4 C3 C8 120.0(3) . . C4 C3 C2 122.1(3) . . C8 C3 C2 117.8(3) . . C3 C4 C5 119.6(3) . . C3 C4 H4 120.2 . . C5 C4 H4 120.2 . . C4 C5 C6 119.6(3) . . C4 C5 C9 121.8(3) . . C6 C5 C9 118.6(3) . . C7 C6 C5 121.6(3) . . C7 C6 H6 119.2 . . C5 C6 H6 119.2 . . C8 C7 C6 117.7(3) . . C8 C7 C25 122.1(3) . . C6 C7 C25 120.1(3) . . C7 C8 C3 121.3(3) . . C7 C8 H8 119.4 . . C3 C8 H8 119.4 . . O2 C9 N2 119.6(3) . . O2 C9 C5 121.7(3) . . N2 C9 C5 118.8(3) . . N2 C10 C11 112.5(3) . . N2 C10 H10A 109.1 . . C11 C10 H10A 109.1 . . N2 C10 H10B 109.1 . . C11 C10 H10B 109.1 . . H10A C10 H10B 107.8 . . C24 C11 C12 120.5(3) . . C24 C11 C10 119.3(3) . . C12 C11 C10 120.1(4) . . C11 C12 C13 122.9(4) . . C11 C12 C17 119.1(3) . . C13 C12 C17 117.9(3) . . C14 C13 C12 121.9(4) . . C14 C13 H13 119.0 . . C12 C13 H13 119.0 . . C13 C14 C15 120.0(4) . . C13 C14 H14 120.0 . . C15 C14 H14 120.0 . . C16 C15 C14 120.8(4) . . C16 C15 H15 119.6 . . C14 C15 H15 119.6 . . C15 C16 C17 121.3(4) . . C15 C16 H16 119.4 . . C17 C16 H16 119.4 . . C18 C17 C16 122.2(4) . . C18 C17 C12 119.8(3) . . C16 C17 C12 118.0(3) . . C19 C18 C17 120.8(3) . . C19 C18 C1 120.3(3) . 2_567 C17 C18 C1 118.9(3) . 2_567 C18 C19 C20 122.7(4) . . C18 C19 C24 118.9(3) . . C20 C19 C24 118.4(3) . . C21 C20 C19 121.0(4) . . C21 C20 H20 119.5 . . C19 C20 H20 119.5 . . C20 C21 C22 120.5(4) . . C20 C21 H21 119.8 . . C22 C21 H21 119.8 . . C23 C22 C21 120.9(4) . . C23 C22 H22 119.5 . . C21 C22 H22 119.5 . . C22 C23 C24 121.3(4) . . C22 C23 H23 119.4 . . C24 C23 H23 119.4 . . C11 C24 C23 121.6(4) . . C11 C24 C19 120.4(3) . . C23 C24 C19 118.0(4) . . C26 C25 C28 108.8(4) . . C26 C25 C7 112.4(3) . . C28 C25 C7 110.7(3) . . C26 C25 C27 108.6(4) . . C28 C25 C27 108.1(4) . . C7 C25 C27 108.1(3) . . C25 C26 H26A 109.5 . . C25 C26 H26B 109.5 . . H26A C26 H26B 109.5 . . C25 C26 H26C 109.5 . . H26A C26 H26C 109.5 . . H26B C26 H26C 109.5 . . C25 C27 H27A 109.5 . . C25 C27 H27B 109.5 . . H27A C27 H27B 109.5 . . C25 C27 H27C 109.5 . . H27A C27 H27C 109.5 . . H27B C27 H27C 109.5 . . C25 C28 H28A 109.5 . . C25 C28 H28B 109.5 . . H28A C28 H28B 109.5 . . C25 C28 H28C 109.5 . . H28A C28 H28C 109.5 . . H28B C28 H28C 109.5 . . Cl3 C1S Cl4 113.3(4) . . Cl3 C1S Cl5 110.7(4) . . Cl4 C1S Cl5 112.4(4) . . Cl3 C1S H1S 106.7 . . Cl4 C1S H1S 106.7 . . Cl5 C1S H1S 106.7 . . H1WA O1W H1WB 110(6) . . H1WA O1W H1WC 107(4) . . H1WB O1W H1WC 105(5) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Au1 Cl1 2.2798(9) . Au1 Cl1 2.2799(9) 2_567 Au1 Cl2 2.2843(9) . Au1 Cl2 2.2843(9) 2_567 O1 C2 1.236(4) . O2 C9 1.241(5) . N1 C2 1.334(5) . N1 C1 1.460(5) . N1 H1N 0.76(5) . N2 C9 1.324(5) . N2 C10 1.464(5) . N2 H2N 0.72(5) . C1 C18 1.524(5) 2_567 C1 H1A 0.9900 . C1 H1B 0.9900 . C2 C3 1.498(5) . C3 C4 1.390(5) . C3 C8 1.396(5) . C4 C5 1.391(5) . C4 H4 0.9500 . C5 C6 1.396(5) . C5 C9 1.502(5) . C6 C7 1.395(5) . C6 H6 0.9500 . C7 C8 1.394(5) . C7 C25 1.534(5) . C8 H8 0.9500 . C10 C11 1.513(5) . C10 H10A 0.9900 . C10 H10B 0.9900 . C11 C24 1.398(6) . C11 C12 1.401(5) . C12 C13 1.426(5) . C12 C17 1.448(5) . C13 