#------------------------------------------------------------------------------ #$Date: 2019-11-26 03:24:08 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242506 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/25/4132536.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132536 loop_ _publ_author_name 'Li, Ke' 'Li, Mao-Lin' 'Zhang, Qi' 'Zhu, Shou-Fei' 'Zhou, Qi-Lin' _publ_section_title ; Highly Enantioselective Nickel-Catalyzed Intramolecular Hydroalkenylation of N- and O-Tethered 1,6-Dienes To Form Six-Membered Heterocycles. ; _journal_issue 24 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 7458 _journal_page_last 7461 _journal_paper_doi 10.1021/jacs.8b04703 _journal_volume 140 _journal_year 2018 _chemical_absolute_configuration ad _chemical_formula_moiety 'C19 H21 N O2 S' _chemical_formula_sum 'C19 H21 N O2 S' _chemical_formula_weight 327.43 _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _audit_creation_date 2016-05-17 _audit_creation_method ; Olex2 1.2-ac21 (compiled 2015.09.16 svn.r134, GUI svn.r4998) ; _cell_angle_alpha 90 _cell_angle_beta 115.687(6) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 5.6458(3) _cell_length_b 26.6994(9) _cell_length_c 6.1070(2) _cell_measurement_reflns_used 4969 _cell_measurement_temperature 113.15 _cell_measurement_theta_max 31.1130 _cell_measurement_theta_min 3.0600 _cell_volume 829.59(7) _computing_cell_refinement ; CrysAlisPro 1.171.38.41 (Rigaku OD, 2015) ; _computing_data_collection ; CrystalClear-SM Expert 2.1 b42 (Rigaku, 2015) ; _computing_data_reduction ; CrysAlisPro 1.171.38.41 (Rigaku OD, 2015) ; _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2008)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 113.15 _diffrn_detector PILT _diffrn_detector_area_resol_mean 5.814 _diffrn_detector_type 'Rigaku Pilatus 200K' _diffrn_measured_fraction_theta_full 0.984 _diffrn_measured_fraction_theta_max 0.904 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames -------------------------------------------------------------------------- 1 \w -120.00 60.00 0.50 5.00 -- -30.00 45.00 0.00 360 2 \w -120.00 60.00 0.50 5.00 -- -30.00 45.00 90.00 360 3 \w -120.00 60.00 0.50 5.00 -- -30.00 45.00 180.00 360 ; _diffrn_measurement_device 'AFC10: Fixed Chi 2 circle' _diffrn_measurement_device_type 'Rigaku Xtalab P200' _diffrn_measurement_method 'profile data from \w-scans' _diffrn_measurement_specimen_support 'Mitegen 50um' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0184478000 _diffrn_orient_matrix_UB_12 0.0121430000 _diffrn_orient_matrix_UB_13 -0.1095816000 _diffrn_orient_matrix_UB_21 -0.0039276000 _diffrn_orient_matrix_UB_22 0.0235304000 _diffrn_orient_matrix_UB_23 0.0521054000 _diffrn_orient_matrix_UB_31 0.1381716000 _diffrn_orient_matrix_UB_32 0.0022993000 _diffrn_orient_matrix_UB_33 0.0433184000 _diffrn_radiation_collimation 0.3 _diffrn_radiation_monochromator Confocal _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0197 _diffrn_reflns_av_unetI/netI 0.0318 _diffrn_reflns_Laue_measured_fraction_full 0.984 _diffrn_reflns_Laue_measured_fraction_max 0.904 _diffrn_reflns_limit_h_max 8 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 38 _diffrn_reflns_limit_k_min -37 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_number 8060 _diffrn_reflns_point_group_measured_fraction_full 0.909 _diffrn_reflns_point_group_measured_fraction_max 0.802 _diffrn_reflns_theta_full 26.000 _diffrn_reflns_theta_max 31.566 _diffrn_reflns_theta_min 1.525 _diffrn_source 'Rotating Anode' _diffrn_source_current 24.0 _diffrn_source_power 1.2 _diffrn_source_target Mo _diffrn_source_type 'Rotating Anode' _diffrn_source_voltage 50.0 _exptl_absorpt_coefficient_mu 0.204 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.42241 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.41 (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.311 _exptl_crystal_description plate _exptl_crystal_F_000 348 _exptl_crystal_size_max 0.32 _exptl_crystal_size_mid 0.28 _exptl_crystal_size_min 0.12 _refine_diff_density_max 0.504 _refine_diff_density_min -0.521 _refine_diff_density_rms 0.055 _refine_ls_abs_structure_details ; Flack x determined using 1698 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.05(3) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.067 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 209 _refine_ls_number_reflns 4450 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.067 _refine_ls_R_factor_all 0.0382 _refine_ls_R_factor_gt 0.0364 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0700P)^2^+0.0330P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1020 _refine_ls_wR_factor_ref 0.1030 _reflns_Friedel_coverage 0.741 _reflns_Friedel_fraction_full 0.830 _reflns_Friedel_fraction_max 0.696 _reflns_number_gt 4227 _reflns_number_total 4450 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b04703_si_002.cif _cod_data_source_block m20160518b _cod_original_cell_volume 829.58(7) _cod_database_code 4132536 _chemical_oxdiff_formula C19H21NO2S _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.976 _shelx_estimated_absorpt_t_min 0.937 _reflns_odcompleteness_completeness 90.44 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 31.49 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C3(H3) 2.b Secondary CH2 refined with riding coordinates: C1(H1A,H1B), C4(H4A,H4B), C5(H5A,H5B) 2.c Aromatic/amide H refined with riding coordinates: C8(H8), C9(H9), C10(H10), C11(H11), C12(H12), C14(H14), C15(H15), C17(H17), C18(H18) 2.d X=CH2 refined with riding coordinates: C6(H6A,H6B) 2.e Idealised Me refined as rotating group: C19(H19A,H19B,H19C) ; _shelx_res_file ; m20160518b.res created by SHELXL-2014/8 TITL m20160518b_a.res in P2(1) REM Old TITL m20160518b in P21/m #11 REM SHELXT solution in P2(1) REM R1 0.085, Rweak 0.022, Alpha 0.006, Orientation as input REM Flack x = 0.149 ( 0.023 ) from Parsons' quotients REM Formula found by SHELXT: C18 N O3 S CELL 0.71073 5.645778 26.699387 6.106961 90 115.6869 90 ZERR 2 0.000284 0.000923 0.000235 0 0.0055 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N O S UNIT 38 42 2 4 2 L.S. 10 PLAN 20 SIZE 0.32 0.28 0.12 TEMP -160 BOND $H CONF htab fmap 2 acta 52 MORE -1 REM REM REM WGHT 0.070000 0.033000 FVAR 1.04553 S1 5 1.028215 0.446711 0.387672 11.00000 0.01664 0.02459 = 0.01984 -0.00155 0.00971 -0.00019 O1 4 1.072894 0.444257 0.173908 11.00000 0.02560 0.03415 = 0.02651 -0.00208 0.01800 0.00078 O2 4 1.247122 0.447866 0.623090 11.00000 0.01602 0.03137 = 0.02561 -0.00227 0.00515 -0.00015 N1 3 0.855803 0.497791 0.363530 11.00000 0.01653 0.02401 = 0.01378 -0.00151 0.00768 -0.00003 C1 1 0.790889 0.507339 0.569774 11.00000 0.01789 0.02439 = 0.01520 0.00007 0.00830 -0.00052 AFIX 23 H1A 2 0.950576 0.503575 0.724921 11.00000 -1.20000 H1B 2 0.658797 0.482730 0.567774 11.00000 -1.20000 AFIX 0 C2 1 0.682885 0.559858 0.550075 11.00000 0.01602 0.02508 = 0.01471 -0.00049 0.00915 -0.00092 C3 1 0.449121 0.570439 0.309826 11.00000 0.01525 0.02356 = 0.01472 -0.00001 0.00700 -0.00076 AFIX 13 H3 2 0.308541 0.546043 0.294962 11.00000 -1.20000 AFIX 0 C4 1 0.529852 0.558167 0.106939 11.00000 0.02133 0.02580 = 0.01361 0.00021 0.00812 0.00019 AFIX 23 H4A 2 0.377887 0.563336 -0.052648 11.00000 -1.20000 H4B 2 0.671906 0.581173 0.117421 11.00000 -1.20000 AFIX 0 C5 1 0.624594 0.504431 0.125501 11.00000 0.01960 0.02553 = 0.01354 -0.00198 0.00687 -0.00018 AFIX 23 H5A 2 0.482682 0.481110 0.112284 11.00000 -1.20000 H5B 2 0.673897 0.497076 -0.008231 11.00000 -1.20000 AFIX 0 C6 1 0.791028 0.592332 0.731972 11.00000 0.01841 0.03041 = 0.01780 -0.00268 0.00838 -0.00061 AFIX 93 H6A 2 0.938212 0.582664 0.876837 11.00000 -1.20000 H6B 2 0.721055 0.625185 0.716973 11.00000 -1.20000 AFIX 0 C7 1 0.334175 0.622319 0.292467 11.00000 0.01586 0.02340 = 0.01720 -0.00121 0.00605 -0.00183 C8 1 0.186004 0.632393 0.420195 11.00000 0.02069 0.02821 = 0.02566 -0.00085 0.01252 -0.00027 AFIX 43 H8 2 0.163099 0.606892 0.517813 11.00000 -1.20000 AFIX 0 C9 1 0.071556 0.678898 0.407403 11.00000 0.02483 0.03138 = 0.03536 -0.00293 0.01651 0.00149 AFIX 43 H9 2 -0.027811 0.685097 0.496468 11.00000 -1.20000 AFIX 0 C10 1 0.102259 0.716436 0.264255 11.00000 0.03115 0.02442 = 0.04605 -0.00055 0.01750 0.00399 AFIX 43 H10 2 0.022997 0.748292 0.253501 11.00000 -1.20000 AFIX 0 C11 1 0.249149 0.706912 0.137949 11.00000 0.03444 0.02582 = 0.04334 0.00745 0.01923 0.00220 AFIX 43 H11 2 0.271298 0.732494 0.040289 11.00000 -1.20000 AFIX 0 C12 1 0.365069 0.660450 0.151593 11.00000 0.02526 0.02553 = 0.02630 0.00342 0.01368 0.00081 AFIX 43 H12 2 0.466371 0.654629 0.064014 11.00000 -1.20000 AFIX 0 C13 1 0.823925 0.396412 0.381315 11.00000 0.02159 0.01883 = 0.02228 -0.00128 0.01063 0.00071 C14 1 0.641246 0.378216 0.158237 11.00000 0.02693 0.02618 = 0.01919 -0.00177 0.00852 0.00001 AFIX 43 H14 2 0.636465 0.391020 0.011238 11.00000 -1.20000 AFIX 0 C15 1 0.466978 0.341363 0.152638 11.00000 0.02567 0.02627 = 0.02608 -0.00305 0.00470 -0.00366 AFIX 43 H15 2 0.343454 0.328636 0.000611 11.00000 -1.20000 AFIX 0 C16 1 0.469564 0.322525 0.366999 11.00000 0.02991 0.02127 = 0.03254 -0.00147 0.01477 -0.00314 C17 1 0.653508 0.341205 0.586867 11.00000 0.03466 0.02448 = 0.02656 -0.00022 0.01682 -0.00259 AFIX 43 H17 2 0.658710 0.328300 0.733856 11.00000 -1.20000 AFIX 0 C18 1 0.830302 0.378321 0.597362 11.00000 0.02647 0.02189 = 0.01797 -0.00083 0.00873 -0.00024 AFIX 43 H18 2 0.953417 0.391133 0.749367 11.00000 -1.20000 AFIX 0 C19 1 0.272975 0.283382 0.359417 11.00000 0.03597 0.03622 = 0.04664 -0.00064 0.01681 -0.01217 AFIX 137 H19A 2 0.094936 0.297190 0.277797 11.00000 -1.50000 H19B 2 0.308896 0.273585 0.525539 11.00000 -1.50000 H19C 2 0.287550 0.253975 0.269995 11.00000 -1.50000 AFIX 0 HKLF 4 REM m20160518b_a.res in P2(1) REM R1 = 0.0364 for 4227 Fo > 4sig(Fo) and 0.0382 for all 4450 data REM 209 parameters refined using 1 restraints END WGHT 0.0707 0.0292 REM Instructions for potential hydrogen bonds EQIV $1 x-1, y, z HTAB C1 O2_$1 REM Highest difference peak 0.504, deepest hole -0.521, 1-sigma level 0.055 Q1 1 1.0216 0.4161 0.3943 11.00000 0.05 0.50 Q2 1 1.0155 0.4763 0.3841 11.00000 0.05 0.48 Q3 1 1.0946 0.4468 0.3060 11.00000 0.05 0.47 Q4 1 0.7402 0.5356 0.5635 11.00000 0.05 0.38 Q5 1 0.5802 0.5313 0.1283 11.00000 0.05 0.37 Q6 1 1.1463 0.4464 0.5130 11.00000 0.05 0.36 Q7 1 0.2598 0.6283 0.3602 11.00000 0.05 0.34 Q8 1 0.3746 0.5966 0.3037 11.00000 0.05 0.34 Q9 1 0.7841 0.3489 0.5748 11.00000 0.05 0.33 Q10 1 0.8345 0.5050 0.4660 11.00000 0.05 0.32 Q11 1 0.5640 0.5656 0.4369 11.00000 0.05 0.31 Q12 1 0.7436 0.3885 0.2721 11.00000 0.05 0.30 Q13 1 0.7399 0.5680 0.6615 11.00000 0.05 0.30 Q14 1 0.4928 0.5660 0.2260 11.00000 0.05 0.30 Q15 1 0.5275 0.3228 0.2766 11.00000 0.05 0.29 Q16 1 0.7479 0.5012 0.2541 11.00000 0.05 0.29 Q17 1 0.5737 0.3256 0.4835 11.00000 0.05 0.28 Q18 1 0.8596 0.3832 0.4760 11.00000 0.05 0.27 Q19 1 0.9351 0.4464 0.4489 11.00000 0.05 0.26 Q20 1 1.2557 0.4757 0.6289 11.00000 0.05 0.25 ; _shelx_res_checksum 65106 _shelx_hkl_file ; 0 0 1 5945.40 154.46 0 0 -1 5905.44 154.50 0 0 1 5907.67 154.71 0 0 2 206.17 6.40 0 0 2 203.60 5.84 0 0 -2 189.11 5.96 0 0 3 95.82 3.25 0 0 3 92.95 4.02 0 0 -3 94.42 3.72 0 0 -4 2471.87 64.35 0 0 4 2391.70 64.83 0 0 4 2357.67 63.18 0 0 -5 315.03 10.79 0 0 5 334.80 11.49 0 0 6 48.40 3.65 0 0 7 110.00 6.10 0 1 1 5286.89 140.55 0 -1 -1 5569.31 140.65 0 -1 1 5474.70 140.86 0 1 -1 5293.13 140.64 0 1 1 5396.75 140.84 0 -1 1 5378.01 140.60 0 1 -2 240.46 7.26 0 1 2 243.92 7.03 0 -1 2 237.81 7.57 0 -1 -2 262.26 7.32 0 -1 2 251.79 7.13 0 1 2 244.70 7.62 0 1 3 271.95 8.77 0 -1 3 261.54 8.71 0 -1 -3 282.56 8.42 0 -1 3 265.12 7.85 0 1 -3 274.11 8.39 0 1 3 263.03 7.75 0 -1 -4 6.12 1.41 0 -1 4 6.90 1.55 0 1 -4 6.68 1.40 0 1 4 5.67 1.00 0 -1 4 5.22 0.97 0 1 4 6.57 1.60 0 -1 5 647.88 20.04 0 1 5 644.62 19.98 0 1 -5 662.50 19.58 