#------------------------------------------------------------------------------ #$Date: 2019-11-26 02:54:55 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242448 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/24/4132475.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132475 loop_ _publ_author_name 'Sil, Debangsu' 'Martinez, Zachary' 'Ding, Shengda' 'Bhuvanesh, Nattamai' 'Darensbourg, Donald J.' 'Hall, Michael B.' 'Darensbourg, Marcetta Y.' _publ_section_title ; Cyanide Docking and Linkage Isomerism in Models for the Artificial [FeFe]-Hydrogenase Maturation Process. ; _journal_issue 31 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 9904 _journal_page_last 9911 _journal_paper_doi 10.1021/jacs.8b04189 _journal_volume 140 _journal_year 2018 _chemical_formula_moiety 'C63 H46 Cu N9 Zn, C H2 Cl2' _chemical_formula_sum 'C64 H48 Cl2 Cu N9 Zn' _chemical_formula_weight 1142.92 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2017-10-26 _audit_creation_method ; Olex2 1.2-beta (compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5335) ; _cell_angle_alpha 90 _cell_angle_beta 90.583(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 14.1151(6) _cell_length_b 18.5419(8) _cell_length_c 19.9898(8) _cell_measurement_reflns_used 9939 _cell_measurement_temperature 110.0 _cell_measurement_theta_max 25.009 _cell_measurement_theta_min 2.421 _cell_volume 5231.5(4) _computing_cell_refinement 'SAINT V8.38A (Bruker, 2016)' _computing_data_reduction 'SAINT V8.38A (Bruker, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 110.0 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0919 _diffrn_reflns_av_unetI/netI 0.0495 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 64165 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.067 _diffrn_reflns_theta_max 25.067 _diffrn_reflns_theta_min 2.422 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.020 _exptl_absorpt_correction_T_max 0.5618 _exptl_absorpt_correction_T_min 0.4925 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0943 before and 0.0678 after correction. The Ratio of minimum to maximum transmission is 0.8766. The \l/2 correction factor is Not present.' _exptl_crystal_colour brown _exptl_crystal_colour_primary brown _exptl_crystal_density_diffrn 1.451 _exptl_crystal_description block _exptl_crystal_F_000 2352 _exptl_crystal_size_max 0.231 _exptl_crystal_size_mid 0.117 _exptl_crystal_size_min 0.063 _refine_diff_density_max 1.194 _refine_diff_density_min -0.555 _refine_diff_density_rms 0.083 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.040 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 694 _refine_ls_number_reflns 9250 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.040 _refine_ls_R_factor_all 0.0721 _refine_ls_R_factor_gt 0.0461 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0284P)^2^+12.7834P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0920 _refine_ls_wR_factor_ref 0.1050 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6882 _reflns_number_total 9250 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b04189_si_004.cif _cod_data_source_block ds _cod_database_code 4132475 _shelx_shelxl_version_number 2017/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.939 _shelx_estimated_absorpt_t_min 0.799 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2.a Secondary CH2 refined with riding coordinates: C51(H51A,H51B), C57(H57A,H57B), C58(H58A,H58B), C3S(H3SA,H3SB) 2.b Aromatic/amide H refined with riding coordinates: C2(H2), C3(H3), C7(H7), C8(H8), C9(H9), C10(H10), C11(H11), C13(H13), C14(H14), C18(H18), C19(H19), C20(H20), C21(H21), C22(H22), C24(H24), C25(H25), C29(H29), C30(H30), C31(H31), C32(H32), C33(H33), C35(H35), C36(H36), C40(H40), C41(H41), C42(H42), C43(H43), C44(H44), C46(H46), C47(H47), C48(H48), C49(H49), C52(H52), C53(H53), C54(H54), C55(H55), C61(H61), C62(H62), C63(H63), C64(H64) ; _shelx_res_file ; TITL ds_a.res in P2(1)/n ds.res created by SHELXL-2017/1 at 09:14:42 on 26-Oct-2017 REM Old TITL DS in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.173, Rweak 0.006, Alpha 0.039, Orientation as input REM Formula found by SHELXT: C65 N10 Cu2 CELL 0.71073 14.1151 18.5419 19.9898 90 90.583 90 ZERR 4 0.0006 0.0008 0.0008 0 0.002 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl Cu N Zn UNIT 256 192 8 4 36 4 L.S. 10 0 0 PLAN 20 SIZE 0.063 0.117 0.231 TEMP -163.15 BOND $H more -1 wpdb -1 htab conf fmap 2 53 acta OMIT -1 1 1 OMIT 1 1 1 OMIT 0 1 2 OMIT 0 0 2 OMIT 0 4 0 REM REM REM WGHT 0.028400 12.783400 FVAR 0.27873 ZN1 6 0.441160 0.253818 0.312620 11.00000 0.01757 0.01495 = 0.01393 -0.00102 -0.00410 0.00032 CU1 4 0.285157 0.486956 0.385478 11.00000 0.01779 0.02164 = 0.02602 -0.00773 0.00152 0.00220 N1 5 0.539224 0.294259 0.244478 11.00000 0.01827 0.01459 = 0.01639 -0.00230 -0.00492 0.00217 N2 5 0.556046 0.236343 0.377060 11.00000 0.01922 0.01561 = 0.01665 -0.00035 -0.00330 -0.00031 N3 5 0.368958 0.173239 0.364751 11.00000 0.01980 0.01742 = 0.01785 0.00116 -0.00709 -0.00205 N4 5 0.347554 0.236924 0.233983 11.00000 0.01984 0.01324 = 0.01451 -0.00185 -0.00466 0.00192 N5 5 0.379958 0.347496 0.345297 11.00000 0.01968 0.02059 = 0.01870 -0.00146 -0.00202 0.00092 N6 5 0.386599 0.554627 0.428510 11.00000 0.01723 0.01744 = 0.01789 -0.00170 -0.00003 0.00399 N7 5 0.220583 0.519488 0.485620 11.00000 0.01757 0.02450 = 0.02406 -0.00434 0.00607 0.00060 N8 5 0.168390 0.542072 0.354118 11.00000 0.01683 0.02010 = 0.03101 -0.00758 0.00140 -0.00056 C1 1 0.517289 0.317876 0.181478 11.00000 0.02111 0.01808 = 0.01650 -0.00365 0.00070 0.00440 C2 1 0.597245 0.355322 0.154056 11.00000 0.02121 0.02731 = 0.01771 -0.00112 0.00115 -0.00055 AFIX 43 H2 2 0.599982 0.377948 0.111480 11.00000 -1.20000 AFIX 0 C3 1 0.667558 0.352287 0.200095 11.00000 0.01871 0.02691 = 0.02158 -0.00043 0.00269 -0.00027 AFIX 43 H3 2 0.729774 0.371103 0.195629 11.00000 -1.20000 AFIX 0 C4 1 0.630288 0.315002 0.257464 11.00000 0.01638 0.01824 = 0.01789 -0.00279 -0.00187 0.00317 C5 1 0.679860 0.304265 0.318027 11.00000 0.01874 0.01448 = 0.01992 -0.00582 -0.00414 0.00159 C6 1 0.777618 0.334726 0.324242 11.00000 0.01835 0.02303 = 0.01608 -0.00526 -0.00235 0.00158 C7 1 0.793904 0.408041 0.313377 11.00000 0.01818 0.02678 = 0.01761 -0.00163 0.00043 -0.00090 AFIX 43 H7 2 0.742775 0.438382 0.300235 11.00000 -1.20000 AFIX 0 C8 1 0.883914 0.437160 0.321542 11.00000 0.03055 0.02851 = 0.02040 -0.00052 0.00327 -0.01063 AFIX 43 H8 2 0.894015 0.487056 0.313510 11.00000 -1.20000 AFIX 0 C9 1 0.958909 0.393900 0.341304 11.00000 0.01982 0.04559 = 0.02347 -0.00592 -0.00342 -0.00697 AFIX 43 H9 2 1.020264 0.414035 0.347486 11.00000 -1.20000 AFIX 0 C10 1 0.944113 0.321743 0.351917 11.00000 0.02105 0.03948 = 0.02876 -0.00968 -0.00386 0.00818 AFIX 43 H10 2 0.995530 0.291967 0.365616 11.00000 -1.20000 AFIX 0 C11 1 0.854518 0.291629 0.342829 11.00000 0.02438 0.02553 = 0.02909 -0.00672 -0.00201 0.00438 AFIX 43 H11 2 0.845689 0.241333 0.349339 11.00000 -1.20000 AFIX 0 C12 1 0.643886 0.267970 0.373827 11.00000 0.01869 0.01768 = 0.01738 -0.00138 -0.00471 -0.00051 C13 1 0.692455 0.258537 0.437231 11.00000 0.02192 0.02149 = 0.02555 -0.00315 -0.00860 -0.00429 AFIX 43 H13 2 0.753880 0.275806 0.448669 11.00000 -1.20000 AFIX 0 C14 1 0.634418 0.220755 0.476962 11.00000 0.02878 0.01986 = 0.02485 0.00399 -0.01228 -0.00520 AFIX 43 H14 2 0.647515 0.206090 0.521644 11.00000 -1.20000 AFIX 0 C15 1 0.549306 0.206629 0.439734 11.00000 0.01934 0.01987 = 0.01854 0.00091 -0.00770 -0.00022 C16 1 0.473947 0.165729 0.464015 11.00000 0.02739 0.01565 = 0.01704 0.00067 -0.00724 -0.00048 C17 1 0.485438 0.137663 0.533966 11.00000 0.02353 0.02099 = 0.02013 0.00208 -0.00854 -0.00407 C18 1 0.541016 0.077290 0.547127 11.00000 0.04168 0.03283 = 0.02287 0.00127 -0.00064 0.00840 AFIX 43 H18 2 0.567659 0.051159 0.511026 11.00000 -1.20000 AFIX 0 C19 1 0.558000 0.054796 0.612169 11.00000 0.05514 0.03818 = 0.02340 0.00824 -0.00338 0.02105 AFIX 43 H19 2 0.595685 0.013205 0.620329 11.00000 -1.20000 AFIX 0 C20 1 0.520523 0.092423 0.665190 11.00000 0.03770 0.04298 = 0.02077 0.00679 -0.00517 0.00549 AFIX 43 H20 2 0.532636 0.077111 0.709816 11.00000 -1.20000 AFIX 0 C21 1 0.465317 0.152460 0.652947 11.00000 0.03286 0.03283 = 0.01980 -0.00273 -0.00709 0.00033 AFIX 43 H21 2 0.439059 0.178416 0.689298 11.00000 -1.20000 AFIX 0 C22 1 0.447885 0.175203 0.587684 11.00000 0.02610 0.02202 = 0.02469 0.00163 -0.00364 0.00076 AFIX 43 H22 2 0.409996 0.216740 0.579769 11.00000 -1.20000 AFIX 0 C23 1 0.390810 0.149421 0.428274 11.00000 0.02435 0.01537 = 0.01357 -0.00005 -0.00506 0.00047 C24 1 0.314663 0.104987 0.452724 11.00000 0.02803 0.01945 = 0.01496 0.00506 -0.00474 -0.00040 AFIX 43 H24 2 0.312165 0.081986 0.495136 11.00000 -1.20000 AFIX 0 C25 1 0.247806 0.102196 0.404230 11.00000 0.02096 0.02008 = 0.02436 0.00091 -0.00139 -0.00453 AFIX 43 H25 2 0.189282 0.077003 0.406022 11.00000 -1.20000 AFIX 0 C26 1 0.282021 0.144830 0.348915 11.00000 0.02153 0.01692 = 0.02010 -0.00310 -0.00199 -0.00077 C27 1 0.231421 0.157085 0.288760 11.00000 0.01965 0.01487 = 0.01863 -0.00210 0.00076 0.00221 C28 1 0.137795 0.120389 0.281335 11.00000 0.01909 0.02615 = 0.01285 -0.00234 -0.00303 -0.00238 C29 1 0.130213 0.045429 0.281846 11.00000 0.02013 0.01859 = 0.02441 0.00051 -0.00460 -0.00029 AFIX 43 H29 2 0.186032 0.016952 0.284986 11.00000 -1.20000 AFIX 0 C30 1 0.042717 0.011700 0.277858 11.00000 0.02610 0.02245 = 0.01919 -0.00061 -0.00201 -0.00469 AFIX 43 H30 2 0.038878 -0.039446 0.278560 11.00000 -1.20000 AFIX 0 C31 1 -0.038808 0.052484 0.272867 11.00000 0.02073 0.03564 = 0.02022 -0.00265 0.00217 -0.00578 AFIX 43 H31 2 -0.098870 0.029443 0.270628 11.00000 -1.20000 AFIX 0 C32 1 -0.033047 0.127108 0.271121 11.00000 0.01863 0.04003 = 0.02209 -0.00557 0.00029 0.00217 AFIX 43 H32 2 -0.089127 0.155217 0.267429 11.00000 -1.20000 AFIX 0 C33 1 0.054778 0.160730 0.274773 11.00000 0.02652 0.02612 = 0.01704 -0.00552 -0.00209 0.00177 AFIX 43 H33 2 0.058373 0.211846 0.272778 11.00000 -1.20000 AFIX 0 C34 1 0.263305 0.200180 0.235747 11.00000 0.01740 0.01485 = 0.01970 -0.00383 -0.00705 0.00067 C35 1 0.213615 0.210393 0.172779 11.00000 0.01888 0.02246 = 0.02186 0.00041 -0.00370 0.00003 AFIX 43 H35 2 0.153742 0.190703 0.160608 11.00000 -1.20000 AFIX 0 C36 1 0.268192 0.253011 0.134760 11.00000 0.02440 0.02229 = 0.01525 -0.00209 -0.00805 0.00159 AFIX 43 H36 2 0.253762 0.269270 0.090756 11.00000 -1.20000 AFIX 0 C37 1 0.352573 0.269525 0.172942 11.00000 0.01924 0.01671 = 0.01740 -0.00363 -0.00313 0.00434 C38 1 0.430047 0.308559 0.148412 11.00000 0.02076 0.01620 = 0.01656 -0.00541 -0.00244 0.00393 C39 1 0.419236 0.342591 0.080862 11.00000 0.01971 0.02280 = 0.01656 -0.00287 -0.00356 -0.00114 C40 1 0.473430 0.320437 0.026720 11.00000 0.02500 0.03051 = 0.02033 -0.00459 -0.00176 0.00493 AFIX 43 H40 2 0.515951 0.281071 0.031913 11.00000 -1.20000 AFIX 0 C41 1 0.466206 0.354923 -0.034447 11.00000 0.03194 0.04995 = 0.01841 -0.00569 0.00197 -0.00187 AFIX 43 H41 2 0.504001 0.339312 -0.070736 11.00000 -1.20000 AFIX 0 C42 1 0.404349 0.411928 -0.043056 11.00000 0.05150 0.04259 = 0.01529 0.00575 -0.00280 0.00493 AFIX 43 H42 2 0.400384 0.436149 -0.084869 11.00000 -1.20000 AFIX 0 C43 1 0.348359 0.433489 0.009419 11.00000 0.05111 0.03598 = 0.02378 0.00579 -0.00831 0.01427 AFIX 43 H43 2 0.304714 0.472017 0.003471 11.00000 -1.20000 AFIX 0 C44 1 0.355593 0.399122 0.070760 11.00000 0.03342 0.02711 = 0.02024 -0.00296 -0.00178 0.01081 AFIX 43 H44 2 0.316550 0.414318 0.106534 11.00000 -1.20000 AFIX 0 C45 1 0.339888 0.399861 0.357549 11.00000 0.01717 0.02400 = 0.01911 -0.00135 0.00015 -0.00437 C46 1 0.460896 0.581842 0.395157 11.00000 0.02093 0.02083 = 0.01827 0.00121 0.00097 0.00421 AFIX 43 H46 2 0.462651 0.575964 0.347976 11.00000 -1.20000 AFIX 0 C47 1 0.534299 0.617727 0.426214 11.00000 0.01778 0.02386 = 0.03008 0.00354 -0.00029 -0.00191 AFIX 43 H47 2 0.585023 0.636939 0.400922 11.00000 -1.20000 AFIX 0 C48 1 0.532854 0.625301 0.494928 11.00000 0.02313 0.02706 = 0.03399 -0.00472 -0.00759 -0.00339 AFIX 43 H48 2 0.582726 0.649656 0.517830 11.00000 -1.20000 AFIX 0 C49 1 0.457871 0.596931 0.529590 11.00000 0.02476 0.02599 = 0.02231 -0.00477 -0.00399 0.00103 AFIX 43 H49 2 0.455704 0.601084 0.576917 11.00000 -1.20000 AFIX 0 C50 1 0.385500 0.562242 0.495000 11.00000 0.02182 0.01823 = 0.01817 -0.00221 -0.00036 0.00487 C51 1 0.301986 0.530204 0.530566 11.00000 0.02323 0.02577 = 0.02238 -0.00524 0.00478 0.00049 AFIX 23 H51A 2 0.320643 0.483254 0.550263 11.00000 -1.20000 H51B 2 0.283408 0.562564 0.567578 11.00000 -1.20000 AFIX 0 C52 1 0.127300 0.538502 0.293674 11.00000 0.01795 0.02389 = 0.03045 -0.00538 -0.00055 -0.00888 AFIX 43 H52 2 0.155223 0.508309 0.260928 11.00000 -1.20000 AFIX 0 C53 1 0.046835 0.576142 0.276319 11.00000 0.01692 0.02442 = 0.03785 0.00083 -0.00505 -0.00809 AFIX 43 H53 2 0.020998 0.573045 0.232345 11.00000 -1.20000 AFIX 0 C54 1 0.004198 0.618766 0.324482 11.00000 0.01814 0.02014 = 0.04864 0.00618 -0.00244 -0.00235 AFIX 43 H54 2 -0.051512 0.645463 0.314179 11.00000 -1.20000 AFIX 0 C55 1 0.044234 0.621570 0.387426 11.00000 0.01401 0.01813 = 0.04165 -0.00286 0.00516 -0.00214 AFIX 43 H55 2 0.015309 0.649250 0.421601 11.00000 -1.20000 AFIX 0 C56 1 0.126648 0.583956 0.400670 11.00000 0.01756 0.01741 = 0.03054 -0.00482 0.00168 -0.00424 C57 1 0.178305 0.589128 0.466263 11.00000 0.01945 0.02286 = 0.03421 -0.00936 0.00233 0.00246 AFIX 23 H57A 2 0.228887 0.625907 0.462961 11.00000 -1.20000 H57B 2 0.133723 0.604837 0.501291 11.00000 -1.20000 AFIX 0 C58 1 0.145647 0.473904 0.514974 11.00000 0.02218 0.03213 = 0.03034 -0.00766 0.00923 -0.00250 AFIX 23 H58A 2 0.088369 0.476323 0.486065 11.00000 -1.20000 H58B 2 0.128849 0.493432 0.559395 11.00000 -1.20000 AFIX 0 C59 1 0.174924 0.396346 0.522725 11.00000 0.01611 0.03199 = 0.03125 -0.00161 0.00636 -0.00342 N60 5 0.196475 0.373880 0.585475 11.00000 0.02714 0.04043 = 0.02813 -0.00270 0.00593 -0.00848 C61 1 0.218420 0.305606 0.592454 11.00000 0.02263 0.03925 = 0.03085 -0.00154 -0.00225 0.00158 AFIX 43 H61 2 0.232722 0.289109 0.636403 11.00000 -1.20000 AFIX 0 C62 1 0.222522 0.255719 0.541519 11.00000 0.02321 0.03127 = 0.04622 0.00448 0.00612 0.00068 AFIX 43 H62 2 0.238204 0.206752 0.550176 11.00000 -1.20000 AFIX 0 C63 1 0.203155 0.279333 0.477940 11.00000 0.02701 0.03017 = 0.03807 -0.00604 0.00727 -0.00639 AFIX 43 H63 2 0.207291 0.247155 0.441102 11.00000 -1.20000 AFIX 0 C64 1 0.177626 0.350201 0.467975 11.00000 0.03121 0.03255 = 0.02537 0.00080 0.00830 0.00003 AFIX 43 H64 2 0.162117 0.367285 0.424418 11.00000 -1.20000 AFIX 0 CL1S 3 0.697887 -0.001789 0.372196 11.00000 0.09747 0.03589 = 0.03958 -0.00633 -0.00592 -0.01642 CL2S 3 0.710369 0.105358 0.267114 11.00000 0.03336 0.04106 = 0.06454 0.01155 -0.00803 -0.00197 C3S 1 0.685457 0.088748 0.351567 11.00000 0.06613 0.03979 = 0.04835 -0.01655 -0.01838 0.02040 AFIX 23 H3SA 2 0.728804 0.117762 0.380016 11.00000 -1.20000 H3SB 2 0.619818 0.104275 0.360962 11.00000 -1.20000 AFIX 0 HKLF 4 REM ds_a.res in P2(1)/n REM R1 = 0.0461 for 6882 Fo > 4sig(Fo) and 0.0721 for all 9250 data REM 694 parameters refined using 0 restraints END WGHT 0.0284 12.7837 REM Instructions for potential hydrogen bonds EQIV $1 -x+3/2, y+1/2, -z+1/2 HTAB C3 Cl1S_$1 HTAB C3S N2 REM Highest difference peak 1.194, deepest hole -0.555, 1-sigma level 0.083 Q1 1 0.2061 0.3807 0.2395 11.00000 0.05 1.19 Q2 1 0.6790 0.1352 0.7631 11.00000 0.05 1.17 Q3 1 0.1091 0.3411 0.4597 11.00000 0.05 0.65 Q4 1 0.2836 0.0154 0.3820 11.00000 0.05 0.47 Q5 1 -0.0993 -0.0171 0.2609 11.00000 0.05 0.43 Q6 1 0.6553 0.0183 0.3435 11.00000 0.05 0.41 Q7 1 0.2396 0.3373 0.5645 11.00000 0.05 0.38 Q8 1 0.3563 0.4474 0.3823 11.00000 0.05 0.30 Q9 1 0.0382 0.6996 0.3987 11.00000 0.05 0.29 Q10 1 0.5560 0.1989 0.3555 11.00000 0.05 0.29 Q11 1 0.9030 0.5174 0.2639 11.00000 0.05 0.28 Q12 1 0.7221 0.3201 0.3156 11.00000 0.05 0.28 Q13 1 0.5352 0.4406 -0.0095 11.00000 0.05 0.28 Q14 1 0.5402 0.2378 0.0997 11.00000 0.05 0.28 Q15 1 0.4200 0.0413 0.5423 11.00000 0.05 0.27 Q16 1 0.4833 0.3055 0.1605 11.00000 0.05 0.27 Q17 1 0.3725 0.1783 0.4028 11.00000 0.05 0.27 Q18 1 0.6571 0.3156 0.2974 11.00000 0.05 0.26 Q19 1 0.7797 0.5201 0.3426 11.00000 0.05 0.26 Q20 1 0.4774 0.4003 -0.0416 11.00000 0.05 0.26 ; _shelx_res_checksum 85978 _shelx_hkl_file ; -2 0 0 130.79 8.80 -2 0 0 125.29 7.40 -2 0 0 118.79 4.80 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36.60 9.90 -5 -9 0 4.30 9.00 -5 -9 0 13.40 9.60 -5 -9 0 24.10 8.20 5 9 0 14.00 4.70 -6 -9 0 2036.60 54.49 -6 -9 0 1990.60 72.19 -6 -9 0 2042.80 68.39 -6 -9 0 2004.50 59.09 6 9 0 1949.90 60.19 -7 -9 0 7.90 6.80 -7 -9 0 2.10 5.40 -7 -9 0 17.30 11.70 -7 -9 0 8.00 9.80 7 9 0 14.50 6.60 -8 -9 0 18.30 15.40 -8 -9 0 4.40 10.00 -8 -9 0 5.30 6.30 -8 -9 0 1.70 6.80 8 9 0 17.10 7.00 -9 -9 0 29.70 8.20 -9 -9 0 29.50 11.70 -9 -9 0 39.40 15.20 9 9 0 40.50 14.90 -10 -9 0 307.37 24.60 -10 -9 0 309.97 28.90 -10 -9 0 273.47 32.60 10 9 0 290.37 25.30 -11 -9 0 217.38 32.90 -11 -9 0 249.78 29.60 -11 -9 0 170.28 23.70 11 9 0 167.88 24.60 -12 -9 0 105.89 25.90 -12 -9 0 122.09 26.10 -12 -9 0 104.89 30.20 12 9 0 118.09 23.20 -13 -9 0 2.60 15.20 -13 -9 0 22.40 18.20 -13 -9 0 16.30 13.40 13 9 0 7.10 10.80 -14 -9 0 12.30 16.50 -14 -9 0 -11.60 20.00 14 9 0 -7.80 12.30 -15 -9 0 7.90 18.70 -15 -9 0 9.30 19.10 15 9 0 6.90 15.60 15 -10 0 -2.10 23.40 -14 10 0 54.09 23.10 13 -10 0 280.37 42.00 13 -10 0 202.58 31.10 -13 10 0 248.68 34.50 -13 10 0 193.48 28.80 12 -10 0 38.30 15.90 12 -10 0 58.79 18.60 -12 10 0 55.09 18.20 11 -10 0 117.29 31.30 11 -10 0 87.39 24.70 -11 10 0 108.19 27.60 10 -10 0 322.47 30.70 10 -10 0 265.27 36.70 -10 10 0 368.06 49.10 -10 10 0 354.76 31.70 9 -10 0 -12.80 11.90 9 -10 0 -18.50 9.40 -9 10 0 -16.10 11.00 -9 10 0 25.50 18.00 8 -10 0 -4.10 12.10 8 -10 0 0.30 9.30 -8 10 0 11.70 13.60 -8 10 0 13.70 15.90 7 -10 0 44.50 14.60 7 -10 0 30.70 11.40 -7 10 0 16.20 11.70 -7 10 0 29.70 12.90 6 -10 0 342.67 24.30 6 -10 0 337.27 26.30 -6 10 0 315.37 26.70 5 -10 0 297.97 22.80 5 -10 0 221.58 25.50 5 -10 0 301.17 24.50 -5 10 0 296.77 25.70 4 -10 0 756.92 36.80 4 -10 0 743.73 35.60 -4 10 0 791.52 36.80 3 -10 0 -6.80 6.00 3 -10 0 7.10 9.60 3 -10 0 18.40 8.00 -3 10 0 -1.40 7.90 2 -10 0 2011.20 64.49 2 -10 0 1927.91 63.69 2 -10 0 1904.91 63.49 2 -10 0 1954.00 63.79 -2 10 0 2053.09 64.99 1 -10 0 658.43 32.70 1 -10 0 664.53 31.00 1 -10 0 620.94 30.00 1 -10 0 637.54 32.50 0 -10 0 14.30 8.90 0 -10 0 14.80 5.50 0 -10 0 16.30 8.40 0 -10 0 7.80 5.50 -1 -10 0 646.04 30.60 -1 -10 0 640.14 26.90 -1 -10 0 649.34 34.30 -1 -10 0 642.44 24.80 -2 -10 0 2022.30 52.59 -2 -10 0 2010.60 55.29 -2 -10 0 2040.30 62.19 -2 -10 0 2037.70 66.89 2 10 0 2099.19 62.29 -3 -10 0 6.80 3.50 -3 -10 0 15.30 7.20 -3 -10 0 8.00 8.90 3 10 0 6.80 4.30 -4 -10 0 793.42 25.10 -4 -10 0 770.12 39.50 -4 -10 0 799.52 32.30 -4 -10 0 778.52 39.20 4 10 0 756.42 31.50 -5 -10 0 290.07 27.20 -5 -10 0 316.17 15.00 -5 -10 0 302.07 25.60 -5 -10 0 324.07 20.10 5 10 0 301.37 19.10 -6 -10 0 345.67 27.70 -6 -10 0 332.57 16.30 -6 -10 0 263.07 27.40 -6 -10 0 335.07 20.10 6 10 0 328.07 20.80 -7 -10 0 26.70 9.90 -7 -10 0 61.19 20.00 -7 -10 0 25.50 13.20 7 10 0 59.09 12.50 -8 -10 0 14.40 14.60 -8 -10 0 20.90 6.30 -8 -10 0 37.40 12.20 -8 -10 0 11.00 12.00 8 10 0 6.70 6.40 -9 -10 0 -1.00 7.70 -9 -10 0 -2.60 5.80 -9 -10 0 2.10 12.00 -9 -10 0 -4.10 14.30 9 10 0 5.90 6.50 -10 -10 0 289.07 22.90 -10 -10 0 249.78 27.60 -10 -10 0 369.36 38.40 10 10 0 308.87 26.50 -11 -10 0 97.59 19.80 -11 -10 0 60.29 18.30 -11 -10 0 126.39 29.90 11 10 0 85.99 22.00 -12 -10 0 47.60 16.60 -12 -10 0 47.40 21.70 -13 -10 0 248.08 38.70 -13 -10 0 203.88 28.20 13 10 0 246.48 31.00 -14 -10 0 25.80 16.30 -14 -10 0 15.70 20.00 14 10 0 10.40 13.30 14 -11 0 119.49 31.30 -14 11 0 213.78 39.60 -14 11 0 143.09 29.60 13 -11 0 47.50 19.30 13 -11 0 105.39 38.90 -13 11 0 65.89 20.90 -13 11 0 35.40 15.30 12 -11 0 43.90 17.60 12 -11 0 132.29 36.60 -12 11 0 31.20 20.20 11 -11 0 -7.80 14.90 11 -11 0 5.60 15.00 -11 11 0 -8.50 15.50 10 -11 0 84.09 21.40 10 -11 0 50.09 14.50 -10 11 0 37.60 16.90 9 -11 0 -11.80 11.10 9 -11 0 36.90 13.80 -9 11 0 2.00 12.50 8 -11 0 164.58 23.80 8 -11 0 110.59 24.90 -8 11 0 110.49 22.80 7 -11 0 19.80 11.70 7 -11 0 14.00 12.30 -7 11 0 1.90 11.70 6 -11 0 3.80 8.80 6 -11 0 1.70 9.00 6 -11 0 4.80 11.10 -6 11 0 24.20 11.40 5 -11 0 -8.20 9.70 5 -11 0 -1.30 9.90 5 -11 0 -5.20 7.50 -5 11 0 7.90 10.10 4 -11 0 465.35 30.10 4 -11 0 486.85 30.40 -4 11 0 495.05 31.30 3 -11 0 49.80 14.90 3 -11 0 47.90 15.80 -3 11 0 63.29 16.20 2 -11 0 400.96 27.00 2 -11 0 375.36 26.20 2 -11 0 364.66 26.40 2 -11 0 423.06 27.90 -2 11 0 380.06 28.10 1 -11 0 55.89 14.90 1 -11 0 54.39 16.70 1 -11 0 51.09 14.40 1 -11 0 61.99 14.20 0 -11 0 -0.30 5.30 0 -11 0 -17.20 7.90 0 -11 0 0.40 4.50 0 -11 0 1.50 9.20 -1 -11 0 68.99 12.10 -1 -11 0 67.99 10.30 -1 -11 0 72.99 13.90 -1 -11 0 72.59 16.70 -2 -11 0 406.66 25.80 -2 -11 0 410.26 18.20 -2 -11 0 427.46 20.50 -2 -11 0 428.96 28.70 2 11 0 428.76 25.20 -3 -11 0 53.49 16.60 -3 -11 0 32.30 9.00 -3 -11 0 34.20 9.80 -3 -11 0 52.89 8.20 3 11 0 37.60 10.80 -4 -11 0 528.05 32.30 -4 -11 0 529.25 18.90 -4 -11 0 510.15 26.90 4 11 0 521.75 26.20 -5 -11 0 5.80 7.60 -5 -11 0 0.30 3.40 -5 -11 0 3.80 10.60 -5 -11 0 -1.10 10.30 5 11 0 6.90 4.50 -6 -11 0 -0.70 12.10 -6 -11 0 14.00 8.80 -6 -11 0 -4.40 10.30 6 11 0 14.50 5.50 -7 -11 0 -12.60 7.90 -7 -11 0 -3.90 11.50 -7 -11 0 12.80 4.90 -7 -11 0 2.80 11.30 7 11 0 8.30 5.70 -8 -11 0 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3 36.60 17.90 -4 17 -3 10.40 15.00 4 -17 3 -2.70 14.70 4 -17 3 -4.80 14.90 4 -17 3 15.60 14.10 4 -17 3 3.50 12.80 -5 17 -3 -11.20 18.10 5 -17 3 -5.30 15.70 5 -17 3 -5.50 14.40 5 -17 3 -17.80 14.30 -6 17 -3 -28.30 15.90 6 -17 3 4.60 13.50 6 -17 3 5.60 14.40 6 -17 3 -9.70 18.80 -7 17 -3 411.46 45.40 7 -17 3 407.76 40.00 7 -17 3 369.86 54.29 7 -17 3 428.96 39.10 7 -17 3 420.96 45.90 -8 17 -3 171.68 36.20 8 -17 3 123.39 31.30 8 -17 3 208.28 31.60 -9 17 -3 563.74 48.30 9 -17 3 414.76 51.69 9 -17 3 579.24 46.80 -10 17 -3 40.10 22.20 10 -17 3 9.60 20.30 10 -17 3 69.19 22.70 11 16 -3 50.29 16.20 -11 -16 3 90.99 23.40 -11 -16 3 75.49 20.00 -11 -16 3 10.20 21.00 10 16 -3 17.80 13.10 -10 -16 3 89.39 24.00 -10 -16 3 16.60 16.60 -10 -16 3 36.20 9.80 9 16 -3 283.77 33.30 -9 -16 3 245.98 38.50 -9 -16 3 264.97 28.20 -9 -16 3 291.27 24.10 8 16 -3 13.80 10.20 -8 -16 3 12.60 18.60 -8 -16 3 5.80 8.70 -8 -16 3 -5.00 13.70 -7 -16 3 38.10 21.60 -7 -16 3 121.19 21.80 -7 -16 3 87.29 18.20 6 16 -3 353.46 33.50 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262.07 37.80 4 -16 3 280.87 31.80 -5 16 -3 6.20 15.50 5 -16 3 -1.90 11.70 5 -16 3 2.40 16.10 5 -16 3 0.70 15.00 -6 16 -3 60.19 19.70 6 -16 3 82.89 24.50 6 -16 3 98.29 34.00 6 -16 3 112.29 33.30 6 -16 3 37.60 18.20 -7 16 -3 369.66 38.10 7 -16 3 322.77 35.70 7 -16 3 253.97 45.50 7 -16 3 323.17 35.20 -8 16 -3 18.20 20.80 8 -16 3 20.30 17.00 8 -16 3 113.29 34.60 8 -16 3 25.50 15.10 -9 16 -3 2.70 19.30 9 -16 3 49.00 19.30 9 -16 3 26.30 17.50 -10 16 -3 16.60 20.80 10 -16 3 -29.70 20.50 10 -16 3 -22.60 16.30 -11 16 -3 11.30 21.10 11 -16 3 34.90 22.30 11 -16 3 27.00 23.30 12 15 -3 22.90 14.50 -12 -15 3 -0.50 12.40 -12 -15 3 -0.30 17.10 11 15 -3 -4.70 12.10 -11 -15 3 2.80 18.60 -11 -15 3 -13.60 11.20 10 15 -3 4.90 11.30 -10 -15 3 -9.60 17.10 -10 -15 3 16.70 10.90 -10 -15 3 15.30 12.80 9 15 -3 47.90 13.70 -9 -15 3 76.39 21.30 -9 -15 3 54.69 15.20 -9 -15 3 48.90 20.40 -8 -15 3 146.89 20.90 -8 -15 3 117.39 29.80 -8 -15 3 103.99 22.10 7 15 -3 254.97 27.90 -7 -15 3 261.27 22.40 -7 -15 3 195.08 33.40 -7 -15 3 297.67 24.80 6 15 -3 245.38 26.80 -6 -15 3 206.68 24.00 -6 -15 3 210.38 20.70 -6 -15 3 198.48 30.70 5 15 -3 2.90 7.70 -5 -15 3 -5.40 12.40 -5 -15 3 -2.60 7.20 -5 -15 3 11.70 11.50 4 15 -3 161.78 26.20 -4 -15 3 176.08 25.60 -4 -15 3 202.48 28.60 -4 -15 3 188.18 19.40 3 15 -3 487.45 36.20 -3 -15 3 544.95 29.40 -3 -15 3 527.05 40.60 -3 -15 3 538.65 35.60 -2 -15 3 321.47 25.00 -2 -15 3 300.97 31.80 -2 -15 3 371.66 29.60 -2 -15 3 332.47 27.70 -1 -15 3 370.96 31.70 -1 -15 3 436.56 31.30 -1 -15 3 391.76 35.20 -1 -15 3 417.16 27.80 0 15 -3 21.50 14.10 0 -15 3 -4.70 8.10 0 -15 3 3.90 12.80 0 -15 3 -6.90 9.10 0 -15 3 -6.60 10.90 -1 15 -3 3.70 12.70 1 -15 3 -5.50 9.80 1 -15 3 -5.40 9.20 1 -15 3 15.00 12.60 1 -15 3 -0.50 10.20 -2 15 -3 15.20 13.50 2 -15 3 -9.10 11.50 2 -15 3 20.80 13.70 2 -15 3 3.30 10.20 2 -15 3 -15.60 9.20 -3 15 -3 83.09 24.90 3 -15 3 34.60 15.80 3 -15 3 75.59 26.80 3 -15 3 43.10 13.60 3 -15 3 58.19 17.30 -4 15 -3 80.59 25.70 4 -15 3 46.90 16.60 4 -15 3 39.00 13.40 4 -15 3 46.80 15.00 -5 15 -3 -14.40 13.30 5 -15 3 7.70 13.50 5 -15 3 16.60 13.90 5 -15 3 16.00 12.20 5 -15 3 12.90 14.70 -6 15 -3 485.05 41.30 6 -15 3 553.64 40.70 6 -15 3 534.65 45.50 6 -15 3 524.55 37.20 -7 15 -3 111.99 29.80 7 -15 3 48.60 17.10 7 -15 3 182.18 31.70 7 -15 3 92.69 26.80 -8 15 -3 12.40 17.00 8 -15 3 -3.40 14.70 8 -15 3 4.50 17.10 8 -15 3 28.60 14.40 -9 15 -3 139.29 35.00 9 -15 3 100.09 27.20 9 -15 3 119.79 36.70 -10 15 -3 46.70 22.40 10 -15 3 55.69 20.70 10 -15 3 47.90 19.50 -11 15 -3 261.07 37.70 11 -15 3 174.18 45.90 11 -15 3 222.18 38.00 -12 15 -3 11.30 20.70 12 -15 3 -27.60 25.30 12 -15 3 18.60 18.80 12 14 -3 160.28 31.20 -12 -14 3 120.89 28.10 -12 -14 3 129.29 35.70 -12 -14 3 63.49 22.20 11 14 -3 78.69 26.40 -11 -14 3 33.50 21.60 -11 -14 3 8.70 19.40 -11 -14 3 36.50 10.20 10 14 -3 21.50 10.10 -10 -14 3 9.70 10.80 -10 -14 3 29.20 11.60 -10 -14 3 6.20 20.80 -9 -14 3 186.18 34.60 -9 -14 3 216.28 24.80 -9 -14 3 206.98 22.30 8 14 -3 142.89 24.00 -8 -14 3 128.79 31.40 -8 -14 3 115.59 19.90 7 14 -3 11.90 9.80 -7 -14 3 -15.60 13.20 -7 -14 3 10.50 11.30 -7 -14 3 7.90 8.30 6 14 -3 487.15 34.80 -6 -14 3 493.35 39.50 -6 -14 3 505.35 28.10 -6 -14 3 443.76 29.70 5 14 -3 232.48 25.40 -5 -14 3 228.98 21.30 -5 -14 3 233.68 30.10 -5 -14 3 215.08 22.20 4 14 -3 51.19 14.30 -4 -14 3 105.69 20.30 -4 -14 3 43.60 15.10 3 14 -3 451.65 33.00 -3 -14 3 446.66 26.10 -3 -14 3 418.36 35.70 -3 -14 3 420.16 30.40 2 14 -3 16.60 8.20 -2 -14 3 9.70 6.30 -2 -14 3 8.80 10.30 -2 -14 3 13.20 10.30 -1 -14 3 107.29 23.30 -1 -14 3 76.49 17.00 -1 -14 3 115.49 22.10 -1 -14 3 86.59 19.40 0 -14 3 313.77 29.50 0 -14 3 291.97 25.10 0 -14 3 311.67 28.80 0 -14 3 272.17 27.00 -1 14 -3 141.89 26.00 1 -14 3 151.38 22.40 1 -14 3 149.19 23.90 1 -14 3 113.09 21.70 1 -14 3 195.88 26.10 -2 14 -3 486.45 37.70 2 -14 3 524.25 35.90 2 -14 3 453.65 36.20 2 -14 3 544.15 36.90 2 -14 3 565.54 38.00 -3 14 -3 -9.00 13.50 3 -14 3 7.40 12.50 3 -14 3 7.20 11.90 3 -14 3 5.90 9.60 3 -14 3 13.90 11.30 -4 14 -3 97.39 26.20 4 -14 3 49.20 12.50 4 -14 3 19.90 12.80 4 -14 3 6.40 15.70 -5 14 -3 552.24 42.80 5 -14 3 586.54 37.30 5 -14 3 519.45 46.40 5 -14 3 557.14 42.30 5 -14 3 600.44 41.60 -6 14 -3 539.35 42.00 6 -14 3 558.44 40.50 6 -14 3 557.94 37.20 -7 14 -3 20.00 16.80 7 -14 3 -1.00 12.00 7 -14 3 3.90 13.80 7 -14 3 18.90 13.60 -8 14 -3 -7.90 12.90 8 -14 3 5.30 13.20 8 -14 3 -1.60 12.20 8 -14 3 4.50 14.90 -9 14 -3 148.49 34.40 9 -14 3 210.78 37.50 9 -14 3 150.38 32.40 -10 14 -3 45.80 20.80 10 -14 3 45.60 17.10 10 -14 3 19.10 18.10 -11 14 -3 -2.00 17.70 11 -14 3 -8.90 19.00 -12 14 -3 56.29 21.30 12 -14 3 67.69 21.80 12 -14 3 19.50 21.30 13 13 -3 55.69 16.10 -13 -13 3 34.30 17.20 -13 -13 3 38.60 21.70 -13 -13 3 22.10 23.10 12 13 -3 10.40 12.50 -12 -13 3 45.90 19.80 -12 -13 3 104.79 28.90 -12 -13 3 34.00 22.20 11 13 -3 2.10 11.00 -11 -13 3 6.40 9.30 -11 -13 3 2.60 11.50 -11 -13 3 11.70 19.80 -11 -13 3 -14.10 14.10 -10 -13 3 20.00 16.00 -10 -13 3 25.30 21.10 -10 -13 3 25.80 10.50 9 13 -3 76.19 21.30 -9 -13 3 71.39 20.70 -9 -13 3 35.00 15.60 -9 -13 3 57.59 17.20 -9 -13 3 31.10 17.90 8 13 -3 69.39 21.40 -8 -13 3 52.79 18.60 -8 -13 3 33.50 11.90 -8 -13 3 41.80 16.30 7 13 -3 57.59 19.30 -7 -13 3 42.50 11.50 -7 -13 3 51.99 16.60 -7 -13 3 53.29 16.90 6 13 -3 278.97 26.30 -6 -13 3 292.77 31.20 -6 -13 3 264.87 23.70 -6 -13 3 324.37 23.60 5 13 -3 949.80 46.40 -5 -13 3 977.40 51.39 -5 -13 3 1041.10 43.10 -5 -13 3 1002.90 