#------------------------------------------------------------------------------ #$Date: 2019-11-26 03:34:00 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242517 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/25/4132555.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132555 loop_ _publ_author_name 'McWilliams, Sean F.' 'Bill, Eckhard' 'Lukat-Rodgers, Gudrun' 'Rodgers, Kenton R.' 'Mercado, Brandon Q.' 'Holland, Patrick L.' _publ_section_title ; Effects of N2 Binding Mode on Iron-Based Functionalization of Dinitrogen to Form an Iron(III) Hydrazido Complex. ; _journal_issue 27 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 8586 _journal_page_last 8598 _journal_paper_doi 10.1021/jacs.8b04828 _journal_volume 140 _journal_year 2018 _chemical_formula_moiety 'C55 H91 Fe K N2 O8' _chemical_formula_sum 'C55 H91 Fe K N2 O8' _chemical_formula_weight 1003.24 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 107.3360(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 17.5430(12) _cell_length_b 16.6901(12) _cell_length_c 20.3235(14) _cell_measurement_reflns_used 1036 _cell_measurement_temperature 93(2) _cell_measurement_theta_max 68.3 _cell_measurement_theta_min 2.6 _cell_volume 5680.3(7) _computing_cell_refinement 'CrystalClear-SM Expert 2.0 r15 (Rigaku, 2011)' _computing_data_collection 'CrystalClear-SM Expert 2.0 r15 (Rigaku, 2011)' _computing_data_reduction 'CrystalClear-SM Expert 2.0 r15 (Rigaku, 2011)' _computing_molecular_graphics ; Dolomanov, O.V.; Bourhis, L.J.; Gildea, R.J.; Howard, J.A.K.; Puschmann, H., OLEX2: A complete structure solution, refinement and analysis program (2009). J. Appl. Cryst., 42, 339-341. ; _computing_publication_material 'SHELXL-2013/2 (Sheldrick, 2014)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXT-2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 93(2) _diffrn_detector_area_resol_mean 22.2 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Rigaku Saturn 944+ CCD' _diffrn_measurement_method \w _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.1164 _diffrn_reflns_av_unetI/netI 0.0305 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_h_min -20 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 23 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 183013 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 63.685 _diffrn_reflns_theta_max 63.685 _diffrn_reflns_theta_min 3.493 _diffrn_source 'Sealed Tube' _exptl_absorpt_coefficient_mu 3.182 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.652 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'Jacobson, R. (1998) Private Communication' _exptl_crystal_colour Red _exptl_crystal_density_diffrn 1.173 _exptl_crystal_density_method 'not measured' _exptl_crystal_description Plate _exptl_crystal_F_000 2176 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.200 _exptl_crystal_size_min 0.020 _refine_diff_density_max 1.338 _refine_diff_density_min -0.448 _refine_diff_density_rms 0.080 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.054 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 642 _refine_ls_number_reflns 9359 _refine_ls_number_restraints 6 _refine_ls_restrained_S_all 1.054 _refine_ls_R_factor_all 0.1103 _refine_ls_R_factor_gt 0.0916 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1627P)^2^+8.7151P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2632 _refine_ls_wR_factor_ref 0.2826 _reflns_Friedel_coverage 0.000 _reflns_number_gt 7236 _reflns_number_total 9359 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b04828_si_003.cif _cod_data_source_block 6 _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 4132555 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.569 _shelx_estimated_absorpt_t_max 0.939 _shelx_res_file ; 007-15133.res created by SHELXL-2014/7 TITL 007-15133 CELL 1.54178 17.543 16.6901 20.3235 90 107.336 90 ZERR 4 0.0012 0.0012 0.0014 0 0.001 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Fe K N O UNIT 220 364 4 4 8 32 DFIX 0.96 C14 H14 C24 H24 C34 H34 C44 H44 C54 H54 C64 H64 L.S. 10 PLAN 20 SIZE 0.2 0.2 0.02! Red Plate TEMP -180 BOND $H MORE -1 CONF ACTA WGHT 0.162700 8.715100 FVAR 0.30830 FE1 3 0.852227 0.661051 0.607851 11.00000 0.05285 0.06545 = 0.03788 -0.00031 0.01122 -0.01162 N11 5 0.957862 0.694221 0.591868 11.00000 0.05844 0.06993 = 0.03496 -0.00733 0.01801 -0.00866 N21 5 0.905835 0.588732 0.685139 11.00000 0.05057 0.04454 = 0.03905 -0.00737 0.01494 -0.00835 C11 1 1.104152 0.700878 0.615573 11.00000 0.07462 0.12565 = 0.10571 0.02473 0.05771 0.00553 AFIX 137 H11A 2 1.092066 0.718674 0.567605 11.00000 -1.50000 H11B 2 1.145326 0.659187 0.624756 11.00000 -1.50000 H11C 2 1.123532 0.746416 0.646474 11.00000 -1.50000 AFIX 0 C21 1 1.029034 0.667335 0.627794 11.00000 0.05948 0.07972 = 0.04657 -0.00937 0.02582 -0.00258 C31 1 1.039738 0.610237 0.680165 11.00000 0.04987 0.06827 = 0.04930 -0.01174 0.01907 -0.00084 AFIX 43 H31 2 1.093595 0.594352 0.700763 11.00000 -1.20000 AFIX 0 C41 1 0.984958 0.572909 0.707085 11.00000 0.05186 0.04956 = 0.04182 -0.01517 0.01403 -0.00218 C51 1 1.018240 0.511928 0.762167 11.00000 0.06015 0.05047 = 0.05943 -0.00659 0.01766 0.00118 AFIX 137 H51A 2 0.981384 0.504731 0.789673 11.00000 -1.50000 H51B 2 1.070073 0.530317 0.792023 11.00000 -1.50000 H51C 2 1.025055 0.460811 0.740866 11.00000 -1.50000 AFIX 0 C12 1 0.952976 0.748715 0.536224 11.00000 0.06724 0.08126 = 0.04156 -0.00138 0.03009 -0.00635 C22 1 0.937524 0.717091 0.468979 11.00000 0.08085 0.09022 = 0.04670 -0.00719 0.03276 -0.00521 C32 1 0.925625 0.771609 0.414293 11.00000 0.09323 0.12024 = 0.04294 -0.00227 0.03710 -0.00800 AFIX 43 H32 2 0.915720 0.751171 0.368889 11.00000 -1.20000 AFIX 0 C42 1 0.927622 0.851950 0.423314 11.00000 0.11706 0.10384 = 0.05438 0.01105 0.04336 -0.02642 AFIX 43 H42 2 0.918729 0.886848 0.384833 11.00000 -1.20000 AFIX 0 C52 1 0.942944 0.883211 0.490010 11.00000 0.11281 0.08353 = 0.06229 0.00290 0.04578 -0.03894 AFIX 43 H52 2 0.943953 0.939561 0.496816 11.00000 -1.20000 AFIX 0 C62 1 0.956671 0.831881 0.546224 11.00000 0.09065 0.07809 = 0.05032 -0.00355 0.03944 -0.02799 C72 1 0.935870 0.627987 0.457202 11.00000 0.09979 0.10136 = 0.04754 -0.01250 0.02863 0.02017 AFIX 13 H72 2 0.916134 0.603392 0.493943 11.00000 -1.20000 AFIX 0 C82 1 1.019135 0.591825 0.465845 11.00000 0.17540 0.15071 = 0.17632 -0.01265 0.11445 0.04866 AFIX 137 H82A 2 1.047160 0.624093 0.440042 11.00000 -1.50000 H82B 2 1.013316 0.536806 0.448203 11.00000 -1.50000 H82C 2 1.049868 0.591586 0.514785 11.00000 -1.50000 AFIX 0 C92 1 0.877130 0.602567 0.388238 11.00000 0.25202 0.09383 = 0.07831 -0.02965 -0.01839 0.00661 AFIX 137 H92A 2 0.822707 0.616916 0.387482 11.00000 -1.50000 H92B 2 0.880553 0.544493 0.382579 11.00000 -1.50000 H92C 2 0.890544 0.630025 0.350523 11.00000 -1.50000 AFIX 0 C102 1 0.978391 0.868697 0.618442 11.00000 0.12857 0.07861 = 0.05328 -0.00976 0.04254 -0.04514 AFIX 13 H102 2 0.990008 0.823969 0.652738 11.00000 -1.20000 AFIX 0 C112 1 1.051388 0.920210 0.632627 11.00000 0.10917 0.10538 = 0.06168 0.00106 0.02307 -0.04176 AFIX 137 H11D 2 1.095320 0.889109 0.624889 11.00000 -1.50000 H11E 2 1.066470 0.938604 0.680581 11.00000 -1.50000 H11F 2 1.040148 0.966629 0.601697 11.00000 -1.50000 