0 -1 -5 650.48 19.51 0 1 6 68.77 4.36 0 1 -6 65.26 4.18 0 -1 6 71.35 4.46 0 1 7 31.67 3.38 0 -1 7 28.35 3.28 0 2 0 2907.01 75.73 0 -2 1 948.17 26.75 0 2 -1 1024.73 26.50 0 -2 -1 1007.62 26.54 0 2 1 1030.57 26.74 0 2 -1 1005.06 26.58 0 2 1 997.15 26.45 0 -2 2 134.07 4.20 0 2 -2 133.44 4.35 0 -2 2 136.22 4.65 0 2 2 132.93 4.07 0 2 2 131.93 4.62 0 -2 -2 136.74 4.31 0 -2 3 83.98 3.02 0 2 -3 75.79 3.27 0 2 3 83.99 2.87 0 -2 -3 83.13 3.31 0 -2 3 81.47 3.65 0 2 3 83.94 3.66 0 -2 4 913.27 26.77 0 -2 -4 958.58 26.27 0 2 4 967.08 26.87 0 2 -4 955.73 26.46 0 2 4 912.63 25.15 0 -2 4 936.78 25.31 0 2 -5 652.10 19.44 0 -2 -5 636.25 19.22 0 -2 5 637.29 19.81 0 2 5 645.54 19.69 0 2 6 26.73 2.79 0 2 -6 25.44 2.69 0 -2 6 23.55 2.75 0 2 7 52.59 4.16 0 -2 7 52.44 4.14 0 3 0 -0.03 0.14 0 3 1 1058.69 28.48 0 3 1 1070.25 28.20 0 -3 -1 1069.88 28.27 0 3 -1 1084.89 28.37 0 3 -1 1072.43 28.27 0 -3 -2 151.41 4.85 0 3 -2 157.11 4.96 0 3 2 160.47 5.21 0 -3 2 159.62 4.84 0 3 2 156.20 4.63 0 3 -3 7.99 1.05 0 -3 3 8.55 1.21 0 -3 3 10.00 0.97 0 3 3 8.48 1.18 0 -3 -3 9.83 1.09 0 3 3 7.97 0.74 0 3 -4 332.75 10.32 0 -3 4 302.51 10.45 0 -3 4 315.18 9.21 0 -3 -4 329.25 10.05 0 3 4 313.56 10.43 0 3 4 305.32 8.96 0 3 -5 6.51 1.75 0 -3 5 5.49 1.71 0 3 5 6.82 1.85 0 -3 -5 6.51 1.65 0 3 -6 75.04 4.47 0 -3 6 75.26 4.63 0 3 6 75.69 4.57 0 3 7 60.22 4.43 0 -3 7 51.75 4.16 0 4 0 564.85 14.88 0 4 -1 104.39 3.26 0 4 -1 105.75 3.18 0 4 1 101.77 3.07 0 -4 -1 109.17 3.14 0 4 1 111.50 3.35 0 4 2 36.29 1.91 0 4 -2 40.55 1.75 0 -4 -2 40.21 1.75 0 4 -2 38.39 1.81 0 4 2 37.36 1.49 0 4 -3 21.64 1.59 0 4 3 23.53 1.75 0 -4 3 19.44 1.34 0 4 3 20.35 1.14 0 -4 -3 21.45 1.48 0 4 -4 365.98 11.50 0 4 4 360.04 10.25 0 -4 4 366.76 10.60 0 -4 -4 361.84 11.25 0 4 4 364.83 11.71 0 4 5 433.36 14.43 0 4 -5 459.79 14.46 0 4 6 3.02 1.56 0 4 -6 3.08 1.55 0 -4 6 2.49 1.66 0 -4 7 51.05 4.19 0 4 7 59.53 4.35 0 5 0 1.37 0.31 0 5 0 -0.08 0.22 0 5 -1 1257.09 33.89 0 -5 -1 1279.00 33.72 0 5 1 1313.64 33.93 0 5 -1 1279.03 33.79 0 5 -2 1121.78 28.62 0 -5 -2 1067.16 28.34 0 5 2 1049.03 28.09 0 5 -2 1012.84 28.29 0 5 2 1063.07 28.71 0 -5 3 514.41 14.14 0 -5 -3 502.73 14.30 0 5 3 488.50 13.70 0 5 -3 484.31 14.52 0 5 3 525.23 14.76 0 5 4 441.19 13.22 0 5 4 415.47 11.68 0 -5 -4 433.18 12.76 0 5 -5 54.40 3.58 0 5 5 63.66 3.80 0 5 6 55.25 3.85 0 5 -6 49.17 3.73 0 5 7 42.10 3.72 0 -6 0 173.74 4.78 0 6 0 163.88 4.62 0 6 0 166.04 4.68 0 -6 -1 1033.73 26.75 0 -6 1 1005.47 27.15 0 6 1 1036.77 26.96 0 6 -1 972.31 26.85 0 6 -2 289.33 8.14 0 6 2 283.09 8.41 0 -6 -2 262.64 8.00 0 6 -2 294.37 8.39 0 6 2 280.83 7.86 0 6 3 532.81 15.48 0 6 3 516.81 14.47 0 6 -3 539.92 15.39 0 -6 -3 542.89 15.02 0 -6 -4 176.32 6.43 0 6 -4 186.02 6.76 0 6 4 188.34 6.92 0 6 4 188.35 5.66 0 6 -5 152.28 6.54 0 6 5 160.38 6.64 0 6 6 3.77 1.68 0 6 -6 3.58 1.62 0 6 -7 33.85 3.64 0 6 7 40.51 3.62 0 7 0 0.26 0.31 0 -7 0 0.12 0.42 0 7 0 -0.02 0.37 0 7 -1 246.47 7.29 0 7 1 247.68 7.37 0 -7 1 268.66 7.62 0 -7 -1 277.01 7.18 0 -7 -2 473.80 13.24 0 7 2 478.94 13.11 0 7 2 487.38 13.65 0 7 -2 497.48 13.68 0 -7 2 468.67 13.85 0 7 -2 486.89 13.39 0 -7 -3 23.81 1.51 0 -7 3 24.29 1.86 0 7 3 23.39 1.22 0 7 3 23.05 1.74 0 7 -3 24.38 1.53 0 7 -3 25.96 1.77 0 7 -4 18.50 1.80 0 7 4 19.81 1.83 0 7 4 17.43 1.20 0 7 -5 1.54 1.34 0 7 5 1.95 1.30 0 7 6 55.85 3.85 0 7 -6 62.87 4.29 0 7 -7 23.60 3.05 0 7 7 26.84 3.05 0 -8 0 1799.46 45.36 0 8 0 1659.89 45.19 0 8 0 1730.44 45.25 0 8 1 65.06 2.27 0 8 -1 61.38 2.21 0 -8 -1 67.66 2.06 0 -8 1 61.77 2.51 0 8 -2 218.85 6.80 0 -8 2 213.63 6.98 0 -8 -2 213.02 6.35 0 8 -2 221.26 6.61 0 8 2 239.13 6.85 0 8 2 213.44 6.28 0 8 -3 21.29 1.45 0 -8 3 18.50 1.68 0 8 3 22.14 1.67 0 8 3 21.23 1.18 0 8 -3 21.36 1.65 0 -8 -3 21.10 1.40 0 8 4 138.95 5.61 0 8 4 146.44 4.58 0 8 -4 143.12 5.73 0 -8 4 135.37 5.84 0 8 -5 35.16 2.85 0 -8 5 37.40 2.96 0 8 5 34.22 2.71 0 8 6 1.83 1.51 0 -8 6 2.90 1.75 0 8 -6 3.13 1.66 0 8 -7 24.78 3.18 0 8 7 29.30 3.09 0 -8 7 25.30 3.16 0 -9 0 -0.01 0.49 0 9 0 -0.01 0.43 0 9 0 0.02 0.36 0 9 1 62.14 2.25 0 -9 -1 66.50 2.02 0 9 -1 57.57 2.29 0 9 -1 59.88 2.20 0 -9 1 67.55 2.52 0 9 -2 424.33 11.87 0 9 2 428.12 12.00 0 -9 -2 429.57 11.60 0 9 2 407.49 11.53 0 -9 2 404.56 12.25 0 9 3 49.27 2.58 0 -9 3 47.46 2.77 0 -9 -3 52.13 2.24 0 9 -3 50.71 2.68 0 9 3 49.94 2.01 0 -9 4 77.27 4.08 0 9 4 83.57 3.93 0 9 4 81.14 2.95 0 9 -4 79.70 4.00 0 9 -5 26.41 2.55 0 -9 5 26.05 2.58 0 9 5 32.52 2.62 0 9 -6 17.28 2.52 0 -9 6 21.17 2.61 0 9 6 22.42 2.50 0 9 7 27.81 3.02 0 -9 7 27.28 3.26 0 9 -7 22.37 3.16 0 10 0 364.11 10.04 0 -10 0 375.32 10.24 0 10 0 356.40 9.99 0 10 -1 35.58 1.69 0 10 1 41.51 1.69 0 -10 -1 40.75 1.38 0 -10 1 39.03 1.83 0 10 -1 37.36 1.60 0 10 2 90.63 2.96 0 10 -2 84.88 3.21 0 -10 2 85.47 3.56 0 -10 -2 87.83 2.91 0 10 2 89.49 3.28 0 10 3 43.81 2.39 0 -10 3 48.31 2.78 0 -10 -3 47.69 2.07 0 10 3 44.32 1.90 0 10 -3 45.77 2.55 0 10 4 198.53 6.98 0 10 -4 191.37 7.20 0 -10 4 176.95 7.23 0 10 4 193.72 5.94 0 10 -5 134.59 6.16 0 10 5 133.13 5.86 0 10 5 144.14 4.63 0 -10 5 127.35 6.16 0 10 6 5.90 1.69 0 10 -6 3.62 1.76 0 -10 6 5.32 1.76 0 10 7 -0.09 1.62 0 -10 7 -0.10 1.72 0 10 -7 0.40 1.89 0 11 0 -0.14 0.47 0 11 0 0.13 0.38 0 -11 0 0.02 0.50 0 11 -1 294.42 8.74 0 -11 1 285.02 8.86 0 11 1 322.72 8.68 0 11 -1 304.07 8.62 0 -11 -1 303.00 8.29 0 -11 -2 83.55 2.73 0 11 -2 81.42 3.07 0 -11 2 76.78 3.39 0 11 2 78.23 2.77 0 11 2 81.72 3.10 0 -11 3 60.98 3.24 0 11 3 62.35 2.90 0 11 -3 62.71 3.11 0 11 3 60.46 2.37 0 -11 4 49.62 3.26 0 11 4 54.02 2.31 0 11 4 55.68 3.06 0 11 -4 56.28 3.32 0 -11 5 33.28 2.96 0 11 5 35.53 2.81 0 11 5 39.66 2.00 0 11 -5 32.21 3.00 0 -11 6 6.41 1.92 0 11 6 5.34 1.71 0 11 -6 6.39 1.97 0 11 7 5.55 1.87 0 -11 7 5.03 2.05 0 11 -7 2.25 2.10 0 12 0 174.66 5.24 0 -12 0 185.57 5.48 0 12 0 171.78 5.27 0 -12 1 254.56 7.51 0 12 -1 244.17 7.28 0 12 1 230.12 7.00 0 12 -1 239.91 7.16 0 12 1 265.29 7.24 0 12 2 16.93 1.07 0 12 -2 15.62 1.33 0 12 2 18.60 1.29 0 -12 2 18.35 1.54 0 12 -2 18.42 1.31 0 -12 -2 20.36 1.03 0 12 -3 14.92 1.53 0 12 3 13.40 1.33 0 -12 3 10.21 1.46 0 12 3 14.20 1.07 0 12 -4 100.01 4.73 0 12 4 99.71 3.56 0 12 4 95.76 4.31 0 -12 4 100.83 4.84 0 12 -5 163.74 7.01 0 12 5 153.83 6.50 0 -12 5 146.64 6.94 0 12 5 171.83 5.38 0 12 6 12.67 1.97 0 12 -6 10.70 2.26 0 -12 6 12.06 2.27 0 12 -7 0.73 1.81 0 12 7 0.25 1.65 0 -12 7 1.14 1.80 0 13 0 0.04 0.46 0 13 0 -0.22 0.51 0 -13 0 -0.14 0.60 0 -13 1 68.53 2.86 0 13 -1 69.78 2.71 0 13 1 70.70 2.46 0 13 1 77.01 2.65 0 13 1 66.00 2.48 0 13 -1 67.73 2.58 0 13 -2 138.23 4.62 0 13 2 134.79 4.54 0 -13 2 124.03 4.93 0 -13 -2 132.22 4.10 0 13 2 135.24 4.28 0 13 -2 131.29 4.80 0 13 3 63.77 2.54 0 -13 3 60.23 3.40 0 13 3 65.99 2.99 0 13 -4 191.04 7.51 0 13 4 198.96 6.14 0 -13 4 183.22 7.53 0 13 4 198.98 7.02 0 13 5 69.23 2.86 0 -13 5 64.07 4.19 0 13 5 61.41 3.64 0 13 -5 58.36 4.05 0 13 -6 35.06 3.52 0 -13 6 35.84 3.38 0 13 6 35.52 2.89 0 -13 7 7.58 2.25 0 13 7 9.23 2.04 0 13 -7 6.13 2.43 0 -14 0 962.36 25.13 0 14 0 902.34 24.84 0 14 0 918.86 24.90 0 14 1 57.94 2.22 0 14 1 52.30 2.12 0 14 -1 52.06 2.29 0 -14 1 47.40 2.38 0 14 1 53.03 2.06 0 14 -1 54.93 2.23 0 -14 2 54.49 2.81 0 14 -2 46.93 2.35 0 14 2 55.94 2.40 0 14 -2 53.88 2.63 0 14 2 53.09 2.20 0 -14 3 21.79 2.11 0 14 3 22.34 1.42 0 14 3 25.62 1.83 0 14 -4 166.82 6.69 0 14 4 163.74 5.23 0 -14 4 156.94 6.69 0 14 4 145.98 5.90 0 14 5 255.00 7.61 0 14 5 234.12 8.66 0 14 -5 231.69 9.38 0 -14 5 234.85 9.53 0 14 -6 0.75 1.83 0 14 6 0.14 1.33 0 -14 6 0.37 1.56 0 14 7 16.88 2.48 0 14 -7 12.02 2.95 0 -14 7 16.06 2.73 0 15 0 -0.69 0.80 0 -15 0 0.17 0.78 0 15 0 -0.38 0.67 0 15 -1 353.56 10.38 0 15 1 344.26 10.16 0 -15 1 358.25 10.78 0 15 1 364.90 10.25 0 15 -1 367.54 10.57 0 15 1 379.75 10.38 0 15 -2 22.34 1.68 0 15 -2 23.83 1.59 0 15 2 21.93 1.37 0 15 2 24.76 1.52 0 -15 2 23.79 1.86 0 -15 3 24.50 2.23 0 15 3 26.02 1.58 0 15 3 29.35 1.94 0 -15 4 103.46 5.17 0 15 -4 103.16 5.05 0 15 4 96.35 4.38 0 15 4 103.30 3.76 0 15 5 53.58 2.57 0 15 5 47.60 3.18 0 15 -5 47.94 3.68 0 -15 5 47.06 3.76 0 15 -6 22.66 3.10 0 -15 6 23.84 2.93 0 15 6 26.49 2.57 0 -15 7 12.09 2.58 0 15 -7 6.78 2.64 0 15 7 9.72 2.00 0 16 0 3136.13 82.33 0 -16 0 3132.87 82.63 0 16 0 3112.70 82.38 0 16 1 567.31 15.80 0 -16 1 591.71 16.42 0 16 -1 563.77 16.09 0 16 1 566.99 15.74 0 16 1 575.66 15.90 0 16 -1 570.25 15.96 0 16 2 58.69 2.52 0 16 -2 63.46 2.98 0 -16 2 63.21 3.22 0 16 -2 60.91 2.79 0 16 2 63.27 2.69 0 16 3 66.93 3.03 0 16 -3 63.66 3.45 0 16 3 62.30 2.67 0 -16 3 61.74 3.57 0 16 4 517.70 14.49 0 16 4 520.72 15.42 0 16 -4 489.72 16.06 0 -16 4 487.21 16.25 0 16 5 159.17 5.41 0 -16 5 146.35 7.13 0 16 -5 156.57 7.15 0 16 5 151.27 6.26 0 16 -6 8.90 2.38 0 -16 6 12.68 2.47 0 16 6 10.36 1.83 0 16 -7 1.49 2.16 0 -16 7 2.21 2.10 0 16 7 2.48 1.75 0 17 0 -0.17 0.89 0 17 0 -0.44 0.98 0 -17 0 1.51 1.01 0 17 -1 548.68 15.46 0 17 -1 554.30 15.58 0 17 1 540.89 15.17 0 -17 1 559.12 15.88 0 17 1 541.87 15.29 0 17 -2 142.00 5.11 0 17 -2 139.43 5.27 0 17 2 138.87 4.75 0 -17 2 147.98 5.69 0 17 2 149.46 4.97 0 17 3 57.69 2.81 0 17 3 53.29 2.47 0 -17 3 51.91 3.32 0 17 -3 56.85 3.23 0 17 4 12.59 1.69 0 17 4 12.14 1.46 0 -17 4 11.06 2.11 0 17 5 108.22 4.95 0 17 -5 108.01 5.69 0 -17 5 103.88 5.72 0 17 5 100.06 4.05 0 17 6 16.60 2.17 0 -17 6 17.68 2.77 0 17 -6 17.58 2.82 0 -17 7 37.42 3.99 0 18 0 3840.39 99.05 0 -18 0 3762.25 99.38 0 18 0 3681.89 99.04 0 18 1 538.33 15.39 0 18 -1 558.10 15.74 0 -18 -1 561.24 15.85 0 18 1 566.10 15.56 0 18 -1 562.93 15.86 0 -18 1 531.59 16.05 0 18 2 46.56 2.33 0 18 -2 45.77 2.63 0 18 -2 43.91 2.43 0 -18 2 45.16 2.85 0 18 2 43.15 2.14 0 18 -3 69.88 3.70 0 -18 3 56.93 3.55 0 18 3 61.36 2.78 0 18 3 67.72 3.11 0 18 4 578.94 17.33 0 -18 4 592.00 18.69 0 18 4 590.24 16.65 0 18 5 133.38 5.66 0 18 -5 131.49 6.49 0 -18 5 135.71 6.73 0 18 5 124.37 4.79 0 18 -6 13.69 2.73 0 -18 6 14.71 2.68 0 18 6 13.61 2.11 0 18 7 5.50 2.07 0 -19 0 -0.78 1.20 0 19 0 0.44 0.92 0 19 0 -0.56 1.06 0 19 -1 377.78 10.89 0 -19 -1 348.82 10.87 0 19 1 356.87 10.46 0 19 1 363.95 10.66 0 -19 2 118.24 4.98 0 19 -2 108.78 4.41 0 19 2 109.00 4.17 0 19 -2 116.26 4.66 0 19 3 88.83 3.61 0 19 -3 98.72 4.62 0 -19 3 98.13 4.73 0 19 3 89.42 3.85 0 -19 4 76.23 4.64 0 19 4 76.26 3.79 0 19 4 73.64 3.34 0 19 5 212.15 7.95 0 19 5 213.25 7.10 0 19 -5 220.36 9.14 0 -19 5 202.67 8.92 0 19 6 44.44 3.30 0 19 -6 36.81 3.97 0 -19 6 45.85 4.04 0 20 0 493.85 13.95 0 20 0 493.65 14.04 0 -20 0 461.50 14.24 0 -20 -1 123.21 4.71 0 20 1 130.22 4.56 0 20 1 126.20 4.39 0 20 -1 126.69 4.80 0 -20 1 125.89 5.03 0 20 -1 129.40 4.77 0 20 -2 16.23 1.63 0 -20 2 14.23 1.80 0 20 2 16.96 1.47 0 20 -2 15.35 1.75 0 20 -3 36.90 2.82 0 20 3 33.26 2.03 0 20 3 33.02 2.21 0 -20 3 34.53 2.81 0 -20 4 252.39 9.91 0 20 4 265.65 8.91 0 20 -4 275.18 10.05 0 20 4 260.15 8.32 0 20 5 198.52 6.77 0 20 5 200.94 7.55 0 -20 5 194.67 8.66 0 20 -6 6.63 2.54 0 20 6 11.03 2.06 0 -20 6 9.79 2.50 0 21 0 0.03 0.92 0 -21 0 -0.20 1.01 0 21 0 -0.67 0.89 0 21 -1 64.15 3.14 0 21 1 66.68 2.95 0 21 -1 65.60 3.15 0 -21 1 70.73 3.47 0 -21 -1 61.33 3.07 0 21 1 63.09 2.79 0 21 -2 371.58 11.33 0 21 -2 343.92 11.00 0 21 2 347.39 10.61 0 -21 2 345.85 11.55 0 21 3 276.40 9.06 0 -21 3 267.49 9.96 0 21 3 280.42 8.76 0 21 -3 298.60 10.09 0 21 -4 133.43 6.36 0 21 4 131.18 5.40 0 21 4 130.24 4.96 0 -21 4 136.28 6.49 0 21 5 23.53 2.13 0 -21 5 24.11 3.08 0 21 5 25.59 2.41 0 21 -6 104.32 6.59 0 21 6 102.31 5.16 0 -21 6 101.50 6.26 0 22 0 208.87 6.93 0 -22 0 203.64 7.13 0 22 0 199.42 6.68 0 22 -1 253.40 8.17 0 22 1 233.70 7.59 0 -22 -1 227.33 7.91 0 22 1 264.10 7.96 0 22 -1 248.66 8.12 0 -22 1 232.48 8.32 0 22 2 56.33 2.84 0 22 -2 62.57 3.41 0 22 -2 59.27 3.25 0 -22 2 57.12 3.55 0 22 3 198.17 6.66 0 22 -3 206.07 7.88 0 -22 3 183.90 7.72 0 22 3 195.82 6.95 0 22 4 34.59 2.32 0 -22 4 34.64 3.27 0 22 -4 37.10 3.30 0 22 4 38.12 2.70 0 22 5 95.74 4.76 0 -22 5 95.35 5.77 0 22 5 101.63 4.31 0 22 -6 22.34 3.53 0 -22 6 22.33 3.26 0 23 