#------------------------------------------------------------------------------ #$Date: 2019-11-26 02:54:25 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242447 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/24/4132474.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132474 loop_ _publ_author_name 'Sil, Debangsu' 'Martinez, Zachary' 'Ding, Shengda' 'Bhuvanesh, Nattamai' 'Darensbourg, Donald J.' 'Hall, Michael B.' 'Darensbourg, Marcetta Y.' _publ_section_title ; Cyanide Docking and Linkage Isomerism in Models for the Artificial [FeFe]-Hydrogenase Maturation Process. ; _journal_issue 31 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 9904 _journal_page_last 9911 _journal_paper_doi 10.1021/jacs.8b04189 _journal_volume 140 _journal_year 2018 _chemical_formula_moiety 'C63 H46 Cu N9 Zn, F6 P' _chemical_formula_sum 'C63 H46 Cu F6 N9 P Zn' _chemical_formula_weight 1202.97 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_date 2017-11-29 _audit_creation_method ; Olex2 1.2-beta (compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5335) ; _cell_angle_alpha 90 _cell_angle_beta 90.768(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.550(2) _cell_length_b 31.109(8) _cell_length_c 19.849(5) _cell_measurement_reflns_used 9908 _cell_measurement_temperature 110.0 _cell_measurement_theta_max 23.662 _cell_measurement_theta_min 2.216 _cell_volume 5896(2) _computing_cell_refinement 'SAINT V8.38A (Bruker, 2016)' _computing_data_reduction 'SAINT V8.38A (Bruker, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 110.0 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0514 _diffrn_reflns_av_unetI/netI 0.0229 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 29 _diffrn_reflns_limit_k_min -29 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 66386 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 19.998 _diffrn_reflns_theta_max 19.998 _diffrn_reflns_theta_min 1.663 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.861 _exptl_absorpt_correction_T_max 0.5614 _exptl_absorpt_correction_T_min 0.4653 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0729 before and 0.0565 after correction. The Ratio of minimum to maximum transmission is 0.8288. The \l/2 correction factor is Not present.' _exptl_crystal_colour blue _exptl_crystal_colour_primary blue _exptl_crystal_density_diffrn 1.355 _exptl_crystal_description plate _exptl_crystal_F_000 2460 _exptl_crystal_size_max 0.332 _exptl_crystal_size_mid 0.287 _exptl_crystal_size_min 0.04 _refine_diff_density_max 0.501 _refine_diff_density_min -0.567 _refine_diff_density_rms 0.072 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.195 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 773 _refine_ls_number_reflns 5491 _refine_ls_number_restraints 512 _refine_ls_restrained_S_all 1.138 _refine_ls_R_factor_all 0.0600 _refine_ls_R_factor_gt 0.0541 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0220P)^2^+35.0860P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1206 _refine_ls_wR_factor_ref 0.1240 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4952 _reflns_number_total 5491 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b04189_si_005.cif _cod_data_source_block znnccupf6_sq _cod_original_cell_volume 5897(2) _cod_database_code 4132474 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.966 _shelx_estimated_absorpt_t_min 0.763 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2. Restrained distances C17-C16 \\sim C17A-C16 with sigma of 0.02 C39-C38 \\sim C39A-C38 with sigma of 0.02 3. Uiso/Uaniso restraints and constraints C17 \\sim C18 \\sim C19 \\sim C20 \\sim C21 \\sim C22 \\sim C17A \\sim C18A \\sim C19A \\sim C20A \\sim C21A \\sim C22A: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 C39 \\sim C40 \\sim C41 \\sim C42 \\sim C43 \\sim C44 \\sim C39A \\sim C40A \\sim C41A \\sim C42A \\sim C43A \\sim C44A: within 2A with sigma of 0.04 and sigma for terminal atoms of 0.08 Uanis(C39A) = Uanis(C39) Uanis(C17) = Uanis(C17A) Uanis(C22A) = Uanis(C22) 4. Rigid body (RIGU) restrains C17, C18, C19, C20, C21, C22, C17A, C18A, C19A, C20A, C21A, C22A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 C39, C40, C41, C42, C43, C44, C39A, C40A, C41A, C42A, C43A, C44A with sigma for 1-2 distances of 0.004 and sigma for 1-3 distances of 0.004 5. Others Sof(C17A)=Sof(C18A)=Sof(H18A)=Sof(C19A)=Sof(H19A)=Sof(C20A)=Sof(H20A)= Sof(C21A)=Sof(H21A)=Sof(C22A)=Sof(H22A)=Sof(C39A)=Sof(C40A)=Sof(H40A)= Sof(C41A)=Sof(H41A)=Sof(C42A)=Sof(H42A)=Sof(C43A)=Sof(H43A)=Sof(C44A)= Sof(H44A)=1-FVAR(1) Sof(C17)=Sof(C18)=Sof(H18)=Sof(C19)=Sof(H19)=Sof(C20)=Sof(H20)=Sof(C21)= Sof(H21)=Sof(C22)=Sof(H22)=Sof(C39)=Sof(C40)=Sof(H40)=Sof(C41)=Sof(H41)= Sof(C42)=Sof(H42)=Sof(C43)=Sof(H43)=Sof(C44)=Sof(H44)=FVAR(1) 6.a Secondary CH2 refined with riding coordinates: C51(H51A,H51B), C57(H57A,H57B), C63(H63A,H63B) 6.b Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C7(H7), C8(H8), C9(H9), C10(H10), C11(H11), C13(H13), C14(H14), C18(H18), C19(H19), C20(H20), C21(H21), C22(H22), C18A(H18A), C19A(H19A), C20A(H20A), C21A(H21A), C22A(H22A), C24(H24), C25(H25), C29(H29), C30(H30), C31(H31), C32(H32), C33(H33), C35(H35), C36(H36), C40(H40), C41(H41), C42(H42), C43(H43), C44(H44), C40A(H40A), C41A(H41A), C42A(H42A), C43A(H43A), C44A(H44A), C46(H46), C47(H47), C48(H48), C49(H49), C52(H52), C53(H53), C54(H54), C55(H55), C58(H58), C59(H59), C60(H60), C61(H61) 6.c Fitted hexagon refined as free rotating group: C17(C18,C19,C20,C21,C22), C17A(C18A,C19A,C20A,C21A,C22A), C39(C40,C41,C42,C43, C44), C39A(C40A,C41A,C42A,C43A,C44A) ; _shelx_res_file ; TITL znnccupf6_a.res in P2(1)/c znnccupf6_sq.res created by SHELXL-2017/1 at 11:15:31 on 29-Nov-2017 REM Old TITL ZnNCCuPF6 in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.185, Rweak 0.021, Alpha 0.066, Orientation as input REM Formula found by SHELXT: C68 N9 F6 P Zn2 CELL 0.71073 9.5504 31.1091 19.8491 90 90.768 90 ZERR 4 0.0023 0.0075 0.0049 0 0.003 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H Cu F N P Zn UNIT 252 184 4 24 36 4 4 SADI C17 C16 C17A C16 SADI C39 C38 C39A C38 SIMU C17 > C22A SIMU C39 > C44A RIGU C17 > C22A RIGU C39 > C44A EADP C39A C39 EADP C17 C17A EADP C22A C22 L.S. 10 0 90 PLAN 20 SIZE 0.04 0.287 0.332 TEMP -163.15 BOND $H wpdb -1 more -1 htab conf ABIN fmap 2 53 acta OMIT -4 40 OMIT 0 1 1 OMIT 0 2 0 OMIT 0 4 0 OMIT -1 4 3 OMIT 1 1 1 OMIT -2 0 16 OMIT 1 0 0 OMIT 0 3 1 OMIT 1 9 11 OMIT 0 0 4 OMIT -6 10 15 OMIT 1 5 14 OMIT -5 13 11 OMIT -1 3 4 OMIT -3 7 9 REM REM REM WGHT 0.022000 35.086002 FVAR 0.16879 0.34962 ZN1 7 0.739800 0.218833 0.765204 11.00000 0.02496 0.01800 = 0.02089 0.00167 -0.00252 -0.00150 CU1 3 0.801621 0.331572 0.585573 11.00000 0.02184 0.02314 = 0.02865 0.00832 0.00146 0.00111 N1 5 0.541423 0.210558 0.723212 11.00000 0.03042 0.01778 = 0.01853 0.00101 -0.00259 -0.00434 N2 5 0.662731 0.271543 0.817365 11.00000 0.02266 0.02280 = 0.02122 -0.00076 -0.00342 -0.00431 N3 5 0.903069 0.216496 0.834324 11.00000 0.02096 0.02171 = 0.01557 0.00312 -0.00047 -0.00147 N4 5 0.783504 0.155864 0.739218 11.00000 0.02820 0.02171 = 0.02297 0.00753 -0.00599 -0.00046 N5 5 0.817378 0.254556 0.683821 11.00000 0.02969 0.02332 = 0.02627 0.00245 -0.00019 0.00422 N6 5 0.663711 0.304727 0.516390 11.00000 0.02070 0.02544 = 0.03181 -0.00002 0.00019 0.00453 N7 5 0.788256 0.381540 0.519776 11.00000 0.02187 0.03183 = 0.03114 0.01150 0.00205 0.00293 N8 5 0.719760 0.377234 0.651017 11.00000 0.01576 0.01944 = 0.03941 0.01095 0.00049 -0.00156 N9 5 1.007613 0.336945 0.563313 11.00000 0.02718 0.02348 = 0.02885 0.00638 0.00051 0.00333 C1 1 0.504948 0.179501 0.677445 11.00000 0.02983 0.02016 = 0.02693 0.00649 -0.00051 -0.00229 C2 1 0.372990 0.190315 0.645634 11.00000 0.05206 0.01764 = 0.03705 -0.00180 -0.01882 -0.00609 AFIX 43 H2 2 0.324579 0.174263 0.611927 11.00000 -1.20000 AFIX 0 C3 1 0.331954 0.227858 0.673365 11.00000 0.02611 0.03039 = 0.03584 0.00932 -0.01471 -0.00650 AFIX 43 H3 2 0.247758 0.242867 0.662996 11.00000 -1.20000 AFIX 0 C4 1 0.437164 0.241137 0.721065 11.00000 0.02099 0.02216 = 0.03239 0.00727 0.00439 -0.00145 C5 1 0.437127 0.279141 0.758090 11.00000 0.01857 0.02354 = 0.02839 0.00305 -0.00068 -0.00198 C6 1 0.315445 0.308956 0.746706 11.00000 0.01980 0.03045 = 0.01488 0.00012 -0.00415 -0.00074 C7 1 0.181209 0.298203 0.765951 11.00000 0.03063 0.02812 = 0.02563 0.00460 0.00340 -0.00338 AFIX 43 H7 2 0.164743 0.270980 0.786033 11.00000 -1.20000 AFIX 0 C8 1 0.070586 0.326327 0.756507 11.00000 0.02294 0.03870 = 0.03049 -0.00142 0.00389 -0.00214 AFIX 43 H8 2 -0.021174 0.318381 0.769578 11.00000 -1.20000 AFIX 0 C9 1 0.094559 0.365949 0.727998 11.00000 0.02758 0.03345 = 0.03640 -0.00560 -0.00221 0.00741 AFIX 43 H9 2 0.019409 0.385649 0.722023 11.00000 -1.20000 AFIX 0 C10 1 0.226740 0.377010 0.708221 11.00000 0.03328 0.02223 = 0.03354 0.00612 -0.00066 0.00255 AFIX 43 H10 2 0.242621 0.404165 0.687808 11.00000 -1.20000 AFIX 0 C11 1 0.336842 0.348829 0.717862 11.00000 0.02206 0.02844 = 0.02435 0.00379 -0.00274 -0.00674 AFIX 43 H11 2 0.428301 0.356920 0.704534 11.00000 -1.20000 AFIX 0 C12 1 0.539021 0.292226 0.804894 11.00000 0.02739 0.01606 = 0.02124 0.00024 -0.00362 0.00056 C13 1 0.526961 0.328276 0.850070 11.00000 0.01697 0.03150 = 0.02054 0.00477 0.00526 0.00471 AFIX 43 H13 2 0.450680 0.347823 0.851865 11.00000 -1.20000 AFIX 0 C14 1 0.641062 0.329291 0.888592 11.00000 0.01717 0.03303 = 0.02692 -0.00346 0.00450 -0.00565 AFIX 43 H14 2 0.661567 0.349506 0.923214 11.00000 -1.20000 AFIX 0 C15 1 0.728651 0.293855 0.868088 11.00000 0.02771 0.02527 = 0.00682 0.00316 0.00552 0.00251 C16 1 0.858035 0.282627 0.898498 11.00000 0.02907 0.01960 = 0.02284 0.00505 -0.00084 -0.00368 PART 1 AFIX 66 C17 1 0.926816 0.310452 0.951847 21.00000 0.02102 0.02276 = 0.02552 -0.00217 -0.00152 -0.00042 C18 1 1.042484 0.336452 0.940484 21.00000 0.03059 0.03489 = 0.02390 0.00537 -0.00798 -0.00918 AFIX 43 H18 2 1.078954 0.338994 0.896369 21.00000 -1.20000 AFIX 65 C19 1 1.104789 0.358733 0.993667 21.00000 0.03324 0.03915 = 0.02919 -0.00251 -0.00234 -0.01385 AFIX 43 H19 2 1.183843 0.376503 0.985901 21.00000 -1.20000 AFIX 65 C20 1 1.051428 0.355014 1.058215 21.00000 0.02748 0.02443 = 0.02516 -0.00010 -0.00780 -0.00123 AFIX 43 H20 2 1.094012 0.370243 1.094563 21.00000 -1.20000 AFIX 65 C21 1 0.935761 0.329014 1.069579 21.00000 0.02872 0.03482 = 0.02569 0.00346 -0.00694 -0.00540 AFIX 43 H21 2 0.899291 0.326473 1.113694 21.00000 -1.20000 AFIX 65 C22 1 0.873453 0.306733 1.016396 21.00000 0.01824 0.02408 = 0.02570 0.00337 -0.00461 -0.00126 AFIX 43 H22 2 0.794400 0.288963 1.024163 21.00000 -1.20000 AFIX 66 PART 0 PART 2 C17A 1 0.910651 0.312332 0.953651 -21.00000 0.02102 0.02276 = 0.02552 -0.00217 -0.00152 -0.00042 C18A 1 0.971171 0.351265 0.935800 -21.00000 0.04901 0.03345 = 0.02763 0.00246 -0.00031 -0.01422 AFIX 43 H18A 2 0.972525 0.359828 0.889873 -21.00000 -1.20000 AFIX 65 C19A 1 1.029710 0.377670 0.985149 -21.00000 0.06094 0.04250 = 0.03988 -0.00467 -0.00425 -0.02107 AFIX 43 H19A 2 1.071073 0.404280 0.972948 -21.00000 -1.20000 AFIX 65 C20A 1 1.027729 0.365142 1.052348 -21.00000 0.04537 0.04624 = 0.03427 -0.01265 -0.00676 -0.01627 AFIX 43 H20A 2 1.067738 0.383189 1.086075 -21.00000 -1.20000 AFIX 65 C21A 1 0.967210 0.326208 1.070199 -21.00000 0.02146 0.04284 = 0.02372 -0.00357 -0.00728 0.00189 AFIX 43 H21A 2 0.965857 0.317646 1.116127 -21.00000 -1.20000 AFIX 65 C22A 1 0.908670 0.299803 1.020852 -21.00000 0.01824 0.02408 = 0.02570 0.00337 -0.00461 -0.00126 AFIX 43 H22A 2 0.867308 0.273194 1.033053 -21.00000 -1.20000 AFIX 0 PART 0 C23 1 0.937017 0.246522 0.882624 11.00000 0.02097 0.02490 = 0.01311 0.00405 0.00021 -0.00598 C24 1 1.065164 0.234803 0.915170 11.00000 0.02598 0.02392 = 0.02857 0.00390 -0.00390 -0.00782 AFIX 43 H24 2 1.111997 0.250307 0.950005 11.00000 -1.20000 AFIX 0 C25 1 1.107407 0.197739 0.887408 11.00000 0.02677 0.02830 = 0.02626 0.00891 -0.00346 0.00026 AFIX 43 H25 2 1.189572 0.182105 0.899235 11.00000 -1.20000 AFIX 0 C26 1 1.006616 0.186052 0.836909 11.00000 0.02096 0.02679 = 0.02388 0.00543 0.00188 -0.00346 C27 1 1.008350 0.147661 0.798892 11.00000 0.02426 0.02354 = 0.03094 0.00853 0.00251 -0.00130 C28 1 1.131426 0.118627 0.810689 11.00000 0.02775 0.02017 = 0.02842 -0.00153 0.00105 0.00251 C29 1 1.264946 0.130923 0.793983 11.00000 0.03930 0.02516 = 0.04561 0.00864 0.00276 0.00351 AFIX 43 H29 2 1.280005 0.158102 0.773498 11.00000 -1.20000 AFIX 0 C30 1 1.377669 0.103905 0.806851 11.00000 0.01986 0.03858 = 0.05921 -0.00858 0.00893 0.00077 AFIX 43 H30 2 1.469233 0.112605 0.794628 11.00000 -1.20000 AFIX 0 C31 1 1.358393 0.065101 0.836782 11.00000 0.03992 0.02569 = 0.05482 0.00381 -0.00439 0.01119 AFIX 43 H31 2 1.436223 0.046894 0.845906 11.00000 -1.20000 AFIX 0 C32 1 1.226281 0.052398 0.853705 11.00000 0.04794 0.02739 = 0.04517 0.00793 0.00465 -0.00017 AFIX 43 H32 2 1.212733 0.025223 0.874455 11.00000 -1.20000 AFIX 0 C33 1 1.111380 0.078916 0.840812 11.00000 0.03674 0.02248 = 0.03475 0.00330 0.00588 0.00542 AFIX 43 H33 2 1.019927 0.069848 0.852583 11.00000 -1.20000 AFIX 0 C34 1 0.904762 0.134035 0.753860 11.00000 0.02479 0.02212 = 0.02883 0.00362 -0.00234 -0.00019 C35 1 0.907696 0.094795 0.715553 11.00000 0.03989 0.02099 = 0.03584 -0.00662 -0.00168 0.00406 AFIX 43 H35 2 0.980345 0.073933 0.716127 11.00000 -1.20000 AFIX 0 C36 1 0.789074 0.093129 0.678950 11.00000 0.05151 0.01504 = 0.03303 -0.00321 -0.00469 0.00015 AFIX 43 H36 2 0.761265 0.070673 0.649223 11.00000 -1.20000 AFIX 0 C37 1 0.711548 0.131673 0.693010 11.00000 0.03961 0.02269 = 0.02568 -0.00132 -0.01090 -0.00433 C38 1 0.583517 0.142230 0.663229 11.00000 0.04375 0.01827 = 0.02514 0.00584 -0.00927 -0.00743 PART 1 AFIX 66 C39 1 0.510743 0.110938 0.614977 21.00000 0.05656 0.01883 = 0.03465 -0.00440 -0.01977 0.00734 C40 1 0.499767 0.121231 0.546966 21.00000 0.07219 0.02860 = 0.03315 -0.00817 -0.01672 -0.00250 AFIX 43 H40 2 0.535673 0.147786 0.531072 21.00000 -1.20000 AFIX 65 C41 1 0.436254 0.092669 0.502212 21.00000 0.08333 0.03837 = 0.03140 -0.00870 -0.02095 -0.00434 AFIX 43 H41 2 0.428752 0.099704 0.455730 21.00000 -1.20000 AFIX 65 C42 1 0.383717 0.053815 0.525468 21.00000 0.07850 0.03325 = 0.04537 -0.00861 -0.03114 -0.00500 AFIX 43 H42 2 0.340309 0.034294 0.494880 21.00000 -1.20000 AFIX 65 C43 1 0.394693 0.043521 0.593478 21.00000 0.08754 0.02641 = 0.05183 0.00173 -0.03458 -0.01264 AFIX 43 H43 2 0.358786 0.016965 0.609372 21.00000 -1.20000 AFIX 65 C44 1 0.458205 0.072082 0.638233 21.00000 0.09116 0.02687 = 0.04122 0.00226 -0.03534 -0.01179 AFIX 43 H44 2 0.465707 0.065047 0.684715 21.00000 -1.20000 AFIX 66 PART 0 PART 2 C39A 1 0.530326 0.111058 0.610093 -21.00000 0.05656 0.01883 = 0.03465 -0.00440 -0.01977 0.00734 C40A 1 0.603932 0.103674 0.551272 -21.00000 0.07381 0.02664 = 0.03129 0.00173 -0.01539 0.00047 AFIX 43 H40A 2 0.688633 0.118737 0.543286 -21.00000 -1.20000 AFIX 65 C41A 1 0.553607 0.074252 0.504136 -21.00000 0.11329 0.03019 = 0.04301 -0.01084 -0.01715 0.00259 AFIX 43 H41A 2 0.603914 0.069206 0.463935 -21.00000 -1.20000 AFIX 65 C42A 1 0.429676 0.052214 0.515821 -21.00000 0.10332 0.03347 = 0.06279 -0.01305 -0.03825 -0.00248 AFIX 43 H42A 2 0.395281 0.032105 0.483605 -21.00000 -1.20000 AFIX 65 C43A 1 0.356068 0.059597 0.574641 -21.00000 0.07855 0.02277 = 0.06952 -0.00208 -0.03926 0.00176 AFIX 43 H43A 2 0.271367 0.044535 0.582627 -21.00000 -1.20000 AFIX 65 C44A 1 0.406392 0.089019 0.621778 -21.00000 0.04921 0.02911 = 0.06093 -0.00650 -0.02297 0.00784 AFIX 43 H44A 2 0.356084 0.094066 0.661979 -21.00000 -1.20000 AFIX 0 PART 0 C45 1 0.813313 0.282908 0.646525 11.00000 0.01522 0.03032 = 0.01762 -0.00105 0.00469 0.00545 C46 1 0.581810 0.270900 0.524297 11.00000 0.03017 0.03165 = 0.03332 -0.01170 -0.00023 0.00310 AFIX 43 H46 2 0.586871 0.255291 0.565394 11.00000 -1.20000 AFIX 0 C47 1 0.489417 0.257637 0.474718 11.00000 0.03462 0.03831 = 0.06153 -0.02540 0.00586 0.00483 AFIX 43 H47 2 0.432602 0.232965 0.481309 11.00000 -1.20000 AFIX 0 C48 1 0.480352 0.280300 0.416054 11.00000 0.02599 0.06267 = 0.04804 -0.03804 0.00035 0.01510 AFIX 43 H48 2 0.416040 0.271754 0.381669 11.00000 -1.20000 AFIX 0 C49 1 0.564617 0.315559 0.406853 11.00000 0.03510 0.05161 = 0.03774 -0.01174 0.00424 0.02156 AFIX 43 H49 2 0.559582 0.331671 0.366236 11.00000 -1.20000 AFIX 0 C50 1 0.657699 0.327175 0.458445 11.00000 0.01561 0.03442 = 0.03634 -0.00298 -0.00215 0.01460 C51 1 0.758233 0.363193 0.452279 11.00000 0.03983 0.04204 = 0.03305 0.00858 -0.00175 0.00677 AFIX 23 H51A 2 0.846108 0.352712 0.432098 11.00000 -1.20000 H51B 2 0.718223 0.385665 0.422412 11.00000 -1.20000 AFIX 0 C52 1 0.717373 0.376692 0.718387 11.00000 0.02064 0.02560 = 0.04276 0.00693 0.00298 -0.00179 AFIX 43 H52 2 0.747503 0.351504 0.741432 11.00000 -1.20000 AFIX 0 C53 1 0.673095 0.411116 0.755218 11.00000 0.03437 0.03179 = 0.04064 -0.00642 0.00083 -0.00247 AFIX 43 H53 2 0.674904 0.410165 0.803059 11.00000 -1.20000 AFIX 0 C54 1 0.626085 0.446995 