40.10 4 13 -3 98.19 19.00 -4 -13 3 119.79 17.50 -4 -13 3 85.39 14.60 -4 -13 3 93.09 22.70 3 13 -3 6.20 8.60 -3 -13 3 0.90 5.80 -3 -13 3 -2.40 8.80 -3 -13 3 21.00 12.90 2 13 -3 54.89 15.80 -2 -13 3 63.59 15.30 -2 -13 3 79.09 18.10 -1 -13 3 159.98 20.00 -1 -13 3 140.39 23.10 -1 -13 3 134.09 20.00 0 -13 3 -4.50 10.60 0 -13 3 -2.50 10.90 0 -13 3 9.10 7.00 0 -13 3 12.00 9.50 -1 13 -3 57.99 16.20 1 -13 3 91.79 21.80 1 -13 3 68.89 18.20 1 -13 3 63.89 19.40 1 -13 3 62.29 18.20 -2 13 -3 92.29 22.80 2 -13 3 101.99 20.30 2 -13 3 123.79 22.00 2 -13 3 91.19 22.60 2 -13 3 116.69 23.00 -3 13 -3 343.17 33.40 3 -13 3 403.46 31.20 3 -13 3 408.76 43.10 3 -13 3 384.66 31.40 -4 13 -3 116.69 24.80 4 -13 3 115.49 25.10 4 -13 3 89.49 23.30 4 -13 3 140.39 20.70 -5 13 -3 25.90 14.70 5 -13 3 39.40 13.00 5 -13 3 40.00 14.80 5 -13 3 17.60 11.50 -6 13 -3 12.60 15.20 6 -13 3 3.10 12.20 6 -13 3 23.00 12.10 6 -13 3 -0.90 12.60 -7 13 -3 158.88 30.70 7 -13 3 157.48 23.80 7 -13 3 126.79 24.40 -8 13 -3 -2.10 14.90 8 -13 3 -11.60 13.70 8 -13 3 -9.70 12.20 -9 13 -3 139.89 28.40 9 -13 3 149.69 27.40 -10 13 -3 16.20 18.00 10 -13 3 13.20 14.70 10 -13 3 14.20 18.10 -11 13 -3 0.40 18.50 11 -13 3 1.40 18.70 11 -13 3 -27.40 18.50 -12 13 -3 124.59 34.00 12 -13 3 89.79 24.50 12 -13 3 112.99 31.50 -13 13 -3 157.38 34.60 13 -13 3 128.69 30.90 13 -13 3 163.78 36.50 13 12 -3 17.70 13.20 -13 -12 3 100.49 33.30 -13 -12 3 -10.80 19.30 -13 -12 3 -4.90 17.10 -12 -12 3 140.49 34.50 -12 -12 3 121.69 31.20 -12 -12 3 95.29 28.20 11 12 -3 251.57 34.80 -11 -12 3 245.88 31.00 -11 -12 3 203.88 31.80 -11 -12 3 228.28 37.70 10 12 -3 288.57 28.80 -10 -12 3 300.07 30.10 -10 -12 3 230.68 35.00 -10 -12 3 219.08 16.80 -10 -12 3 219.28 30.50 9 12 -3 222.18 25.00 -9 -12 3 239.78 25.10 -9 -12 3 175.28 19.60 -9 -12 3 148.69 27.60 -9 -12 3 151.98 31.50 8 12 -3 -1.30 7.50 -8 -12 3 -9.90 8.00 -8 -12 3 6.10 13.50 -8 -12 3 -5.50 12.60 -8 -12 3 -13.90 8.50 7 12 -3 62.19 17.80 -7 -12 3 42.80 15.80 -7 -12 3 49.99 17.10 -7 -12 3 45.90 14.40 6 12 -3 10.70 7.60 -6 -12 3 5.10 6.90 -6 -12 3 48.50 14.80 -6 -12 3 13.50 13.10 5 12 -3 163.88 19.20 -5 -12 3 134.39 24.10 -5 -12 3 136.19 17.70 -5 -12 3 140.39 18.50 -4 -12 3 33.30 12.20 -4 -12 3 43.30 14.20 3 12 -3 102.79 18.10 -3 -12 3 114.79 21.70 -3 -12 3 114.09 15.30 -3 -12 3 79.79 16.10 2 12 -3 124.69 18.90 -2 -12 3 133.19 19.80 -2 -12 3 133.19 16.30 -2 -12 3 161.88 21.10 -1 -12 3 692.73 38.30 -1 -12 3 686.23 33.30 -1 -12 3 710.43 35.90 0 -12 3 123.99 17.60 0 -12 3 145.39 20.10 0 -12 3 102.69 19.90 -1 12 -3 1838.82 68.79 1 -12 3 1814.12 67.49 1 -12 3 1779.52 63.99 1 -12 3 1835.82 64.79 1 -12 3 1687.53 63.29 -2 12 -3 21.70 12.90 2 -12 3 30.60 12.30 2 -12 3 31.60 10.60 2 -12 3 39.30 13.10 -3 12 -3 173.88 24.10 3 -12 3 170.88 20.80 3 -12 3 191.78 28.50 3 -12 3 156.08 24.40 3 -12 3 200.08 22.80 -4 12 -3 458.45 35.40 4 -12 3 444.66 35.70 4 -12 3 444.96 32.90 4 -12 3 413.26 28.00 -5 12 -3 143.79 25.20 5 -12 3 145.59 20.10 5 -12 3 140.99 22.50 -6 12 -3 363.16 34.10 6 -12 3 377.46 28.00 6 -12 3 381.36 36.20 6 -12 3 351.36 31.70 -7 12 -3 313.87 31.90 7 -12 3 306.57 27.50 7 -12 3 353.06 35.10 7 -12 3 291.47 30.60 -8 12 -3 40.00 18.00 8 -12 3 100.59 27.90 8 -12 3 40.50 18.30 -9 12 -3 26.10 17.50 9 -12 3 29.30 16.10 9 -12 3 86.69 22.20 -10 12 -3 6.60 15.50 10 -12 3 6.50 14.80 10 -12 3 -6.60 14.90 -11 12 -3 -5.20 16.90 11 -12 3 38.00 18.50 11 -12 3 9.30 16.70 -12 12 -3 67.99 23.70 12 -12 3 67.09 22.40 12 -12 3 71.89 21.80 -13 12 -3 8.50 18.00 13 -12 3 10.50 18.80 14 11 -3 -3.90 13.00 -14 -11 3 17.00 20.10 -14 -11 3 -24.60 16.90 13 11 -3 22.30 14.20 -13 -11 3 -9.90 16.00 -13 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22.10 12 -11 3 108.79 37.90 12 -11 3 132.09 29.00 -13 11 -3 2.70 13.40 -13 11 -3 25.40 24.60 13 -11 3 21.40 18.20 13 -11 3 4.30 19.80 -14 11 -3 -11.40 14.30 -14 11 -3 8.00 20.30 14 -11 3 -24.10 21.40 14 -11 3 0.40 19.40 14 10 -3 32.70 15.70 -14 -10 3 8.70 18.00 -14 -10 3 -11.40 25.10 -14 -10 3 -16.50 17.50 13 10 -3 257.57 36.40 -13 -10 3 313.87 38.40 -13 -10 3 204.18 32.10 -13 -10 3 277.87 40.60 -12 -10 3 41.90 16.50 -12 -10 3 85.79 26.30 -12 -10 3 73.19 23.40 11 10 -3 103.29 24.30 -11 -10 3 99.89 32.60 -11 -10 3 123.79 26.50 10 10 -3 89.79 21.50 -10 -10 3 9.70 14.30 -10 -10 3 39.30 11.50 -10 -10 3 40.40 16.00 9 10 -3 622.74 36.90 -9 -10 3 593.24 43.30 -9 -10 3 619.94 35.70 -9 -10 3 572.34 38.90 -9 -10 3 584.44 22.20 8 10 -3 151.68 19.50 -8 -10 3 146.79 20.00 -8 -10 3 111.29 24.50 -8 -10 3 117.89 13.20 -8 -10 3 142.39 23.30 7 10 -3 0.80 6.00 -7 -10 3 -4.60 7.10 -7 -10 3 -5.70 9.90 -7 -10 3 -4.30 6.70 -7 -10 3 -4.20 11.00 6 10 -3 189.18 19.90 -6 -10 3 214.88 26.00 -6 -10 3 179.98 16.00 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10 -3 220.48 26.80 7 -10 3 212.48 21.50 7 -10 3 196.18 23.60 7 -10 3 174.48 29.40 -8 10 -3 227.98 27.50 8 -10 3 216.58 26.70 8 -10 3 262.17 31.60 -9 10 -3 488.15 39.00 9 -10 3 546.65 45.10 9 -10 3 487.25 36.30 -10 10 -3 396.56 36.80 10 -10 3 338.07 32.30 10 -10 3 372.46 40.20 -11 10 -3 243.48 31.80 11 -10 3 165.68 27.90 11 -10 3 254.37 37.20 -12 10 -3 2.70 17.80 12 -10 3 -2.70 17.20 12 -10 3 -0.30 14.80 -13 10 -3 235.28 26.00 -13 10 -3 208.28 32.50 13 -10 3 188.38 31.30 13 -10 3 161.38 29.90 -14 10 -3 219.08 28.40 -14 10 -3 194.38 42.20 14 -10 3 305.07 53.79 14 -10 3 305.87 36.00 15 9 -3 157.88 39.20 -15 -9 3 121.39 32.20 -14 -9 3 28.80 22.20 -14 -9 3 -6.40 16.50 -14 -9 3 12.30 18.60 13 9 -3 470.55 39.60 -13 -9 3 444.06 43.30 -13 -9 3 417.56 47.60 -13 -9 3 441.86 40.20 -12 -9 3 10.90 13.60 -12 -9 3 17.40 14.70 -12 -9 3 -4.80 15.90 11 9 -3 112.79 23.70 -11 -9 3 70.59 26.40 -11 -9 3 90.19 23.00 -11 -9 3 63.09 22.30 10 9 -3 34.70 11.30 -10 -9 3 27.60 11.60 -10 -9 3 13.40 13.70 -10 -9 3 18.50 14.90 9 9 -3 0.60 7.20 -9 -9 3 9.60 11.70 -9 -9 3 4.20 9.20 -9 -9 3 -4.80 10.90 -9 -9 3 7.80 5.50 8 9 -3 93.89 17.10 -8 -9 3 72.59 18.10 -8 -9 3 59.49 16.60 -8 -9 3 97.09 21.40 -8 -9 3 61.19 10.40 7 9 -3 125.59 16.80 -7 -9 3 71.99 19.30 -7 -9 3 102.59 20.60 -7 -9 3 99.69 17.90 -7 -9 3 109.19 12.50 6 9 -3 93.39 15.40 -6 -9 3 101.69 20.50 -6 -9 3 104.79 18.70 -6 -9 3 102.79 16.00 5 9 -3 1674.93 57.89 -5 -9 3 1694.73 50.89 -5 -9 3 1717.03 61.79 -5 -9 3 1690.33 54.89 4 9 -3 225.18 20.00 -4 -9 3 227.88 16.90 -4 -9 3 225.68 21.40 -4 -9 3 213.18 17.90 3 9 -3 14.90 6.30 -3 -9 3 15.30 6.20 -3 -9 3 18.90 7.70 -3 -9 3 -2.50 8.20 2 9 -3 1.50 4.90 -2 -9 3 0.60 7.70 -2 -9 3 8.60 4.80 -2 -9 3 -1.60 6.40 1 9 -3 1278.37 48.80 -1 -9 3 1132.99 50.59 -1 -9 3 1239.08 44.50 -1 -9 3 1265.37 44.10 0 -9 3 0.80 7.90 0 -9 3 -4.20 4.90 0 -9 3 6.20 8.20 -1 9 -3 228.08 21.00 1 -9 3 248.68 22.30 1 -9 3 257.27 20.60 1 -9 3 243.58 20.00 -2 9 -3 86.99 15.90 2 -9 3 72.59 16.90 2 -9 3 76.99 14.10 2 -9 3 95.49 15.10 2 -9 3 94.59 17.40 -3 9 -3 115.99 18.90 3 -9 3 117.49 17.40 3 -9 3 105.39 14.40 3 -9 3 113.29 20.70 -4 9 -3 395.36 28.30 4 -9 3 378.56 29.30 4 -9 3 356.76 22.40 4 -9 3 392.56 27.20 -5 9 -3 203.78 22.70 5 -9 3 204.88 24.90 5 -9 3 174.78 20.90 5 -9 3 188.68 17.90 -6 9 -3 9.90 11.50 6 -9 3 8.10 8.80 6 -9 3 2.60 10.10 6 -9 3 13.60 8.20 -7 9 -3 553.54 36.10 7 -9 3 520.35 34.10 7 -9 3 503.25 39.00 -8 9 -3 9.00 12.70 8 -9 3 26.40 11.70 8 -9 3 20.70 12.90 -9 9 -3 1080.19 54.19 9 -9 3 1004.70 48.40 9 -9 3 1102.39 59.39 -10 9 -3 19.70 14.40 10 -9 3 19.50 14.10 10 -9 3 81.99 28.80 -11 9 -3 39.00 18.50 11 -9 3 94.19 30.40 11 -9 3 40.60 17.70 -12 9 -3 11.80 13.00 -12 9 -3 21.50 16.60 12 -9 3 34.00 15.80 12 -9 3 20.80 15.10 -13 9 -3 220.08 26.00 13 -9 3 233.88 31.30 13 -9 3 238.78 44.60 -14 9 -3 112.09 31.60 -14 9 -3 106.59 24.30 14 -9 3 180.48 32.30 14 -9 3 121.89 27.30 -15 9 -3 -5.50 21.60 -15 9 -3 -20.30 15.30 15 -9 3 19.30 23.00 15 -9 3 -18.50 18.00 15 8 -3 6.30 16.50 -15 -8 3 -4.90 19.10 -15 -8 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815.52 35.10 -3 -8 3 774.52 40.20 -3 -8 3 827.22 31.60 -3 -8 3 863.01 33.10 2 8 -3 320.67 21.70 -2 -8 3 284.97 18.50 -2 -8 3 312.87 21.80 -2 -8 3 307.87 19.50 1 8 -3 800.82 35.90 -1 -8 3 796.72 34.50 -1 -8 3 853.51 33.80 -1 -8 3 839.72 33.50 0 -8 3 601.14 28.70 0 -8 3 634.24 29.40 0 -8 3 571.74 28.80 -1 8 -3 488.65 27.80 1 -8 3 495.85 25.40 1 -8 3 459.35 27.90 1 -8 3 508.45 27.30 -2 8 -3 30.80 10.00 2 -8 3 18.00 7.50 2 -8 3 30.00 9.60 2 -8 3 24.10 7.90 -3 8 -3 2067.49 67.59 3 -8 3 2155.98 62.09 3 -8 3 2189.48 67.69 -4 8 -3 365.06 26.20 4 -8 3 343.27 27.20 4 -8 3 349.57 21.20 4 -8 3 331.77 24.20 -5 8 -3 87.29 17.20 5 -8 3 98.49 18.80 5 -8 3 115.99 15.20 5 -8 3 119.09 17.20 -6 8 -3 -0.70 10.40 6 -8 3 5.80 10.30 6 -8 3 12.90 9.00 6 -8 3 9.40 7.50 -7 8 -3 2564.74 84.59 7 -8 3 2553.74 80.99 7 -8 3 2655.53 93.39 -8 8 -3 84.79 22.80 8 -8 3 76.69 16.50 8 -8 3 54.49 14.10 -9 8 -3 141.19 24.50 9 -8 3 113.49 19.10 9 -8 3 193.58 27.60 -10 8 -3 34.30 16.50 10 -8 3 82.09 27.30 10 -8 3 29.70 15.50 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632.94 34.90 -8 -7 3 662.63 37.40 -8 -7 3 605.34 17.80 -8 -7 3 613.14 38.90 7 7 -3 594.54 31.90 -7 -7 3 575.64 35.70 -7 -7 3 591.54 34.10 -7 -7 3 579.14 31.70 -7 -7 3 579.74 19.80 6 7 -3 120.69 15.30 -6 -7 3 177.58 19.20 -6 -7 3 133.99 17.20 -6 -7 3 129.29 11.40 -6 -7 3 146.29 17.80 5 7 -3 77.99 13.50 -5 -7 3 61.19 13.10 -5 -7 3 52.49 14.40 -5 -7 3 82.49 15.40 -5 -7 3 67.19 10.20 4 7 -3 1694.23 54.39 -4 -7 3 1651.93 52.09 -4 -7 3 1676.83 55.59 -4 -7 3 1665.83 56.49 -4 -7 3 1709.23 48.20 3 7 -3 601.44 28.30 -3 -7 3 591.24 26.50 -3 -7 3 648.94 29.50 -3 -7 3 573.34 27.50 2 7 -3 141.29 14.30 -2 -7 3 142.99 15.20 -2 -7 3 130.89 13.30 -2 -7 3 150.48 13.80 1 7 -3 443.16 25.10 -1 -7 3 431.66 22.10 -1 -7 3 432.36 23.80 -1 -7 3 438.26 22.80 0 7 -3 937.41 38.80 0 -7 3 916.81 35.10 0 -7 3 997.90 35.90 0 -7 3 917.61 36.50 -1 7 -3 30.80 9.40 1 -7 3 46.00 10.90 1 -7 3 40.00 11.30 1 -7 3 23.30 7.30 2 -7 3 83.19 13.70 2 -7 3 98.99 12.70 -3 7 -3 1529.35 52.39 3 -7 3 1417.96 56.59 3 -7 3 1500.05 50.99 3 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2.40 11.40 11 -6 3 15.50 11.50 -12 6 -3 2.10 9.70 -12 6 -3 -5.90 14.00 12 -6 3 -4.60 11.30 12 -6 3 -24.80 13.60 -13 6 -3 297.07 36.20 -13 6 -3 306.97 25.00 13 -6 3 244.28 39.10 13 -6 3 231.48 26.60 -14 6 -3 14.10 20.20 -14 6 -3 6.90 12.10 14 -6 3 9.70 18.20 14 -6 3 -21.70 13.60 -15 6 -3 10.30 13.40 -15 6 -3 11.80 20.00 15 -6 3 43.00 21.50 15 -6 3 30.00 15.90 -16 6 -3 11.90 19.10 16 -6 3 21.40 22.70 16 5 -3 33.80 20.90 -16 -5 3 22.00 19.20 -16 -5 3 42.70 26.10 15 5 -3 128.99 35.70 -15 -5 3 72.59 23.10 -15 -5 3 25.80 22.80 14 5 -3 33.00 15.00 -14 -5 3 30.60 18.60 -14 -5 3 5.50 14.20 -14 -5 3 5.70 18.00 13 5 -3 93.09 27.50 -13 -5 3 95.09 23.50 -13 -5 3 75.69 19.80 -13 -5 3 52.79 17.90 -12 -5 3 7.80 12.50 -12 -5 3 9.60 14.60 -12 -5 3 -3.30 14.70 11 5 -3 11.00 8.60 -11 -5 3 19.40 12.70 -11 -5 3 19.90 12.80 -11 -5 3 32.80 15.30 10 5 -3 342.77 28.20 -10 -5 3 328.47 31.50 -10 -5 3 314.17 31.90 -10 -5 3 322.37 27.10 9 5 -3 55.69 15.80 -9 -5 3 36.20 14.50 -9 -5 3 31.80 11.70 -9 -5 3 30.20 11.90 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454.05 23.80 3 -5 3 432.66 18.40 3 -5 3 460.15 23.40 -4 5 -3 108.19 17.10 4 -5 3 88.69 16.70 4 -5 3 118.79 10.70 4 -5 3 117.69 13.40 -5 5 -3 1.00 8.20 5 -5 3 0.50 6.40 5 -5 3 0.60 5.90 -6 5 -3 930.81 40.30 6 -5 3 904.41 37.20 6 -5 3 876.71 43.30 -7 5 -3 106.49 18.20 7 -5 3 80.59 19.60 7 -5 3 83.49 13.70 -8 5 -3 466.45 32.50 8 -5 3 454.15 34.60 8 -5 3 476.85 27.30 -9 5 -3 462.45 23.80 -9 5 -3 457.75 33.80 9 -5 3 455.95 28.80 9 -5 3 447.06 36.70 -10 5 -3 260.77 28.80 -10 5 -3 307.57 20.30 10 -5 3 315.47 24.20 10 -5 3 313.07 31.80 -11 5 -3 16.20 14.30 -11 5 -3 13.20 9.60 11 -5 3 22.60 12.60 11 -5 3 5.90 13.00 -12 5 -3 168.18 29.70 12 -5 3 171.58 30.30 12 -5 3 191.88 22.60 -13 5 -3 154.48 30.80 -13 5 -3 137.09 21.00 13 -5 3 135.39 21.90 13 -5 3 112.79 36.50 -14 5 -3 13.00 11.80 -14 5 -3 5.60 18.50 14 -5 3 6.30 16.00 14 -5 3 8.80 13.70 -15 5 -3 9.60 21.20 -15 5 -3 25.50 14.20 15 -5 3 46.10 16.00 15 -5 3 33.40 18.00 -16 5 -3 28.80 23.00 -16 5 -3 15.30 14.60 16 -5 3 -0.10 21.60 16 -5 3 -20.40 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14.30 13.80 -10 4 -3 20.10 8.20 10 -4 3 0.50 9.60 10 -4 3 2.60 9.00 -11 4 -3 13.20 8.30 -11 4 -3 16.20 16.00 11 -4 3 15.00 11.30 11 -4 3 7.90 10.30 -12 4 -3 191.58 22.40 -12 4 -3 194.28 31.80 12 -4 3 184.68 32.50 12 -4 3 173.58 21.40 -13 4 -3 56.49 17.90 -13 4 -3 18.50 19.40 13 -4 3 0.40 13.40 13 -4 3 15.20 11.70 -14 4 -3 180.98 22.70 -14 4 -3 164.68 32.50 14 -4 3 201.08 39.20 14 -4 3 138.79 23.90 -15 4 -3 270.17 27.70 -15 4 -3 317.47 43.20 15 -4 3 260.37 28.70 15 -4 3 388.06 49.80 -16 4 -3 47.40 15.50 -16 4 -3 27.70 20.70 16 -4 3 94.09 26.70 16 3 -3 58.99 19.90 -16 -3 3 21.00 24.20 -16 -3 3 7.70 15.90 -16 -3 3 -0.70 24.70 -15 -3 3 199.18 32.60 -15 -3 3 195.08 37.00 -15 -3 3 216.98 48.60 14 3 -3 103.39 32.60 -14 -3 3 -5.50 16.50 -14 -3 3 20.80 13.80 -14 -3 3 6.20 17.20 13 3 -3 110.69 27.20 -13 -3 3 43.70 18.30 -13 -3 3 80.89 22.90 -13 -3 3 56.19 19.10 12 3 -3 74.69 24.50 -12 -3 3 -19.20 14.00 -12 -3 3 -4.90 13.40 -12 -3 3 9.00 11.40 11 3 -3 72.09 21.70 -11 -3 3 2.10 12.70 -11 -3 3 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123.49 37.30 11 15 -4 2.90 13.70 -11 -15 4 -33.90 17.30 -11 -15 4 13.60 13.70 10 15 -4 -2.00 11.90 -10 -15 4 6.20 12.70 -10 -15 4 5.50 17.60 -10 -15 4 -3.00 12.90 9 15 -4 17.80 11.70 -9 -15 4 -9.80 18.70 -9 -15 4 -11.40 11.70 -8 -15 4 411.86 30.00 -8 -15 4 420.56 41.90 -8 -15 4 388.46 29.10 7 15 -4 144.29 24.30 -7 -15 4 151.58 23.00 -7 -15 4 146.59 22.00 -7 -15 4 144.79 30.00 6 15 -4 6.00 10.40 -6 -15 4 -6.30 8.60 -6 -15 4 9.40 12.00 -6 -15 4 -6.70 13.70 5 15 -4 14.00 8.90 -5 -15 4 21.90 9.10 -5 -15 4 6.00 11.60 -5 -15 4 13.60 14.80 4 15 -4 43.20 12.30 -4 -15 4 60.29 17.60 -4 -15 4 41.90 16.80 -4 -15 4 68.69 18.70 3 15 -4 36.40 11.80 -3 -15 4 10.00 15.10 -3 -15 4 25.40 9.10 -3 -15 4 27.80 12.50 -2 -15 4 200.38 24.10 -2 -15 4 208.08 22.10 -2 -15 4 187.08 28.50 -1 -15 4 207.98 23.40 -1 -15 4 192.98 24.40 -1 -15 4 236.08 28.30 -1 -15 4 167.58 26.50 0 15 -4 625.04 44.70 0 -15 4 590.64 