AFIX 0 C122 1 0.911964 0.918761 0.630199 11.00000 0.11848 0.25510 = 0.12575 -0.11527 0.06265 -0.04684 AFIX 137 H12A 2 0.889290 0.953159 0.590043 11.00000 -1.50000 H12B 2 0.933235 0.952131 0.671265 11.00000 -1.50000 H12C 2 0.870246 0.883490 0.636921 11.00000 -1.50000 AFIX 0 C13 1 0.854776 0.549594 0.717817 11.00000 0.05090 0.04123 = 0.04769 -0.00407 0.01670 -0.00550 C23 1 0.823960 0.472887 0.696503 11.00000 0.05877 0.04467 = 0.07948 -0.01505 0.02649 -0.00797 C33 1 0.766422 0.441319 0.723548 11.00000 0.08074 0.04555 = 0.11470 -0.01071 0.05070 -0.01671 AFIX 43 H33 2 0.744892 0.389823 0.708960 11.00000 -1.20000 AFIX 0 C43 1 0.740122 0.482413 0.770480 11.00000 0.08029 0.06349 = 0.11657 0.00936 0.05782 -0.00566 AFIX 43 H43 2 0.699552 0.460311 0.787212 11.00000 -1.20000 AFIX 0 C53 1 0.772920 0.557035 0.793905 11.00000 0.07880 0.05574 = 0.07839 0.00725 0.04735 0.00852 AFIX 43 H53 2 0.755632 0.585042 0.827578 11.00000 -1.20000 AFIX 0 C63 1 0.830361 0.590389 0.768413 11.00000 0.05907 0.03914 = 0.05111 0.00316 0.02167 0.00460 C73 1 0.851673 0.422877 0.645439 11.00000 0.06569 0.05514 = 0.08192 -0.02915 0.02324 -0.00908 AFIX 13 H73 2 0.891439 0.454765 0.629944 11.00000 -1.20000 AFIX 0 C83 1 0.892250 0.344784 0.679415 11.00000 0.08615 0.05704 = 0.10806 -0.02630 0.03247 -0.00483 AFIX 137 H83A 2 0.935780 0.357916 0.720982 11.00000 -1.50000 H83B 2 0.913771 0.315835 0.646930 11.00000 -1.50000 H83C 2 0.852924 0.311090 0.691874 11.00000 -1.50000 AFIX 0 C93 1 0.782302 0.401990 0.582717 11.00000 0.08308 0.08637 = 0.09967 -0.04652 0.01021 -0.00599 AFIX 137 H93A 2 0.741285 0.373533 0.597401 11.00000 -1.50000 H93B 2 0.801267 0.367682 0.551717 11.00000 -1.50000 H93C 2 0.759556 0.451267 0.558527 11.00000 -1.50000 AFIX 0 C103 1 0.867642 0.670467 0.796236 11.00000 0.06449 0.04054 = 0.03969 -0.00065 0.01577 0.00318 AFIX 13 H103 2 0.884549 0.696519 0.758523 11.00000 -1.20000 AFIX 0 C113 1 0.941889 0.661193 0.856957 11.00000 0.08673 0.04891 = 0.05607 -0.00608 0.00762 0.00836 AFIX 137 H11G 2 0.927843 0.635845 0.895271 11.00000 -1.50000 H11H 2 0.965247 0.714054 0.871345 11.00000 -1.50000 H11I 2 0.980707 0.627667 0.843616 11.00000 -1.50000 AFIX 0 C123 1 0.810069 0.727973 0.815164 11.00000 0.08271 0.05551 = 0.08088 -0.01974 0.01135 0.01714 AFIX 137 H12D 2 0.765605 0.740086 0.773997 11.00000 -1.50000 H12E 2 0.838176 0.777643 0.833572 11.00000 -1.50000 H12F 2 0.789391 0.703182 0.850099 11.00000 -1.50000 AFIX 0 C14 1 0.761276 0.743376 0.621014 11.00000 0.05342 0.08193 = 0.06201 0.01122 0.01213 0.00223 H14 2 0.765015 0.784981 0.654474 11.00000 0.08145 C24 1 0.780712 0.753535 0.558434 11.00000 0.05553 0.08947 = 0.05810 0.02400 0.00668 -0.00434 H24 2 0.801784 0.802780 0.547589 11.00000 0.10821 C34 1 0.772598 0.688931 0.512897 11.00000 0.06297 0.10893 = 0.04644 0.00632 0.00019 -0.01779 H34 2 0.785749 0.693202 0.470244 11.00000 0.07658 C44 1 0.745148 0.615546 0.530066 11.00000 0.06743 0.10387 = 0.05512 -0.00985 0.00203 -0.02359 H44 2 0.734752 0.564943 0.506676 11.00000 0.08080 C54 1 0.706225 0.612650 0.582577 11.00000 0.07636 0.08969 = 0.07216 0.01507 0.00204 -0.02075 H54 2 0.676174 0.567624 0.591527 11.00000 0.07009 C64 1 0.713850 0.676151 0.627824 11.00000 0.07596 0.07972 = 0.06381 0.01855 0.01925 0.00275 H64 2 0.691000 0.678174 0.665399 11.00000 0.06013 K1 4 0.602357 0.755997 0.480366 11.00000 0.06984 0.06188 = 0.04291 -0.00005 0.00131 -0.01243 O10 6 0.659860 0.918012 0.493498 11.00000 0.14174 0.07819 = 0.07081 -0.00209 0.00195 -0.01766 C20 1 0.683607 0.950904 0.441455 11.00000 0.13805 0.09605 = 0.09917 0.01914 0.02194 -0.04106 AFIX 23 H20A 2 0.728113 0.988752 0.460776 11.00000 -1.20000 H20B 2 0.638767 0.981106 0.410107 11.00000 -1.20000 AFIX 0 C30 1 0.710128 0.886527 0.402163 11.00000 0.14987 0.09155 = 0.07841 0.01937 -0.03490 -0.04787 AFIX 23 H30A 2 0.729844 0.911314 0.366068 11.00000 -1.20000 H30B 2 0.754944 0.856609 0.433829 11.00000 -1.20000 AFIX 0 O40 6 0.649158 0.833781 0.371687 11.00000 0.10259 0.09783 = 0.07911 0.02116 0.01476 -0.00379 C50 1 0.671788 0.772443 0.332596 11.00000 0.08575 0.16538 = 0.09073 -0.04669 0.01531 0.02985 AFIX 23 H50A 2 0.715772 0.740457 0.363128 11.00000 -1.20000 H50B 2 0.691503 0.797073 0.296437 11.00000 -1.20000 AFIX 0 C60 1 0.603286 0.719140 0.299980 11.00000 0.14625 0.11061 = 0.04958 -0.00048 0.03931 -0.01023 AFIX 23 H60A 2 0.556874 0.751345 0.273520 11.00000 -1.20000 H60B 2 0.617657 0.681579 0.267883 11.00000 -1.20000 AFIX 0 O70 6 0.583448 0.675154 0.353687 11.00000 0.12177 0.08476 = 0.06332 -0.00043 0.01741 0.00967 C80 1 0.526245 0.622005 0.334457 11.00000 0.14525 0.04866 = 0.15511 -0.00263 0.08216 -0.00713 AFIX 23 H80A 2 0.541152 0.582777 0.303880 11.00000 -1.20000 H80B 2 0.477214 0.649616 0.306794 11.00000 -1.20000 AFIX 0 C90 1 0.507241 0.577690 0.390142 11.00000 0.13515 0.05974 = 0.06420 -0.02045 0.02685 -0.00773 AFIX 23 H90A 2 0.466500 0.536048 0.370920 11.00000 -1.20000 H90B 2 0.555665 0.551566 0.420503 11.00000 -1.20000 AFIX 0 O100 6 0.476966 0.636683 0.427963 11.00000 0.10360 0.06278 = 0.07235 0.00320 0.02363 -0.00133 C110 1 0.460963 0.606800 0.484017 11.00000 0.12634 0.07597 = 0.05933 0.01694 0.02063 0.02547 AFIX 23 H11J 2 0.511257 0.587260 0.516904 11.00000 -1.20000 H11K 2 0.424611 0.560374 0.469967 11.00000 -1.20000 AFIX 0 C120 1 0.425332 0.663785 0.517966 11.00000 0.08794 0.06710 = 0.06559 -0.00637 0.02001 -0.02242 AFIX 23 H12G 2 0.406294 0.636913 0.553564 11.00000 -1.20000 H12H 2 0.379102 0.689604 0.484344 11.00000 -1.20000 AFIX 0 O130 6 0.484201 0.722363 0.549094 11.00000 0.08948 0.08862 = 0.06794 -0.01148 0.01344 0.00656 C140 1 0.461772 0.783008 0.580624 11.00000 0.17639 0.07181 = 0.09173 -0.02121 -0.00116 -0.00210 AFIX 23 H14A 2 0.439266 0.761897 0.616410 11.00000 -1.20000 H14B 2 0.419034 0.813109 0.546791 11.00000 -1.20000 AFIX 0 C150 1 0.526492 0.837077 0.612460 11.00000 0.12912 0.06890 = 0.05123 -0.00947 0.01503 -0.00299 AFIX 23 H15A 2 0.509806 0.874894 0.643086 11.00000 -1.20000 H15B 2 0.573114 0.806402 0.640656 11.00000 -1.20000 AFIX 0 O160 6 0.547115 0.879096 0.561412 11.00000 0.12146 0.07166 = 0.07357 -0.00954 0.00670 -0.00747 C170 1 0.607944 0.930591 0.588621 11.00000 0.15845 0.07098 = 0.08224 -0.01046 0.01927 -0.01852 AFIX 23 H17A 2 0.654828 0.901109 0.617834 11.00000 -1.20000 H17B 2 0.591699 0.970845 0.617623 11.00000 -1.20000 AFIX 0 C180 1 0.629552 0.972557 0.528820 11.00000 0.12891 0.06306 = 0.11168 -0.00709 0.01292 -0.02674 AFIX 23 H18A 2 0.581289 0.997795 0.497386 11.00000 -1.20000 H18B 2 0.669477 1.015126 0.547369 11.00000 -1.20000 AFIX 0 O190 6 0.230386 0.861854 0.576073 11.00000 0.14559 0.10938 = 0.07274 0.00822 -0.00153 -0.05956 C200 1 0.289575 0.877364 0.697537 11.00000 0.27662 0.30454 = 0.08575 0.02779 -0.00603 -0.19657 AFIX 137 H20C 2 0.293449 0.935676 0.693859 11.00000 -1.50000 H20D 2 0.336828 0.857248 0.732849 11.00000 -1.50000 H20E 2 0.241523 0.863864 0.710369 11.00000 -1.50000 AFIX 0 C210 1 0.285193 0.842175 0.634173 11.00000 0.12598 0.27508 = 0.13338 0.08414 0.03938 -0.01229 AFIX 23 H21A 2 0.337701 0.850922 0.626482 11.00000 -1.20000 H21B 2 0.280176 0.783722 0.640061 11.00000 -1.20000 AFIX 0 C220 1 0.219601 0.827994 0.516851 11.00000 0.13254 0.13173 = 0.12808 0.03095 0.06256 0.01713 AFIX 23 H22A 2 0.211476 