0.721966 11.00000 0.04056 0.02105 = 0.06120 -0.01150 -0.00126 0.00269 AFIX 43 H54 2 0.594629 0.471284 0.746514 11.00000 -1.20000 AFIX 0 C55 1 0.624858 0.447521 0.652430 11.00000 0.02432 0.02401 = 0.05306 0.00319 -0.00515 0.00285 AFIX 43 H55 2 0.590959 0.472022 0.628758 11.00000 -1.20000 AFIX 0 C56 1 0.673111 0.412283 0.617456 11.00000 0.01255 0.02154 = 0.04602 0.00739 0.00089 -0.00171 C57 1 0.672891 0.409691 0.542295 11.00000 0.02583 0.02741 = 0.04033 0.01525 0.00453 -0.00056 AFIX 23 H57A 2 0.582132 0.398052 0.525953 11.00000 -1.20000 H57B 2 0.684629 0.438818 0.523090 11.00000 -1.20000 AFIX 0 C58 1 1.107645 0.308255 0.576882 11.00000 0.02723 0.02954 = 0.02856 0.00343 -0.00314 0.00413 AFIX 43 H58 2 1.083037 0.282116 0.598451 11.00000 -1.20000 AFIX 0 C59 1 1.245568 0.315242 0.560671 11.00000 0.01989 0.04721 = 0.02859 -0.00409 0.00099 0.00481 AFIX 43 H59 2 1.315716 0.294707 0.571886 11.00000 -1.20000 AFIX 0 C60 1 1.278709 0.352224 0.528255 11.00000 0.02020 0.05067 = 0.03633 -0.00531 0.00184 -0.00574 AFIX 43 H60 2 1.373112 0.357441 0.516173 11.00000 -1.20000 AFIX 0 C61 1 1.177795 0.382212 0.512666 11.00000 0.03482 0.04158 = 0.02413 -0.00022 0.00875 -0.01417 AFIX 43 H61 2 1.200343 0.408074 0.489788 11.00000 -1.20000 AFIX 0 C62 1 1.041371 0.373204 0.531703 11.00000 0.02884 0.02652 = 0.02595 0.00108 -0.00247 0.00208 C63 1 0.924253 0.404769 0.522682 11.00000 0.02960 0.03130 = 0.03325 0.01011 0.00736 -0.00531 AFIX 23 H63A 2 0.924598 0.425333 0.560749 11.00000 -1.20000 H63B 2 0.937266 0.421200 0.480513 11.00000 -1.20000 AFIX 0 P1 6 1.261348 0.493413 0.595527 11.00000 0.04336 0.03424 = 0.04546 0.01294 -0.00925 -0.00676 F1 4 1.126685 0.469491 0.621544 11.00000 0.04260 0.07702 = 0.09174 0.03677 -0.00925 -0.01844 F2 4 1.340140 0.449447 0.581143 11.00000 0.07628 0.05249 = 0.09031 -0.01578 -0.03108 0.01227 F3 4 1.197954 0.493730 0.521016 11.00000 0.08475 0.06211 = 0.05161 0.01245 -0.03423 -0.01442 F4 4 1.400431 0.516822 0.568436 11.00000 0.06569 0.06550 = 0.06444 0.01430 -0.00381 -0.01112 F5 4 1.198913 0.539493 0.607326 11.00000 0.09066 0.04898 = 0.06170 0.00556 -0.00718 0.02926 F6 4 1.327258 0.493221 0.669790 11.00000 0.04733 0.06239 = 0.03845 0.00813 -0.00652 0.00476 HKLF 4 REM znnccupf6_a.res in P2(1)/c REM R1 = 0.0541 for 4952 Fo > 4sig(Fo) and 0.0600 for all 5491 data REM 773 parameters refined using 512 restraints END WGHT 0.0220 35.0860 REM Instructions for potential hydrogen bonds EQIV $1 -x+2, -y+1, -z+1 HTAB C51 F5_$1 EQIV $2 x-1, y, z HTAB C55 F4_$2 HTAB C57 F3_$1 HTAB C57 F4_$1 HTAB C63 F5_$1 REM Highest difference peak 0.501, deepest hole -0.567, 1-sigma level 0.072 Q1 1 1.3687 0.4793 0.5427 11.00000 0.05 0.50 Q2 1 0.7066 0.0610 0.4631 11.00000 0.05 0.38 Q3 1 0.7443 0.3384 0.6363 11.00000 0.05 0.33 Q4 1 0.7360 0.0739 0.4786 11.00000 0.05 0.30 Q5 1 1.1726 0.5395 0.6601 11.00000 0.05 0.27 Q6 1 1.0440 0.4343 0.9602 11.00000 0.05 0.26 Q7 1 1.2996 0.5435 0.6055 11.00000 0.05 0.25 Q8 1 0.7897 0.0608 0.6465 11.00000 0.05 0.25 Q9 1 0.6798 0.2222 0.8114 11.00000 0.05 0.25 Q10 1 1.0860 0.4982 0.6526 11.00000 0.05 0.24 Q11 1 0.9334 0.0598 0.7379 11.00000 0.05 0.24 Q12 1 0.6779 0.4349 0.4392 11.00000 0.05 0.23 Q13 1 1.2734 0.5515 0.6580 11.00000 0.05 0.23 Q14 1 1.1405 0.5162 0.5563 11.00000 0.05 0.23 Q15 1 0.3703 0.0589 0.7148 11.00000 0.05 0.23 Q16 1 0.3693 0.0656 0.5336 11.00000 0.05 0.23 Q17 1 0.5505 0.0418 0.6384 11.00000 0.05 0.23 Q18 1 0.7617 0.3405 0.5190 11.00000 0.05 0.23 Q19 1 0.9195 0.4010 1.1019 11.00000 0.05 0.22 Q20 1 0.5805 0.0358 0.5455 11.00000 0.05 0.22 ; _shelx_res_checksum 83759 _shelx_hkl_file ; -1 0 0 32.40 1.70 1 0 0 34.70 1.90 1 0 0 30.70 1.60 1 0 0 36.80 1.80 -1 0 0 30.10 1.50 -1 0 0 33.00 1.50 -1 0 0 32.10 1.70 2 0 0 1566.54 45.10 2 0 0 1561.74 46.10 -2 0 0 1570.04 45.40 -2 0 0 1492.15 45.00 -2 0 0 1508.35 45.60 2 0 0 1503.55 45.50 2 0 0 1526.15 45.20 2 0 0 1553.34 45.40 -2 0 0 1538.95 45.20 -2 0 0 1519.75 45.50 3 0 0 169.28 7.20 3 0 0 171.78 6.60 3 0 0 171.58 8.00 3 0 0 168.68 7.00 -3 0 0 179.28 7.00 -3 0 0 175.48 6.80 -3 0 0 166.48 7.20 -3 0 0 167.48 6.50 -3 0 0 168.18 7.20 3 0 0 167.78 6.70 4 0 0 286.27 11.90 4 0 0 267.47 10.60 -4 0 0 289.57 10.90 -4 0 0 262.27 9.80 -4 0 0 268.37 10.10 4 0 0 274.67 10.00 4 0 0 270.47 10.80 4 0 0 274.77 10.20 -4 0 0 279.87 11.10 -4 0 0 274.37 10.60 -5 0 0 10.30 3.00 5 0 0 12.70 3.30 -5 0 0 8.40 2.60 -5 0 0 9.80 3.50 5 0 0 7.90 2.60 -5 0 0 10.10 2.60 5 0 0 14.70 4.20 5 0 0 10.20 3.00 -6 0 0 65.69 5.70 6 0 0 61.59 6.90 6 0 0 52.79 5.20 6 0 0 58.49 6.00 -6 0 0 66.69 6.10 6 0 0 71.19 6.50 -6 0 0 63.69 5.30 -6 0 0 59.49 5.20 7 0 0 91.49 8.30 -7 0 0 111.69 7.20 -7 0 0 117.79 8.00 -7 0 0 114.99 9.30 7 0 0 114.19 9.70 7 0 0 108.39 7.70 7 0 0 117.19 9.10 -8 0 0 -5.40 3.30 -8 0 0 7.30 4.30 8 0 0 3.70 4.10 8 0 0 1.80 4.60 -8 0 0 0.40 5.30 8 0 0 4.10 6.00 9 0 0 26.70 6.10 9 0 0 15.00 7.80 -9 0 0 27.70 6.10 -9 0 0 12.60 5.00 9 0 0 23.10 7.30 -9 0 0 25.60 7.90 -10 0 0 9.40 8.90 10 0 0 16.70 6.80 -10 0 0 6.50 5.70 10 0 0 6.80 7.20 10 0 0 19.10 9.30 1 -1 0 2311.17 65.59 -1 -1 0 2215.68 65.59 -1 -1 0 2354.16 65.69 1 -1 0 2061.39 65.89 1 -1 0 2310.07 65.69 1 -1 0 2206.68 65.59 -1 -1 0 2333.57 65.69 -1 1 0 2082.79 65.49 -1 1 0 2274.67 65.89 1 1 0 2413.16 66.09 -1 1 0 2447.35 65.59 -1 1 0 2292.97 65.69 1 1 0 2278.97 65.69 1 1 0 2111.99 65.59 2 -1 0 3.50 1.80 -2 -1 0 2.20 1.30 -2 -1 0 2.50 1.50 2 -1 0 4.40 1.50 -2 -1 0 2.80 1.30 2 1 0 3.20 1.40 -2 1 0 0.40 1.10 2 1 0 2.90 1.80 -2 1 0 2.40 1.30 -2 1 0 0.40 1.20 -2 1 0 5.10 1.60 2 1 0 5.40 1.60 -2 1 0 3.80 1.30 3 -1 0 656.73 21.50 -3 -1 0 700.03 21.20 3 -1 0 679.73 21.20 -3 -1 0 681.83 21.50 3 -1 0 676.63 22.40 -3 -1 0 672.13 21.00 -3 -1 0 670.13 21.70 3 -1 0 688.13 21.00 3 -1 0 668.73 21.60 3 1 0 687.23 21.60 -3 1 0 658.03 21.00 -3 1 0 696.63 21.50 -3 1 0 679.73 21.10 3 1 0 670.73 21.10 3 1 0 668.33 21.60 3 1 0 693.93 22.50 -3 1 0 668.33 21.60 -3 1 0 662.13 21.80 -4 -1 0 158.18 7.30 4 -1 0 144.69 7.30 4 -1 0 151.48 7.20 4 -1 0 153.28 8.40 -4 -1 0 155.48 6.60 -4 -1 0 155.48 6.80 -4 -1 0 149.99 7.50 4 -1 0 165.58 6.70 4 -1 0 156.78 6.80 -4 1 0 162.08 7.50 4 1 0 148.39 7.20 4 1 0 154.98 8.30 -4 1 0 151.18 6.70 -4 1 0 160.38 7.60 -4 1 0 167.98 6.90 -4 1 0 147.19 7.10 4 1 0 154.88 7.50 4 1 0 164.68 7.00 -5 -1 0 153.18 7.80 5 -1 0 152.78 7.80 -5 -1 0 143.89 8.10 5 -1 0 152.58 7.20 5 -1 0 147.89 7.90 5 -1 0 145.99 8.90 -5 -1 0 146.19 7.20 -5 -1 0 140.39 6.70 5 -1 0 149.88 6.70 -5 1 0 147.29 8.40 5 1 0 148.79 8.80 5 1 0 141.09 7.90 5 1 0 149.79 7.20 -5 1 0 138.59 7.50 -5 1 0 152.08 7.80 5 1 0 151.28 7.80 -5 1 0 151.08 7.20 -5 1 0 133.69 6.70 6 -1 0 15.70 3.60 6 -1 0 7.40 4.30 -6 -1 0 17.90 3.50 6 -1 0 16.50 4.00 6 -1 0 18.30 4.20 -6 -1 0 12.30 3.40 -6 -1 0 17.10 4.40 -6 -1 0 18.50 3.20 -6 -1 0 14.00 3.70 6 1 0 17.00 4.00 -6 1 0 20.30 3.50 -6 1 0 17.40 3.40 -6 1 0 15.10 3.50 6 1 0 14.30 4.00 -6 1 0 21.60 4.80 6 1 0 14.20 3.50 6 1 0 10.50 4.40 -7 -1 0 1.00 2.90 -7 -1 0 1.50 3.30 7 -1 0 9.80 4.40 7 -1 0 5.70 3.50 -7 -1 0 0.20 4.20 7 -1 0 1.30 4.40 7 1 0 5.60 4.60 7 1 0 3.30 3.70 7 1 0 6.80 3.60 -7 1 0 4.00 3.30 -7 1 0 2.00 2.90 7 1 0 1.30 4.40 -7 1 0 -0.10 3.00 -7 1 0 4.10 4.30 8 -1 0 14.10 5.50 -8 -1 0 19.70 5.00 8 -1 0 3.60 5.80 8 -1 0 20.70 5.10 -8 -1 0 21.00 6.40 -8 -1 0 22.30 5.00 8 1 0 19.90 5.10 8 1 0 12.70 5.40 -8 1 0 32.80 7.40 8 1 0 9.90 5.70 -8 1 0 13.80 4.80 -8 1 0 8.20 3.90 9 -1 0 13.20 7.60 9 -1 0 13.90 7.20 -9 -1 0 21.70 8.00 9 -1 0 20.80 6.00 -9 -1 0 16.30 5.30 -9 -1 0 12.50 5.40 9 1 0 3.50 6.70 -9 1 0 15.80 5.80 9 1 0 20.70 7.30 -9 1 0 14.60 5.50 9 1 0 18.40 5.90 -9 1 0 7.60 5.90 10 -1 0 26.30 8.90 10 -1 0 22.30 7.00 -10 -1 0 34.70 7.80 10 -1 0 33.20 9.90 -10 -1 0 33.40 9.30 -10 1 0 12.00 8.90 10 1 0 36.70 7.70 10 1 0 28.40 9.00 10 1 0 20.20 9.60 -10 1 0 44.80 7.80 0 -2 0 -0.30 0.20 0 -2 0 0.10 0.30 0 -2 0 0.30 0.40 0 2 0 0.10 0.30 0 2 0 0.20 0.20 0 2 0 -0.10 0.40 -1 -2 0 7.90 1.20 -1 -2 0 9.20 1.10 -1 -2 0 4.10 0.80 -1 2 0 0.80 0.70 -1 2 0 0.90 0.70 -2 -2 0 187.28 6.80 2 -2 0 186.48 6.90 -2 -2 0 189.38 7.00 -2 -2 0 182.98 6.70 2 -2 0 200.28 6.70 2 -2 0 192.38 7.50 -2 -2 0 192.18 7.10 2 -2 0 184.48 7.00 -2 -2 0 183.58 6.90 2 -2 0 177.88 6.50 -2 2 0 182.18 6.90 2 2 0 197.38 6.70 -2 2 0 182.58 6.60 2 2 0 197.18 7.10 2 2 0 200.98 7.10 -2 2 0 182.08 7.40 -2 2 0 189.28 6.80 2 2 0 196.48 7.60 -2 2 0 184.08 7.00 2 2 0 187.48 6.60 3 -2 0 417.96 14.20 -3 -2 0 390.36 13.50 3 -2 0 403.86 13.60 -3 -2 0 411.56 14.00 3 -2 0 411.86 14.00 3 -2 0 419.46 13.50 3 -2 0 424.96 15.00 -3 -2 0 414.26 14.10 -3 -2 0 425.46 13.70 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21.40 3.50 6 -2 0 23.20 3.80 -6 -2 0 21.40 3.70 6 -2 0 19.50 5.00 6 -2 0 29.60 4.80 6 -2 0 24.90 4.30 -6 -2 0 19.00 3.90 -6 2 0 24.50 4.00 6 2 0 22.70 4.40 6 2 0 21.10 5.00 -6 2 0 32.30 4.70 6 2 0 23.40 3.80 -6 2 0 27.80 5.20 -6 2 0 26.70 4.60 -6 2 0 24.80 3.90 6 2 0 30.80 4.90 7 -2 0 -2.10 3.30 7 -2 0 9.30 4.40 7 -2 0 0.20 3.40 -7 -2 0 -0.30 4.30 7 -2 0 -1.70 4.30 -7 -2 0 1.80 3.00 -7 -2 0 1.00 3.10 -7 2 0 -2.30 2.80 7 2 0 -0.80 3.30 7 2 0 -0.30 3.90 -7 2 0 2.90 3.20 -7 2 0 5.50 4.40 7 2 0 3.70 3.50 7 2 0 8.20 4.80 -7 2 0 -0.60 3.20 7 2 0 -4.50 3.40 -8 -2 0 21.70 4.90 -8 -2 0 4.40 6.00 -8 -2 0 18.00 5.00 8 -2 0 18.60 5.50 8 -2 0 17.70 6.90 8 -2 0 6.10 5.30 8 -2 0 8.50 4.70 8 2 0 21.80 6.10 -8 2 0 27.10 5.30 -8 2 0 14.60 5.60 8 2 0 10.20 6.00 8 2 0 11.10 4.70 -8 2 0 13.00 4.10 9 -2 0 11.60 5.10 9 -2 0 8.60 7.40 9 -2 0 5.80 5.70 -9 -2 0 10.90 5.20 -9 -2 0 6.60 4.90 -9 -2 0 12.90 6.90 -9 2 0 9.20 5.20 -9 2 0 1.90 6.20 9 2 0 21.40 6.80 9 2 0 12.80 5.80 9 2 0 13.20 7.10 -10 -2 0 3.50 5.80 10 -2 0 14.70 9.00 10 -2 0 3.00 5.90 -10 -2 0 12.10 7.30 10 -2 0 16.40 8.30 10 2 0 1.50 8.00 10 2 0 4.00 5.40 -10 2 0 15.10 9.50 10 2 0 -3.70 6.80 -10 2 0 -2.30 5.10 0 -3 0 -0.50 0.70 0 -3 0 0.00 0.50 0 -3 0 0.40 0.50 0 -3 0 0.40 0.60 0 3 0 1.40 0.70 0 3 0 0.30 0.40 0 3 0 0.00 0.40 0 3 0 0.30 0.60 0 3 0 0.70 0.70 -1 -3 0 597.54 17.50 -1 -3 0 593.24 17.80 1 -3 0 593.04 17.80 1 -3 0 595.04 17.90 -1 -3 0 581.04 17.90 1 -3 0 563.14 18.10 -1 -3 0 584.54 18.10 1 -3 0 590.14 17.90 -1 -3 0 608.24 17.70 1 -3 0 593.34 17.60 1 3 0 595.04 17.70 -1 3 0 577.24 17.60 -1 3 0 566.54 17.80 -1 3 0 591.64 18.00 1 3 0 577.84 17.80 1 3 0 593.44 18.10 -1 3 0 582.44 17.70 1 3 0 586.54 17.60 1 3 0 601.04 17.90 -1 3 0 579.84 17.80 -2 -3 0 113.79 5.00 -2 -3 0 109.19 4.80 2 -3 0 109.99 5.00 2 -3 0 118.09 5.50 -2 -3 0 110.09 5.00 2 -3 0 115.49 4.70 -2 -3 0 106.49 4.80 2 -3 0 108.59 4.80 2 -3 0 114.79 4.60 -2 -3 0 114.29 4.80 2 3 0 113.89 5.50 -2 3 0 113.69 4.90 -2 3 0 108.99 4.80 2 3 0 114.99 4.60 2 3 0 108.99 4.90 -2 3 0 115.79 5.30 2 3 0 114.29 4.70 -2 3 0 110.59 4.90 2 3 0 111.09 5.00 -2 3 0 110.89 4.60 3 -3 0 32.30 2.70 -3 -3 0 31.90 3.20 -3 -3 0 28.10 3.10 -3 -3 0 29.00 2.80 -3 -3 0 30.40 3.10 3 -3 0 23.20 3.20 3 -3 0 31.40 3.80 3 -3 0 33.10 3.20 3 -3 0 30.90 3.00 -3 -3 0 34.20 3.00 -3 3 0 27.10 2.80 -3 3 0 26.80 3.80 -3 3 0 26.40 3.10 3 3 0 31.50 2.90 3 3 0 35.50 3.00 3 3 0 32.50 3.30 -3 3 0 29.80 3.10 -3 3 0 21.20 3.10 3 3 0 25.40 3.70 3 3 0 34.40 3.40 -4 -3 0 1.30 2.10 4 -3 0 3.70 2.60 4 -3 0 3.10 1.90 4 -3 0 4.60 2.30 -4 -3 0 4.20 2.00 -4 -3 0 1.10 2.10 -4 -3 0 3.20 2.20 4 -3 0 0.80 2.10 -4 -3 0 2.50 1.90 4 -3 0 2.60 2.00 4 3 0 1.10 2.80 -4 3 0 3.70 2.70 4 3 0 3.00 1.90 -4 3 0 1.00 1.60 -4 3 0 0.30 2.10 -4 3 0 4.90 2.10 4 3 0 2.70 2.00 4 3 0 2.90 2.40 -4 3 0 1.10 1.90 4 3 0 2.00 2.30 5 -3 0 11.80 3.20 -5 -3 0 14.90 3.00 -5 -3 0 14.80 3.40 -5 -3 0 14.80 2.90 -5 -3 0 16.60 3.50 5 -3 0 15.90 3.00 5 -3 0 16.40 3.30 5 -3 0 11.80 4.00 -5 -3 0 11.10 3.50 5 -3 0 16.80 2.80 -5 3 0 19.20 3.20 -5 3 0 16.10 3.00 5 3 0 16.40 3.10 5 3 0 16.40 2.90 -5 3 0 15.40 3.20 5 3 0 19.00 3.70 -5 3 0 15.80 3.70 5 3 0 15.30 4.00 5 3 0 17.90 3.40 -5 3 0 17.20 3.40 6 -3 0 13.20 3.70 -6 -3 0 12.20 3.30 6 -3 0 7.50 4.10 -6 -3 0 8.00 3.20 6 -3 0 13.10 3.90 6 -3 0 7.80 2.90 -6 -3 0 10.10 3.80 6 -3 0 14.30 3.10 -6 -3 0 8.60 3.30 -6 -3 0 7.00 2.80 -6 3 0 11.00 3.10 6 3 0 9.90 3.20 -6 3 0 14.90 3.50 6 3 0 6.20 3.50 -6 3 0 9.00 3.40 6 3 0 11.50 3.40 6 3 0 14.30 4.80 6 3 0 12.60 3.80 -6 3 0 12.40 3.30 -6 3 0 14.20 4.70 7 -3 0 80.69 8.10 7 -3 0 66.29 6.90 -7 -3 0 70.89 6.40 7 -3 0 79.79 8.70 7 -3 0 73.99 7.70 -7 -3 0 67.39 6.80 -7 -3 0 78.69 8.20 7 3 0 79.69 6.50 7 3 0 76.79 8.50 -7 3 0 79.29 7.50 -7 3 0 64.49 6.60 7 3 0 86.09 8.00 7 3 0 94.39 8.10 -7 3 0 71.39 6.20 -7 3 0 77.39 6.40 7 3 0 77.19 6.80 -8 -3 0 24.70 5.40 -8 -3 0 25.50 7.00 8 -3 0 32.90 6.00 8 -3 0 35.20 6.30 8 -3 0 33.80 7.90 -8 -3 0 28.50 5.30 8 -3 0 23.00 6.90 -8 3 0 34.70 6.20 -8 3 0 17.60 4.80 -8 3 0 24.20 4.60 -8 3 0 29.00 7.40 8 3 0 29.80 6.60 8 3 0 30.70 5.70 8 3 0 19.70 6.70 9 -3 0 76.19 13.20 9 -3 0 90.89 9.70 9 -3 0 69.39 10.80 -9 -3 0 87.49 8.90 -9 -3 0 87.19 10.80 -9 -3 0 70.99 9.20 9 3 0 85.59 11.50 -9 3 0 88.19 11.60 -9 3 0 80.89 9.10 9 3 0 79.29 8.90 9 3 0 63.29 11.70 10 -3 0 10.90 7.30 10 -3 0 18.60 6.90 -10 -3 0 13.10 8.10 -10 -3 0 16.40 6.90 10 -3 0 6.70 7.90 -10 3 0 10.40 8.80 10 3 0 28.80 7.10 10 3 0 6.20 7.10 -10 3 0 8.90 5.60 10 3 0 8.10 8.60 0 -4 0 11.60 1.30 0 -4 0 11.10 1.90 0 -4 0 12.50 1.50 0 -4 0 11.40 1.50 0 4 0 12.20 1.50 0 4 0 10.00 1.40 0 4 0 10.60 1.70 0 4 0 9.90 1.20 0 4 0 11.50 1.20 0 4 0 10.10 1.60 -1 -4 0 368.96 11.30 -1 -4 0 357.26 11.00 -1 -4 0 341.47 11.20 1 -4 0 338.67 11.40 1 -4 0 354.16 11.40 1 -4 0 339.77 11.10 1 -4 0 349.67 11.20 -1 -4 0 322.17 10.70 1 -4 0 361.36 11.00 -1 -4 0 343.97 11.60 -1 4 0 350.46 10.90 -1 4 0 362.06 11.10 1 4 0 341.27 11.20 1 4 0 346.57 10.90 1 4 0 359.86 11.10 -1 4 0 350.06 11.20 -1 4 0 367.26 11.40 -1 4 0 338.57 11.10 1 4 0 347.97 11.40 1 4 0 343.07 11.10 -2 -4 0 21.50 2.50 -2 -4 0 24.00 2.60 -2 -4 0 24.30 2.70 2 -4 0 18.90 2.80 -2 -4 0 25.30 2.50 2 -4 0 16.40 2.20 -2 -4 0 22.40 2.40 2 -4 0 24.70 2.50 2 -4 0 23.70 2.80 -2 4 0 15.50 2.20 -2 4 0 13.90 2.10 2 4 0 23.20 2.40 -2 4 0 14.10 2.50 -2 4 0 14.80 2.60 -2 4 0 17.10 2.40 2 4 0 22.00 2.40 -3 -4 0 65.49 4.00 3 -4 0 60.99 4.30 3 -4 0 65.39 4.20 3 -4 0 60.79 3.80 -3 -4 0 65.19 4.10 3 -4 0 67.79 3.80 3 -4 0 68.19 5.00 -3 -4 0 66.59 4.30 -3 -4 0 68.59 4.30 -3 -4 0 72.69 4.00 -3 4 0 66.09 4.90 -3 4 0 64.79 4.10 -3 4 0 65.39 4.10 -3 4 0 63.59 3.70 3 4 0 64.89 4.40 3 4 0 70.79 5.00 3 4 0 64.69 3.90 3 4 0 67.99 3.90 3 4 0 62.59 4.20 -3 4 0 69.39 4.40 4 -4 0 37.40 4.10 4 -4 0 35.70 3.40 -4 -4 0 41.20 3.70 -4 -4 0 41.50 4.20 -4 -4 0 35.80 4.20 4 -4 0 41.50 4.80 -4 -4 0 45.40 3.90 -4 -4 0 32.80 4.00 4 -4 0 41.60 3.70 4 -4 0 37.60 3.90 -4 4 0 37.30 4.40 4 4 0 43.20 3.80 -4 4 0 38.00 3.90 4 4 0 35.40 3.40 -4 4 0 36.20 3.90 4 4 0 38.40 4.30 -4 4 0 40.50 4.20 4 4 0 34.10 5.00 4 4 0 36.50 4.30 -4 4 0 40.80 3.50 -5 -4 0 35.20 4.70 5 -4 0 31.70 3.90 5 -4 0 37.40 4.40 -5 -4 0 32.60 4.10 5 -4 0 36.00 3.70 -5 -4 0 41.80 4.70 5 -4 0 36.90 5.40 5 -4 0 36.10 4.80 -5 -4 0 34.00 3.90 -5 -4 0 34.40 4.60 -5 4 0 34.00 5.50 5 4 0 35.40 4.10 -5 4 0 33.90 3.90 5 4 0 33.60 4.10 -5 4 0 38.20 4.40 -5 4 0 35.00 4.40 -5 4 0 36.50 4.50 5 4 0 44.20 4.80 5 4 0 32.70 4.90 5 4 0 31.10 5.30 -6 -4 0 55.69 5.70 6 -4 0 48.20 4.50 6 -4 0 45.00 5.10 -6 -4 0 33.60 5.10 -6 -4 0 50.29 5.10 -6 -4 0 51.79 4.80 6 -4 0 39.80 5.70 -6 -4 0 61.49 6.10 6 -4 0 48.20 6.60 6 -4 0 53.59 5.90 6 4 0 50.49 7.10 -6 4 0 51.29 4.70 6 4 0 45.00 6.20 -6 4 0 43.40 5.50 6 4 0 51.09 5.10 6 4 0 57.69 5.90 6 4 0 48.80 5.00 -6 4 0 49.90 5.30 -6 4 0 45.80 5.90 -6 4 0 44.40 5.20 7 -4 0 66.69 7.50 7 -4 0 52.49 7.70 -7 -4 0 46.70 5.80 -7 -4 0 44.00 6.20 -7 -4 0 48.00 6.90 7 -4 0 48.20 6.10 7 -4 0 49.30 7.10 -7 4 0 48.90 5.50 -7 4 0 47.00 5.70 7 4 0 58.09 7.30 7 4 0 62.99 6.70 7 4 0 63.39 8.70 -7 4 0 49.30 6.00 7 4 0 36.90 5.60 -7 4 0 45.00 6.80 7 4 0 59.59 7.70 -8 -4 0 27.80 5.50 -8 -4 0 26.90 6.30 8 -4 0 29.80 5.70 -8 -4 0 34.40 5.60 8 -4 0 21.70 6.90 8 -4 0 24.60 6.10 8 -4 0 25.80 7.20 -8 4 0 12.10 3.90 -8 4 0 24.90 5.20 -8 4 0 35.00 6.60 -8 4 0 20.00 6.00 8 4 0 18.50 7.10 8 4 0 21.40 5.10 -9 -4 0 23.00 6.80 9 -4 0 37.80 7.90 9 -4 0 32.00 6.60 -9 -4 0 34.50 6.30 9 -4 0 17.60 7.80 -9 -4 0 21.40 6.20 -9 4 0 23.10 5.80 -9 4 0 24.90 7.80 9 4 0 31.10 7.30 9 4 0 23.60 8.50 9 4 0 29.30 6.40 10 -4 0 82.79 10.60 10 -4 0 82.39 13.70 -10 -4 0 79.49 11.10 -10 -4 0 81.09 10.80 10 -4 0 75.09 12.60 10 4 0 78.89 12.00 -10 4 0 64.39 9.60 10 4 0 91.09 10.90 -10 4 0 97.79 13.40 10 4 0 93.59 14.50 0 -5 0 -0.10 1.10 0 -5 0 1.80 1.60 0 -5 0 0.00 1.10 0 -5 0 0.10 1.10 0 5 0 -1.30 0.90 0 5 0 1.10 1.30 0 5 0 2.30 1.50 0 5 0 -1.40 1.00 0 5 0 -0.40 1.10 0 5 0 0.90 0.90 -1 -5 0 192.98 6.60 1 -5 0 190.48 6.80 1 -5 0 192.68 7.10 1 -5 0 177.78 7.00 1 -5 0 187.98 6.70 -1 -5 0 196.88 6.90 1 -5 0 203.78 6.60 -1 -5 0 175.78 6.10 -1 -5 0 203.28 7.50 -1 -5 0 185.88 6.80 -1 5 0 169.98 6.90 1 5 0 186.28 6.70 1 5 0 193.88 6.90 1 5 0 190.98 7.00 1 5 0 189.38 6.50 -1 5 0 183.38 6.90 -1 5 0 180.28 6.60 -1 5 0 180.58 6.40 1 5 0 198.68 6.80 -1 5 0 177.68 6.70 2 -5 0 117.19 5.30 2 -5 0 113.29 4.80 -2 -5 0 114.29 5.20 2 -5 0 115.19 5.10 -2 -5 0 114.29 5.00 2 -5 0 108.29 5.50 -2 -5 0 110.49 