0 0.43 0.96 0 23 0 0.07 0.94 0 -23 0 0.04 1.11 0 23 1 337.09 10.24 0 23 -1 341.77 10.55 0 23 -1 332.50 10.45 0 -23 1 315.33 10.71 0 -23 -1 313.46 10.30 0 23 -2 451.14 14.13 0 23 -2 482.57 14.41 0 -23 2 442.61 14.51 0 23 3 97.73 4.12 0 23 -3 99.87 5.08 0 23 3 92.97 4.15 0 -23 3 85.57 4.80 0 23 4 27.62 2.13 0 23 -4 33.41 3.18 0 23 4 26.97 2.33 0 -23 4 28.97 3.08 0 -23 5 -0.09 1.83 0 23 5 -0.04 1.38 0 23 -5 0.69 1.94 0 23 -6 12.77 3.07 0 -23 6 15.10 2.94 0 24 0 143.04 5.34 0 -24 0 140.70 5.76 0 24 0 155.77 5.64 0 -24 1 41.77 2.89 0 24 -1 41.31 2.70 0 -24 -1 41.22 2.65 0 24 -1 40.77 2.64 0 24 1 38.69 2.47 0 -24 -2 44.66 2.77 0 24 -2 44.91 3.08 0 -24 2 45.31 3.23 0 24 -2 42.82 2.97 0 24 3 161.61 5.85 0 24 -3 161.30 6.97 0 24 3 148.18 5.80 0 -24 3 145.36 6.69 0 24 -4 114.03 6.06 0 24 4 109.08 4.68 0 -24 4 105.30 5.79 0 24 5 21.64 2.13 0 -24 5 19.92 2.94 0 24 -5 21.65 3.15 0 -24 6 47.49 4.56 0 25 0 0.35 1.08 0 25 0 0.04 1.05 0 -25 0 1.01 1.26 0 -25 -1 36.26 2.55 0 25 1 44.29 2.64 0 25 -1 40.67 2.80 0 -25 1 41.19 2.97 0 25 -1 42.22 2.73 0 -25 2 352.65 12.35 0 -25 -2 342.13 11.54 0 25 -2 398.56 12.31 0 25 -2 383.24 12.12 0 -25 3 79.50 4.64 0 25 -3 92.87 5.02 0 25 3 82.41 3.93 0 -25 4 15.28 2.47 0 25 4 11.39 1.81 0 25 -4 14.19 2.51 0 25 5 9.14 1.79 0 -25 5 9.86 2.59 0 25 -5 9.42 2.67 0 -25 6 81.06 5.91 0 -26 0 241.66 8.82 0 26 0 242.45 8.34 0 26 -1 136.56 5.54 0 -26 -1 109.61 4.98 0 -26 1 114.88 5.45 0 26 -1 131.49 5.34 0 26 1 124.74 5.13 0 -26 2 2.06 1.59 0 -26 -2 3.34 1.30 0 26 -2 2.02 1.47 0 26 -3 15.28 2.36 0 -26 3 12.22 2.20 0 26 3 14.66 1.83 0 -26 4 34.42 3.39 0 26 4 34.25 2.63 0 26 -4 36.43 3.63 0 26 -5 75.77 5.41 0 26 5 62.81 3.67 0 -26 5 64.63 4.93 0 -27 0 -0.34 1.49 0 27 0 -0.21 1.33 0 27 1 2.38 1.26 0 27 -1 3.09 1.33 0 -27 -1 1.72 1.18 0 -27 1 2.58 1.42 0 27 -1 2.50 1.39 0 -27 -2 59.52 3.39 0 27 -2 69.83 4.03 0 -27 2 64.87 4.08 0 27 3 44.42 2.91 0 27 -3 42.01 3.59 0 -27 3 38.35 3.37 0 -27 4 39.32 3.80 0 27 4 40.18 2.93 0 27 -4 43.86 4.03 0 27 -5 5.20 2.44 0 -27 5 5.73 2.38 0 27 5 4.33 1.70 0 28 0 227.12 8.05 0 -28 0 191.94 7.85 0 28 -1 4.31 1.48 0 28 1 4.51 1.48 0 28 -1 4.99 1.59 0 -28 1 3.79 1.47 0 -28 -1 2.85 1.35 0 28 -2 5.00 1.82 0 -28 2 4.01 1.77 0 28 2 5.97 1.55 0 -28 -2 5.00 1.43 0 28 3 31.70 2.62 0 -28 3 27.44 3.02 0 -28 4 43.91 3.95 0 28 -4 50.46 4.37 0 28 4 45.68 3.21 0 28 -5 34.13 4.12 0 -28 5 33.34 3.73 0 28 5 34.65 2.92 0 -29 0 0.43 1.41 0 29 0 0.42 1.52 0 29 -1 3.35 1.50 0 -29 1 4.03 1.64 0 -29 -1 3.59 1.43 0 29 -1 4.21 1.70 0 29 1 2.71 1.40 0 -29 2 54.22 3.93 0 29 2 60.04 3.50 0 29 -2 60.56 3.98 0 -29 3 30.86 3.15 0 29 -3 38.41 3.62 0 29 3 35.43 2.79 0 -29 -3 27.30 2.57 0 29 -4 2.59 2.22 0 -29 4 3.43 2.15 0 29 4 4.09 1.68 0 29 -5 5.49 2.82 0 29 5 4.46 1.85 0 -29 5 3.60 2.32 0 30 0 120.38 5.60 0 -30 0 109.00 5.43 0 30 -1 32.31 3.02 0 -30 1 28.04 2.85 0 30 1 33.06 2.80 0 -30 -1 24.86 2.47 0 30 -2 5.58 1.95 0 -30 -2 4.70 1.53 0 -30 2 4.23 1.94 0 30 2 6.58 1.73 0 30 3 25.69 2.59 0 -30 3 20.83 2.84 0 30 -3 29.49 3.40 0 30 4 62.97 3.97 0 -30 4 65.84 4.89 0 30 -4 70.29 5.46 0 -30 5 70.88 5.38 0 30 5 65.54 4.17 0 -31 0 0.47 1.76 0 31 0 -0.14 1.62 0 31 1 16.75 2.32 0 31 -1 17.11 2.56 0 -31 1 13.54 2.28 0 31 2 72.17 4.27 0 31 -2 75.95 4.79 0 -31 3 6.71 2.12 0 31 3 9.24 2.00 0 31 -3 8.49 2.50 0 31 4 11.28 2.21 0 31 -4 10.01 3.17 0 -31 4 9.77 2.63 0 32 0 313.55 11.32 0 32 -1 46.54 3.92 0 32 1 48.45 3.66 0 32 2 11.21 2.20 0 32 -2 13.73 2.56 0 32 3 15.66 2.36 0 32 -3 17.60 3.12 0 32 4 52.17 3.86 0 32 -4 66.54 5.51 0 33 0 -0.55 2.12 0 33 1 63.86 4.36 0 33 -1 69.35 4.81 0 33 2 49.49 3.78 0 33 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3 75.85 3.89 -1 22 -3 81.08 4.51 1 -22 3 84.43 4.77 1 22 3 78.37 3.69 1 22 4 183.51 6.68 1 22 4 183.18 7.21 1 -22 4 203.88 8.55 1 22 5 51.34 3.61 -1 22 -5 58.00 4.62 1 -22 6 2.70 2.39 -1 -23 6 42.18 4.05 1 23 -6 46.88 4.50 -1 23 6 46.35 2.97 -1 -23 5 58.22 4.40 -1 23 5 55.58 3.16 1 23 -5 64.05 4.58 -1 -23 4 7.85 1.95 1 23 -4 8.90 2.01 -1 23 4 7.21 1.48 -1 -23 3 192.75 8.11 1 23 -3 186.06 7.60 -1 -23 2 9.83 1.88 1 -23 -2 13.17 1.49 1 23 -2 15.80 2.01 1 23 -2 18.68 1.94 -1 23 2 13.05 1.63 -1 23 2 15.70 1.52 1 23 -1 379.34 11.73 -1 23 1 344.59 11.03 1 -23 -1 350.75 10.91 -1 23 1 351.13 10.65 -1 -23 1 355.32 11.70 1 23 -1 370.54 11.02 1 -23 0 489.86 14.83 1 23 0 527.10 15.30 -1 23 0 529.00 14.63 -1 23 0 488.85 15.03 -1 -23 0 461.18 15.00 -1 -23 -1 54.28 3.13 1 -23 1 55.64 3.31 -1 23 -1 62.06 2.99 -1 23 -1 56.55 3.22 1 23 2 9.36 1.49 -1 23 -2 8.84 1.71 1 23 2 8.60 1.39 1 -23 2 10.21 1.81 -1 23 -3 41.50 3.32 1 23 3 39.00 2.79 1 -23 3 42.82 3.45 1 23 3 40.56 2.59 1 23 4 102.95 4.65 1 23 4 100.15 4.97 -1 23 -5 23.46 3.39 1 -23 5 25.54 3.50 1 23 5 20.44 2.52 1 -23 6 13.88 3.06 -1 24 6 6.26 1.67 -1 -24 6 6.96 2.32 1 24 -6 5.41 2.32 -1 24 5 2.68 1.43 -1 -24 5 2.44 1.89 1 24 -5 2.83 2.06 1 24 -4 39.91 3.41 -1 24 4 37.43 2.48 -1 -24 4 31.91 3.17 -1 -24 3 79.17 4.76 1 24 -3 78.05 4.39 1 24 -3 89.43 4.68 1 -24 -2 188.85 6.82 -1 -24 2 195.82 7.95 1 24 -2 207.91 7.87 -1 24 2 207.17 6.87 -1 -24 1 16.08 2.09 1 -24 -1 12.54 1.62 -1 24 1 9.24 1.58 1 24 -1 14.93 1.97 1 24 -1 11.27 1.54 -1 24 1 10.53 1.40 -1 -24 0 45.94 2.95 -1 24 0 44.10 2.88 1 -24 0 44.31 2.79 -1 24 0 46.73 2.59 1 24 0 47.84 2.99 -1 -24 -1 50.52 3.04 -1 24 -1 51.25 3.12 -1 24 -1 58.51 3.00 1 -24 1 47.36 3.13 1 24 2 73.76 3.70 1 -24 2 78.49 4.28 -1 24 -2 83.88 4.40 1 24 2 81.34 3.94 1 24 3 4.99 1.42 1 -24 3 4.20 1.76 -1 24 -3 3.44 1.72 1 24 3 4.96 1.45 1 24 4 180.88 6.77 1 -24 4 183.57 8.24 1 24 4 168.26 7.00 1 24 5 132.15 6.16 -1 24 -5 139.57 7.69 1 -24 5 145.08 7.62 -1 -25 6 26.30 3.45 -1 25 6 26.89 2.45 1 25 -6 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394.06 11.20 2 4 -2 360.54 11.50 -2 4 2 381.95 11.53 2 4 -2 390.16 11.28 -2 4 2 372.13 10.60 2 4 -1 17.03 1.42 2 4 -1 15.59 1.10 -2 4 1 13.81 1.31 -2 -4 1 18.30 1.07 2 4 0 83.50 3.22 2 4 0 85.23 2.98 2 -4 0 89.98 2.93 2 -4 0 90.42 2.82 -2 4 0 87.65 3.08 2 4 0 88.38 2.65 2 4 1 1368.51 35.43 2 -4 1 1415.84 35.87 2 4 1 1334.01 35.72 -2 4 -1 1395.78 35.55 -2 4 -1 1282.57 34.82 -2 -4 -1 1324.08 35.00 2 4 2 455.19 12.57 2 -4 2 455.20 13.61 2 4 2 444.98 13.47 -2 4 -2 458.29 12.98 2 -4 3 35.55 2.57 2 4 3 34.56 2.49 -2 4 -3 35.46 2.20 2 4 4 42.98 3.06 2 -4 4 43.01 3.09 -2 4 -4 40.89 2.78 2 -4 5 71.29 4.46 2 4 5 75.23 4.46 2 -4 6 39.94 3.75 2 4 6 43.98 3.78 -2 -5 8 14.55 2.69 -2 5 8 13.92 2.50 2 5 -8 13.77 2.71 -2 -5 7 29.47 3.15 -2 5 7 36.64 3.21 2 5 -7 29.71 3.10 2 -5 -7 30.62 2.98 2 5 -6 379.96 13.04 -2 5 6 382.31 12.73 -2 -5 6 375.30 12.60 -2 5 6 380.70 11.98 2 -5 -6 368.34 12.51 -2 -5 6 349.86 12.76 -2 -5 5 407.84 13.72 -2 5 5 442.29 13.48 2 5 -5 405.00 13.70 -2 -5 5 438.19 13.93 2 -5 -5 441.95 13.56 -2 5 5 432.90 13.54 -2 -5 4 150.53 5.93 2 5 -4 145.93 5.93 -2 5 4 157.45 6.01 -2 5 4 168.89 5.79 2 -5 -4 152.75 5.76 -2 -5 3 2.49 0.86 -2 5 3 3.02 0.77 2 -5 -3 1.89 0.79 2 5 -3 3.23 1.12 -2 -5 2 213.99 6.65 -2 5 2 205.19 6.12 2 5 -2 212.28 7.17 2 -5 -2 223.71 6.70 2 5 -2 219.02 6.87 -2 5 2 208.66 7.01 -2 -5 1 121.07 3.89 -2 5 1 117.37 4.20 2 5 -1 113.66 3.92 2 5 0 80.67 3.07 2 -5 0 77.43 2.62 2 5 0 83.21 2.43 2 5 0 79.80 2.84 2 -5 0 77.20 2.74 -2 5 0 82.75 2.86 2 -5 1 63.30 2.64 2 5 1 56.92 2.51 -2 5 -1 58.60 2.41 -2 -5 -1 56.96 1.87 2 5 1 57.96 2.31 2 5 2 234.46 6.83 2 -5 2 225.03 7.70 2 5 2 227.16 7.57 -2 5 -2 233.58 7.22 2 -5 3 200.55 7.61 2 5 3 226.64 7.76 -2 5 -3 212.80 7.16 2 5 4 56.07 3.50 -2 5 -4 50.92 3.11 2 -5 4 50.73 3.37 2 -5 5 8.09 1.96 2 5 5 8.91 1.94 2 5 6 101.46 5.80 2 -5 6 114.62 6.15 -2 -6 8 3.88 2.17 2 6 -8 1.22 1.92 -2 6 8 4.90 1.98 2 6 -7 0.44 1.56 -2 6 7 0.40 1.60 -2 -6 7 0.93 1.61 -2 6 6 20.35 2.39 -2 -6 6 20.98 2.56 2 6 -6 23.67 2.70 -2 -6 6 25.07 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21.42 2.75 -2 7 7 25.26 2.72 2 7 -7 22.94 2.89 -2 7 6 192.63 7.51 2 7 -6 170.32 7.70 -2 -7 6 189.26 7.67 -2 -7 6 181.37 7.90 -2 7 6 194.16 6.99 2 -7 -6 193.34 7.56 2 7 -5 483.79 15.98 -2 -7 5 517.98 16.17 -2 7 5 513.78 15.56 -2 -7 5 518.14 16.20 -2 7 5 518.90 15.52 2 -7 -5 520.86 15.73 2 -7 -4 42.30 2.51 -2 -7 4 40.47 2.70 -2 7 4 40.98 2.36 2 7 -4 41.11 2.78 -2 7 4 41.19 2.57 -2 -7 3 55.43 2.87 2 7 -3 54.80 2.82 2 -7 -3 50.89 2.55 2 7 -3 52.87 2.98 -2 7 3 56.18 2.37 2 7 -2 586.29 15.80 2 7 -2 553.01 16.13 -2 7 2 546.77 14.82 -2 -7 2 541.59 15.62 -2 7 2 544.31 15.81 2 -7 -2 544.18 15.49 -2 -7 1 2636.96 70.23 2 7 -1 2675.80 70.17 2 -7 -1 2683.54 70.11 -2 7 1 2638.10 70.38 2 7 0 437.11 13.12 2 -7 0 462.43 12.67 2 7 0 459.94 12.96 2 7 0 457.78 12.30 -2 7 0 481.18 12.75 -2 7 0 472.56 13.10 2 7 1 258.83 7.89 2 7 1 264.49 7.72 -2 7 -1 251.79 7.79 2 -7 1 257.16 7.97 2 7 2 401.28 11.42 2 -7 2 406.20 12.35 -2 7 -2 405.39 11.84 2 -7 3 39.58 2.79 -2 7 -3 41.04 2.43 -2 7 -4 42.93 2.90 2 -7 4 39.79 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178.60 6.22 -2 11 -2 177.02 6.12 2 11 2 176.55 5.73 2 11 3 214.07 6.69 2 -11 3 204.69 7.77 2 11 3 221.87 7.70 -2 11 -3 208.61 7.43 2 -11 4 176.04 7.24 2 11 4 172.06 6.81 -2 11 -4 157.94 6.70 2 -11 5 2.19 1.79 2 11 5 0.07 1.62 -2 11 -5 -0.81 1.63 2 -11 6 70.46 5.04 2 11 6 63.20 4.47 2 12 -8 37.67 4.19 -2 -12 8 36.62 3.97 -2 12 7 8.08 1.42 2 12 -7 8.19 2.21 -2 -12 7 7.26 2.18 2 12 -6 5.23 1.90 -2 -12 6 4.55 1.88 -2 12 6 8.03 1.50 -2 -12 5 103.34 5.35 2 -12 -5 115.03 4.78 -2 12 5 101.51 4.40 -2 -12 4 163.09 6.61 2 12 -4 161.71 6.56 2 -12 -4 168.67 5.93 2 12 -4 175.93 6.81 -2 12 4 163.63 5.97 -2 -12 3 94.32 4.31 2 12 -3 97.03 4.29 2 12 -3 102.52 4.60 -2 12 3 95.08 3.92 2 -12 -3 100.25 3.83 -2 -12 2 14.05 1.48 2 12 -2 16.21 1.42 2 -12 -2 14.74 1.18 -2 12 2 15.56 1.27 2 12 -2 14.74 1.58 2 -12 -1 353.03 9.78 -2 -12 1 368.07 10.77 2 12 -1 368.12 10.34 2 -12 -1 357.30 10.33 -2 12 1 358.31 10.27 2 12 0 99.92 3.79 2 -12 0 109.81 3.29 2 12 0 97.08 3.55 -2 12 0 99.76 3.08 2 12 1 487.35 13.78 2 -12 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271.59 8.07 2 -14 -1 284.51 7.62 -2 14 1 259.98 7.89 2 -14 0 132.91 4.36 2 14 0 130.66 4.86 -2 14 0 126.81 4.02 2 14 1 942.87 25.66 2 -14 1 920.73 25.49 2 14 1 920.93 25.48 -2 14 -1 901.96 25.73 2 -14 2 267.60 9.13 2 14 2 281.14 8.54 2 14 2 279.68 8.94 -2 14 -2 268.13 8.97 2 14 3 3.81 0.96 -2 14 -3 3.91 1.29 2 -14 3 3.46 1.36 2 14 3 2.77 1.13 2 -14 4 21.09 2.55 2 14 4 17.81 2.17 -2 14 -4 21.94 2.38 -2 14 -5 67.88 4.59 2 -14 5 77.42 5.02 2 14 5 79.39 4.59 2 -14 6 9.85 2.95 -2 14 -6 7.03 2.61 2 14 6 5.93 2.43 2 15 -7 37.80 3.87 -2 15 7 35.32 2.47 -2 -15 7 36.91 3.80 -2 -15 6 27.29 3.06 -2 15 6 31.53 2.21 2 15 -5 5.17 1.65 -2 -15 5 6.68 1.76 -2 15 5 5.26 1.19 -2 -15 4 15.54 2.10 2 15 -4 16.90 2.10 2 15 -4 18.14 2.19 -2 15 4 17.26 1.63 2 -15 -4 18.49 1.59 -2 -15 3 425.81 13.45 2 -15 -3 434.22 12.43 2 15 -3 447.68 13.32 2 15 -3 402.82 13.39 -2 15 3 410.11 12.45 2 15 -2 409.07 11.95 2 15 -2 385.60 12.47 -2 -15 2 386.11 12.23 2 -15 -2 421.24 11.07 -2 15 2 372.45 11.47 2 -15 -2 396.47 11.55 2 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19.01 1.38 2 16 -2 17.67 1.57 -2 -16 2 16.03 1.72 2 16 -2 17.54 1.83 -2 16 2 16.99 1.33 2 -16 -1 55.44 2.17 2 16 -1 57.03 2.49 2 16 -1 58.94 3.10 -2 16 1 56.11 2.36 2 16 0 104.99 4.40 -2 16 0 108.17 4.46 -2 16 0 105.68 3.57 2 16 1 175.98 6.26 2 -16 1 192.09 6.38 2 16 1 182.01 6.29 2 16 2 147.38 5.26 2 -16 2 144.79 5.78 2 16 2 146.33 5.59 -2 16 -2 140.54 5.67 2 16 3 79.95 3.52 2 -16 3 89.12 4.49 2 16 3 79.82 3.94 -2 16 -3 79.28 4.16 2 -16 4 44.01 3.58 2 16 4 41.03 3.02 -2 16 -4 37.47 3.26 2 16 5 33.92 3.07 -2 16 -5 41.43 3.55 2 -16 5 44.36 3.98 2 -16 6 17.75 3.22 -2 16 -6 8.02 2.55 -2 -17 7 82.88 5.54 -2 17 7 78.71 3.90 -2 -17 6 40.22 3.77 2 17 -6 42.76 3.76 -2 17 6 41.32 2.56 -2 -17 5 160.73 7.31 2 17 -5 171.36 7.52 -2 17 5 166.22 6.00 2 -17 -4 34.81 2.14 2 17 -4 38.52 3.02 2 17 -4 37.59 3.04 -2 17 4 33.98 2.24 2 17 -3 1483.11 41.07 2 -17 -3 1440.27 39.63 2 17 -3 1493.93 40.72 -2 17 3 1486.42 39.76 