0.770163 0.523279 11.00000 -1.20000 H22B 2 0.270448 0.832920 0.505410 11.00000 -1.20000 AFIX 0 C230 1 0.158184 0.852463 0.457969 11.00000 0.16945 0.13917 = 0.09502 -0.03354 0.00906 -0.03462 AFIX 137 H23A 2 0.106490 0.834898 0.462072 11.00000 -1.50000 H23B 2 0.166820 0.828495 0.416749 11.00000 -1.50000 H23C 2 0.158591 0.910988 0.454193 11.00000 -1.50000 AFIX 0 O240 6 0.576303 0.410091 0.305405 11.00000 0.08652 0.08928 = 0.09433 -0.01871 0.03498 -0.01079 C250 1 0.518081 0.367598 0.254523 11.00000 0.12649 0.07824 = 0.06844 -0.01110 0.04545 -0.00535 AFIX 23 H25A 2 0.534921 0.311072 0.253808 11.00000 -1.20000 H25B 2 0.512600 0.391232 0.208664 11.00000 -1.20000 AFIX 0 C260 1 0.441724 0.370930 0.268822 11.00000 0.09758 0.10089 = 0.12808 -0.03501 0.02799 -0.01681 AFIX 137 H26A 2 0.449960 0.361388 0.318033 11.00000 -1.50000 H26B 2 0.406072 0.329753 0.241800 11.00000 -1.50000 H26C 2 0.417673 0.423895 0.256272 11.00000 -1.50000 AFIX 0 C270 1 0.652476 0.411703 0.296022 11.00000 0.11936 0.09822 = 0.12682 0.00161 0.05959 0.00364 AFIX 23 H27A 2 0.649215 0.435464 0.250632 11.00000 -1.20000 H27B 2 0.673507 0.356498 0.297277 11.00000 -1.20000 AFIX 0 C280 1 0.706614 0.460440 0.352094 11.00000 0.08766 0.25951 = 0.26929 -0.08880 0.03702 -0.02071 AFIX 137 H28A 2 0.683061 0.513490 0.353146 11.00000 -1.50000 H28B 2 0.758462 0.466291 0.343592 11.00000 -1.50000 H28C 2 0.713947 0.433615 0.396446 11.00000 -1.50000 AFIX 0 HKLF 4 REM 007-15133 REM R1 = 0.0916 for 7236 Fo > 4sig(Fo) and 0.1103 for all 9359 data REM 642 parameters refined using 6 restraints END WGHT 0.1626 8.7160 REM Highest difference peak 1.338, deepest hole -0.448, 1-sigma level 0.080 Q1 1 0.6097 0.8948 0.5339 11.00000 0.05 1.34 Q2 1 0.6630 0.8834 0.4277 11.00000 0.05 0.99 Q3 1 0.5069 0.7869 0.5460 11.00000 0.05 0.93 Q4 1 0.7242 0.8374 0.3677 11.00000 0.05 0.88 Q5 1 0.6631 0.7336 0.3697 11.00000 0.05 0.80 Q6 1 0.6080 0.6025 0.3397 11.00000 0.05 0.73 Q7 1 0.4557 0.5739 0.4312 11.00000 0.05 0.73 Q8 1 0.5470 0.6361 0.3829 11.00000 0.05 0.66 Q9 1 0.4965 0.6510 0.4892 11.00000 0.05 0.66 Q10 1 0.8578 0.6112 0.6319 11.00000 0.05 0.58 Q11 1 0.4800 0.7008 0.5961 11.00000 0.05 0.47 Q12 1 0.9979 0.6252 0.4130 11.00000 0.05 0.45 Q13 1 0.6338 0.6646 0.3146 11.00000 0.05 0.44 Q14 1 0.7212 0.9077 0.4031 11.00000 0.05 0.42 Q15 1 0.4799 0.7337 0.2483 11.00000 0.05 0.42 Q16 1 0.5990 0.7090 0.4774 11.00000 0.05 0.40 Q17 1 0.9392 0.8420 0.6570 11.00000 0.05 0.40 Q18 1 0.1794 0.8735 0.5210 11.00000 0.05 0.37 Q19 1 0.7741 0.4642 0.8128 11.00000 0.05 0.36 Q20 1 1.1072 0.6411 0.6034 11.00000 0.05 0.36 ; _shelx_res_checksum 47635 _shelx_hkl_file ; 0 0 2 2558.81 70.58 0 0 -2 2500.10 68.62 0 0 -2 2892.15 79.57 0 0 2 2730.98 75.27 0 0 2 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6.94 0 -10 7 20.98 5.22 0 -10 7 23.55 5.48 0 -10 7 21.44 4.88 0 -10 -7 25.36 6.42 0 -10 -7 21.62 14.00 0 10 8 82.36 14.38 0 -10 -8 62.58 11.70 0 -10 -8 71.81 15.65 0 10 8 75.71 10.69 0 -10 8 67.22 9.59 0 10 8 67.28 11.36 0 -10 8 57.22 8.36 0 -10 8 59.34 11.72 0 10 -8 55.06 6.09 0 -10 -8 46.03 8.36 0 10 8 39.03 6.44 0 -10 -8 30.17 6.61 0 10 8 32.93 6.49 0 -10 8 44.07 8.17 0 -10 -8 36.78 6.08 0 -10 -8 29.66 8.58 0 -10 8 33.88 6.12 0 -10 -8 22.54 7.00 0 -10 -8 24.02 5.73 0 -10 8 22.26 5.21 0 -10 -8 28.54 6.49 0 -10 8 26.18 7.16 0 10 8 18.42 4.67 0 -10 8 30.71 9.67 0 -10 -8 18.57 8.63 0 -10 8 27.69 9.74 0 -10 8 22.28 5.96 0 -10 8 19.93 4.58 0 -10 -8 20.56 6.35 0 -10 -8 17.96 11.69 0 10 9 68.85 9.88 0 -10 -9 67.31 9.81 0 -10 -9 44.58 12.73 0 10 9 59.87 9.77 0 -10 9 53.18 8.12 0 10 -9 50.65 8.97 0 10 9 69.84 9.75 0 -10 9 58.53 10.00 0 10 -9 94.91 13.15 0 -10 -9 60.64 9.56 0 10 9 81.94 11.07 0 -10 -9 80.83 11.14 0 10 9 91.86 12.73 0 -10 9 71.92 11.37 0 -10 -9 76.86 10.42 0 -10 -9 83.78 14.70 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122.88 10.58 0 -11 6 113.49 10.09 0 -11 -6 150.48 12.63 0 -11 6 82.06 11.19 0 -11 -6 129.07 10.67 0 -11 -6 114.43 10.98 0 -11 6 128.05 9.98 0 -11 -6 105.04 9.36 0 -11 6 88.67 12.74 0 -11 -6 130.03 10.77 0 -11 6 93.93 18.14 0 11 6 92.68 13.05 0 -11 6 100.13 11.28 0 -11 -6 88.54 26.64 0 -11 6 91.23 15.31 0 -11 6 98.67 9.39 0 -11 6 85.79 12.11 0 -11 -6 106.43 8.80 0 -11 -6 88.95 24.07 0 -11 -7 -6.67 11.36 0 11 7 3.53 6.53 0 -11 7 7.14 3.93 0 11 -7 6.26 6.22 0 11 7 1.66 6.42 0 -11 7 1.49 5.14 0 11 -7 5.03 5.19 0 -11 -7 5.32 6.06 0 11 7 11.91 3.89 0 -11 7 10.14 3.76 0 -11 -7 8.69 3.19 0 -11 -7 14.93 5.11 0 -11 7 12.28 3.03 0 -11 -7 14.03 3.75 0 -11 7 11.30 3.53 0 -11 -7 13.77 5.44 0 -11 7 12.59 5.12 0 11 7 7.55 3.94 0 -11 7 21.79 7.32 0 -11 -7 17.47 5.16 0 -11 7 24.08 7.75 0 -11 7 15.51 5.72 0 -11 7 10.08 3.02 0 -11 -7 11.72 3.75 0 -11 -7 15.27 6.65 0 -11 -8 117.23 15.77 0 11 8 122.97 13.25 0 -11 8 107.81 11.18 0 11 -8 115.98 12.10 0 11 8 128.39 12.69 0 -11 8 112.18 13.63 0 11 -8 107.13 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-3 167.43 11.81 4 -3 -2 10.54 2.59 4 3 -2 15.10 3.07 -4 3 2 13.32 3.09 -4 -3 2 16.54 2.91 -4 -3 2 14.09 2.31 4 -3 -2 14.79 5.97 -4 -3 2 18.60 3.69 4 3 -2 21.72 2.51 -4 3 2 22.08 2.39 -4 -3 2 20.22 3.65 4 3 -2 28.86 4.10 4 -3 -2 16.95 3.01 4 3 -2 21.33 2.80 4 -3 -2 22.30 5.15 -4 -3 2 27.23 4.11 4 -3 -1 2043.92 57.08 4 3 -1 1983.68 55.07 -4 3 1 2174.15 69.26 -4 -3 1 2162.04 61.09 -4 -3 1 1886.57 55.63 4 -3 -1 2146.59 60.19 -4 3 1 1958.90 54.67 -4 3 1 1604.01 82.13 4 3 -1 1902.85 52.94 4 -3 -1 2067.42 56.65 -4 3 1 1965.18 54.25 -4 -3 1 2006.85 55.69 4 3 -1 1940.02 53.88 4 3 -1 2115.84 58.45 4 -3 -1 2063.27 56.68 -4 -3 1 2070.74 57.35 4 -3 0 283.08 16.64 4 3 0 286.86 18.28 -4 3 0 315.47 16.63 -4 -3 0 335.53 18.55 -4 -3 0 296.05 4.62 4 -3 0 292.97 9.95 4 3 0 323.27 17.21 -4 3 0 294.44 3.13 -4 3 0 256.89 15.46 4 3 0 289.02 20.85 4 -3 0 280.41 29.43 -4 3 0 269.81 18.95 -4 -3 0 270.78 29.52 4 3 0 296.16 12.88 4 -3 0 254.49 27.76 4 -3 0 291.15 20.43 4 3 0 265.75 15.94 -4 3 0 318.33 19.93 -4 -3 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456.45 26.20 4 4 -7 491.74 28.24 4 -4 -7 413.27 21.52 -4 4 7 473.28 26.28 -4 -4 7 520.40 29.79 -4 -4 7 598.97 43.36 4 4 -7 377.94 19.52 4 -4 -7 462.39 24.40 4 -4 -7 493.82 28.53 4 4 -6 429.32 22.63 -4 4 6 390.00 22.58 -4 -4 6 420.91 13.67 4 -4 -6 374.82 23.28 4 -4 -6 443.98 24.30 -4 4 6 428.27 24.88 -4 -4 6 408.36 27.79 4 4 -6 437.97 22.49 4 -4 -6 376.24 22.16 -4 4 6 330.17 29.09 -4 -4 6 400.54 21.09 -4 -4 6 431.17 35.63 4 4 -6 382.38 21.01 4 -4 -6 431.28 26.51 4 -4 -6 380.56 21.10 4 4 -5 122.04 8.86 -4 4 5 115.31 9.05 -4 -4 5 133.38 10.90 4 -4 -5 120.57 9.56 4 -4 -5 141.88 9.27 -4 4 5 131.25 8.65 -4 -4 5 138.84 8.59 4 4 -5 131.13 8.82 4 -4 -5 133.89 8.88 -4 4 5 140.13 9.00 -4 -4 5 130.60 8.81 4 4 -5 147.21 12.00 4 4 -5 115.19 7.63 4 -4 -5 136.51 8.47 -4 -4 5 110.59 7.88 4 -4 -5 146.58 9.77 4 4 -4 1162.49 60.30 -4 4 4 1055.24 61.02 -4 -4 4 1197.47 66.00 4 -4 -4 1096.36 70.41 4 -4 -4 1304.41 71.83 -4 4 4 1231.79 63.58 -4 -4 4 1271.24 66.68 4 4 -4 1251.25 65.31 4 -4 -4 1242.00 63.78 -4 4 4 1278.95 66.06 -4 -4 4 1217.37 63.08 4 4 -4 1421.29 76.68 4 -4 -4 1233.06 63.63 -4 -4 4 1046.03 62.47 4 -4 -4 1206.97 62.65 4 4 -3 15.27 3.28 -4 4 3 13.15 2.77 -4 -4 3 18.19 3.60 4 -4 -3 14.27 3.03 4 -4 -3 12.69 5.04 -4 4 3 17.95 3.03 -4 -4 3 19.25 3.51 4 4 -3 19.24 3.48 