5.40 2 -5 0 100.89 4.90 -2 -5 0 111.09 5.20 -2 -5 0 110.19 4.60 -2 5 0 113.09 4.70 2 5 0 113.89 4.90 2 5 0 108.09 5.10 -2 5 0 106.79 5.10 2 5 0 116.49 4.90 -2 5 0 117.99 5.60 -2 5 0 110.89 5.00 2 5 0 112.99 5.20 2 5 0 116.99 5.60 -2 5 0 108.09 5.10 -3 -5 0 16.00 2.70 3 -5 0 18.40 2.80 3 -5 0 19.50 2.90 -3 -5 0 20.90 2.70 3 -5 0 16.20 2.50 3 -5 0 18.10 2.70 -3 -5 0 17.70 3.00 -3 -5 0 15.00 2.70 3 -5 0 19.50 3.50 -3 -5 0 17.20 2.60 3 5 0 19.20 3.30 -3 5 0 18.20 3.00 3 5 0 23.40 3.40 -3 5 0 16.70 3.20 -3 5 0 16.50 2.50 3 5 0 18.20 2.90 3 5 0 15.80 2.60 -3 5 0 20.70 3.20 -3 5 0 17.10 2.50 3 5 0 21.80 3.10 4 -5 0 341.17 12.50 -4 -5 0 344.97 13.00 4 -5 0 356.56 12.40 4 -5 0 357.26 13.30 -4 -5 0 332.07 12.70 -4 -5 0 342.17 13.20 -4 -5 0 359.96 13.20 4 -5 0 357.36 14.20 -4 -5 0 361.76 12.70 4 -5 0 347.57 13.10 4 5 0 341.17 14.10 4 5 0 349.17 13.00 -4 5 0 336.97 12.60 4 5 0 365.86 12.40 4 5 0 349.67 12.60 -4 5 0 363.46 13.40 -4 5 0 361.26 14.10 4 5 0 351.36 13.30 -4 5 0 355.76 12.90 -4 5 0 353.46 12.40 5 -5 0 18.50 3.70 5 -5 0 19.30 4.20 -5 -5 0 20.70 3.70 5 -5 0 20.60 3.30 -5 -5 0 16.10 3.40 -5 -5 0 20.10 3.70 -5 -5 0 18.10 3.20 -5 -5 0 20.00 3.50 5 -5 0 19.90 3.70 5 -5 0 15.10 2.90 -5 5 0 19.30 3.10 5 5 0 19.80 4.70 -5 5 0 15.80 3.50 -5 5 0 24.80 4.60 -5 5 0 14.50 3.20 -5 5 0 16.30 3.30 5 5 0 14.70 3.60 5 5 0 19.10 3.60 5 5 0 16.10 3.00 5 5 0 19.10 3.30 -6 -5 0 2.80 3.30 6 -5 0 9.60 3.50 6 -5 0 4.70 3.90 -6 -5 0 2.30 2.70 -6 -5 0 4.20 3.10 6 -5 0 3.00 2.80 -6 -5 0 4.80 3.20 6 -5 0 6.00 3.50 6 -5 0 5.50 2.70 -6 -5 0 4.20 3.00 6 5 0 8.10 4.50 -6 5 0 1.70 2.60 -6 5 0 4.50 2.60 6 5 0 5.80 3.50 -6 5 0 0.60 2.80 -6 5 0 6.00 4.20 6 5 0 -0.80 3.50 -6 5 0 3.60 3.20 6 5 0 11.30 3.20 6 5 0 3.70 2.90 7 -5 0 43.40 6.90 -7 -5 0 38.20 6.40 -7 -5 0 36.70 5.70 7 -5 0 46.00 6.20 7 -5 0 48.20 8.30 7 -5 0 49.40 7.20 -7 -5 0 40.40 5.80 -7 5 0 54.29 7.10 7 5 0 48.60 5.80 -7 5 0 47.90 5.60 7 5 0 44.50 6.80 7 5 0 43.80 7.90 7 5 0 39.20 6.80 -7 5 0 43.90 5.30 -7 5 0 46.70 6.00 7 5 0 50.19 6.00 8 -5 0 129.49 11.80 8 -5 0 137.89 11.00 -8 -5 0 105.79 8.80 8 -5 0 106.69 9.10 -8 -5 0 125.59 10.00 -8 -5 0 116.39 9.50 8 -5 0 77.39 10.20 -8 5 0 110.79 9.30 8 5 0 114.09 8.80 8 5 0 86.59 13.30 -8 5 0 109.59 8.90 -8 5 0 126.49 10.40 -8 5 0 113.29 7.80 8 5 0 106.49 10.60 9 -5 0 50.59 8.50 -9 -5 0 40.70 8.10 -9 -5 0 45.00 7.80 9 -5 0 37.10 7.20 9 -5 0 36.70 9.20 -9 -5 0 47.90 7.90 9 5 0 54.19 9.00 -9 5 0 43.10 8.00 9 5 0 36.70 7.30 -9 5 0 40.70 8.30 9 5 0 68.09 11.70 10 -5 0 31.70 9.30 -10 -5 0 14.90 9.90 -10 -5 0 23.10 7.30 10 -5 0 18.40 9.40 10 -5 0 26.40 7.40 -10 5 0 23.40 9.20 10 5 0 20.10 6.90 -10 5 0 25.30 6.50 10 5 0 12.00 9.00 10 5 0 24.70 8.60 0 -6 0 1060.19 33.70 0 -6 0 1088.59 32.70 0 -6 0 1071.69 33.00 0 -6 0 1086.19 32.90 0 6 0 1088.99 32.80 0 6 0 1098.99 33.10 0 6 0 1101.39 32.50 0 6 0 1114.99 33.00 0 6 0 1116.89 32.60 0 6 0 1137.09 33.20 1 -6 0 1094.69 32.70 -1 -6 0 1075.09 32.90 -1 -6 0 1033.20 31.40 -1 -6 0 1081.59 31.90 1 -6 0 1047.40 32.10 1 -6 0 1051.19 32.40 1 -6 0 1072.59 31.90 1 -6 0 1056.59 32.10 -1 -6 0 1038.90 32.20 -1 -6 0 1075.59 32.20 -1 6 0 1054.89 32.10 1 6 0 1079.89 32.10 1 6 0 1034.90 32.10 1 6 0 1047.90 32.00 1 6 0 1056.49 32.20 -1 6 0 1067.49 31.70 -1 6 0 1045.20 31.90 -1 6 0 1096.89 32.30 1 6 0 1078.99 31.80 -1 6 0 1118.29 32.40 2 -6 0 46.80 3.50 2 -6 0 40.20 3.70 2 -6 0 49.50 3.20 -2 -6 0 55.39 3.70 2 -6 0 51.89 3.50 2 -6 0 41.60 3.30 -2 -6 0 48.70 2.90 -2 -6 0 53.69 4.00 -2 -6 0 52.39 3.50 -2 -6 0 47.10 3.40 -2 6 0 45.20 3.80 2 6 0 57.29 3.60 -2 6 0 45.00 4.20 -2 6 0 46.60 3.30 2 6 0 53.49 3.70 2 6 0 54.59 3.30 -2 6 0 42.50 3.40 2 6 0 52.99 3.60 -2 6 0 48.70 3.10 2 6 0 53.89 4.00 3 -6 0 4.80 2.00 -3 -6 0 9.40 2.10 3 -6 0 7.40 2.00 -3 -6 0 7.00 2.00 -3 -6 0 5.70 2.00 3 -6 0 7.20 1.90 -3 -6 0 6.60 2.20 -3 -6 0 5.10 1.90 3 -6 0 5.10 2.10 3 -6 0 4.60 2.50 -3 6 0 1.40 1.70 3 6 0 7.60 2.20 -3 6 0 3.60 1.80 3 6 0 9.20 2.00 -3 6 0 2.00 2.00 -3 6 0 4.00 2.40 3 6 0 12.30 2.20 3 6 0 7.50 2.70 -3 6 0 3.50 1.60 4 -6 0 242.98 9.60 -4 -6 0 230.38 9.90 4 -6 0 236.58 9.90 -4 -6 0 233.18 9.60 4 -6 0 246.88 10.30 4 -6 0 236.58 11.00 -4 -6 0 243.58 10.20 4 -6 0 251.77 9.60 -4 -6 0 242.28 10.10 -4 -6 0 249.68 9.70 4 6 0 241.68 11.00 4 6 0 248.08 9.60 -4 6 0 244.98 9.80 -4 6 0 247.68 10.20 4 6 0 254.87 9.60 -4 6 0 236.68 9.80 -4 6 0 250.87 9.40 4 6 0 226.18 10.20 -4 6 0 244.38 10.80 4 6 0 237.88 10.00 5 -6 0 226.48 11.60 5 -6 0 232.98 10.20 -5 -6 0 219.78 10.00 5 -6 0 225.78 9.80 -5 -6 0 220.38 10.00 -5 -6 0 233.88 9.90 -5 -6 0 237.48 10.50 -5 -6 0 214.68 10.30 5 -6 0 238.58 10.70 5 -6 0 228.08 9.40 5 6 0 216.48 9.60 5 6 0 239.48 9.60 -5 6 0 225.58 10.00 5 6 0 226.58 10.40 5 6 0 224.48 11.40 -5 6 0 243.28 11.20 -5 6 0 230.68 9.40 -5 6 0 233.68 10.50 -5 6 0 228.78 9.90 5 6 0 237.68 10.70 -6 -6 0 53.39 5.70 -6 -6 0 48.00 5.30 6 -6 0 48.90 6.10 -6 -6 0 53.39 5.80 6 -6 0 61.29 6.00 -6 -6 0 47.50 5.10 6 -6 0 51.29 6.60 -6 -6 0 43.20 5.40 6 -6 0 50.19 5.20 6 -6 0 41.90 4.70 -6 6 0 53.49 7.00 6 6 0 56.29 5.30 -6 6 0 40.10 5.50 6 6 0 45.40 6.30 6 6 0 55.59 6.20 6 6 0 48.20 7.20 -6 6 0 41.50 4.60 -6 6 0 52.79 5.60 6 6 0 45.80 5.20 -6 6 0 47.30 5.30 -7 -6 0 12.00 4.50 7 -6 0 11.80 5.60 -7 -6 0 15.50 4.20 -7 -6 0 15.10 4.70 7 -6 0 20.40 5.20 7 -6 0 16.50 4.10 7 -6 0 22.00 4.90 -7 -6 0 5.10 3.60 7 6 0 13.90 4.10 7 6 0 13.20 4.10 7 6 0 22.80 6.10 -7 6 0 15.30 4.30 7 6 0 17.60 5.20 -7 6 0 10.90 4.10 -7 6 0 9.50 3.50 -7 6 0 15.00 5.00 7 6 0 15.60 4.60 -8 -6 0 6.00 4.60 8 -6 0 1.50 5.90 -8 -6 0 4.60 4.20 8 -6 0 13.60 5.80 8 -6 0 18.00 6.00 -8 -6 0 3.10 4.50 8 -6 0 13.10 4.70 -8 6 0 2.90 5.10 8 6 0 7.20 4.50 -8 6 0 10.40 5.40 -8 6 0 11.90 3.90 -8 6 0 2.70 4.10 8 6 0 8.00 5.10 8 6 0 8.40 6.40 9 -6 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3.10 2 -7 0 29.40 3.50 -2 -7 0 32.00 3.70 2 -7 0 28.60 3.10 2 -7 0 31.10 3.20 -2 -7 0 31.00 3.20 2 -7 0 28.90 3.00 2 7 0 30.50 2.80 -2 7 0 27.00 3.00 -2 7 0 22.70 3.20 -2 7 0 25.40 3.70 2 7 0 31.70 3.20 -2 7 0 26.50 3.00 2 7 0 30.20 3.20 2 7 0 32.80 3.60 2 7 0 31.80 3.30 -2 7 0 24.70 2.50 -3 -7 0 187.48 7.60 -3 -7 0 184.58 8.20 -3 -7 0 185.78 7.80 3 -7 0 165.98 7.80 -3 -7 0 180.78 7.20 -3 -7 0 171.58 7.80 3 -7 0 172.98 7.60 3 -7 0 183.58 8.50 3 -7 0 182.48 7.40 3 -7 0 180.78 7.70 3 7 0 186.08 7.50 3 7 0 177.08 7.80 -3 7 0 190.38 7.90 3 7 0 181.28 7.40 3 7 0 182.68 8.00 -3 7 0 183.58 7.60 3 7 0 174.78 8.40 -3 7 0 191.08 8.70 -3 7 0 181.18 7.90 -3 7 0 181.28 7.10 4 -7 0 729.63 24.20 4 -7 0 696.53 23.40 -4 -7 0 726.43 24.10 -4 -7 0 712.33 23.50 -4 -7 0 722.03 23.70 4 -7 0 688.83 23.40 4 -7 0 736.13 24.20 -4 -7 0 725.33 24.00 -4 -7 0 719.23 24.30 4 -7 0 723.73 25.20 4 7 0 729.23 23.40 -4 7 0 758.32 25.10 -4 7 0 735.73 23.70 -4 7 0 741.23 23.20 4 7 0 710.53 24.10 4 7 0 723.73 23.90 -4 7 0 724.83 24.10 -4 7 0 725.53 23.70 4 7 0 733.43 23.30 4 7 0 714.83 25.00 -5 -7 0 3.80 2.70 5 -7 0 13.10 2.90 5 -7 0 5.90 2.50 -5 -7 0 5.00 2.90 5 -7 0 14.70 3.30 -5 -7 0 9.40 3.10 5 -7 0 9.00 3.10 -5 -7 0 8.80 3.00 5 -7 0 2.70 3.40 -5 -7 0 8.40 2.90 -5 7 0 7.40 3.30 5 7 0 3.90 3.80 5 7 0 3.70 2.90 -5 7 0 2.80 3.50 5 7 0 5.80 2.60 -5 7 0 6.10 2.60 -5 7 0 2.50 2.10 5 7 0 3.30 3.20 5 7 0 3.40 2.70 -5 7 0 7.00 3.00 -6 -7 0 251.37 11.50 -6 -7 0 235.38 11.70 -6 -7 0 246.68 11.30 6 -7 0 270.77 12.40 -6 -7 0 245.18 11.10 6 -7 0 255.37 12.00 6 -7 0 234.28 12.80 6 -7 0 250.47 10.80 6 -7 0 225.18 11.00 -6 -7 0 244.78 11.60 6 7 0 259.87 10.90 -6 7 0 243.48 11.20 -6 7 0 234.98 10.40 -6 7 0 278.37 15.40 6 7 0 244.58 12.90 6 7 0 245.18 11.90 6 7 0 243.38 11.00 -6 7 0 251.47 13.00 -6 7 0 244.88 11.00 6 7 0 265.47 12.30 -7 -7 0 90.69 7.70 -7 -7 0 83.69 7.50 7 -7 0 81.99 8.80 7 -7 0 66.69 8.60 7 -7 0 83.69 8.70 -7 -7 0 80.19 7.60 7 -7 0 86.79 7.40 -7 -7 0 102.89 8.00 7 7 0 80.99 7.20 7 7 0 104.79 8.60 -7 7 0 91.39 7.40 -7 7 0 100.39 8.80 -7 7 0 84.29 7.30 -7 7 0 90.99 6.50 7 7 0 78.59 8.40 7 7 0 106.29 7.60 7 7 0 90.49 8.70 -8 -7 0 14.80 5.10 8 -7 0 23.90 7.00 8 -7 0 10.50 4.80 -8 -7 0 18.80 5.50 -8 -7 0 17.70 5.20 8 -7 0 6.40 5.40 8 -7 0 9.30 6.70 -8 7 0 14.60 4.80 8 7 0 16.50 5.50 -8 7 0 9.70 4.10 8 7 0 2.20 5.80 -8 7 0 14.80 5.40 -8 7 0 21.40 6.50 8 7 0 11.50 5.00 9 -7 0 6.90 6.30 -9 -7 0 17.80 6.00 -9 -7 0 9.00 6.40 -9 -7 0 15.90 6.20 9 -7 0 12.10 8.10 9 -7 0 8.40 5.70 -9 7 0 2.00 6.10 9 7 0 -7.70 5.90 -9 7 0 8.00 5.10 9 7 0 20.80 6.80 9 7 0 14.20 6.00 10 -7 0 3.40 6.20 -10 -7 0 0.70 6.20 10 -7 0 1.20 8.80 -10 -7 0 4.70 8.70 10 -7 0 14.20 7.90 10 7 0 -0.60 6.20 10 7 0 -4.80 6.00 10 7 0 -13.90 6.50 -10 7 0 11.20 7.10 -10 7 0 -1.20 5.20 0 -8 0 8.50 2.10 0 -8 0 14.20 3.20 0 -8 0 11.30 2.20 0 -8 0 16.50 2.80 0 8 0 11.10 2.60 0 8 0 7.80 2.00 0 8 0 6.30 2.30 0 8 0 8.70 1.90 0 8 0 8.50 1.70 0 8 0 11.10 1.90 -1 -8 0 176.08 8.00 1 -8 0 163.18 6.60 1 -8 0 164.68 7.10 -1 -8 0 164.28 7.00 1 -8 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9.60 4 -8 0 225.88 9.50 -4 -8 0 222.78 10.20 -4 -8 0 225.88 10.10 -4 -8 0 226.38 9.40 4 -8 0 229.88 11.00 4 -8 0 234.28 9.60 -4 -8 0 244.88 10.20 4 -8 0 233.48 9.90 -4 8 0 232.78 9.10 -4 8 0 232.78 9.80 4 8 0 240.08 11.30 4 8 0 237.88 10.10 -4 8 0 231.08 10.00 -4 8 0 236.38 9.80 4 8 0 237.58 9.50 -4 8 0 224.48 10.90 4 8 0 245.08 10.50 4 8 0 228.58 9.40 -5 -8 0 31.00 4.20 5 -8 0 34.60 5.40 -5 -8 0 34.10 4.90 -5 -8 0 29.70 4.70 5 -8 0 32.90 4.90 5 -8 0 33.70 4.30 -5 -8 0 33.60 5.00 5 -8 0 32.90 3.90 5 -8 0 42.00 5.10 -5 -8 0 34.00 4.50 -5 8 0 37.10 5.50 5 8 0 33.60 5.50 5 8 0 34.60 5.00 -5 8 0 34.70 4.80 -5 8 0 40.40 5.10 -5 8 0 41.70 4.70 5 8 0 35.00 4.50 -5 8 0 35.50 3.90 5 8 0 39.20 5.30 5 8 0 34.50 4.50 6 -8 0 134.29 8.80 6 -8 0 112.09 7.50 6 -8 0 119.79 7.40 -6 -8 0 125.09 7.90 6 -8 0 138.99 8.90 6 -8 0 103.79 9.60 -6 -8 0 140.19 8.50 -6 -8 0 138.89 8.40 -6 -8 0 140.99 8.50 -6 -8 0 124.29 8.10 6 8 0 139.59 7.80 -6 8 0 120.69 7.80 -6 8 0 125.99 7.70 6 8 0 125.29 7.80 -6 8 0 118.19 6.90 6 8 0 133.59 8.60 -6 8 0 139.09 9.70 6 8 0 128.89 9.90 6 8 0 124.59 8.70 7 -8 0 126.89 8.80 7 -8 0 125.99 10.60 -7 -8 0 125.69 8.90 7 -8 0 148.99 10.40 -7 -8 0 134.19 9.70 -7 -8 0 122.79 9.20 -7 -8 0 120.39 9.00 7 -8 0 127.39 9.30 7 8 0 106.19 9.70 -7 8 0 133.09 10.00 -7 8 0 139.39 7.80 7 8 0 127.69 9.60 -7 8 0 117.99 8.50 7 8 0 120.59 8.70 7 8 0 143.19 9.00 -7 8 0 136.79 8.70 -8 -8 0 3.10 4.70 8 -8 0 -2.60 4.90 -8 -8 0 4.30 4.80 8 -8 0 0.60 4.60 8 -8 0 6.20 4.60 -8 -8 0 2.30 4.40 8 -8 0 -5.80 5.20 -8 8 0 -2.20 4.40 -8 8 0 6.20 6.40 -8 8 0 -3.50 3.60 8 8 0 0.30 4.50 8 8 0 3.00 5.00 -9 -8 0 77.79 10.10 9 -8 0 61.49 9.30 9 -8 0 69.09 10.50 -9 -8 0 66.19 10.20 9 -8 0 58.39 10.80 -9 -8 0 55.89 9.10 9 8 0 56.19 10.60 9 8 0 80.09 11.40 -9 8 0 56.79 8.50 -9 8 0 55.49 10.40 9 8 0 67.79 9.30 -10 -8 0 11.40 8.40 10 -8 0 -8.90 8.50 -10 -8 0 15.90 7.10 10 -8 0 7.10 6.50 10 -8 0 8.30 7.40 -10 8 0 4.30 8.80 10 8 0 10.20 7.50 -10 8 0 7.70 5.80 10 8 0 -5.20 8.40 10 8 0 0.30 6.50 0 -9 0 2.10 1.80 0 -9 0 1.00 1.80 0 -9 0 1.60 2.40 0 -9 0 0.60 1.70 0 9 0 0.20 1.50 0 9 0 -3.60 1.50 0 9 0 -0.10 1.60 0 9 0 0.40 1.70 0 9 0 -2.00 2.20 0 9 0 0.60 2.10 1 -9 0 331.17 11.70 1 -9 0 314.37 11.70 -1 -9 0 326.77 11.60 1 -9 0 332.27 11.50 -1 -9 0 307.37 11.60 1 -9 0 315.37 11.10 -1 -9 0 314.87 11.20 1 -9 0 296.97 12.20 -1 -9 0 323.77 12.70 -1 9 0 317.87 10.90 -1 9 0 314.47 11.90 1 9 0 334.97 11.80 -1 9 0 335.97 11.60 -1 9 0 317.17 11.20 1 9 0 340.87 11.80 1 9 0 331.27 11.60 1 9 0 328.17 10.50 -1 9 0 322.17 11.50 1 9 0 329.97 11.00 1 9 0 317.37 11.30 -2 -9 0 2.60 1.70 2 -9 0 1.50 2.00 2 -9 0 0.20 1.80 -2 -9 0 5.40 2.50 2 -9 0 -1.10 1.90 -2 -9 0 0.80 1.80 2 -9 0 1.80 1.70 -2 -9 0 2.80 1.30 -2 -9 0 0.80 1.80 -2 9 0 -2.10 2.10 2 9 0 3.00 1.70 2 9 0 1.80 2.00 2 9 0 7.10 2.40 -2 9 0 0.20 1.70 -2 9 0 -2.50 1.50 -2 9 0 0.70 1.40 2 9 0 4.50 2.50 -2 9 0 2.50 2.50 2 9 0 3.20 2.00 3 -9 0 12.00 2.70 3 -9 0 17.30 2.70 3 -9 0 10.80 2.70 3 -9 0 13.00 3.10 -3 -9 0 12.40 2.80 -3 -9 0 11.10 2.50 -3 -9 0 8.70 2.00 -3 -9 0 14.30 2.80 3 -9 0 11.90 2.70 -3 -9 0 14.80 3.20 3 9 0 8.30 2.80 -3 9 0 10.50 2.10 3 9 0 9.20 3.20 3 9 0 11.80 2.80 -3 9 0 9.10 2.30 -3 9 0 8.60 2.50 3 9 0 9.60 2.20 3 9 0 9.60 2.60 -3 9 0 10.30 2.90 -3 9 0 9.50 3.50 4 -9 0 145.49 8.00 -4 -9 0 154.38 8.00 -4 -9 0 148.89 8.10 4 -9 0 150.48 7.50 -4 -9 0 158.98 7.70 4 -9 0 153.58 7.40 4 -9 0 161.98 7.90 4 -9 0 148.09 8.80 -4 -9 0 163.38 8.20 -4 -9 0 152.38 7.20 -4 9 0 149.69 7.90 4 9 0 154.98 8.20 -4 9 0 152.98 7.90 -4 9 0 155.98 7.60 -4 9 0 159.58 7.10 4 9 0 161.08 7.60 4 9 0 156.38 7.30 4 9 0 151.88 7.90 -4 9 0 161.68 9.00 4 9 0 159.88 8.80 5 -9 0 33.70 4.30 -5 -9 0 27.50 4.30 5 -9 0 21.40 4.80 5 -9 0 31.00 4.90 -5 -9 0 25.60 4.60 5 -9 0 38.70 5.10 -5 -9 0 30.00 4.80 -5 -9 0 26.00 4.70 5 -9 0 22.00 4.00 -5 -9 0 26.50 4.40 5 9 0 25.70 4.30 -5 9 0 27.10 4.40 5 9 0 27.10 5.30 -5 9 0 26.10 3.60 5 9 0 25.20 4.70 5 9 0 34.10 4.70 5 9 0 23.90 4.50 -5 9 0 26.70 4.30 -5 9 0 27.20 5.10 -5 9 0 29.70 4.70 6 -9 0 86.99 7.30 -6 -9 0 92.59 7.40 -6 -9 0 85.39 7.30 6 -9 0 73.59 6.30 6 -9 0 89.19 8.20 -6 -9 0 78.59 6.90 -6 -9 0 72.59 6.60 -6 -9 0 92.79 7.20 6 -9 0 91.39 7.60 6 -9 0 84.69 6.60 6 9 0 91.99 7.70 6 9 0 93.59 6.60 -6 9 0 82.49 5.80 6 9 0 87.89 8.50 6 9 0 99.09 6.90 -6 9 0 86.19 6.60 -6 9 0 101.79 7.20 6 9 0 84.59 7.50 -6 9 0 82.19 7.80 -7 -9 0 35.10 5.90 7 -9 0 31.30 5.70 -7 -9 0 27.90 5.60 -7 -9 0 38.90 5.90 7 -9 0 35.70 7.60 7 -9 0 28.30 5.20 7 -9 0 30.40 6.10 -7 -9 0 42.90 7.10 7 9 0 36.90 6.10 -7 9 0 31.90 4.80 -7 9 0 40.40 6.10 7 9 0 38.60 6.60 7 9 0 41.40 6.30 -7 9 0 32.30 7.10 7 9 0 23.50 6.30 -7 9 0 34.90 6.00 -8 -9 0 28.40 6.60 8 -9 0 21.40 8.20 8 -9 0 46.20 10.00 8 -9 0 42.20 6.80 -8 -9 0 32.70 6.50 -8 -9 0 32.90 7.70 8 -9 0 29.00 6.80 -8 9 0 32.40 8.00 8 9 0 33.60 7.00 8 9 0 31.80 6.10 -8 9 0 27.30 5.50 -8 9 0 37.00 7.50 8 9 0 16.50 7.20 -9 -9 0 13.80 6.10 9 -9 0 21.40 7.40 9 -9 0 18.30 8.40 -9 -9 0 14.20 6.00 -9 -9 0 13.90 6.90 9 -9 0 17.20 6.20 9 9 0 18.00 9.30 -9 9 0 11.70 7.50 -9 9 0 20.20 5.80 9 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4 13 0 50.59 5.30 -5 -13 0 150.08 9.20 5 -13 0 162.68 9.10 -5 -13 0 161.58 9.60 -5 -13 0 163.88 8.80 5 -13 0 161.38 8.80 5 -13 0 162.58 10.20 5 -13 0 162.08 9.50 -5 -13 0 168.88 8.10 5 -13 0 181.78 10.00 -5 -13 0 155.78 10.20 -5 13 0 160.38 7.70 -5 13 0 151.78 8.50 5 13 0 173.78 9.90 -5 13 0 148.19 10.50 5 13 0 160.58 8.40 5 13 0 152.18 9.10 -5 13 0 148.79 9.50 5 13 0 161.98 10.40 5 13 0 158.18 9.00 -6 -13 0 396.36 17.90 6 -13 0 406.46 17.60 -6 -13 0 400.16 16.80 6 -13 0 434.56 19.30 -6 -13 0 423.26 16.10 -6 -13 0 420.26 17.90 6 -13 0 422.06 16.90 6 -13 0 412.76 16.60 6 -13 0 412.46 17.80 -6 -13 0 418.06 18.50 6 13 0 437.86 19.00 6 13 0 407.56 16.50 -6 13 0 425.26 19.20 6 13 0 401.46 17.30 -6 13 0 421.16 17.40 6 13 0 406.96 16.30 -6 13 0 376.66 15.00 -6 13 0 404.66 16.30 7 -13 0 329.77 18.50 -7 -13 0 350.26 15.60 7 -13 0 332.77 15.50 -7 -13 0 313.57 16.40 7 -13 0 356.76 16.90 -7 -13 0 307.37 15.60 7 -13 0 352.66 17.50 -7 -13 0 328.87 16.90 7 13 0 346.17 16.70 7 13 0 351.96 16.00 -7 13 0 335.87 16.00 7 13 0 363.16 15.40 -7 13 0 351.96 17.60 7 13 0 339.07 17.60 -7 13 0 351.26 15.00 8 -13 0 109.09 11.50 -8 -13 0 107.59 11.20 8 -13 0 129.09 10.50 -8 -13 0 99.19 10.10 8 -13 0 120.19 12.40 -8 13 0 132.69 12.70 8 13 0 92.49 12.20 8 13 0 114.29 11.40 -8 13 0 117.09 11.00 8 13 0 122.49 10.20 -8 13 0 111.99 9.30 -9 -13 0 112.29 11.40 9 -13 0 112.69 11.40 9 -13 0 96.59 13.30 -9 -13 0 96.69 11.80 9 -13 0 94.19 12.80 9 13 0 107.89 11.00 -9 13 0 114.19 13.70 -9 13 0 107.69 9.80 9 13 0 108.69 14.10 9 13 0 102.79 13.00 10 -13 0 44.20 10.60 10 -13 0 25.60 10.80 -10 -13 0 29.60 8.50 10 -13 0 38.20 8.30 -10 13 0 21.20 6.10 10 13 0 29.90 8.90 -10 13 0 24.60 10.30 10 13 0 20.40 11.70 0 -14 0 40.00 5.70 0 -14 0 34.40 4.30 0 -14 0 27.30 4.40 0 -14 0 28.80 4.10 0 14 0 33.20 5.10 0 14 0 43.80 4.80 0 14 0 36.50 3.60 0 14 0 32.40 4.70 0 14 0 32.00 3.80 0 14 0 39.40 4.20 1 -14 0 38.30 4.70 1 -14 0 41.20 5.60 1 -14 0 46.10 4.40 -1 -14 0 50.09 4.80 -1 -14 0 52.09 4.90 -1 -14 0 55.89 4.90 -1 -14 0 52.49 6.20 1 -14 0 41.80 4.60 -1 14 0 41.80 4.90 1 14 0 48.60 5.20 1 14 0 50.29 4.20 -1 14 0 39.30 4.30 -1 14 0 36.20 5.50 -1 14 0 40.80 3.80 -1 14 0 46.30 4.40 1 14 0 51.59 3.80 1 14 0 45.90 5.60 1 14 0 47.20 5.00 1 14 0 48.00 4.70 2 -14 0 211.98 9.70 2 -14 0 192.18 9.40 -2 -14 0 209.18 9.40 2 -14 0 215.48 9.20 2 -14 0 218.78 10.10 2 -14 0 193.28 10.50 -2 -14 0 226.38 10.10 -2 -14 0 220.18 11.50 -2 -14 0 212.88 9.80 2 14 0 210.58 9.30 2 14 0 213.18 9.70 -2 14 0 202.18 9.80 2 14 0 226.18 8.90 -2 14 0 200.88 10.10 -2 14 0 203.48 9.70 2 14 0 208.08 8.00 2 14 0 206.78 9.90 -2 14 0 213.88 8.50 -2 14 0 212.58 9.10 2 14 0 215.48 10.00 3 -14 0 141.79 7.90 3 -14 0 153.18 8.70 3 -14 0 147.79 7.40 -3 -14 0 133.39 6.10 3 -14 0 137.19 8.30 -3 -14 0 142.89 7.70 3 -14 0 149.59 8.10 -3 -14 0 134.49 9.40 -3 -14 0 143.99 8.10 -3 -14 0 142.79 7.90 3 14 0 135.39 7.10 -3 14 0 147.39 8.80 -3 14 0 145.39 6.80 -3 14 0 136.99 8.30 3 14 0 135.89 8.40 -3 14 0 145.19 8.00 3 14 0 141.19 8.00 3 14 0 140.49 8.10 