2 17 -2 320.60 11.04 2 -17 -2 352.32 10.10 2 17 -2 345.79 10.53 -2 17 2 331.93 10.04 2 17 -1 166.31 6.28 2 17 -1 170.60 5.46 -2 17 1 165.73 5.97 -2 17 1 163.14 5.28 -2 17 0 60.00 3.17 -2 17 0 61.48 2.43 2 17 0 63.70 3.21 2 17 1 496.42 14.98 2 17 1 494.47 14.95 2 17 2 119.17 4.73 2 17 2 119.42 4.95 -2 17 -2 126.41 5.21 2 17 3 64.21 3.11 2 -17 3 68.08 4.00 2 17 3 62.69 3.49 -2 17 -3 65.15 3.79 2 -17 4 163.52 7.30 2 17 4 152.66 6.39 -2 17 -4 148.90 6.78 2 -17 5 14.47 2.73 -2 17 -5 12.87 2.46 2 17 5 13.73 2.14 2 -17 6 25.74 3.58 -2 18 7 4.15 1.61 2 18 -6 27.85 3.21 -2 18 6 30.54 2.25 2 18 -5 27.00 2.96 -2 18 5 25.23 2.05 2 18 -4 72.75 4.23 -2 18 4 69.09 3.23 2 18 -4 71.50 4.16 2 18 -3 17.87 2.00 2 18 -3 19.98 2.27 2 -18 -3 16.10 1.47 -2 18 3 17.61 1.60 2 18 -2 30.38 2.45 2 18 -2 29.97 2.06 2 -18 -2 30.17 1.78 -2 18 2 27.46 1.74 2 18 -1 25.82 2.12 2 18 -1 26.99 1.61 -2 18 1 24.15 1.95 -2 18 1 24.64 1.52 2 18 0 81.40 3.80 -2 18 0 84.40 3.89 -2 18 0 79.57 2.99 2 18 1 167.25 6.13 2 18 1 162.33 6.04 2 18 2 126.45 4.89 2 18 2 122.39 5.07 2 -18 2 132.67 5.48 -2 18 -2 123.13 5.31 2 18 3 56.27 3.00 2 -18 3 61.95 3.86 2 18 3 54.43 3.29 -2 18 -3 55.63 3.65 2 -18 4 24.16 2.85 2 18 4 17.40 2.17 -2 18 -4 21.35 2.59 2 -18 5 11.21 2.61 2 18 5 6.20 1.75 -2 18 -5 7.33 2.13 -2 19 7 53.49 3.15 2 19 -6 28.38 3.32 -2 19 6 29.94 2.31 -2 19 5 7.07 1.37 2 19 -5 9.10 2.10 2 19 -4 124.60 5.80 2 19 -4 126.47 5.91 2 19 -3 190.82 7.08 2 19 -3 187.05 7.38 2 -19 -3 184.20 6.15 -2 19 3 181.27 6.22 2 19 -2 37.42 2.75 2 -19 -2 33.12 1.96 2 19 -2 36.94 2.27 -2 19 2 34.80 1.95 2 19 -1 127.16 5.23 -2 19 1 116.61 4.80 -2 19 1 117.85 4.14 2 19 0 30.83 2.32 -2 -19 0 27.50 2.14 -2 19 0 34.79 2.47 -2 19 0 33.08 1.72 2 19 1 103.33 4.46 2 19 1 104.67 4.35 -2 19 -1 103.30 4.67 2 -19 2 71.44 3.80 2 19 2 67.42 3.53 2 19 2 64.86 3.29 -2 19 -2 66.08 3.72 2 19 3 130.18 5.29 2 -19 3 148.03 6.37 2 19 3 134.51 5.66 -2 19 -3 140.36 6.18 2 19 4 24.74 2.48 2 -19 4 28.18 3.15 -2 19 -4 26.78 2.88 2 19 5 4.51 1.69 -2 19 -5 2.64 1.99 2 20 -7 37.00 4.12 -2 20 7 33.86 2.64 2 20 -6 29.25 3.41 -2 20 6 32.32 2.41 2 20 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148.04 5.97 -2 21 1 156.33 5.22 -2 -21 0 53.21 3.02 -2 21 0 53.05 3.18 -2 21 0 52.62 2.40 2 21 1 85.79 4.13 2 21 1 83.54 3.88 -2 21 -1 87.42 4.37 2 21 2 40.19 2.62 2 21 2 33.39 2.53 2 21 3 24.99 2.36 2 21 3 26.16 2.23 -2 21 -3 26.58 2.82 2 21 4 37.29 3.02 -2 21 -4 42.10 3.69 2 21 5 5.60 1.83 -2 21 -5 7.36 2.29 -2 22 7 15.80 2.15 -2 -22 6 33.86 3.77 2 22 -6 37.21 4.00 -2 22 6 34.37 2.65 -2 -22 5 164.96 7.92 2 22 -5 174.91 8.06 -2 22 5 173.06 6.35 -2 -22 4 150.95 7.31 2 22 -4 169.79 7.24 2 22 -4 171.52 7.19 -2 -22 3 22.63 2.50 2 22 -3 25.54 2.32 2 22 -3 26.81 2.68 -2 22 3 23.78 1.81 -2 -22 2 10.10 1.82 2 22 -2 10.94 1.85 -2 22 2 11.53 1.65 2 22 -2 10.01 1.45 -2 22 2 12.30 1.32 -2 -22 1 112.83 4.99 2 22 -1 118.30 5.28 -2 22 1 105.83 4.83 -2 22 1 110.42 4.11 -2 -22 0 72.00 3.73 -2 22 0 73.81 3.90 -2 22 0 76.51 3.11 -2 22 -1 172.67 6.83 2 22 1 170.81 6.58 -2 -22 -1 157.19 6.51 2 22 2 28.97 2.38 2 22 2 28.51 2.37 2 22 3 11.06 1.69 2 22 3 8.84 1.71 -2 22 -3 12.12 2.20 -2 22 -4 2.01 1.93 2 22 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24 -2 5.57 1.75 -2 24 2 4.07 1.10 -2 24 2 2.90 1.36 -2 -24 1 306.47 10.59 2 24 -1 324.54 10.98 -2 24 1 292.15 10.22 -2 24 1 308.93 9.41 -2 -24 0 229.55 8.51 -2 24 0 233.72 8.57 -2 24 0 240.18 7.59 -2 -24 -1 11.71 1.80 2 24 1 11.53 1.83 -2 24 -1 12.30 1.99 -2 24 -2 0.64 1.62 2 24 2 1.30 1.41 2 24 2 1.64 1.25 2 24 3 22.23 2.37 2 24 3 20.99 2.32 2 24 4 41.28 3.33 -2 24 -4 46.35 4.18 -2 -25 6 20.94 3.20 2 25 -6 25.27 3.48 -2 25 6 25.36 2.35 -2 -25 5 92.42 5.97 -2 25 5 100.88 4.52 -2 -25 4 2.40 1.76 2 25 -4 0.97 1.69 2 25 -4 1.83 1.64 -2 -25 3 93.49 5.37 2 25 -3 105.33 4.96 2 25 -3 95.08 5.27 -2 25 3 92.54 4.01 -2 -25 2 68.44 4.22 2 25 -2 73.53 4.54 -2 25 2 67.24 3.78 -2 25 2 75.62 3.35 -2 -25 1 250.01 9.25 2 25 -1 269.71 9.71 -2 25 1 243.71 8.91 -2 25 1 254.72 8.09 -2 -25 0 93.67 4.72 -2 25 0 99.76 4.87 2 25 1 61.46 3.73 -2 25 -1 54.73 3.68 2 25 2 99.63 4.85 2 25 2 82.46 4.36 -2 25 -2 96.04 5.22 2 25 3 44.44 3.23 2 25 3 44.03 3.21 -2 25 -4 -1.28 2.33 2 25 4 2.71 1.74 -2 26 6 1.91 1.59 2 26 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4.05 1.54 -2 27 -1 4.54 1.80 2 27 1 4.33 1.74 2 27 2 46.17 3.48 -2 -27 -2 41.06 3.37 -2 27 -2 46.78 3.84 2 27 3 74.62 4.37 -2 27 -3 71.07 4.97 2 27 4 33.20 3.10 2 28 -6 50.72 4.99 -2 -28 5 5.86 2.34 -2 28 5 2.22 1.58 2 28 -5 4.13 2.46 -2 -28 4 58.68 4.65 2 28 -4 59.00 4.43 -2 28 4 57.47 3.38 -2 -28 3 1.32 1.75 2 28 -3 0.64 1.67 -2 28 3 0.77 1.20 -2 -28 2 7.62 2.13 2 28 -2 11.43 2.43 -2 28 2 9.41 1.54 -2 28 2 8.62 1.90 -2 28 1 9.46 2.07 2 28 -1 12.35 2.50 -2 -28 1 9.65 2.20 -2 28 1 13.79 1.81 -2 -28 0 11.73 2.06 -2 28 0 15.39 2.32 -2 -28 -1 4.95 1.61 -2 28 -1 4.84 1.76 2 28 1 3.67 1.80 2 28 2 59.37 4.09 -2 28 -2 68.56 4.64 2 28 3 22.84 2.84 2 28 3 18.13 2.40 -2 28 -3 19.81 3.25 2 28 4 39.99 3.50 -2 -29 5 64.92 5.13 -2 29 5 62.84 3.75 -2 29 4 4.24 1.61 -2 -29 4 2.87 2.10 2 29 -4 3.64 2.09 -2 -29 3 65.68 4.76 2 29 -3 67.70 4.77 -2 29 3 60.03 3.39 -2 -29 2 21.07 2.79 -2 29 2 26.12 2.17 -2 -29 1 146.84 7.08 2 29 -1 180.32 7.93 -2 29 1 151.60 6.77 -2 29 1 171.76 6.27 2 29 0 64.20 4.49 -2 -29 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2.32 -4 3 3 23.26 2.44 4 -3 -3 23.44 1.92 -4 -3 2 127.28 4.44 4 -3 -2 122.29 4.56 4 3 -2 111.36 5.38 -4 3 2 103.72 5.12 4 3 -2 111.62 4.49 4 -3 -1 230.78 6.98 4 3 -1 224.22 8.15 4 3 -1 219.65 6.79 -4 3 1 208.79 7.69 -4 -3 1 212.64 6.95 4 -3 0 330.78 9.90 4 3 0 348.41 10.27 -4 3 0 364.90 10.54 4 -3 1 157.89 5.40 4 3 1 155.67 5.52 -4 3 -1 151.40 5.34 4 -3 2 20.67 1.92 4 3 2 18.42 1.94 4 -3 3 65.71 3.61 4 3 3 58.31 3.59 4 -3 4 75.34 4.28 4 3 4 77.14 4.42 4 -3 5 97.21 5.32 4 3 5 103.91 5.58 4 -4 -8 149.63 7.22 -4 -4 8 141.25 7.33 -4 4 8 146.21 6.98 4 4 -8 131.47 7.11 4 -4 -7 42.00 3.43 -4 -4 7 42.16 3.84 -4 4 7 44.16 3.71 4 4 -7 37.22 3.47 4 -4 -6 18.71 2.29 -4 -4 6 17.49 2.19 -4 4 6 15.43 2.49 -4 -4 6 13.47 2.37 -4 -4 5 12.91 1.81 4 -4 -5 15.30 1.94 -4 -4 5 14.54 2.56 4 4 -5 15.89 2.12 4 4 -4 205.23 7.73 -4 -4 4 193.24 7.12 -4 4 4 209.87 8.37 -4 -4 3 80.82 3.53 4 4 -3 81.93 3.97 4 4 -3 77.67 4.49 -4 4 3 85.51 4.54 4 -4 -3 81.72 3.78 -4 -4 2 9.56 1.22 4 -4 -2 9.28 1.19 4 4 -2 7.71 1.71 4 4 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4 5 0 400.41 12.58 4 5 0 388.33 11.68 -4 5 0 408.34 11.99 4 -5 1 116.79 4.25 4 5 1 112.35 4.47 -4 5 -1 110.44 4.42 4 -5 2 92.51 4.07 4 5 2 90.30 4.17 4 -5 3 31.07 2.56 4 5 3 29.63 2.58 4 -5 4 31.18 2.80 4 5 4 32.43 2.97 4 -6 -8 172.59 7.96 -4 -6 8 154.13 7.92 -4 6 8 177.83 7.69 4 6 -8 164.26 8.19 -4 -6 7 9.22 2.06 4 -6 -7 11.72 2.11 -4 -6 7 10.40 2.47 4 6 -7 7.74 2.07 -4 6 7 10.08 2.20 -4 -6 6 3.29 1.51 -4 -6 6 3.47 1.87 4 -6 -6 4.48 1.56 4 6 -6 1.52 1.43 -4 6 6 3.51 1.67 -4 -6 5 17.74 2.06 4 -6 -5 19.78 2.21 -4 -6 5 18.11 2.79 4 6 -5 14.79 2.11 -4 -6 4 612.04 18.36 4 6 -4 584.03 19.41 4 -6 -4 613.27 18.33 -4 6 4 628.24 19.30 4 6 -4 622.38 18.72 -4 -6 3 424.64 12.90 4 6 -3 423.28 13.24 -4 6 3 423.14 13.85 -4 -6 2 2.76 0.96 4 6 -2 5.15 1.49 4 -6 -2 3.47 0.87 4 6 -2 2.89 0.94 -4 6 2 4.32 1.35 -4 -6 1 52.77 2.69 4 6 -1 61.00 2.44 4 6 -1 59.54 3.46 4 -6 -1 53.27 2.53 -4 6 1 62.87 3.22 4 6 0 438.84 13.63 4 6 0 440.75 12.76 -4 6 0 428.66 12.99 4 6 1 428.34 12.70 -4 6 -1 415.42 12.64 4 6 2 13.36 1.68 4 6 3 62.21 3.71 4 6 4 53.62 3.78 4 -7 -8 57.85 4.48 -4 -7 8 52.38 4.58 -4 7 8 59.70 4.29 4 7 -8 48.26 4.51 4 -7 -7 13.92 2.20 -4 -7 7 12.68 2.35 -4 -7 7 15.84 2.72 -4 7 7 13.01 2.28 -4 -7 6 4.81 1.57 -4 -7 6 2.55 1.85 4 7 -6 4.30 1.66 -4 7 6 4.41 1.77 4 -7 -6 6.27 1.64 -4 -7 5 361.05 12.31 4 -7 -5 383.25 12.49 4 7 -5 368.93 12.82 -4 -7 4 342.45 11.26 4 7 -4 334.05 12.33 4 -7 -4 342.84 11.19 -4 7 4 348.70 12.06 4 7 -4 328.92 11.43 4 7 -3 429.11 13.60 -4 -7 3 452.66 13.46 -4 7 3 437.43 14.24 -4 -7 2 30.85 2.14 4 7 -2 29.53 2.67 4 7 -2 34.43 2.13 4 -7 -2 33.91 2.05 -4 7 2 33.80 2.53 -4 -7 1 62.27 2.97 4 7 -1 64.36 2.57 4 7 -1 63.02 3.60 4 -7 -1 63.13 2.81 -4 7 1 68.30 3.40 4 7 0 74.53 3.87 4 7 0 68.22 3.14 -4 7 0 77.61 3.53 4 7 1 185.42 6.44 -4 7 -1 178.93 6.40 4 7 2 51.78 2.97 -4 7 -2 42.54 2.67 4 7 3 70.79 4.00 4 7 4 18.54 2.39 -4 -8 8 234.98 10.70 4 -8 -8 270.74 10.68 -4 8 8 274.09 10.28 4 8 -8 260.93 11.05 -4 -8 7 57.22 4.17 4 -8 -7 58.53 4.03 -4 -8 7 56.36 4.46 -4 8 7 49.43 3.83 -4 -8 6 38.14 3.12 4 -8 -6 36.46 3.00 -4 -8 6 36.00 3.59 -4 8 6 37.32 3.21 4 8 -6 31.47 3.08 -4 -8 5 109.71 5.27 4 -8 -5 111.36 5.18 4 8 -5 105.63 5.90 4 8 -5 110.63 5.56 -4 -8 4 2529.47 67.58 4 8 -4 2357.37 68.84 4 -8 -4 2501.18 67.43 -4 8 4 2573.76 68.48 4 8 -4 2499.58 67.83 4 8 -3 1047.59 29.65 -4 -8 3 1045.85 29.51 -4 8 3 1073.11 30.40 -4 -8 2 45.85 2.67 4 8 -2 54.70 2.75 4 8 -2 46.02 3.28 4 -8 -2 47.40 2.50 -4 8 2 55.04 3.20 -4 -8 1 1.30 0.86 4 -8 -1 1.09 0.71 4 8 -1 1.81 0.65 4 8 -1 1.30 1.27 -4 8 1 2.11 1.13 4 8 0 799.36 23.22 4 8 0 804.65 22.35 -4 8 0 794.90 22.74 4 8 1 187.30 6.61 -4 8 -1 187.05 6.64 -4 8 -2 5.18 1.24 4 8 2 6.01 1.35 4 8 3 71.93 3.98 4 8 4 12.11 2.14 4 -9 -8 7.45 2.52 -4 -9 8 5.62 2.65 -4 9 8 10.57 2.82 4 9 -8 3.95 2.56 -4 -9 7 29.35 3.24 4 -9 -7 35.77 3.19 -4 -9 7 29.74 3.48 -4 9 7 32.84 3.11 -4 -9 6 6.66 1.80 4 -9 -6 8.75 1.76 -4 -9 6 6.23 2.11 4 9 -6 9.45 2.00 -4 9 6 10.28 1.96 -4 -9 5 92.27 4.88 4 9 -5 102.37 5.70 4 -9 -5 90.50 4.58 4 9 -5 96.19 5.08 -4 -9 4 46.60 3.31 4 9 -4 48.98 4.08 -4 9 4 47.34 3.51 4 -9 -4 50.49 3.11 4 9 -4 43.07 3.25 4 -9 -3 323.47 10.50 -4 9 3 332.82 11.24 -4 -9 3 344.52 10.80 4 9 -3 332.15 10.80 -4 -9 2 110.21 4.59 4 9 -2 119.88 4.58 4 9 -2 106.56 5.32 -4 9 2 115.20 4.94 -4 -9 1 48.97 2.71 4 -9 -1 54.72 2.59 4 9 -1 58.60 3.48 4 9 0 25.90 2.33 4 9 0 24.24 1.82 -4 9 0 22.45 2.07 4 9 1 401.96 12.14 -4 9 -1 382.90 12.17 4 9 2 28.26 2.26 -4 9 -2 25.33 2.13 4 9 3 20.44 2.25 4 9 4 12.66 2.21 -4 -10 8 169.77 8.61 4 -10 -8 193.22 8.46 4 10 -8 158.70 8.43 -4 10 8 183.63 7.83 -4 -10 7 73.69 4.96 4 -10 -7 80.31 4.70 -4 -10 7 72.22 5.21 4 10 -7 75.64 5.04 -4 10 7 77.10 4.66 -4 -10 6 8.35 1.95 4 -10 -6 9.47 1.77 4 10 -6 8.75 2.01 -4 -10 6 9.45 2.46 -4 10 6 9.73 1.92 -4 -10 5 129.89 6.05 4 10 -5 124.34 6.65 4 -10 -5 142.91 5.89 4 10 -5 127.68 6.12 -4 -10 4 669.88 20.12 4 10 -4 694.72 21.53 -4 10 4 670.21 20.39 4 10 -4 648.05 20.15 4 -10 -4 675.33 19.75 -4 -10 3 748.24 21.44 4 -10 -3 721.61 21.07 -4 10 3 724.55 21.71 4 10 -3 751.93 21.42 -4 -10 2 41.51 2.64 4 10 -2 46.13 2.55 4 10 -2 47.11 3.39 -4 10 2 49.49 2.92 -4 -10 1 12.14 1.44 4 -10 -1 12.78 1.29 4 10 -1 15.47 1.98 4 10 0 239.52 8.65 4 10 0 246.44 7.99 -4 10 0 250.18 8.49 4 10 1 203.95 7.16 -4 10 -1 204.33 7.30 4 10 2 16.76 1.87 -4 10 -2 16.41 1.84 4 10 3 15.19 2.03 4 10 4 102.04 5.33 -4 -11 8 106.61 6.70 -4 11 8 107.38 5.73 -4 -11 7 26.17 3.15 4 -11 -7 31.46 2.97 -4 -11 7 28.43 3.48 4 11 -7 25.93 3.16 -4 11 7 32.17 3.02 -4 -11 6 3.49 1.81 4 11 -6 3.57 1.74 4 -11 -6 5.23 1.54 -4 11 6 4.87 1.61 -4 -11 5 28.60 2.76 4 11 -5 29.01 3.28 4 -11 -5 29.02 2.43 4 11 -5 26.71 2.65 -4 11 5 27.95 2.67 -4 -11 4 258.64 9.17 4 11 -4 257.16 10.17 -4 11 4 260.12 9.26 4 11 -4 246.27 9.05 4 -11 -4 241.32 8.61 -4 -11 3 133.54 5.50 4 -11 -3 129.42 5.10 -4 11 3 126.45 5.55 4 11 -3 132.19 5.36 4 11 -2 80.04 3.47 4 11 -2 80.05 4.42 -4 11 2 78.55 3.73 -4 -11 1 24.83 1.97 4 11 -1 27.65 2.45 4 -11 -1 29.90 1.93 4 11 0 34.66 2.67 4 11 0 32.42 2.17 -4 11 0 31.17 2.47 4 11 1 78.85 4.13 4 11 1 76.64 3.78 -4 11 -1 77.56 3.91 4 11 2 63.93 3.51 -4 11 -2 61.27 3.42 4 11 3 129.39 5.79 4 11 4 21.94 2.71 -4 -12 8 138.98 7.81 -4 12 8 146.62 6.66 -4 -12 7 12.46 2.57 4 12 -7 12.29 2.49 4 -12 -7 11.97 2.11 -4 -12 7 9.79 2.71 -4 12 7 13.36 2.30 -4 -12 6 42.83 3.66 4 12 -6 40.41 3.93 4 -12 -6 41.23 3.13 4 12 -6 37.54 3.44 -4 12 6 43.56 3.34 -4 -12 5 25.23 2.65 4 12 -5 24.04 3.08 4 12 -5 20.87 2.46 -4 12 