36.80 0 -15 4 643.04 42.50 0 -15 4 645.44 40.80 0 -15 4 682.63 43.10 -1 15 -4 -14.50 12.80 1 -15 4 8.90 11.20 1 -15 4 10.10 10.60 1 -15 4 1.00 12.50 1 -15 4 24.60 14.20 -2 15 -4 25.90 15.10 2 -15 4 36.60 13.20 2 -15 4 19.10 13.10 2 -15 4 29.70 16.10 2 -15 4 15.80 11.60 -3 15 -4 448.56 40.50 3 -15 4 503.65 40.50 3 -15 4 457.85 38.00 3 -15 4 487.15 35.20 -4 15 -4 34.20 17.60 4 -15 4 29.70 13.20 4 -15 4 18.40 15.40 4 -15 4 92.19 25.10 4 -15 4 20.50 15.20 -5 15 -4 8.40 16.20 5 -15 4 33.80 16.00 5 -15 4 74.49 20.10 5 -15 4 40.40 15.70 5 -15 4 28.90 16.40 -6 15 -4 411.06 38.20 6 -15 4 417.86 35.10 6 -15 4 447.36 47.90 6 -15 4 358.26 36.20 6 -15 4 339.27 52.39 -7 15 -4 -3.80 14.00 7 -15 4 7.30 14.40 7 -15 4 -4.70 14.70 7 -15 4 -8.30 13.60 -8 15 -4 31.20 19.70 8 -15 4 52.99 15.50 8 -15 4 41.40 18.70 -9 15 -4 1.10 18.80 9 -15 4 16.50 18.60 9 -15 4 7.30 15.60 -10 15 -4 301.87 44.70 10 -15 4 331.97 38.20 10 -15 4 413.86 49.20 -11 15 -4 -1.60 19.60 11 -15 4 -24.90 16.30 11 -15 4 29.00 25.10 12 14 -4 15.20 13.50 -12 -14 4 -5.90 17.40 -12 -14 4 8.40 15.80 11 14 -4 20.00 13.00 -11 -14 4 7.10 13.70 -11 -14 4 8.60 10.50 -11 -14 4 -10.90 15.70 10 14 -4 341.47 35.10 -10 -14 4 359.36 32.50 -10 -14 4 249.08 34.90 -10 -14 4 320.67 24.00 -9 -14 4 23.30 11.40 -9 -14 4 28.20 17.10 -9 -14 4 4.40 11.50 -8 -14 4 95.79 22.50 -8 -14 4 102.39 28.70 -8 -14 4 80.69 18.80 7 14 -4 168.88 24.70 -7 -14 4 129.59 27.90 -7 -14 4 133.89 21.50 -7 -14 4 191.58 23.70 6 14 -4 282.77 27.90 -6 -14 4 321.47 26.00 -6 -14 4 316.07 36.00 -6 -14 4 303.47 26.30 5 14 -4 299.27 29.40 -5 -14 4 265.77 31.40 -5 -14 4 304.77 25.30 -5 -14 4 312.57 25.30 4 14 -4 656.13 40.80 -4 -14 4 667.23 45.00 -4 -14 4 631.04 33.40 -4 -14 4 665.73 36.00 3 14 -4 428.26 32.40 -3 -14 4 415.86 34.10 -3 -14 4 418.36 27.30 -3 -14 4 379.36 29.20 2 14 -4 510.55 37.80 -2 -14 4 513.35 37.50 -2 -14 4 495.95 33.40 -2 -14 4 510.05 30.70 -1 -14 4 58.59 17.80 -1 -14 4 55.59 16.70 -1 -14 4 45.90 15.90 0 14 -4 59.99 18.50 0 -14 4 78.09 23.20 0 -14 4 110.79 21.50 0 -14 4 105.89 20.20 -1 14 -4 136.09 25.70 1 -14 4 165.08 24.00 1 -14 4 156.58 27.70 1 -14 4 163.88 24.40 1 -14 4 143.29 23.60 -2 14 -4 168.08 26.80 2 -14 4 192.98 25.90 2 -14 4 151.68 23.40 2 -14 4 236.98 28.00 2 -14 4 156.48 26.80 -3 14 -4 13.60 13.00 3 -14 4 7.70 10.80 3 -14 4 19.90 12.60 3 -14 4 21.50 11.80 -4 14 -4 704.73 46.60 4 -14 4 752.02 50.19 4 -14 4 767.02 49.30 4 -14 4 779.72 41.20 4 -14 4 731.23 45.20 -5 14 -4 -9.40 14.00 5 -14 4 12.30 13.20 5 -14 4 24.60 14.50 5 -14 4 12.90 13.30 5 -14 4 5.50 11.20 -6 14 -4 361.16 35.50 6 -14 4 384.66 32.90 6 -14 4 381.36 37.00 6 -14 4 381.06 39.10 -7 14 -4 55.39 19.20 7 -14 4 109.09 28.50 7 -14 4 79.49 23.60 7 -14 4 94.99 32.30 -8 14 -4 12.00 15.70 8 -14 4 30.60 18.50 8 -14 4 29.60 13.80 8 -14 4 26.30 14.90 -9 14 -4 100.79 30.10 9 -14 4 85.19 27.50 9 -14 4 147.19 38.50 -10 14 -4 58.59 24.00 10 -14 4 111.99 28.00 10 -14 4 175.08 40.80 -11 14 -4 -8.70 19.10 11 -14 4 17.60 17.70 11 -14 4 17.10 20.90 -12 14 -4 258.27 41.70 12 -14 4 178.78 50.39 12 -14 4 240.38 37.40 13 13 -4 19.40 15.40 -13 -13 4 35.50 20.10 -13 -13 4 2.30 18.20 12 13 -4 30.70 14.90 -12 -13 4 23.70 23.20 -12 -13 4 1.90 16.10 -12 -13 4 11.00 15.20 11 13 -4 234.98 32.70 -11 -13 4 218.18 32.40 -11 -13 4 200.18 34.20 -11 -13 4 174.28 15.60 -11 -13 4 131.49 28.70 -10 -13 4 587.14 45.20 -10 -13 4 653.93 40.50 9 13 -4 -2.60 10.40 -9 -13 4 -18.10 14.90 -9 -13 4 6.30 10.80 -9 -13 4 -0.50 10.20 8 13 -4 31.30 10.90 -8 -13 4 14.70 15.90 -8 -13 4 37.60 11.20 -8 -13 4 29.60 11.00 7 13 -4 4.10 8.50 -7 -13 4 41.90 11.70 -7 -13 4 14.80 8.60 -7 -13 4 12.80 11.80 6 13 -4 778.42 42.90 -6 -13 4 857.61 40.10 -6 -13 4 826.42 49.50 -6 -13 4 892.91 38.90 5 13 -4 1.10 7.70 -5 -13 4 28.10 11.80 -5 -13 4 5.60 11.20 -5 -13 4 15.70 7.80 4 13 -4 91.59 19.30 -4 -13 4 71.49 16.00 -4 -13 4 47.10 16.30 -4 -13 4 86.49 18.30 3 13 -4 230.28 25.30 -3 -13 4 233.98 22.80 -3 -13 4 257.47 28.40 -3 -13 4 235.88 22.10 2 13 -4 -2.50 7.10 -2 -13 4 0.80 8.30 -2 -13 4 0.90 10.40 -2 -13 4 -3.90 9.70 -1 -13 4 1.10 9.30 -1 -13 4 7.50 10.90 0 13 -4 306.07 30.30 0 -13 4 380.06 31.90 0 -13 4 307.87 27.70 0 -13 4 323.97 27.50 -1 13 -4 227.08 26.80 1 -13 4 207.48 24.10 1 -13 4 218.98 24.90 1 -13 4 299.07 30.60 1 -13 4 242.88 26.20 -2 13 -4 353.66 33.10 2 -13 4 412.06 35.20 2 -13 4 395.66 29.80 2 -13 4 396.76 31.70 -3 13 -4 233.68 30.90 3 -13 4 221.78 46.10 3 -13 4 215.88 25.20 3 -13 4 241.38 25.60 3 -13 4 199.58 28.40 -4 13 -4 80.39 22.40 4 -13 4 83.79 20.60 4 -13 4 70.49 21.40 4 -13 4 42.20 13.30 -5 13 -4 -10.90 13.20 5 -13 4 14.40 11.30 5 -13 4 16.00 12.50 5 -13 4 24.70 13.30 -6 13 -4 52.29 18.00 6 -13 4 74.89 21.80 6 -13 4 45.00 12.80 6 -13 4 45.10 14.60 -7 13 -4 33.80 18.90 7 -13 4 71.89 22.00 7 -13 4 41.80 18.60 7 -13 4 42.30 15.50 -8 13 -4 1004.50 56.19 8 -13 4 994.90 47.10 8 -13 4 1189.58 63.29 8 -13 4 970.80 54.59 -9 13 -4 18.90 17.00 9 -13 4 12.80 17.90 9 -13 4 10.40 16.60 -10 13 -4 17.90 17.60 10 -13 4 30.80 16.10 10 -13 4 37.70 17.90 -11 13 -4 7.60 20.10 11 -13 4 -5.60 17.80 11 -13 4 -10.70 17.40 -12 13 -4 162.38 37.20 12 -13 4 143.39 45.80 12 -13 4 125.79 32.40 -13 13 -4 21.40 21.10 13 -13 4 -30.30 17.00 13 -13 4 -28.20 25.00 13 12 -4 38.50 16.30 -13 -12 4 41.10 20.30 -13 -12 4 39.10 23.30 -13 -12 4 21.90 17.40 12 12 -4 447.36 38.40 -12 -12 4 364.06 43.10 -12 -12 4 348.97 39.10 -12 -12 4 389.36 44.20 11 12 -4 -11.00 10.30 -11 -12 4 18.40 16.60 -11 -12 4 21.30 20.50 -11 -12 4 6.50 13.10 10 12 -4 31.20 11.60 -10 -12 4 64.89 13.90 -10 -12 4 91.19 29.80 -10 -12 4 21.50 14.80 -10 -12 4 19.10 12.30 9 12 -4 5.30 9.30 -9 -12 4 4.00 10.30 -9 -12 4 5.60 9.10 -9 -12 4 14.90 14.60 -9 -12 4 -0.60 13.60 8 12 -4 3.30 7.60 -8 -12 4 0.70 11.30 -8 -12 4 2.40 8.90 -8 -12 4 22.70 9.40 7 12 -4 244.78 25.80 -7 -12 4 188.38 22.60 -7 -12 4 223.08 27.40 -7 -12 4 253.27 21.20 6 12 -4 5.80 8.00 -6 -12 4 5.10 7.60 -6 -12 4 14.70 12.70 -6 -12 4 2.40 8.90 5 12 -4 11.10 7.60 -5 -12 4 2.60 7.00 -5 -12 4 -5.50 9.10 -5 -12 4 -2.70 12.40 4 12 -4 179.78 21.40 -4 -12 4 187.28 24.80 -4 -12 4 186.28 20.70 3 12 -4 132.59 19.50 -3 -12 4 139.49 17.70 -3 -12 4 107.99 18.80 -3 -12 4 119.29 21.70 2 12 -4 54.59 16.60 -2 -12 4 50.09 16.60 -2 -12 4 63.09 14.40 -2 -12 4 54.49 17.00 -1 -12 4 578.84 35.90 -1 -12 4 599.14 32.20 -1 -12 4 549.74 32.70 0 12 -4 745.53 42.10 0 -12 4 751.92 39.00 0 -12 4 732.63 38.20 0 -12 4 739.13 38.80 -1 12 -4 10.20 11.00 1 -12 4 19.10 9.90 1 -12 4 17.60 12.40 1 -12 4 5.90 7.30 -2 12 -4 854.71 45.50 2 -12 4 793.32 43.50 2 -12 4 1081.89 75.89 2 -12 4 861.31 42.50 2 -12 4 833.92 44.70 -3 12 -4 74.59 21.00 3 -12 4 110.19 23.90 3 -12 4 96.79 24.30 3 -12 4 66.49 17.80 3 -12 4 89.59 20.00 -4 12 -4 0.80 12.60 4 -12 4 12.40 13.00 4 -12 4 2.20 10.80 4 -12 4 -16.20 16.20 4 -12 4 -13.60 9.00 -5 12 -4 16.90 14.70 5 -12 4 9.00 12.20 5 -12 4 11.00 10.00 5 -12 4 19.40 11.20 -6 12 -4 15.40 15.10 6 -12 4 15.60 11.70 6 -12 4 11.60 10.60 6 -12 4 9.00 13.60 -7 12 -4 306.87 33.20 7 -12 4 247.08 34.90 7 -12 4 246.98 25.00 7 -12 4 248.48 28.60 -8 12 -4 1.70 14.90 8 -12 4 19.00 13.80 8 -12 4 13.70 15.60 -9 12 -4 0.50 14.30 9 -12 4 18.40 15.40 9 -12 4 34.90 15.90 -10 12 -4 203.68 32.90 10 -12 4 201.78 30.10 10 -12 4 289.57 39.10 -11 12 -4 151.98 32.60 11 -12 4 159.18 30.00 11 -12 4 209.88 40.40 -12 12 -4 26.90 20.10 12 -12 4 5.10 19.80 12 -12 4 21.10 17.30 -13 12 -4 13.70 22.20 13 -12 4 -15.60 20.70 13 -12 4 4.20 18.40 14 11 -4 49.40 16.00 -14 -11 4 62.49 21.70 -14 -11 4 45.60 19.40 13 11 -4 87.69 29.80 -13 -11 4 14.50 19.20 -13 -11 4 3.90 15.20 -13 -11 4 9.80 18.50 12 11 -4 109.69 28.00 -12 -11 4 74.19 23.70 -12 -11 4 85.79 18.20 -12 -11 4 50.59 19.90 11 11 -4 0.70 9.20 -11 -11 4 -18.60 12.70 -11 -11 4 -20.20 14.00 -11 -11 4 5.20 12.80 10 11 -4 27.50 11.00 -10 -11 4 8.40 11.30 -10 -11 4 24.90 18.30 -10 -11 4 -8.60 14.20 -10 -11 4 51.89 12.20 9 11 -4 78.39 21.60 -9 -11 4 75.09 13.50 -9 -11 4 92.49 26.90 -9 -11 4 60.49 17.80 -9 -11 4 73.19 21.60 8 11 -4 61.49 18.80 -8 -11 4 30.10 15.30 -8 -11 4 31.90 9.80 -8 -11 4 23.80 10.20 -8 -11 4 10.80 12.80 7 11 -4 384.76 28.60 -7 -11 4 373.56 27.20 -7 -11 4 387.86 33.20 -7 -11 4 392.26 23.10 6 11 -4 64.59 15.60 -6 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28.90 18.90 -12 13 -5 1.10 17.60 12 -13 5 14.30 20.70 12 -13 5 20.30 17.70 -13 13 -5 51.09 24.10 13 -13 5 45.20 22.00 13 -13 5 24.60 25.90 13 12 -5 32.20 16.20 -13 -12 5 50.49 23.90 -13 -12 5 11.80 19.40 -13 -12 5 71.79 26.10 12 12 -5 22.70 13.90 -12 -12 5 9.50 17.60 -12 -12 5 20.70 19.30 -12 -12 5 25.50 17.30 11 12 -5 14.30 12.30 -11 -12 5 -1.20 16.80 -11 -12 5 -10.00 9.10 -11 -12 5 -10.70 13.30 -11 -12 5 -2.10 16.00 10 12 -5 117.29 24.30 -10 -12 5 34.30 17.50 -10 -12 5 87.39 16.20 -10 -12 5 59.49 15.60 9 12 -5 116.99 23.70 -9 -12 5 112.69 16.80 -9 -12 5 76.49 20.50 -9 -12 5 118.89 25.70 8 12 -5 79.29 22.40 -8 -12 5 101.49 16.80 -8 -12 5 130.89 24.80 -8 -12 5 97.49 24.50 7 12 -5 754.62 43.00 -7 -12 5 761.02 34.10 -7 -12 5 759.92 40.50 -7 -12 5 714.13 45.40 6 12 -5 -7.50 7.90 -6 -12 5 4.80 9.90 -6 -12 5 1.70 7.70 -6 -12 5 11.40 13.00 5 12 -5 391.26 30.60 -5 -12 5 450.75 27.80 -5 -12 5 364.36 32.00 -5 -12 5 380.26 27.30 4 12 -5 605.94 38.20 -4 -12 5 593.74 33.10 -4 -12 5 629.44 39.90 -4 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429.56 39.70 8 -12 5 456.45 29.40 8 -12 5 451.85 37.30 8 -12 5 441.46 45.00 -9 12 -5 178.48 33.40 9 -12 5 210.48 31.50 9 -12 5 275.97 40.30 -10 12 -5 113.39 29.80 10 -12 5 180.58 37.40 -11 12 -5 42.00 20.50 11 -12 5 61.19 19.60 11 -12 5 83.59 26.90 -12 12 -5 -5.20 18.80 12 -12 5 32.40 21.10 12 -12 5 10.50 17.60 -13 12 -5 4.10 18.80 13 -12 5 -9.60 19.40 13 -12 5 10.30 22.50 14 11 -5 14.50 16.70 -14 -11 5 52.99 24.20 -14 -11 5 52.99 20.90 13 11 -5 472.05 43.50 -13 -11 5 335.57 44.70 -13 -11 5 385.26 44.80 -13 -11 5 304.57 41.30 12 11 -5 93.99 28.50 -12 -11 5 56.19 18.50 -12 -11 5 72.89 26.10 -12 -11 5 32.70 19.70 11 11 -5 46.50 14.30 -11 -11 5 51.69 20.10 -11 -11 5 35.20 18.10 -11 -11 5 49.90 16.00 10 11 -5 7.80 10.60 -10 -11 5 11.80 16.70 -10 -11 5 11.10 7.70 -10 -11 5 4.60 11.80 -10 -11 5 -12.40 15.30 9 11 -5 280.57 29.30 -9 -11 5 247.58 29.60 -9 -11 5 255.87 33.20 -9 -11 5 239.58 31.30 8 11 -5 121.69 22.80 -8 -11 5 164.78 17.00 -8 -11 5 125.39 25.00 -8 -11 5 96.79 23.30 7 11 -5 3.70 8.60 -7 -11 5 -3.60 8.90 -7 -11 5 2.70 8.20 -7 -11 5 -8.70 11.50 6 11 -5 51.79 17.60 -6 -11 5 48.30 14.80 -6 -11 5 38.80 13.30 -6 -11 5 47.40 16.80 5 11 -5 794.02 42.00 -5 -11 5 881.01 45.30 -5 -11 5 846.02 37.20 4 11 -5 -2.80 5.70 -4 -11 5 7.40 10.70 -4 -11 5 -5.40 6.40 -4 -11 5 10.00 9.80 3 11 -5 187.18 22.10 -3 -11 5 150.58 19.20 -3 -11 5 188.68 19.80 -3 -11 5 187.88 22.40 2 11 -5 325.07 27.90 -2 -11 5 353.06 25.40 -2 -11 5 319.57 25.70 -2 -11 5 303.77 26.90 1 11 -5 2187.48 78.39 -1 -11 5 2072.69 69.89 -1 -11 5 2110.39 70.29 -1 -11 5 2167.68 72.49 0 11 -5 13.30 11.80 0 -11 5 4.40 9.50 0 -11 5 21.50 11.60 0 -11 5 0.20 8.10 -1 11 -5 507.75 34.20 1 -11 5 470.25 32.00 1 -11 5 465.35 32.20 1 -11 5 478.35 30.50 -2 11 -5 13.20 12.10 2 -11 5 13.00 10.40 2 -11 5 20.10 12.30 2 -11 5 8.30 9.00 -3 11 -5 9.10 12.30 3 -11 5 6.30 9.00 3 -11 5 20.30 10.50 3 -11 5 3.50 9.50 3 -11 5 -2.70 10.10 -4 11 -5 367.86 31.90 4 -11 5 368.76 29.80 4 -11 5 347.77 32.30 4 -11 5 361.96 26.60 4 -11 5 327.17 33.00 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171.68 26.20 -10 -10 5 153.78 27.80 -10 -10 5 189.08 12.60 -10 -10 5 207.08 31.20 -10 -10 5 182.88 28.40 9 10 -5 19.30 10.90 -9 -10 5 18.90 10.50 -9 -10 5 42.00 17.30 -9 -10 5 41.20 8.70 -9 -10 5 30.00 15.40 8 10 -5 218.28 25.10 -8 -10 5 228.28 25.70 -8 -10 5 205.18 26.70 -8 -10 5 187.08 27.60 -8 -10 5 207.18 20.00 7 10 -5 1041.30 48.60 -7 -10 5 979.80 36.50 -7 -10 5 1005.30 50.29 -7 -10 5 983.00 45.70 6 10 -5 263.37 24.30 -6 -10 5 278.07 36.70 -6 -10 5 249.78 27.10 -6 -10 5 263.97 20.60 5 10 -5 108.69 17.10 -5 -10 5 88.89 16.40 -5 -10 5 121.39 20.30 -5 -10 5 106.99 15.30 4 10 -5 48.40 15.50 -4 -10 5 57.39 14.70 -4 -10 5 38.30 11.90 -4 -10 5 60.69 15.20 3 10 -5 516.75 32.80 -3 -10 5 516.65 29.30 -3 -10 5 500.85 30.80 -3 -10 5 554.64 30.20 2 10 -5 56.79 17.40 -2 -10 5 65.59 16.80 -2 -10 5 74.59 16.40 -2 -10 5 84.59 15.80 1 10 -5 71.69 18.20 -1 -10 5 91.99 15.80 -1 -10 5 110.89 16.60 -1 -10 5 116.19 17.60 0 10 -5 135.49 21.10 0 -10 5 175.78 19.90 0 -10 5 162.48 20.20 0 -10 5 172.48 20.50 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5 69.09 22.60 -14 -9 5 66.49 24.40 13 9 -5 19.00 15.20 -13 -9 5 11.50 16.40 -13 -9 5 43.00 18.60 -13 -9 5 17.80 17.20 12 9 -5 162.28 30.80 -12 -9 5 195.78 37.10 -12 -9 5 111.79 30.00 -12 -9 5 201.28 31.00 11 9 -5 1203.48 57.89 -11 -9 5 1214.28 60.29 -11 -9 5 1179.48 62.89 -11 -9 5 1179.88 60.09 10 9 -5 25.60 11.50 -10 -9 5 41.50 16.20 -10 -9 5 41.70 8.20 -10 -9 5 28.80 11.80 -10 -9 5 25.70 14.80 9 9 -5 0.30 9.10 -9 -9 5 -7.10 9.60 -9 -9 5 7.30 6.90 -9 -9 5 -13.90 11.30 -9 -9 5 -0.10 11.80 -8 -9 5 13.60 13.30 -8 -9 5 23.20 12.70 -8 -9 5 -0.60 7.30 -8 -9 5 -2.80 8.00 7 9 -5 45.00 15.20 -7 -9 5 19.30 12.10 -7 -9 5 38.20 10.40 -6 -9 5 42.50 13.20 -6 -9 5 51.99 16.50 -6 -9 5 45.90 12.70 5 9 -5 621.74 36.00 -5 -9 5 693.93 30.40 -5 -9 5 682.03 34.30 -5 -9 5 691.73 37.10 4 9 -5 343.37 25.90 -4 -9 5 305.07 25.50 -4 -9 5 288.87 22.60 -4 -9 5 334.27 22.00 3 9 -5 1031.50 45.40 -3 -9 5 1083.19 42.60 -3 -9 5 1078.79 45.00 -3 -9 5 992.50 39.20 2 9 -5 22.90 7.80 -2 -9 5 20.00 7.60 -2 -9 5 5.90 8.90 -2 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75.19 21.10 -3 -10 9 85.89 19.60 -3 -10 9 73.69 19.60 -3 -10 9 114.19 20.40 2 10 -9 363.56 31.50 2 10 -9 414.26 35.20 -2 -10 9 347.67 27.70 -2 -10 9 379.86 30.40 -2 -10 9 405.06 30.40 1 10 -9 136.09 24.50 1 10 -9 126.29 22.90 -1 -10 9 147.39 20.30 -1 -10 9 140.59 22.20 -1 -10 9 149.39 19.80 0 10 -9 12.90 10.50 0 -10 9 10.30 10.60 0 -10 9 4.60 9.30 0 -10 9 9.00 9.00 -1 10 -9 241.28 27.10 1 -10 9 169.48 22.00 1 -10 9 249.08 23.80 1 -10 9 246.68 28.30 -2 10 -9 103.99 23.10 2 -10 9 164.98 24.50 2 -10 9 135.29 19.00 2 -10 9 127.39 26.70 -3 