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7.90 -4 -19 0 104.39 8.80 4 -19 0 87.09 7.20 4 -19 0 82.89 8.20 4 -19 0 88.59 8.50 4 -19 0 91.79 8.00 -4 -19 0 76.89 9.40 -4 19 0 88.99 5.70 4 19 0 78.69 8.20 -4 19 0 82.59 8.40 -4 19 0 68.79 8.40 4 19 0 95.59 9.00 4 19 0 84.39 7.50 4 19 0 78.89 6.90 -4 19 0 77.49 6.70 -5 -19 0 22.00 5.30 5 -19 0 21.40 5.50 -5 -19 0 31.00 6.10 5 -19 0 23.10 5.10 5 -19 0 27.60 6.20 -5 -19 0 29.00 7.30 -5 -19 0 22.90 5.50 5 -19 0 18.10 5.20 5 -19 0 29.60 6.30 -5 19 0 19.10 6.30 -5 19 0 27.90 6.80 -5 19 0 17.50 4.50 5 19 0 21.20 6.80 5 19 0 25.90 5.00 5 19 0 21.80 6.00 5 19 0 21.80 5.40 -6 -19 0 0.30 4.80 6 -19 0 0.40 4.80 -6 -19 0 1.60 6.80 6 -19 0 0.60 4.20 6 -19 0 -1.60 4.90 -6 -19 0 5.10 5.10 6 -19 0 4.10 5.90 -6 19 0 -12.50 6.30 -6 19 0 -1.40 6.20 6 19 0 1.10 4.30 6 19 0 -1.70 4.70 6 19 0 4.50 5.70 6 19 0 -11.10 5.10 -6 19 0 2.40 4.10 -7 -19 0 16.10 6.50 7 -19 0 23.20 6.10 7 -19 0 8.60 7.00 -7 -19 0 30.00 7.00 7 -19 0 24.00 7.50 -7 -19 0 4.00 8.00 -7 19 0 11.40 8.20 7 19 0 14.20 5.50 7 19 0 23.50 6.90 7 19 0 12.70 7.60 -7 19 0 36.40 8.00 -7 19 0 12.20 4.70 8 -19 0 11.80 6.10 8 -19 0 -0.10 6.70 -8 -19 0 3.70 7.30 -8 -19 0 6.50 6.60 8 -19 0 6.60 7.90 -8 19 0 4.30 4.70 -8 19 0 9.40 9.30 8 19 0 -1.50 7.90 -8 19 0 2.50 8.50 8 19 0 0.20 6.20 -9 -19 0 -11.50 6.50 9 -19 0 4.00 8.60 -9 -19 0 -3.50 7.30 9 -19 0 5.50 6.20 9 -19 0 9.30 8.00 -9 19 0 5.50 9.90 -9 19 0 0.40 6.50 9 19 0 1.10 7.70 9 19 0 0.50 7.50 0 -20 0 189.18 11.70 0 -20 0 175.88 9.10 0 -20 0 162.98 9.80 0 -20 0 166.88 9.40 0 20 0 171.28 8.70 0 20 0 171.78 9.10 0 20 0 193.78 12.20 0 20 0 163.48 8.00 0 20 0 180.08 10.40 0 20 0 166.98 10.60 -1 -20 0 36.20 5.80 -1 -20 0 45.70 7.10 1 -20 0 25.50 4.80 -1 -20 0 45.70 6.30 1 -20 0 35.90 5.30 -1 -20 0 26.80 4.50 1 -20 0 41.10 5.80 1 -20 0 44.80 6.90 1 20 0 33.20 6.40 -1 20 0 41.40 5.30 1 20 0 42.30 4.60 1 20 0 40.40 5.50 1 20 0 31.10 4.20 1 20 0 36.80 6.30 1 20 0 43.30 6.80 -1 20 0 35.40 4.30 -1 20 0 38.50 6.20 -1 20 0 38.20 5.60 2 -20 0 35.70 5.50 2 -20 0 29.10 4.70 -2 -20 0 41.30 7.50 -2 -20 0 31.60 4.90 2 -20 0 33.40 5.30 2 -20 0 30.00 5.20 -2 -20 0 28.00 5.40 2 -20 0 30.00 6.30 -2 -20 0 32.20 5.40 2 20 0 25.50 5.80 -2 20 0 29.30 4.10 2 20 0 34.10 5.80 -2 20 0 32.60 5.50 2 20 0 30.80 4.90 2 20 0 34.00 5.70 -2 20 0 39.40 6.90 -2 20 0 26.60 4.90 2 20 0 29.40 6.20 3 -20 0 51.39 6.80 3 -20 0 46.10 6.80 -3 -20 0 39.90 7.40 3 -20 0 40.40 7.30 -3 -20 0 42.60 6.30 3 -20 0 36.90 5.70 -3 -20 0 46.70 7.10 -3 -20 0 47.00 6.60 -3 20 0 46.10 4.70 -3 20 0 45.50 6.90 3 20 0 51.69 5.80 3 20 0 47.10 7.10 3 20 0 49.40 6.60 3 20 0 57.09 7.40 -3 20 0 45.90 5.70 -3 20 0 44.80 7.00 -4 -20 0 87.29 8.30 -4 -20 0 118.19 9.30 4 -20 0 107.59 8.00 -4 -20 0 120.49 9.40 4 -20 0 102.29 9.20 4 -20 0 106.79 9.00 4 -20 0 120.09 9.70 -4 -20 0 93.69 10.50 4 -20 0 119.89 9.20 4 20 0 102.79 9.60 -4 20 0 93.59 9.20 -4 20 0 113.69 9.50 4 20 0 110.19 8.80 4 20 0 108.49 7.50 4 20 0 96.59 8.20 -4 20 0 85.79 7.30 -5 -20 0 6.20 4.70 5 -20 0 8.40 5.60 5 -20 0 -1.40 4.10 5 -20 0 1.90 3.90 -5 -20 0 3.80 4.80 5 -20 0 -0.50 4.20 -5 -20 0 -5.80 6.20 -5 -20 0 1.10 4.40 5 -20 0 -1.00 4.70 -5 20 0 12.20 6.10 5 20 0 1.90 4.80 5 20 0 -0.60 5.30 -5 20 0 1.80 3.80 -5 20 0 -11.00 4.90 5 20 0 6.90 5.90 5 20 0 3.40 4.20 -6 -20 0 2.60 5.60 6 -20 0 -1.10 5.20 6 -20 0 9.30 5.30 -6 -20 0 5.90 5.20 -6 -20 0 10.80 7.90 6 -20 0 3.00 4.60 6 -20 0 1.20 6.10 -6 20 0 0.60 7.00 6 20 0 13.30 7.50 -6 20 0 4.30 4.20 6 20 0 10.50 5.60 6 20 0 -4.70 6.10 6 20 0 4.30 4.70 -6 20 0 0.70 7.40 -7 -20 0 6.50 6.40 -7 -20 0 5.40 6.00 7 -20 0 -4.90 6.10 7 -20 0 1.30 6.40 7 -20 0 0.30 5.20 -7 -20 0 -6.80 7.70 -7 20 0 -0.10 4.10 7 20 0 4.90 6.00 7 20 0 -17.40 6.70 -7 20 0 11.40 8.30 7 20 0 0.20 4.90 -7 20 0 -0.10 6.30 -8 -20 0 -3.40 6.20 8 -20 0 -1.70 5.50 -8 -20 0 6.80 6.80 8 -20 0 -14.90 6.00 8 -20 0 -1.30 7.60 8 20 0 -3.50 9.30 8 20 0 -2.00 6.20 -8 20 0 4.30 4.50 -8 20 0 -0.60 9.10 -8 20 0 -10.40 8.30 9 -20 0 1.30 6.20 9 -20 0 4.30 8.70 -9 -20 0 6.50 8.40 -9 -20 0 5.20 7.70 9 20 0 10.30 7.70 -9 20 0 -10.40 9.40 9 20 0 16.50 10.90 0 -21 0 0.80 3.30 0 -21 0 7.70 3.50 0 -21 0 2.70 4.70 0 -21 0 6.20 3.80 0 21 0 7.10 3.50 0 21 0 -2.40 4.50 0 21 0 1.80 2.80 0 21 0 0.70 5.20 0 21 0 1.70 3.30 1 -21 0 315.57 13.90 -1 -21 0 279.47 15.40 -1 -21 0 283.37 13.70 1 -21 0 288.37 12.70 1 -21 0 295.87 15.40 -1 -21 0 277.27 13.30 1 -21 0 292.77 13.80 1 21 0 251.47 13.80 -1 21 0 277.37 12.60 -1 21 0 263.57 14.20 1 21 0 297.37 11.60 -1 21 0 287.97 12.30 1 21 0 293.27 13.80 -1 21 0 306.67 11.40 1 21 0 275.77 12.40 1 21 0 276.67 11.40 -2 -21 0 60.79 7.20 -2 -21 0 44.20 8.20 2 -21 0 45.20 7.50 -2 -21 0 54.79 6.30 2 -21 0 58.19 7.30 2 -21 0 49.50 6.10 2 -21 0 59.19 7.20 2 -21 0 49.80 6.60 -2 -21 0 49.80 7.00 -2 21 0 63.89 8.40 2 21 0 43.10 6.90 2 21 0 49.00 6.40 2 21 0 47.60 5.50 2 21 0 51.79 7.50 -2 21 0 51.49 6.50 -2 21 0 53.19 4.80 -2 21 0 51.39 5.80 -3 -21 0 172.68 11.00 3 -21 0 155.08 9.40 3 -21 0 161.58 10.70 -3 -21 0 163.48 10.70 3 -21 0 173.38 11.60 -3 -21 0 156.78 9.80 3 -21 0 185.78 10.90 -3 -21 0 173.58 12.70 -3 21 0 156.68 9.10 -3 21 0 165.68 10.80 3 21 0 153.58 10.70 3 21 0 166.18 9.70 -3 21 0 121.39 10.60 -3 21 0 160.98 8.10 3 21 0 207.28 12.20 3 21 0 165.18 8.90 -4 -21 0 19.60 5.50 4 -21 0 17.80 4.70 -4 -21 0 13.90 5.30 -4 -21 0 19.00 5.50 4 -21 0 22.40 6.10 4 -21 0 16.40 5.40 -4 -21 0 13.40 7.10 4 -21 0 15.00 5.20 4 -21 0 19.00 5.20 4 21 0 11.00 4.90 -4 21 0 6.50 5.50 -4 21 0 17.50 4.40 -4 21 0 24.40 6.70 4 21 0 11.90 6.50 4 21 0 16.20 4.50 4 21 0 23.90 6.30 5 -21 0 2.30 4.20 5 -21 0 6.40 5.00 -5 -21 0 5.40 4.90 5 -21 0 11.50 5.70 -5 -21 0 7.30 5.10 5 -21 0 6.00 5.60 5 -21 0 6.90 5.20 -5 -21 0 0.50 6.60 5 21 0 4.20 6.10 -5 21 0 2.10 3.90 -5 21 0 0.20 5.70 5 21 0 5.20 4.90 -5 21 0 14.60 7.00 5 21 0 9.60 5.70 5 21 0 6.50 4.40 6 -21 0 3.10 6.00 6 -21 0 11.40 6.30 -6 -21 0 4.90 5.80 -6 -21 0 -2.60 7.80 6 -21 0 4.00 4.70 -6 -21 0 3.20 5.20 6 -21 0 0.00 5.10 6 21 0 7.20 7.00 6 21 0 9.20 5.60 -6 21 0 1.40 7.30 6 21 0 -0.10 4.60 -6 21 0 -5.80 7.00 -6 21 0 7.30 4.40 6 21 0 7.70 6.60 -7 -21 0 -1.30 6.00 7 -21 0 -11.40 5.80 7 -21 0 -2.40 7.00 -7 -21 0 -4.20 6.40 7 -21 0 12.70 5.80 -7 -21 0 2.40 8.60 7 21 0 4.70 9.40 -7 21 0 -8.30 6.60 7 21 0 -4.90 5.80 -7 21 0 1.60 4.40 -7 21 0 -3.80 7.10 -8 -21 0 0.40 7.30 8 -21 0 -4.00 7.80 8 -21 0 -6.70 6.60 8 -21 0 1.40 5.60 -8 -21 0 -7.50 6.30 -8 21 0 -3.50 8.80 -8 21 0 -3.80 4.20 8 21 0 -1.20 6.90 -8 21 0 -17.80 7.80 0 -22 0 189.18 12.50 0 -22 0 193.38 11.20 0 -22 0 178.78 10.00 0 -22 0 192.28 10.80 0 22 0 183.88 9.60 0 22 0 189.98 9.90 0 22 0 201.88 11.60 0 22 0 196.68 12.00 0 22 0 181.08 8.70 1 -22 0 36.60 6.50 1 -22 0 29.40 5.40 -1 -22 0 41.60 6.50 1 -22 0 31.50 5.10 -1 -22 0 33.60 7.10 1 -22 0 40.90 7.40 -1 -22 0 32.40 5.80 1 22 0 38.80 5.90 -1 22 0 41.20 6.90 -1 22 0 35.20 5.50 -1 22 0 28.80 4.40 1 22 0 33.00 4.90 -1 22 0 35.80 5.80 1 22 0 32.70 6.70 1 22 0 19.40 5.90 2 -22 0 55.39 7.40 2 -22 0 52.09 8.00 2 -22 0 62.79 6.60 -2 -22 0 67.99 7.70 -2 -22 0 64.29 6.90 -2 -22 0 53.79 8.80 2 -22 0 47.60 7.00 -2 -22 0 61.49 7.30 2 -22 0 63.29 7.30 -2 22 0 53.49 7.40 2 22 0 61.99 6.90 2 22 0 62.49 5.90 -2 22 0 53.89 8.40 2 22 0 60.99 8.00 -2 22 0 57.19 6.20 -2 22 0 66.89 5.10 2 22 0 65.89 8.40 3 -22 0 128.59 8.90 3 -22 0 139.29 10.00 -3 -22 0 137.29 10.20 -3 -22 0 148.59 9.60 -3 -22 0 129.69 12.40 3 -22 0 137.39 10.30 3 -22 0 146.59 11.20 -3 -22 0 137.89 10.20 -3 22 0 141.49 8.70 -3 22 0 129.29 10.60 3 22 0 128.69 11.10 3 22 0 149.29 10.60 3 22 0 132.99 9.40 -3 22 0 134.49 10.90 3 22 0 138.89 8.50 4 -22 0 5.40 4.10 -4 -22 0 -1.90 6.20 -4 -22 0 7.40 4.70 4 -22 0 0.60 4.40 4 -22 0 -1.10 4.70 -4 -22 0 6.30 5.30 4 -22 0 -1.70 4.20 -4 -22 0 0.70 4.70 4 -22 0 -2.90 4.20 -4 22 0 -1.70 5.10 4 22 0 -0.70 5.60 4 22 0 -1.00 4.00 -4 22 0 1.30 3.80 4 22 0 -2.10 4.50 -4 22 0 -1.30 5.90 4 22 0 -1.50 5.50 5 -22 0 52.19 8.40 5 -22 0 47.40 8.40 -5 -22 0 35.40 7.10 5 -22 0 40.80 7.40 5 -22 0 48.40 7.30 -5 -22 0 33.20 9.20 -5 -22 0 46.10 7.50 5 -22 0 50.19 8.80 -5 22 0 58.89 9.30 -5 22 0 41.10 6.60 5 22 0 48.20 7.70 5 22 0 53.99 9.00 5 22 0 38.40 6.50 -5 22 0 40.20 8.80 5 22 0 44.50 8.00 6 -22 0 62.69 10.30 6 -22 0 44.60 8.10 -6 -22 0 60.99 10.00 6 -22 0 60.49 9.80 -6 -22 0 61.89 11.40 -6 -22 0 48.30 8.20 6 -22 0 55.59 8.80 -6 22 0 36.10 9.60 -6 22 0 57.19 7.30 -6 22 0 60.49 9.90 6 22 0 47.50 8.80 6 22 0 46.60 8.30 6 22 0 57.89 10.40 6 22 0 64.99 9.60 7 -22 0 0.70 7.20 -7 -22 0 -11.40 6.20 7 -22 0 -10.10 6.30 -7 -22 0 2.60 9.10 -7 -22 0 0.30 6.40 7 -22 0 -2.70 5.30 -7 22 0 1.70 7.00 7 22 0 12.80 12.00 -7 22 0 -3.30 4.00 7 22 0 -2.70 5.60 -7 22 0 1.20 8.20 -8 -22 0 0.80 7.20 -8 -22 0 -1.70 7.80 8 -22 0 4.60 8.60 8 -22 0 0.40 7.10 8 -22 0 -2.40 5.80 -8 22 0 2.90 9.40 -8 22 0 5.70 9.90 8 22 0 4.70 6.80 0 -23 0 3.90 4.10 0 -23 0 5.70 5.30 0 -23 0 5.40 4.30 0 -23 0 5.90 3.80 0 23 0 4.40 5.30 0 23 0 5.80 3.10 0 23 0 2.60 3.70 0 23 0 -1.50 3.90 0 23 0 5.80 5.60 -1 -23 0 144.99 11.70 1 -23 0 144.29 9.70 1 -23 0 130.69 11.30 1 -23 0 143.69 9.20 -1 -23 0 124.59 9.60 1 -23 0 149.69 10.10 -1 -23 0 142.19 10.10 1 23 0 142.09 7.60 -1 23 0 126.39 8.80 -1 23 0 144.59 8.60 1 23 0 118.79 10.70 -1 23 0 133.59 7.20 -1 23 0 138.29 10.80 1 23 0 120.69 9.80 1 23 0 136.69 8.70 -2 -23 0 9.30 4.20 2 -23 0 -0.60 4.00 2 -23 0 8.20 4.10 -2 -23 0 2.60 4.40 2 -23 0 6.10 4.50 -2 -23 0 6.10 4.60 2 -23 0 8.20 5.60 -2 -23 0 4.60 6.00 2 -23 0 3.80 4.30 -2 23 0 10.20 5.40 2 23 0 -0.60 5.50 2 23 0 4.80 4.30 2 23 0 10.50 3.80 -2 23 0 9.20 3.90 -2 23 0 4.60 5.80 2 23 0 7.50 6.10 -3 -23 0 131.99 9.90 -3 -23 0 111.69 9.00 3 -23 0 122.09 11.10 -3 -23 0 129.49 10.20 3 -23 0 114.79 9.60 -3 -23 0 97.99 11.10 3 -23 0 120.09 8.70 3 -23 0 121.59 10.00 3 23 0 111.29 10.00 3 23 0 120.19 10.90 -3 23 0 118.89 8.30 -3 23 0 105.69 10.60 3 23 0 131.59 8.20 -3 23 0 115.59 9.90 3 23 0 117.49 9.10 -4 -23 0 21.10 5.60 4 -23 0 26.20 6.70 4 -23 0 18.80 5.90 4 -23 0 22.40 6.30 4 -23 0 18.80 5.90 -4 -23 0 14.40 7.80 4 -23 0 18.30 5.20 -4 -23 0 28.80 6.50 -4 -23 0 28.80 6.90 4 23 0 17.40 7.20 4 23 0 23.50 5.80 -4 23 0 25.00 5.10 4 23 0 27.00 7.50 -4 23 0 28.60 7.30 4 23 0 19.90 5.00 -4 23 0 25.70 7.20 5 -23 0 22.90 7.60 -5 -23 0 13.60 6.00 -5 -23 0 20.50 8.80 5 -23 0 18.30 6.10 5 -23 0 18.00 6.40 5 -23 0 10.30 5.00 5 -23 0 13.60 6.10 -5 -23 0 11.80 6.20 5 23 0 10.90 8.30 -5 23 0 16.70 8.00 -5 23 0 14.40 4.70 5 23 0 19.80 6.00 5 23 0 9.30 6.60 5 23 0 22.50 5.40 -5 23 0 24.00 8.20 -6 -23 0 5.40 6.10 6 -23 0 3.90 6.30 -6 -23 0 -4.30 7.50 -6 -23 0 9.40 6.50 6 -23 0 12.20 6.70 6 -23 0 8.50 5.30 -6 23 0 8.50 4.60 6 23 0 9.00 8.40 -6 23 0 3.10 8.10 6 23 0 12.00 7.20 6 23 0 10.70 5.90 -6 23 0 -9.70 7.40 7 -23 0 38.30 9.80 7 -23 0 27.50 9.00 -7 -23 0 34.00 10.60 -7 -23 0 43.10 8.80 7 -23 0 52.49 8.30 -7 -23 0 51.29 9.60 7 23 0 47.50 8.70 -7 23 0 41.40 10.60 -7 23 0 50.59 9.70 -7 23 0 52.19 7.40 7 23 0 39.70 11.20 8 -23 0 12.90 6.90 8 -23 0 6.80 7.90 -8 -23 0 -0.50 7.60 8 -23 0 12.90 9.10 -8 -23 0 13.50 7.90 -8 23 0 10.20 9.30 -8 23 0 11.10 10.20 8 23 0 15.20 7.90 0 -24 0 166.68 11.50 0 -24 0 187.48 10.50 0 -24 0 183.98 11.40 0 -24 0 179.48 12.80 0 24 0 210.78 12.20 0 24 0 198.18 12.90 0 24 0 179.48 10.10 0 24 0 192.18 9.30 -1 -24 0 34.30 6.20 1 -24 0 41.70 6.50 -1 -24 0 50.59 7.80 1 -24 0 43.30 8.10 -1 -24 0 32.80 7.60 1 -24 0 31.80 5.70 1 -24 0 50.59 7.90 1 24 0 36.80 7.40 -1 24 0 35.00 6.00 1 24 0 44.10 6.50 1 24 0 35.80 7.20 1 24 0 43.70 5.30 -1 24 0 39.80 7.60 -1 24 0 38.70 6.20 2 -24 0 200.18 12.20 2 -24 0 183.18 13.30 -2 -24 0 218.68 13.00 2 -24 0 214.98 12.70 -2 -24 0 218.18 14.60 -2 -24 0 208.48 11.50 -2 -24 0 232.08 12.40 2 -24 0 204.18 12.40 2 -24 0 219.68 11.40 2 24 0 215.88 13.40 -2 24 0 190.88 13.10 2 24 0 192.18 13.30 2 24 0 213.38 9.90 -2 24 0 226.08 10.90 2 24 0 213.58 11.50 -2 24 0 218.88 12.30 3 -24 0 192.48 12.40 3 -24 0 204.58 13.90 3 -24 0 195.58 11.20 -3 -24 0 204.58 12.70 -3 -24 0 205.78 12.50 3 -24 0 200.58 12.70 -3 -24 0 164.78 13.70 -3 -24 0 204.78 11.60 3 24 0 192.68 10.00 3 24 0 205.78 13.80 -3 24 0 193.08 12.80 3 24 0 188.28 11.70 3 24 0 201.88 13.20 -3 24 0 207.98 10.70 -3 24 0 185.78 13.20 4 -24 0 102.79 10.30 -4 -24 0 104.39 9.70 4 -24 0 90.99 10.00 4 -24 0 111.99 10.20 -4 -24 0 97.89 10.70 4 -24 0 104.79 10.60 -4 -24 0 92.19 11.90 4 -24 0 106.69 8.90 -4 24 0 107.39 10.50 4 24 0 100.49 10.80 4 24 0 122.19 11.60 4 24 0 108.39 8.80 -4 24 0 91.69 10.30 -4 24 0 106.09 8.20 4 24 0 99.39 9.10 5 -24 0 29.00 7.10 -5 -24 0 15.50 6.30 5 -24 0 13.20 5.50 5 -24 0 26.40 7.90 5 -24 0 15.20 6.80 -5 -24 0 26.10 6.40 5 -24 0 16.90 6.50 -5 -24 0 25.10 8.80 5 24 0 25.60 9.40 5 24 0 20.60 8.20 -5 24 0 16.80 5.00 -5 24 0 18.50 7.50 -5 24 0 12.20 8.00 5 24 0 18.90 6.20 -6 -24 0 -10.20 6.10 6 -24 0 1.70 6.40 6 -24 0 1.00 6.40 -6 -24 0 1.50 8.20 6 -24 0 4.70 5.60 -6 -24 0 10.40 6.30 -6 24 0 -3.70 7.10 6 24 0 22.80 8.10 6 24 0 12.10 9.70 -6 24 0 -1.80 7.80 6 24 0 12.30 6.40 -6 24 0 11.90 4.70 7 -24 0 11.00 7.90 -7 -24 0 14.90 7.90 -7 -24 0 23.60 7.90 -7 -24 0 0.00 8.70 7 -24 0 18.10 6.90 7 -24 0 20.20 8.40 7 24 0 15.90 7.40 -7 24 0 14.70 5.30 -7 24 0 22.00 9.40 7 24 0 6.20 9.80 -7 24 0 22.00 10.10 -8 -24 0 35.80 10.60 8 -24 0 29.20 8.00 8 -24 0 28.50 10.00 8 -24 0 39.30 9.90 -8 -24 0 23.50 8.80 8 24 0 32.80 9.40 -8 24 0 34.00 11.50 -8 24 0 30.60 11.70 0 -25 0 12.60 5.30 0 -25 0 8.80 4.50 0 -25 0 -0.70 4.80 0 -25 0 7.80 5.70 0 25 0 2.00 6.40 0 25 0 6.60 6.00 0 25 0 1.30 4.20 -1 -25 0 267.37 13.10 1 -25 0 260.47 15.90 1 -25 0 247.98 13.80 -1 -25 0 263.27 13.70 1 -25 0 260.07 13.00 1 -25 0 253.97 13.70 -1 -25 0 260.37 16.00 1 -25 0 252.87 14.00 -1 -25 0 277.57 14.50 1 25 0 251.07 12.50 1 25 0 237.68 14.70 -1 25 0 250.37 12.10 -1 25 0 243.08 14.70 -1 25 0 256.47 16.90 1 25 0 266.07 14.40 2 -25 0 20.10 5.60 -2 -25 0 31.70 6.20 -2 -25 0 22.90 7.40 2 -25 0 23.50 5.30 2 -25 0 13.80 6.40 -2 -25 0 22.50 5.90 2 -25 0 17.20 5.70 2 -25 0 18.30 5.80 -2 25 0 18.70 4.70 2 25 0 16.00 5.20 2 25 0 14.80 6.80 2 25 0 22.80 7.40 -2 25 0 16.90 6.50 -2 25 0 19.30 7.20 3 -25 0 1.40 5.10 -3 -25 0 -7.30 4.20 3 -25 0 11.00 4.70 3 -25 0 7.80 6.50 -3 -25 0 8.90 5.40 -3 -25 0 1.10 6.50 3 -25 0 9.50 5.10 -3 -25 0 6.60 5.00 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18.80 11.30 7 25 0 11.70 6.80 -7 25 0 15.20 9.80 0 -26 0 169.38 10.80 0 -26 0 189.18 12.10 0 -26 0 174.88 13.20 0 -26 0 174.28 11.90 0 26 0 136.49 12.90 0 26 0 172.58 11.80 0 26 0 159.98 10.00 -1 -26 0 6.80 5.00 -1 -26 0 15.80 5.40 -1 -26 0 13.70 6.70 1 -26 0 11.90 5.20 1 -26 0 3.70 4.80 -1 -26 0 8.70 4.70 1 -26 0 3.90 4.50 1 -26 0 3.00 5.80 1 -26 0 4.80 4.80 1 26 0 4.40 4.60 -1 26 0 8.80 4.50 1 26 0 20.10 7.50 -1 26 0 9.20 6.70 1 26 0 11.00 6.20 -2 -26 0 8.50 5.50 -2 -26 0 3.70 6.70 2 -26 0 3.40 5.70 2 -26 0 1.60 4.50 -2 -26 0 10.40 5.40 2 -26 0 6.20 5.20 2 -26 0 13.50 5.50 2 -26 0 0.60 5.20 -2 26 0 13.90 7.30 -2 26 0 15.60 4.70 2 26 0 2.50 6.50 -2 26 0 -2.70 6.00 2 26 0 9.70 6.90 2 26 0 3.20 4.80 -3 -26 0 14.60 6.00 3 -26 0 15.40 7.10 -3 -26 0 21.50 5.70 -3 -26 0 14.40 8.10 -3 -26 0 9.40 7.40 3 -26 0 16.40 5.40 3 -26 0 5.40 5.70 3 -26 0 5.10 5.20 3 26 0 7.80 5.20 3 26 0 6.60 7.10 -3 26 0 10.40 4.50 -3 26 0 3.60 6.70 3 26 0 16.40 8.30 -3 26 0 11.20 6.70 4 -26 0 7.40 5.90 -4 -26 0 9.10 5.80 -4 -26 0 -0.90 6.00 4 -26 0 2.70 6.50 4 -26 0 10.30 6.50 -4 -26 0 7.30 8.50 4 -26 0 8.90 5.50 4 -26 0 11.20 6.40 -4 26 0 5.10 4.40 4 26 0 -0.10 7.20 4 26 0 -2.40 7.90 4 26 0 11.00 5.90 -4 26 0 5.90 7.30 -4 26 0 11.30 7.40 -5 -26 0 -2.80 7.70 -5 -26 0 44.60 8.60 5 -26 0 9.80 6.70 5 -26 0 2.00 5.20 -5 -26 0 11.90 6.30 5 -26 0 5.70 6.70 5 -26 0 9.80 7.70 5 26 0 4.10 8.50 5 26 0 8.10 9.60 5 26 0 8.80 5.80 -5 26 0 16.80 5.00 -5 26 0 2.20 7.70 -5 26 0 10.90 8.10 6 -26 0 8.90 7.40 -6 -26 0 12.50 7.00 6 -26 0 14.80 7.90 -6 -26 0 19.10 7.90 -6 -26 0 9.40 9.90 6 -26 0 23.80 7.10 -6 26 0 18.70 5.20 -6 26 0 11.60 9.70 6 26 0 3.10 10.70 6 26 0 20.70 7.30 -6 26 0 11.40 8.90 6 26 0 -2.20 9.00 7 -26 0 29.60 9.90 7 -26 0 47.80 8.80 -7 -26 0 39.30 10.10 -7 -26 0 32.10 12.20 -7 -26 0 45.60 9.30 7 -26 0 33.70 9.30 -7 26 0 37.90 10.60 -7 26 0 21.20 10.90 7 26 0 32.50 8.20 0 -27 0 3.70 4.50 0 -27 0 20.50 6.80 0 -27 0 11.40 5.70 0 -27 0 7.30 5.20 0 27 0 -0.40 6.00 0 27 0 13.10 4.80 0 27 0 -2.20 6.60 -1 -27 0 189.58 12.70 1 -27 0 198.78 12.60 1 -27 0 206.98 12.70 -1 -27 0 196.38 11.70 1 -27 0 190.98 12.70 1 -27 0 191.18 11.60 -1 -27 0 174.98 14.20 -1 -27 0 192.58 12.60 1 -27 0 181.48 13.70 -1 27 0 186.78 13.80 1 27 0 174.48 10.80 1 27 0 197.18 12.80 1 27 0 170.88 13.60 -1 27 0 195.38 10.70 -2 -27 0 28.40 6.90 2 -27 0 16.40 5.70 2 -27 0 18.20 6.20 -2 -27 0 31.20 7.10 2 -27 0 22.40 6.80 -2 -27 0 29.70 8.30 2 -27 0 25.60 7.40 2 -27 0 19.00 5.60 -2 27 0 30.30 7.90 2 27 0 19.70 5.60 2 27 0 28.30 8.00 2 27 0 28.00 8.10 -2 27 0 19.00 5.10 -3 -27 0 17.90 6.20 3 -27 0 12.60 6.20 3 -27 0 7.70 7.10 -3 -27 0 13.80 7.90 3 -27 0 8.20 5.80 3 -27 0 2.00 4.70 3 27 0 12.60 5.60 -3 27 0 -3.00 6.60 -3 27 0 -2.50 6.60 -3 27 0 12.70 4.60 3 27 0 10.40 8.00 3 27 0 