C14 1.355(6) . C13 H13 0.9500 . C14 C15 1.421(7) . C14 H14 0.9500 . C15 C16 1.352(6) . C15 H15 0.9500 . C16 C17 1.433(5) . C16 H16 0.9500 . C17 C18 1.401(5) . C18 C19 1.401(5) . C19 C20 1.431(5) . C19 C24 1.441(5) . C20 C21 1.365(6) . C20 H20 0.9500 . C21 C22 1.413(7) . C21 H21 0.9500 . C22 C23 1.346(7) . C22 H22 0.9500 . C23 C24 1.439(5) . C23 H23 0.9500 . C25 C26 1.520(6) . C25 C28 1.531(6) . C25 C27 1.546(7) . C26 H26A 0.9800 . C26 H26B 0.9800 . C26 H26C 0.9800 . C27 H27A 0.9800 . C27 H27B 0.9800 . C27 H27C 0.9800 . C28 H28A 0.9800 . C28 H28B 0.9800 . C28 H28C 0.9800 . C1S Cl3 1.701(7) . C1S Cl4 1.734(7) . C1S Cl5 1.739(8) . C1S H1S 1.0000 . O1W H1WA 0.90(6) . O1W H1WB 0.98(9) . O1W H1WC 1.218(4) . loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A N1 H1N Cl1 0.76(5) 2.76(5) 3.500(4) 165(4) . N2 H2N Cl2 0.72(5) 2.91(5) 3.535(4) 147(5) 2_567 O1W H1WA O2 0.90(6) 1.67(6) 2.574(4) 177(6) 1_565 O1W H1WB O1 0.98(9) 1.63(9) 2.583(4) 162(8) . O1W H1WC O1W 1.218(4) 1.218(4) 2.436(8) 180.000(3) 2_576 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_4 C2 N1 C1 C18 -177.0(3) . 2_567 C1 N1 C2 O1 0.8(6) . . C1 N1 C2 C3 179.8(3) . . O1 C2 C3 C4 -157.4(3) . . N1 C2 C3 C4 23.6(5) . . O1 C2 C3 C8 22.4(5) . . N1 C2 C3 C8 -156.6(3) . . C8 C3 C4 C5 1.7(5) . . C2 C3 C4 C5 -178.5(3) . . C3 C4 C5 C6 -0.8(5) . . C3 C4 C5 C9 178.3(3) . . C4 C5 C6 C7 0.4(6) . . C9 C5 C6 C7 -178.7(3) . . C5 C6 C7 C8 -0.9(6) . . C5 C6 C7 C25 176.2(4) . . C6 C7 C8 C3 1.7(5) . . C25 C7 C8 C3 -175.2(3) . . C4 C3 C8 C7 -2.2(5) . . C2 C3 C8 C7 178.0(3) . . C10 N2 C9 O2 0.5(6) . . C10 N2 C9 C5 -178.2(4) . . C4 C5 C9 O2 174.0(4) . . C6 C5 C9 O2 -6.9(6) . . C4 C5 C9 N2 -7.3(5) . . C6 C5 C9 N2 171.8(4) . . C9 N2 C10 C11 159.7(4) . . N2 C10 C11 C24 -82.2(5) . . N2 C10 C11 C12 101.9(4) . . C24 C11 C12 C13 173.2(3) . . C10 C11 C12 C13 -10.9(5) . . C24 C11 C12 C17 -6.2(5) . . C10 C11 C12 C17 169.7(3) . . C11 C12 C13 C14 179.8(4) . . C17 C12 C13 C14 -0.8(6) . . C12 C13 C14 C15 -0.2(7) . . C13 C14 C15 C16 0.1(7) . . C14 C15 C16 C17 1.1(7) . . C15 C16 C17 C18 176.7(4) . . C15 C16 C17 C12 -2.1(6) . . C11 C12 C17 C18 2.5(5) . . C13 C12 C17 C18 -176.9(3) . . C11 C12 C17 C16 -178.7(3) . . C13 C12 C17 C16 1.9(5) . . C16 C17 C18 C19 -174.8(3) . . C12 C17 C18 C19 3.9(5) . . C16 C17 C18 C1 5.9(5) . 2_567 C12 C17 C18 C1 -175.4(3) . 2_567 C17 C18 C19 C20 174.0(3) . . C1 C18 C19 C20 -6.7(5) 2_567 . C17 C18 C19 C24 -6.6(5) . . C1 C18 C19 C24 172.7(3) 2_567 . C18 C19 C20 C21 178.8(4) . . C24 C19 C20 C21 -0.6(5) . . C19 C20 C21 C22 -0.3(6) . . C20 C21 C22 C23 0.5(7) . . C21 C22 C23 C24 0.3(7) . . C12 C11 C24 C23 -175.5(3) . . C10 C11 C24 C23 8.7(5) . . C12 C11 C24 C19 3.5(5) . . C10 C11 C24 C19 -172.4(3) . . C22 C23 C24 C11 177.8(4) . . C22 C23 C24 C19 -1.2(6) . . C18 C19 C24 C11 2.9(5) . . C20 C19 C24 C11 -177.7(3) . . C18 C19 C24 C23 -178.1(3) . . C20 C19 C24 C23 1.3(5) . . C8 C7 C25 C26 -10.9(6) . . C6 C7 C25 C26 172.2(4) . . C8 C7 C25 C28 -132.7(4) . . C6 C7 C25 C28 50.4(5) . . C8 C7 C25 C27 109.0(4) . . C6 C7 C25 C27 -67.9(5) . .