4 -4 -3 18.38 3.84 -4 4 3 17.90 3.23 -4 -4 3 19.88 4.98 4 4 -3 18.82 5.15 4 4 -3 20.58 3.36 4 -4 -3 18.83 4.04 -4 -4 3 16.58 3.93 4 -4 -3 21.42 3.25 4 -4 -2 1595.93 91.37 4 4 -2 1761.42 48.54 -4 4 2 1782.60 62.68 -4 -4 2 2042.88 67.52 -4 -4 2 1745.78 48.01 4 -4 -2 1866.02 57.64 -4 4 2 2076.05 57.24 -4 -4 2 2089.20 58.94 4 4 -2 2080.76 58.71 4 -4 -2 1941.16 52.97 -4 4 2 2004.63 54.65 -4 -4 2 1951.58 53.55 4 4 -2 1925.67 63.61 4 -4 -2 1854.08 50.66 4 4 -2 1759.43 49.06 4 -4 -2 2026.60 55.20 -4 -4 2 1982.23 54.94 4 -4 -2 2032.85 56.45 4 -4 -1 322.18 16.46 4 4 -1 335.35 16.80 -4 4 1 325.66 19.62 -4 -4 1 371.73 18.38 -4 -4 1 301.59 16.51 4 -4 -1 278.19 17.04 -4 4 1 348.44 17.22 -4 -4 1 377.52 18.43 4 4 -1 310.07 15.71 4 -4 -1 367.15 20.25 -4 4 1 360.35 18.19 -4 -4 1 362.22 18.31 4 4 -1 356.10 17.74 4 -4 -1 340.94 16.63 4 4 -1 379.05 19.28 4 -4 -1 377.06 19.75 -4 -4 1 362.43 18.12 4 -4 -1 369.41 18.82 4 -4 0 89.67 5.97 4 4 0 86.56 11.59 -4 4 0 91.08 6.78 -4 -4 0 110.25 12.04 -4 -4 0 93.88 6.49 4 -4 0 104.41 7.31 4 4 0 110.57 7.37 -4 4 0 101.00 6.72 4 4 0 105.61 7.34 4 -4 0 106.62 9.57 -4 4 0 104.61 7.13 -4 -4 0 107.74 8.70 4 4 0 118.80 8.57 4 -4 0 98.12 6.65 4 -4 0 113.80 8.81 -4 4 0 133.47 8.99 -4 -4 0 114.79 7.80 4 -4 1 58.11 5.20 4 4 1 58.30 7.95 -4 4 -1 59.71 5.62 -4 -4 -1 67.06 10.30 -4 -4 -1 63.49 5.85 4 -4 1 69.56 6.73 4 4 1 62.04 5.85 4 -4 1 62.13 5.84 4 4 1 57.31 7.86 4 -4 1 58.83 5.87 -4 4 -1 57.26 5.49 -4 -4 -1 61.32 11.65 4 4 1 62.60 10.49 4 -4 1 52.46 5.32 4 -4 1 55.58 6.08 -4 4 -1 51.88 6.38 -4 -4 -1 50.34 5.75 4 -4 2 60.39 5.45 4 4 2 60.76 6.14 -4 4 -2 59.71 5.64 -4 -4 -2 64.88 6.84 -4 -4 -2 66.70 6.61 4 -4 2 72.03 6.74 4 4 2 75.25 7.16 4 -4 2 73.53 6.84 4 4 2 70.78 6.74 4 -4 2 70.21 7.12 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12.64 -8 -6 4 132.49 14.00 -8 -6 4 152.65 13.66 8 -6 -4 142.89 3.99 8 -6 -4 180.79 16.33 8 6 -4 134.93 14.11 8 -6 -4 170.59 16.35 -8 -6 4 209.42 17.88 -8 -6 4 171.20 14.75 -8 -6 4 208.91 21.27 -8 -6 4 195.96 18.93 8 -6 -4 193.60 17.82 -8 -6 4 233.17 22.64 8 6 -4 212.26 18.64 8 -6 -4 226.67 20.38 -8 6 4 184.39 16.16 -8 -6 4 212.82 18.13 8 -6 -4 222.63 20.06 8 -6 -3 250.70 21.47 8 6 -3 293.16 23.36 -8 6 3 192.97 18.64 -8 -6 3 282.03 23.11 8 -6 -3 274.83 23.21 -8 -6 3 258.13 23.28 8 6 -3 254.63 22.18 8 -6 -3 266.93 4.42 -8 6 3 286.45 22.30 -8 -6 3 254.27 22.01 8 6 -3 259.69 23.11 8 -6 -3 252.39 21.77 -8 6 3 281.03 22.81 -8 -6 3 243.01 21.90 8 6 -3 230.56 19.70 -8 -6 3 249.20 22.26 -8 -6 3 264.33 4.85 8 -6 -3 282.79 23.18 8 -6 -3 286.09 24.90 -8 -6 3 246.38 24.33 -8 -6 3 263.55 5.21 -8 -6 3 284.19 27.95 -8 -6 3 303.77 27.15 8 -6 -3 296.27 24.36 -8 -6 3 372.14 35.54 8 6 -3 318.02 25.43 8 -6 -3 296.93 23.11 8 -6 -3 344.50 28.32 -8 -6 3 328.25 25.54 8 -6 -3 352.52 29.08 8 -6 -2 370.28 29.29 8 6 -2 387.85 31.02 -8 6 2 310.69 31.08 -8 -6 2 345.79 30.80 8 -6 -2 370.19 30.92 8 6 -2 430.25 34.63 8 6 -2 351.74 29.12 8 -6 -2 437.41 33.93 -8 6 2 426.41 33.36 -8 -6 2 430.39 34.71 8 6 -2 404.63 32.01 8 -6 -2 429.31 33.51 -8 6 2 492.12 39.32 -8 -6 2 421.29 34.29 8 6 -2 336.83 27.49 -8 -6 2 378.40 31.38 -8 -6 2 457.67 35.33 8 -6 -2 409.05 33.32 8 -6 -2 464.38 35.89 8 -6 -2 456.70 38.88 -8 -6 2 548.37 42.32 -8 -6 2 408.41 31.89 8 6 -2 492.43 39.71 -8 -6 2 463.70 39.33 8 -6 -2 547.93 44.43 -8 -6 2 586.70 50.22 8 6 -2 439.50 35.21 8 -6 -2 598.23 47.25 -8 -6 2 529.63 41.13 8 -6 -2 561.05 47.14 8 -6 -1 1.97 2.14 8 6 -1 -1.26 2.85 -8 -6 1 -1.15 2.88 8 -6 -1 1.20 3.47 8 6 -1 6.65 3.82 8 6 -1 3.13 3.37 8 -6 -1 -1.09 4.29 -8 6 1 1.66 3.08 -8 -6 1 1.50 3.52 8 6 -1 0.17 3.80 8 -6 -1 0.35 2.05 8 -6 -1 0.65 4.35 -8 6 1 0.94 4.71 -8 -6 1 4.53 3.70 8 6 -1 4.75 1.81 -8 -6 1 4.35 2.18 -8 -6 1 0.58 2.61 -8 -6 1 5.55 2.94 8 -6 -1 4.96 3.99 8 -6 -1 6.07 3.17 8 -6 -1 4.99 3.75 -8 -6 1 6.00 2.96 -8 -6 1 5.11 2.05 8 6 -1 7.26 3.83 -8 -6 1 5.32 4.03 -8 -6 1 9.00 3.36 8 -6 -1 5.06 5.19 8 6 -1 9.78 4.28 8 6 -1 6.64 3.48 8 -6 -1 8.26 4.62 -8 -6 1 9.03 2.94 -8 -6 1 7.84 3.29 8 -6 -1 11.10 5.80 8 -6 0 25.00 5.20 8 6 0 37.19 6.59 -8 6 0 21.95 4.97 -8 -6 0 32.80 6.35 -8 -6 0 32.20 5.44 8 -6 0 29.50 4.28 8 6 0 26.53 6.20 8 6 0 23.68 6.10 8 -6 0 30.37 5.38 -8 6 0 25.40 5.38 8 6 0 24.71 6.22 8 -6 0 30.01 2.49 8 -6 0 31.72 5.61 -8 6 0 22.18 6.02 -8 -6 0 34.77 7.39 8 6 0 29.40 2.33 -8 -6 0 33.92 5.61 -8 -6 0 26.24 5.62 -8 -6 0 26.58 5.69 8 -6 0 27.51 5.54 8 -6 0 29.60 2.80 8 -6 0 27.21 5.77 8 -6 0 36.10 6.49 -8 -6 0 26.63 5.92 -8 -6 0 24.55 5.05 8 6 0 24.77 5.62 -8 -6 0 35.69 6.14 -8 -6 0 31.70 5.49 8 -6 0 41.65 7.14 8 6 0 28.69 3.31 8 6 0 35.54 5.92 8 -6 0 40.23 6.73 8 -6 0 48.08 7.64 -8 -6 0 30.51 4.91 8 -6 0 40.66 8.29 8 6 1 -0.17 4.13 -8 -6 -1 -2.79 6.01 -8 -6 -1 2.91 2.67 8 -6 1 6.89 3.84 8 6 1 2.13 3.03 8 6 1 4.83 3.17 8 -6 1 -0.35 4.91 -8 -6 -1 0.68 2.82 8 6 1 4.13 4.17 8 -6 1 3.89 2.18 8 -6 1 2.53 3.24 -8 6 -1 8.05 5.68 -8 -6 -1 4.86 3.71 8 6 1 2.05 1.92 -8 -6 -1 2.39 2.60 -8 -6 -1 1.93 2.59 -8 -6 -1 3.13 2.51 8 -6 1 7.19 3.95 8 -6 1 4.48 2.37 8 -6 1 5.33 2.84 -8 -6 -1 3.64 3.30 -8 -6 -1 2.57 1.35 8 6 1 3.84 4.96 -8 -6 -1 6.76 4.07 -8 -6 -1 4.38 4.88 8 -6 1 4.96 3.73 8 6 1 3.42 4.92 8 6 1 5.81 3.49 8 -6 1 5.19 2.78 8 -6 1 0.30 3.83 -8 -6 -1 1.89 1.85 -8 -6 -1 3.09 3.80 8 -6 1 5.56 4.71 8 6 2 16.85 9.11 -8 -6 -2 20.66 8.97 -8 6 -2 25.99 7.20 8 6 2 30.87 6.49 8 6 2 31.10 6.18 8 -6 2 29.64 7.64 -8 -6 -2 32.99 7.01 8 6 2 38.91 8.06 8 -6 2 37.22 7.11 8 -6 2 34.51 8.52 -8 6 -2 47.33 9.95 -8 -6 -2 39.73 7.89 8 6 2 41.47 7.82 -8 -6 -2 47.19 8.81 -8 -6 -2 53.45 7.51 -8 -6 -2 56.53 7.58 8 -6 2 74.15 10.09 8 -6 2 73.66 9.88 8 -6 2 78.54 10.75 -8 -6 -2 84.74 11.41 -8 -6 -2 59.07 7.83 8 6 2 93.02 12.70 8 -6 2 78.58 10.41 8 6 2 88.54 12.63 8 -6 2 93.90 12.75 -8 -6 -2 68.36 9.48 8 6 3 23.23 21.31 -8 -6 -3 23.92 13.26 -8 6 -3 28.51 10.65 8 6 3 41.21 8.44 8 6 3 27.63 5.79 8 -6 3 25.61 10.53 -8 -6 -3 26.12 7.59 8 6 3 34.70 14.69 8 -6 3 39.20 7.83 8 -6 3 33.76 9.71 -8 6 -3 59.55 9.37 -8 -6 -3 45.35 9.11 8 6 3 34.44 8.26 -8 -6 -3 41.97 9.48 -8 -6 -3 50.98 9.66 -8 -6 -3 51.55 9.45 8 -6 3 63.08 9.22 8 -6 3 57.18 8.21 8 -6 3 64.90 9.96 -8 -6 -3 65.77 9.66 -8 -6 -3 42.89 7.89 8 6 3 74.26 10.42 8 -6 3 64.87 8.73 8 6 3 80.16 11.05 -8 -6 -3 71.06 10.62 8 -6 3 74.07 11.53 8 6 3 76.15 11.70 8 -6 3 65.57 8.79 8 6 3 56.72 8.27 8 -6 3 66.96 9.37 8 -6 3 73.99 10.52 -8 -6 -3 71.94 10.44 8 -6 3 79.53 12.69 -8 -6 -4 22.22 21.15 -8 6 -4 26.35 9.75 8 6 4 27.32 6.67 8 -6 4 28.07 11.95 -8 -6 -4 30.10 7.83 8 6 4 35.96 7.51 8 -6 4 39.79 7.41 8 -6 4 43.57 9.66 -8 6 -4 44.95 7.74 -8 -6 -4 39.44 7.37 8 6 4 37.01 7.23 -8 -6 -4 30.57 7.30 -8 -6 -4 45.88 7.32 -8 -6 -4 49.27 7.43 -8 -6 -4 81.24 9.39 8 -6 4 57.15 8.82 8 -6 4 65.51 10.15 -8 -6 -4 64.67 9.80 8 6 4 64.00 10.98 8 -6 4 75.31 9.27 8 6 4 77.70 10.75 -8 -6 -4 69.43 6.48 8 -6 4 81.91 10.46 8 6 4 85.77 10.85 8 -6 4 77.04 9.36 8 -6 4 82.99 10.36 8 -6 4 88.54 11.77 8 -6 4 97.08 13.11 8 6 5 11.41 4.62 -8 -6 -5 10.70 4.35 -8 6 -5 10.83 5.26 -8 -6 -5 13.28 4.23 8 6 5 3.05 5.15 8 -6 5 8.85 5.09 8 6 5 9.86 6.24 8 -6 5 10.84 4.18 8 -6 5 8.56 3.61 -8 6 -5 6.32 4.39 -8 -6 -5 9.98 4.51 8 6 5 8.00 2.31 -8 -6 -5 10.13 3.07 8 6 5 8.82 2.79 -8 -6 -5 10.56 3.15 8 -6 5 8.81 4.47 8 -6 5 7.71 3.67 8 -6 5 6.35 4.25 -8 -6 -5 7.35 2.49 8 6 5 3.59 5.56 8 -6 