6.60 8.50 -4 -27 0 2.20 5.70 4 -27 0 7.70 7.80 4 -27 0 1.20 6.40 -4 -27 0 3.90 8.00 4 -27 0 16.20 5.90 -4 -27 0 -5.90 5.60 4 -27 0 15.30 6.90 4 -27 0 8.10 7.10 -4 27 0 0.60 7.40 4 27 0 9.70 6.00 4 27 0 1.80 8.60 -4 27 0 11.50 5.10 -4 27 0 -10.90 7.10 4 27 0 12.00 8.00 -5 -27 0 41.10 8.10 -5 -27 0 25.20 10.00 5 -27 0 45.10 8.80 5 -27 0 41.30 7.40 5 -27 0 30.30 8.50 -5 -27 0 63.69 10.00 5 -27 0 43.10 10.00 -5 27 0 55.89 7.20 5 27 0 48.00 13.50 5 27 0 16.30 9.30 5 27 0 43.50 8.00 -5 27 0 39.50 10.20 -5 27 0 53.69 10.80 -6 -27 0 1.40 6.60 6 -27 0 5.80 7.50 6 -27 0 3.20 7.30 -6 -27 0 -12.70 8.90 6 -27 0 -6.70 5.60 -6 -27 0 -15.90 6.60 -6 27 0 -8.30 8.70 6 27 0 7.00 6.50 6 27 0 -1.70 8.90 -6 27 0 8.70 9.80 -7 -27 0 -5.00 10.30 7 -27 0 -2.00 8.50 7 -27 0 3.10 6.70 -7 -27 0 -16.10 6.50 7 -27 0 2.30 8.20 -7 -27 0 1.40 7.10 -7 27 0 5.30 9.70 -7 27 0 -10.00 9.00 7 27 0 1.00 7.40 0 -28 0 10.00 6.90 0 -28 0 13.90 5.50 0 -28 0 7.60 5.70 0 -28 0 12.70 6.30 0 28 0 7.20 7.70 0 28 0 17.40 7.20 0 28 0 11.60 5.00 -1 -28 0 17.80 7.50 1 -28 0 9.40 5.40 1 -28 0 5.90 5.60 1 -28 0 0.30 5.40 1 -28 0 4.30 5.30 -1 -28 0 3.60 5.20 -1 -28 0 11.90 5.50 1 -28 0 7.60 6.20 -1 -28 0 -3.40 5.20 1 28 0 3.70 7.60 -1 28 0 7.20 4.50 -1 28 0 5.80 7.40 1 28 0 5.70 4.60 1 28 0 12.00 7.30 2 -28 0 3.10 4.90 2 -28 0 13.60 6.60 -2 -28 0 4.40 5.60 -2 -28 0 10.10 7.50 2 -28 0 10.90 7.10 2 -28 0 5.70 5.60 2 -28 0 12.60 6.10 -2 -28 0 13.10 5.40 2 28 0 16.90 8.00 2 28 0 6.70 5.10 -2 28 0 7.50 4.70 -2 28 0 17.20 8.30 2 28 0 1.70 7.50 3 -28 0 74.59 8.90 3 -28 0 57.59 8.70 3 -28 0 63.89 10.60 3 -28 0 57.89 9.00 -3 -28 0 69.79 9.50 -3 -28 0 56.79 11.10 -3 28 0 71.49 14.00 3 28 0 56.49 9.90 3 28 0 61.09 8.60 3 28 0 72.09 14.30 -3 28 0 58.49 7.40 -3 28 0 43.60 9.80 4 -28 0 59.09 9.70 -4 -28 0 82.39 10.00 -4 -28 0 45.00 10.70 4 -28 0 71.39 9.20 -4 -28 0 54.69 10.30 4 -28 0 62.19 10.80 4 -28 0 60.09 10.60 4 28 0 65.79 9.00 -4 28 0 66.49 11.10 4 28 0 43.10 10.10 -4 28 0 60.39 10.10 -4 28 0 73.99 7.60 5 -28 0 7.90 6.00 -5 -28 0 1.40 6.30 5 -28 0 6.80 8.30 -5 -28 0 11.70 9.30 -5 -28 0 7.10 6.30 5 -28 0 -2.40 7.10 5 -28 0 2.80 6.80 5 28 0 5.70 6.20 -5 28 0 7.40 4.90 -5 28 0 -6.00 8.20 5 28 0 -2.50 8.80 -5 28 0 -0.10 7.80 6 -28 0 22.90 7.30 6 -28 0 24.10 8.90 -6 -28 0 37.00 8.90 -6 -28 0 14.10 11.00 6 -28 0 5.40 8.30 -6 -28 0 15.60 8.40 6 28 0 13.00 7.30 -6 28 0 8.60 9.80 6 28 0 29.80 11.10 -6 28 0 22.40 10.70 0 -29 0 -2.60 6.00 0 -29 0 9.90 7.10 0 -29 0 2.90 5.40 0 -29 0 -0.60 5.10 0 29 0 -4.20 7.40 0 29 0 -5.80 4.40 -1 -29 0 6.30 7.40 1 -29 0 4.00 5.10 1 -29 0 0.70 6.10 -1 -29 0 2.10 5.20 -1 -29 0 -11.60 5.50 1 -29 0 -2.40 5.50 1 -29 0 0.30 5.20 1 -29 0 8.00 6.10 1 29 0 1.60 7.60 -1 29 0 -7.70 6.90 -1 29 0 8.10 4.80 1 29 0 -4.40 4.60 -2 -29 0 4.10 5.60 2 -29 0 2.50 6.10 2 -29 0 3.00 6.10 -2 -29 0 -3.00 7.10 2 -29 0 -2.00 5.00 2 -29 0 1.80 6.60 -2 -29 0 -8.70 5.40 2 -29 0 7.90 6.00 -2 29 0 9.80 7.80 2 29 0 3.90 7.50 -2 29 0 3.40 4.60 2 29 0 2.20 5.10 3 -29 0 8.30 6.30 3 -29 0 10.00 7.80 -3 -29 0 -1.40 8.00 -3 -29 0 11.30 6.40 3 -29 0 15.40 5.90 3 29 0 7.30 7.80 -3 29 0 -3.30 7.90 -3 29 0 8.50 4.70 3 29 0 -1.80 5.10 4 -29 0 5.90 6.60 4 -29 0 -1.10 6.60 4 -29 0 0.40 5.30 -4 -29 0 -3.00 8.40 -4 -29 0 -7.90 6.20 4 -29 0 -3.40 6.40 -4 29 0 -4.00 7.60 4 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0 5.50 7.60 3 -30 0 0.40 5.30 -3 30 0 16.70 5.00 3 30 0 12.90 6.00 -3 30 0 11.50 8.50 3 30 0 7.00 9.00 4 -30 0 38.10 8.90 -4 -30 0 30.10 8.60 4 -30 0 31.70 7.40 4 -30 0 20.90 8.70 4 -30 0 48.00 9.10 -4 -30 0 28.00 10.40 -4 30 0 34.80 8.10 -4 30 0 27.80 9.70 4 30 0 33.50 7.40 4 30 0 34.40 10.10 5 -30 0 11.50 7.90 5 -30 0 2.40 8.90 5 -30 0 -1.90 7.80 -5 -30 0 7.40 9.30 -5 -30 0 4.90 6.50 5 -30 0 7.40 6.40 -5 30 0 5.50 8.80 5 30 0 0.00 9.90 5 30 0 3.40 6.60 -5 30 0 16.30 10.70 0 -31 0 -3.00 6.50 0 -31 0 1.00 7.10 0 -31 0 3.40 6.10 0 31 0 -0.40 8.30 0 31 0 1.90 4.90 1 -31 0 60.89 10.80 -1 -31 0 23.70 8.60 -1 -31 0 46.70 8.60 1 -31 0 38.40 7.30 -1 -31 0 37.20 7.50 1 -31 0 36.50 8.50 1 31 0 27.00 9.90 -1 31 0 40.20 7.10 1 31 0 40.70 7.60 -1 31 0 12.40 9.00 -2 -31 0 -4.30 6.00 2 -31 0 -1.50 6.70 -2 -31 0 -0.70 7.30 2 -31 0 -0.20 5.80 2 -31 0 1.20 7.20 -2 -31 0 -2.80 6.40 2 31 0 -1.90 5.20 -2 31 0 -2.30 4.50 -2 31 0 9.00 9.10 2 31 0 -4.00 8.10 3 -31 0 20.60 9.00 3 -31 0 42.30 7.70 -3 -31 0 22.90 8.20 -3 -31 0 27.60 7.60 -3 -31 0 9.60 8.80 -3 31 0 34.10 6.40 3 31 0 44.60 7.30 3 31 0 17.00 9.70 -3 31 0 30.90 9.50 4 -31 0 119.59 13.00 4 -31 0 95.39 10.70 4 -31 0 79.89 11.40 -4 -31 0 95.59 14.00 -4 -31 0 99.09 12.90 4 31 0 86.39 9.90 -4 31 0 87.69 13.00 4 31 0 66.69 12.10 -5 -31 0 20.50 10.50 5 -31 0 33.80 11.00 5 -31 0 35.40 9.30 5 -31 0 40.90 8.40 -5 -31 0 28.60 8.30 -5 31 0 30.30 11.30 5 31 0 32.70 8.30 5 31 0 35.80 11.00 0 -32 0 61.29 9.90 0 -32 0 40.30 9.50 0 -32 0 43.80 8.10 0 32 0 47.40 7.40 0 32 0 38.20 10.20 1 -32 0 18.50 7.90 -1 -32 0 6.30 6.30 -1 -32 0 26.70 7.90 1 -32 0 6.50 6.10 1 -32 0 22.20 8.20 -1 -32 0 12.60 8.30 1 32 0 16.00 9.20 -1 32 0 5.30 5.00 1 32 0 13.80 5.80 -1 32 0 -0.60 8.60 -2 -32 0 58.89 9.70 -2 -32 0 68.89 10.20 2 -32 0 61.59 11.20 -2 -32 0 66.09 12.10 2 -32 0 49.50 10.70 2 -32 0 76.49 9.80 2 32 0 60.19 11.50 2 32 0 74.59 8.80 -2 32 0 71.09 8.80 -2 32 0 59.89 11.80 -3 -32 0 9.50 7.00 3 -32 0 25.10 8.20 3 -32 0 15.60 6.50 -3 -32 0 12.20 7.40 3 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69.39 9.80 7 -12 -4 93.99 8.60 -7 -12 4 76.79 8.10 7 -12 -4 85.09 9.10 -7 12 4 96.09 10.70 7 12 -4 89.09 9.90 7 12 -4 66.09 9.50 7 12 -4 88.09 9.60 7 12 -4 75.59 9.70 -7 12 4 91.59 9.00 7 12 -4 80.09 8.60 6 -12 -4 1.50 3.30 -6 -12 4 -0.50 4.20 6 -12 -4 0.20 3.40 6 -12 -4 4.50 3.80 6 -12 -4 2.50 4.30 -6 -12 4 6.20 4.10 -6 -12 4 0.00 3.40 6 12 -4 1.70 4.20 -6 12 4 -0.80 4.20 6 12 -4 1.60 3.70 6 12 -4 5.00 5.20 -6 12 4 3.80 4.80 6 12 -4 -1.30 4.20 6 12 -4 -0.40 4.70 -5 -12 4 1.00 2.90 5 -12 -4 1.90 2.80 5 -12 -4 3.20 2.70 5 -12 -4 4.00 2.90 5 -12 -4 -1.10 3.00 -5 -12 4 -2.60 3.40 5 -12 -4 -2.40 3.40 -5 -12 4 -4.60 2.60 5 12 -4 0.50 3.30 -5 12 4 3.90 4.70 5 12 -4 2.90 3.90 5 12 -4 5.70 4.20 5 12 -4 2.60 4.00 5 12 -4 1.20 4.10 -5 12 4 1.80 4.10 -4 -12 4 79.79 5.10 4 -12 -4 67.29 7.10 4 -12 -4 67.99 5.30 4 -12 -4 61.69 5.70 -4 -12 4 70.59 6.00 4 -12 -4 72.19 5.20 4 -12 -4 77.89 5.60 -4 -12 4 73.99 5.80 -4 -12 4 71.29 5.80 -4 -12 4 60.09 6.60 4 12 -4 63.49 6.30 4 12 -4 66.09 6.40 -4 12 4 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257.37 10.40 -1 12 4 239.78 10.70 1 12 -4 243.38 9.80 -1 12 4 258.77 9.60 0 -12 -4 444.96 17.50 0 -12 -4 465.65 14.40 0 -12 4 502.95 18.10 0 -12 4 455.25 15.30 0 -12 4 466.15 16.60 0 -12 -4 471.45 16.20 0 -12 4 466.55 16.00 0 12 -4 490.35 17.00 0 12 4 469.65 16.70 0 12 -4 463.85 16.70 0 12 -4 477.45 17.00 0 12 -4 462.25 15.90 0 12 4 451.15 14.60 0 12 4 478.65 18.00 0 12 -4 447.26 16.30 1 -12 4 249.28 11.40 1 -12 4 264.17 10.50 -1 -12 -4 239.88 8.60 1 -12 4 252.47 9.90 -1 -12 -4 250.27 9.10 1 -12 4 240.38 9.20 -1 -12 -4 255.37 9.90 -1 -12 -4 251.57 11.50 1 -12 4 268.17 9.30 -1 12 -4 252.87 11.10 -1 12 -4 246.38 10.90 1 12 4 269.27 12.00 -1 12 -4 239.98 10.00 1 12 4 248.18 10.40 -1 12 -4 232.58 10.50 -1 12 -4 243.18 10.70 -2 -12 -4 42.90 3.50 2 -12 4 43.70 4.20 2 -12 4 48.10 5.20 2 -12 4 46.10 3.60 2 -12 4 43.40 4.50 -2 -12 -4 46.20 3.90 -2 -12 -4 40.10 4.10 2 -12 4 48.20 4.10 -2 -12 -4 50.89 5.50 -2 12 -4 42.50 4.60 -2 12 -4 47.80 5.80 -2 12 -4 41.90 4.90 2 12 4 43.30 4.60 2 12 4 41.20 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6.00 -6 13 -4 37.50 5.70 -6 13 -4 41.80 6.90 -6 13 -4 45.10 6.70 6 13 4 33.50 5.50 6 13 4 40.70 7.40 -6 13 -4 40.70 7.90 -6 13 -4 39.70 6.30 -7 -13 -4 1.50 4.10 7 -13 4 1.40 4.00 7 -13 4 10.70 4.20 7 -13 4 -1.40 5.00 7 -13 4 3.30 5.10 -7 -13 -4 3.10 4.80 -7 -13 -4 6.70 5.30 -7 -13 -4 2.90 5.60 -7 13 -4 -6.80 5.90 -7 13 -4 1.80 4.00 7 13 4 -0.40 4.00 -7 13 -4 2.30 4.50 7 13 4 4.10 7.00 8 -13 4 65.09 8.00 -8 -13 -4 73.49 11.20 8 -13 4 71.49 9.90 -8 -13 -4 70.39 11.90 8 -13 4 62.39 10.70 -8 -13 -4 60.19 9.90 8 13 4 69.49 11.00 -8 13 -4 76.39 8.70 -8 13 -4 76.49 10.60 8 13 4 59.99 8.30 -8 13 -4 65.89 9.40 9 -13 4 -4.10 7.70 -9 -13 -4 7.90 7.30 9 -13 4 8.50 6.40 9 -13 4 9.00 5.40 -9 -13 -4 -15.30 6.10 9 13 4 8.20 6.00 -9 13 -4 12.20 6.60 -9 13 -4 7.40 7.60 -9 13 -4 8.60 5.60 9 13 4 6.90 8.90 9 -14 -4 21.80 8.00 -9 -14 4 6.10 5.80 9 -14 -4 8.80 6.50 9 -14 -4 15.10 9.00 9 -14 -4 9.30 8.40 -9 14 4 21.50 10.00 9 14 -4 12.20 8.10 9 14 -4 2.30 6.40 -9 14 4 1.00 9.60 -8 -14 4 30.80 7.80 8 -14 -4 22.80 6.40 8 -14 -4 24.30 8.60 8 -14 -4 19.50 7.00 8 -14 -4 26.10 7.40 -8 -14 4 24.40 6.30 8 14 -4 29.70 7.00 -8 14 4 29.10 8.00 8 14 -4 25.70 7.60 8 14 -4 16.30 10.00 8 14 -4 16.90 7.10 -8 14 4 37.10 9.40 7 -14 -4 28.70 6.30 -7 -14 4 33.90 6.30 7 -14 -4 29.40 6.20 -7 -14 4 29.80 6.70 7 -14 -4 40.10 8.30 7 -14 -4 29.10 6.50 7 14 -4 26.70 6.00 7 14 -4 40.50 7.70 7 14 -4 38.10 7.10 -7 14 4 34.40 7.40 7 14 -4 45.90 8.10 -7 14 4 35.30 8.70 7 14 -4 18.70 6.70 6 -14 -4 -1.70 3.60 -6 -14 4 5.90 4.20 6 -14 -4 6.30 5.00 -6 -14 4 -0.40 3.70 6 -14 -4 6.20 4.00 6 -14 -4 -0.90 3.40 -6 -14 4 -6.10 4.60 6 14 -4 8.40 4.10 6 14 -4 3.10 4.90 6 14 -4 0.60 4.90 6 14 -4 3.80 5.40 -6 14 4 2.40 4.80 -6 14 4 9.00 6.00 6 14 -4 5.50 4.70 -5 -14 4 75.29 6.70 -5 -14 4 65.19 7.90 5 -14 -4 62.49 6.50 5 -14 -4 70.19 6.20 5 -14 -4 61.19 8.10 5 -14 -4 65.49 6.50 5 -14 -4 56.09 5.90 -5 -14 4 69.29 6.60 5 14 -4 68.79 7.40 -5 14 4 63.59 7.20 5 14 -4 52.09 7.10 5 14 -4 69.59 7.30 5 14 -4 57.69 7.50 -5 14 4 55.59 7.00 5 14 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4.30 3 15 -4 1.80 3.30 3 15 -4 2.30 3.10 3 15 -4 7.30 3.80 3 15 -4 5.50 3.00 -2 -15 4 18.50 4.60 2 -15 -4 20.40 3.20 -2 -15 4 21.30 3.70 2 -15 -4 23.60 4.80 2 -15 -4 23.80 4.80 -2 -15 4 27.10 4.40 -2 -15 4 17.60 3.10 2 -15 -4 21.60 3.60 2 -15 -4 23.30 3.90 2 15 -4 21.00 3.90 2 15 -4 22.50 3.50 2 15 -4 15.40 3.60 2 15 -4 19.40 3.60 2 15 -4 19.10 4.40 -2 15 4 20.50 4.60 -2 15 4 23.30 3.90 -1 -15 4 279.37 12.10 1 -15 -4 285.27 11.70 1 -15 -4 282.07 13.30 1 -15 -4 285.57 11.10 -1 -15 4 278.67 11.50 -1 -15 4 278.87 10.90 -1 -15 4 275.97 13.40 1 -15 -4 283.97 10.40 1 15 -4 265.47 11.30 1 15 -4 269.77 12.40 1 15 -4 271.17 11.90 1 15 -4 307.07 11.00 -1 15 4 291.27 10.80 1 15 -4 298.17 12.40 -1 15 4 276.67 13.20 1 15 -4 289.37 11.90 -1 15 4 284.77 12.40 0 -15 -4 36.10 4.40 0 -15 4 30.90 3.80 0 -15 4 31.70 4.80 0 -15 4 34.50 5.50 0 -15 -4 43.10 5.90 0 -15 -4 39.90 3.90 0 -15 -4 42.60 3.60 0 15 4 33.60 3.00 0 15 -4 37.70 5.00 0 15 -4 29.50 4.50 0 15 -4 27.50 4.90 0 15 -4 39.10 5.00 0 15 -4 30.20 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31.50 10.10 -8 -5 10 24.80 6.90 8 -5 -10 28.40 8.20 8 -5 -10 41.80 7.20 8 -5 -10 41.90 8.30 8 5 -10 39.90 8.70 -8 5 10 31.60 9.40 -8 5 10 37.00 11.20 8 5 -10 33.00 9.50 8 5 -10 43.20 7.90 7 -5 -10 10.40 5.00 -7 -5 10 21.70 7.10 7 -5 -10 8.80 6.30 7 5 -10 19.70 7.70 7 5 -10 16.60 4.90 -7 5 10 14.90 6.20 7 5 -10 19.20 8.50 -7 5 10 10.30 7.10 7 5 -10 6.20 5.20 6 -5 -10 0.30 3.60 -6 -5 10 10.60 5.30 6 -5 -10 4.80 5.00 6 5 -10 -2.20 4.80 -6 5 10 -5.70 5.20 6 5 -10 -1.90 3.40 6 5 -10 -2.10 3.70 -6 5 10 3.30 5.00 6 5 -10 -2.60 4.60 -5 -5 10 42.40 6.10 5 -5 -10 39.00 7.00 5 -5 -10 38.10 4.80 -5 5 10 44.80 7.30 5 5 -10 32.70 4.30 5 5 -10 44.20 6.50 5 5 -10 38.70 5.50 -5 5 10 35.40 5.80 5 5 -10 34.80 6.10 -4 -5 10 60.49 5.10 4 -5 -10 56.49 4.60 4 -5 -10 65.99 7.10 -4 -5 10 55.59 6.70 4 5 -10 54.39 6.60 4 5 -10 67.09 6.10 4 5 -10 57.69 5.30 -4 5 10 65.79 6.60 -4 5 10 68.99 6.60 -3 -5 10 -0.70 2.10 -3 -5 10 0.60 2.70 3 -5 -10 -1.80 1.50 3 -5 -10 0.30 2.10 3 -5 -10 -1.00 1.30 3 -5 -10 4.20 3.10 -3 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65.09 7.70 -7 6 10 56.39 8.20 -7 6 10 69.29 10.60 7 6 -10 42.50 8.80 -6 -6 10 18.00 5.30 6 -6 -10 19.60 4.70 6 -6 -10 34.30 6.80 6 6 -10 24.70 4.90 -6 6 10 22.60 6.60 6 6 -10 25.60 5.40 6 6 -10 22.20 6.50 6 6 -10 21.80 6.20 -6 6 10 33.60 7.40 -5 -6 10 13.70 5.00 5 -6 -10 14.00 5.00 5 -6 -10 17.70 3.60 5 6 -10 12.10 4.60 -5 6 10 15.80 5.90 -5 6 10 4.90 4.20 5 6 -10 14.70 4.20 5 6 -10 13.60 5.00 5 6 -10 17.90 3.40 4 -6 -10 -2.00 2.00 -4 -6 10 2.50 2.40 4 -6 -10 -0.10 3.60 -4 -6 10 -0.30 3.10 -4 6 10 0.50 3.70 4 6 -10 2.10 2.60 -4 6 10 -1.90 3.60 4 6 -10 1.80 3.90 4 6 -10 7.10 3.50 3 -6 -10 67.09 4.10 3 -6 -10 61.09 3.80 3 -6 -10 59.89 4.80 3 -6 -10 74.79 6.90 -3 -6 10 71.89 5.60 -3 -6 10 76.39 6.40 3 6 -10 56.59 6.40 3 6 -10 62.99 5.10 3 6 -10 63.59 5.10 -3 6 10 74.39 6.70 -3 6 10 62.59 6.40 -2 -6 10 269.47 11.90 2 -6 -10 277.37 9.00 -2 -6 10 256.27 12.30 2 6 -10 286.27 10.60 -2 6 10 257.67 11.90 2 6 -10 272.57 10.20 2 6 -10 260.27 10.60 2 6 -10 281.47 12.30 -2 6 10 290.07 12.00 -1 -6 10 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2.80 -3 6 -10 10.60 4.60 3 6 10 4.30 3.90 -4 -6 -10 68.59 5.90 4 -6 10 84.79 8.10 -4 -6 -10 62.39 5.40 4 -6 10 75.59 6.70 4 6 10 67.99 8.20 -4 6 -10 70.49 8.00 4 6 10 76.79 8.10 -4 6 -10 65.19 7.80 -4 6 -10 62.29 5.90 -4 6 -10 85.69 5.70 5 -6 10 87.89 8.90 -5 -6 -10 89.59 6.10 5 -6 10 99.19 8.50 -5 -6 -10 101.49 7.20 -5 -6 -10 94.19 7.30 5 6 10 108.19 9.60 -5 6 -10 102.19 7.80 -5 6 -10 88.89 9.30 5 6 10 87.29 8.80 -5 6 -10 93.99 7.80 -5 6 -10 100.29 7.20 6 -6 10 72.69 9.10 6 -6 10 47.00 7.90 -6 -6 -10 56.09 6.10 -6 -6 -10 59.39 6.70 -6 -6 -10 40.60 6.30 -6 6 -10 53.79 7.80 6 6 10 52.79 8.30 -6 6 -10 53.89 7.00 -6 6 -10 45.80 7.30 -6 6 -10 49.00 6.70 6 6 10 44.80 8.30 7 -6 10 49.20 9.00 7 -6 10 52.89 9.00 -7 -6 -10 60.99 8.00 -7 6 -10 61.09 10.10 -7 6 -10 63.09 7.60 7 6 10 61.79 10.20 -7 6 -10 61.59 8.50 -7 6 -10 50.89 9.60 -8 -6 -10 63.29 9.20 8 -6 10 66.79 14.20 8 -6 10 49.70 10.50 -8 6 -10 58.69 9.50 -8 6 -10 77.89 9.10 -8 6 -10 49.70 8.80 -8 6 -10 56.99 10.70 8 6 10 56.29 11.60 9 -6 10 21.30 10.30 -9 -6 -10 24.70 7.50 -9 -6 -10 36.50 9.70 -9 -6 -10 34.20 9.30 -9 -6 -10 50.09 15.50 -9 6 -10 23.90 9.00 -9 6 -10 50.69 8.70 -9 6 -10 23.70 7.80 9 6 10 28.80 10.90 9 -7 -10 7.50 7.60 9 -7 -10 17.50 7.60 -9 -7 10 21.90 9.20 9 -7 -10 1.80 7.30 9 7 -10 15.00 7.70 9 7 -10 5.40 9.20 9 7 -10 19.30 9.30 -9 7 10 11.00 8.00 9 7 -10 32.90 10.10 -9 7 10 29.80 10.10 -8 -7 10 31.90 8.70 8 -7 -10 29.20 6.80 8 -7 -10 31.60 7.60 8 -7 -10 22.60 7.60 8 7 -10 20.70 7.10 -8 7 10 17.30 7.50 8 7 -10 30.80 7.90 8 7 -10 30.60 10.60 -8 7 10 15.20 7.70 8 7 -10 23.70 7.60 7 -7 -10 78.79 9.00 -7 -7 10 78.29 9.80 7 -7 -10 79.69 11.10 7 7 -10 64.29 11.60 7 7 -10 69.29 9.20 7 7 -10 81.99 8.30 -7 7 10 99.09 9.50 7 7 -10 106.79 10.10 -7 7 10 85.69 11.10 6 -7 -10 21.80 4.80 -6 -7 10 23.10 5.90 6 -7 -10 15.00 6.00 -6 7 10 19.00 6.80 6 7 -10 22.80 6.10 6 7 -10 19.80 6.40 6 7 -10 20.70 4.50 6 7 -10 26.00 5.40 -6 7 10 19.30 5.80 5 -7 -10 4.80 2.90 5 -7 -10 2.40 4.30 -5 -7 10 5.90 4.10 5 7 -10 0.90 3.90 5 7 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9 12 79.09 8.90 4 -9 12 20.10 6.00 4 -9 12 17.40 4.80 -4 9 -12 10.30 5.90 4 9 12 13.40 6.10 -4 9 -12 9.30 3.80 -4 9 -12 8.20 3.50 5 -9 12 33.60 6.40 5 -9 12 49.90 8.50 -5 9 -12 35.30 5.60 -5 9 -12 24.80 5.40 -5 9 -12 26.90 6.40 5 9 12 34.70 8.00 6 -9 12 2.50 6.40 6 -9 12 0.00 5.20 -6 -9 -12 4.30 4.20 6 9 12 -6.10 6.50 -6 9 -12 -2.20 4.10 -6 9 -12 2.00 4.50 -6 9 -12 -0.90 5.90 7 -9 12 9.90 7.00 -7 -9 -12 2.50 4.40 -7 -9 -12 0.20 6.60 -7 -9 -12 1.50 5.30 7 -9 12 5.50 7.60 -7 9 -12 2.70 7.70 -7 9 -12 7.60 5.20 7 9 12 -1.30 7.10 -7 9 -12 3.90 5.30 8 -9 12 8.90 8.30 -8 -9 -12 2.20 6.50 -8 -9 -12 -9.60 6.50 8 -9 12 -1.00 8.80 -8 -9 -12 18.30 6.60 -8 9 -12 7.80 7.60 -8 9 -12 16.10 6.20 -8 9 -12 3.20 8.00 -8 9 -12 -6.40 5.70 8 9 12 6.60 8.70 -8 -10 12 26.70 9.30 8 -10 -12 22.60 6.80 8 -10 -12 15.90 8.50 -8 10 12 32.70 10.90 -8 10 12 35.40 9.10 8 10 -12 27.00 7.60 8 10 -12 28.00 8.80 8 10 -12 15.20 8.90 7 -10 -12 137.29 10.90 7 -10 -12 129.99 13.60 -7 -10 12 175.18 15.00 -7 10 12 153.78 12.70 7 10 -12 154.48 12.50 7 10 -12 152.48 12.10 -7 10 12 170.18 14.50 6 -10 -12 6.20 3.90 6 -10 -12 1.80 5.90 -6 -10 12 1.30 4.50 6 10 -12 -1.90 4.70 6 10 -12 0.20 4.90 -6 10 12 17.10 7.40 -6 10 12 4.30 6.50 6 10 -12 0.90 5.80 -5 -10 12 12.20 5.90 5 -10 -12 3.60 3.10 5 -10 -12 13.10 5.90 -5 10 12 5.30 5.90 5 10 -12 8.50 4.80 -5 10 12 10.30 5.80 5 10 -12 16.10 6.00 5 10 -12 6.20 4.20 4 -10 -12 7.20 5.30 -4 -10 12 6.10 3.90 -4 -10 12 9.60 4.90 4 -10 -12 5.00 2.70 4 10 -12 5.40 4.00 -4 10 12 12.80 5.90 4 10 -12 8.90 5.20 -4 10 12 8.90 4.80 3 -10 -12 44.00 5.60 3 -10 -12 45.60 7.40 3 -10 -12 35.90 3.80 -3 -10 12 51.59 6.80 -3 -10 12 57.59 6.60 3 10 -12 62.09 7.30 3 10 -12 55.79 6.00 -3 10 12 50.39 6.70 -3 10 12 46.70 7.10 2 -10 -12 5.90 3.40 -2 -10 12 4.20 3.60 2 -10 -12 5.40 2.00 -2 -10 12 7.20 4.00 2 -10 -12 4.30 1.50 2 10 -12 -0.70 3.50 -2 10 12 3.20 3.80 -2 10 12 4.10 4.30 2 10 -12 3.20 2.70 1 -10 -12 35.10 2.70 1 -10 -12 33.20 2.30 -1 -10 12 27.40 5.40 1 -10 -12 28.50 5.20 1 10 -12 33.50 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102.29 12.40 6 -11 -12 34.80 5.60 -6 -11 12 39.70 8.40 6 -11 -12 33.80 