10 -9 1005.60 52.69 3 -10 9 1062.19 57.69 3 -10 9 959.50 51.19 3 -10 9 970.10 41.30 -4 10 -9 54.29 19.20 4 -10 9 95.29 21.50 4 -10 9 87.39 28.10 -5 10 -9 171.08 27.80 5 -10 9 172.48 26.40 5 -10 9 164.88 32.60 5 -10 9 182.48 19.90 -6 10 -9 250.77 33.60 6 -10 9 286.27 31.60 6 -10 9 288.77 22.70 -7 10 -9 196.98 31.10 7 -10 9 228.08 21.50 7 -10 9 208.78 29.10 7 -10 9 122.29 35.80 -8 10 -9 0.80 15.70 8 -10 9 42.30 18.30 8 -10 9 32.60 19.70 -9 10 -9 134.69 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18.40 -7 -13 10 20.80 17.00 6 13 -10 231.58 34.30 -6 -13 10 218.18 32.80 -6 -13 10 198.38 27.10 5 13 -10 -1.90 12.70 -5 -13 10 9.80 14.40 -5 -13 10 -8.70 13.10 -5 -13 10 -0.90 14.90 4 13 -10 32.30 14.60 -4 -13 10 26.40 15.70 -4 -13 10 25.40 14.90 -4 -13 10 15.10 11.70 3 13 -10 -22.20 12.80 3 13 -10 2.20 13.70 -3 -13 10 -5.30 10.60 -3 -13 10 11.70 15.90 -3 -13 10 5.50 14.10 2 13 -10 163.28 31.50 2 13 -10 130.19 28.40 -2 -13 10 192.48 31.10 -2 -13 10 156.98 25.60 -2 -13 10 181.48 29.90 1 13 -10 432.56 38.70 -1 -13 10 461.75 38.80 -1 -13 10 549.15 39.30 -1 -13 10 478.25 36.90 0 13 -10 11.30 13.20 0 -13 10 0.40 11.70 0 -13 10 2.60 13.20 0 -13 10 -9.50 13.00 -1 13 -10 9.70 13.40 1 -13 10 29.20 14.20 1 -13 10 2.30 12.70 1 -13 10 18.40 14.60 -2 13 -10 66.19 19.90 2 -13 10 68.99 21.30 2 -13 10 85.59 30.60 2 -13 10 82.99 20.60 -3 13 -10 8.60 16.00 3 -13 10 7.00 14.20 3 -13 10 -3.80 13.70 3 -13 10 4.80 15.00 -4 13 -10 12.20 18.10 4 -13 10 18.30 17.60 4 -13 10 5.40 15.00 4 -13 10 2.20 10.60 -5 13 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431.66 43.20 -7 -12 10 29.70 14.70 -7 -12 10 78.79 24.90 -7 -12 10 52.29 15.50 6 12 -10 519.75 43.20 -6 -12 10 535.55 40.80 -6 -12 10 503.25 35.10 -6 -12 10 474.25 40.80 5 12 -10 196.08 32.30 -5 -12 10 240.98 30.30 -5 -12 10 288.17 31.70 -5 -12 10 297.67 29.10 4 12 -10 140.89 30.60 -4 -12 10 141.89 27.70 -4 -12 10 171.78 25.30 -4 -12 10 125.69 25.80 3 12 -10 4.10 12.40 -3 -12 10 1.20 9.80 -3 -12 10 0.70 12.60 -3 -12 10 1.70 12.30 2 12 -10 -1.60 13.70 2 12 -10 -0.50 12.20 -2 -12 10 -7.30 12.50 -2 -12 10 -5.40 12.60 -2 -12 10 -14.60 9.80 1 12 -10 -10.80 12.50 1 12 -10 -14.30 11.20 -1 -12 10 5.60 12.90 -1 -12 10 2.70 11.10 -1 -12 10 2.60 16.90 0 12 -10 57.19 17.60 0 -12 10 115.79 24.10 0 -12 10 63.59 19.50 -1 12 -10 0.00 12.60 1 -12 10 14.00 13.20 1 -12 10 0.80 13.50 1 -12 10 15.90 11.20 -2 12 -10 104.89 27.00 2 -12 10 117.99 21.80 2 -12 10 139.59 31.50 2 -12 10 69.09 20.60 -3 12 -10 168.88 30.20 3 -12 10 178.78 28.60 3 -12 10 166.48 22.60 3 -12 10 189.68 36.40 -4 12 -10 445.46 43.10 4 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33.20 3 -11 10 307.47 26.20 3 -11 10 341.07 37.60 3 -11 10 257.07 31.50 -4 11 -10 -17.00 15.70 4 -11 10 3.50 14.30 4 -11 10 -1.40 10.30 4 -11 10 -13.90 14.20 -5 11 -10 43.90 20.70 5 -11 10 53.69 19.10 5 -11 10 34.30 16.90 5 -11 10 49.60 13.00 -6 11 -10 -6.40 16.80 6 -11 10 25.40 18.10 6 -11 10 -0.10 14.60 6 -11 10 15.90 10.00 -7 11 -10 6.80 16.50 7 -11 10 1.10 17.40 7 -11 10 18.30 16.60 -8 11 -10 207.48 33.00 8 -11 10 252.97 40.00 8 -11 10 222.58 25.80 8 -11 10 217.68 35.40 -9 11 -10 290.97 40.30 9 -11 10 317.67 45.60 9 -11 10 322.67 38.90 -10 11 -10 412.66 43.00 10 -11 10 506.25 52.89 10 -11 10 456.15 43.80 -11 11 -10 -4.10 19.10 11 -11 10 20.90 21.60 11 -11 10 10.50 19.00 -12 11 -10 10.90 19.10 -12 11 -10 38.40 24.30 12 -11 10 64.69 26.00 12 -11 10 98.69 32.20 13 10 -10 -5.50 19.60 -13 -10 10 -25.20 19.50 12 10 -10 161.98 39.60 -12 -10 10 122.99 28.10 -12 -10 10 82.19 25.70 -12 -10 10 81.99 23.30 11 10 -10 291.27 38.00 -11 -10 10 239.58 22.60 -11 -10 10 243.28 44.20 -11 -10 10 205.38 34.80 10 10 -10 143.49 34.30 -10 -10 10 112.19 22.40 -10 -10 10 70.79 22.90 -10 -10 10 88.39 22.30 9 10 -10 50.39 17.20 -9 -10 10 46.40 14.20 -9 -10 10 52.79 16.10 -9 -10 10 33.20 19.90 8 10 -10 154.78 28.70 -8 -10 10 133.49 29.70 -8 -10 10 121.79 29.90 -8 -10 10 175.58 23.60 7 10 -10 6.40 12.60 -7 -10 10 -7.80 13.10 -7 -10 10 -10.10 13.60 6 10 -10 4.50 10.10 -6 -10 10 0.80 9.90 -6 -10 10 -0.90 13.00 -6 -10 10 -4.50 10.50 5 10 -10 8.30 11.00 -5 -10 10 -0.40 9.40 -5 -10 10 -8.20 12.60 -5 -10 10 -8.60 11.70 4 10 -10 263.57 31.90 -4 -10 10 237.28 27.80 -4 -10 10 244.78 26.70 -4 -10 10 228.88 27.40 3 10 -10 46.60 14.90 -3 -10 10 80.39 19.10 -3 -10 10 89.29 21.60 -3 -10 10 64.19 15.70 2 10 -10 -0.90 9.30 2 10 -10 -4.80 9.80 -2 -10 10 -7.10 10.50 -2 -10 10 1.90 10.70 -2 -10 10 -4.80 9.30 1 10 -10 66.99 21.50 -1 -10 10 52.39 16.50 -1 -10 10 80.79 19.80 0 10 -10 151.58 24.50 0 -10 10 223.38 22.40 0 -10 10 166.48 27.20 0 -10 10 152.18 24.80 -1 10 -10 384.96 34.10 1 -10 10 404.16 36.20 1 -10 10 388.56 28.60 1 -10 10 317.07 31.30 -2 10 -10 1077.39 55.19 2 -10 10 1026.50 53.19 2 -10 10 1063.29 57.49 2 -10 10 998.40 43.10 -3 10 -10 64.19 18.70 3 -10 10 73.29 20.10 3 -10 10 41.60 15.10 -4 10 -10 21.90 13.20 4 -10 10 -2.80 12.00 4 -10 10 10.30 13.10 -5 10 -10 236.78 32.30 5 -10 10 233.48 36.60 5 -10 10 276.47 31.20 5 -10 10 302.37 23.80 -6 10 -10 46.70 18.20 6 -10 10 60.69 22.10 6 -10 10 64.19 17.00 6 -10 10 52.69 19.00 -7 10 -10 92.89 26.60 7 -10 10 182.28 21.00 7 -10 10 137.19 27.40 7 -10 10 141.79 28.30 -8 10 -10 210.68 34.00 8 -10 10 179.08 29.80 8 -10 10 193.68 42.70 -9 10 -10 -3.70 17.50 9 -10 10 -12.10 18.80 9 -10 10 -8.30 14.20 -10 10 -10 298.97 38.70 10 -10 10 330.77 38.00 -11 10 -10 16.70 19.80 11 -10 10 101.89 31.40 11 -10 10 15.80 22.50 -12 10 -10 47.40 25.60 12 -10 10 192.08 55.69 12 -10 10 86.89 28.70 -13 10 -10 -5.00 17.70 13 -10 10 -26.90 19.00 13 -10 10 59.19 27.80 13 9 -10 73.69 21.20 -13 -9 10 56.59 21.60 -13 -9 10 45.80 28.20 12 9 -10 45.80 18.00 -12 -9 10 17.90 10.20 -12 -9 10 27.80 21.20 -12 -9 10 29.20 23.00 11 9 -10 53.79 17.10 -11 -9 10 59.09 20.70 -11 -9 10 14.60 18.70 -11 -9 10 33.70 13.10 10 9 -10 186.78 33.70 -10 -9 10 138.49 30.70 -10 -9 10 143.39 21.10 -10 -9 10 114.89 37.10 9 9 -10 9.80 13.10 -9 -9 10 5.30 11.50 -9 -9 10 28.60 16.70 -9 -9 10 91.39 31.30 8 9 -10 125.09 27.70 -8 -9 10 110.69 21.20 -8 -9 10 119.79 27.50 -8 -9 10 126.79 29.40 7 9 -10 -10.30 10.20 -7 -9 10 1.70 11.30 -7 -9 10 19.50 12.10 -7 -9 10 -21.40 11.50 6 9 -10 51.69 14.90 -6 -9 10 35.40 13.60 -6 -9 10 28.20 14.90 -6 -9 10 64.19 23.30 5 9 -10 64.69 22.70 -5 -9 10 25.80 11.20 -5 -9 10 63.09 20.30 -5 -9 10 37.10 15.20 4 9 -10 19.30 11.60 -4 -9 10 14.20 9.50 -4 -9 10 -3.90 11.40 -4 -9 10 20.30 13.20 3 9 -10 175.88 26.30 -3 -9 10 116.09 19.40 -3 -9 10 158.68 24.40 -3 -9 10 130.49 22.10 2 9 -10 323.37 29.80 2 9 -10 369.46 34.40 -2 -9 10 384.66 28.20 -2 -9 10 365.36 31.60 -2 -9 10 332.67 27.20 1 9 -10 976.20 50.09 1 9 -10 1063.39 55.89 -1 -9 10 1030.80 48.40 -1 -9 10 1022.90 50.79 -1 -9 10 1038.00 44.70 0 9 -10 -10.10 10.50 0 -9 10 3.40 8.10 0 -9 10 -2.60 9.20 0 -9 10 -4.70 10.30 -1 9 -10 642.84 40.80 1 -9 10 740.73 36.20 1 -9 10 697.83 41.30 1 -9 10 698.63 44.20 -2 9 -10 2.60 10.60 2 -9 10 17.10 12.60 2 -9 10 17.00 13.70 -3 9 -10 73.49 22.40 3 -9 10 39.50 11.40 3 -9 10 33.30 14.60 3 -9 10 48.10 16.90 -4 9 -10 175.88 27.10 4 -9 10 177.08 26.20 4 -9 10 119.79 30.00 4 -9 10 170.18 19.60 -5 9 -10 10.60 14.90 5 -9 10 13.50 14.50 5 -9 10 1.30 12.10 5 -9 10 3.90 9.20 -6 9 -10 407.26 38.60 6 -9 10 423.86 24.20 6 -9 10 352.36 34.50 -7 9 -10 300.07 36.00 7 -9 10 274.67 38.90 7 -9 10 356.46 34.40 7 -9 10 373.26 23.10 -8 9 -10 97.79 29.40 8 -9 10 86.39 22.40 -9 9 -10 19.50 16.40 9 -9 10 -0.60 17.70 9 -9 10 5.80 15.10 -10 9 -10 -3.90 18.30 10 -9 10 16.80 17.50 10 -9 10 2.80 16.40 -11 9 -10 214.18 37.30 -11 9 -10 268.67 19.70 11 -9 10 251.07 37.20 11 -9 10 286.97 47.30 -12 9 -10 55.49 23.00 12 -9 10 62.99 25.00 12 -9 10 63.79 22.50 -13 9 -10 56.99 24.60 13 -9 10 71.59 22.70 13 -9 10 155.78 55.79 14 8 -10 404.96 49.50 -14 -8 10 274.97 40.00 -13 -8 10 -7.90 16.00 -13 -8 10 -1.60 24.40 12 8 -10 -7.70 15.00 -12 -8 10 7.70 9.40 -12 -8 10 -9.40 18.40 -12 -8 10 3.90 19.60 11 8 -10 204.98 34.40 -11 -8 10 194.28 42.10 -11 -8 10 147.59 32.40 10 8 -10 5.40 11.50 -10 -8 10 -0.90 12.40 -10 -8 10 11.10 12.10 -10 -8 10 -6.00 14.90 9 8 -10 396.96 36.90 -9 -8 10 337.87 39.80 -9 -8 10 289.07 34.70 -9 -8 10 337.97 26.60 8 8 -10 446.66 38.40 -8 -8 10 469.75 29.30 -8 -8 10 527.85 39.60 -8 -8 10 509.05 40.90 7 8 -10 343.37 32.00 -7 -8 10 299.67 31.40 -7 -8 10 317.77 25.60 -7 -8 10 316.47 34.80 6 8 -10 442.56 36.70 -6 -8 10 461.85 35.80 -6 -8 10 415.06 33.30 -6 -8 10 481.55 30.60 -5 -8 10 -7.60 9.30 -5 -8 10 7.20 10.60 -5 -8 10 -1.50 12.30 4 8 -10 134.59 24.00 -4 -8 10 105.59 21.40 -4 -8 10 136.39 19.20 -4 -8 10 99.29 23.50 3 8 -10 22.90 9.60 -3 -8 10 14.50 10.80 -3 -8 10 0.70 8.30 -3 -8 10 -9.00 10.10 2 8 -10 -11.80 9.20 2 8 -10 -11.40 7.50 -2 -8 10 1.40 10.40 -2 -8 10 -17.90 8.60 -2 -8 10 5.60 8.70 1 8 -10 4.20 9.30 1 8 -10 -2.10 10.20 -1 -8 10 6.30 8.30 -1 -8 10 -0.70 9.10 -1 -8 10 4.30 9.90 0 8 -10 290.47 29.30 0 8 -10 280.87 27.10 0 -8 10 295.77 22.50 0 -8 10 286.17 27.00 0 -8 10 288.67 29.50 -1 8 -10 416.46 31.70 1 -8 10 391.16 28.00 1 -8 10 387.56 32.00 1 -8 10 415.76 34.30 -2 8 -10 599.24 38.20 2 -8 10 598.54 37.90 2 -8 10 626.24 30.50 2 -8 10 613.74 43.40 -3 8 -10 30.20 12.10 3 -8 10 19.70 13.00 3 -8 10 14.80 13.80 3 -8 10 19.20 9.00 -4 8 -10 510.65 37.50 4 -8 10 558.14 37.80 4 -8 10 495.85 41.40 4 -8 10 563.64 27.60 -5 8 -10 207.18 29.00 5 -8 10 195.28 18.50 5 -8 10 246.38 27.60 5 -8 10 200.78 32.50 -6 8 -10 5.70 13.60 6 -8 10 -3.10 7.60 6 -8 10 3.90 15.00 -7 8 -10 384.76 37.80 7 -8 10 432.96 22.30 7 -8 10 387.56 34.50 -8 8 -10 -0.80 14.50 8 -8 10 12.70 15.40 8 -8 10 -3.50 13.00 -9 8 -10 94.09 29.40 9 -8 10 166.08 35.80 9 -8 10 126.89 28.00 -10 8 -10 621.54 23.60 -10 8 -10 696.63 51.49 10 -8 10 628.04 43.80 10 -8 10 764.92 57.19 -11 8 -10 21.70 18.50 11 -8 10 12.50 17.10 11 -8 10 -4.30 19.40 -12 8 -10 144.99 35.20 12 -8 10 140.59 33.40 12 -8 10 199.28 48.60 -13 8 -10 9.10 19.10 13 -8 10 -23.00 22.00 13 -8 10 5.00 18.90 -14 -7 10 232.58 59.99 13 7 -10 7.50 18.10 -13 -7 10 16.20 22.70 -13 -7 10 -4.80 18.00 12 7 -10 103.49 35.50 -12 -7 10 51.29 23.50 -12 -7 10 77.09 23.30 -12 -7 10 105.69 16.10 11 7 -10 36.80 15.00 -11 -7 10 12.60 16.50 -11 -7 10 36.80 20.30 10 7 -10 76.69 26.50 -10 -7 10 89.09 25.20 -10 -7 10 78.89 14.20 -10 -7 10 66.69 19.10 9 7 -10 23.40 12.10 -9 -7 10 16.10 12.90 -9 -7 10 9.20 14.10 8 7 -10 109.59 24.30 -8 -7 10 106.39 29.00 -8 -7 10 73.79 18.90 -8 -7 10 74.99 23.10 7 7 -10 68.09 20.90 -7 -7 10 76.49 18.10 -7 -7 10 52.09 14.60 -7 -7 10 80.79 21.30 6 7 -10 3.80 7.90 -6 -7 10 16.60 11.10 -6 -7 10 11.10 12.30 -6 -7 10 8.50 10.20 5 7 -10 387.86 33.20 -5 -7 10 400.96 31.00 -5 -7 10 397.06 32.20 -5 -7 10 396.46 28.10 4 7 -10 572.64 38.40 -4 -7 10 563.24 36.50 -4 -7 10 542.35 31.60 -4 -7 10 541.95 34.70 3 7 -10 267.87 26.90 -3 -7 10 249.08 24.00 -3 -7 10 264.57 25.50 -3 -7 10 235.68 22.80 2 7 -10 274.17 25.00 2 7 -10 269.67 28.60 -2 -7 10 301.37 25.30 -2 -7 10 276.77 26.80 -2 -7 10 295.47 24.40 1 7 -10 229.88 25.10 1 7 -10 217.88 23.10 -1 -7 10 235.08 21.00 -1 -7 10 228.28 25.80 -1 -7 10 256.37 24.40 0 7 -10 287.27 28.60 0 7 -10 236.38 24.40 0 -7 10 220.08 26.60 0 -7 10 248.08 21.20 0 -7 10 243.38 25.80 -1 7 -10 185.68 23.90 1 -7 10 186.78 18.60 1 -7 10 233.88 26.70 1 -7 10 184.48 23.90 -2 7 -10 -1.90 10.30 2 -7 10 -0.60 9.40 2 -7 10 18.00 11.60 2 -7 10 3.30 6.80 -3 7 -10 63.99 20.60 3 -7 10 91.69 24.10 3 -7 10 38.40 9.60 3 -7 10 38.20 13.80 -4 7 -10 152.78 25.00 4 -7 10 161.78 27.80 4 -7 10 178.18 16.80 4 -7 10 161.48 23.20 -5 7 -10 -10.30 10.00 5 -7 10 2.30 10.60 5 -7 10 0.30 12.30 5 -7 10 -12.80 6.90 -6 7 -10 648.74 43.00 6 -7 10 610.14 39.80 6 -7 10 675.93 25.40 -7 7 -10 114.39 27.40 7 -7 10 87.19 23.30 -8 7 -10 373.96 38.10 8 -7 10 298.67 41.30 8 -7 10 377.26 32.00 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46.80 15.60 5 -6 10 60.69 11.70 5 -6 10 68.29 20.40 -6 6 -10 28.20 14.20 6 -6 10 40.10 11.10 6 -6 10 18.80 12.40 -7 6 -10 20.60 15.10 7 -6 10 10.30 14.60 -8 6 -10 37.10 18.40 8 -6 10 6.50 13.70 8 -6 10 -20.00 12.60 -9 6 -10 329.17 37.40 9 -6 10 302.87 32.50 9 -6 10 359.86 42.60 -10 6 -10 141.19 29.70 10 -6 10 115.49 28.20 -11 6 -10 32.00 18.90 11 -6 10 132.09 36.60 11 -6 10 83.49 27.30 -12 6 -10 330.97 39.30 12 -6 10 474.45 52.89 12 -6 10 327.27 35.70 -13 6 -10 3.70 19.10 13 -6 10 -19.40 16.40 13 -6 10 1.10 23.70 -14 6 -10 148.29 37.50 14 -6 10 138.19 33.10 -14 -5 10 26.20 20.10 -14 -5 10 18.30 19.70 -14 -5 10 42.90 27.50 13 5 -10 29.30 16.60 -13 -5 10 3.30 16.10 -13 -5 10 -0.90 14.40 -13 -5 10 3.70 20.30 -12 -5 10 46.30 23.90 -12 -5 10 34.40 16.80 -12 -5 10 32.40 10.90 -12 -5 10 23.80 15.80 11 5 -10 17.80 11.70 -11 -5 10 18.30 18.10 -11 -5 10 42.40 13.20 -11 -5 10 5.30 14.30 10 5 -10 19.80 11.40 -10 -5 10 33.20 11.10 -10 -5 10 27.40 19.00 -10 -5 10 26.80 14.70 9 5 -10 17.00 10.80 -9 -5 10 46.80 12.30 -9 -5 10 46.80 15.60 8 5 -10 343.27 31.30 -8 -5 10 311.07 23.10 -8 -5 10 306.57 29.70 -8 -5 10 358.36 35.20 7 5 -10 177.98 24.50 -7 -5 10 130.39 23.60 -7 -5 10 114.49 25.60 -7 -5 10 167.28 19.60 6 5 -10 379.26 30.30 -6 -5 10 377.46 26.00 -6 -5 10 352.96 31.10 -6 -5 10 338.77 27.80 5 5 -10 64.69 18.70 -5 -5 10 47.80 12.50 -5 -5 10 61.59 20.70 -5 -5 10 69.69 17.70 4 5 -10 54.19 17.50 -4 -5 10 85.69 17.10 -4 -5 10 63.29 14.40 -4 -5 10 57.59 19.60 3 5 -10 1079.89 51.09 -3 -5 10 1105.59 45.20 -3 -5 10 1122.19 46.30 -3 -5 10 1089.69 48.80 2 5 -10 1058.09 43.40 2 5 -10 1092.79 49.99 -2 -5 10 1049.09 44.80 -2 -5 10 1047.40 47.50 1 5 -10 95.19 15.10 1 5 -10 100.79 18.80 -1 -5 10 95.29 15.30 -1 -5 10 88.49 16.60 -1 -5 10 83.09 17.70 0 5 -10 743.73 36.40 0 5 -10 713.23 41.00 0 -5 10 801.62 33.10 0 -5 10 742.23 40.10 0 -5 10 825.92 40.40 -1 5 -10 249.97 23.10 1 -5 10 242.28 25.70 1 -5 10 265.07 19.10 1 -5 10 292.97 24.50 -2 5 -10 24.10 10.10 2 -5 10 14.00 10.60 2 -5 10 20.50 6.90 2 -5 10 24.10 11.80 -3 5 -10 244.88 26.20 3 -5 10 284.87 25.50 3 -5 10 263.87 28.40 3 -5 10 311.27 17.60 -4 5 -10 -7.10 8.60 4 -5 10 -3.50 10.50 4 -5 10 5.70 5.80 4 -5 10 2.70 9.90 -5 5 -10 50.39 15.60 5 -5 10 68.29 18.90 5 -5 10 64.29 10.10 -6 5 -10 