5 10.90 4.94 8 6 5 3.03 4.36 -8 -6 -5 8.53 4.50 8 -6 5 3.81 5.14 8 6 5 10.38 6.59 8 -6 5 7.45 2.71 8 -6 5 4.51 3.63 8 -6 5 9.26 4.13 -8 -6 -5 14.35 5.49 8 -6 5 11.42 5.10 8 6 6 75.75 10.56 -8 -6 -6 75.35 10.70 -8 6 -6 62.44 10.24 -8 -6 -6 76.83 11.25 8 6 6 69.63 10.09 8 -6 6 70.79 10.02 8 6 6 64.28 9.60 8 -6 6 72.91 10.31 8 -6 6 62.21 8.84 -8 -6 -6 68.04 10.09 8 6 6 66.43 8.88 -8 -6 -6 69.05 9.28 8 6 6 68.33 9.67 -8 -6 -6 75.50 10.62 8 -6 6 75.02 10.33 8 -6 6 68.78 9.68 8 -6 6 74.98 10.48 -8 -6 -6 63.49 8.73 8 6 6 69.54 9.98 8 -6 6 73.63 10.56 8 6 6 82.16 11.59 -8 -6 -6 74.73 10.90 8 6 6 69.13 10.31 8 -6 6 69.65 9.79 8 -6 6 70.67 9.78 8 -6 6 65.84 9.60 -8 -6 -6 89.65 13.82 8 -6 6 65.87 10.79 8 6 7 5.83 4.00 -8 -6 -7 7.03 3.80 -8 6 -7 9.40 4.34 -8 -6 -7 5.89 4.05 8 6 7 7.88 4.22 8 -6 7 8.91 3.86 8 6 7 7.41 6.15 8 -6 7 6.50 5.42 8 -6 7 3.70 4.94 -8 -6 -7 7.83 5.48 8 6 7 4.39 2.49 -8 -6 -7 4.57 2.36 8 6 7 3.58 3.73 -8 -6 -7 5.39 3.64 8 -6 7 11.02 4.91 8 -6 7 6.12 4.01 8 -6 7 11.89 5.54 -8 -6 -7 4.59 3.60 8 6 7 4.48 3.84 8 -6 7 5.11 4.77 8 6 7 16.14 7.49 -8 6 -7 8.28 5.38 -8 -6 -7 3.24 4.58 8 6 7 8.97 7.19 8 -6 7 7.13 5.39 8 -6 7 12.03 4.76 8 -6 7 6.99 5.17 -8 -6 -7 6.65 7.98 8 -6 7 10.72 4.92 8 6 8 14.90 4.18 -8 -6 -8 19.30 5.57 -8 6 -8 21.14 5.57 -8 -6 -8 20.34 5.05 8 6 8 10.29 5.68 8 -6 8 17.76 5.55 8 6 8 21.48 5.45 8 -6 8 12.03 5.17 -8 6 -8 18.70 5.34 -8 -6 -8 16.81 4.59 8 6 8 18.92 3.77 -8 -6 -8 20.49 3.92 8 6 8 14.90 5.74 -8 -6 -8 13.67 4.01 8 -6 8 18.65 4.48 8 -6 8 17.62 4.18 8 -6 8 17.37 4.65 -8 -6 -8 12.50 2.60 8 6 8 10.58 4.54 8 -6 8 15.94 4.71 8 6 8 10.36 6.24 8 -6 8 12.59 3.40 -8 -6 -8 18.13 6.00 8 6 8 9.03 4.96 8 -6 8 12.50 5.39 8 -6 8 5.09 4.67 8 -6 8 12.82 4.48 -8 -6 -8 15.00 5.85 8 -6 8 9.48 7.51 8 6 9 14.55 3.98 -8 -6 -9 5.93 4.45 -8 6 -9 0.99 5.86 -8 -6 -9 6.50 5.08 8 6 9 3.41 4.25 8 -6 9 2.01 5.66 8 6 9 4.90 6.36 8 -6 9 6.72 5.45 -8 6 -9 1.73 6.18 -8 -6 -9 1.89 4.65 8 6 9 4.58 3.67 -8 -6 -9 1.58 3.23 8 6 9 7.54 3.98 -8 -6 -9 -0.30 4.62 8 -6 9 5.26 3.73 8 -6 9 4.38 3.43 8 -6 9 0.07 4.64 8 6 9 0.79 5.14 8 -6 9 2.05 3.76 8 6 9 -0.02 5.96 8 -6 9 7.36 5.42 -8 -6 -9 2.80 4.27 8 6 9 0.62 6.32 8 -6 9 1.00 6.37 8 -6 9 4.71 5.16 8 -6 9 -1.40 5.04 -8 6 -9 -0.41 9.81 -8 -6 -9 9.20 8.82 8 6 10 116.31 12.05 -8 -6 -10 108.88 11.35 -8 -6 -10 98.41 11.59 8 6 10 69.36 11.69 8 -6 10 86.65 9.86 8 6 10 65.96 10.79 8 -6 10 76.90 9.97 -8 6 -10 64.16 10.44 8 6 10 88.54 9.49 -8 -6 -10 92.45 10.18 8 6 10 63.87 10.46 -8 -6 -10 70.64 11.72 8 -6 10 73.14 12.39 8 -6 10 75.28 3.93 8 -6 10 64.70 12.04 8 6 10 55.26 9.20 8 -6 10 79.50 9.22 8 6 10 64.63 11.60 8 -6 10 77.56 8.92 -8 -6 -10 68.43 11.01 8 6 10 65.10 11.14 8 -6 10 74.90 6.95 8 -6 10 74.49 12.26 8 -6 10 66.42 11.64 -8 6 -10 45.77 9.45 -8 -6 -10 74.31 14.60 8 6 11 6.73 4.04 -8 -6 -11 10.56 4.32 8 6 11 3.53 5.79 -8 -6 -11 4.62 4.54 8 -6 11 7.70 3.95 8 -6 11 5.78 3.75 8 -6 11 8.67 4.38 8 6 11 3.75 4.13 8 -6 11 3.51 6.41 8 6 11 6.95 5.40 8 -6 11 5.16 4.92 -8 -6 -11 6.01 4.57 8 6 11 10.29 7.31 8 -6 11 7.41 5.42 8 -6 11 5.84 5.49 8 -6 11 4.47 5.14 -8 6 -11 4.22 7.05 -8 -6 -11 10.93 5.84 8 6 12 121.91 13.54 -8 -6 -12 144.53 15.86 8 6 12 116.24 13.59 -8 6 -12 111.73 13.79 -8 -6 -12 146.69 16.31 8 -6 12 148.90 16.67 8 -6 12 108.24 12.50 8 6 12 81.21 9.92 8 -6 12 146.98 16.54 8 6 12 118.37 15.22 8 -6 12 135.70 15.54 -8 -6 -12 129.02 14.46 8 6 12 108.20 13.44 8 -6 12 139.81 15.97 8 -6 12 143.62 16.49 8 -6 12 124.75 14.35 -8 6 -12 82.08 10.53 -8 -6 -12 147.19 16.76 8 6 13 2.85 3.09 -8 -6 -13 1.09 3.22 8 6 13 -3.36 4.86 -8 6 -13 4.97 4.39 -8 -6 -13 0.70 4.40 8 -6 13 0.50 3.32 8 -6 13 -2.50 3.88 8 -6 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81.68 10.91 8 7 5 71.93 10.14 -8 -7 -5 61.15 8.15 -8 -7 -5 69.28 9.40 8 -7 5 82.34 11.19 8 -7 5 74.67 10.01 8 -7 5 81.01 11.78 -8 -7 -5 63.94 8.87 -8 -7 -5 53.44 7.47 8 7 5 65.10 9.56 8 -7 5 71.86 10.02 8 7 5 75.63 11.08 -8 -7 -5 80.31 11.36 8 -7 5 74.54 11.12 8 7 5 76.26 11.39 8 -7 5 74.03 10.56 8 -7 5 81.71 11.85 8 -7 5 75.41 11.31 -8 -7 -5 67.12 10.65 8 -7 5 76.83 12.57 8 7 6 4.51 4.80 -8 -7 -6 3.23 3.93 -8 7 -6 3.77 4.30 -8 -7 -6 6.73 4.06 8 7 6 11.72 4.06 8 7 6 7.29 4.65 8 -7 6 8.67 3.67 8 -7 6 9.61 3.95 -8 -7 -6 8.55 4.57 8 7 6 7.55 2.42 -8 -7 -6 6.45 2.50 8 7 6 3.17 4.64 -8 -7 -6 10.09 3.01 8 -7 6 6.97 5.10 8 -7 6 6.33 3.26 8 -7 6 6.84 3.71 -8 -7 -6 4.91 3.26 8 7 6 5.37 4.09 8 -7 6 14.93 5.25 8 7 6 10.06 7.74 -8 -7 -6 3.02 4.96 8 -7 6 14.87 4.93 8 7 6 -1.43 6.14 8 -7 6 8.53 3.99 8 -7 6 9.68 4.38 8 -7 6 9.15 4.98 -8 -7 -6 7.30 5.91 8 -7 6 10.72 5.15 8 7 7 21.12 4.54 -8 -7 -7 17.61 4.82 -8 7 -7 16.33 6.58 -8 -7 -7 19.04 5.66 8 -7 7 15.24 5.20 8 -7 7 7.55 6.20 8 -7 7 10.88 4.35 8 7 7 3.69 2.74 -8 -7 -7 11.28 2.62 8 7 7 10.10 3.59 -8 -7 -7 9.04 4.36 8 -7 7 9.59 3.24 8 -7 7 9.03 3.29 8 -7 7 4.42 5.27 -8 -7 -7 8.63 3.55 8 7 7 1.56 4.24 8 -7 7 1.26 3.49 8 7 7 6.59 5.56 -8 -7 -7 10.69 6.83 8 7 7 2.53 4.85 8 -7 7 6.55 6.36 8 -7 7 11.22 5.46 8 -7 7 6.13 4.76 -8 -7 -7 10.18 5.60 8 -7 7 5.55 7.34 8 7 8 48.03 7.70 -8 -7 -8 45.52 7.90 -8 7 -8 35.11 6.85 -8 -7 -8 36.01 7.47 8 7 8 35.25 8.36 8 -7 8 39.69 7.89 8 7 8 31.97 6.89 8 -7 8 38.68 7.19 -8 7 -8 37.45 7.92 -8 -7 -8 38.28 6.77 8 7 8 41.22 3.22 -8 -7 -8 37.53 6.07 8 7 8 23.50 5.91 -8 -7 -8 40.84 3.14 8 -7 8 41.74 7.53 8 -7 8 35.27 6.33 8 -7 8 38.65 7.45 -8 -7 -8 30.71 5.52 8 7 8 29.35 6.74 8 -7 8 39.09 7.30 8 7 8 41.04 6.29 -8 -7 -8 31.12 6.45 8 7 8 31.57 7.39 8 -7 8 39.91 7.11 8 -7 8 40.99 4.22 8 -7 8 34.98 9.27 -8 -7 -8 28.31 6.53 8 -7 8 37.91 8.27 8 7 9 64.18 10.30 -8 -7 -9 48.20 9.15 -8 -7 -9 43.82 8.90 8 7 9 30.37 6.10 8 -7 9 43.51 7.70 8 7 9 29.41 5.73 8 -7 9 44.19 7.70 -8 7 -9 38.44 6.21 -8 -7 -9 44.12 8.05 8 7 9 52.18 9.03 -8 -7 -9 49.62 8.00 8 7 9 47.87 8.22 -8 -7 -9 58.78 10.10 8 -7 9 51.66 8.79 8 -7 9 51.36 8.71 8 -7 9 59.44 9.97 8 7 9 35.72 7.10 8 -7 9 61.50 11.25 8 7 9 55.78 11.02 8 -7 9 60.98 9.86 -8 -7 -9 55.01 9.39 8 7 9 49.99 8.88 8 -7 9 53.97 9.28 8 -7 9 54.37 9.97 8 -7 9 59.28 11.88 -8 7 -9 48.82 10.19 -8 -7 -9 61.48 11.52 8 7 10 24.65 5.98 -8 -7 -10 17.16 6.14 -8 7 -10 1.26 5.32 -8 -7 -10 1.90 5.11 8 7 10 3.87 4.51 8 -7 10 0.21 4.69 8 7 10 4.45 4.63 8 -7 10 4.64 4.28 -8 7 -10 -2.48 4.82 8 7 10 11.91 5.15 -8 -7 -10 -2.91 4.01 8 7 10 5.50 5.66 -8 -7 -10 6.78 5.83 8 -7 10 2.16 3.86 8 -7 10 0.82 3.82 8 -7 10 0.59 4.40 8 7 10 -2.91 4.73 8 -7 10 -2.08 6.02 8 7 10 -0.92 7.92 8 -7 10 3.41 5.67 8 7 10 -1.72 5.15 8 -7 10 7.08 5.09 8 -7 10 -2.49 7.18 8 -7 10 5.57 5.20 -8 7 -10 5.20 8.81 -8 -7 -10 5.12 7.07 8 7 11 58.27 7.54 -8 -7 -11 51.10 6.77 8 7 11 30.91 5.86 -8 -7 -11 47.76 7.97 8 -7 11 42.16 7.35 8 -7 11 50.94 6.84 8 -7 11 38.91 7.53 8 7 11 24.89 4.29 8 -7 11 48.93 8.15 8 7 11 28.04 7.23 8 -7 11 43.02 4.92 -8 -7 -11 34.68 6.99 8 7 11 32.39 8.00 8 -7 11 43.97 7.45 8 -7 11 40.26 6.59 8 -7 11 40.26 6.71 -8 7 -11 21.68 7.74 -8 -7 -11 39.16 7.72 8 7 12 7.07 6.53 -8 -7 -12 8.40 5.51 8 7 12 6.91 3.89 -8 7 -12 7.00 4.53 -8 -7 -12 13.48 5.46 8 -7 12 8.45 3.75 8 -7 12 13.98 3.78 8 -7 12 13.01 5.04 8 7 12 2.97 4.70 8 -7 12 8.24 5.04 -8 -7 -12 4.42 5.04 8 7 12 3.99 5.15 8 -7 12 4.36 7.18 8 -7 12 12.69 4.47 8 -7 12 8.51 6.43 -8 -7 -12 3.42 7.19 8 7 13 15.85 5.44 -8 -7 -13 15.19 3.66 8 7 13 11.72 5.20 -8 7 -13 10.44 4.64 -8 -7 -13 11.75 5.16 8 -7 13 9.40 3.89 8 -7 13 13.33 3.53 8 -7 13 11.29 5.54 8 7 13 6.58 4.88 8 -7 13 7.23 4.97 -8 -7 -13 6.18 6.00 8 7 13 6.89 4.32 8 -7 13 6.81 6.85 8 -7 13 7.77 4.30 8 -7 13 12.63 4.90 -8 -7 -13 11.08 6.21 8 7 14 18.49 3.09 -8 -7 -14 21.41 3.26 8 7 14 9.22 4.03 -8 7 -14 11.47 4.98 -8 -7 -14 17.33 4.28 8 -7 14 20.48 2.79 8 -7 14 15.54 4.23 8 -7 14 11.54 6.16 8 7 14 10.06 6.22 8 -7 14 7.82 5.93 8 7 14 9.27 3.19 8 -7 14 14.43 5.57 8 -7 14 14.72 3.81 8 -7 14 9.84 3.87 -8 -7 -14 10.94 10.31 8 7 15 21.82 3.42 -8 -7 -15 23.46 3.69 8 7 15 7.95 3.95 -8 7 -15 4.71 4.00 -8 -7 -15 17.25 4.68 8 -7 15 16.62 3.03 -8 7 -15 13.88 3.54 8 -7 15 18.86 4.41 8 7 15 14.75 4.16 8 -7 15 23.34 5.79 8 -7 15 12.14 3.86 8 -7 15 11.89 4.11 -8 -7 -15 16.58 7.31 8 7 16 2.99 3.00 -8 -7 -16 3.92 3.03 8 7 16 -0.41 3.24 -8 7 -16 -1.20 3.72 -8 -7 -16 5.98 5.08 8 -7 16 -0.58 2.36 -8 7 -16 0.56 3.71 8 -7 16 1.62 5.35 8 7 16 -0.65 4.41 8 -7 16 2.59 4.79 8 -7 16 5.63 4.15 8 -7 16 4.56 5.19 -8 8 21 7.02 3.96 8 -8 -21 9.78 3.90 -8 -8 21 5.06 4.40 8 -8 -21 8.22 4.40 8 8 -21 8.40 4.90 8 -8 -21 2.39 6.18 -8 8 21 2.53 4.81 -8 -8 21 3.63 5.00 -8 -8 21 -1.99 5.77 -8 -8 21 9.05 5.28 -8 -8 21 9.37 6.13 8 8 -21 2.73 6.08 8 8 -21 10.69 6.47 -8 8 20 2.16 3.69 8 -8 -20 1.50 3.47 -8 -8 20 2.33 5.39 8 -8 -20 6.81 4.68 8 8 -20 2.26 6.77 8 -8 -20 7.32 7.71 -8 8 20 8.17 4.96 -8 -8 20 6.41 4.77 -8 -8 20 -5.55 6.53 -8 -8 20 7.66 6.81 -8 -8 20 9.42 6.93 8 8 -20 6.45 7.74 8 8 -20 6.84 7.02 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10.48 6.31 -8 8 16 12.05 5.44 8 -8 -16 10.70 8.16 8 8 -16 2.45 6.83 8 -8 -16 1.10 10.24 -8 8 16 11.07 6.53 -8 -8 16 11.06 6.29 -8 -8 16 7.43 9.92 -8 -8 16 12.17 8.76 -8 -8 16 13.56 8.32 -8 -8 16 -0.27 8.98 8 8 -16 5.46 6.48 8 -8 -16 10.84 7.53 -8 8 16 6.89 9.48 -8 -8 16 -0.47 7.14 8 -8 -16 4.19 7.08 -8 8 15 155.30 17.33 8 -8 -15 154.51 17.49 -8 -8 15 172.05 19.56 -8 8 15 208.24 21.50 8 -8 -15 184.10 20.66 8 8 -15 186.93 21.85 8 -8 -15 170.33 34.09 -8 8 15 146.83 17.76 -8 -8 15 143.52 16.98 -8 -8 15 197.19 24.92 -8 -8 15 186.05 21.88 -8 -8 15 177.63 21.74 -8 -8 15 201.49 24.49 8 8 -15 164.75 19.13 8 -8 -15 165.00 18.71 -8 8 15 211.75 22.54 -8 -8 15 103.68 13.95 8 -8 -15 144.42 17.35 -8 8 14 6.50 6.35 8 -8 -14 0.04 5.71 8 -8 -14 1.75 6.35 -8 -8 14 -3.75 7.68 8 8 -14 4.17 6.30 -8 8 14 -1.34 5.51 -8 -8 14 5.31 4.33 8 8 -14 0.81 8.04 8 -8 -14 -0.99 5.08 -8 8 14 6.25 6.18 8 -8 -14 -0.50 5.52 -8 -8 14 -2.53 7.26 -8 -8 14 -1.44 3.61 8 -8 -14 1.84 6.15 8 8 -14 -2.90 5.72 8 -8 -14 -9.50 10.91 -8 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4.99 -8 -8 12 111.33 11.70 -8 -8 12 71.74 10.64 8 -8 -12 92.71 13.67 8 -8 -12 101.10 12.28 8 8 -12 106.75 12.15 8 -8 -12 124.74 16.70 -8 8 12 89.17 14.49 -8 -8 12 115.67 12.52 -8 -8 12 118.71 16.21 -8 -8 12 105.21 14.55 8 -8 -12 105.79 12.11 -8 -8 12 103.33 14.15 -8 -8 12 109.49 15.10 8 -8 -12 92.73 15.23 -8 8 12 137.14 15.22 -8 -8 12 95.60 16.10 8 -8 -12 108.57 13.60 8 -8 -11 26.80 7.08 -8 -8 11 26.58 6.24 8 8 -11 36.79 9.36 -8 8 11 33.93 8.11 -8 -8 11 31.45 7.43 8 8 -11 31.09 8.06 8 -8 -11 24.05 6.38 -8 8 11 37.60 8.97 -8 8 11 27.62 5.66 8 -8 -11 23.63 5.15 -8 -8 11 37.20 6.90 -8 -8 11 29.55 6.00 8 -8 -11 48.25 8.63 8 -8 -11 34.93 7.70 8 8 -11 37.16 8.21 8 -8 -11 50.87 10.13 -8 8 11 31.70 7.58 -8 -8 11 36.50 8.22 -8 -8 11 46.91 13.24 -8 -8 11 43.22 9.14 8 -8 -11 49.57 9.55 -8 -8 11 47.48 10.69 -8 -8 11 57.03 11.06 8 -8 -11 46.66 11.35 -8 8 11 64.05 11.89 -8 -8 11 39.40 9.59 8 -8 -11 51.73 11.20 8 -8 -10 9.66 4.54 -8 8 10 3.84 4.77 8 -8 -10 4.03 4.67 -8 -8 10 8.42 4.00 8 8 -10 2.76 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141.88 16.76 -10 -2 11 151.58 15.04 10 2 -11 198.71 16.74 10 -2 -11 179.46 15.37 10 -2 -11 154.87 17.38 -10 2 11 165.99 14.78 -10 -2 11 158.82 13.74 -10 2 11 168.74 13.44 -10 -2 11 180.05 14.25 -10 -2 11 151.92 15.01 -10 -2 11 132.21 11.98 10 2 -11 194.11 16.39 10 -2 -11 166.63 13.55 10 2 -11 159.32 15.08 10 -2 -11 198.16 18.52 -10 2 11 218.86 19.12 -10 -2 11 135.42 13.57 10 -2 -10 33.40 6.58 10 2 -10 35.56 6.43 -10 2 10 30.13 7.89 -10 -2 10 32.65 8.15 10 -2 -10 27.99 6.66 -10 -2 10 24.32 6.41 10 2 -10 24.94 7.35 10 -2 -10 24.36 8.30 -10 2 10 20.02 9.44 -10 -2 10 21.65 8.36 10 2 -10 16.68 6.44 10 2 -10 19.00 6.47 10 -2 -10 18.59 6.88 -10 2 10 14.42 4.38 -10 -2 10 16.57 4.30 -10 2 10 22.29 6.06 -10 -2 10 20.31 5.57 10 -2 -10 22.35 5.74 10 2 -10 19.97 5.73 -10 2 10 18.88 7.10 -10 -2 10 18.77 7.08 10 2 -10 14.53 4.71 10 -2 -10 15.13 7.11 10 -2 -10 23.53 6.42 -10 2 10 22.24 6.14 -10 -2 10 12.39 5.34 -10 2 10 21.88 5.54 -10 -2 10 15.15 4.23 -10 -2 10 20.32 5.52 -10 -2 10 16.28 4.85 10 2 -10 17.70 6.95 10 -2 -10 15.60 5.97 10 2 -10 15.89 6.16 10 -2 -10 24.91 10.14 -10 2 10 24.85 6.97 -10 -2 10 21.16 8.04 10 -2 -9 14.63 5.23 10 2 -9 16.49 4.96 -10 2 9 16.91 5.42 -10 -2 9 11.47 5.40 10 -2 -9 13.30 4.07 -10 -2 9 14.49 4.67 10 2 -9 14.89 6.22 10 -2 -9 24.77 9.22 -10 2 9 16.31 8.80 -10 -2 9 20.16 7.80 10 2 -9 15.82 6.44 10 2 -9 10.95 6.44 10 -2 -9 14.57 7.71 -10 2 9 19.59 5.51 -10 -2 9 16.51 4.79 -10 2 9 20.49 5.61 -10 -2 9 19.91 5.62 10 -2 -9 22.65 5.14 10 2 -9 22.34 5.55 -10 2 9 22.06 5.75 -10 -2 9 27.33 6.41 10 2 -9 22.24 6.04 10 -2 -9 20.08 6.21 10 -2 -9 23.38 6.18 -10 -2 9 23.28 6.02 -10 2 9 21.96 4.61 -10 -2 9 24.43 5.29 -10 -2 9 19.53 6.37 10 -2 -9 31.45 6.84 -10 -2 9 17.27 5.44 10 2 -9 22.82 6.72 10 -2 -9 26.41 6.73 10 2 -9 18.64 6.02 10 -2 -9 28.53 7.65 -10 2 9 32.57 7.99 -10 -2 9 32.13 7.78 10 -2 -8 1.79 5.16 10 2 -8 3.02 5.38 -10 2 8 -0.80 5.75 -10 -2 8 -3.18 6.31 10 -2 -8 1.60 3.34 -10 -2 8 1.05 3.14 10 2 -8 2.94 3.81 10 -2 -8 5.12 5.81 -10 2 8 -7.55 5.40 -10 -2 8 4.24 4.09 10 2 -8 6.01 4.82 10 2 -8 6.22 4.09 10 -2 -8 -0.34 5.50 -10 2 8 5.33 4.59 -10 -2 8 3.49 3.94 -10 2 8 3.18 4.29 -10 -2 8 -2.89 4.90 10 -2 -8 1.86 4.05 10 2 -8 -1.18 4.38 -10 2 8 4.53 4.15 -10 -2 8 1.26 3.44 10 -2 -8 4.17 1.81 10 2 -8 4.36 3.51 10 -2 -8 5.14 3.60 10 -2 -8 5.12 4.40 -10 -2 8 5.81 3.78 -10 -2 8 5.96 3.44 -10 -2 8 5.29 5.09 10 -2 -8 5.08 2.95 -10 -2 8 5.69 4.39 10 2 -8 9.85 5.21 10 -2 -8 4.86 3.96 10 2 -8 11.34 4.71 10 -2 -8 6.62 5.19 -10 2 8 6.99 5.05 -10 -2 8 6.35 5.37 10 -2 -7 92.32 10.36 10 2 -7 93.64 10.13 -10 2 7 88.72 10.56 -10 -2 7 93.03 10.61 10 -2 -7 54.61 10.25 -10 -2 7 75.85 8.32 10 2 -7 91.72 10.60 10 -2 -7 95.05 10.43 -10 2 7 83.17 9.40 -10 -2 7 82.87 9.72 10 2 -7 87.06 9.19 10 2 -7 78.39 9.78 10 -2 -7 95.02 10.44 -10 2 7 70.07 8.87 -10 -2 7 79.47 9.50 -10 2 7 97.17 10.61 -10 -2 7 95.48 10.85 10 -2 -7 92.66 10.47 10 2 -7 88.14 10.39 -10 2 7 68.96 8.96 -10 -2 7 99.95 10.89 10 -2 -7 71.98 7.40 10 2 -7 81.54 9.14 10 -2 -7 85.09 9.62 10 -2 -7 91.86 10.25 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105.17 10.96 10 -2 -4 86.22 9.66 10 2 -4 100.48 12.33 -10 2 4 113.28 11.58 -10 -2 4 86.54 9.80 10 -2 -4 71.79 7.90 10 2 -4 86.35 9.05 10 -2 -4 98.55 10.29 10 -2 -4 83.95 8.94 -10 2 4 139.50 14.59 -10 -2 4 88.22 11.68 10 2 -4 111.78 11.85 10 -2 -4 99.82 10.31 10 -2 -4 108.06 11.94 10 2 -4 111.71 11.98 10 -2 -4 113.52 11.65 10 -2 -4 106.90 11.98 10 2 -4 81.18 8.73 -10 -2 4 110.20 11.69 10 -2 -4 99.83 11.07 10 -2 -3 5.89 3.60 10 2 -3 9.60 3.90 -10 2 3 7.34 4.22 -10 -2 3 3.55 3.65 -10 2 3 4.97 