8.00 6 11 -12 35.70 7.00 -6 11 12 46.30 9.10 6 11 -12 45.80 7.10 -6 11 12 44.50 8.70 6 11 -12 21.20 7.10 5 -11 -12 8.10 3.20 5 -11 -12 12.50 6.20 -5 -11 12 9.60 4.80 5 11 -12 -2.00 4.50 5 11 -12 9.80 4.30 -5 11 12 18.00 6.60 -5 11 12 6.40 5.80 5 11 -12 3.50 6.00 -4 -11 12 235.58 13.70 4 -11 -12 233.98 14.70 -4 -11 12 252.37 13.10 4 -11 -12 248.48 10.60 -4 11 12 243.08 13.40 4 11 -12 238.38 12.40 4 11 -12 230.78 12.00 4 11 -12 256.17 13.80 -4 11 12 269.07 14.00 3 -11 -12 186.28 12.60 -3 -11 12 205.58 12.00 -3 -11 12 194.48 11.60 3 -11 -12 193.88 10.60 3 -11 -12 196.58 8.50 3 11 -12 188.48 10.20 -3 11 12 200.08 11.30 3 11 -12 198.58 11.60 -3 11 12 222.88 12.10 2 -11 -12 17.80 4.40 -2 -11 12 22.40 5.20 2 -11 -12 12.70 2.20 2 -11 -12 18.60 2.90 -2 -11 12 19.90 4.60 -2 11 12 14.50 4.40 -2 11 12 15.90 5.00 2 11 -12 15.00 3.70 2 11 -12 8.70 4.40 1 -11 -12 39.20 3.20 1 -11 -12 37.90 2.70 1 -11 -12 40.80 5.80 -1 -11 12 36.20 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21.90 5.80 -5 13 -12 21.90 5.80 -5 13 -12 16.40 5.10 5 13 12 10.40 7.40 -5 13 -12 25.70 8.40 -6 -13 -12 8.20 4.90 -6 -13 -12 7.20 5.10 6 -13 12 -1.40 7.60 6 13 12 -1.20 7.30 -6 13 -12 2.10 5.10 -6 13 -12 10.40 7.50 -6 13 -12 0.50 4.70 -6 13 -12 -12.90 5.00 7 -13 12 92.49 13.00 -7 -13 -12 122.39 15.20 -7 -13 -12 92.29 12.90 -7 -13 -12 128.99 10.70 -7 13 -12 86.59 9.80 -7 13 -12 110.89 13.50 -7 13 -12 117.29 13.20 -7 13 -12 116.59 11.60 7 13 12 76.79 12.80 -8 -13 -12 15.40 7.80 8 -13 12 3.90 9.10 -8 -13 -12 19.40 7.10 -8 13 -12 14.20 8.70 -8 13 -12 10.60 9.10 -8 13 -12 8.50 6.30 -8 13 -12 7.40 9.70 8 13 12 9.30 9.70 8 -14 -12 0.40 5.90 8 -14 -12 20.50 8.00 -8 -14 12 11.30 8.50 8 14 -12 14.20 8.20 8 14 -12 -5.60 7.00 -8 14 12 -5.40 8.10 -8 14 12 0.00 9.40 -7 -14 12 50.39 10.20 7 -14 -12 45.60 7.50 7 -14 -12 36.60 9.20 -7 14 12 43.40 9.60 7 14 -12 43.70 8.10 7 14 -12 32.30 9.20 -7 14 12 49.70 10.50 6 -14 -12 46.60 7.50 -6 -14 12 51.99 9.10 6 -14 -12 63.99 10.50 6 14 -12 64.89 8.00 -6 14 12 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17.50 4.50 -5 -7 -14 1.90 3.50 5 -7 14 0.60 6.30 -5 7 -14 -3.20 4.10 -5 7 -14 0.50 3.50 5 7 14 -0.60 6.50 5 7 14 5.30 5.80 -5 7 -14 -2.80 6.00 -6 -7 -14 1.30 4.10 6 -7 14 1.30 9.50 -6 7 -14 4.30 7.20 -6 7 -14 5.60 4.10 -6 7 -14 4.30 4.70 6 7 14 7.00 7.60 6 7 14 11.70 7.30 7 -7 14 102.89 13.70 -7 -7 -14 71.79 9.90 7 -7 14 54.89 13.30 -7 7 -14 62.79 11.20 -7 7 -14 102.49 10.10 -7 7 -14 71.29 9.70 7 7 14 82.49 13.30 -8 -7 -14 9.80 5.60 8 -7 14 -9.80 9.80 8 -7 14 11.40 10.20 -8 7 -14 -2.00 6.00 8 7 14 6.70 9.50 -8 7 -14 9.60 8.30 -8 7 -14 -3.10 6.30 -8 -8 14 15.00 9.20 8 -8 -14 9.50 6.30 8 -8 -14 -2.70 6.60 8 8 -14 1.10 7.80 -8 8 14 8.40 9.90 -8 8 14 10.70 11.50 8 8 -14 2.40 8.00 -7 -8 14 28.70 9.40 7 -8 -14 20.50 8.30 7 -8 -14 14.70 6.10 -7 8 14 17.60 9.40 7 8 -14 14.60 7.80 7 8 -14 19.10 7.20 -7 8 14 20.70 9.30 6 -8 -14 5.30 3.80 6 -8 -14 1.40 6.00 -6 -8 14 6.60 5.90 -6 8 14 13.80 7.00 6 8 -14 1.30 4.80 -6 8 14 -4.60 6.80 6 8 -14 4.40 6.30 5 -8 -14 24.90 4.60 5 -8 -14 26.30 7.20 -5 -8 14 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8.70 -7 -9 14 -5.60 6.40 7 -9 -14 3.50 7.40 7 -9 -14 5.20 4.70 -7 9 14 -7.70 7.10 -7 9 14 12.60 8.60 7 9 -14 10.30 7.50 7 9 -14 -5.40 5.70 -6 -9 14 6.10 7.40 6 -9 -14 10.60 6.80 6 -9 -14 15.40 4.40 6 9 -14 14.50 6.90 -6 9 14 21.60 8.60 -6 9 14 19.50 7.80 6 9 -14 17.20 6.40 5 -9 -14 4.70 3.00 5 -9 -14 -3.60 5.20 -5 -9 14 6.00 5.90 -5 9 14 2.00 6.10 -5 9 14 4.50 6.40 5 9 -14 1.60 4.30 5 9 -14 -3.50 6.20 4 -9 -14 43.50 7.80 4 -9 -14 34.50 4.20 -4 -9 14 26.50 6.10 4 9 -14 38.40 6.10 -4 9 14 51.19 8.00 -4 9 14 46.10 7.70 4 9 -14 32.10 6.60 3 -9 -14 1.80 2.10 -3 -9 14 6.10 4.30 3 -9 -14 -0.40 4.40 -3 -9 14 3.90 4.10 -3 9 14 -0.40 4.80 -3 9 14 -1.60 4.90 3 9 -14 4.00 5.20 3 9 -14 0.10 3.30 -2 -9 14 77.39 8.40 -2 -9 14 75.59 8.30 2 -9 -14 93.49 8.10 -2 9 14 92.69 8.30 -2 9 14 88.69 8.20 2 9 -14 77.59 6.20 2 9 -14 73.29 8.40 1 -9 -14 12.90 4.30 -1 -9 14 12.80 4.70 -1 9 14 11.90 5.30 1 9 -14 5.90 3.00 -1 9 14 8.00 4.60 -1 9 14 16.40 4.80 1 9 -14 0.10 4.10 1 9 -14 11.20 4.70 0 -9 14 41.70 7.30 0 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8.70 2 11 14 123.79 11.40 -3 -11 -14 6.10 3.10 3 -11 14 2.90 6.00 -3 -11 -14 -1.20 4.30 -3 11 -14 4.40 5.70 3 11 14 -0.10 5.70 -3 11 -14 -1.90 3.20 -4 -11 -14 60.69 9.20 4 -11 14 55.39 9.60 -4 -11 -14 52.19 6.40 -4 11 -14 44.60 6.60 -4 11 -14 45.30 6.80 4 11 14 55.49 9.70 -4 11 -14 63.89 9.90 -5 -11 -14 26.60 7.50 5 -11 14 12.40 8.10 -5 -11 -14 38.20 6.60 -5 11 -14 22.60 7.10 -5 11 -14 29.40 5.50 -5 11 -14 30.10 6.40 5 11 14 23.20 8.50 -6 -11 -14 7.80 5.60 -6 -11 -14 13.20 7.70 6 -11 14 10.10 8.00 -6 11 -14 5.30 5.30 -6 11 -14 -2.50 7.40 -6 11 -14 0.60 4.80 6 11 14 -2.90 7.40 7 -11 14 -1.20 8.50 -7 -11 -14 0.60 5.80 -7 -11 -14 0.10 8.60 -7 -11 -14 6.10 5.80 -7 11 -14 -4.30 8.10 -7 11 -14 11.70 6.10 7 11 14 -0.50 8.50 7 -12 -14 34.30 6.70 7 -12 -14 32.40 8.70 -7 -12 14 48.80 10.20 7 12 -14 20.00 9.00 -7 12 14 44.90 10.20 7 12 -14 34.40 9.10 -7 12 14 31.10 9.40 7 12 -14 19.80 8.30 6 -12 -14 36.80 6.00 6 -12 -14 25.10 8.00 -6 -12 14 41.20 9.40 -6 12 14 42.40 9.50 6 12 -14 33.50 8.40 -6 12 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5.60 -6 -15 15 10.50 7.60 6 -15 -15 15.90 7.70 6 -15 -15 13.40 5.30 6 15 -15 10.90 7.40 -6 15 15 5.20 8.50 6 15 -15 -5.90 7.60 -6 15 15 3.60 8.80 6 15 -15 18.30 7.90 5 -15 -15 105.79 12.90 -5 -15 15 76.39 11.90 5 -15 -15 57.59 6.90 5 15 -15 39.00 9.50 -5 15 15 88.19 12.20 5 15 -15 72.49 10.20 -5 15 15 77.09 11.30 -4 -15 15 109.99 11.30 4 -15 -15 141.19 13.00 4 -15 -15 101.09 7.20 4 15 -15 94.69 9.60 -4 15 15 116.29 10.90 4 15 -15 79.89 10.80 -4 15 15 78.79 11.70 3 -15 -15 8.10 6.50 3 -15 -15 14.80 3.10 -3 -15 15 15.20 6.60 -3 15 15 16.40 6.00 3 15 -15 16.50 5.20 -3 15 15 15.10 7.70 3 15 -15 19.60 6.40 2 -15 -15 77.29 9.70 2 -15 -15 71.89 5.80 -2 -15 15 88.19 10.90 2 15 -15 70.29 7.80 2 15 -15 75.29 10.00 -2 15 15 91.69 10.10 2 15 -15 83.99 11.20 -1 -15 15 42.10 8.30 1 -15 -15 51.19 7.60 1 -15 -15 43.20 4.90 -1 15 15 47.80 9.10 1 15 -15 42.50 6.60 1 15 -15 57.29 8.80 1 15 -15 34.50 8.30 -1 15 15 54.49 7.90 0 -15 15 29.30 8.00 0 -15 -15 10.20 6.00 0 -15 -15 15.00 3.50 0 15 -15 11.40 4.50 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15 13.10 7.70 -6 16 15 6.10 9.30 6 16 -15 7.80 7.10 -6 16 15 14.30 8.90 6 16 -15 25.30 8.00 -5 -16 15 34.80 7.80 5 -16 -15 41.30 10.20 5 -16 -15 18.90 5.10 5 16 -15 47.50 8.30 -5 16 15 28.90 8.90 -5 16 15 33.40 10.20 5 16 -15 32.60 8.40 -4 -16 15 -0.70 5.40 4 -16 -15 7.60 6.90 4 -16 -15 0.00 3.30 4 16 -15 7.30 6.40 -4 16 15 -4.00 7.50 -4 16 15 4.30 6.60 4 16 -15 4.00 5.40 3 -16 -15 73.89 11.10 -3 -16 15 73.29 10.70 3 -16 -15 79.79 6.10 3 16 -15 64.59 9.90 -3 16 15 77.19 10.50 3 16 -15 57.39 8.30 2 -16 -15 4.80 6.10 -2 -16 15 2.90 6.10 2 -16 -15 -2.00 2.70 2 16 -15 7.80 6.80 2 16 -15 4.30 6.20 2 16 -15 3.60 4.60 -2 16 15 -4.10 6.50 1 -16 -15 89.79 6.40 1 -16 -15 105.99 10.80 -1 -16 15 80.69 10.40 1 16 -15 93.89 9.00 -1 16 15 92.49 10.60 1 16 -15 83.59 11.50 1 16 -15 119.89 10.90 -1 16 15 78.59 11.20 0 -16 -15 35.60 4.50 0 -16 -15 37.40 7.80 0 -16 15 29.90 8.30 0 16 -15 33.90 7.50 0 16 15 32.60 6.90 0 16 -15 23.30 5.70 0 16 -15 33.30 8.20 0 16 15 36.30 8.70 1 -16 15 10.60 7.10 -1 -16 -15 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0.99 0.00 5 2 20 -1.54 0.00 -5 3 20 0.10 0.00 -4 3 20 2.07 0.00 -3 3 20 3.07 0.00 -2 3 20 -1.08 0.00 -1 3 20 1.22 0.00 0 3 20 -1.52 0.00 1 3 20 -3.65 0.00 2 3 20 2.71 0.00 3 3 20 4.55 0.00 4 3 20 -1.49 0.00 -5 4 20 -0.23 0.00 -4 4 20 -1.12 0.00 -3 4 20 1.01 0.00 -2 4 20 3.23 0.00 -1 4 20 -2.54 0.00 0 4 20 4.37 0.00 1 4 20 -0.93 0.00 2 4 20 -2.31 0.00 3 4 20 -1.42 0.00 4 4 20 -0.38 0.00 -5 5 20 0.68 0.00 -4 5 20 1.77 0.00 -3 5 20 3.19 0.00 -2 5 20 -2.32 0.00 -1 5 20 1.26 0.00 0 5 20 -0.76 0.00 1 5 20 -4.46 0.00 2 5 20 1.72 0.00 3 5 20 4.08 0.00 4 5 20 -1.18 0.00 -4 6 20 -1.82 0.00 -3 6 20 -0.92 0.00 -2 6 20 1.19 0.00 -1 6 20 -1.55 0.00 0 6 20 3.35 0.00 1 6 20 -1.02 0.00 2 6 20 -1.22 0.00 3 6 20 -1.61 0.00 4 6 20 -1.78 0.00 -4 7 20 1.61 0.00 -3 7 20 2.11 0.00 -2 7 20 -3.15 0.00 -1 7 20 1.60 0.00 0 7 20 1.12 0.00 1 7 20 -4.86 0.00 2 7 20 -0.74 0.00 3 7 20 1.40 0.00 4 7 20 -0.78 0.00 -4 8 20 -2.60 0.00 -3 8 20 -2.09 0.00 -2 8 20 -0.08 0.00 -1 8 20 -0.38 0.00 0 8 20 1.80 0.00 1 8 20 -2.00 0.00 2 8 20 -0.78 0.00 3 8 20 -0.77 0.00 4 8 20 -2.69 0.00 -4 9 20 2.38 0.00 -3 9 20 1.41 0.00 -2 9 20 -2.76 0.00 -1 9 20 2.08 0.00 0 9 20 2.88 0.00 1 9 20 -5.02 0.00 2 9 20 -2.47 0.00 3 9 20 -1.44 0.00 4 9 20 -1.19 0.00 -4 10 20 -2.69 0.00 -3 10 20 -2.99 0.00 -2 10 20 -0.50 0.00 -1 10 20 0.30 0.00 0 10 20 -0.51 0.00 1 10 20 -3.32 0.00 2 10 20 -0.16 0.00 3 10 20 0.10 0.00 4 10 20 -3.04 0.00 -4 11 20 2.85 0.00 -3 11 20 1.68 0.00 -2 11 20 -1.34 0.00 -1 11 20 1.56 0.00 0 11 20 3.31 0.00 1 11 20 -4.06 0.00 2 11 20 -2.10 0.00 3 11 20 -2.97 0.00 -3 12 20 -3.66 0.00 -2 12 20 -0.96 0.00 -1 12 20 0.40 0.00 0 12 20 -1.94 0.00 1 12 20 -3.86 0.00 2 12 20 0.74 0.00 3 12 20 0.13 0.00 -3 13 20 1.92 0.00 -2 13 20 0.01 0.00 -1 13 20 0.09 0.00 0 13 20 2.06 0.00 1 13 20 -2.10 0.00 2 13 20 -0.22 0.00 3 13 20 -2.92 0.00 -3 14 20 -3.48 0.00 -2 14 20 -1.64 0.00 -1 14 20 0.34 0.00 0 14 20 -1.07 0.00 1 14 20 -2.96 0.00 2 14 20 1.31 0.00 -2 15 20 0.42 0.00 -1 15 20 -0.84 0.00 0 15 20 0.02 0.00 1 15 20 -0.64 0.00 2 15 20 1.39 0.00 -1 16 20 0.48 0.00 0 16 20 0.96 0.00 1 16 20 -1.14 0.00 0 17 20 -1.35 0.00 -4 1 21 0.86 0.00 -3 1 21 -0.33 0.00 -2 1 21 -6.57 0.00 -1 1 21 2.04 0.00 0 1 21 -2.82 0.00 1 1 21 -4.30 0.00 2 1 21 4.78 0.00 3 1 21 4.77 0.00 4 1 21 1.16 0.00 -4 2 21 -1.21 0.00 -3 2 21 -3.47 0.00 -2 2 21 -1.62 0.00 -1 2 21 -0.47 0.00 0 2 21 -1.05 0.00 1 2 21 0.75 0.00 2 2 21 -0.24 0.00 3 2 21 -2.51 0.00 4 2 21 -0.46 0.00 -4 3 21 0.03 0.00 -3 3 21 -0.67 0.00 -2 3 21 -6.03 0.00 -1 3 21 1.28 0.00 0 3 21 -1.67 0.00 1 3 21 -3.54 0.00 2 3 21 3.07 0.00 3 3 21 2.88 0.00 -4 4 21 -1.45 0.00 -3 4 21 -4.81 0.00 -2 4 21 -2.18 0.00 -1 4 21 -0.28 0.00 0 4 21 -2.27 0.00 1 4 21 0.54 0.00 2 4 21 -0.33 0.00 3 4 21 -3.08 0.00 -3 5 21 -1.15 0.00 -2 5 21 -4.45 0.00 -1 5 21 0.64 0.00 0 5 21 -0.35 0.00 1 5 21 -2.64 0.00 2 5 21 1.35 0.00 3 5 21 0.25 0.00 -3 6 21 -3.76 0.00 -2 6 21 -1.31 0.00 -1 6 21 -0.07 0.00 0 6 21 -4.11 0.00 1 6 21 -0.31 0.00 2 6 21 -0.01 0.00 3 6 21 -1.69 0.00 -3 7 21 -1.03 0.00 -2 7 21 -2.02 0.00 -1 7 21 0.55 0.00 0 7 21 0.62 0.00 1 7 21 -1.59 0.00 2 7 21 0.99 0.00 3 7 21 -1.67 0.00 -3 8 21 -2.04 0.00 -2 8 21 0.10 0.00 -1 8 21 -0.48 0.00 0 8 21 -6.23 0.00 1 8 21 -0.84 0.00 2 8 21 0.82 0.00 3 8 21 0.01 0.00 -3 9 21 0.00 0.00 -2 9 21 0.27 0.00 -1 9 21 0.59 0.00 0 9 21 1.37 0.00 1 9 21 0.15 0.00 2 9 21 1.79 0.00 3 9 21 -2.06 0.00 -2 10 21 0.74 0.00 -1 10 21 -0.92 0.00 0 10 21 -6.94 0.00 1 10 21 -0.75 0.00 2 10 21 1.36 0.00 -2 11 21 1.67 0.00 -1 11 21 0.62 0.00 0 11 21 1.59 0.00 1 11 21 2.03 0.00 2 11 21 2.64 0.00 -2 12 21 0.50 0.00 -1 12 21 -0.60 0.00 0 12 21 -5.26 0.00 1 12 21 -0.31 0.00 -1 13 21 0.92 0.00 0 13 21 0.73 0.00 1 13 21 2.59 0.00 -2 0 22 2.57 0.00 -1 0 22 1.30 0.00 0 0 22 0.28 0.00 1 0 22 4.09 0.00 2 0 22 -2.92 0.00 -2 1 22 1.07 0.00 -1 1 22 -0.13 0.00 0 1 22 0.84 0.00 1 1 22 0.52 0.00 2 1 22 -0.29 0.00 -2 2 22 2.74 0.00 -1 2 22 1.72 0.00 0 2 22 -0.03 0.00 1 2 22 3.59 0.00 2 2 22 -2.61 0.00 -2 3 22 2.99 0.00 -1 3 22 -0.24 0.00 0 3 22 2.21 0.00 1 3 22 1.53 0.00 2 3 22 -0.49 0.00 -2 4 22 2.93 0.00 -1 4 22 2.12 0.00 0 4 22 -0.84 0.00 1 4 22 2.72 0.00 2 4 22 -1.92 0.00 -2 5 22 3.88 0.00 -1 5 22 -0.01 0.00 0 5 22 3.20 0.00 1 5 22 2.44 0.00 2 5 22 -0.07 0.00 -2 6 22 2.36 0.00 -1 6 22 1.50 0.00 0 6 22 -1.67 0.00 1 6 22 2.30 0.00 -1 7 22 0.49 0.00 0 7 22 4.27 0.00 1 7 22 3.22 0.00 -1 8 22 0.39 0.00 0 8 22 -1.84 0.00 1 8 22 2.02 0.00 0 9 22 4.87 0.00 11 0 0 4.33 0.00 11 1 0 -0.29 0.00 11 2 0 3.60 0.00 11 3 0 -0.73 0.00 10 15 0 -1.68 0.00 6 30 0 0.33 0.00 5 32 0 -1.64 0.00 0 36 0 -1.44 0.00 -11 1 1 -2.52 0.00 11 1 1 -3.58 0.00 -11 2 1 -1.54 0.00 11 2 1 0.30 0.00 -11 3 1 -1.58 0.00 11 3 1 -2.61 0.00 -10 15 1 0.60 0.00 10 15 1 -2.93 0.00 -6 30 1 0.94 0.00 6 30 1 2.32 0.00 -5 32 1 -0.15 0.00 5 32 1 0.80 0.00 -11 0 2 -0.39 0.00 0 0 2 -33.87 0.00 11 0 2 2.56 0.00 -11 1 2 0.75 0.00 -11 2 2 -0.19 0.00 -2 2 2 20.85 0.00 -10 15 2 -1.72 0.00 -6 30 2 0.81 0.00 6 30 2 -1.56 0.00 -2 35 2 1.76 0.00 2 35 2 -1.25 0.00 -10 14 3 -0.36 0.00 10 14 3 -1.86 0.00 -9 20 3 0.16 0.00 9 20 3 1.56 0.00 8 24 3 -0.65 0.00 -4 33 3 -1.21 0.00 4 33 3 -0.08 0.00 -2 35 3 -0.25 0.00 2 35 3 -0.48 0.00 10 13 4 0.10 0.00 -10 14 4 2.59 0.00 -9 20 4 1.02 0.00 -8 24 4 0.71 0.00 -7 27 4 0.73 0.00 7 27 4 -0.69 0.00 -4 33 4 -0.56 0.00 -3 34 4 1.08 0.00 3 34 4 1.86 0.00 10 12 5 0.69 0.00 -10 13 5 -1.21 0.00 -9 19 5 -1.08 0.00 9 19 5 -1.79 0.00 8 23 5 -0.41 0.00 -6 29 5 -0.05 0.00 6 29 5 0.41 0.00 -5 31 5 -0.08 0.00 5 31 5 1.53 0.00 -1 35 5 -0.35 0.00 0 35 5 -0.74 0.00 1 35 5 0.40 0.00 10 11 6 -0.03 0.00 -10 12 6 -0.45 0.00 9 18 6 3.01 0.00 -8 23 6 2.17 0.00 -7 26 6 0.87 0.00 7 26 6 -1.08 0.00 -4 32 6 -1.59 0.00 4 32 6 0.32 0.00 3 33 6 1.55 0.00 -2 34 6 -1.58 0.00 2 34 6 -0.84 0.00 10 9 7 -2.75 0.00 10 10 7 0.18 0.00 -10 11 7 -0.23 0.00 9 17 7 -2.32 0.00 -9 18 7 -0.66 0.00 -8 22 7 -0.80 0.00 8 22 7 1.30 0.00 -6 28 7 -0.17 0.00 6 28 7 -0.74 0.00 -5 30 7 0.29 0.00 5 30 7 -0.90 0.00 -1 34 7 -0.35 0.00 0 34 7 -0.79 0.00 1 34 7 -0.05 0.00 10 7 8 -1.28 0.00 10 8 8 2.07 0.00 -10 9 8 0.54 0.00 9 16 8 0.43 0.00 -9 17 8 0.56 0.00 8 21 8 -0.52 0.00 -7 25 8 1.21 0.00 6 27 8 0.71 0.00 -4 31 8 -1.31 0.00 4 31 8 0.27 0.00 3 32 8 -0.31 0.00 -2 33 8 0.61 0.00 2 33 8 0.11 0.00 10 1 9 -5.12 0.00 10 2 9 -0.22 0.00 10 3 9 -4.57 0.00 10 4 9 -0.33 0.00 10 5 9 -3.38 0.00 -10 6 9 -1.70 0.00 -10 7 9 1.24 0.00 9 15 9 0.82 0.00 8 20 9 -0.51 0.00 -7 24 9 0.07 0.00 4 30 9 1.39 0.00 -1 33 9 -2.26 0.00 0 33 9 -1.15 0.00 -10 0 10 -2.94 0.00 -10 1 10 0.55 0.00 -10 2 10 -2.47 0.00 9 13 10 -1.23 0.00 -9 14 10 -1.33 0.00 -8 19 10 0.60 0.00 8 19 10 1.22 0.00 -7 23 10 -1.44 0.00 -6 26 10 0.17 0.00 -5 28 10 -1.09 0.00 -1 32 10 2.03 0.00 1 32 10 0.20 0.00 9 11 11 -1.27 0.00 -9 12 11 -0.82 0.00 8 17 11 -0.21 0.00 -8 18 11 -2.18 0.00 -7 22 11 1.12 0.00 -6 25 11 -0.36 0.00 -5 27 11 1.44 0.00 -3 30 11 1.35 0.00 3 30 11 -0.75 0.00 -2 31 11 0.06 0.00 9 7 12 -2.16 0.00 9 8 12 1.72 0.00 -9 9 12 0.68 0.00 -8 16 12 1.16 0.00 7 20 12 1.62 0.00 6 23 12 -0.72 0.00 -5 26 12 -0.12 0.00 -3 29 12 1.38 0.00 3 29 12 -0.97 0.00 -2 30 12 0.13 0.00 9 1 13 0.04 0.00 9 2 13 -0.19 0.00 -9 4 13 -0.82 0.00 -9 5 13 -1.29 0.00 -9 6 13 -1.01 0.00 8 13 13 0.81 0.00 -8 14 13 2.51 0.00 -7 19 13 -1.69 0.00 6 22 13 0.82 0.00 -5 25 13 -0.46 0.00 -3 28 13 -0.81 0.00 -2 29 13 0.63 0.00 8 10 14 -1.93 0.00 8 11 14 -0.18 0.00 -8 12 14 -0.14 0.00 -7 17 14 -2.12 0.00 6 20 14 0.49 0.00 -6 21 14 0.43 0.00 5 23 14 1.29 0.00 4 25 14 1.54 0.00 -1 28 14 -0.11 0.00 1 28 14 1.05 0.00 8 6 15 -1.52 0.00 8 7 15 0.31 0.00 -8 8 15 -0.63 0.00 -8 9 15 2.09 0.00 7 14 15 -0.97 0.00 -7 15 15 -1.01 0.00 -6 19 15 -0.50 0.00 -5 22 15 -2.39 0.00 -4 24 15 -2.12 0.00 3 25 15 0.87 0.00 2 26 15 -0.13 0.00 -1 27 15 -0.55 0.00 0 27 15 0.52 0.00 1 27 15 0.56 0.00 -8 0 16 -0.36 0.00 -8 1 16 -0.49 0.00 -8 2 16 -0.76 0.00 7 11 16 0.72 0.00 -7 12 16 -0.97 0.00 6 16 16 2.35 0.00 -6 17 16 -0.64 0.00 -5 20 16 0.96 0.00 -4 22 16 -0.15 0.00 4 22 16 -0.47 0.00 -3 24 16 1.48 0.00 -2 25 16 0.02 0.00 7 6 17 0.58 0.00 7 7 17 0.67 0.00 -7 8 17 1.78 0.00 -7 9 17 2.39 0.00 6 13 17 -0.80 0.00 -6 14 17 0.56 0.00 5 17 17 -0.25 0.00 -5 18 17 0.09 0.00 -4 20 17 -1.01 0.00 4 20 17 -0.02 0.00 -3 22 17 0.85 0.00 3 22 17 -2.06 0.00 -2 23 17 0.34 0.00 2 23 17 -0.49 0.00 -1 24 17 0.33 0.00 0 24 17 1.98 0.00 6 10 18 1.01 0.00 -6 11 18 -0.45 0.00 -5 15 18 0.62 0.00 -4 18 18 -2.05 0.00 -3 20 18 -0.63 0.00 -2 21 18 0.17 0.00 2 21 18 -2.01 0.00 -1 22 18 0.59 0.00 0 22 18 1.20 0.00 1 22 18 0.42 0.00 6 1 19 -4.72 0.00 6 2 19 -0.65 0.00 6 3 19 -2.70 0.00 -6 4 19 -0.49 0.00 -6 5 19 0.72 0.00 -6 6 19 -1.13 0.00 5 11 19 0.52 0.00 -5 12 19 -1.31 0.00 -4 15 19 3.01 0.00 4 15 19 0.45 0.00 3 17 19 -0.22 0.00 -2 19 19 -1.02 0.00 2 19 19 -1.68 0.00 -1 20 19 0.65 0.00 0 20 19 3.16 0.00 5 3 20 -1.94 0.00 5 4 20 -0.78 0.00 5 5 20 -2.43 0.00 -5 6 20 -0.62 0.00 5 6 20 -0.40 0.00 -5 7 20 1.08 0.00 4 11 20 -1.84 0.00 -4 12 20 -1.74 0.00 3 14 20 -0.36 0.00 -3 15 20 1.20 0.00 -2 16 20 -1.57 0.00 2 16 20 1.32 0.00 -1 17 20 -0.50 0.00 1 17 20 -0.42 0.00 4 3 21 1.69 0.00 4 4 21 -0.79 0.00 -4 5 21 -0.21 0.00 4 5 21 1.93 0.00 -4 6 21 -1.07 0.00 -4 7 21 0.69 0.00 -3 10 21 -1.13 0.00 3 10 21 0.67 0.00 -3 11 21 1.13 0.00 2 12 21 0.94 0.00 -2 13 21 2.12 0.00 -1 14 21 0.06 0.00 0 14 21 -2.49 0.00 1 14 21 0.30 0.00 -3 0 22 -1.99 0.00 3 0 22 -5.56 0.00 -3 1 22 0.78 0.00 3 1 22 -0.16 0.00 -3 2 22 -1.13 0.00 3 2 22 -4.28 0.00 -3 3 22 1.60 0.00 -3 4 22 0.87 0.00 2 6 22 -1.28 0.00 -2 7 22 3.23 0.00 2 7 22 0.22 0.00 -2 8 22 0.90 0.00 -1 9 22 0.92 0.00 1 9 22 3.48 0.00 -1 10 22 -0.23 0.00 0 10 22 -1.08 0.00 0 0 0 0.00 0.00 # SQUEEZE RESULTS (Version = 160617) # Note: Data are Listed for all Voids in the P1 Unit Cell # i.e. Centre of Gravity, Solvent Accessible Volume, # Recovered number of Electrons in the Void and # Details about the Squeezed Material loop_ _platon_squeeze_void_nr _platon_squeeze_void_average_x _platon_squeeze_void_average_y _platon_squeeze_void_average_z _platon_squeeze_void_volume _platon_squeeze_void_count_electrons _platon_squeeze_void_content 1 0.000 0.000 0.500 347 160 ' ' 2 0.000 0.500 1.000 347 160 ' ' # Missing Reflections Below sin(th)/lambda = 0.25 loop_ _platon_missing_refln_index_h _platon_missing_refln_index_k _platon_missing_refln_index_l _platon_missing_refln_theta 0 0 2 2.052 -2 2 2 4.892 _platon_squeeze_void_probe_radius 1.20 _platon_squeeze_details ) TITL znnccupf6 P 1 21/c 1 R = 0.12 CELL 9.5500 31.1090 19.8490 90.00 90.77 90.00 SPGR P21/c # Solvent Accessible Volume = 695 # Electrons Found in S.A.V. = 320 # Note: Atoms in Void are Labelled as Cxxx and Qxxx for all Others C101 0.718 0.969 0.653 ! 