802.12 45.60 6 -5 10 877.31 23.90 6 -5 10 840.02 45.90 -7 5 -10 15.90 13.50 7 -5 10 22.50 13.60 -8 5 -10 241.98 30.30 8 -5 10 217.78 25.40 8 -5 10 184.88 31.10 -9 5 -10 190.68 30.70 9 -5 10 216.88 26.70 9 -5 10 288.37 37.90 -10 5 -10 414.66 41.80 10 -5 10 400.66 32.50 10 -5 10 450.25 43.60 -11 5 -10 -1.30 15.40 11 -5 10 -9.40 14.80 11 -5 10 1.80 15.20 -12 5 -10 126.99 30.70 12 -5 10 82.99 26.80 12 -5 10 123.99 39.00 -13 5 -10 118.89 34.20 13 -5 10 113.79 30.00 13 -5 10 164.78 47.20 -14 5 -10 69.39 24.70 14 -5 10 95.89 23.60 15 4 -10 33.20 22.60 -15 -4 10 -25.90 31.20 -15 -4 10 4.00 20.30 14 4 -10 151.38 41.70 -14 -4 10 155.38 32.40 -14 -4 10 128.69 35.80 -13 -4 10 184.38 18.00 -13 -4 10 163.28 51.19 -13 -4 10 241.98 36.10 -13 -4 10 233.98 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4 -10 60.19 21.50 13 -4 10 130.29 42.30 13 -4 10 70.09 20.00 -14 4 -10 -18.80 21.10 14 -4 10 21.90 19.30 14 -4 10 13.60 19.00 15 3 -10 78.49 22.30 -15 -3 10 29.60 39.20 -15 -3 10 67.59 23.70 -15 -3 10 43.60 23.40 14 3 -10 8.90 19.60 -14 -3 10 -18.20 16.50 -14 -3 10 33.40 27.70 -14 -3 10 12.80 18.10 13 3 -10 177.08 38.00 -13 -3 10 139.09 31.10 -13 -3 10 153.98 18.20 -13 -3 10 164.58 30.40 12 3 -10 107.39 34.00 -12 -3 10 37.60 20.30 -12 -3 10 56.39 18.30 -12 -3 10 64.99 19.80 -12 -3 10 67.89 22.70 -11 -3 10 24.60 11.40 -11 -3 10 9.30 17.90 -11 -3 10 47.50 16.90 -11 -3 10 12.70 13.60 10 3 -10 272.77 31.10 -10 -3 10 212.68 21.20 -10 -3 10 197.88 25.50 -10 -3 10 223.48 28.10 9 3 -10 14.20 10.30 -9 -3 10 23.00 13.30 -9 -3 10 69.99 15.40 -9 -3 10 34.70 15.00 8 3 -10 5.50 8.50 -8 -3 10 4.70 9.20 -8 -3 10 9.40 10.60 7 3 -10 98.99 21.10 -7 -3 10 53.89 16.10 -7 -3 10 99.49 20.90 -7 -3 10 89.99 16.40 6 3 -10 17.30 8.70 -6 -3 10 9.60 9.40 -6 -3 10 18.90 11.40 -6 -3 10 18.60 11.20 5 3 -10 72.99 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19.00 -8 3 -10 396.06 35.00 8 -3 10 358.56 31.60 -9 3 -10 50.49 18.60 9 -3 10 41.50 16.20 9 -3 10 62.59 20.60 -10 3 -10 95.89 27.10 10 -3 10 36.40 15.60 10 -3 10 59.29 17.50 -11 3 -10 38.80 21.30 11 -3 10 105.69 33.60 11 -3 10 58.79 19.00 -12 3 -10 -5.90 18.00 12 -3 10 12.60 15.20 12 -3 10 19.80 15.70 -13 3 -10 50.69 24.50 13 -3 10 108.29 27.70 13 -3 10 53.99 17.50 -14 3 -10 82.79 23.10 14 -3 10 120.29 27.60 -15 3 -10 6.50 21.40 15 -3 10 7.80 23.80 15 2 -10 80.89 23.20 -15 -2 10 121.79 34.90 -15 -2 10 246.98 70.99 -15 -2 10 117.49 32.70 14 2 -10 19.20 19.60 -14 -2 10 24.90 11.40 -14 -2 10 9.70 18.20 -14 -2 10 32.80 18.50 -14 -2 10 166.18 57.09 13 2 -10 -17.90 14.70 -13 -2 10 -12.80 13.70 -13 -2 10 5.30 14.50 -13 -2 10 -2.00 21.90 12 2 -10 936.01 59.09 -12 -2 10 981.60 56.59 -12 -2 10 1056.99 51.39 -12 -2 10 872.41 66.19 -12 -2 10 975.30 38.60 -11 -2 10 118.99 25.60 -11 -2 10 117.09 26.80 -11 -2 10 93.79 22.90 10 2 -10 193.98 28.30 -10 -2 10 60.89 17.50 -10 -2 10 137.69 34.60 -10 -2 10 109.79 22.50 9 2 -10 4.60 9.40 -9 -2 10 14.90 12.60 -9 -2 10 9.60 13.40 8 2 -10 173.08 24.10 -8 -2 10 206.58 24.60 -8 -2 10 151.88 29.90 7 2 -10 16.30 9.10 -7 -2 10 29.60 12.50 -7 -2 10 24.80 11.40 6 2 -10 285.77 26.60 -6 -2 10 295.97 29.50 -6 -2 10 361.86 28.20 5 2 -10 155.28 18.90 -5 -2 10 103.19 20.80 -5 -2 10 114.49 17.80 4 2 -10 132.59 19.30 -4 -2 10 124.59 16.70 -4 -2 10 126.99 19.90 3 2 -10 3.20 6.40 3 2 -10 0.30 5.90 -3 -2 10 1.50 6.00 2 2 -10 92.79 16.50 2 2 -10 124.29 13.90 -2 -2 10 141.09 17.70 -2 -2 10 100.59 15.20 1 2 -10 957.30 36.10 -1 -2 10 920.91 35.10 -1 -2 10 894.61 41.20 0 2 -10 675.73 30.50 0 2 -10 675.13 36.30 0 -2 10 670.63 27.50 0 -2 10 621.74 34.50 0 -2 10 675.33 33.90 1 -2 10 347.77 24.30 1 -2 10 341.57 26.50 1 -2 10 355.36 19.10 -2 2 -10 931.31 39.20 2 -2 10 969.50 42.50 2 -2 10 910.91 43.50 2 -2 10 910.81 30.00 -3 2 -10 4.90 9.10 3 -2 10 8.90 8.40 3 -2 10 33.20 8.80 3 -2 10 15.40 10.80 -4 2 -10 163.88 19.80 4 -2 10 117.19 9.00 4 -2 10 145.69 19.40 -5 2 -10 13.30 11.50 5 -2 10 24.80 12.20 -6 2 -10 315.27 28.60 6 -2 10 298.07 26.10 -7 2 -10 15.60 13.10 7 -2 10 26.50 12.80 -8 2 -10 601.24 40.30 8 -2 10 606.04 35.60 -9 2 -10 18.40 13.60 9 -2 10 1.70 11.90 9 -2 10 10.80 12.50 -10 2 -10 5.90 14.70 10 -2 10 8.80 11.50 10 -2 10 11.50 12.70 -11 2 -10 92.99 30.30 11 -2 10 116.59 25.10 11 -2 10 111.79 32.90 -12 2 -10 84.39 25.10 12 -2 10 120.69 27.30 12 -2 10 145.99 34.40 -13 2 -10 -15.00 16.80 13 -2 10 31.70 22.80 -14 2 -10 25.90 22.40 14 -2 10 1.10 18.60 14 -2 10 20.00 17.70 -15 2 -10 -16.90 22.50 15 -2 10 6.10 19.20 15 -2 10 -14.30 20.40 15 1 -10 91.69 23.90 -15 -1 10 265.27 69.49 14 1 -10 343.47 44.40 -14 -1 10 229.28 33.00 -14 -1 10 320.47 60.89 -14 -1 10 252.87 36.90 13 1 -10 33.90 16.20 -13 -1 10 15.90 15.40 -13 -1 10 156.48 48.70 -13 -1 10 11.20 14.70 12 1 -10 11.80 15.50 -12 -1 10 -2.50 13.30 -12 -1 10 8.20 14.20 -12 -1 10 -7.10 18.50 11 1 -10 97.29 30.00 -11 -1 10 160.08 24.90 -11 -1 10 137.79 27.00 -11 -1 10 80.39 27.80 10 1 -10 211.28 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7 -13 119.19 33.60 -9 -7 13 104.99 28.80 -9 -7 13 75.59 17.60 -9 -7 13 163.98 40.00 8 7 -13 13.10 13.70 -8 -7 13 -12.20 15.20 -8 -7 13 -21.90 12.50 -8 -7 13 -13.70 13.50 7 7 -13 33.50 13.10 -7 -7 13 27.60 17.00 -7 -7 13 38.70 19.30 -7 -7 13 90.89 22.80 -6 -7 13 35.70 17.80 -6 -7 13 76.69 22.30 -6 -7 13 42.30 15.20 5 7 -13 1.90 11.40 -5 -7 13 -8.40 11.30 -5 -7 13 18.60 12.90 -5 -7 13 8.40 11.90 4 7 -13 23.00 12.10 4 7 -13 11.20 10.10 -4 -7 13 15.80 12.50 -4 -7 13 8.00 13.10 -4 -7 13 0.70 11.10 3 7 -13 156.68 25.30 3 7 -13 185.88 28.80 -3 -7 13 140.59 26.40 -3 -7 13 200.28 25.70 -3 -7 13 177.08 23.90 2 7 -13 4.70 9.50 2 7 -13 25.90 11.10 -2 -7 13 -6.60 12.10 -2 -7 13 15.30 11.60 -2 -7 13 5.00 10.60 1 7 -13 6.90 12.20 1 7 -13 -2.30 9.50 -1 -7 13 18.20 9.80 -1 -7 13 10.50 11.40 -1 -7 13 22.50 14.00 0 7 -13 133.49 23.80 0 7 -13 203.98 27.80 0 -7 13 156.08 20.60 0 -7 13 120.79 24.30 0 -7 13 100.79 26.80 -1 7 -13 10.70 11.20 1 -7 13 -3.80 10.60 1 -7 13 6.60 12.00 1 -7 13 11.00 9.20 -2 7 -13 259.77 29.10 2 -7 13 222.28 21.20 2 -7 13 191.58 29.40 2 -7 13 235.58 28.10 -3 7 -13 52.39 16.00 3 -7 13 79.39 17.40 3 -7 13 55.79 19.30 3 -7 13 51.29 18.70 -4 7 -13 41.30 16.70 4 -7 13 31.20 16.30 4 -7 13 41.00 15.80 4 -7 13 43.50 11.10 -5 7 -13 423.26 38.10 5 -7 13 419.06 38.30 5 -7 13 379.66 23.10 5 -7 13 455.75 46.40 -6 7 -13 259.37 32.70 6 -7 13 256.97 17.60 6 -7 13 258.17 32.90 6 -7 13 234.28 38.00 -7 7 -13 64.99 21.10 7 -7 13 36.50 18.30 7 -7 13 28.80 17.80 -8 7 -13 -9.10 16.80 8 -7 13 14.30 16.70 -9 7 -13 22.50 18.30 9 -7 13 22.60 17.70 9 -7 13 2.30 18.60 -10 7 -13 0.80 19.30 10 -7 13 2.60 18.10 10 -7 13 -7.50 19.70 -11 7 -13 3.40 21.60 11 -7 13 57.59 22.70 11 -7 13 159.58 49.20 -12 7 -13 -7.20 20.40 12 -7 13 48.60 37.00 12 -7 13 -17.90 20.10 13 6 -13 34.60 19.50 -13 -6 13 -15.60 21.10 -13 -6 13 24.70 30.30 -13 -6 13 5.60 16.20 12 6 -13 -4.50 18.10 -12 -6 13 -9.50 15.20 -12 -6 13 -17.40 25.50 11 6 -13 17.00 15.40 -11 -6 13 0.50 15.40 -11 -6 13 39.30 15.80 -11 -6 13 30.90 21.10 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7 -14 900.31 48.30 3 7 -14 950.20 57.29 -3 -7 14 994.10 48.10 -3 -7 14 1010.60 55.39 -3 -7 14 952.60 51.09 2 7 -14 24.30 11.40 2 7 -14 5.70 12.60 -2 -7 14 15.90 14.10 -2 -7 14 12.30 11.40 -2 -7 14 -3.50 13.50 1 7 -14 149.79 24.50 1 7 -14 159.38 29.50 -1 -7 14 181.18 23.70 -1 -7 14 201.28 27.30 -1 -7 14 163.08 30.40 0 7 -14 30.70 13.10 0 -7 14 6.40 10.50 0 -7 14 27.00 13.40 0 -7 14 13.60 15.50 -1 7 -14 553.54 38.60 1 -7 14 531.65 40.70 1 -7 14 531.85 43.00 1 -7 14 508.35 31.60 -2 7 -14 746.13 45.00 2 -7 14 749.92 50.79 2 -7 14 708.43 47.00 -3 7 -14 11.40 14.30 3 -7 14 -13.80 12.00 3 -7 14 4.70 9.50 3 -7 14 3.60 15.20 -4 7 -14 -0.90 14.40 4 -7 14 4.30 15.50 4 -7 14 -10.40 13.80 4 -7 14 12.80 10.00 -5 7 -14 18.90 16.10 5 -7 14 -30.50 14.40 5 -7 14 -14.00 12.50 5 -7 14 -16.00 9.60 -6 7 -14 13.30 16.40 6 -7 14 8.00 17.60 6 -7 14 8.00 8.30 6 -7 14 -5.30 14.90 -7 7 -14 83.99 25.00 7 -7 14 83.79 23.90 7 -7 14 167.58 40.70 -8 7 -14 17.70 17.10 8 -7 14 8.10 19.40 8 -7 14 25.40 18.50 -9 7 -14 314.87 41.80 9 -7 14 334.67 47.00 9 -7 14 350.56 37.50 -10 7 -14 508.75 49.90 10 -7 14 529.35 49.30 10 -7 14 426.56 56.29 -11 7 -14 39.10 20.90 11 -7 14 159.88 54.79 11 -7 14 53.69 22.60 -12 7 -14 -3.40 21.00 12 -7 14 6.30 21.40 12 -7 14 34.40 24.70 12 6 -14 9.90 18.60 -12 -6 14 -12.60 16.30 -12 -6 14 -0.90 18.60 -12 -6 14 9.80 27.50 11 6 -14 -5.00 18.30 -11 -6 14 8.20 17.20 -11 -6 14 -5.90 23.90 -11 -6 14 -17.00 15.60 10 6 -14 455.15 44.30 -10 -6 14 414.66 34.40 -10 -6 14 308.07 40.70 -10 -6 14 379.36 51.79 9 6 -14 111.09 31.70 -9 -6 14 124.79 37.90 8 6 -14 176.08 31.90 -8 -6 14 91.79 26.30 -8 -6 14 99.79 24.10 -8 -6 14 116.99 24.40 7 6 -14 -3.20 14.60 -7 -6 14 1.40 12.30 -7 -6 14 13.20 13.50 -7 -6 14 32.30 20.40 6 6 -14 201.08 31.10 -6 -6 14 142.99 25.70 -6 -6 14 165.48 30.00 -6 -6 14 119.89 25.70 5 6 -14 4.10 11.00 -5 -6 14 3.20 12.30 -5 -6 14 -21.10 13.90 -5 -6 14 -17.00 13.50 4 6 -14 42.60 15.40 4 6 -14 4.50 11.40 -4 -6 14 6.60 13.80 -4 -6 14 11.60 13.90 -4 -6 14 35.60 13.80 3 6 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4 -15 266.37 31.10 0 -4 15 220.18 22.10 0 -4 15 238.88 28.80 0 -4 15 235.78 33.00 -1 4 -15 468.45 34.20 1 -4 15 544.45 40.50 1 -4 15 499.35 41.50 -2 4 -15 -2.30 13.80 2 -4 15 14.30 14.10 2 -4 15 66.59 17.40 2 -4 15 26.40 12.70 -3 4 -15 18.20 12.90 3 -4 15 -1.70 9.10 3 -4 15 -16.80 10.90 3 -4 15 -3.10 13.00 -4 4 -15 13.90 14.70 4 -4 15 18.30 8.60 4 -4 15 -1.60 12.40 4 -4 15 16.00 14.10 -5 4 -15 218.38 30.80 5 -4 15 209.98 34.10 5 -4 15 214.18 31.00 5 -4 15 166.98 16.20 -6 4 -15 -7.10 14.20 6 -4 15 1.00 13.70 6 -4 15 -14.50 16.40 -7 4 -15 165.28 32.40 7 -4 15 188.88 37.90 7 -4 15 201.98 30.70 -8 4 -15 -6.70 14.40 8 -4 15 6.00 16.30 8 -4 15 10.00 15.50 -9 4 -15 128.79 34.10 9 -4 15 57.99 22.40 -10 4 -15 7.80 18.20 10 -4 15 4.80 19.50 10 -4 15 -30.50 18.50 -11 4 -15 117.99 37.50 11 -4 15 151.28 50.99 11 -4 15 146.49 30.00 -12 4 -15 12.80 19.90 12 -4 15 3.40 22.20 12 -4 15 11.40 19.20 12 3 -15 150.08 42.00 -12 -3 15 52.89 20.60 -12 -3 15 110.09 29.90 -12 -3 15 83.59 30.60 11 3 -15 241.28 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119.69 37.60 -3 -3 -22 -0.70 19.60 3 3 22 16.10 14.40 -4 -3 -22 3.90 19.70 4 3 22 32.20 17.70 4 3 22 36.90 20.00 4 3 22 -17.20 14.40 -5 -3 -22 24.30 21.10 5 3 22 29.70 17.80 5 3 22 37.70 23.00 5 -4 -22 18.30 20.50 -5 4 22 38.40 23.90 -5 4 22 35.60 19.90 4 -4 -22 -7.60 18.40 -4 4 22 16.50 17.50 -4 4 22 14.40 19.90 3 -4 -22 14.00 17.20 -3 4 22 -6.40 18.40 -3 4 22 5.40 16.60 -2 4 22 220.28 44.40 -2 4 22 284.67 35.80 -1 4 22 0.50 16.40 -1 4 22 3.00 17.00 0 -4 -22 -29.70 16.20 0 4 22 -17.20 16.80 0 4 22 -21.30 15.00 -1 -4 -22 26.60 18.00 1 4 22 36.10 17.70 1 4 22 7.20 16.80 -2 -4 -22 157.98 32.50 2 4 22 108.79 33.60 -3 -4 -22 41.70 19.40 3 4 22 41.90 17.70 3 4 22 30.20 16.40 -4 -4 -22 222.38 36.80 4 4 22 191.78 37.70 4 4 22 170.18 29.50 -5 -4 -22 17.10 21.50 5 4 22 5.80 16.20 5 4 22 4.20 16.60 5 4 22 -17.20 20.20 5 -5 -22 13.40 20.70 -5 5 22 -23.40 17.20 -5 5 22 -7.10 22.20 4 -5 -22 13.60 18.50 -4 5 22 113.49 33.20 -4 5 22 19.90 21.20 3 -5 -22 25.00 17.40 -3 5 22 -2.10 19.20 -3 5 22 -2.90 17.90 -2 5 22 39.70 18.80 1 -5 -22 -7.10 13.80 -1 5 22 -18.30 16.30 -1 5 22 16.70 17.00 0 -5 -22 10.90 16.10 0 5 22 10.20 16.20 -1 -5 -22 -14.80 16.70 1 5 22 -8.20 15.40 1 5 22 15.40 16.40 -2 -5 -22 155.28 32.70 2 5 22 120.09 27.50 2 5 22 170.78 34.60 -3 -5 -22 -21.40 19.60 3 5 22 -5.40 13.40 3 5 22 6.70 15.40 -4 -5 -22 276.07 37.40 4 5 22 305.37 39.90 4 5 22 273.57 32.70 5 5 22 131.29 34.80 4 -6 -22 55.89 20.70 -4 6 22 75.49 23.40 -4 6 22 134.99 34.20 -3 6 22 -12.90 19.60 -3 6 22 -18.90 17.70 -2 6 22 -18.90 14.70 -2 6 22 -8.90 17.80 -1 6 22 30.90 19.10 0 6 22 340.97 39.40 0 6 22 298.57 36.50 -1 -6 -22 -6.50 16.10 1 6 22 30.50 15.90 1 6 22 8.50 15.10 -2 -6 -22 62.89 19.30 2 6 22 56.49 17.50 2 6 22 47.30 16.20 -3 -6 -22 -23.70 18.70 3 6 22 0.50 14.10 3 6 22 -8.00 14.80 -4 -6 -22 77.09 23.30 4 6 22 92.89 32.70 4 6 22 132.59 29.60 -3 7 22 94.19 23.40 -3 7 22 154.88 31.60 -2 7 22 57.49 20.80 -1 7 22 9.60 15.00 -1 7 22 -5.90 14.30 0 -7 -22 210.48 32.00 0 7 22 265.97 38.30 0 7 22 231.78 33.30 -1 -7 -22 -6.80 16.40 1 7 22 -12.50 15.10 1 7 22 4.70 14.80 -2 -7 -22 39.90 19.20 2 7 22 14.90 16.00 2 7 22 20.20 14.80 -3 -7 -22 66.89 22.70 3 7 22 92.49 32.10 3 7 22 47.90 17.00 -2 8 22 300.97 37.60 -2 8 22 323.87 45.10 -1 8 22 -18.20 17.60 -1 8 22 9.30 15.90 0 8 22 -5.70 14.50 0 8 22 22.90 16.60 -1 -8 -22 -7.20 16.80 1 8 22 11.20 14.50 1 8 22 19.90 16.90 2 5 -23 28.80 21.90 -2 -5 23 43.80 19.40 -2 -5 23 -45.20 25.40 1 5 -23 184.68 37.20 -1 -5 23 173.08 34.20 -1 -5 23 107.29 30.30 0 -5 23 10.80 25.30 0 -5 23 33.10 17.00 0 -5 23 10.60 21.00 -1 5 -23 58.39 22.80 1 -5 23 50.59 21.30 1 -5 23 65.49 18.90 1 -5 23 19.50 28.80 3 4 -23 39.10 22.70 3 4 -23 17.80 21.50 -3 -4 23 25.60 19.30 -3 -4 23 14.80 28.00 -3 -4 23 39.40 26.80 2 4 -23 21.20 19.60 -2 -4 23 -11.30 25.70 -2 -4 23 -8.60 16.60 1 4 -23 -22.20 20.20 -1 -4 23 -11.60 16.80 -1 -4 23 30.80 27.40 0 4 -23 26.90 23.90 0 -4 23 42.80 18.40 0 -4 23 7.50 24.10 -1 4 -23 104.89 32.80 1 -4 23 21.00 17.30 1 -4 23 32.60 25.00 -2 4 -23 -4.20 18.80 2 -4 23 17.20 23.80 2 -4 23 30.10 20.80 2 -4 23 -5.40 16.10 3 3 -23 16.50 19.50 -3 -3 23 18.10 16.40 -3 -3 23 4.80 20.30 -3 -3 23 24.40 26.00 2 3 -23 35.60 22.00 -2 -3 23 2.00 20.20 -2 -3 23 -1.00 26.70 -2 -3 23 8.90 16.90 1 3 -23 131.89 33.10 -1 -3 23 210.68 33.50 -1 -3 23 128.89 38.50 0 3 -23 74.29 21.60 0 -3 23 47.30 24.50 0 -3 23 97.89 29.40 -1 3 -23 29.60 21.70 1 -3 23 8.10 25.10 1 -3 23 18.70 15.90 2 -3 23 94.49 31.50 2 -3 23 83.19 26.40 2 -3 23 123.79 29.90 -3 3 -23 -13.70 18.80 3 -3 23 39.80 21.00 3 -3 23 7.70 17.00 3 -3 23 -43.20 23.00 4 2 -23 12.50 37.40 4 2 -23 -15.10 20.40 -4 -2 23 6.40 16.70 -4 -2 23 -43.50 25.80 -4 -2 23 -29.20 18.70 3 2 -23 3.30 25.00 3 2 -23 43.60 20.40 -3 -2 23 131.19 33.50 -3 -2 23 30.00 19.90 -3 -2 23 75.39 28.80 2 2 -23 2.90 18.10 -2 -2 23 -36.50 24.30 -2 -2 23 7.90 17.50 -2 -2 23 15.40 19.20 1 2 -23 111.69 32.40 -1 -2 23 95.49 28.70 -1 -2 23 76.89 33.10 0 2 -23 118.59 33.40 0 -2 23 56.39 25.20 0 -2 23 59.59 18.00 0 -2 23 73.09 28.30 -1 2 -23 32.00 20.00 1 -2 23 38.70 16.90 1 -2 23 30.10 22.20 -2 2 -23 42.70 20.70 2 -2 23 0.50 21.20 2 -2 23 21.30 17.60 -3 2 -23 18.80 21.30 3 -2 23 42.70 27.10 3 -2 23 58.49 24.40 3 -2 23 103.19 28.40 4 1 -23 -12.20 22.40 4 1 -23 15.90 18.20 -4 -1 23 2.00 19.60 -4 -1 23 -16.60 15.60 -4 -1 23 -35.00 24.80 3 1 -23 15.80 18.30 -3 -1 23 9.80 24.40 -3 -1 23 15.00 16.50 -3 -1 23 33.20 20.40 2 1 -23 26.40 18.80 -2 -1 23 15.10 23.10 -2 -1 23 28.80 20.30 -2 -1 23 41.20 20.10 1 1 -23 115.59 31.70 -1 -1 23 48.10 20.30 -1 -1 23 14.00 24.50 -1 -1 23 80.49 25.20 0 1 -23 180.38 32.10 0 -1 23 153.28 41.90 0 -1 23 170.68 30.40 0 -1 23 183.58 49.99 -1 1 -23 46.30 19.80 1 -1 23 29.80 21.20 1 -1 23 90.39 26.80 -2 1 -23 -22.90 19.70 2 -1 23 -4.80 23.00 2 -1 23 12.10 16.20 -3 1 -23 20.20 17.70 3 -1 23 12.60 28.30 3 -1 23 35.50 24.50 3 -1 23 -7.10 15.30 -4 1 -23 63.29 22.40 4 -1 23 21.90 20.80 4 -1 23 52.79 25.10 4 -1 23 46.80 21.60 4 0 -23 0.60 16.30 4 0 -23 21.00 26.30 -4 0 23 -20.20 16.90 -4 0 23 -22.50 20.40 -4 0 23 -22.80 23.20 3 0 -23 178.78 49.90 3 0 -23 230.18 29.60 -3 0 23 155.28 51.69 -3 0 23 217.68 35.10 -3 0 23 204.28 42.30 2 0 -23 6.80 16.60 -2 0 23 6.70 18.00 -2 0 23 -12.90 17.60 -2 0 23 20.30 26.20 1 0 -23 8.30 17.60 -1 0 23 49.99 23.90 -1 0 23 0.90 17.00 -1 0 23 -12.30 20.90 0 0 -23 -20.90 17.20 0 0 23 15.00 23.70 0 0 23 -31.10 14.30 0 0 23 -11.70 22.00 -1 0 -23 3.10 17.10 1 0 23 39.60 20.50 1 0 23 26.60 28.30 1 0 23 36.80 17.90 -2 0 -23 16.80 18.90 2 0 23 -1.20 15.80 2 0 23 -6.30 21.60 -3 0 -23 118.79 34.40 3 0 23 215.28 30.40 3 0 23 197.78 50.09 -4 0 -23 17.90 20.20 4 0 23 -0.70 15.90 4 0 23 2.00 20.90 4 0 23 34.90 18.20 4 -1 -23 24.10 23.40 -4 1 23 -3.20 18.70 -4 1 23 23.90 26.40 3 -1 -23 -12.90 19.90 3 -1 -23 -0.70 16.70 -3 1 23 6.30 17.90 -3 1 23 -21.30 21.30 2 -1 -23 -0.50 16.60 -2 1 23 30.10 17.80 -2 1 23 -0.20 22.60 1 -1 -23 42.60 18.30 -1 1 23 10.90 19.90 -1 1 23 50.59 17.80 0 -1 -23 127.29 31.70 0 1 23 177.98 47.90 0 1 23 197.58 40.50 0 1 23 169.28 30.30 -1 -1 -23 66.49 21.40 1 1 23 43.70 17.20 1 1 23 27.10 21.20 -2 -1 -23 3.50 19.30 2 1 23 -2.80 20.90 2 1 23 -25.20 14.60 -3 -1 -23 -8.80 18.30 3 1 23 12.60 19.30 3 1 23 16.00 16.30 -4 -1 -23 39.40 23.00 4 1 23 36.20 16.20 4 -2 -23 -3.80 21.20 -4 2 23 -7.10 16.20 -4 2 23 -1.80 23.20 3 -2 -23 47.90 21.60 -3 2 23 -2.60 24.30 -3 2 23 9.30 17.60 2 -2 -23 6.40 16.60 -2 2 23 -16.20 19.80 -2 2 23 15.90 16.50 1 -2 -23 15.00 17.50 -1 2 23 102.49 28.80 -1 2 23 27.00 24.50 0 -2 -23 73.19 20.10 0 2 23 51.29 17.70 0 2 23 25.20 21.00 -1 -2 -23 38.90 19.90 1 2 23 49.99 17.40 1 2 23 44.10 21.80 -2 -2 -23 18.50 20.70 2 2 23 -7.10 17.30 2 2 23 33.30 17.80 -3 -2 -23 46.20 22.00 3 2 23 16.90 22.80 3 2 23 8.10 23.10 3 2 23 31.00 17.00 3 -3 -23 28.10 20.50 -3 3 23 26.20 17.80 -3 3 23 29.80 21.80 -2 3 23 27.30 17.50 -2 3 23 -31.60 19.60 1 -3 -23 50.29 17.90 -1 3 23 100.49 31.70 -1 3 23 70.29 23.20 0 3 23 97.29 28.00 0 3 23 54.59 22.70 -1 -3 -23 8.20 19.40 1 3 23 98.79 27.60 1 3 23 46.10 21.70 -2 -3 -23 148.29 33.60 2 3 23 165.08 42.90 2 3 23 108.39 27.20 -3 -3 -23 -6.20 20.30 3 3 23 -6.20 15.40 3 3 23 27.20 18.40 -3 4 23 26.20 18.30 -3 4 23 14.40 21.20 -2 4 23 -14.70 20.40 -2 4 23 11.90 16.80 -1 4 23 -13.60 18.10 -1 4 23 -3.90 16.90 0 -4 -23 -26.90 17.70 0 4 23 1.90 20.30 0 4 23 10.60 16.10 -1 -4 -23 23.00 19.80 1 4 23 -10.50 17.90 1 4 23 26.70 18.30 -2 -4 -23 12.60 21.50 2 4 23 2.40 16.90 2 4 23 27.80 16.50 -2 5 23 16.10 20.00 -2 5 23 10.30 20.60 -1 5 23 30.70 20.30 -1 5 23 77.19 22.50 0 -5 -23 25.90 17.20 0 5 23 48.20 19.00 0 5 23 20.30 32.90 -1 -5 -23 50.89 19.60 1 5 23 34.60 17.00 1 5 23 50.99 19.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 26144 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn Zn1 Zn 0.44116(3) 0.25382(2) 0.31262(2) 0.01551(10) Uani 1 1 d . Cu1 Cu 0.28516(3) 0.48696(2) 0.38548(2) 0.02181(12) Uani 1 1 d . N1 N 0.53922(19) 0.29426(14) 0.24448(14) 0.0164(6) Uani 1 1 d . N2 N 0.5560(2) 0.23634(15) 0.37706(14) 0.0172(6) Uani 1 1 d . N3 N 0.3690(2) 0.17324(15) 0.36475(14) 0.0184(6) Uani 1 1 d . N4 N 0.34755(19) 0.23692(14) 0.23398(14) 0.0159(6) Uani 1 1 d . N5 N 0.3800(2) 0.34750(16) 0.34530(15) 0.0197(7) Uani 1 1 d . N6 N 0.3866(2) 0.55463(15) 0.42851(14) 0.0175(6) Uani 1 1 d . N7 N 0.2206(2) 0.51949(16) 0.48562(15) 0.0220(7) Uani 1 1 d . N8 N 0.1684(2) 0.54207(16) 0.35412(16) 0.0226(7) Uani 1 1 d . C1 C 0.5173(2) 0.31788(18) 0.18148(17) 0.0186(8) Uani 1 1 d . C2 C 0.5972(2) 0.3553(2) 0.15406(18) 0.0221(8) Uani 1 1 d . H2 H 0.599982 0.377948 0.111480 0.026 Uiso 1 1 calc R C3 C 0.6676(3) 0.3523(2) 0.20010(18) 0.0224(8) Uani 1 1 d . H3 H 0.729774 0.371103 0.195629 0.027 Uiso 1 1 calc R C4 C 0.6303(2) 0.31500(18) 0.25746(17) 0.0175(7) Uani 1 1 d . C5 C 0.6799(2) 0.30427(18) 0.31803(17) 0.0177(8) Uani 1 1 d . C6 C 0.7776(2) 0.33473(19) 0.32424(17) 0.0192(8) Uani 1 1 d . C7 C 0.7939(2) 0.4080(2) 0.31338(17) 0.0209(8) Uani 1 1 d . H7 H 0.742775 0.438382 0.300235 0.025 Uiso 1 1 calc R C8 C 0.8839(3) 0.4372(2) 0.32154(18) 0.0265(9) Uani 1 1 d . H8 H 0.894015 0.487056 0.313510 0.032 Uiso 1 1 calc R C9 C 0.9589(3) 0.3939(2) 0.34130(19) 0.0297(9) Uani 1 1 d . H9 H 1.020264 0.414035 0.347486 0.036 Uiso 1 1 calc R C10 C 0.9441(3) 0.3217(2) 0.3519(2) 0.0298(9) Uani 1 1 d . H10 H 0.995530 0.291967 0.365616 0.036 Uiso 1 1 calc R C11 C 0.8545(3) 0.2916(2) 0.34283(19) 0.0263(9) Uani 1 1 d . H11 H 0.845689 0.241333 0.349339 0.032 Uiso 1 1 calc R C12 C 0.6439(2) 0.26797(18) 0.37383(17) 0.0179(8) Uani 1 1 d . C13 C 0.6925(3) 0.25854(19) 0.43723(18) 0.0230(8) Uani 1 1 d . H13 H 0.753880 0.275806 0.448669 0.028 Uiso 1 1 calc R C14 C 0.6344(3) 0.22075(19) 0.47696(19) 0.0246(8) Uani 1 1 d . H14 H 0.647515 0.206090 0.521644 0.029 Uiso 1 1 calc R C15 C 0.5493(2) 0.20663(19) 0.43973(18) 0.0193(8) Uani 1 1 d . C16 C 0.4739(3) 0.16573(18) 0.46401(17) 0.0201(8) Uani 1 1 d . C17 C 0.4854(3) 0.13766(19) 0.53397(18) 0.0216(8) Uani 1 1 d . C18 C 0.5410(3) 0.0773(2) 0.5471(2) 0.0325(10) Uani 1 1 d . H18 H 0.567659 0.051159 0.511026 0.039 Uiso 1 1 calc R C19 C 0.5580(3) 0.0548(2) 0.6122(2) 0.0389(11) Uani 1 1 d . H19 H 0.595685 0.013205 0.620329 0.047 Uiso 1 1 calc R C20 C 0.5205(3) 0.0924(2) 0.6652(2) 0.0339(10) Uani 1 1 d . H20 H 0.532636 0.077111 0.709816 0.041 Uiso 1 1 calc R C21 C 0.4653(3) 0.1525(2) 0.65295(19) 0.0285(9) Uani 1 1 d . H21 H 0.439059 0.178416 0.689298 0.034 Uiso 1 1 calc R C22 C 0.4479(3) 0.1752(2) 0.58768(18) 0.0243(8) Uani 1 1 d . H22 H 0.409996 0.216740 0.579769 0.029 Uiso 1 1 calc R C23 C 0.3908(2) 0.14942(18) 0.42827(17) 0.0178(8) Uani 1 1 d . C24 C 0.3147(3) 0.10499(19) 0.45272(17) 0.0208(8) Uani 1 1 d . H24 H 0.312165 0.081986 0.495136 0.025 Uiso 1 1 calc R C25 C 0.2478(3) 0.10220(19) 0.40423(18) 0.0218(8) Uani 1 1 d . H25 H 0.189282 0.077003 0.406022 0.026 Uiso 1 1 calc R C26 C 0.2820(2) 0.14483(18) 0.34892(18) 0.0195(8) Uani 1 1 d . C27 C 0.2314(2) 0.15709(18) 0.28876(17) 0.0177(7) Uani 1 1 d . C28 C 0.1378(2) 0.12039(19) 0.28133(17) 0.0194(8) Uani 1 1 d . C29 C 0.1302(3) 0.04543(19) 0.28185(18) 0.0211(8) Uani 1 1 d . H29 H 0.186032 0.016952 0.284986 0.025 Uiso 1 1 calc R C30 C 0.0427(3) 0.0117(2) 0.27786(18) 0.0226(8) Uani 1 1 d . H30 H 0.038878 -0.039446 0.278560 0.027 Uiso 1 1 calc R C31 C -0.0388(3) 0.0525(2) 0.27287(18) 0.0255(9) Uani 1 1 d . H31 H -0.098870 0.029443 0.270628 0.031 Uiso 1 1 calc R C32 C -0.0330(3) 0.1271(2) 0.27112(19) 0.0269(9) Uani 1 1 d . H32 H -0.089127 0.155217 0.267429 0.032 Uiso 1 1 calc R C33 C 0.0548(3) 0.1607(2) 0.27477(17) 0.0232(8) Uani 1 1 d . H33 H 0.058373 0.211846 0.272778 0.028 Uiso 1 1 calc R C34 C 0.2633(2) 0.20018(18) 0.23575(17) 0.0174(7) Uani 1 1 d . C35 C 0.2136(3) 0.21039(19) 0.17278(18) 0.0211(8) Uani 1 1 d . H35 H 0.153742 0.190703 0.160608 0.025 Uiso 1 1 calc R C36 C 0.2682(2) 0.25301(19) 0.13476(17) 0.0207(8) Uani 1 1 d . H36 H 0.253762 0.269270 0.090756 0.025 Uiso 1 1 calc R C37 C 0.3526(2) 0.26952(18) 0.17294(17) 0.0178(8) Uani 1 1 d . C38 C 0.4300(2) 0.30856(18) 0.14841(17) 0.0179(8) Uani 1 1 d . C39 C 0.4192(2) 0.34259(19) 0.08086(17) 0.0197(8) Uani 1 1 d . C40 C 0.4734(3) 0.3204(2) 0.02672(18) 0.0253(9) Uani 1 1 d . H40 H 0.515951 0.281071 0.031913 0.030 Uiso 1 1 calc R C41 C 0.4662(3) 0.3549(2) -0.03445(19) 0.0334(10) Uani 1 1 d . H41 H 0.504001 0.339312 -0.070736 0.040 Uiso 1 1 calc R C42 C 0.4043(3) 0.4119(2) -0.0431(2) 0.0365(10) Uani 1 1 d . H42 H 0.400384 0.436149 -0.084869 0.044 Uiso 1 1 calc R C43 C 0.3484(3) 0.4335(2) 0.0094(2) 0.0370(11) Uani 1 1 d . H43 H 0.304714 0.472017 0.003471 0.044 Uiso 1 1 calc R C44 C 0.3556(3) 0.3991(2) 0.07076(19) 0.0269(9) Uani 1 1 d . H44 H 0.316550 0.414318 0.106534 0.032 Uiso 1 1 calc R C45 C 0.3399(2) 0.3999(2) 0.35755(18) 0.0201(8) Uani 1 1 d . C46 C 0.4609(2) 0.58184(18) 0.39516(18) 0.0200(8) Uani 1 1 d . H46 H 0.462651 0.575964 0.347976 0.024 Uiso 1 1 calc R C47 C 0.5343(3) 0.61773(19) 0.42621(19) 0.0239(8) Uani 1 1 d . H47 H 0.585023 0.636939 0.400922 0.029 Uiso 1 1 calc R C48 C 0.5329(3) 0.6253(2) 0.4949(2) 0.0281(9) Uani 1 1 d . H48 H 0.582726 0.649656 0.517830 0.034 Uiso 1 1 calc R C49 C 0.4579(3) 0.5969(2) 0.52959(19) 0.0244(8) Uani 1 1 d . H49 H 0.455704 0.601084 0.576917 0.029 Uiso 1 1 calc R C50 C 0.3855(2) 0.56224(18) 0.49500(18) 0.0194(8) Uani 1 1 d . C51 C 0.3020(2) 0.5302(2) 0.53057(18) 0.0238(8) Uani 1 1 d . H51A H 0.320643 0.483254 0.550263 0.029 Uiso 1 1 calc R H51B H 0.283408 0.562564 0.567578 0.029 Uiso 1 1 calc R C52 C 0.1273(3) 0.5385(2) 0.29367(19) 0.0241(8) Uani 1 1 d . H52 H 0.155223 0.508309 0.260928 0.029 Uiso 1 1 calc R C53 C 0.0468(3) 0.5761(2) 0.2763(2) 0.0264(9) Uani 1 1 d . H53 H 0.020998 0.573045 0.232345 0.032 Uiso 1 1 calc R C54 C 0.0042(3) 0.6188(2) 0.3245(2) 0.0290(9) Uani 1 1 d . H54 H -0.051512 0.645463 0.314179 0.035 Uiso 1 1 calc R C55 C 0.0442(2) 0.62157(19) 0.3874(2) 0.0246(9) Uani 1 1 d . H55 H 0.015309 0.649250 0.421601 0.029 Uiso 1 1 calc R C56 C 0.1266(2) 0.58396(19) 0.40067(19) 0.0218(8) Uani 1 1 d . C57 C 0.1783(3) 0.5891(2) 0.46626(19) 0.0255(9) Uani 1 1 d . H57A H 0.228887 0.625907 0.462961 0.031 Uiso 1 1 calc R H57B H 0.133723 0.604837 0.501291 0.031 Uiso 1 1 calc R C58 C 0.1456(3) 0.4739(2) 0.5150(2) 0.0282(9) Uani 1 1 d . H58A H 0.088369 0.476323 0.486065 0.034 Uiso 1 1 calc R H58B H 0.128849 0.493432 0.559395 0.034 Uiso 1 1 calc R C59 C 0.1749(3) 0.3963(2) 0.5227(2) 0.0264(9) Uani 1 1 d . N60 N 0.1965(2) 0.37388(19) 0.58548(17) 0.0319(8) Uani 1 1 d . C61 C 0.2184(3) 0.3056(2) 0.5925(2) 0.0309(9) Uani 1 1 d . H61 H 0.232722 0.289109 0.636403 0.037 Uiso 1 1 calc R C62 C 0.2225(3) 0.2557(2) 0.5415(2) 0.0335(10) Uani 1 1 d . H62 H 0.238204 0.206752 0.550176 0.040 Uiso 1 1 calc R C63 C 0.2032(3) 0.2793(2) 0.4779(2) 0.0317(10) Uani 1 1 d . H63 H 0.207291 0.247155 0.441102 0.038 Uiso 1 1 calc R C64 C 0.1776(3) 0.3502(2) 0.4680(2) 0.0297(9) Uani 1 1 d . H64 H 0.162117 0.367285 0.424418 0.036 Uiso 1 1 calc R Cl1S Cl 0.69789(11) -0.00179(6) 0.37220(6) 0.0577(4) Uani 1 1 d . Cl2S Cl 0.71037(8) 0.10536(6) 0.26711(7) 0.0464(3) Uani 1 1 d . C3S C 0.6855(4) 0.0887(2) 0.3516(2) 0.0516(13) Uani 1 1 d . H3SA H 0.728804 0.117762 0.380016 0.062 Uiso 1 1 calc R H3SB H 0.619818 0.104275 0.360962 0.062 Uiso 1 1 calc R loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.0176(2) 0.0149(2) 0.0139(2) -0.00102(16) -0.00410(15) 0.00032(16) Cu1 0.0178(2) 0.0216(2) 0.0260(3) -0.0077(2) 0.00152(19) 0.00220(18) N1 0.0183(15) 0.0146(15) 0.0164(15) -0.0023(12) -0.0049(12) 0.0022(12) N2 0.0192(15) 0.0156(15) 0.0167(15) -0.0003(12) -0.0033(12) -0.0003(12) N3 0.0198(15) 0.0174(15) 0.0178(16) 0.0012(12) -0.0071(13) -0.0020(12) N4 0.0198(15) 0.0132(14) 0.0145(15) -0.0018(12) -0.0047(12) 0.0019(12) N5 0.0197(16) 0.0206(16) 0.0187(16) -0.0015(13) -0.0020(13) 0.0009(13) N6 0.0172(15) 0.0174(15) 0.0179(16) -0.0017(12) 0.0000(12) 0.0040(12) N7 0.0176(15) 0.0245(16) 0.0241(17) -0.0043(14) 0.0061(13) 0.0006(13) N8 0.0168(16) 0.0201(16) 0.0310(18) -0.0076(14) 0.0014(14) -0.0006(13) C1 0.0211(19) 0.0181(18) 0.0165(18) -0.0037(14) 0.0007(15) 0.0044(15) C2 0.0212(19) 0.027(2) 0.0177(19) -0.0011(16) 0.0012(16) -0.0005(16) C3 0.0187(19) 0.027(2) 0.022(2) -0.0004(16) 0.0027(16) -0.0003(16) C4 0.0164(18) 0.0182(18) 0.0179(18) -0.0028(15) -0.0019(15) 0.0032(14) C5 0.0187(18) 0.0145(17) 0.0199(19) -0.0058(14) -0.0041(15) 0.0016(14) C6 0.0184(18) 0.0230(19) 0.0161(18) -0.0053(15) -0.0023(15) 0.0016(15) C7 0.0182(19) 0.027(2) 0.0176(19) -0.0016(16) 0.0004(15) -0.0009(15) C8 0.031(2) 0.029(2) 0.020(2) -0.0005(17) 0.0033(17) -0.0106(17) C9 0.020(2) 0.046(3) 0.023(2) -0.0059(19) -0.0034(17) -0.0070(18) C10 0.021(2) 0.039(2) 0.029(2) -0.0097(19) -0.0039(17) 0.0082(18) C11 0.024(2) 0.026(2) 0.029(2) -0.0067(17) -0.0020(17) 0.0044(17) C12 0.0187(18) 0.0177(18) 0.0174(18) -0.0014(14) -0.0047(15) -0.0005(14) C13 0.0219(19) 0.0215(19) 0.026(2) -0.0031(16) -0.0086(16) -0.0043(16) C14 0.029(2) 0.0199(19) 0.025(2) 0.0040(16) -0.0123(17) -0.0052(16) C15 0.0193(19) 0.0199(18) 0.0185(19) 0.0009(15) -0.0077(15) -0.0002(15) C16 0.027(2) 0.0157(18) 0.0170(19) 0.0007(15) -0.0072(16) -0.0005(15) C17 0.024(2) 0.0210(19) 0.020(2) 0.0021(16) -0.0085(16) -0.0041(15) C18 0.042(2) 0.033(2) 0.023(2) 0.0013(18) -0.0006(19) 0.0084(19) C19 0.055(3) 0.038(2) 0.023(2) 0.0082(19) -0.003(2) 0.021(2) C20 0.038(2) 0.043(3) 0.021(2) 0.0068(19) -0.0052(18) 0.005(2) C21 0.033(2) 0.033(2) 0.020(2) -0.0027(17) -0.0071(17) 0.0003(18) C22 0.026(2) 0.022(2) 0.025(2) 0.0016(16) -0.0036(17) 0.0008(16) C23 0.0244(19) 0.0154(17) 0.0136(18) 0.0000(14) -0.0051(15) 0.0005(15) C24 0.028(2) 0.0194(18) 0.0150(18) 0.0051(15) -0.0047(16) -0.0004(16) C25 0.0210(19) 0.0201(19) 0.024(2) 0.0009(16) -0.0014(16) -0.0045(15) C26 0.0215(19) 0.0169(18) 0.0201(19) -0.0031(15) -0.0020(15) -0.0008(15) C27 0.0197(18) 0.0149(17) 0.0186(18) -0.0021(14) 0.0008(15) 0.0022(14) C28 0.0191(18) 0.026(2) 