3.05 -10 -2 3 7.61 3.18 10 2 -3 4.80 2.08 10 2 -3 8.62 4.44 10 -2 -3 7.80 4.11 -10 2 3 8.71 3.82 -10 -2 3 9.46 4.21 10 2 -3 7.08 3.84 10 -2 -3 10.03 3.87 10 -2 -3 5.61 4.30 10 2 -3 6.88 3.17 -10 2 3 10.04 4.67 -10 -2 3 8.64 4.38 -10 2 3 8.13 2.99 -10 -2 3 12.80 3.67 10 -2 -3 9.26 2.91 10 2 -3 7.66 3.29 -10 2 3 13.21 4.22 -10 -2 3 11.00 3.41 10 -2 -3 11.88 3.48 10 2 -3 8.74 3.48 10 -2 -3 10.94 3.57 10 -2 -3 11.72 3.12 -10 2 3 14.48 4.62 -10 -2 3 16.10 4.65 10 2 -3 11.37 4.75 -10 -2 3 19.39 6.29 10 -2 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85.66 8.92 -10 -2 1 97.91 10.43 10 2 -1 95.40 10.14 10 -2 -1 105.05 11.17 10 -2 -1 104.83 11.49 10 2 -1 93.29 9.85 -10 2 1 129.33 13.79 -10 -2 1 119.74 13.20 10 -2 -1 90.38 9.13 10 2 -1 94.20 9.56 -10 2 1 94.41 10.41 -10 -2 1 113.12 12.11 -10 2 1 106.90 11.27 -10 -2 1 131.10 13.28 10 -2 -1 124.79 12.64 10 2 -1 126.75 12.97 10 -2 -1 139.85 14.12 10 -2 -1 128.81 13.04 10 2 -1 150.63 13.19 -10 -2 1 144.66 14.59 10 2 0 7.32 4.58 10 -2 0 5.83 2.67 -10 -2 0 4.13 3.20 -10 2 0 3.07 5.06 -10 -2 0 4.54 3.11 10 2 0 -0.27 5.77 10 -2 0 5.79 3.73 -10 -2 0 4.70 2.59 10 2 0 5.33 6.60 10 -2 0 8.62 3.63 10 -2 0 -1.37 3.11 10 2 0 1.49 2.80 -10 2 0 4.15 4.09 -10 -2 0 9.94 5.66 10 2 0 1.14 2.59 10 -2 0 4.29 1.78 -10 -2 0 -2.59 3.32 -10 2 0 2.91 1.90 -10 -2 0 2.59 2.09 10 -2 0 1.15 3.14 10 2 0 2.01 2.43 10 -2 0 1.16 3.40 10 -2 0 0.87 2.31 -10 2 0 -0.25 3.44 -10 -2 0 0.04 4.00 10 2 0 -1.02 3.22 10 -2 0 6.10 2.99 -10 -2 0 -2.10 3.95 10 -2 0 -1.51 3.75 10 2 0 2.73 4.48 10 2 0 1.92 5.11 10 -2 0 1.27 3.24 10 -2 0 1.95 3.15 -10 -2 0 -0.06 4.16 10 -2 0 1.62 5.43 10 -2 1 123.81 11.89 10 2 1 129.96 12.80 -10 2 -1 112.81 11.30 -10 -2 -1 129.60 13.04 -10 2 -1 120.03 13.54 -10 -2 -1 115.18 11.53 10 2 1 136.34 13.31 10 -2 1 119.52 12.74 10 2 1 130.28 13.26 10 -2 1 136.17 13.21 10 -2 1 134.19 12.96 10 2 1 112.16 10.96 -10 2 -1 103.80 11.35 -10 -2 -1 122.79 12.40 10 -2 1 121.92 11.46 10 2 1 129.59 12.23 -10 2 -1 115.90 11.59 -10 -2 -1 140.92 13.74 -10 -2 -1 117.08 11.23 10 -2 1 133.22 13.02 10 2 1 121.23 11.60 10 2 1 105.83 10.13 10 -2 1 119.75 11.42 10 -2 1 109.29 10.87 -10 2 -1 97.24 6.14 -10 -2 -1 141.81 13.76 10 2 1 122.49 11.98 10 -2 1 124.53 11.98 10 2 1 110.45 10.65 -10 -2 -1 100.72 11.16 10 -2 1 130.50 13.47 10 2 1 111.89 11.37 10 -2 1 120.24 11.71 10 2 1 118.24 11.77 10 -2 1 110.16 10.84 10 -2 1 104.82 10.46 -10 -2 -1 88.71 13.19 10 -2 1 114.96 13.50 10 2 2 51.16 10.09 10 -2 2 58.15 7.93 -10 -2 -2 52.80 4.39 -10 2 -2 48.54 9.10 -10 2 -2 61.63 10.25 -10 -2 -2 56.34 8.01 10 2 2 54.88 12.12 10 -2 2 64.23 9.84 10 2 2 65.72 10.46 10 -2 2 59.05 8.73 10 -2 2 58.09 8.36 10 2 2 52.59 3.22 -10 2 -2 57.35 10.01 -10 -2 -2 63.60 9.22 10 2 2 48.02 9.03 10 -2 2 51.04 9.22 -10 -2 -2 48.08 9.28 -10 2 -2 45.13 8.56 10 -2 2 56.94 8.18 10 2 2 40.35 7.61 10 2 2 45.15 8.41 10 -2 2 56.06 7.66 10 -2 2 52.29 2.74 -10 2 -2 52.24 4.36 -10 -2 -2 58.48 8.58 10 2 2 56.60 9.16 10 -2 2 62.48 9.38 10 2 2 55.87 8.16 -10 2 -2 56.05 11.13 -10 -2 -2 66.01 9.75 10 2 2 54.55 8.36 10 -2 2 61.11 8.52 10 2 2 50.57 10.35 10 -2 2 54.38 8.12 10 -2 2 47.57 9.49 -10 -2 -2 61.69 10.06 10 -2 2 56.93 9.23 10 2 3 95.79 11.41 10 -2 3 84.39 9.81 -10 2 -3 83.63 10.29 -10 -2 -3 91.71 10.87 -10 2 -3 86.66 11.82 -10 -2 -3 101.74 12.74 10 2 3 105.11 12.85 10 -2 3 105.90 12.78 10 2 3 108.17 13.08 10 -2 3 118.51 14.31 10 -2 3 111.69 13.20 10 2 3 87.58 10.15 -10 2 -3 97.37 12.17 -10 -2 -3 113.95 13.90 10 -2 3 99.21 11.34 10 2 3 103.39 11.82 -10 2 -3 91.54 10.89 -10 -2 -3 120.09 13.79 10 -2 3 122.02 14.07 10 2 3 121.04 13.80 10 -2 3 115.25 13.43 10 2 3 88.22 10.04 10 -2 3 124.63 14.34 -10 2 -3 114.59 13.40 -10 -2 -3 115.61 13.50 10 2 3 122.74 14.92 10 -2 3 133.64 15.37 10 2 3 80.31 10.07 -10 2 -3 140.91 17.14 -10 -2 -3 153.82 12.78 10 2 3 131.01 15.37 10 -2 3 133.19 15.53 10 2 3 127.01 15.40 10 -2 3 123.94 14.60 10 -2 3 126.42 14.71 -10 -2 -3 155.20 12.51 10 -2 4 483.32 39.54 10 2 4 474.28 39.85 -10 -2 -4 496.47 42.16 -10 2 -4 460.89 37.83 -10 2 -4 484.91 40.64 -10 -2 -4 480.62 38.04 10 2 4 489.30 38.47 10 -2 4 495.08 38.24 10 2 4 516.36 6.87 10 -2 4 510.17 5.73 10 -2 4 472.30 36.20 -10 2 -4 477.45 38.61 -10 -2 -4 476.25 37.06 10 -2 4 451.45 34.55 10 2 4 454.77 34.90 -10 -2 -4 483.81 38.07 -10 2 -4 409.96 33.23 10 -2 4 531.08 9.50 10 2 4 562.64 13.37 10 -2 4 447.19 34.03 10 -2 4 482.70 37.51 -10 2 -4 393.92 31.46 -10 -2 -4 476.40 36.83 10 2 4 485.99 37.58 10 -2 4 526.99 5.57 10 2 4 372.02 32.53 -10 2 -4 471.79 42.12 -10 -2 -4 469.51 39.92 10 2 4 518.63 7.08 10 -2 4 476.25 36.43 10 2 4 442.29 34.07 10 -2 4 470.20 36.15 10 -2 4 419.24 32.26 -10 -2 -4 551.35 31.21 10 -2 4 413.98 35.23 10 -2 5 148.60 14.46 10 2 5 166.17 14.87 -10 2 -5 150.62 14.15 -10 -2 -5 153.23 13.72 -10 2 -5 146.75 14.36 -10 -2 -5 161.16 13.07 10 2 5 151.81 13.59 10 -2 5 169.63 15.37 10 2 5 151.36 12.45 10 -2 5 157.86 12.57 10 -2 5 141.41 12.05 -10 2 -5 132.40 11.62 10 -2 5 152.48 12.05 10 2 5 169.10 13.20 -10 2 -5 138.58 11.35 -10 -2 -5 151.90 11.92 10 -2 5 169.74 13.50 10 2 5 109.78 8.81 10 -2 5 132.25 10.53 10 -2 5 145.08 11.52 -10 -2 -5 127.25 10.50 10 2 5 151.55 12.38 10 -2 5 146.19 12.00 10 2 5 113.17 10.26 10 -2 5 139.06 10.82 -10 2 -5 108.16 10.62 -10 -2 -5 121.40 12.70 10 2 5 141.62 11.82 10 -2 5 131.29 10.58 10 2 5 117.00 10.02 10 -2 5 115.73 9.86 10 -2 5 110.46 9.88 10 -2 5 132.10 14.24 10 2 6 210.62 18.09 10 -2 6 217.44 17.21 -10 -2 -6 211.09 19.69 -10 2 -6 218.90 19.52 -10 2 -6 222.67 19.58 -10 -2 -6 188.99 16.54 10 2 6 203.54 16.06 10 -2 6 214.46 17.25 10 2 6 219.45 19.57 10 -2 6 213.21 19.46 10 -2 6 219.55 17.18 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5.69 10 -3 -7 19.64 5.89 -10 -3 7 19.07 5.03 10 3 -7 28.40 7.29 10 -3 -7 25.91 6.83 -10 3 7 30.16 7.29 -10 -3 7 26.01 7.94 10 3 -7 31.56 7.08 10 3 -7 21.15 5.37 10 -3 -7 22.84 7.54 -10 3 7 43.53 8.80 -10 -3 7 28.42 6.21 -10 3 7 21.49 4.69 -10 -3 7 19.75 5.42 10 -3 -7 26.33 5.63 10 3 -7 21.08 3.57 -10 3 7 45.45 9.54 -10 -3 7 31.79 7.45 10 -3 -7 27.61 5.81 10 3 -7 34.10 7.03 10 -3 -7 29.18 6.71 10 -3 -7 32.80 7.30 -10 -3 7 33.35 7.00 -10 -3 7 23.15 4.74 -10 -3 7 30.96 7.76 10 -3 -7 34.68 7.41 -10 -3 7 27.51 6.50 10 3 -7 42.29 8.58 10 -3 -7 37.12 7.34 10 3 -7 23.58 5.31 10 -3 -7 38.07 8.56 -10 3 7 47.67 9.26 -10 -3 7 41.72 9.59 10 -3 -7 35.74 7.35 10 -3 -6 15.41 4.41 10 3 -6 12.80 4.54 -10 3 6 15.79 4.79 -10 -3 6 11.63 5.27 -10 -3 6 26.05 5.66 10 3 -6 29.67 3.96 10 -3 -6 29.67 3.98 -10 3 6 29.08 3.88 -10 -3 6 34.16 8.69 10 3 -6 37.84 7.42 10 3 -6 27.99 6.30 10 -3 -6 35.84 7.87 -10 3 6 44.01 9.21 -10 -3 6 33.06 5.89 -10 3 6 43.45 6.97 -10 -3 6 31.91 6.25 10 -3 -6 44.54 7.46 10 3 -6 43.09 7.99 -10 3 6 36.21 7.13 -10 -3 6 52.71 8.41 10 -3 -6 44.53 7.30 10 3 -6 49.71 8.05 10 -3 -6 52.45 8.27 10 -3 -6 52.58 8.35 -10 -3 6 61.58 9.67 -10 -3 6 42.80 6.81 10 3 -6 58.89 9.16 -10 -3 6 42.85 6.64 10 -3 -6 62.12 9.77 -10 -3 6 51.03 9.36 10 3 -6 61.54 10.64 10 -3 -6 58.38 9.51 10 3 -6 38.96 6.42 10 -3 -6 56.46 9.89 -10 3 6 53.75 8.87 -10 -3 6 48.86 8.58 10 -3 -6 55.96 9.00 10 -3 -5 18.28 5.51 10 3 -5 13.56 4.91 -10 3 5 11.34 4.09 -10 -3 5 13.01 5.34 10 -3 -5 8.73 3.75 -10 -3 5 8.59 3.59 10 3 -5 10.00 4.57 10 -3 -5 7.72 5.33 -10 3 5 9.80 4.94 -10 -3 5 5.08 5.31 