7.17 eA-3 C102 0.024 0.526 0.169 ! 6.16 eA-3 Q103 0.592 0.505 0.160 ! 4.00 eA-3 C104 0.851 0.523 0.202 ! 3.80 eA-3 Q105 0.202 0.556 0.011 ! 2.80 eA-3 C106 0.963 0.012 0.532 ! 2.63 eA-3 Q107 0.256 0.945 0.580 ! 1.19 eA-3 C108 0.156 0.488 0.902 ! 1.08 eA-3 C109 0.168 0.546 0.082 ! 1.06 eA-3 Q110 0.963 0.543 0.092 ! 0.90 eA-3 Q111 0.123 0.990 0.334 ! 0.87 eA-3 Q112 0.730 0.016 0.281 ! 0.86 eA-3 C113 0.975 0.497 0.223 ! 0.80 eA-3 Q114 0.168 0.960 0.672 ! 0.79 eA-3 Q115 0.475 0.431-0.004 ! 0.79 eA-3 Q116 0.522 0.383 0.109 ! 0.78 eA-3 Q117 0.320 0.718 0.701 ! 0.78 eA-3 Q118 0.622 0.525 0.440 ! 0.77 eA-3 C119 0.997 0.967 0.425 ! 0.77 eA-3 C120 0.967 0.500 0.903 ! 0.77 eA-3 Q121 0.410 0.088 0.642 ! 0.75 eA-3 Q122 0.566 0.446 0.048 ! 0.74 eA-3 Q123 0.380 0.055 0.547 ! 0.73 eA-3 Q124 0.754 0.336 0.626 ! 0.71 eA-3 Q125 0.655 0.543 0.047 ! 0.67 eA-3 Q126 0.119 0.920 0.611 ! 0.66 eA-3 Q127 0.134 0.899 0.675 ! 0.66 eA-3 Q128 0.136 0.536 0.912 ! 0.66 eA-3 Q129 0.592 0.484 0.922 ! 0.65 eA-3 C130 0.285 0.507 0.905 ! 0.64 eA-3 Q131 0.123 0.472 0.966 ! 0.64 eA-3 Q132 1.020 0.080 0.375 ! 0.64 eA-3 Q133 0.154 0.897 0.348 ! 0.63 eA-3 Q134 0.784 0.450 0.059 ! 0.63 eA-3 Q135 1.002 0.883 0.467 ! 0.62 eA-3 Q136 0.077 0.571 0.033 ! 0.62 eA-3 Q137 0.212 0.049 0.421 ! 0.61 eA-3 Q138 0.111 0.544 0.231 ! 0.61 eA-3 Q139 0.617 0.016 0.562 ! 0.61 eA-3 Q140 0.878 0.064 0.563 ! 0.61 eA-3 Q141 0.341 0.523 0.842 ! 0.61 eA-3 Q142 0.626 0.424 0.001 ! 0.59 eA-3 Q143 0.804 0.065 0.357 ! 0.59 eA-3 Q144 0.266 0.549 0.952 ! 0.58 eA-3 Q145 0.957 0.936 0.548 ! 0.58 eA-3 Q146 0.506 0.463 0.013 ! 0.58 eA-3 Q147 0.190 0.396 0.933 ! 0.58 eA-3 Q148 0.344 0.541 0.018 ! 0.58 eA-3 Q149 0.222 0.984 0.271 ! 0.58 eA-3 Q150 0.460 0.514 0.798 ! 0.57 eA-3 Q151 0.584 0.515 0.967 ! 0.57 eA-3 Q152 0.940 0.516 0.404 ! 0.56 eA-3 Q153 0.562 0.455 0.126 ! 0.56 eA-3 Q154 0.892 0.427 0.001 ! 0.56 eA-3 Q155 0.463 0.668 0.125 ! 0.56 eA-3 Q156 0.537 0.332 0.875 ! 0.56 eA-3 Q157 0.601 0.008 0.360 ! 0.56 eA-3 Q158 0.177 0.620 0.032 ! 0.56 eA-3 Q159 0.145 0.429 0.967 ! 0.56 eA-3 Q160 0.283 0.042 0.487 ! 0.56 eA-3 Q161 0.182 0.933 0.281 ! 0.55 eA-3 Q162 0.555 0.319 0.894 ! 0.55 eA-3 Q163 0.914 0.625-0.005 ! 0.55 eA-3 Q164 0.030 0.647 0.942 ! 0.55 eA-3 Q165 0.869 0.984 0.394 ! 0.55 eA-3 Q166 0.841 0.008 0.392 ! 0.55 eA-3 Q167 0.751 0.015 0.548 ! 0.55 eA-3 Q168 0.277 0.448 0.046 ! 0.55 eA-3 Q169 0.444 0.463 0.892 ! 0.54 eA-3 Q170 0.814 0.047 0.653 ! 0.54 eA-3 Q171 0.611 0.578 0.908 ! 0.54 eA-3 Q172 0.665 0.398 0.046 ! 0.54 eA-3 Q173 0.648 0.947 0.499 ! 0.53 eA-3 Q174 0.385 0.921 0.607 ! 0.53 eA-3 Q175 0.599 0.281 0.592 ! 0.52 eA-3 Q176 0.034 0.358 0.967 ! 0.52 eA-3 Q177 0.402 0.595 0.968 ! 0.52 eA-3 Q178 0.145 0.572 0.184 ! 0.52 eA-3 Q179 0.723 0.177 0.355 ! 0.52 eA-3 Q180 0.700 0.898 0.658 ! 0.52 eA-3 Q181 0.180 0.009 0.768 ! 0.52 eA-3 Q182 0.470 0.467 0.078 ! 0.51 eA-3 Q183 0.880 0.063 0.644 ! 0.51 eA-3 Q184 0.593 0.234 0.075 ! 0.51 eA-3 Q185 0.464 0.115 0.683 ! 0.51 eA-3 Q186 0.568 0.562 0.092 ! 0.51 eA-3 Q187 0.458 0.112 0.499 ! 0.51 eA-3 Q188 0.652 0.017 0.498 ! 0.51 eA-3 Q189 0.724 0.459 0.184 ! 0.51 eA-3 Q190 0.431 0.094 0.326 ! 0.51 eA-3 Q191 0.087 0.852 0.544 ! 0.51 eA-3 Q192 0.069 0.150 0.532 ! 0.50 eA-3 ) ; _shelx_fab_checksum 84795 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.73980(8) 0.21883(2) 0.76520(4) 0.0213(2) Uani 1 1 d . . . . . Cu1 Cu 0.80162(8) 0.33157(3) 0.58557(4) 0.0245(3) Uani 1 1 d . . . . . N1 N 0.5414(6) 0.21056(17) 0.7232(3) 0.0223(14) Uani 1 1 d . . . . . N2 N 0.6627(6) 0.27154(17) 0.8174(3) 0.0223(14) Uani 1 1 d . . . . . N3 N 0.9031(5) 0.21650(17) 0.8343(3) 0.0194(13) Uani 1 1 d . . . . . N4 N 0.7835(6) 0.15586(17) 0.7392(3) 0.0244(14) Uani 1 1 d . . . . . N5 N 0.8174(6) 0.25456(19) 0.6838(3) 0.0264(14) Uani 1 1 d . . . . . N6 N 0.6637(5) 0.30473(19) 0.5164(3) 0.0260(14) Uani 1 1 d . . . . . N7 N 0.7883(5) 0.38154(17) 0.5198(3) 0.0283(15) Uani 1 1 d . . . . . N8 N 0.7198(5) 0.37723(17) 0.6510(3) 0.0249(14) Uani 1 1 d . . . . . N9 N 1.0076(6) 0.33695(18) 0.5633(3) 0.0265(14) Uani 1 1 d . . . . . C1 C 0.5049(7) 0.1795(2) 0.6774(3) 0.0256(18) Uani 1 1 d . . . . . C2 C 0.3730(8) 0.1903(2) 0.6456(4) 0.036(2) Uani 1 1 d . . . . . H2 H 0.324579 0.174263 0.611927 0.043 Uiso 1 1 calc R . . . . C3 C 0.3320(7) 0.2279(2) 0.6734(4) 0.0309(19) Uani 1 1 d . . . . . H3 H 0.247758 0.242867 0.662996 0.037 Uiso 1 1 calc R . . . . C4 C 0.4372(7) 0.2411(2) 0.7211(3) 0.0251(18) Uani 1 1 d . . . . . C5 C 0.4371(7) 0.2791(2) 0.7581(3) 0.0235(17) Uani 1 1 d . . . . . C6 C 0.3154(7) 0.3090(2) 0.7467(3) 0.0217(17) Uani 1 1 d . . . . . C7 C 0.1812(7) 0.2982(2) 0.7660(3) 0.0281(18) Uani 1 1 d . . . . . H7 H 0.164743 0.270980 0.786033 0.034 Uiso 1 1 calc R . . . . C8 C 0.0706(7) 0.3263(2) 0.7565(3) 0.0307(18) Uani 1 1 d . . . . . H8 H -0.021174 0.318381 0.769578 0.037 Uiso 1 1 calc R . . . . C9 C 0.0946(8) 0.3659(2) 0.7280(4) 0.0325(19) Uani 1 1 d . . . . . H9 H 0.019409 0.385649 0.722023 0.039 Uiso 1 1 calc R . . . . C10 C 0.2267(7) 0.3770(2) 0.7082(3) 0.0297(18) Uani 1 1 d . . . . . H10 H 0.242621 0.404165 0.687808 0.036 Uiso 1 1 calc R . . . . C11 C 0.3368(7) 0.3488(2) 0.7179(3) 0.0250(17) Uani 1 1 d . . . . . H11 H 0.428301 0.356920 0.704534 0.030 Uiso 1 1 calc R . . . . C12 C 0.5390(7) 0.2922(2) 0.8049(3) 0.0216(17) Uani 1 1 d . . . . . C13 C 0.5270(7) 0.3283(2) 0.8501(3) 0.0230(17) Uani 1 1 d . . . . . H13 H 0.450680 0.347823 0.851865 0.028 Uiso 1 1 calc R . . . . C14 C 0.6411(7) 0.3293(2) 0.8886(3) 0.0257(17) Uani 1 1 d . . . . . H14 H 0.661567 0.349506 0.923214 0.031 Uiso 1 1 calc R . . . . C15 C 0.7287(7) 0.2939(2) 0.8681(3) 0.0199(17) Uani 1 1 d . . . . . C16 C 0.8580(7) 0.2826(2) 0.8985(3) 0.0238(17) Uani 1 1 d D . . . . C17 C 0.9268(18) 0.3105(5) 0.9518(9) 0.0231(17) Uani 0.350(9) 1 d D U P A 1 C18 C 1.0425(18) 0.3365(5) 0.9405(6) 0.030(5) Uani 0.350(9) 1 d G U P A 1 H18 H 1.078954 0.338994 0.896369 0.036 Uiso 0.350(9) 1 calc R . P A 1 C19 C 1.1048(17) 0.3587(5) 0.9937(8) 0.034(5) Uani 0.350(9) 1 d G U P A 1 H19 H 1.183843 0.376503 0.985901 0.041 Uiso 0.350(9) 1 calc R . P A 1 C20 C 1.051(2) 0.3550(6) 1.0582(7) 0.026(5) Uani 0.350(9) 1 d G U P A 1 H20 H 1.094012 0.370243 1.094563 0.031 Uiso 0.350(9) 1 calc R . P A 1 C21 C 0.936(2) 0.3290(8) 1.0696(7) 0.030(5) Uani 0.350(9) 1 d G U P A 1 H21 H 0.899291 0.326473 1.113694 0.036 Uiso 0.350(9) 1 calc R . P A 1 C22 C 0.873(2) 0.3067(7) 1.0164(10) 0.023(3) Uani 0.350(9) 1 d G U P A 1 H22 H 0.794400 0.288963 1.024163 0.027 Uiso 0.350(9) 1 calc R . P A 1 C17A C 0.9107(10) 0.3123(3) 0.9537(5) 0.0231(17) Uani 0.650(9) 1 d D U P A 2 C18A C 0.9712(11) 0.3513(3) 0.9358(4) 0.037(3) Uani 0.650(9) 1 d G U P A 2 H18A H 0.972525 0.359828 0.889873 0.044 Uiso 0.650(9) 1 calc R . P A 2 C19A C 1.0297(11) 0.3777(3) 0.9851(5) 0.048(4) Uani 0.650(9) 1 d G U P A 2 H19A H 1.071073 0.404280 0.972948 0.057 Uiso 0.650(9) 1 calc R . P A 2 C20A C 1.0277(11) 0.3651(3) 1.0523(4) 0.042(4) Uani 0.650(9) 1 d G U P A 2 H20A H 1.067738 0.383189 1.086075 0.050 Uiso 0.650(9) 1 calc R . P A 2 C21A C 0.9672(12) 0.3262(4) 1.0702(4) 0.029(3) Uani 0.650(9) 1 d G U P A 2 H21A H 0.965857 0.317646 1.116127 0.035 Uiso 0.650(9) 1 calc R . P A 2 C22A C 0.9087(11) 0.2998(3) 1.0209(5) 0.023(3) Uani 0.650(9) 1 d G U P A 2 H22A H 0.867308 0.273194 1.033053 0.027 Uiso 0.650(9) 1 calc R . P A 2 C23 C 0.9370(7) 0.2465(2) 0.8826(3) 0.0197(17) Uani 1 1 d . . . . . C24 C 1.0652(7) 0.2348(2) 0.9152(3) 0.0262(18) Uani 1 1 d . . . . . H24 H 1.111997 0.250307 0.950005 0.031 Uiso 1 1 calc R . . . . C25 C 1.1074(7) 0.1977(2) 0.8874(3) 0.0271(18) Uani 1 1 d . . . . . H25 H 1.189572 0.182105 0.899235 0.033 Uiso 1 1 calc R . . . . C26 C 1.0066(7) 0.1861(2) 0.8369(3) 0.0239(17) Uani 1 1 d . . . . . C27 C 1.0083(7) 0.1477(2) 0.7989(3) 0.0262(18) Uani 1 1 d . . . . . C28 C 1.1314(7) 0.1186(2) 0.8107(3) 0.0254(18) Uani 1 1 d . . . . . C29 C 1.2649(8) 0.1309(2) 0.7940(4) 0.037(2) Uani 1 1 d . . . . . H29 H 1.280005 0.158102 0.773498 0.044 Uiso 1 1 calc R . . . . C30 C 1.3777(7) 0.1039(2) 0.8069(4) 0.039(2) Uani 1 1 d . . . . . H30 H 1.469233 0.112605 0.794628 0.047 Uiso 1 1 calc R . . . . C31 C 1.3584(8) 0.0651(2) 0.8368(4) 0.040(2) Uani 1 1 d . . . . . H31 H 1.436223 0.046894 0.845906 0.048 Uiso 1 1 calc R . . . . C32 C 1.2263(8) 0.0524(2) 0.8537(4) 0.040(2) Uani 1 1 d . . . . . H32 H 1.212733 0.025223 0.874455 0.048 Uiso 1 1 calc R . . . . C33 C 1.1114(8) 0.0789(2) 0.8408(3) 0.0313(19) Uani 1 1 d . . . . . H33 H 1.019927 0.069848 0.852583 0.038 Uiso 1 1 calc R . . . . C34 C 0.9048(7) 0.1340(2) 0.7539(3) 0.0253(18) Uani 1 1 d . . . . . C35 C 0.9077(8) 0.0948(2) 0.7156(4) 0.0323(19) Uani 1 1 d . . . . . H35 H 0.980345 0.073933 0.716127 0.039 Uiso 1 1 calc R . . . . C36 C 0.7891(8) 0.0931(2) 0.6790(4) 0.0332(19) Uani 1 1 d . . . . . H36 H 0.761265 0.070673 0.649223 0.040 Uiso 1 1 calc R . . . . C37 C 0.7115(8) 0.1317(2) 0.6930(3) 0.0294(18) Uani 1 1 d . . . . . C38 C 0.5835(8) 0.1422(2) 0.6632(3) 0.0291(19) Uani 1 1 d D . . . . C39 C 0.5107(18) 0.1109(4) 0.6150(6) 0.0369(19) Uani 0.350(9) 1 d D U P A 1 C40 C 0.4998(19) 0.1212(4) 0.5470(7) 0.045(5) Uani 0.350(9) 1 d G U P A 1 H40 H 0.535673 0.147786 0.531072 0.054 Uiso 0.350(9) 1 calc R . P A 1 C41 C 0.436(2) 0.0927(5) 0.5022(5) 0.051(5) Uani 0.350(9) 1 d G U P A 1 H41 H 0.428752 0.099704 0.455730 0.061 Uiso 0.350(9) 1 calc R . P A 1 C42 C 0.384(2) 0.0538(4) 0.5255(7) 0.053(6) Uani 0.350(9) 1 d G U P A 1 H42 H 0.340309 0.034294 0.494880 0.063 Uiso 0.350(9) 1 calc R . P A 1 C43 C 0.395(2) 0.0435(4) 0.5935(8) 0.056(6) Uani 0.350(9) 1 d G U P A 1 H43 H 0.358786 0.016965 0.609372 0.067 Uiso 0.350(9) 1 calc R . P A 1 C44 C 0.458(2) 0.0721(5) 0.6382(6) 0.053(6) Uani 0.350(9) 1 d G U P A 1 H44 H 0.465707 0.065047 0.684715 0.064 Uiso 0.350(9) 1 calc R . P A 1 C39A C 0.5303(9) 0.1111(2) 0.6101(4) 0.0369(19) Uani 0.650(9) 1 d D U P A 2 C40A C 0.6039(9) 0.1037(3) 0.5513(4) 0.044(3) Uani 0.650(9) 1 d G U P A 2 H40A H 0.688633 0.118737 0.543286 0.053 Uiso 0.650(9) 1 calc R . P A 2 C41A C 0.5536(11) 0.0743(3) 0.5041(4) 0.062(4) Uani 0.650(9) 1 d G U P A 2 H41A H 0.603914 0.069206 0.463935 0.075 Uiso 0.650(9) 1 calc R . P A 2 C42A C 0.4297(11) 0.0522(2) 0.5158(5) 0.067(4) Uani 0.650(9) 1 d G U P A 2 H42A H 0.395281 0.032105 0.483605 0.080 Uiso 0.650(9) 1 calc R . P A 2 C43A C 0.3561(8) 0.0596(3) 0.5746(5) 0.057(4) Uani 0.650(9) 1 d G U P A 2 H43A H 0.271367 0.044535 0.582627 0.069 Uiso 0.650(9) 1 calc R . P A 2 C44A C 0.4064(8) 0.0890(3) 0.6218(4) 0.047(3) Uani 0.650(9) 1 d G U P A 2 H44A H 0.356084 0.094066 0.661979 0.056 Uiso 0.650(9) 1 calc R . P A 2 C45 C 0.8133(6) 0.2829(2) 0.6465(3) 0.0210(16) Uani 1 1 d . . . . . C46 C 0.5818(7) 0.2709(2) 0.5243(4) 0.0317(19) Uani 1 1 d . . . . . H46 H 0.586871 0.255291 0.565394 0.038 Uiso 1 1 calc R . . . . C47 C 0.4894(8) 0.2576(3) 0.4747(5) 0.045(2) Uani 1 1 d . . . . . H47 H 0.432602 0.232965 0.481309 0.054 Uiso 1 1 calc R . . . . C48 C 0.4804(8) 0.2803(3) 0.4161(5) 0.046(2) Uani 1 1 d . . . . . H48 H 0.416040 0.271754 0.381669 0.055 Uiso 1 1 calc R . . . . C49 C 0.5646(8) 0.3156(3) 0.4069(4) 0.041(2) Uani 1 1 d . . . . . H49 H 0.559582 0.331671 0.366236 0.050 Uiso 1 1 calc R . . . . C50 C 0.6577(7) 0.3272(2) 0.4584(4) 0.0288(18) Uani 1 1 d . . . . . C51 C 0.7582(8) 0.3632(2) 0.4523(4) 0.038(2) Uani 1 1 d . . . . . H51A H 0.846108 0.352712 0.432098 0.046 Uiso 1 1 calc R . . . . H51B H 0.718223 0.385665 0.422412 0.046 Uiso 1 1 calc R . . . . C52 C 0.7174(7) 0.3767(2) 0.7184(4) 0.0296(18) Uani 1 1 d . . . . . H52 H 0.747503 0.351504 0.741432 0.036 Uiso 1 1 calc R . . . . C53 C 0.6731(7) 0.4111(2) 0.7552(4) 0.0356(19) Uani 1 1 d . . . . . H53 H 0.674904 0.410165 0.803059 0.043 Uiso 1 1 calc R . . . . C54 C 0.6261(8) 0.4470(2) 0.7220(4) 0.041(2) Uani 1 1 d . . . . . H54 H 0.594629 0.471284 0.746514 0.049 Uiso 1 1 calc R . . . . C55 C 0.6249(7) 0.4475(2) 0.6524(4) 0.034(2) Uani 1 1 d . . . . . H55 H 0.590959 0.472022 0.628758 0.041 Uiso 1 1 calc R . . . . C56 C 0.6731(6) 0.4123(2) 0.6175(4) 0.0267(18) Uani 1 1 d . . . . . C57 C 0.6729(7) 0.4097(2) 0.5423(4) 0.0312(19) Uani 1 1 d . . . . . H57A H 0.582132 0.398052 0.525953 0.037 Uiso 1 1 calc R . . . . H57B H 0.684629 0.438818 0.523090 0.037 Uiso 1 1 calc R . . . . C58 C 1.1076(7) 0.3083(2) 0.5769(3) 0.0285(18) Uani 1 1 d . . . . . H58 H 1.083037 0.282116 0.598451 0.034 Uiso 1 1 calc R . . . . C59 C 1.2456(7) 0.3152(3) 0.5607(3) 0.0319(19) Uani 1 1 d . . . . . H59 H 1.315716 0.294707 0.571886 0.038 Uiso 1 1 calc R . . . . C60 C 1.2787(8) 0.3522(3) 0.5283(4) 0.036(2) Uani 1 1 d . . . . . H60 H 1.373112 0.357441 0.516173 0.043 Uiso 1 1 calc R . . . . C61 C 1.1778(8) 0.3822(2) 0.5127(3) 0.0334(19) Uani 1 1 d . . . . . H61 H 1.200343 0.408074 0.489788 0.040 Uiso 1 1 calc R . . . . C62 C 1.0414(7) 0.3732(2) 0.5317(3) 0.0271(18) Uani 1 1 d . . . . . C63 C 0.9243(7) 0.4048(2) 0.5227(4) 0.0313(19) Uani 1 1 d . . . . . H63A H 0.924598 0.425333 0.560749 0.038 Uiso 1 1 calc R . . . . H63B H 0.937266 0.421200 0.480513 0.038 Uiso 1 1 calc R . . . . P1 P 1.2613(2) 0.49341(7) 0.59553(11) 0.0411(6) Uani 1 1 d . . . . . F1 F 1.1267(5) 0.46949(16) 0.6215(3) 0.0705(15) Uani 1 1 d . . . . . F2 F 1.3401(5) 0.44945(15) 0.5811(3) 0.0733(16) Uani 1 1 d . . . . . F3 F 1.1980(5) 0.49373(15) 0.5210(2) 0.0665(15) Uani 1 1 d . . . . . F4 F 1.4004(5) 0.51682(15) 0.5684(2) 0.0653(14) Uani 1 1 d . . . . . F5 F 1.1989(5) 0.53949(15) 0.6073(2) 0.0672(15) Uani 1 1 d . . . . . F6 F 1.3273(4) 0.49322(14) 0.6698(2) 0.0495(12) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.0250(5) 0.0180(5) 0.0209(5) 0.0017(4) -0.0025(4) -0.0015(4) Cu1 0.0218(5) 0.0231(5) 0.0286(5) 0.0083(4) 0.0015(4) 0.0011(4) N1 0.030(4) 0.018(3) 0.019(3) 0.001(3) -0.003(3) -0.004(3) N2 0.023(3) 0.023(3) 0.021(3) -0.001(3) -0.003(3) -0.004(3) N3 0.021(3) 0.022(3) 0.016(3) 0.003(3) 0.000(3) -0.001(3) N4 0.028(4) 0.022(3) 0.023(3) 0.008(3) -0.006(3) 0.000(3) N5 0.030(4) 0.023(4) 0.026(4) 0.002(3) 0.000(3) 0.004(3) N6 0.021(3) 0.025(4) 0.032(4) 0.000(3) 0.000(3) 0.005(3) N7 0.022(4) 0.032(4) 0.031(4) 0.012(3) 0.002(3) 0.003(3) N8 0.016(3) 0.019(4) 0.039(4) 0.011(3) 0.000(3) -0.002(3) N9 0.027(4) 0.023(4) 0.029(4) 0.006(3) 0.001(3) 0.003(3) C1 0.030(5) 0.020(4) 0.027(4) 0.006(4) -0.001(4) -0.002(4) C2 0.052(5) 0.018(5) 0.037(5) -0.002(4) -0.019(4) -0.006(4) C3 0.026(4) 0.030(5) 0.036(5) 0.009(4) -0.015(4) -0.007(4) C4 0.021(4) 0.022(5) 0.032(5) 0.007(4) 0.004(4) -0.001(4) C5 0.019(4) 0.024(4) 0.028(4) 0.003(4) -0.001(4) -0.002(3) C6 0.020(4) 0.030(5) 0.015(4) 0.000(3) -0.004(3) -0.001(4) C7 0.031(5) 0.028(4) 0.026(4) 0.005(3) 0.003(4) -0.003(4) C8 0.023(4) 0.039(5) 0.030(4) -0.001(4) 0.004(3) -0.002(4) C9 0.028(5) 0.033(5) 0.036(5) -0.006(4) -0.002(4) 0.007(4) C10 0.033(5) 0.022(4) 0.034(5) 0.006(3) -0.001(4) 0.003(4) C11 0.022(4) 0.028(5) 0.024(4) 0.004(4) -0.003(3) -0.007(4) C12 0.027(5) 0.016(4) 0.021(4) 0.000(3) -0.004(4) 0.001(3) C13 0.017(4) 0.031(5) 0.021(4) 0.005(4) 0.005(4) 0.005(3) C14 0.017(4) 0.033(5) 0.027(4) -0.003(4) 0.004(4) -0.006(4) C15 0.028(4) 0.025(4) 0.007(4) 0.003(3) 0.006(3) 0.003(4) C16 0.029(4) 0.020(4) 0.023(4) 0.005(3) -0.001(4) -0.004(4) C17 0.021(4) 0.023(4) 0.026(3) -0.002(3) -0.002(3) 0.000(3) C18 0.031(10) 0.035(11) 0.024(8) 0.005(8) -0.008(7) -0.009(8) C19 0.033(11) 0.039(12) 0.029(8) -0.003(8) -0.002(8) -0.014(9) C20 0.027(9) 0.024(10) 0.025(8) 0.000(8) -0.008(8) -0.001(8) C21 0.029(10) 0.035(11) 0.026(8) 0.003(8) -0.007(7) -0.005(9) C22 0.018(6) 0.024(5) 0.026(3) 0.003(3) -0.005(4) -0.001(5) C17A 0.021(4) 0.023(4) 0.026(3) -0.002(3) -0.002(3) 0.000(3) C18A 0.049(8) 0.033(6) 0.028(6) 0.002(5) 0.000(6) -0.014(6) C19A 0.061(9) 0.042(8) 0.040(6) -0.005(5) -0.004(6) -0.021(7) C20A 0.045(8) 0.046(7) 0.034(6) -0.013(6) -0.007(6) -0.016(6) C21A 0.021(7) 0.043(7) 0.024(6) -0.004(5) -0.007(5) 0.002(6) C22A 0.018(6) 0.024(5) 0.026(3) 0.003(3) -0.005(4) -0.001(5) C23 0.021(4) 0.025(4) 