0.0128(18) -0.0023(15) -0.0030(15) -0.0024(15) C29 0.0201(19) 0.0186(18) 0.024(2) 0.0005(15) -0.0046(16) -0.0003(15) C30 0.026(2) 0.0224(19) 0.0192(19) -0.0006(16) -0.0020(16) -0.0047(16) C31 0.021(2) 0.036(2) 0.020(2) -0.0026(17) 0.0022(16) -0.0058(17) C32 0.0186(19) 0.040(2) 0.022(2) -0.0056(18) 0.0003(16) 0.0022(17) C33 0.027(2) 0.026(2) 0.0170(19) -0.0055(16) -0.0021(16) 0.0018(16) C34 0.0174(18) 0.0149(17) 0.0197(19) -0.0038(15) -0.0070(15) 0.0007(14) C35 0.0189(19) 0.0225(19) 0.022(2) 0.0004(16) -0.0037(16) 0.0000(15) C36 0.0244(19) 0.0223(19) 0.0153(18) -0.0021(15) -0.0081(15) 0.0016(16) C37 0.0192(18) 0.0167(18) 0.0174(18) -0.0036(14) -0.0031(15) 0.0043(14) C38 0.0208(19) 0.0162(17) 0.0166(18) -0.0054(14) -0.0024(15) 0.0039(14) C39 0.0197(18) 0.0228(19) 0.0166(18) -0.0029(15) -0.0036(15) -0.0011(15) C40 0.025(2) 0.031(2) 0.020(2) -0.0046(17) -0.0018(16) 0.0049(17) C41 0.032(2) 0.050(3) 0.018(2) -0.0057(19) 0.0020(18) -0.002(2) C42 0.051(3) 0.043(3) 0.015(2) 0.0058(18) -0.0028(19) 0.005(2) C43 0.051(3) 0.036(2) 0.024(2) 0.0058(19) -0.008(2) 0.014(2) C44 0.033(2) 0.027(2) 0.020(2) -0.0030(17) -0.0018(17) 0.0108(17) C45 0.0172(18) 0.024(2) 0.0191(19) -0.0014(16) 0.0002(15) -0.0044(16) C46 0.0209(19) 0.0208(19) 0.0183(19) 0.0012(15) 0.0010(15) 0.0042(15) C47 0.0178(19) 0.024(2) 0.030(2) 0.0035(17) -0.0003(16) -0.0019(16) C48 0.023(2) 0.027(2) 0.034(2) -0.0047(18) -0.0076(18) -0.0034(17) C49 0.025(2) 0.026(2) 0.022(2) -0.0048(16) -0.0040(16) 0.0010(16) C50 0.0218(19) 0.0182(18) 0.0182(19) -0.0022(15) -0.0004(15) 0.0049(15) C51 0.023(2) 0.026(2) 0.022(2) -0.0052(16) 0.0048(16) 0.0005(16) C52 0.0180(19) 0.024(2) 0.030(2) -0.0054(17) -0.0005(17) -0.0089(16) C53 0.0169(19) 0.024(2) 0.038(2) 0.0008(18) -0.0051(17) -0.0081(16) C54 0.018(2) 0.020(2) 0.049(3) 0.0062(18) -0.0024(19) -0.0023(16) C55 0.0140(18) 0.0181(19) 0.042(2) -0.0029(17) 0.0052(17) -0.0021(15) C56 0.0176(19) 0.0174(18) 0.031(2) -0.0048(16) 0.0017(16) -0.0042(15) C57 0.0194(19) 0.023(2) 0.034(2) -0.0094(17) 0.0023(17) 0.0025(16) C58 0.022(2) 0.032(2) 0.030(2) -0.0077(18) 0.0092(17) -0.0025(17) C59 0.0161(19) 0.032(2) 0.031(2) -0.0016(18) 0.0064(17) -0.0034(16) N60 0.0271(18) 0.040(2) 0.0281(19) -0.0027(16) 0.0059(15) -0.0085(16) C61 0.023(2) 0.039(2) 0.031(2) -0.0015(19) -0.0023(18) 0.0016(18) C62 0.023(2) 0.031(2) 0.046(3) 0.004(2) 0.0061(19) 0.0007(18) C63 0.027(2) 0.030(2) 0.038(2) -0.0060(19) 0.0073(19) -0.0064(18) C64 0.031(2) 0.033(2) 0.025(2) 0.0008(18) 0.0083(18) 0.0000(18) Cl1S 0.0975(11) 0.0359(7) 0.0396(7) -0.0063(5) -0.0059(7) -0.0164(7) Cl2S 0.0334(6) 0.0411(6) 0.0645(8) 0.0116(6) -0.0080(6) -0.0020(5) C3S 0.066(3) 0.040(3) 0.048(3) -0.017(2) -0.018(3) 0.020(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N1 Zn1 N3 155.44(11) N2 Zn1 N1 86.70(11) N2 Zn1 N3 87.77(11) N4 Zn1 N1 88.92(11) N4 Zn1 N2 158.90(11) N4 Zn1 N3 87.69(11) N5 Zn1 N1 100.82(11) N5 Zn1 N2 105.21(11) N5 Zn1 N3 103.73(12) N5 Zn1 N4 95.89(11) N6 Cu1 N7 76.01(11) N8 Cu1 N6 112.10(11) N8 Cu1 N7 78.95(12) C45 Cu1 N6 110.96(13) C45 Cu1 N7 130.95(13) C45 Cu1 N8 132.49(14) C1 N1 Zn1 124.8(2) C4 N1 Zn1 127.3(2) C4 N1 C1 106.8(3) C12 N2 Zn1 126.9(2) C15 N2 Zn1 124.4(2) C15 N2 C12 106.6(3) C23 N3 Zn1 125.6(2) C26 N3 Zn1 126.8(2) C26 N3 C23 106.4(3) C34 N4 Zn1 127.1(2) C37 N4 Zn1 125.1(2) C37 N4 C34 107.2(3) C45 N5 Zn1 172.8(3) C46 N6 Cu1 123.8(2) C50 N6 Cu1 117.3(2) C50 N6 C46 118.0(3) C51 N7 Cu1 104.8(2) C51 N7 C57 110.8(3) C51 N7 C58 113.2(3) C57 N7 Cu1 99.5(2) C57 N7 C58 108.4(3) C58 N7 Cu1 119.3(2) C52 N8 Cu1 126.6(3) C52 N8 C56 117.6(3) C56 N8 Cu1 115.7(2) N1 C1 C2 109.6(3) N1 C1 C38 125.8(3) C38 C1 C2 124.6(3) C1 C2 H2 126.4 C3 C2 C1 107.1(3) C3 C2 H2 126.4 C2 C3 H3 126.5 C2 C3 C4 106.9(3) C4 C3 H3 126.5 N1 C4 C3 109.5(3) N1 C4 C5 125.7(3) C5 C4 C3 124.7(3) C4 C5 C6 118.0(3) C12 C5 C4 124.9(3) C12 C5 C6 117.2(3) C7 C6 C5 120.5(3) C11 C6 C5 121.4(3) C11 C6 C7 118.1(3) C6 C7 H7 119.6 C8 C7 C6 120.8(3) C8 C7 H7 119.6 C7 C8 H8 119.8 C9 C8 C7 120.3(4) C9 C8 H8 119.8 C8 C9 H9 120.2 C10 C9 C8 119.5(4) C10 C9 H9 120.2 C9 C10 H10 119.6 C9 C10 C11 120.7(4) C11 C10 H10 119.6 C6 C11 H11 119.7 C10 C11 C6 120.5(4) C10 C11 H11 119.7 N2 C12 C5 125.2(3) N2 C12 C13 109.1(3) C5 C12 C13 125.7(3) C12 C13 H13 126.4 C14 C13 C12 107.1(3) C14 C13 H13 126.4 C13 C14 H14 126.2 C13 C14 C15 107.6(3) C15 C14 H14 126.2 N2 C15 C14 109.6(3) N2 C15 C16 126.5(3) C16 C15 C14 123.8(3) C15 C16 C17 115.9(3) C15 C16 C23 125.2(3) C23 C16 C17 118.9(3) C18 C17 C16 120.8(3) C22 C17 C16 120.6(3) C22 C17 C18 118.4(3) C17 C18 H18 119.6 C19 C18 C17 120.8(4) C19 C18 H18 119.6 C18 C19 H19 119.8 C20 C19 C18 120.4(4) C20 C19 H19 119.8 C19 C20 H20 120.2 C19 C20 C21 119.5(4) C21 C20 H20 120.2 C20 C21 H21 119.8 C20 C21 C22 120.4(4) C22 C21 H21 119.8 C17 C22 C21 120.5(4) C17 C22 H22 119.7 C21 C22 H22 119.7 N3 C23 C16 125.5(3) N3 C23 C24 109.6(3) C16 C23 C24 125.0(3) C23 C24 H24 126.4 C25 C24 C23 107.3(3) C25 C24 H24 126.4 C24 C25 H25 126.5 C24 C25 C26 107.0(3) C26 C25 H25 126.5 N3 C26 C25 109.8(3) N3 C26 C27 125.4(3) C27 C26 C25 124.7(3) C26 C27 C28 116.8(3) C34 C27 C26 124.8(3) C34 C27 C28 118.3(3) C29 C28 C27 121.5(3) C29 C28 C33 118.1(3) C33 C28 C27 120.5(3) C28 C29 H29 119.4 C30 C29 C28 121.2(3) C30 C29 H29 119.4 C29 C30 H30 120.0 C31 C30 C29 119.9(3) C31 C30 H30 120.0 C30 C31 H31 120.0 C30 C31 C32 120.0(4) C32 C31 H31 120.0 C31 C32 H32 120.0 C31 C32 C33 119.9(4) C33 C32 H32 120.0 C28 C33 H33 119.6 C32 C33 C28 120.8(4) C32 C33 H33 119.6 N4 C34 C27 125.9(3) N4 C34 C35 109.0(3) C27 C34 C35 125.1(3) C34 C35 H35 126.5 C36 C35 C34 107.0(3) C36 C35 H35 126.5 C35 C36 H36 126.2 C35 C36 C37 107.5(3) C37 C36 H36 126.2 N4 C37 C36 109.2(3) N4 C37 C38 126.1(3) C38 C37 C36 124.5(3) C1 C38 C37 125.6(3) C1 C38 C39 117.0(3) C37 C38 C39 117.4(3) C40 C39 C38 121.6(3) C40 C39 C44 117.9(3) C44 C39 C38 120.5(3) C39 C40 H40 119.5 C41 C40 C39 121.0(4) C41 C40 H40 119.5 C40 C41 H41 119.8 C42 C41 C40 120.3(4) C42 C41 H41 119.8 C41 C42 H42 120.2 C43 C42 C41 119.6(4) C43 C42 H42 120.2 C42 C43 H43 119.9 C42 C43 C44 120.2(4) C44 C43 H43 119.9 C39 C44 H44 119.5 C43 C44 C39 121.1(4) C43 C44 H44 119.5 N5 C45 Cu1 173.3(3) N6 C46 H46 118.5 N6 C46 C47 123.0(3) C47 C46 H46 118.5 C46 C47 H47 120.7 C46 C47 C48 118.7(3) C48 C47 H47 120.7 C47 C48 H48 120.6 C49 C48 C47 118.8(3) C49 C48 H48 120.6 C48 C49 H49 120.2 C48 C49 C50 119.6(4) C50 C49 H49 120.2 N6 C50 C49 121.9(3) N6 C50 C51 116.4(3) C49 C50 C51 121.6(3) N7 C51 C50 112.2(3) N7 C51 H51A 109.2 N7 C51 H51B 109.2 C50 C51 H51A 109.2 C50 C51 H51B 109.2 H51A C51 H51B 107.9 N8 C52 H52 118.2 N8 C52 C53 123.6(4) C53 C52 H52 118.2 C52 C53 H53 120.7 C52 C53 C54 118.5(4) C54 C53 H53 120.7 C53 C54 H54 120.7 C55 C54 C53 118.6(4) C55 C54 H54 120.7 C54 C55 H55 120.2 C54 C55 C56 119.6(4) C56 C55 H55 120.2 N8 C56 C55 122.1(4) N8 C56 C57 115.3(3) C55 C56 C57 122.5(3) N7 C57 C56 111.5(3) N7 C57 H57A 109.3 N7 C57 H57B 109.3 C56 C57 H57A 109.3 C56 C57 H57B 109.3 H57A C57 H57B 108.0 N7 C58 H58A 109.0 N7 C58 H58B 109.0 N7 C58 C59 113.0(3) H58A C58 H58B 107.8 C59 C58 H58A 109.0 C59 C58 H58B 109.0 N60 C59 C58 116.7(3) N60 C59 C64 122.2(4) C64 C59 C58 121.1(4) C61 N60 C59 116.5(4) N60 C61 H61 117.2 N60 C61 C62 125.6(4) C62 C61 H61 117.2 C61 C62 H62 121.2 C63 C62 C61 117.5(4) C63 C62 H62 121.2 C62 C63 H63 120.4 C62 C63 C64 119.3(4) C64 C63 H63 120.4 C59 C64 H64 120.6 C63 C64 C59 118.9(4) C63 C64 H64 120.6 Cl1S C3S Cl2S 112.2(3) Cl1S C3S H3SA 109.2 Cl1S C3S H3SB 109.2 Cl2S C3S H3SA 109.2 Cl2S C3S H3SB 109.2 H3SA C3S H3SB 107.9 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Zn1 N1 2.091(3) Zn1 N2 2.086(3) Zn1 N3 2.092(3) Zn1 N4 2.067(3) Zn1 N5 2.050(3) Cu1 N6 2.083(3) Cu1 N7 2.289(3) Cu1 N8 2.033(3) Cu1 C45 1.878(4) N1 C1 1.366(4) N1 C4 1.364(4) N2 C12 1.374(4) N2 C15 1.373(4) N3 C23 1.376(4) N3 C26 1.370(4) N4 C34 1.371(4) N4 C37 1.364(4) N5 C45 1.151(4) N6 C46 1.347(4) N6 C50 1.337(4) N7 C51 1.465(5) N7 C57 1.473(5) N7 C58 1.480(5) N8 C52 1.337(5) N8 C56 1.352(5) C1 C2 1.438(5) C1 C38 1.402(5) C2 H2 0.9500 C2 C3 1.348(5) C3 H3 0.9500 C3 C4 1.443(5) C4 C5 1.406(5) C5 C6 1.495(5) C5 C12 1.402(5) C6 C7 1.396(5) C6 C11 1.395(5) C7 H7 0.9500 C7 C8 1.389(5) C8 H8 0.9500 C8 C9 1.383(6) C9 H9 0.9500 C9 C10 1.371(6) C10 H10 0.9500 C10 C11 1.393(5) C11 H11 0.9500 C12 C13 1.445(5) C13 H13 0.9500 C13 C14 1.344(5) C14 H14 0.9500 C14 C15 1.431(5) C15 C16 1.397(5) C16 C17 1.499(5) C16 C23 1.401(5) C17 C18 1.391(5) C17 C22 1.389(5) C18 H18 0.9500 C18 C19 1.384(5) C19 H19 0.9500 C19 C20 1.379(6) C20 H20 0.9500 C20 C21 1.379(6) C21 H21 0.9500 C21 C22 1.391(5) C22 H22 0.9500 C23 C24 1.443(5) C24 H24 0.9500 C24 C25 1.347(5) C25 H25 0.9500 C25 C26 1.446(5) C26 C27 1.411(5) C27 C28 1.492(5) C27 C34 1.405(5) C28 C29 1.394(5) C28 C33 1.395(5) C29 H29 0.9500 C29 C30 1.386(5) C30 H30 0.9500 C30 C31 1.380(5) C31 H31 0.9500 C31 C32 1.387(5) C32 H32 0.9500 C32 C33 1.389(5) C33 H33 0.9500 C34 C35 1.447(5) C35 H35 0.9500 C35 C36 1.344(5) C36 H36 0.9500 C36 C37 1.441(5) C37 C38 1.404(5) C38 C39 1.497(5) C39 C40 1.394(5) C39 C44 1.394(5) C40 H40 0.9500 C40 C41 1.383(5) C41 H41 0.9500 C41 C42 1.381(6) C42 H42 0.9500 C42 C43 1.379(6) C43 H43 0.9500 C43 C44 1.385(5) C44 H44 0.9500 C46 H46 0.9500 C46 C47 1.374(5) C47 H47 0.9500 C47 C48 1.381(5) C48 H48 0.9500 C48 C49 1.375(5) C49 H49 0.9500 C49 C50 1.386(5) C50 C51 1.505(5) C51 H51A 0.9900 C51 H51B 0.9900 C52 H52 0.9500 C52 C53 1.375(5) C53 H53 0.9500 C53 C54 1.388(6) C54 H54 0.9500 C54 C55 1.375(6) C55 H55 0.9500 C55 C56 1.380(5) C56 C57 1.497(5) C57 H57A 0.9900 C57 H57B 0.9900 C58 H58A 0.9900 C58 H58B 0.9900 C58 C59 1.504(5) C59 N60 1.353(5) C59 C64 1.390(5) N60 C61 1.310(5) C61 H61 0.9500 C61 C62 1.377(6) C62 H62 0.9500 C62 C63 1.369(6) C63 H63 0.9500 C63 C64 1.377(6) C64 H64 0.9500 Cl1S C3S 1.737(5) Cl2S C3S 1.755(5) C3S H3SA 0.9900 C3S H3SB 0.9900 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion Zn1 N1 C1 C2 168.2(2) Zn1 N1 C1 C38 -10.8(5) Zn1 N1 C4 C3 -169.1(2) Zn1 N1 C4 C5 8.9(5) Zn1 N2 C12 C5 -16.3(5) Zn1 N2 C12 C13 163.0(2) Zn1 N2 C15 C14 -163.8(2) Zn1 N2 C15 C16 19.0(5) Zn1 N3 C23 C16 -11.8(5) Zn1 N3 C23 C24 168.1(2) Zn1 N3 C26 C25 -167.8(2) Zn1 N3 C26 C27 10.2(5) Zn1 N4 C34 C27 -10.9(5) Zn1 N4 C34 C35 171.5(2) Zn1 N4 C37 C36 -171.5(2) Zn1 N4 C37 C38 13.0(5) Cu1 N6 C46 C47 -170.4(3) Cu1 N6 C50 C49 170.1(3) Cu1 N6 C50 C51 -9.1(4) Cu1 N7 C51 C50 35.8(3) Cu1 N7 C57 C56 45.0(3) Cu1 N7 C58 C59 54.7(4) Cu1 N8 C52 C53 178.4(3) Cu1 N8 C56 C55 -176.7(3) Cu1 N8 C56 C57 5.9(4) N1 C1 C2 C3 1.6(4) N1 C1 C38 C37 -4.2(6) N1 C1 C38 C39 176.5(3) N1 C4 C5 C6 -176.4(3) N1 C4 C5 C12 2.5(6) N2 C12 C13 C14 1.0(4) N2 C15 C16 C17 178.3(3) N2 C15 C16 C23 -1.5(6) N3 C23 C24 C25 0.0(4) N3 C26 C27 C28 179.6(3) N3 C26 C27 C34 0.4(6) N4 C34 C35 C36 -0.3(4) N4 C37 C38 C1 3.1(6) N4 C37 C38 C39 -177.6(3) N6 C46 C47 C48 1.1(5) N6 C50 C51 N7 -20.9(4) N7 C58 C59 N60 105.0(4) N7 C58 C59 C64 -76.2(5) N8 C52 C53 C54 -1.8(5) N8 C56 C57 N7 -38.5(4) C1 N1 C4 C3 -0.8(4) C1 N1 C4 C5 177.2(3) C1 C2 C3 C4 -2.0(4) C1 C38 C39 C40 64.9(5) C1 C38 C39 C44 -113.6(4) C2 C1 C38 C37 177.0(3) C2 C1 C38 C39 -2.3(5) C2 C3 C4 N1 1.8(4) C2 C3 C4 C5 -176.2(3) C3 C4 C5 C6 1.2(5) C3 C4 C5 C12 -179.9(3) C4 N1 C1 C2 -0.5(4) C4 N1 C1 C38 -179.4(3) C4 C5 C6 C7 55.7(5) C4 C5 C6 C11 -126.2(4) C4 C5 C12 N2 1.5(6) C4 C5 C12 C13 -177.8(3) C5 C6 C7 C8 177.5(3) C5 C6 C11 C10 -176.5(3) C5 C12 C13 C14 -179.7(3) C6 C5 C12 N2 -179.6(3) C6 C5 C12 C13 1.2(5) C6 C7 C8 C9 -0.7(5) C7 C6 C11 C10 1.7(5) C7 C8 C9 C10 0.9(6) C8 C9 C10 C11 0.2(6) C9 C10 C11 C6 -1.5(6) C11 C6 C7 C8 -0.6(5) C12 N2 C15 C14 0.8(4) C12 N2 C15 C16 -176.5(3) C12 C5 C6 C7 -123.3(4) C12 C5 C6 C11 54.8(5) C12 C13 C14 C15 -0.5(4) C13 C14 C15 N2 -0.2(4) C13 C14 C15 C16 177.2(3) C14 C15 C16 C17 1.5(5) C14 C15 C16 C23 -178.3(3) C15 N2 C12 C5 179.6(3) C15 N2 C12 C13 -1.0(4) C15 C16 C17 C18 -78.8(4) C15 C16 C17 C22 95.4(4) C15 C16 C23 N3 -2.5(6) C15 C16 C23 C24 177.6(3) C16 C17 C18 C19 174.7(4) C16 C17 C22 C21 -174.6(3) C16 C23 C24 C25 179.9(3) C17 C16 C23 N3 177.8(3) C17 C16 C23 C24 -2.1(5) C17 C18 C19 C20 -0.5(7) C18 C17 C22 C21 -0.3(6) C18 C19 C20 C21 0.5(7) C19 C20 C21 C22 -0.3(6) C20 C21 C22 C17 0.3(6) C22 C17 C18 C19 0.5(6) C23 N3 C26 C25 0.3(4) C23 N3 C26 C27 178.3(3) C23 C16 C17 C18 101.0(4) C23 C16 C17 C22 -84.9(4) C23 C24 C25 C26 0.2(4) C24 C25 C26 N3 -0.3(4) C24 C25 C26 C27 -178.3(3) C25 C26 C27 C28 -2.8(5) C25 C26 C27 C34 178.1(3) C26 N3 C23 C16 179.9(3) C26 N3 C23 C24 -0.2(4) C26 C27 C28 C29 -61.4(5) C26 C27 C28 C33 117.5(4) C26 C27 C34 N4 -0.1(6) C26 C27 C34 C35 177.1(3) C27 C28 C29 C30 177.2(3) C27 C28 C33 C32 -176.8(3) C27 C34 C35 C36 -178.0(3) C28 C27 C34 N4 -179.3(3) C28 C27 C34 C35 -2.0(5) C28 C29 C30 C31 0.4(6) C29 C28 C33 C32 2.1(5) C29 C30 C31 C32 0.7(6) C30 C31 C32 C33 -0.4(6) C31 C32 C33 C28 -1.1(6) C33 C28 C29 C30 -1.8(5) C34 N4 C37 C36 0.2(4) C34 N4 C37 C38 -175.3(3) C34 C27 C28 C29 117.8(4) C34 C27 C28 C33 -63.3(4) C34 C35 C36 C37 0.4(4) C35 C36 C37 N4 -0.4(4) C35 C36 C37 C38 175.2(3) C36 C37 C38 C1 -171.8(3) C36 C37 C38 C39 7.5(5) C37 N4 C34 C27 177.7(3) C37 N4 C34 C35 0.0(4) C37 C38 C39 C40 -114.5(4) C37 C38 C39 C44 67.1(4) C38 C1 C2 C3 -179.4(3) C38 C39 C40 C41 -176.6(3) C38 C39 C44 C43 176.7(4) C39 C40 C41 C42 -0.4(6) C40 C39 C44 C43 -1.8(6) C40 C41 C42 C43 -1.2(7) C41 C42 C43 C44 1.3(7) C42 C43 C44 C39 0.2(7) C44 C39 C40 C41 1.9(6) C46 N6 C50 C49 0.0(5) C46 N6 C50 C51 -179.2(3) C46 C47 C48 C49 -0.3(5) C47 C48 C49 C50 -0.6(6) C48 C49 C50 N6 0.8(5) C48 C49 C50 C51 179.9(3) C49 C50 C51 N7 159.9(3) C50 N6 C46 C47 -1.0(5) C51 N7 C57 C56 154.9(3) C51 N7 C58 C59 -69.2(4) C52 N8 C56 C55 0.5(5) C52 N8 C56 C57 -176.9(3) C52 C53 C54 C55 0.0(5) C53 C54 C55 C56 1.8(5) C54 C55 C56 N8 -2.2(5) C54 C55 C56 C57 175.0(3) C55 C56 C57 N7 144.1(3) C56 N8 C52 C53 1.5(5) C57 N7 C51 C50 -70.6(4) C57 N7 C58 C59 167.4(3) C58 N7 C51 C50 167.3(3) C58 N7 C57 C56 -80.3(4) C58 C59 N60 C61 177.5(3) C58 C59 C64 C63 -178.8(3) C59 N60 C61 C62 0.9(6) N60 C59 C64 C63 -0.1(6) N60 C61 C62 C63 0.8(6) C61 C62 C63 C64 -2.2(6) C62 C63 C64 C59 1.8(6) C64 C59 N60 C61 -1.3(5)