5 27.27 2.57 4 -12 -5 23.59 2.24 -4 -12 4 235.03 8.74 4 12 -4 238.98 9.65 -4 12 4 229.92 8.55 4 12 -4 223.35 8.52 4 -12 -4 232.28 8.12 -4 -12 3 92.56 4.46 4 -12 -3 94.28 4.08 -4 12 3 91.90 4.38 4 12 -3 90.00 4.21 4 -12 -2 87.64 3.69 -4 -12 2 80.24 4.02 4 12 -2 90.40 3.75 4 12 -2 81.70 4.62 -4 12 2 88.93 4.00 -4 -12 1 35.41 2.36 4 12 -1 34.41 2.77 4 -12 -1 37.67 2.21 4 12 0 231.22 8.26 4 12 0 213.34 7.38 -4 12 0 220.31 7.91 4 12 1 295.42 10.12 4 12 1 311.62 9.80 4 12 2 62.02 3.52 -4 12 -2 59.78 3.48 4 12 3 33.04 2.79 -4 12 -3 26.55 2.56 4 12 4 144.34 6.62 -4 -13 8 11.16 3.04 4 13 -8 12.18 2.98 -4 13 8 17.16 2.53 -4 -13 7 121.64 6.76 4 -13 -7 126.37 6.09 -4 -13 7 120.73 7.10 4 13 -7 110.13 6.48 -4 13 7 128.61 6.05 -4 -13 6 169.70 7.86 4 13 -6 173.83 8.31 4 -13 -6 173.60 7.06 4 13 -6 158.95 7.54 -4 13 6 174.44 7.32 -4 -13 5 127.25 6.27 4 13 -5 141.01 7.11 4 13 -5 120.39 6.03 -4 13 5 130.46 5.91 4 -13 -5 135.45 5.67 4 -13 -4 128.54 5.39 -4 -13 4 140.92 6.09 4 13 -4 130.00 6.59 4 13 -4 124.67 5.67 -4 13 4 133.13 5.75 -4 -13 3 1.86 1.39 4 -13 -3 1.78 0.99 -4 13 3 3.12 1.31 4 13 -3 2.54 1.20 -4 -13 2 299.44 9.99 4 -13 -2 293.35 9.44 4 13 -2 288.88 10.71 -4 13 2 317.47 9.82 -4 -13 1 156.30 5.94 4 13 -1 165.88 6.78 4 13 0 482.66 14.95 4 13 0 464.04 14.04 -4 13 0 465.28 14.58 4 13 1 230.51 8.43 4 13 1 231.58 7.99 -4 13 -1 215.46 8.13 4 13 2 58.10 3.43 -4 13 -2 53.67 3.41 4 13 3 40.69 3.11 -4 13 -3 37.03 3.00 4 13 4 13.79 2.41 -4 -14 8 67.98 5.34 -4 14 8 67.57 4.16 -4 -14 7 25.01 3.30 -4 -14 7 22.91 3.52 4 -14 -7 28.86 2.86 4 14 -7 27.00 3.26 -4 14 7 25.64 2.79 -4 -14 6 0.62 1.81 4 14 -6 3.81 2.31 4 14 -6 1.09 1.64 4 -14 -6 2.38 1.54 -4 14 6 2.06 1.61 4 -14 -5 2.73 1.30 -4 -14 5 3.85 1.79 4 14 -5 3.46 2.17 4 14 -5 3.47 1.53 -4 14 5 4.78 1.58 -4 -14 4 54.58 3.72 4 -14 -4 54.91 3.15 4 14 -4 60.41 4.39 4 14 -4 56.51 3.47 -4 14 4 62.05 3.57 -4 -14 3 451.17 14.71 4 14 -3 452.96 15.68 4 -14 -3 467.82 13.96 -4 14 3 486.35 14.47 4 14 -3 453.24 14.21 -4 -14 2 80.75 4.13 4 14 -2 86.83 4.76 4 -14 -2 83.74 3.70 -4 14 2 94.20 4.03 -4 -14 1 297.37 10.01 4 14 -1 309.76 10.93 -4 14 1 327.10 10.47 4 14 0 34.65 2.86 4 14 0 32.50 2.36 -4 14 0 33.30 2.71 4 14 1 258.61 9.40 4 14 1 259.92 8.93 -4 14 -1 262.12 9.27 -4 14 -2 4.15 1.46 4 14 2 5.36 1.50 4 14 3 72.61 4.24 -4 14 -3 74.11 4.27 4 14 4 0.89 1.57 -4 15 8 2.80 1.82 -4 -15 7 28.40 3.56 -4 -15 7 25.47 3.59 4 15 -7 28.95 3.43 4 -15 -7 27.19 2.78 -4 15 7 27.41 2.69 -4 -15 6 125.70 6.77 4 15 -6 143.54 7.55 4 15 -6 118.64 6.47 -4 15 6 135.69 6.11 4 -15 -6 140.07 6.02 -4 -15 5 117.73 6.31 4 15 -5 128.42 6.90 4 15 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37.77 2.53 4 16 -3 40.18 2.64 4 -16 -3 34.83 2.35 -4 -16 2 42.79 2.99 4 16 -2 41.02 3.34 -4 16 2 47.56 2.54 4 -16 -2 40.04 2.47 -4 -16 1 71.72 3.78 4 16 -1 82.80 4.57 -4 16 1 79.09 4.12 4 16 0 117.38 5.52 -4 16 0 116.35 5.33 -4 -16 0 106.45 5.01 4 16 1 134.39 6.07 4 16 1 133.37 5.55 -4 16 -1 133.63 5.96 -4 16 -2 -0.38 1.35 4 16 2 0.96 1.30 4 16 3 20.06 2.42 -4 16 -3 22.39 2.58 4 16 4 17.88 2.52 -4 -17 7 48.06 4.38 -4 -17 7 47.91 4.78 4 17 -7 45.15 4.25 -4 17 7 44.64 3.36 -4 -17 6 53.16 4.38 4 17 -6 57.60 4.80 4 17 -6 50.61 4.06 -4 17 6 51.61 3.47 4 -17 -6 59.06 3.57 4 -17 -5 75.61 3.88 -4 -17 5 70.71 4.87 4 17 -5 78.35 5.31 4 17 -5 72.65 4.42 -4 17 5 75.46 4.09 -4 -17 4 202.61 8.31 4 17 -4 207.86 8.99 4 -17 -4 197.18 7.13 4 17 -4 191.13 7.58 -4 17 4 199.85 7.38 -4 -17 3 1.66 1.46 4 -17 -3 3.69 1.08 4 17 -3 3.14 1.83 -4 17 3 3.81 1.21 -4 -17 2 96.95 4.78 4 -17 -2 94.98 4.17 4 17 -2 99.86 5.34 -4 17 2 105.71 4.17 -4 -17 1 91.81 4.45 4 17 -1 99.19 5.20 -4 17 1 92.97 4.68 4 17 0 104.55 5.39 -4 17 0 114.04 5.41 -4 -17 0 110.23 5.06 4 17 1 40.04 3.30 4 17 1 33.35 2.65 -4 17 -1 38.29 3.19 -4 17 -2 9.26 1.94 4 17 2 9.95 1.79 -4 17 -3 6.34 1.91 4 17 3 6.56 1.84 -4 17 -4 43.01 3.82 -4 -18 7 96.14 6.28 4 18 -7 82.30 5.81 -4 18 7 94.27 4.87 4 -18 -6 31.83 2.69 -4 -18 6 31.40 3.55 4 18 -6 40.02 4.16 4 18 -6 34.16 3.31 -4 18 6 30.20 2.72 -4 -18 5 31.25 3.43 4 -18 -5 28.43 2.31 4 18 -5 27.60 3.33 4 18 -5 25.85 2.73 -4 18 5 28.96 2.48 -4 -18 4 137.72 6.66 4 18 -4 146.66 7.26 4 -18 -4 137.44 5.45 4 18 -4 136.24 5.95 -4 18 4 138.41 5.63 -4 -18 3 269.26 9.79 4 -18 -3 263.65 8.73 4 18 -3 260.17 10.43 -4 18 3 261.80 8.77 -4 -18 2 95.59 4.72 4 18 -2 86.52 5.08 4 -18 -2 94.10 4.10 -4 18 2 91.00 3.84 -4 -18 1 43.63 3.04 4 18 -1 43.53 3.46 -4 18 1 40.41 3.10 -4 -18 0 22.46 2.37 4 18 0 22.04 2.57 -4 18 0 25.75 2.69 4 18 1 329.48 11.68 4 18 1 337.99 11.13 -4 18 -1 333.66 11.67 4 18 2 129.71 5.87 -4 18 -2 137.81 6.30 -4 18 -3 11.70 2.36 4 18 3 12.81 2.14 -4 18 -4 4.84 2.28 -4 19 7 1.99 1.69 -4 -19 7 3.63 2.35 4 19 -7 1.79 2.09 -4 -19 6 4.72 2.14 4 -19 -6 4.64 1.49 4 19 -6 5.63 2.00 4 19 -6 5.11 2.54 -4 -19 5 27.24 3.25 4 -19 -5 26.31 2.21 4 19 -5 28.10 3.34 4 19 -5 22.88 2.67 -4 19 5 23.85 2.27 -4 -19 4 66.54 4.53 4 19 -4 73.00 5.02 4 19 -4 67.17 3.89 4 -19 -4 66.95 3.46 -4 19 4 66.99 3.61 -4 -19 3 2.34 1.60 4 19 -3 5.18 1.98 4 -19 -3 3.68 1.16 -4 19 3 2.98 1.21 -4 -19 2 7.35 1.71 4 19 -2 8.10 2.03 4 -19 -2 8.39 1.40 -4 19 2 8.15 1.23 4 19 -1 57.03 4.00 -4 -19 1 54.21 3.45 -4 -19 0 145.30 6.34 4 19 0 156.13 7.02 -4 19 0 157.38 6.82 -4 19 -1 16.19 2.51 4 19 1 21.21 2.63 4 19 1 17.56 2.19 -4 19 -2 10.70 2.27 4 19 2 14.21 2.06 4 19 3 44.99 3.52 -4 19 -3 40.71 3.76 -4 20 7 2.77 1.52 -4 -20 7 0.70 2.08 4 20 -7 2.35 1.95 -4 -20 6 64.47 4.94 4 20 -6 67.51 5.22 4 20 -6 62.27 4.62 -4 -20 5 29.23 3.42 4 20 -5 28.25 3.44 4 -20 -5 26.60 2.24 4 20 -5 27.24 2.83 -4 20 5 28.45 2.37 -4 -20 4 56.22 4.20 4 20 -4 59.78 4.64 4 -20 -4 58.55 3.17 -4 20 4 57.57 3.28 -4 -20 3 157.18 6.89 4 20 -3 164.57 7.57 4 -20 -3 146.48 5.74 -4 20 3 155.60 5.78 -4 -20 2 162.38 6.87 4 20 -2 169.07 7.64 -4 20 2 162.65 5.78 -4 -20 1 11.83 1.87 4 20 -1 13.95 2.37 -4 -20 0 71.79 4.22 4 20 0 77.53 4.75 -4 20 0 78.69 4.63 4 20 1 112.98 5.75 4 20 1 105.70 5.09 -4 20 -1 115.57 5.76 4 20 2 46.25 3.34 -4 20 -2 47.83 3.74 4 20 3 33.81 3.19 -4 20 -3 35.51 3.65 -4 21 7 4.52 1.67 -4 -21 7 3.80 2.38 4 21 -7 4.99 2.18 -4 -21 6 2.20 2.08 4 21 -6 1.29 1.78 4 21 -6 1.07 2.25 -4 -21 5 28.12 3.39 4 21 -5 25.56 3.38 4 21 -5 22.72 2.61 4 -21 -5 22.08 2.02 -4 21 5 25.24 2.30 -4 -21 4 33.20 3.42 4 21 -4 41.11 3.95 -4 21 4 36.80 2.61 4 -21 -4 38.52 2.55 -4 -21 3 22.95 2.70 4 21 -3 23.26 2.95 -4 21 3 23.90 2.02 4 -21 -3 23.86 2.03 -4 -21 2 10.75 2.03 -4 21 2 10.45 1.37 -4 21 2 7.28 1.84 -4 -21 1 28.15 2.59 4 21 -1 27.09 3.01 -4 -21 0 109.56 5.45 4 21 0 125.82 6.24 -4 21 0 123.02 5.90 4 21 1 47.06 3.78 -4 21 -1 40.61 3.75 -4 21 -2 0.57 1.81 -4 21 -3 20.13 3.05 4 22 -7 18.05 3.14 -4 -22 6 38.24 4.02 4 22 -6 38.34 4.26 4 22 -6 38.39 3.68 -4 22 5 4.08 1.40 4 -22 -5 4.28 1.25 -4 -22 5 2.63 1.98 4 22 -5 3.21 1.74 4 22 -5 4.51 2.22 -4 -22 4 109.29 5.98 4 -22 -4 100.36 4.46 4 22 -4 109.39 6.40 -4 22 4 102.35 4.60 -4 -22 3 29.19 2.99 4 -22 -3 29.40 2.25 4 22 -3 35.25 3.60 -4 22 3 33.37 2.29 -4 -22 2 28.01 2.80 -4 22 2 21.54 2.54 -4 22 2 29.03 2.02 -4 -22 1 52.56 3.57 4 22 -1 63.11 4.41 -4 22 1 55.20 3.91 -4 -22 0 19.45 2.52 4 22 0 24.55 2.95 -4 22 0 21.22 2.83 4 22 1 159.28 7.47 -4 22 -1 162.45 7.59 -4 -22 -1 170.63 7.60 -4 22 -2 71.97 4.81 -4 22 -3 6.11 2.34 -4 -23 6 18.31 3.15 4 23 -6 19.44 2.89 -4 -23 5 45.07 4.18 4 23 -5 40.58 4.12 -4 23 5 34.43 2.67 -4 -23 4 15.79 2.83 4 23 -4 19.62 3.23 4 -23 -4 17.11 1.85 -4 23 4 16.64 1.98 -4 -23 3 21.01 2.77 4 23 -3 22.64 3.04 4 -23 -3 20.45 1.97 -4 23 3 22.08 1.98 -4 23 2 2.98 1.12 -4 -23 2 4.40 1.78 -4 23 2 2.02 1.53 -4 -23 1 18.51 2.32 4 23 -1 19.73 2.81 -4 23 1 15.76 2.48 -4 -23 0 79.82 4.66 4 23 0 89.08 5.27 4 23 1 47.07 4.05 -4 23 -1 47.23 4.18 -4 -23 -1 51.68 4.11 -4 23 -2 11.83 2.59 -4 -24 6 2.49 2.13 4 24 -6 2.33 1.88 -4 -24 5 17.47 3.14 4 24 -5 20.19 3.41 -4 24 5 14.76 1.98 -4 -24 4 332.76 12.19 4 24 -4 322.53 12.81 4 -24 -4 305.01 10.08 -4 24 4 305.41 10.18 -4 -24 3 225.72 9.22 4 24 -3 219.30 9.78 4 -24 -3 221.92 7.89 -4 24 3 225.16 7.69 -4 -24 2 10.02 2.12 -4 24 2 10.18 2.10 -4 -24 1 16.20 2.30 4 24 -1 19.06 2.87 -4 24 1 17.09 2.53 -4 -24 0 109.49 5.69 4 24 0 124.95 6.45 -4 -24 -1 153.95 7.45 4 24 1 160.29 7.68 -4 24 -1 164.52 7.78 -4 24 -2 11.64 2.59 -4 -25 6 1.04 2.05 4 25 -6 2.07 1.95 -4 -25 5 113.86 6.73 4 25 -5 100.36 6.62 -4 25 5 100.94 4.78 -4 -25 4 60.55 4.90 4 25 -4 63.81 5.38 -4 25 4 60.46 3.52 4 -25 -4 58.27 3.35 -4 -25 3 54.48 4.24 4 25 -3 57.82 4.77 -4 25 3 56.53 3.19 -4 -25 2 101.44 5.51 -4 25 2 93.83 5.24 -4 -25 1 25.89 2.83 -4 25 1 29.77 3.19 -4 -25 0 17.23 2.57 4 25 0 18.09 2.92 -4 -25 -1 47.36 4.08 4 25 1 50.81 4.28 -4 25 -1 52.06 4.38 -4 25 -2 5.60 2.33 -4 -26 5 15.53 3.07 4 26 -5 13.65 3.21 -4 26 5 14.34 2.04 -4 -26 4 331.45 12.96 4 -26 -4 323.61 10.77 4 26 -4 343.68 13.74 -4 26 4 343.78 10.93 -4 -26 3 111.92 6.07 4 26 -3 114.75 6.72 -4 26 3 97.47 5.48 -4 26 3 107.22 4.59 -4 -26 2 15.78 2.54 -4 26 2 11.62 2.35 -4 26 1 2.08 1.85 -4 -26 1 1.47 1.63 4 26 -1 1.88 1.87 -4 -26 0 148.99 7.12 4 26 0 162.03 7.81 -4 26 0 141.19 7.16 -4 -26 -1 52.12 4.21 4 26 1 50.66 4.36 -4 -26 -2 4.56 2.36 -4 26 -2 3.40 2.35 -4 27 5 5.15 1.64 -4 -27 5 5.31 2.45 4 27 -5 3.55 2.61 -4 27 4 1.43 1.58 -4 -27 4 -0.61 2.17 4 27 -4 1.95 2.43 -4 -27 3 36.05 3.66 4 27 -3 33.86 3.89 -4 27 3 31.16 3.31 -4 27 3 34.99 2.54 -4 -27 2 3.04 1.88 -4 27 2 4.32 1.95 -4 27 1 7.30 2.18 4 27 -1 8.27 2.37 -4 -27 0 22.06 2.95 -4 27 0 15.56 2.94 4 27 0 21.98 3.25 -4 -27 -1 32.23 3.56 4 27 1 36.73 3.92 -4 28 5 5.24 1.67 -4 -28 5 5.21 2.59 4 28 -5 4.96 2.73 -4 -28 4 14.99 2.99 4 28 -4 16.17 3.32 -4 28 4 15.41 2.00 -4 -28 3 40.53 3.81 4 28 -3 43.52 4.37 -4 28 3 29.96 3.36 -4 28 3 38.68 2.73 -4 -28 2 6.17 2.20 -4 28 2 6.76 2.15 -4 28 1 0.25 1.76 -4 -28 1 0.26 1.64 4 28 -1 -0.23 2.07 -4 -28 0 23.32 3.00 4 28 0 29.38 3.64 -4 28 0 24.35 3.29 4 28 1 39.35 4.05 -4 29 5 32.32 2.71 -4 29 4 1.90 1.48 -4 -29 4 -0.86 2.14 4 29 -4 1.70 2.54 -4 29 4 -0.08 1.82 -4 29 3 7.20 1.64 -4 -29 3 7.08 2.38 4 29 -3 6.57 2.66 -4 29 3 7.01 2.29 -4 -29 2 27.98 3.34 -4 29 2 26.41 3.24 4 29 -1 35.02 4.00 -4 29 1 30.48 3.51 4 29 0 56.25 4.85 -4 29 0 44.62 4.29 4 29 1 28.14 3.81 -4 29 -1 31.51 3.86 -4 30 4 55.66 4.39 -4 30 4 64.53 3.75 4 30 -3 22.52 3.67 -4 30 3 19.00 2.95 -4 30 3 22.77 2.31 4 30 -2 7.36 2.86 -4 30 2 3.93 2.38 -4 30 1 8.97 2.55 4 30 -1 9.07 2.96 4 30 0 35.02 4.13 -4 30 0 29.46 3.78 4 30 1 61.98 5.21 -4 31 4 9.57 2.02 4 31 -4 13.61 3.48 4 31 -3 16.31 3.39 -4 31 3 16.05 2.93 -4 31 3 20.20 2.28 4 31 -2 168.63 9.30 -4 31 2 160.88 7.87 4 31 -1 104.92 7.07 -4 31 1 96.47 6.11 -4 31 0 11.99 3.05 4 31 0 13.68 3.25 4 32 -3 30.41 4.29 -4 32 3 29.16 3.51 -4 32 3 27.47 2.62 4 32 -2 31.60 4.44 -4 32 2 30.87 3.84 4 32 -1 161.29 8.97 -4 32 1 137.44 7.53 -4 33 3 7.38 1.90 -4 33 3 6.94 2.59 -4 33 2 38.31 3.98 -4 33 1 5.65 2.64 -4 34 2 1.30 2.13 5 0 -8 72.10 5.05 -5 0 8 71.29 5.32 5 0 -7 0.64 1.62 -5 0 7 0.88 2.05 -5 0 6 0.67 2.02 5 0 -5 47.04 3.60 -5 0 5 48.38 4.45 5 0 -4 113.99 5.37 -5 0 4 122.40 6.71 -5 0 3 124.90 6.48 5 0 -3 129.30 5.31 5 0 -2 0.26 0.81 -5 0 2 0.35 1.34 5 0 -1 53.10 2.51 5 -1 -8 42.08 3.88 -5 -1 8 34.77 3.94 -5 1 8 37.64 4.03 5 1 -8 32.34 3.61 5 1 -7 33.66 3.37 5 -1 -7 41.01 3.52 -5 -1 7 39.23 3.94 -5 1 7 38.18 3.84 5 1 -6 3.25 1.67 -5 -1 6 4.46 2.25 -5 1 6 5.95 2.25 5 1 -5 412.57 14.48 5 -1 -5 437.33 14.67 -5 -1 5 461.03 16.43 -5 1 5 472.24 16.33 5 1 -4 630.91 19.64 5 -1 -4 640.00 19.63 -5 -1 4 695.67 21.88 -5 1 4 666.91 21.42 -5 -1 3 34.89 3.39 -5 1 3 32.62 3.19 5 1 -3 34.85 2.52 5 -1 -3 36.09 2.52 5 1 -2 65.61 3.07 5 -1 -2 60.14 2.97 -5 -1 2 54.77 3.81 -5 1 2 55.58 3.74 5 1 -1 235.54 7.48 5 -1 -1 246.90 7.61 5 2 -8 106.26 6.25 5 -2 -8 103.53 6.10 -5 -2 8 112.02 6.60 -5 2 8 110.16 6.47 5 -2 -7 3.15 1.78 -5 -2 7 4.46 2.29 -5 2 7 5.45 2.32 5 2 -6 12.84 2.26 -5 -2 6 12.22 2.80 5 2 -5 27.89 2.84 5 -2 -5 27.79 2.78 -5 -2 5 32.41 3.87 -5 2 5 32.63 3.64 5 2 -4 199.70 7.94 -5 -2 4 210.88 9.62 5 -2 -4 212.21 7.97 -5 2 4 225.12 9.47 -5 -2 3 193.33 8.71 -5 2 3 204.44 8.58 5 2 -3 207.94 7.44 5 -2 -3 206.48 7.45 5 2 -2 116.19 4.43 5 -2 -2 103.81 4.30 -5 2 2 107.66 5.31 5 2 -1 9.48 1.13 5 2 -1 10.53 1.99 5 -2 -1 11.10 1.26 5 2 0 117.75 4.36 5 2 1 266.20 8.60 5 2 2 15.71 1.83 5 3 -8 31.06 3.69 5 -3 -8 34.04 3.60 -5 -3 8 37.02 4.03 -5 3 8 35.80 3.92 5 -3 -7 107.01 5.83 -5 -3 7 102.37 6.35 -5 3 7 101.03 6.28 5 3 -6 100.54 5.56 5 -3 -6 112.00 5.72 -5 -3 6 102.19 6.45 5 3 -5 286.29 10.70 5 -3 -5 285.65 10.53 -5 -3 5 303.56 12.37 -5 3 5 309.92 11.97 5 3 -4 608.04 18.72 -5 -3 4 649.46 20.93 -5 3 4 613.51 20.03 5 -3 -4 588.45 18.46 -5 3 3 31.19 3.04 5 3 -3 28.15 2.32 5 -3 -3 28.50 2.27 5 3 -2 59.52 2.88 5 3 -2 56.72 3.94 5 -3 -2 52.86 2.79 -5 3 2 52.28 3.50 5 -3 -1 146.77 5.30 5 3 -1 157.45 5.14 5 3 -1 167.27 6.86 5 3 0 343.97 10.34 5 3 1 1.24 1.08 5 3 2 36.85 2.64 5 3 3 19.00 2.22 5 4 -8 47.38 4.32 5 -4 -8 55.75 4.38 -5 -4 8 49.39 4.53 -5 4 8 53.74 4.44 5 -4 -7 110.28 5.95 -5 -4 7 114.34 6.72 -5 4 7 112.95 6.53 5 -4 -6 5.05 1.86 5 4 -6 5.06 1.93 -5 -4 6 5.29 2.35 5 4 -5 64.37 4.19 -5 -4 5 73.64 5.49 -5 4 5 69.02 4.93 5 4 -4 610.31 18.66 -5 -4 4 634.28 20.82 -5 4 4 574.96 19.66 5 -4 -4 607.51 18.45 5 -4 -3 283.95 9.62 5 4 -3 283.69 11.04 5 4 -3 294.14 9.73 -5 4 3 292.58 10.82 5 4 -2 54.36 2.76 5 4 -2 50.75 3.77 -5 4 2 51.07 3.44 5 -4 -2 49.87 2.73 5 -4 -1 94.70 3.81 5 4 -1 92.98 4.97 5 4 0 80.70 3.42 5 4 1 75.15 3.52 5 4 2 76.68 3.89 5 4 3 46.27 3.29 5 4 4 4.83 1.87 5 -5 -8 25.51 3.17 -5 -5 8 29.75 3.80 -5 5 8 31.13 3.57 5 -5 -7 4.77 1.91 5 5 -7 0.56 1.78 -5 -5 7 2.78 2.37 -5 5 7 2.51 2.02 5 5 -6 111.16 5.88 5 -5 -6 108.83 5.61 -5 -5 6 111.58 6.78 5 5 -5 149.58 6.86 -5 -5 5 158.64 8.33 -5 5 5 161.88 7.73 5 5 -4 189.91 7.51 -5 5 4 191.18 8.45 5 -5 -4 187.55 7.32 5 -5 -3 122.89 5.12 5 5 -3 118.95 6.25 5 5 -3 127.48 5.26 -5 5 3 117.25 5.95 5 5 -2 276.42 8.63 5 5 -2 256.06 10.18 -5 5 2 250.20 9.50 5 -5 -2 269.22 8.69 5 -5 -1 131.70 4.86 5 5 -1 129.78 6.09 5 5 0 34.05 2.12 -5 5 0 38.11 2.57 5 5 1 2.52 1.15 5 5 2 30.28 2.49 5 5 3 68.58 4.07 5 5 4 26.20 2.80 5 -6 -8 111.31 6.30 -5 -6 8 113.98 6.86 -5 6 8 115.31 6.42 5 -6 -7 27.72 2.97 -5 -6 7 29.11 3.63 -5 6 7 27.58 3.34 5 6 -7 24.60 2.99 5 6 -6 1.01 1.52 5 -6 -6 1.69 1.39 -5 -6 6 0.12 2.10 5 6 -5 43.18 3.37 -5 6 5 43.70 3.82 5 6 -4 51.24 3.36 -5 6 4 52.89 3.98 5 -6 -4 44.60 3.06 5 -6 -3 127.42 5.26 5 6 -3 128.20 6.54 5 6 -3 129.92 5.38 -5 6 3 127.99 6.07 5 6 -2 35.18 2.20 5 6 -2 33.60 3.18 -5 6 2 33.39 2.82 5 -6 -2 34.22 2.24 5 6 -1 51.31 3.57 5 -6 -1 46.85 2.57 5 6 0 39.71 2.32 -5 6 0 38.73 2.69 5 6 1 30.64 2.26 5 6 2 41.97 2.92 5 6 3 71.30 4.20 5 -7 -8 23.90 3.20 -5 -7 8 22.44 3.67 -5 7 8 25.62 3.34 5 7 -7 5.65 1.98 5 -7 -7 8.64 2.02 -5 -7 7 4.97 2.44 -5 7 7 5.02 2.17 5 -7 -6 23.72 2.54 -5 -7 6 23.79 3.49 5 7 -6 23.30 2.77 5 7 -5 37.20 3.16 5 -7 -5 37.47 2.97 -5 7 5 45.76 3.87 5 7 -4 68.36 3.97 -5 7 4 71.59 4.56 5 -7 -3 57.05 3.18 5 7 -3 56.24 4.25 5 7 -3 58.97 3.28 -5 7 3 60.94 3.96 5 7 -2 144.44 6.82 -5 7 2 144.50 6.21 5 -7 -2 143.02 5.46 5 7 -2 148.23 5.35 5 7 -1 26.58 2.71 5 -7 -1 28.25 2.01 5 7 0 98.69 4.15 -5 7 0 112.49 4.82 5 7 1 87.24 4.06 5 7 2 89.96 4.41 5 7 3 98.71 5.02 5 -8 -8 161.49 7.65 -5 -8 8 161.79 8.42 -5 8 8 160.72 7.70 5 8 -8 151.10 8.04 5 -8 -7 63.67 4.31 -5 -8 7 61.63 5.11 -5 8 7 62.69 4.61 5 8 -7 61.00 4.57 5 -8 -6 70.46 4.29 -5 -8 6 66.97 5.38 5 8 -6 62.04 4.45 5 8 -5 33.24 3.05 5 8 -5 44.04 4.05 -5 8 5 42.75 3.68 5 -8 -5 41.24 3.05 5 8 -4 1.28 1.30 -5 8 4 0.60 1.61 5 -8 -3 131.81 5.38 5 8 -3 135.45 5.53 5 8 -3 134.02 6.83 -5 8 3 138.16 6.31 5 -8 -2 288.96 9.27 5 8 -2 284.08 10.80 -5 8 2 303.48 10.29 -5 -8 2 276.72 9.46 -5 -8 1 42.76 2.64 5 -8 -1 43.62 2.55 5 8 0 53.52 2.85 -5 8 0 55.62 3.40 5 8 1 51.51 3.09 5 8 2 34.58 2.77 5 8 3 41.47 3.32 5 -9 -8 47.99 3.97 -5 -9 8 46.82 4.72 -5 9 8 44.81 4.09 5 9 -8 41.20 4.25 5 -9 -7 32.06 3.10 -5 -9 7 32.16 4.05 -5 9 7 32.99 3.42 5 9 -7 31.70 3.40 -5 -9 6 51.61 4.79 5 -9 -6 48.21 3.52 5 9 -6 46.31 3.83 5 9 -5 26.52 3.36 -5 9 5 28.32 3.04 5 -9 -5 24.27 2.44 5 9 -5 23.86 2.66 -5 -9 4 32.79 2.79 5 9 -4 35.71 2.83 -5 9 4 37.57 3.25 -5 -9 3 33.32 2.69 5 9 -3 35.16 2.52 5 -9 -3 33.26 2.38 5 9 -3 30.96 3.29 -5 9 3 35.61 2.99 -5 -9 2 196.32 7.28 5 -9 -2 207.95 7.09 5 9 -2 198.18 8.44 -5 -9 1 316.92 10.42 5 9 -1 372.46 12.08 5 9 0 184.42 6.61 -5 9 0 197.09 7.32 5 9 1 79.06 3.91 -5 9 -1 79.71 4.09 5 9 2 109.27 5.09 5 9 3 44.49 3.45 5 -10 -8 60.33 4.47 -5 -10 8 61.32 5.18 -5 10 8 67.01 4.68 5 10 -8 56.04 4.83 5 -10 -7 15.51 2.38 -5 10 7 16.69 2.73 -5 -10 7 14.91 3.15 5 10 -7 15.10 2.66 -5 -10 6 22.70 3.66 5 -10 -6 21.92 2.50 -5 10 6 20.72 2.85 5 10 -6 21.08 2.73 -5 -10 5 56.50 3.95 5 10 -5 61.64 4.81 -5 10 5 63.98 4.32 5 -10 -5 57.55 3.64 5 10 -5 56.52 3.89 5 -10 -4 130.22 5.43 -5 -10 4 117.35 5.70 5 10 -4 112.95 5.47 -5 10 4 127.14 6.12 -5 -10 3 25.46 2.58 5 10 -3 22.04 2.08 5 10 -3 20.16 2.80 5 -10 -3 22.65 2.01 -5 10 3 20.98 2.37 -5 -10 2 185.68 7.12 5 -10 -2 194.01 6.77 5 10 -2 191.53 8.23 5 10 -1 121.32 5.88 -5 10 1 133.70 5.48 5 10 0 4.08 1.24 -5 10 0 2.61 1.60 -5 10 -1 0.44 1.30 5 10 1 0.39 1.16 5 10 2 4.75 1.64 5 10 3 79.27 4.60 5 -11 -8 50.85 4.05 -5 -11 8 39.47 4.42 -5 11 8 47.30 4.12 5 11 -8 41.67 4.33 -5 -11 7 55.15 5.05 5 -11 -7 52.89 3.84 -5 11 7 51.64 4.06 5 11 -7 52.91 4.26 -5 -11 6 44.18 3.73 -5 11 6 48.90 3.89 5 -11 -6 48.68 3.50 5 11 -6 43.78 3.72 -5 -11 5 61.58 4.20 5 11 -5 63.29 4.92 -5 11 5 67.47 4.44 5 -11 -5 67.62 3.89 5 11 -5 55.94 3.95 5 11 -4 166.58 6.95 -5 -11 4 170.33 7.30 5 -11 -4 170.98 6.71 -5 11 4 183.95 7.59 -5 -11 3 254.34 9.27 5 11 -3 261.00 8.90 5 11 -3 238.90 10.10 -5 11 3 257.85 9.40 -5 -11 2 205.84 7.60 5 11 -2 210.43 8.75 5 -11 -2 207.75 7.25 5 11 -1 113.19 5.52 -5 11 1 102.81 4.83 5 11 0 24.90 2.09 -5 11 0 28.65 2.67 -5 11 -1 2.10 1.45 5 11 1 3.00 1.27 5 11 2 63.77 3.78 5 11 3 14.58 2.34 -5 -12 8 41.20 4.44 5 -12 -8 40.31 3.65 -5 12 8 37.66 3.69 -5 -12 7 18.40 2.92 -5 -12 7 24.90 3.83 5 -12 -7 23.94 2.70 -5 12 7 20.93 2.84 5 12 -7 19.33 2.90 -5 -12 6 37.99 3.63 -5 12 6 42.02 3.57 5 -12 -6 46.31 3.38 5 12 -6 38.60 3.53 -5 -12 5 42.50 3.79 5 12 -5 44.97 4.33 -5 12 5 52.43 3.81 5 12 -5 40.28 3.36 5 -12 -5 45.27 3.19 5 12 -4 295.45 10.37 -5 -12 4 303.64 10.89 5 -12 -4 293.18 10.08 -5 12 4 308.64 10.91 -5 -12 3 130.16 5.83 5 12 -3 117.21 6.41 -5 12 3 125.38 5.65 -5 -12 2 175.26 6.84 5 12 -2 171.98 7.87 5 -12 -2 182.39 6.49 -5 -12 1 55.14 3.20 5 12 -1 66.89 4.27 -5 12 1 59.45 3.70 5 12 0 34.09 3.09 -5 12 0 28.47 2.78 5 12 1 42.98 2.86 -5 12 -1 36.96 3.01 5 12 2 3.04 1.60 5 12 3 14.84 2.28 5 -13 -8 22.23 2.96 -5 -13 8 20.02 3.73 -5 -13 7 13.49 2.77 -5 -13 7 16.93 3.53 -5 13 7 16.52 2.54 5 -13 -7 16.10 2.36 5 13 -7 15.23 2.72 -5 -13 6 79.43 5.23 5 13 -6 91.88 6.09 -5 13 6 84.38 4.99 5 13 -6 81.77 5.09 5 -13 -6 84.86 4.69 5 -13 -5 259.24 9.38 -5 -13 5 274.03 10.44 5 13 -5 287.17 11.62 -5 13 5 253.27 9.89 5 13 -5 245.37 9.68 5 13 -4 290.50 10.29 -5 -13 4 300.61 10.93 5 -13 -4 299.27 10.09 -5 13 4 296.66 10.67 -5 -13 3 48.28 3.45 5 13 -3 48.29 4.02 -5 13 3 49.72 3.30 -5 -13 2 50.26 3.25 5 13 -2 58.26 4.14 5 -13 -2 51.88 2.97 -5 -13 1 37.89 2.71 5 13 -1 45.63 3.59 -5 13 1 42.57 3.16 5 13 0 91.04 5.06 -5 13 0 82.15 4.61 -5 13 -1 6.79 1.91 5 13 1 9.27 1.71 -5 13 -2 5.75 1.78 5 13 2 7.07 1.80 5 13 3 3.86 1.75 -5 -14 8 58.64 5.40 -5 -14 7 30.57 3.57 -5 -14 7 32.17 4.34 -5 14 7 33.47 3.32 5 14 -7 31.66 3.51 5 -14 -7 30.83 3.01 -5 -14 6 42.20 3.87 5 14 -6 47.59 4.59 -5 14 6 49.94 3.82 5 14 -6 39.75 3.62 5 -14 -6 46.16 3.38 5 -14 -5 33.76 2.77 -5 -14 5 34.14 3.55 5 14 -5 35.38 4.00 -5 14 5 34.65 3.14 5 14 -5 28.89 2.93 5 14 -4 106.12 5.21 -5 -14 4 116.27 5.86 5 14 -4 106.52 6.49 5 -14 -4 114.70 5.13 -5 14 4 118.69 5.56 -5 -14 3 81.76 4.61 5 14 -3 85.00 5.33 -5 14 3 91.39 4.44 5 -14 -3 81.68 4.02 -5 -14 2 41.52 2.98 5 -14 -2 40.55 2.59 5 14 -2 44.18 3.72 -5 -14 1 10.99 1.71 5 14 -1 12.80 2.28 -5 14 1 9.85 1.94 5 14 0 193.16 8.01 -5 14 0 190.00 7.70 -5 -14 0 170.79 7.05 5 14 1 104.22 4.90 -5 14 -1 102.64 5.33 -5 14 -2 12.11 2.07 5 14 2 13.26 2.10 5 14 3 2.21 1.78 -5 -15 8 12.26 3.58 -5 -15 7 11.74 2.77 -5 -15 7 15.80 3.58 -5 15 7 13.91 2.41 5 15 -7 14.49 2.63 5 -15 -7 13.99 2.22 -5 -15 6 85.37 5.55 5 15 -6 88.53 6.18 -5 15 6 88.47 5.10 5 15 -6 83.99 5.16 5 -15 -6 78.40 4.51 -5 -15 5 152.49 7.43 5 -15 -5 146.06 6.17 5 15 -5 168.16 8.39 -5 15 5 152.16 6.76 5 15 -5 131.82 6.49 -5 -15 4 173.43 7.52 5 15 -4 174.26 8.40 5 -15 -4 159.40 6.46 -5 15 4 177.91 7.14 5 -15 -3 11.00 1.58 -5 -15 3 12.26 2.14 5 15 -3 11.42 2.42 -5 15 3 11.62 1.81 -5 -15 2 1.47 1.38 5 15 -2 4.87 1.92 -5 -15 1 27.19 2.35 5 15 -1 34.53 3.29 -5 15 1 30.35 2.84 5 15 0 206.29 8.48 -5 15 0 207.12 8.20 -5 -15 0 189.02 7.58 -5 15 -1 3.10 1.93 5 15 1 3.09 1.61 5 15 2 16.11 2.20 -5 15 -2 14.35 2.29 5 15 3 48.60 3.81 5 -16 -7 -0.54 1.67 -5 -16 7 1.55 2.07 -5 -16 7 0.73 2.69 5 16 -7 2.71 2.03 -5 16 7 1.21 1.69 5 -16 -6 58.53 3.74 -5 -16 6 55.82 4.58 5 16 -6 60.80 5.26 -5 16 6 62.46 4.12 5 16 -6 51.50 4.09 -5 -16 5 1.44 2.02 5 -16 -5 3.63 1.42 5 16 -5 2.80 2.30 -5 16 5 3.26 1.73 5 16 -5 3.54 1.62 -5 -16 4 128.97 6.50 5 16 -4 132.84 7.24 5 -16 -4 123.23 5.35 -5 16 4 132.57 5.92 -5 -16 3 74.68 4.45 5 -16 -3 72.24 3.71 5 16 -3 71.89 5.01 -5 16 3 80.26 4.07 -5 -16 2 21.45 2.31 5 16 -2 24.29 3.01 -5 -16 1 0.62 1.48 5 16 -1 2.66 1.81 -5 16 1 -0.41 1.60 -5 -16 0 70.71 4.24 5 16 0 85.94 5.02 -5 16 0 75.70 4.76 5 16 1 177.72 7.24 -5 16 -1 200.96 8.06 5 16 2 16.48 2.30 -5 16 -2 15.62 2.52 -5 -17 7 34.22 4.01 5 17 -7 31.00 3.60 -5 17 7 32.56 3.11 5 -17 -7 36.75 3.17 -5 -17 6 2.10 1.98 5 -17 -6 3.89 1.52 5 17 -6 5.02 2.63 5 17 -6 4.80 1.99 -5 17 6 6.18 1.94 -5 -17 5 127.01 6.74 5 -17 -5 116.15 5.29 5 17 -5 114.72 7.09 -5 17 5 121.35 5.76 5 17 -5 108.10 5.65 -5 -17 4 225.84 9.32 5 17 -4 240.57 10.35 5 -17 -4 212.45 7.96 -5 17 4 236.48 8.57 -5 -17 3 18.11 2.51 5 17 -3 19.21 2.96 5 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3.85 5 -19 -6 35.50 2.85 5 19 -6 41.04 4.59 5 19 -6 34.01 3.38 -5 19 6 34.77 3.02 -5 -19 5 170.57 8.31 5 19 -5 165.73 8.75 5 -19 -5 157.14 6.51 -5 19 5 171.03 6.91 -5 -19 4 143.73 7.22 5 19 -4 162.05 8.20 -5 19 4 148.99 6.17 5 -19 -4 150.04 6.09 -5 -19 3 3.65 1.92 5 -19 -3 4.36 1.34 5 19 -3 3.93 2.19 -5 19 3 4.88 1.42 -5 -19 2 56.00 3.85 5 19 -2 63.70 4.68 -5 19 2 57.79 3.97 -5 -19 1 106.59 5.27 5 19 -1 111.52 6.18 -5 19 1 111.01 5.79 -5 -19 0 192.41 8.00 5 19 0 209.50 8.97 -5 19 0 207.45 8.61 -5 19 -1 22.34 3.19 5 19 2 13.31 2.31 -5 19 -2 18.19 2.95 5 20 -7 25.69 3.92 5 20 -7 19.90 3.14 -5 -20 6 11.70 2.88 5 -20 -6 13.57 2.04 5 20 -6 13.99 3.34 5 20 -6 11.39 2.38 -5 20 6 11.68 2.14 -5 -20 5 13.06 2.86 5 20 -5 16.05 3.31 5 -20 -5 10.53 1.78 -5 20 5 13.58 2.11 -5 -20 4 42.50 3.99 5 -20 -4 45.17 2.98 5 20 -4 51.94 4.68 -5 20 4 44.45 3.07 -5 -20 3 131.62 6.56 5 -20 -3 130.93 5.46 5 20 -3 130.94 7.30 -5 20 3 134.67 5.46 -5 -20 2 25.23 2.77 5 20 -2 29.31 3.41 -5 20 2 21.09 2.82 -5 -20 1 -0.33 1.53 5 20 -1 -0.38 1.89 -5 20 1 -0.94 1.95 -5 -20 0 65.62 4.34 -5 20 0 67.43 4.77 -5 20 -1 120.30 6.56 -5 -20 -1 126.27 6.60 -5 20 -2 4.13 2.29 5 20 2 5.53 1.90 5 21 -7 12.86 2.82 -5 -21 6 56.66 5.06 5 21 -6 65.15 5.57 5 -21 -6 58.86 3.62 -5 21 6 56.68 3.77 -5 -21 5 106.79 6.45 5 21 -5 112.40 7.02 5 -21 -5 101.49 4.84 -5 21 5 100.99 5.00 -5 -21 4 96.62 5.89 5 -21 -4 97.71 4.59 5 21 -4 105.71 6.61 -5 21 4 96.79 4.66 -5 -21 3 30.25 3.38 5 21 -3 39.21 4.18 5 -21 -3 35.96 2.70 -5 21 3 37.52 2.66 -5 -21 2 107.50 5.58 5 21 -2 107.82 6.35 -5 -21 1 47.96 3.55 5 21 -1 57.02 4.44 -5 21 1 52.67 4.03 -5 -21 0 56.31 4.01 5 21 0 57.19 4.55 -5 21 0 56.57 4.35 -5 -21 -1 1.55 2.14 -5 21 -1 1.65 2.20 5 21 2 24.53 2.92 -5 21 -2 24.59 3.36 -5 22 6 6.10 1.84 -5 -22 6 4.83 2.52 5 22 -6 6.56 2.95 5 -22 -6 5.91 1.63 -5 22 5 9.21 1.88 -5 -22 5 7.84 2.63 5 -22 -5 9.33 1.78 5 22 -5 8.73 2.91 -5 -22 4 113.87 6.41 5 22 -4 114.48 7.03 5 -22 -4 103.88 4.85 -5 22 4 107.63 4.94 -5 -22 3 125.72 6.64 5 -22 -3 135.17 5.66 -5 -22 2 28.23 3.06 5 22 -2 40.16 3.94 -5 -22 1 1.15 1.62 5 22 -1 6.65 2.36 -5 22 1 2.74 2.07 -5 -22 0 20.14 2.70 5 22 0 26.87 3.41 -5 22 0 22.82 3.15 -5 -22 -1 51.79 4.34 -5 22 -1 52.13 4.46 -5 -23 6 16.72 3.29 5 23 -6 20.12 3.92 5 -23 -6 20.11 2.26 -5 23 6 20.68 2.45 5 -23 -5 29.83 2.53 -5 -23 5 33.37 3.88 5 23 -5 36.64 4.28 -5 23 5 32.06 2.72 -5 -23 4 54.65 4.52 5 23 -4 58.65 5.15 -5 23 4 56.62 3.38 5 -23 -4 49.40 3.21 -5 -23 3 0.09 1.77 -5 -23 2 46.24 3.75 5 23 -2 48.99 4.44 -5 23 2 37.78 3.59 -5 -23 1 57.00 4.04 -5 23 1 58.00 4.49 -5 -23 0 25.50 2.93 5 23 0 34.43 3.76 -5 23 0 30.50 3.46 -5 -23 -1 6.84 2.48 -5 23 -1 6.48 2.57 5 24 -6 29.68 4.31 -5 24 5 5.33 1.64 -5 -24 5 4.57 2.42 5 24 -5 7.48 2.83 5 -24 -5 5.96 1.58 -5 24 4 5.79 1.57 -5 -24 4 3.54 2.19 5 -24 -4 4.97 1.48 5 24 -4 4.56 2.54 -5 -24 3 49.72 4.11 -5 24 3 40.13 3.74 -5 -24 2 114.71 6.06 5 24 -2 122.19 6.99 -5 -24 1 8.99 2.24 5 24 -1 11.02 2.77 -5 24 0 4.47 2.45 -5 -24 0 6.82 2.16 5 24 0 7.60 2.68 -5 -24 -1 10.58 2.72 -5 24 -1 11.85 2.83 -5 25 5 4.27 1.60 -5 -25 5 4.45 2.42 5 25 -5 7.94 2.90 5 -25 -5 4.04 1.44 -5 -25 4 40.90 4.11 5 -25 -4 40.72 2.97 5 25 -4 48.20 4.85 -5 25 4 42.25 2.95 -5 -25 3 45.56 4.04 -5 25 3 34.72 3.63 -5 -25 2 36.60 3.63 5 25 -2 36.60 4.07 -5 25 2 28.98 3.55 -5 -25 1 99.67 5.66 5 25 -1 110.41 6.71 -5 -25 0 75.53 5.05 5 25 0 79.54 5.67 -5 25 0 80.22 5.52 5 -26 -5 7.28 1.61 -5 26 5 7.58 1.72 -5 -26 5 9.80 2.86 5 26 -5 10.20 3.00 -5 -26 4 13.58 2.85 5 26 -4 13.83 3.33 5 -26 -4 9.38 1.81 -5 26 4 13.37 1.95 -5 -26 3 40.16 3.90 -5 26 3 35.48 3.64 -5 -26 2 24.01 3.17 5 26 -2 26.15 3.85 -5 26 2 18.53 3.05 -5 -26 1 4.65 2.04 5 26 -1 2.97 2.48 -5 26 0 4.33 2.58 -5 -26 0 3.42 2.32 5 26 0 4.48 2.66 -5 27 5 28.12 2.73 -5 27 4 4.00 1.59 -5 -27 4 2.23 2.28 5 27 -4 2.85 2.69 -5 -27 3 53.40 4.46 -5 27 3 43.15 4.22 -5 -27 2 98.65 6.00 5 27 -2 104.99 6.86 -5 27 2 89.76 5.84 -5 -27 1 19.07 3.03 5 27 -1 24.77 3.71 -5 27 1 22.27 3.32 -5 -27 0 59.45 4.77 5 27 0 70.70 5.55 -5 27 0 57.92 4.99 -5 -28 4 35.04 4.09 5 28 -4 44.55 5.09 -5 28 4 38.08 3.88 -5 28 4 38.33 2.93 -5 -28 3 9.68 2.58 -5 28 3 4.71 2.45 -5 -28 2 11.53 2.83 5 28 -2 15.40 3.58 -5 28 2 11.71 2.93 -5 -28 1 73.72 5.30 -5 28 1 74.93 5.40 5 28 0 13.70 3.23 -5 29 4 55.25 4.75 -5 29 4 63.96 3.78 -5 -29 3 12.07 2.78 -5 29 3 10.55 2.72 -5 -29 2 28.08 3.72 5 29 -2 30.55 4.23 -5 29 2 28.28 3.70 5 29 -1 6.33 2.96 -5 30 3 10.72 2.90 -6 0 8 69.72 5.66 6 0 -7 83.08 5.38 -6 0 7 81.93 6.18 6 0 -6 1.56 1.80 -6 0 6 3.76 2.71 6 0 -5 54.25 3.95 -6 0 5 64.72 5.48 -6 0 4 214.78 9.98 6 0 -4 230.99 8.61 6 0 -3 237.97 8.26 -6 0 3 216.11 9.47 6 0 -2 27.95 2.15 -6 -1 8 18.26 3.64 -6 1 8 15.58 3.48 6 1 -7 4.45 2.13 6 -1 -7 4.94 2.07 -6 -1 7 2.87 2.62 -6 1 7 2.66 2.63 6 1 -6 97.82 5.64 6 -1 -6 107.40 5.77 -6 -1 6 110.22 7.33 -6 1 6 106.25 6.97 6 1 -5 290.40 10.61 -6 -1 5 293.11 12.58 -6 1 5 308.64 12.67 6 -1 -5 261.50 10.27 -6 -1 4 264.26 11.20 -6 1 4 257.37 10.96 6 1 -4 260.52 9.44 6 -1 -4 252.21 9.35 6 1 -3 12.21 1.76 6 -1 -3 16.02 1.90 -6 1 3 13.74 2.49 -6 -1 3 12.26 2.46 6 -1 -2 193.00 6.79 6 1 -2 194.59 6.76 -6 -2 8 49.91 4.86 -6 2 8 54.86 5.05 6 2 -7 59.09 4.50 -6 -2 7 62.82 5.53 6 2 -6 23.37 2.91 6 -2 -6 24.27 2.91 -6 -2 6 25.44 4.00 -6 2 6 29.23 4.06 6 2 -5 80.73 4.81 -6 -2 5 96.79 6.68 -6 2 5 91.86 6.30 6 -2 -5 87.74 4.94 -6 -2 4 75.06 5.58 -6 2 4 79.68 5.49 6 2 -4 77.37 4.32 6 -2 -4 78.57 4.31 6 2 -3 125.97 5.18 6 -2 -3 114.60 5.07 -6 -2 3 116.26 6.42 -6 2 3 119.29 6.21 6 -2 -2 112.42 4.61 6 2 -2 111.56 4.53 -6 -3 8 52.74 5.07 -6 3 8 53.37 4.97 -6 -3 7 3.23 2.71 6 3 -7 0.30 1.92 6 3 -6 77.59 4.99 6 -3 -6 71.68 4.73 -6 -3 6 81.82 6.36 -6 3 6 83.08 6.09 6 3 -5 113.45 5.75 -6 -3 5 128.31 7.78 -6 3 5 121.02 7.20 6 -3 -5 107.09 5.62 -6 -3 4 59.29 4.92 -6 3 4 60.74 4.63 6 3 -4 54.75 3.55 6 -3 -4 58.13 3.64 6 3 -3 8.07 1.62 6 -3 -3 6.90 1.54 -6 -3 3 8.99 2.43 -6 3 3 6.73 2.05 6 -3 -2 78.49 3.73 -6 -4 8 48.70 5.01 6 4 -7 35.19 3.66 -6 -4 7 31.32 4.21 6 4 -6 93.12 5.58 -6 -4 6 116.80 7.63 6 -4 -6 98.63 5.54 -6 4 6 113.38 6.98 6 4 -5 97.22 5.32 -6 -4 5 110.34 7.33 -6 4 5 106.09 6.60 6 -4 -5 102.90 5.36 6 -4 -4 33.91 2.86 -6 -4 4 41.88 4.28 -6 4 4 34.65 3.63 6 4 -4 38.59 2.96 6 4 -3 319.37 10.21 6 -4 -3 306.17 10.17 -6 -4 3 276.79 11.69 -6 4 3 291.88 11.32 6 -4 -2 120.43 4.88 6 5 -7 104.13 6.19 6 -5 -7 111.26 6.12 -6 -5 7 116.04 7.58 -6 -5 6 11.65 3.42 -6 5 6 8.49 2.80 6 5 -6 6.92 2.08 6 5 -5 70.11 4.43 -6 -5 5 84.24 6.32 -6 5 5 79.23 5.52 6 -5 -5 72.61 4.35 6 -5 -4 136.05 5.93 -6 -5 4 133.35 7.65 -6 5 4 134.42 6.97 6 5 -4 128.85 5.85 6 5 -3 38.08 2.72 6 -5 -3 36.73 2.66 -6 5 3 39.05 3.45 6 -5 -2 159.91 6.04 6 5 -2 168.92 7.75 6 6 -7 34.85 3.74 6 -6 -7 40.76 3.77 -6 -6 7 41.28 4.91 -6 6 6 15.15 3.12 6 6 -6 12.48 2.40 6 6 -5 36.76 3.23 -6 -6 5 42.80 4.83 -6 6 5 49.04 4.34 6 -6 -5 36.58 3.13 6 -6 -4 13.90 1.98 6 6 -4 14.21 2.06 -6 6 4 17.20 2.75 -6 -6 4 13.48 3.03 6 6 -3 74.21 5.18 -6 6 3 76.32 4.75 6 -6 -3 77.26 3.93 6 6 -2 174.78 7.97 6 -6 -2 161.92 6.13 6 7 -7 108.23 6.42 -6 -7 7 120.87 7.96 6 -7 -7 120.45 6.31 6 7 -6 142.37 7.18 -6 7 6 169.13 8.47 6 7 -5 63.86 4.24 -6 7 5 70.21 5.15 6 -7 -5 60.75 4.00 6 -7 -4 138.36 6.03 6 7 -4 139.23 7.56 6 7 -4 141.37 6.16 -6 7 4 150.15 7.25 6 7 -3 140.40 7.31 6 -7 -3 137.46 5.69 6 7 -2 300.99 11.59 6 -7 -2 294.57 9.70 -6 7 1 94.70 4.82 6 8 -7 145.23 7.65 -6 -8 7 167.24 9.55 6 -8 -7 158.84 7.45 6 8 -6 8.00 2.30 -6 8 6 9.91 2.84 6 -8 -6 10.02 2.19 6 8 -5 93.56 5.19 -6 -8 5 100.09 7.10 -6 8 5 109.64 6.32 6 -8 -5 94.41 5.06 6 8 -4 1.22 1.46 6 -8 -4 2.20 1.49 6 8 -4 3.16 2.25 -6 8 4 3.61 1.97 6 8 -3 28.41 3.40 6 -8 -3 27.75 2.37 6 8 -2 134.05 6.86 6 -8 -2 120.78 5.07 -6 8 1 27.97 2.77 6 9 -7 181.34 8.64 -6 -9 7 203.58 10.80 6 -9 -7 187.32 8.31 6 9 -6 127.89 6.60 -6 9 6 146.11 7.56 6 9 -5 115.10 5.85 -6 9 5 125.19 6.80 6 -9 -4 185.84 7.45 6 9 -4 205.11 9.45 6 9 -4 193.03 7.58 -6 9 4 206.25 8.66 6 9 -3 58.34 4.64 6 -9 -3 59.65 3.43 6 -9 -2 11.90 1.72 6 9 -2 13.98 2.61 -6 9 1 21.24 2.58 6 10 -7 36.37 3.76 -6 -10 7 37.29 5.06 -6 10 7 37.89 4.05 6 -10 -7 33.01 3.36 6 -10 -6 4.16 1.82 6 10 -6 4.38 2.04 -6 10 6 5.94 2.38 6 10 -5 66.64 4.32 -6 10 5 81.98 5.24 6 -10 -4 18.49 2.19 6 10 -4 20.47 3.27 -6 10 4 21.76 2.77 6 10 -3 119.22 6.76 6 -10 -3 118.45 5.19 6 -10 -2 31.62 2.43 6 10 -2 29.34 3.46 -6 10 1 17.79 2.49 6 10 1 22.42 2.28 6 11 -7 68.78 5.04 -6 -11 7 82.75 6.85 -6 11 7 83.42 5.55 6 -11 -7 73.77 4.78 6 11 -6 60.57 4.34 -6 11 6 64.99 4.83 6 -11 -6 58.68 4.02 6 11 -5 9.43 2.02 -6 11 5 14.16 2.51 6 11 -4 64.74 5.09 6 -11 -4 61.93 3.69 -6 11 4 66.27 4.34 6 -11 -3 39.15 2.83 6 11 -3 42.33 4.19 6 11 -2 122.75 6.51 6 -11 -2 104.86 4.75 -6 11 1 62.99 4.14 -6 11 0 126.99 6.18 6 11 1 11.00 1.89 6 11 2 42.91 3.38 6 -12 -7 4.08 1.92 6 12 -7 2.12 1.93 -6 -12 7 3.60 3.24 -6 12 7 1.35 2.14 6 -12 -6 17.70 2.41 6 12 -6 13.50 2.41 -6 12 6 18.01 2.85 6 12 -5 18.92 2.43 6 -12 -5 16.00 2.13 -6 12 5 18.50 2.69 6 12 -4 7.50 2.51 -6 12 4 10.15 2.07 6 -12 -4 8.89 1.67 6 -12 -3 83.25 4.19 6 12 -3 90.22 5.85 6 12 -2 211.17 9.21 6 -12 -2 200.36 7.44 -6 12 1 68.33 4.53 -6 12 0 24.08 2.97 6 12 1 19.33 2.23 6 12 2 39.96 3.28 6 13 -7 21.39 3.00 -6 -13 7 23.30 4.38 -6 13 7 24.11 3.15 6 -13 -7 22.41 2.76 6 -13 -6 22.65 2.59 6 13 -6 17.99 2.63 -6 13 6 20.13 2.86 6 -13 -5 64.00 3.94 -6 13 5 65.49 4.48 6 13 -4 66.74 5.24 -6 13 4 63.35 4.19 6 -13 -3 22.83 2.21 6 13 -3 24.83 3.31 6 13 -2 16.77 2.88 6 -13 -2 13.08 1.95 -6 13 1 48.41 4.02 -6 13 0 41.51 3.68 6 13 1 8.72 1.92 6 13 2 12.67 2.33 6 -14 -7 19.26 2.62 6 14 -7 17.19 2.87 -6 -14 7 21.20 4.33 -6 14 7 20.59 3.03 6 14 -6 17.54 2.61 6 -14 -6 18.83 2.37 6 14 -6 18.91 3.65 -6 14 6 23.54 3.04 6 -14 -5 2.17 1.56 -6 14 5 0.94 1.86 6 14 -4 63.02 5.15 -6 14 4 62.74 4.16 6 14 -3 32.15 3.74 6 -14 -3 31.85 2.54 6 14 -2 50.68 4.38 6 14 -1 75.65 5.12 -6 14 1 65.78 4.56 -6 14 0 13.48 2.55 6 14 1 13.83 2.12 6 15 -7 1.45 1.90 6 -15 -7 0.80 1.58 -6 -15 7 3.28 3.28 6 15 -6 45.86 3.81 6 -15 -6 52.11 3.67 6 15 -6 50.55 5.20 -6 15 6 53.11 4.17 6 15 -5 96.43 6.81 6 -15 -5 94.29 4.87 -6 15 5 107.55 5.66 6 15 -4 25.03 3.65 -6 15 4 25.72 2.73 6 15 -3 51.12 4.59 6 -15 -3 47.51 3.13 6 15 -2 135.42 7.14 -6 15 2 118.17 6.04 6 15 -1 27.99 3.44 -6 15 1 24.23 3.18 -6 15 0 11.78 2.59 6 16 -7 26.38 3.28 6 -16 -6 21.25 2.60 6 16 -6 20.43 3.87 -6 16 6 21.14 3.00 6 16 -5 90.98 6.65 6 -16 -5 88.43 4.74 -6 16 5 96.78 5.37 6 -16 -4 82.40 4.36 6 16 -4 86.07 6.15 -6 16 4 88.07 4.86 6 16 -3 152.52 8.06 -6 -16 2 44.95 3.53 6 16 -2 50.62 4.50 -6 16 2 42.65 3.82 -6 -16 1 17.86 2.39 -6 16 1 17.35 2.95 -6 -16 0 29.51 2.92 -6 16 0 32.37 3.56 -6 16 -1 27.76 3.33 6 17 -7 9.36 2.44 6 -17 -6 77.21 4.58 6 17 -6 94.11 6.81 -6 17 6 91.83 5.33 6 17 -5 105.45 7.23 6 -17 -5 104.46 5.18 -6 17 5 109.50 5.72 -6 -17 4 81.94 5.40 6 -17 -4 76.89 4.17 6 17 -4 73.78 5.82 -6 17 4 80.37 4.53 -6 -17 3 1.64 2.07 6 17 -3 2.44 2.39 -6 -17 2 39.95 3.37 6 17 -2 47.37 4.37 -6 17 2 41.98 3.73 -6 -17 1 103.93 5.44 -6 17 1 121.37 6.32 -6 -17 0 36.54 3.22 -6 17 0 36.23 3.84 -6 -17 -1 1.24 1.95 -6 17 -1 -1.53 2.34 6 -18 -6 17.80 2.40 6 18 -6 19.11 3.91 -6 18 6 22.32 2.81 6 -18 -5 6.34 1.74 -6 -18 5 3.72 2.64 6 18 -5 8.92 3.21 -6 18 5 6.61 2.02 -6 -18 4 48.44 4.40 6 -18 -4 54.12 3.45 6 18 -4 52.77 4.98 -6 18 4 58.62 3.81 -6 -18 3 93.32 5.52 6 18 -3 99.48 6.50 -6 -18 2 24.89 2.86 6 18 -2 31.64 3.76 -6 18 2 27.73 3.22 -6 -18 1 0.27 1.65 6 18 -1 3.28 2.32 -6 18 1 -1.03 2.30 -6 -18 0 18.55 2.62 -6 18 0 21.13 3.21 -6 18 -1 19.41 3.16 -6 -18 -1 17.90 2.86 -6 -19 6 21.06 3.87 6 19 -6 31.49 4.29 6 -19 -6 24.48 2.63 -6 19 6 29.25 3.05 -6 -19 5 55.45 5.02 6 19 -5 52.96 5.38 -6 19 5 56.46 3.87 6 -19 -5 54.03 3.58 -6 -19 4 67.20 5.04 6 19 -4 73.71 5.70 6 -19 -4 63.29 3.82 -6 19 4 73.25 4.13 -6 -19 3 1.03 1.93 6 19 -3 1.48 2.38 6 -19 -3 1.10 1.44 -6 -19 2 24.31 3.00 -6 19 2 26.65 3.21 -6 -19 1 16.56 2.40 6 19 -1 23.66 3.46 -6 19 1 21.61 3.08 -6 -19 0 23.87 2.86 -6 19 0 26.78 3.40 6 -20 -6 5.56 1.77 -6 -20 6 6.19 2.97 -6 20 6 4.87 1.84 6 -20 -5 25.04 2.56 -6 -20 5 29.53 3.95 6 20 -5 32.36 4.43 -6 20 5 28.25 2.81 -6 -20 4 -0.10 2.23 6 20 -4 1.20 2.38 6 -20 -4 1.51 1.42 -6 -20 3 53.06 4.10 6 -20 -3 41.97 3.15 6 20 -3 45.99 4.70 -6 -20 2 59.27 4.38 -6 20 2 59.29 4.65 -6 -20 1 17.76 2.72 6 20 -1 24.24 3.69 -6 20 1 18.41 3.11 -6 20 0 0.47 2.17 -6 -20 0 -0.31 1.91 -6 -21 6 19.28 3.59 -6 -21 5 68.27 5.56 6 -21 -5 65.20 3.97 6 21 -5 73.80 6.16 -6 21 5 69.07 4.19 -6 -21 4 44.32 4.33 6 21 -4 56.34 5.21 6 -21 -4 47.39 3.29 -6 -21 3 1.35 2.09 6 21 -3 -1.03 2.59 -6 -21 2 91.07 5.57 6 21 -2 109.77 7.00 -6 21 2 101.69 6.07 6 21 -1 139.55 7.67 -6 21 1 129.86 7.00 -6 -21 0 33.94 3.44 -6 21 0 41.50 4.15 -6 -22 5 11.49 3.17 6 -22 -5 11.91 1.98 6 22 -5 12.30 3.48 -6 22 5 14.53 2.26 -6 -22 4 30.77 3.80 6 -22 -4 30.25 2.77 6 22 -4 30.18 4.39 -6 -22 3 133.91 7.18 6 22 -3 139.69 8.18 -6 -22 2 58.92 4.63 -6 22 2 57.90 4.89 -6 22 1 15.85 3.26 -6 -22 1 14.82 2.65 6 22 -1 22.49 3.78 -6 -22 0 -0.26 2.17 -6 -23 5 32.61 4.31 6 -23 -5 34.37 2.91 -6 23 5 36.28 3.07 -6 -23 4 25.32 3.56 6 -23 -4 25.35 2.58 -6 -23 3 54.64 4.56 6 23 -3 62.30 5.60 -6 -23 2 113.15 6.55 -6 23 2 124.77 7.02 -6 -23 1 36.11 3.57 -6 23 1 37.63 4.16 -6 -24 4 6.36 2.42 6 -24 -4 4.66 1.72 -6 -24 3 20.30 3.23 6 24 -3 28.70 4.24 -6 -24 2 39.55 3.97 -6 24 2 34.22 4.22 -6 -24 1 -0.94 1.95 6 24 -1 2.17 2.61 -6 -25 4 19.80 3.35 -6 -25 3 58.74 4.77 6 25 -3 66.59 5.88 -6 25 3 51.72 4.79 -6 -25 2 28.28 3.55 6 25 -2 34.59 4.48 6 25 -1 17.64 3.57 7 0 -7 207.84 9.49 -7 0 7 252.64 12.11 -7 0 6 38.99 4.85 7 0 -6 33.23 3.36 7 0 -5 0.53 1.50 -7 0 5 -0.54 2.39 7 0 -4 40.09 3.08 -7 0 4 36.71 3.88 7 1 -7 32.78 3.77 7 -1 -7 29.53 3.62 -7 -1 7 33.42 5.05 -7 1 7 34.78 4.94 7 1 -6 16.44 2.63 -7 -1 6 16.03 3.79 -7 1 6 14.69 3.59 7 -1 -6 11.06 2.39 7 1 -5 1.13 1.54 7 -1 -5 0.30 1.54 -7 -1 5 3.17 2.63 -7 1 5 1.06 2.45 7 1 -4 57.85 3.62 7 -1 -4 57.35 3.66 -7 -1 4 48.32 4.46 -7 1 4 49.65 4.41 7 -1 -3 74.15 4.03 7 2 -7 80.84 5.42 7 -2 -7 79.83 5.36 7 -2 -6 2.50 1.80 7 2 -6 4.12 1.94 -7 -2 6 5.37 3.25 -7 2 6 5.57 3.01 7 -2 -5 43.93 3.47 -7 -2 5 42.97 4.71 -7 2 5 43.66 4.59 7 2 -5 41.16 3.38 7 2 -4 43.45 3.15 7 -2 -4 41.91 3.15 -7 -2 4 44.76 4.32 -7 2 4 41.42 3.99 7 -2 -3 223.53 8.17 7 3 -7 2.16 2.23 7 -3 -7 3.51 2.19 -7 -3 6 39.64 5.05 7 3 -6 31.39 3.25 -7 3 6 37.29 4.64 7 -3 -6 31.56 3.34 7 -3 -5 20.59 2.62 -7 -3 5 22.78 3.77 -7 3 5 26.45 3.74 7 3 -5 24.79 2.75 7 3 -4 16.06 2.12 7 -3 -4 18.09 2.22 -7 3 4 15.65 2.82 -7 -3 4 15.71 3.04 7 -3 -3 54.50 3.47 7 4 -7 128.72 6.93 7 4 -6 48.16 3.96 -7 4 6 53.37 5.40 7 -4 -6 47.60 3.99 7 4 -5 14.29 2.29 7 -4 -5 15.01 2.31 -7 -4 5 20.11 3.67 -7 4 5 16.87 3.23 -7 -4 4 7.11 2.56 -7 4 4 7.60 2.41 7 -4 -4 5.83 1.63 7 -4 -3 146.53 6.06 7 -4 -2 29.57 2.55 7 5 -7 71.84 5.20 7 5 -6 184.23 8.36 -7 -5 6 210.75 11.13 -7 5 6 210.59 10.40 7 -5 -6 187.92 8.37 7 -5 -5 58.68 4.02 -7 -5 5 59.75 5.68 -7 5 5 68.86 5.33 7 5 -5 64.83 4.16 7 -5 -4 46.35 3.30 -7 -5 4 42.63 4.40 7 -5 -3 18.10 2.19 7 -5 -2 59.79 3.51 7 6 -7 178.16 8.49 7 -6 -6 13.99 2.63 7 6 -6 19.23 2.80 -7 -6 6 20.46 4.33 -7 6 6 17.35 3.77 7 -6 -5 17.83 2.48 -7 -6 5 19.05 3.83 7 6 -5 16.88 2.45 -7 6 5 19.51 3.27 -7 -6 4 32.71 4.04 7 -6 -4 36.45 2.96 7 -6 -3 75.22 4.01 7 7 -7 33.65 3.75 7 -7 -6 21.58 2.91 7 7 -6 24.17 2.93 -7 7 6 30.92 4.14 -7 -7 6 21.70 4.45 7 -7 -5 96.56 5.32 -7 -7 5 107.04 7.50 -7 7 5 112.55 6.75 -7 -7 4 66.06 5.48 7 -7 -4 65.44 3.96 7 -7 -3 47.01 3.25 7 8 -7 17.01 2.87 7 -8 -6 96.49 5.55 7 8 -6 92.01 5.49 -7 -8 6 115.24 8.12 -7 8 6 119.42 7.14 7 -8 -5 60.70 4.05 -7 -8 5 56.37 5.66 -7 8 5 55.41 4.72 7 -8 -4 12.88 2.08 -7 -8 4 14.59 3.26 7 -8 -3 37.72 2.95 7 9 -7 7.05 2.24 7 -9 -6 24.90 2.96 7 9 -6 18.60 2.66 -7 9 6 23.13 3.70 -7 -9 6 24.07 4.73 7 -9 -5 65.61 4.26 -7 -9 5 72.50 6.18 -7 9 5 71.45 5.18 7 -9 -4 108.62 5.29 7 9 -3 76.29 5.58 7 -9 -3 68.80 3.99 -7 9 2 12.48 2.60 7 10 -7 10.15 2.54 7 -10 -6 11.92 2.29 -7 -10 6 8.83 3.69 -7 10 6 10.93 2.98 7 -10 -5 29.59 2.95 -7 -10 5 30.65 4.50 -7 10 5 31.35 3.56 7 -10 -4 8.85 1.93 7 10 -4 7.67 2.95 7 10 -3 122.95 7.15 7 -10 -3 114.58 5.33 -7 10 2 143.48 6.66 -7 -11 6 46.20 5.58 -7 11 6 47.78 4.53 7 -11 -5 80.04 4.66 -7 11 5 84.67 5.43 7 -11 -4 10.47 1.93 7 11 -4 11.61 3.03 7 -11 -3 23.02 2.56 7 11 -3 28.18 3.77 -7 11 2 14.03 2.78 -7 -12 6 42.86 5.54 -7 12 6 38.34 3.97 7 -12 -5 37.09 3.23 -7 12 5 48.43 4.06 7 -12 -4 25.21 2.60 7 12 -4 27.54 3.85 7 -12 -3 43.53 3.23 7 12 -3 50.54 4.75 -7 12 2 29.76 3.26 -7 13 6 17.50 3.01 7 -13 -5 4.67 1.73 7 13 -5 7.14 3.00 -7 13 5 9.21 2.38 7 -13 -4 54.16 3.62 7 13 -4 57.82 5.17 7 -13 -3 10.89 2.09 7 13 -3 13.65 3.24 -7 13 2 65.57 4.75 7 14 -5 18.30 3.62 -7 14 5 21.81 2.89 7 14 -4 12.98 3.26 7 -14 -4 10.49 2.06 7 14 -3 209.71 10.18 7 -14 -3 199.42 7.95 -7 14 2 15.20 3.02 -7 14 1 5.47 2.34 7 15 -5 13.58 3.40 -7 15 5 14.22 2.55 7 15 -4 53.71 5.29 7 -15 -4 51.21 3.56 7 -15 -3 5.70 2.16 7 15 -3 5.90 3.09 -7 15 2 60.66 4.79 -7 15 1 12.86 2.86 7 16 -5 12.19 3.28 -7 16 5 11.25 2.39 7 16 -4 4.98 2.93 7 -16 -4 4.63 1.71 7 16 -3 178.51 9.52 -7 16 2 139.09 7.31 -7 16 1 33.03 3.96 7 17 -4 29.45 4.36 7 -17 -4 29.36 2.82 7 17 -3 13.50 3.79 -7 17 2 -0.63 2.86 7 18 -4 19.36 3.77 7 18 -3 166.40 9.13 -7 18 3 146.21 7.64 7 19 -3 28.97 4.42 7 19 -2 97.99 6.88 7 20 -2 4.30 3.06 8 0 -5 20.11 2.54 -8 0 5 22.06 3.55 8 -1 -5 12.43 2.21 -8 -1 5 9.92 3.06 -8 -2 5 -1.05 2.30 8 -2 -5 1.17 1.67 8 -3 -5 13.28 2.15 -8 -3 5 15.51 3.42 -8 -4 5 16.98 3.48 8 -4 -5 14.22 2.32 8 -4 -4 5.45 1.89 8 -5 -5 79.11 4.73 8 -5 -4 99.11 5.09 8 -6 -4 32.02 3.03 8 -7 -4 59.79 3.91 8 -8 -4 17.59 2.46 8 -8 -3 93.17 5.01 0 0 0 0.00 0.00 TITL m20160518b in P2(1)/m REM P2(1)/m (#11 in standard setting) CELL 0.71073 5.645778 26.699387 6.106961 90.0000 115.6869 90.0000 ZERR 2.00 0.000284 0.000923 0.000235 0.0000 0.0055 0.0000 LATT 1 SYMM -x, y+1/2,-z SFAC C H N O S UNIT 38.00 42.00 2.00 4.00 2.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 82573 _shelx_shelxl_version_number 2014/8 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling - Detector area scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.789 _oxdiff_exptl_absorpt_empirical_full_min 0.446 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn S1 S 1.02822(9) 0.44671(2) 0.38767(8) 0.01971(12) Uani 1 1 d . O1 O 1.0729(3) 0.44426(7) 0.1739(3) 0.0264(3) Uani 1 1 d . O2 O 1.2471(3) 0.44787(7) 0.6231(3) 0.0257(3) Uani 1 1 d . N1 N 0.8558(4) 0.49779(6) 0.3635(3) 0.0177(3) Uani 1 1 d . C1 C 0.7909(4) 0.50734(8) 0.5698(4) 0.0188(4) Uani 1 1 d . H1A H 0.9506 0.5036 0.7249 0.023 Uiso 1 1 calc R H1B H 0.6588 0.4827 0.5678 0.023 Uiso 1 1 calc R C2 C 0.6829(4) 0.55986(8) 0.5501(3) 0.0177(4) Uani 1 1 d . C3 C 0.4491(4) 0.57044(7) 0.3098(4) 0.0177(4) Uani 1 1 d . H3 H 0.3085 0.5460 0.2950 0.021 Uiso 1 1 calc R C4 C 0.5299(5) 0.55817(8) 0.1069(3) 0.0201(4) Uani 1 1 d . H4A H 0.3779 0.5633 -0.0526 0.024 Uiso 1 1 calc R H4B H 0.6719 0.5812 0.1174 0.024 Uiso 1 1 calc R C5 C 0.6246(4) 0.50443(8) 0.1255(3) 0.0197(4) Uani 1 1 d . H5A H 0.4827 0.4811 0.1123 0.024 Uiso 1 1 calc R H5B H 0.6739 0.4971 -0.0082 0.024 Uiso 1 1 calc R C6 C 0.7910(4) 0.59233(8) 0.7320(4) 0.0220(4) Uani 1 1 d . H6A H 0.9382 0.5827 0.8768 0.026 Uiso 1 1 calc R H6B H 0.7211 0.6252 0.7170 0.026 Uiso 1 1 calc R C7 C 0.3342(4) 0.62232(8) 0.2925(4) 0.0192(4) Uani 1 1 d . C8 C 0.1860(4) 0.63239(8) 0.4202(4) 0.0240(4) Uani 1 1 d . H8 H 0.1631 0.6069 0.5178 0.029 Uiso 1 1 calc R C9 C 0.0716(5) 0.67890(9) 0.4074(4) 0.0293(5) Uani 1 1 d . H9 H -0.0278 0.6851 0.4965 0.035 Uiso 1 1 calc R C10 C 0.1023(5) 0.71644(9) 0.2643(5) 0.0336(5) Uani 1 1 d . H10 H 0.0230 0.7483 0.2535 0.040 Uiso 1 1 calc R C11 C 0.2491(5) 0.70691(9) 0.1379(5) 0.0337(5) Uani 1 1 d . H11 H 0.2713 0.7325 0.0403 0.040 Uiso 1 1 calc R C12 C 0.3651(5) 0.66045(8) 0.1516(4) 0.0248(4) Uani 1 1 d . H12 H 0.4664 0.6546 0.0640 0.030 Uiso 1 1 calc R C13 C 0.8239(4) 0.39641(8) 0.3813(4) 0.0205(4) Uani 1 1 d . C14 C 0.6412(5) 0.37822(8) 0.1582(4) 0.0246(4) Uani 1 1 d . H14 H 0.6365 0.3910 0.0112 0.030 Uiso 1 1 calc R C15 C 0.4670(5) 0.34136(9) 0.1526(5) 0.0283(5) Uani 1 1 d . H15 H 0.3435 0.3286 0.0006 0.034 Uiso 1 1 calc R C16 C 0.4696(6) 0.32252(9) 0.3670(5) 0.0275(5) Uani 1 1 d . C17 C 0.6535(5) 0.34120(9) 0.5869(4) 0.0273(5) Uani 1 1 d . H17 H 0.6587 0.3283 0.7339 0.033 Uiso 1 1 calc R C18 C 0.8303(4) 0.37832(8) 0.5974(4) 0.0224(4) Uani 1 1 d . H18 H 0.9534 0.3911 0.7494 0.027 Uiso 1 1 calc R C19 C 0.2730(6) 0.28338(11) 0.3594(6) 0.0400(6) Uani 1 1 d . H19A H 0.0949 0.2972 0.2778 0.060 Uiso 1 1 calc GR H19B H 0.3089 0.2736 0.5255 0.060 Uiso 1 1 calc GR H19C H 0.2876 0.2540 0.2700 0.060 Uiso 1 1 calc GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0166(2) 0.0246(2) 0.0198(2) -0.00155(18) 0.00971(17) -0.00019(19) O1 0.0256(8) 0.0341(7) 0.0265(7) -0.0021(7) 0.0180(6) 0.0008(8) O2 0.0160(7) 0.0314(7) 0.0256(7) -0.0023(7) 0.0051(5) -0.0001(7) N1 0.0165(9) 0.0240(8) 0.0138(7) -0.0015(6) 0.0077(6) 0.0000(6) C1 0.0179(10) 0.0244(9) 0.0152(8) 0.0001(7) 0.0083(7) -0.0005(7) C2 0.0160(9) 0.0251(9) 0.0147(8) -0.0005(7) 0.0091(7) -0.0009(7) C3 0.0153(9) 0.0236(9) 0.0147(8) 0.0000(7) 0.0070(7) -0.0008(7) C4 0.0213(10) 0.0258(10) 0.0136(8) 0.0002(7) 0.0081(7) 0.0002(8) C5 0.0196(10) 0.0255(9) 0.0135(8) -0.0020(7) 0.0069(7) -0.0002(7) C6 0.0184(10) 0.0304(10) 0.0178(8) -0.0027(7) 0.0084(8) -0.0006(8) C7 0.0159(10) 0.0234(9) 0.0172(8) -0.0012(7) 0.0060(7) -0.0018(7) C8 0.0207(10) 0.0282(10) 0.0257(10) -0.0008(8) 0.0125(8) -0.0003(8) C9 0.0248(12) 0.0314(11) 0.0354(12) -0.0029(9) 0.0165(10) 0.0015(9) C10 0.0312(13) 0.0244(10) 0.0461(14) -0.0005(9) 0.0175(12) 0.0040(9) C11 0.0344(14) 0.0258(11) 0.0433(14) 0.0074(9) 0.0192(11) 0.0022(9) C12 0.0253(11) 0.0255(9) 0.0263(9) 0.0034(8) 0.0137(9) 0.0008(8) C13 0.0216(11) 0.0188(9) 0.0223(9) -0.0013(7) 0.0106(8) 0.0007(7) C14 0.0269(12) 0.0262(10) 0.0192(9) -0.0018(7) 0.0085(9) 0.0000(8) C15 0.0257(12) 0.0263(10) 0.0261(10) -0.0031(8) 0.0047(9) -0.0037(8) C16 0.0299(12) 0.0213(10) 0.0325(12) -0.0015(8) 0.0148(10) -0.0031(9) C17 0.0347(14) 0.0245(10) 0.0266(11) -0.0002(8) 0.0168(10) -0.0026(9) C18 0.0265(12) 0.0219(9) 0.0180(9) -0.0008(7) 0.0087(9) -0.0002(8) C19 0.0360(15) 0.0362(13) 0.0466(15) -0.0006(11) 0.0168(12) -0.0122(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O1 S1 N1 106.68(10) O1 S1 C13 108.49(10) O2 S1 O1 119.90(9) O2 S1 N1 106.95(10) O2 S1 C13 108.09(11) N1 S1 C13 105.91(9) C1 N1 S1 114.98(13) C1 N1 C5 112.10(15) C5 N1 S1 114.95(13) N1 C1 H1A 109.8 N1 C1 H1B 109.8 N1 C1 C2 109.41(15) H1A C1 H1B 108.2 C2 C1 H1A 109.8 C2 C1 H1B 109.8 C1 C2 C3 113.68(16) C6 C2 C1 120.95(19) C6 C2 C3 125.4(2) C2 C3 H3 106.9 C2 C3 C4 107.71(16) C4 C3 H3 106.9 C7 C3 C2 113.92(16) C7 C3 H3 106.9 C7 C3 C4 114.11(16) C3 C4 H4A 109.4 C3 C4 H4B 109.4 H4A C4 H4B 108.0 C5 C4 C3 111.16(16) C5 C4 H4A 109.4 C5 C4 H4B 109.4 N1 C5 C4 108.53(16) N1 C5 H5A 110.0 N1 C5 H5B 110.0 C4 C5 H5A 110.0 C4 C5 H5B 110.0 H5A C5 H5B 108.4 C2 C6 H6A 120.0 C2 C6 H6B 120.0 H6A C6 H6B 120.0 C8 C7 C3 118.69(18) C12 C7 C3 123.22(18) C12 C7 C8 118.1(2) C7 C8 H8 119.4 C9 C8 C7 121.3(2) C9 C8 H8 119.4 C8 C9 H9 120.0 C8 C9 C10 120.0(2) C10 C9 H9 120.0 C9 C10 H10 120.4 C11 C10 C9 119.2(2) C11 C10 H10 120.4 C10 C11 H11 119.6 C10 C11 C12 120.9(2) C12 C11 H11 119.6 C7 C12 H12 119.7 C11 C12 C7 120.6(2) C11 C12 H12 119.7 C14 C13 S1 119.24(17) C18 C13 S1 119.80(17) C18 C13 C14 120.7(2) C13 C14 H14 120.3 C15 C14 C13 119.4(2) C15 C14 H14 120.3 C14 C15 H15 119.5 C14 C15 C16 121.0(2) C16 C15 H15 119.5 C15 C16 C19 120.8(2) C17 C16 C15 118.5(2) C17 C16 C19 120.7(2) C16 C17 H17 119.2 C16 C17 C18 121.6(2) C18 C17 H17 119.2 C13 C18 H18 120.6 C17 C18 C13 118.8(2) C17 C18 H18 120.6 C16 C19 H19A 109.5 C16 C19 H19B 109.5 C16 C19 H19C 109.5 H19A C19 H19B 109.5 H19A C19 H19C 109.5 H19B C19 H19C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance S1 O1 1.4344(13) S1 O2 1.4335(14) S1 N1 1.6446(18) S1 C13 1.760(2) N1 C1 1.478(2) N1 C5 1.484(3) C1 H1A 0.9900 C1 H1B 0.9900 C1 C2 1.513(3) C2 C3 1.515(3) C2 C6 1.331(3) C3 H3 1.0000 C3 C4 1.530(3) C3 C7 1.514(3) C4 H4A 0.9900 C4 H4B 0.9900 C4 C5 1.518(3) C5 H5A 0.9900 C5 H5B 0.9900 C6 H6A 0.9500 C6 H6B 0.9500 C7 C8 1.395(3) C7 C12 1.392(3) C8 H8 0.9500 C8 C9 1.386(3) C9 H9 0.9500 C9 C10 1.389(3) C10 H10 0.9500 C10 C11 1.379(4) C11 H11 0.9500 C11 C12 1.388(3) C12 H12 0.9500 C13 C14 1.392(3) C13 C18 1.391(3) C14 H14 0.9500 C14 C15 1.381(3) C15 H15 0.9500 C15 C16 1.397(3) C16 C17 1.386(3) C16 C19 1.511(4) C17 H17 0.9500 C17 C18 1.388(3) C18 H18 0.9500 C19 H19A 0.9800 C19 H19B 0.9800 C19 H19C 0.9800 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion S1 N1 C1 C2 168.53(14) S1 N1 C5 C4 -165.42(14) S1 C13 C14 C15 -175.04(18) S1 C13 C18 C17 175.16(17) O1 S1 N1 C1 -179.48(15) O1 S1 N1 C5 48.10(16) O1 S1 C13 C14 -30.4(2) O1 S1 C13 C18 155.26(18) O2 S1 N1 C1 -50.04(16) O2 S1 N1 C5 177.55(14) O2 S1 C13 C14 -161.89(17) O2 S1 C13 C18 23.8(2) N1 S1 C13 C14 83.78(18) N1 S1 C13 C18 -90.53(18) N1 C1 C2 C3 55.2(2) N1 C1 C2 C6 -124.59(19) C1 N1 C5 C4 60.8(2) C1 C2 C3 C4 -54.4(2) C1 C2 C3 C7 177.94(16) C2 C3 C4 C5 56.6(2) C2 C3 C7 C8 -74.2(2) C2 C3 C7 C12 106.9(2) C3 C4 C5 N1 -60.3(2) C3 C7 C8 C9 -178.7(2) C3 C7 C12 C11 178.3(2) C4 C3 C7 C8 161.54(19) C4 C3 C7 C12 -17.3(3) C5 N1 C1 C2 -57.7(2) C6 C2 C3 C4 125.4(2) C6 C2 C3 C7 -2.3(3) C7 C3 C4 C5 -175.87(18) C7 C8 C9 C10 0.4(4) C8 C7 C12 C11 -0.6(3) C8 C9 C10 C11 -0.6(4) C9 C10 C11 C12 0.2(4) C10 C11 C12 C7 0.3(4) C12 C7 C8 C9 0.2(3) C13 S1 N1 C1 65.07(16) C13 S1 N1 C5 -67.34(15) C13 C14 C15 C16 0.7(4) C14 C13 C18 C17 0.9(3) C14 C15 C16 C17 -0.8(4) C14 C15 C16 C19 178.1(2) C15 C16 C17 C18 0.9(4) C16 C17 C18 C13 -1.0(3) C18 C13 C14 C15 -0.8(3) C19 C16 C17 C18 -177.9(2)