0.013(4) 0.004(4) 0.000(3) -0.006(4) C24 0.026(4) 0.024(5) 0.029(4) 0.004(4) -0.004(4) -0.008(4) C25 0.027(4) 0.028(5) 0.026(4) 0.009(4) -0.003(4) 0.000(4) C26 0.021(4) 0.027(5) 0.024(4) 0.005(4) 0.002(4) -0.003(4) C27 0.024(4) 0.024(4) 0.031(4) 0.009(4) 0.003(4) -0.001(4) C28 0.028(5) 0.020(4) 0.028(4) -0.002(4) 0.001(3) 0.003(4) C29 0.039(5) 0.025(4) 0.046(5) 0.009(4) 0.003(4) 0.004(4) C30 0.020(4) 0.039(5) 0.059(6) -0.009(5) 0.009(4) 0.001(4) C31 0.040(6) 0.026(5) 0.055(6) 0.004(4) -0.004(4) 0.011(4) C32 0.048(6) 0.027(5) 0.045(5) 0.008(4) 0.005(4) 0.000(5) C33 0.037(5) 0.022(5) 0.035(5) 0.003(4) 0.006(4) 0.005(4) C34 0.025(5) 0.022(4) 0.029(4) 0.004(4) -0.002(4) 0.000(4) C35 0.040(5) 0.021(5) 0.036(5) -0.007(4) -0.002(4) 0.004(4) C36 0.052(5) 0.015(4) 0.033(5) -0.003(3) -0.005(4) 0.000(4) C37 0.040(5) 0.023(5) 0.026(4) -0.001(4) -0.011(4) -0.004(4) C38 0.044(5) 0.018(4) 0.025(4) 0.006(4) -0.009(4) -0.007(4) C39 0.057(5) 0.019(4) 0.035(4) -0.004(3) -0.020(4) 0.007(3) C40 0.072(13) 0.029(10) 0.033(7) -0.008(7) -0.017(8) -0.002(9) C41 0.083(13) 0.038(10) 0.031(9) -0.009(7) -0.021(9) -0.004(9) C42 0.078(14) 0.033(10) 0.045(10) -0.009(9) -0.031(10) -0.005(10) C43 0.088(14) 0.026(11) 0.052(10) 0.002(8) -0.035(10) -0.013(10) C44 0.091(15) 0.027(9) 0.041(10) 0.002(7) -0.035(10) -0.012(9) C39A 0.057(5) 0.019(4) 0.035(4) -0.004(3) -0.020(4) 0.007(3) C40A 0.074(8) 0.027(7) 0.031(6) 0.002(5) -0.015(5) 0.000(6) C41A 0.113(10) 0.030(7) 0.043(7) -0.011(5) -0.017(7) 0.003(6) C42A 0.103(10) 0.033(8) 0.063(8) -0.013(7) -0.038(7) -0.002(6) C43A 0.079(9) 0.023(7) 0.070(9) -0.002(6) -0.039(7) 0.002(6) C44A 0.049(7) 0.029(8) 0.061(8) -0.006(6) -0.023(6) 0.008(5) C45 0.015(4) 0.030(5) 0.018(4) -0.001(4) 0.005(3) 0.005(3) C46 0.030(4) 0.032(5) 0.033(5) -0.012(4) 0.000(4) 0.003(4) C47 0.035(5) 0.038(5) 0.062(7) -0.025(5) 0.006(5) 0.005(4) C48 0.026(5) 0.063(6) 0.048(6) -0.038(5) 0.000(4) 0.015(5) C49 0.035(5) 0.052(6) 0.038(5) -0.012(4) 0.004(4) 0.022(5) C50 0.016(4) 0.034(5) 0.036(5) -0.003(4) -0.002(4) 0.015(4) C51 0.040(5) 0.042(5) 0.033(5) 0.009(4) -0.002(4) 0.007(4) C52 0.021(4) 0.026(5) 0.043(6) 0.007(4) 0.003(4) -0.002(3) C53 0.034(5) 0.032(5) 0.041(5) -0.006(5) 0.001(4) -0.002(4) C54 0.041(5) 0.021(5) 0.061(7) -0.012(4) -0.001(4) 0.003(4) C55 0.024(4) 0.024(5) 0.053(6) 0.003(4) -0.005(4) 0.003(4) C56 0.013(4) 0.022(5) 0.046(5) 0.007(4) 0.001(4) -0.002(3) C57 0.026(4) 0.027(4) 0.040(5) 0.015(4) 0.005(4) -0.001(4) C58 0.027(5) 0.030(5) 0.029(4) 0.003(4) -0.003(4) 0.004(4) C59 0.020(5) 0.047(6) 0.029(5) -0.004(4) 0.001(3) 0.005(4) C60 0.020(4) 0.051(6) 0.036(5) -0.005(4) 0.002(4) -0.006(4) C61 0.035(5) 0.042(5) 0.024(4) 0.000(4) 0.009(4) -0.014(4) C62 0.029(5) 0.027(5) 0.026(4) 0.001(4) -0.002(4) 0.002(4) C63 0.030(5) 0.031(5) 0.033(5) 0.010(4) 0.007(4) -0.005(4) P1 0.0434(13) 0.0342(13) 0.0455(14) 0.0129(11) -0.0092(11) -0.0068(11) F1 0.043(3) 0.077(4) 0.092(4) 0.037(3) -0.009(3) -0.018(3) F2 0.076(4) 0.052(3) 0.090(4) -0.016(3) -0.031(3) 0.012(3) F3 0.085(4) 0.062(3) 0.052(3) 0.012(3) -0.034(3) -0.014(3) F4 0.066(3) 0.066(3) 0.064(3) 0.014(3) -0.004(3) -0.011(3) F5 0.091(4) 0.049(3) 0.062(3) 0.006(3) -0.007(3) 0.029(3) F6 0.047(3) 0.062(3) 0.038(3) 0.008(2) -0.007(2) 0.005(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N1 Zn1 N2 88.3(2) N1 Zn1 N5 94.9(2) N2 Zn1 N5 95.5(2) N3 Zn1 N1 160.0(2) N3 Zn1 N2 88.1(2) N3 Zn1 N4 88.8(2) N3 Zn1 N5 105.0(2) N4 Zn1 N1 88.2(2) N4 Zn1 N2 160.8(2) N4 Zn1 N5 103.6(2) N6 Cu1 N8 116.7(2) N7 Cu1 N6 81.3(2) N7 Cu1 N8 81.9(2) N9 Cu1 N6 120.0(2) N9 Cu1 N7 81.4(2) N9 Cu1 N8 116.9(2) C45 Cu1 N6 97.5(3) C45 Cu1 N7 178.6(3) C45 Cu1 N8 99.3(2) C45 Cu1 N9 98.8(2) C1 N1 Zn1 125.3(4) C1 N1 C4 106.8(5) C4 N1 Zn1 125.6(4) C12 N2 Zn1 126.4(4) C12 N2 C15 106.4(5) C15 N2 Zn1 127.1(4) C23 N3 Zn1 127.5(4) C26 N3 Zn1 126.0(4) C26 N3 C23 106.3(5) C34 N4 Zn1 126.1(4) C37 N4 Zn1 126.0(4) C37 N4 C34 106.6(5) C45 N5 Zn1 152.7(5) C46 N6 Cu1 128.0(5) C46 N6 C50 119.7(6) C50 N6 Cu1 112.2(5) C51 N7 Cu1 107.2(4) C51 N7 C57 111.4(5) C51 N7 C63 112.4(5) C57 N7 Cu1 107.4(4) C57 N7 C63 110.7(5) C63 N7 Cu1 107.4(4) C52 N8 Cu1 128.8(5) C52 N8 C56 119.6(6) C56 N8 Cu1 111.5(5) C58 N9 Cu1 126.6(5) C58 N9 C62 119.0(6) C62 N9 Cu1 114.4(4) N1 C1 C2 109.8(6) N1 C1 C38 125.6(6) C38 C1 C2 124.6(7) C1 C2 H2 126.9 C3 C2 C1 106.3(6) C3 C2 H2 126.9 C2 C3 H3 125.9 C2 C3 C4 108.3(6) C4 C3 H3 125.9 N1 C4 C3 108.8(6) N1 C4 C5 125.1(6) C5 C4 C3 126.1(6) C4 C5 C6 116.8(6) C4 C5 C12 126.4(6) C12 C5 C6 116.8(6) C7 C6 C5 121.8(6) C11 C6 C5 119.9(6) C11 C6 C7 118.3(6) C6 C7 H7 119.4 C8 C7 C6 121.2(6) C8 C7 H7 119.4 C7 C8 H8 120.3 C9 C8 C7 119.4(7) C9 C8 H8 120.3 C8 C9 H9 120.0 C10 C9 C8 120.1(7) C10 C9 H9 120.0 C9 C10 H10 119.9 C9 C10 C11 120.2(7) C11 C10 H10 119.9 C6 C11 H11 119.6 C10 C11 C6 120.7(6) C10 C11 H11 119.6 N2 C12 C5 125.2(6) N2 C12 C13 109.3(6) C5 C12 C13 125.4(6) C12 C13 H13 126.1 C14 C13 C12 107.8(6) C14 C13 H13 126.1 C13 C14 H14 126.4 C13 C14 C15 107.1(6) C15 C14 H14 126.4 N2 C15 C14 109.4(6) N2 C15 C16 125.5(6) C16 C15 C14 125.1(6) C15 C16 C17 121.8(9) C15 C16 C17A 116.0(6) C23 C16 C15 125.2(6) C23 C16 C17 112.9(9) C23 C16 C17A 118.7(6) C18 C17 C16 124.0(12) C18 C17 C22 120.0 C22 C17 C16 115.9(12) C17 C18 H18 120.0 C19 C18 C17 120.0 C19 C18 H18 120.0 C18 C19 H19 120.0 C18 C19 C20 120.0 C20 C19 H19 120.0 C19 C20 H20 120.0 C19 C20 C21 120.0 C21 C20 H20 120.0 C20 C21 H21 120.0 C22 C21 C20 120.0 C22 C21 H21 120.0 C17 C22 H22 120.0 C21 C22 C17 120.0 C21 C22 H22 120.0 C18A C17A C16 118.9(7) C18A C17A C22A 120.0 C22A C17A C16 121.0(7) C17A C18A H18A 120.0 C19A C18A C17A 120.0 C19A C18A H18A 120.0 C18A C19A H19A 120.0 C18A C19A C20A 120.0 C20A C19A H19A 120.0 C19A C20A H20A 120.0 C21A C20A C19A 120.0 C21A C20A H20A 120.0 C20A C21A H21A 120.0 C20A C21A C22A 120.0 C22A C21A H21A 120.0 C17A C22A H22A 120.0 C21A C22A C17A 120.0 C21A C22A H22A 120.0 N3 C23 C16 125.7(6) N3 C23 C24 109.6(6) C16 C23 C24 124.7(6) C23 C24 H24 126.4 C25 C24 C23 107.2(6) C25 C24 H24 126.4 C24 C25 H25 126.2 C24 C25 C26 107.7(6) C26 C25 H25 126.2 N3 C26 C25 109.3(6) N3 C26 C27 125.3(6) C27 C26 C25 125.3(6) C26 C27 C28 116.2(6) C34 C27 C26 126.0(6) C34 C27 C28 117.8(6) C29 C28 C27 121.5(6) C29 C28 C33 119.0(6) C33 C28 C27 119.5(6) C28 C29 H29 119.8 C28 C29 C30 120.4(7) C30 C29 H29 119.8 C29 C30 H30 119.7 C31 C30 C29 120.6(7) C31 C30 H30 119.7 C30 C31 H31 120.2 C30 C31 C32 119.6(7) C32 C31 H31 120.2 C31 C32 H32 119.7 C31 C32 C33 120.7(7) C33 C32 H32 119.7 C28 C33 C32 119.6(7) C28 C33 H33 120.2 C32 C33 H33 120.2 N4 C34 C27 125.3(6) N4 C34 C35 109.3(6) C27 C34 C35 125.4(6) C34 C35 H35 126.4 C36 C35 C34 107.3(6) C36 C35 H35 126.4 C35 C36 H36 126.4 C35 C36 C37 107.2(6) C37 C36 H36 126.4 N4 C37 C36 109.5(6) N4 C37 C38 126.0(6) C38 C37 C36 124.5(7) C1 C38 C39 114.2(9) C1 C38 C39A 119.4(6) C37 C38 C1 125.2(6) C37 C38 C39 120.4(9) C37 C38 C39A 115.4(6) C40 C39 C38 119.4(10) C40 C39 C44 120.0 C44 C39 C38 120.6(10) C39 C40 H40 120.0 C41 C40 C39 120.0 C41 C40 H40 120.0 C40 C41 H41 120.0 C40 C41 C42 120.0 C42 C41 H41 120.0 C41 C42 H42 120.0 C43 C42 C41 120.0 C43 C42 H42 120.0 C42 C43 H43 120.0 C44 C43 C42 120.0 C44 C43 H43 120.0 C39 C44 H44 120.0 C43 C44 C39 120.0 C43 C44 H44 120.0 C40A C39A C38 121.5(6) C40A C39A C44A 120.0 C44A C39A C38 118.5(6) C39A C40A H40A 120.0 C41A C40A C39A 120.0 C41A C40A H40A 120.0 C40A C41A H41A 120.0 C40A C41A C42A 120.0 C42A C41A H41A 120.0 C41A C42A H42A 120.0 C41A C42A C43A 120.0 C43A C42A H42A 120.0 C42A C43A H43A 120.0 C44A C43A C42A 120.0 C44A C43A H43A 120.0 C39A C44A H44A 120.0 C43A C44A C39A 120.0 C43A C44A H44A 120.0 N5 C45 Cu1 178.0(6) N6 C46 H46 119.0 N6 C46 C47 121.9(7) C47 C46 H46 119.0 C46 C47 H47 120.4 C48 C47 C46 119.2(8) C48 C47 H47 120.4 C47 C48 H48 120.1 C47 C48 C49 119.7(8) C49 C48 H48 120.1 C48 C49 H49 120.7 C48 C49 C50 118.5(8) C50 C49 H49 120.7 N6 C50 C49 120.8(7) N6 C50 C51 116.3(6) C49 C50 C51 122.9(7) N7 C51 C50 109.5(6) N7 C51 H51A 109.8 N7 C51 H51B 109.8 C50 C51 H51A 109.8 C50 C51 H51B 109.8 H51A C51 H51B 108.2 N8 C52 H52 118.9 N8 C52 C53 122.3(7) C53 C52 H52 118.9 C52 C53 H53 120.6 C52 C53 C54 118.9(7) C54 C53 H53 120.6 C53 C54 H54 120.3 C53 C54 C55 119.3(7) C55 C54 H54 120.3 C54 C55 H55 120.2 C56 C55 C54 119.7(7) C56 C55 H55 120.2 N8 C56 C55 120.2(7) N8 C56 C57 116.4(6) C55 C56 C57 123.3(7) N7 C57 C56 110.0(5) N7 C57 H57A 109.7 N7 C57 H57B 109.7 C56 C57 H57A 109.7 C56 C57 H57B 109.7 H57A C57 H57B 108.2 N9 C58 H58 118.9 N9 C58 C59 122.2(7) C59 C58 H58 118.9 C58 C59 H59 120.8 C60 C59 C58 118.3(7) C60 C59 H59 120.8 C59 C60 H60 119.5 C59 C60 C61 121.0(7) C61 C60 H60 119.5 C60 C61 H61 121.3 C60 C61 C62 117.3(7) C62 C61 H61 121.3 N9 C62 C61 122.2(6) N9 C62 C63 115.2(6) C61 C62 C63 122.5(7) N7 C63 C62 109.7(5) N7 C63 H63A 109.7 N7 C63 H63B 109.7 C62 C63 H63A 109.7 C62 C63 H63B 109.7 H63A C63 H63B 108.2 F1 P1 F2 92.5(3) F1 P1 F3 90.3(3) F1 P1 F4 178.7(3) F1 P1 F6 90.5(3) F2 P1 F3 90.8(3) F2 P1 F4 86.3(3) F2 P1 F6 88.9(3) F3 P1 F4 89.5(3) F3 P1 F6 179.1(3) F5 P1 F1 93.9(3) F5 P1 F2 173.6(3) F5 P1 F3 89.6(3) F5 P1 F4 87.3(3) F5 P1 F6 90.7(3) F6 P1 F4 89.6(2) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Zn1 N1 2.076(5) Zn1 N2 2.079(5) Zn1 N3 2.064(5) Zn1 N4 2.070(5) Zn1 N5 2.104(6) Cu1 N6 2.066(6) Cu1 N7 2.033(5) Cu1 N8 2.084(6) Cu1 N9 2.029(5) Cu1 C45 1.940(8) N1 C1 1.368(8) N1 C4 1.377(8) N2 C12 1.365(8) N2 C15 1.369(8) N3 C23 1.374(8) N3 C26 1.370(8) N4 C34 1.370(8) N4 C37 1.365(8) N5 C45 1.152(8) N6 C46 1.322(9) N6 C50 1.346(9) N7 C51 1.481(9) N7 C57 1.481(8) N7 C63 1.487(8) N8 C52 1.338(9) N8 C56 1.350(8) N9 C58 1.332(8) N9 C62 1.332(8) C1 C2 1.442(10) C1 C38 1.412(10) C2 H2 0.9500 C2 C3 1.351(10) C3 H3 0.9500 C3 C4 1.432(9) C4 C5 1.392(9) C5 C6 1.502(9) C5 C12 1.397(9) C6 C7 1.384(9) C6 C11 1.383(9) C7 H7 0.9500 C7 C8 1.383(9) C8 H8 0.9500 C8 C9 1.377(10) C9 H9 0.9500 C9 C10 1.371(10) C10 H10 0.9500 C10 C11 1.380(9) C11 H11 0.9500 C12 C13 1.441(9) C13 H13 0.9500 C13 C14 1.323(9) C14 H14 0.9500 C14 C15 1.446(9) C15 C16 1.412(9) C16 C17 1.511(13) C16 C17A 1.513(9) C16 C23 1.391(9) C17 C18 1.3900 C17 C22 1.3900 C18 H18 0.9500 C18 C19 1.3900 C19 H19 0.9500 C19 C20 1.3900 C20 H20 0.9500 C20 C21 1.3900 C21 H21 0.9500 C21 C22 1.3900 C22 H22 0.9500 C17A C18A 1.3900 C17A C22A 1.3900 C18A H18A 0.9500 C18A C19A 1.3900 C19A H19A 0.9500 C19A C20A 1.3900 C20A H20A 0.9500 C20A C21A 1.3900 C21A H21A 0.9500 C21A C22A 1.3900 C22A H22A 0.9500 C23 C24 1.424(9) C24 H24 0.9500 C24 C25 1.342(9) C25 H25 0.9500 C25 C26 1.427(9) C26 C27 1.413(10) C27 C28 1.498(9) C27 C34 1.391(9) C28 C29 1.376(10) C28 C33 1.387(9) C29 H29 0.9500 C29 C30 1.387(10) C30 H30 0.9500 C30 C31 1.359(10) C31 H31 0.9500 C31 C32 1.368(10) C32 H32 0.9500 C32 C33 1.394(10) C33 H33 0.9500 C34 C35 1.439(9) C35 H35 0.9500 C35 C36 1.339(10) C36 H36 0.9500 C36 C37 1.439(10) C37 C38 1.390(10) C38 C39 1.526(12) C38 C39A 1.515(9) C39 C40 1.3900 C39 C44 1.3900 C40 H40 0.9500 C40 C41 1.3900 C41 H41 0.9500 C41 C42 1.3900 C42 H42 0.9500 C42 C43 1.3900 C43 H43 0.9500 C43 C44 1.3900 C44 H44 0.9500 C39A C40A 1.3900 C39A C44A 1.3900 C40A H40A 0.9500 C40A C41A 1.3900 C41A H41A 0.9500 C41A C42A 1.3900 C42A H42A 0.9500 C42A C43A 1.3900 C43A H43A 0.9500 C43A C44A 1.3900 C44A H44A 0.9500 C46 H46 0.9500 C46 C47 1.376(10) C47 H47 0.9500 C47 C48 1.363(11) C48 H48 0.9500 C48 C49 1.374(11) C49 H49 0.9500 C49 C50 1.395(10) C50 C51 1.482(10) C51 H51A 0.9900 C51 H51B 0.9900 C52 H52 0.9500 C52 C53 1.367(10) C53 H53 0.9500 C53 C54 1.369(10) C54 H54 0.9500 C54 C55 1.380(10) C55 H55 0.9500 C55 C56 1.380(10) C56 C57 1.494(10) C57 H57A 0.9900 C57 H57B 0.9900 C58 H58 0.9500 C58 C59 1.377(9) C59 H59 0.9500 C59 C60 1.358(10) C60 H60 0.9500 C60 C61 1.374(10) C61 H61 0.9500 C61 C62 1.390(10) C62 C63 1.497(9) C63 H63A 0.9900 C63 H63B 0.9900 P1 F1 1.579(5) P1 F2 1.589(5) P1 F3 1.591(5) P1 F4 1.613(5) P1 F5 1.571(5) P1 F6 1.595(5) loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion Zn1 N1 C1 C2 -164.1(4) Zn1 N1 C1 C38 16.1(9) Zn1 N1 C4 C3 164.7(4) Zn1 N1 C4 C5 -13.7(9) Zn1 N2 C12 C5 5.6(9) Zn1 N2 C12 C13 -177.4(4) Zn1 N2 C15 C14 177.6(4) Zn1 N2 C15 C16 -5.8(9) Zn1 N3 C23 C16 6.9(9) Zn1 N3 C23 C24 -174.0(4) Zn1 N3 C26 C25 174.4(4) Zn1 N3 C26 C27 -9.7(9) Zn1 N4 C34 C27 12.4(9) Zn1 N4 C34 C35 -167.8(4) Zn1 N4 C37 C36 168.4(4) Zn1 N4 C37 C38 -11.2(10) Cu1 N6 C46 C47 176.8(5) Cu1 N6 C50 C49 -176.3(5) Cu1 N6 C50 C51 5.9(7) Cu1 N7 C51 C50 39.4(6) Cu1 N7 C57 C56 38.5(6) Cu1 N7 C63 C62 36.8(6) Cu1 N8 C52 C53 172.9(5) Cu1 N8 C56 C55 -175.1(5) Cu1 N8 C56 C57 6.9(7) Cu1 N9 C58 C59 -178.9(5) Cu1 N9 C62 C61 180.0(5) Cu1 N9 C62 C63 4.2(7) N1 C1 C2 C3 -0.3(8) N1 C1 C38 C37 -1.0(11) N1 C1 C38 C39 174.2(8) N1 C1 C38 C39A -179.0(7) N1 C4 C5 C6 178.0(6) N1 C4 C5 C12 -2.1(11) N2 C12 C13 C14 0.2(7) N2 C15 C16 C17 176.8(10) N2 C15 C16 C17A 179.8(7) N2 C15 C16 C23 -1.6(10) N3 C23 C24 C25 -0.8(7) N3 C26 C27 C28 -179.0(6) N3 C26 C27 C34 -1.4(11) N4 C34 C35 C36 -0.5(8) N4 C37 C38 C1 -1.7(11) N4 C37 C38 C39 -176.7(9) N4 C37 C38 C39A 176.3(7) N6 C46 C47 C48 -0.9(11) N6 C50 C51 N7 -30.7(8) N8 C52 C53 C54 1.8(10) N8 C56 C57 N7 -30.8(8) N9 C58 C59 C60 -1.7(10) N9 C62 C63 N7 -27.8(8) C1 N1 C4 C3 1.2(7) C1 N1 C4 C5 -177.2(6) C1 C2 C3 C4 1.1(8) C1 C38 C39 C40 73.2(13) C1 C38 C39 C44 -108.1(11) C1 C38 C39A C40A 115.8(7) C1 C38 C39A C44A -65.4(8) C2 C1 C38 C37 179.3(7) C2 C1 C38 C39 -5.5(11) C2 C1 C38 C39A 1.3(11) C2 C3 C4 N1 -1.5(8) C2 C3 C4 C5 176.9(7) C3 C4 C5 C6 -0.1(10) C3 C4 C5 C12 179.7(7) C4 N1 C1 C2 -0.6(7) C4 N1 C1 C38 179.6(6) C4 C5 C6 C7 67.5(8) C4 C5 C6 C11 -114.2(7) C4 C5 C12 N2 6.5(11) C4 C5 C12 C13 -169.9(6) C5 C6 C7 C8 178.6(6) C5 C6 C11 C10 -178.7(6) C5 C12 C13 C14 177.2(6) C6 C5 C12 N2 -173.6(6) C6 C5 C12 C13 9.9(10) C6 C7 C8 C9 -0.6(10) C7 C6 C11 C10 -0.4(10) C7 C8 C9 C10 1.0(10) C8 C9 C10 C11 -1.2(10) C9 C10 C11 C6 0.8(10) C11 C6 C7 C8 0.3(10) C12 N2 C15 C14 1.0(7) C12 N2 C15 C16 177.6(6) C12 C5 C6 C7 -112.4(7) C12 C5 C6 C11 65.9(8) C12 C13 C14 C15 0.4(7) C13 C14 C15 N2 -0.9(7) C13 C14 C15 C16 -177.5(6) C14 C15 C16 C17 -7.2(13) C14 C15 C16 C17A -4.2(10) C14 C15 C16 C23 174.4(6) C15 N2 C12 C5 -177.8(6) C15 N2 C12 C13 -0.8(7) C15 C16 C17 C18 -105.2(14) C15 C16 C17 C22 79.0(12) C15 C16 C17A C18A -77.4(8) C15 C16 C17A C22A 107.4(7) C15 C16 C23 N3 1.1(10) C15 C16 C23 C24 -177.9(6) C16 C17 C18 C19 -175.6(16) C16 C17 C22 C21 175.9(15) C16 C17A C18A C19A -175.2(8) C16 C17A C22A C21A 175.1(8) C16 C23 C24 C25 178.3(6) C17 C16 C23 N3 -177.4(9) C17 C16 C23 C24 3.6(12) C17 C18 C19 C20 0.0 C18 C17 C22 C21 0.0 C18 C19 C20 C21 0.0 C19 C20 C21 C22 0.0 C20 C21 C22 C17 0.0 C22 C17 C18 C19 0.0 C17A C16 C23 N3 179.6(7) C17A C16 C23 C24 0.7(10) C17A C18A C19A C20A 0.0 C18A C17A C22A C21A 0.0 C18A C19A C20A C21A 0.0 C19A C20A C21A C22A 0.0 C20A C21A C22A C17A 0.0 C22A C17A C18A C19A 0.0 C23 N3 C26 C25 -0.6(7) C23 N3 C26 C27 175.4(6) C23 C16 C17 C18 73.4(15) C23 C16 C17 C22 -102.4(10) C23 C16 C17A C18A 103.9(8) C23 C16 C17A C22A -71.2(8) C23 C24 C25 C26 0.4(7) C24 C25 C26 N3 0.1(7) C24 C25 C26 C27 -175.8(6) C25 C26 C27 C28 -3.7(10) C25 C26 C27 C34 174.0(6) C26 N3 C23 C16 -178.2(6) C26 N3 C23 C24 0.8(7) C26 C27 C28 C29 -65.4(9) C26 C27 C28 C33 112.8(7) C26 C27 C34 N4 -0.1(11) C26 C27 C34 C35 -179.9(6) C27 C28 C29 C30 178.5(7) C27 C28 C33 C32 -178.1(6) C27 C34 C35 C36 179.3(7) C28 C27 C34 N4 177.5(6) C28 C27 C34 C35 -2.2(10) C28 C29 C30 C31 -0.7(12) C29 C28 C33 C32 0.2(10) C29 C30 C31 C32 0.7(12) C30 C31 C32 C33 -0.3(12) C31 C32 C33 C28 -0.2(11) C33 C28 C29 C30 0.3(11) C34 N4 C37 C36 0.9(7) C34 N4 C37 C38 -178.7(7) C34 C27 C28 C29 116.8(8) C34 C27 C28 C33 -65.0(9) C34 C35 C36 C37 1.0(8) C35 C36 C37 N4 -1.2(8) C35 C36 C37 C38 178.4(7) C36 C37 C38 C1 178.7(7) C36 C37 C38 C39 3.8(12) C36 C37 C38 C39A -3.3(10) C37 N4 C34 C27 179.9(6) C37 N4 C34 C35 -0.3(7) C37 C38 C39 C40 -111.3(11) C37 C38 C39 C44 67.4(14) C37 C38 C39A C40A -62.3(8) C37 C38 C39A C44A 116.4(7) C38 C1 C2 C3 179.5(6) C38 C39 C40 C41 178.7(15) C38 C39 C44 C43 -178.7(15) C38 C39A C40A C41A 178.8(7) C38 C39A C44A C43A -178.8(7) C39 C40 C41 C42 0.0 C40 C39 C44 C43 0.0 C40 C41 C42 C43 0.0 C41 C42 C43 C44 0.0 C42 C43 C44 C39 0.0 C44 C39 C40 C41 0.0 C39A C40A C41A C42A 0.0 C40A C39A C44A C43A 0.0 C40A C41A C42A C43A 0.0 C41A C42A C43A C44A 0.0 C42A C43A C44A C39A 0.0 C44A C39A C40A C41A 0.0 C46 N6 C50 C49 0.9(9) C46 N6 C50 C51 -176.8(6) C46 C47 C48 C49 0.9(11) C47 C48 C49 C50 0.0(10) C48 C49 C50 N6 -0.9(10) C48 C49 C50 C51 176.7(6) C49 C50 C51 N7 151.6(6) C50 N6 C46 C47 0.0(10) C51 N7 C57 C56 155.7(6) C51 N7 C63 C62 -80.9(7) C52 N8 C56 C55 0.8(9) C52 N8 C56 C57 -177.3(6) C52 C53 C54 C55 -0.1(11) C53 C54 C55 C56 -1.1(11) C54 C55 C56 N8 0.8(10) C54 C55 C56 C57 178.7(6) C55 C56 C57 N7 151.2(6) C56 N8 C52 C53 -2.1(9) C57 N7 C51 C50 -77.8(7) C57 N7 C63 C62 153.8(5) C58 N9 C62 C61 -0.3(10) C58 N9 C62 C63 -176.1(6) C58 C59 C60 C61 0.8(11) C59 C60 C61 C62 0.3(10) C60 C61 C62 N9 -0.6(10) C60 C61 C62 C63 174.9(6) C61 C62 C63 N7 156.4(6) C62 N9 C58 C59 1.5(10) C63 N7 C51 C50 157.3(5) C63 N7 C57 C56 -78.5(7)