10 3 -5 9.26 4.04 10 3 -5 0.57 4.45 10 -3 -5 4.17 5.37 -10 3 5 7.66 4.27 -10 -3 5 3.98 4.46 -10 3 5 5.38 3.80 -10 -3 5 4.85 3.58 10 -3 -5 1.34 3.80 10 3 -5 4.24 4.21 -10 3 5 7.61 3.46 -10 -3 5 3.80 4.30 10 -3 -5 5.83 3.05 10 3 -5 5.68 3.23 10 -3 -5 8.49 3.42 10 -3 -5 7.30 3.52 -10 -3 5 5.57 5.56 10 3 -5 10.50 3.88 -10 -3 5 5.46 3.18 10 -3 -5 8.07 4.47 -10 -3 5 3.59 4.09 10 3 -5 12.22 4.70 10 -3 -5 6.32 3.57 10 -3 -5 7.31 7.30 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2.76 -10 3 2 7.14 3.84 -10 -3 2 10.18 4.21 10 3 -2 3.35 3.40 -10 -3 2 -2.54 2.99 -10 -3 2 8.04 5.25 10 -3 -2 6.18 5.05 10 3 -2 5.89 4.67 10 3 -2 1.60 4.61 10 -3 -2 6.26 3.23 10 -3 -2 4.79 4.44 -10 -3 2 4.33 2.65 10 -3 -2 8.99 4.64 10 -3 -1 50.77 7.76 10 3 -1 59.40 9.11 -10 3 1 42.95 7.12 -10 -3 1 45.48 7.19 -10 3 1 52.64 9.68 -10 -3 1 50.13 7.87 10 3 -1 39.32 6.30 10 3 -1 47.55 7.97 10 -3 -1 52.74 8.52 -10 3 1 41.27 6.59 -10 -3 1 42.27 6.87 10 3 -1 34.86 7.06 10 -3 -1 44.06 6.99 10 -3 -1 46.50 8.29 10 3 -1 37.11 6.14 -10 3 1 41.36 8.38 -10 -3 1 38.11 10.00 10 3 -1 42.16 6.37 -10 3 1 35.45 5.74 -10 -3 1 43.50 6.87 -10 3 1 25.62 5.35 -10 -3 1 40.76 6.72 10 -3 -1 33.19 5.42 10 3 -1 33.06 5.60 10 -3 -1 41.46 6.97 10 -3 -1 37.71 6.10 -10 3 1 36.68 6.64 -10 -3 1 46.50 7.80 10 3 -1 35.44 6.07 -10 -3 1 30.86 6.16 10 -3 -1 44.41 8.09 10 3 -1 32.67 6.33 10 3 -1 38.59 6.71 10 -3 -1 44.63 7.30 10 -3 -1 35.62 7.80 10 -3 -1 46.54 8.23 10 -3 0 99.69 9.72 10 3 0 110.60 11.58 -10 3 0 88.37 12.66 -10 -3 0 107.62 10.78 -10 3 0 109.28 12.79 -10 -3 0 89.89 12.23 10 3 0 99.25 9.72 10 3 0 101.10 10.84 10 -3 0 107.44 10.90 -10 -3 0 102.09 10.09 10 3 0 101.36 10.33 10 -3 0 109.30 10.59 10 -3 0 104.96 11.00 -10 3 0 105.34 11.16 -10 -3 0 121.23 12.70 10 -3 0 90.93 11.92 10 3 0 91.64 12.18 -10 3 0 81.83 11.39 -10 -3 0 121.43 12.24 -10 -3 0 96.32 3.29 10 -3 0 99.69 10.01 10 3 0 91.63 12.17 10 -3 0 106.51 10.26 10 -3 0 101.83 10.29 -10 3 0 92.89 14.24 -10 -3 0 118.83 12.72 10 3 0 109.26 11.19 10 -3 0 105.92 10.21 10 3 0 85.05 11.70 -10 -3 0 100.12 11.75 10 -3 0 128.92 13.28 10 3 0 106.19 10.50 10 3 0 105.42 11.04 10 -3 0 115.76 11.28 10 -3 0 96.91 5.67 -10 -3 0 119.40 13.80 10 -3 0 105.92 12.51 10 -3 1 24.25 5.58 10 3 1 28.02 5.73 -10 3 -1 21.42 5.51 -10 -3 -1 27.22 5.77 -10 3 -1 26.41 7.25 -10 -3 -1 25.75 5.52 10 -3 1 23.57 5.55 -10 -3 -1 18.29 4.77 10 3 1 19.52 9.78 10 -3 1 23.55 5.63 10 -3 1 16.54 4.94 -10 3 -1 19.52 6.79 -10 -3 -1 24.72 7.86 10 -3 1 19.57 4.56 10 3 1 17.84 4.39 -10 3 -1 14.71 3.96 -10 -3 -1 16.75 4.62 -10 -3 -1 17.55 4.12 10 -3 1 13.97 4.73 10 3 1 10.78 3.31 10 -3 1 13.39 4.50 10 -3 1 16.35 5.08 -10 3 -1 25.50 6.97 -10 -3 -1 19.85 6.01 10 3 1 21.08 4.05 10 -3 1 20.55 5.28 10 3 1 21.49 4.71 -10 -3 -1 17.88 6.78 10 -3 1 19.30 7.58 10 3 1 19.57 5.56 10 -3 1 22.88 4.81 10 3 1 23.64 5.57 10 -3 1 18.02 5.33 10 -3 1 23.06 6.13 -10 -3 -1 39.32 8.35 10 -3 1 23.39 8.79 10 3 2 20.74 8.42 10 -3 2 22.60 5.02 -10 3 -2 19.18 4.86 -10 -3 -2 26.60 7.52 -10 3 -2 22.54 6.20 -10 -3 -2 23.18 5.73 10 -3 2 19.61 8.49 10 3 2 24.30 11.33 10 -3 2 19.21 10.19 10 -3 2 30.58 7.30 -10 3 -2 30.30 8.27 -10 -3 -2 26.19 6.44 10 3 2 23.97 5.77 10 -3 2 23.40 4.65 -10 -3 -2 30.28 7.34 -10 3 -2 21.96 4.52 10 -3 2 31.52 6.59 10 3 2 23.04 4.65 10 -3 2 30.88 6.42 10 -3 2 34.22 5.63 -10 3 -2 50.63 9.10 -10 -3 -2 41.31 7.64 10 3 2 40.26 7.14 10 -3 2 44.71 7.06 10 3 2 43.19 7.01 -10 -3 -2 41.77 8.85 10 -3 2 49.91 9.71 10 3 2 44.58 7.83 10 -3 2 42.66 7.35 10 3 2 43.43 7.17 10 -3 2 42.53 7.49 10 -3 2 44.88 7.63 -10 -3 -2 49.73 9.03 10 -3 2 47.06 8.96 10 -3 3 19.22 4.47 10 3 3 25.23 9.00 -10 3 -3 15.47 4.74 -10 -3 -3 19.62 7.43 -10 3 -3 27.67 7.47 -10 -3 -3 24.20 6.07 10 3 3 18.69 5.39 10 -3 3 16.11 7.65 10 3 3 17.60 5.83 10 -3 3 20.80 6.51 10 -3 3 15.66 5.49 -10 -3 -3 24.62 6.39 10 -3 3 13.36 2.73 10 3 3 16.56 4.21 -10 3 -3 8.71 2.21 -10 -3 -3 17.82 4.36 -10 -3 -3 40.82 7.06 10 -3 3 21.68 5.28 10 -3 3 16.02 4.23 10 -3 3 18.20 5.12 -10 3 -3 29.57 6.42 -10 -3 -3 21.06 5.89 10 3 3 23.82 6.26 10 -3 3 25.89 6.03 10 3 3 19.25 6.50 -10 3 -3 30.06 9.39 -10 -3 -3 27.21 7.42 10 3 3 27.32 8.05 10 -3 3 22.06 5.74 10 3 3 19.65 6.19 10 -3 3 20.89 5.63 10 -3 3 17.80 5.75 -10 -3 -3 43.91 8.68 10 -3 3 28.15 7.65 10 -3 4 1.14 3.53 10 3 4 3.29 5.46 -10 3 -4 3.38 4.75 -10 -3 -4 0.99 4.94 -10 3 -4 3.96 4.34 -10 -3 -4 1.15 3.89 10 3 4 1.81 3.46 10 -3 4 1.79 5.35 10 3 4 3.34 6.09 10 -3 4 6.88 3.31 10 -3 4 6.67 5.90 -10 3 -4 7.19 5.98 -10 -3 -4 8.56 5.15 10 -3 4 2.19 2.03 10 3 4 6.42 2.85 -10 3 -4 7.43 2.28 -10 -3 -4 5.57 2.73 -10 -3 -4 7.61 3.69 10 -3 4 8.69 3.71 10 -3 4 11.04 3.99 10 -3 4 6.72 3.14 -10 -3 -4 5.91 4.47 10 3 4 11.20 5.60 10 -3 4 6.42 3.41 10 3 4 5.72 3.87 -10 3 -4 -0.98 7.08 -10 -3 -4 3.89 4.30 10 3 4 10.36 6.42 10 -3 4 9.15 3.32 10 3 4 7.41 5.05 10 -3 4 7.34 3.77 10 -3 4 3.77 3.53 -10 -3 -4 7.31 6.77 10 -3 4 12.50 6.55 10 3 5 156.35 12.69 10 -3 5 161.41 12.74 -10 -3 -5 163.55 13.36 -10 3 -5 146.85 11.99 -10 3 -5 162.62 14.30 -10 -3 -5 159.59 12.92 10 3 5 131.81 10.76 10 -3 5 137.89 11.06 10 3 5 134.60 11.66 10 -3 5 153.92 12.73 10 -3 5 131.15 10.39 -10 3 -5 112.31 10.20 -10 -3 -5 141.19 12.28 10 3 5 114.84 8.92 10 -3 5 114.50 8.76 -10 -3 -5 118.21 9.42 -10 3 -5 99.28 8.21 -10 -3 -5 109.06 10.35 10 -3 5 134.45 11.29 10 -3 5 116.00 9.03 10 -3 5 110.26 9.85 -10 -3 -5 99.78 8.29 10 3 5 128.51 10.53 10 -3 5 128.08 10.36 10 3 5 116.27 10.02 -10 3 -5 129.10 13.27 -10 -3 -5 118.88 11.24 10 3 5 127.31 11.70 10 -3 5 127.37 10.79 10 3 5 113.61 9.92 10 -3 5 117.37 9.65 10 -3 5 115.05 9.44 -10 -3 -5 163.56 14.36 10 -3 5 146.30 13.20 10 3 6 16.21 4.68 10 -3 6 18.66 4.22 -10 -3 -6 14.27 3.96 -10 3 -6 12.40 3.24 -10 3 -6 14.00 4.87 -10 -3 -6 12.44 4.19 10 3 6 11.05 4.07 10 -3 6 15.63 3.98 10 3 6 16.70 5.57 10 -3 6 13.38 4.17 -10 3 -6 6.27 4.75 -10 -3 -6 13.07 4.19 10 3 6 14.50 2.53 10 -3 6 10.06 1.90 -10 -3 -6 13.39 2.71 -10 3 -6 9.42 2.10 -10 -3 -6 10.20 3.75 10 -3 6 18.42 5.51 10 -3 6 13.61 3.72 10 -3 6 9.10 3.66 -10 -3 -6 9.13 3.59 10 3 6 7.13 4.42 10 -3 6 11.02 5.56 10 3 6 18.25 5.63 10 -3 6 12.96 3.12 -10 3 -6 8.32 5.90 -10 -3 -6 11.19 4.96 10 3 6 12.03 5.55 10 -3 6 15.18 4.34 10 3 6 7.86 4.10 10 -3 6 16.15 4.13 10 -3 6 14.31 5.11 -10 -3 -6 22.11 10.64 10 -3 6 15.83 6.07 10 3 7 -2.25 5.43 -10 -3 -7 7.16 5.00 -10 3 -7 -4.10 5.39 -10 -3 -7 3.71 5.83 10 3 7 -1.81 4.81 10 -3 7 3.93 3.65 10 3 7 -1.26 4.56 10 -3 7 3.77 3.89 10 -3 7 1.52 3.49 -10 -3 -7 3.95 4.86 10 3 7 0.99 3.82 10 -3 7 -1.04 1.86 -10 -3 -7 3.11 4.06 -10 3 -7 -0.54 1.81 -10 -3 -7 0.08 3.65 10 -3 7 1.96 5.57 10 -3 7 1.27 3.05 10 -3 7 -1.67 3.49 10 3 7 0.42 6.58 10 -3 7 3.06 4.00 10 3 7 -2.12 5.51 10 -3 7 0.00 3.53 -10 3 -7 -5.67 5.22 -10 -3 -7 0.02 4.32 10 3 7 -2.19 5.42 10 -3 7 1.46 5.05 10 3 7 1.20 3.32 10 -3 7 -1.70 4.10 10 -3 7 -0.62 4.75 -10 3 -7 -6.18 7.99 -10 -3 -7 1.21 6.33 10 3 8 -1.90 3.98 -10 -3 -8 3.08 3.34 -10 3 -8 4.73 6.84 -10 -3 -8 1.18 4.29 10 -3 8 1.33 3.63 10 3 8 7.26 4.62 10 -3 8 8.97 5.49 -10 3 -8 4.30 3.13 -10 -3 -8 10.20 4.93 10 3 8 3.80 2.41 -10 -3 -8 5.00 3.09 -10 -3 -8 10.85 4.99 10 -3 8 4.06 6.39 10 -3 8 4.90 3.35 10 -3 8 6.97 5.50 10 3 8 9.20 5.20 10 -3 8 11.99 4.29 10 3 8 5.83 5.62 10 -3 8 9.04 3.87 -10 3 -8 11.43 4.29 -10 -3 -8 12.01 4.56 10 3 8 13.78 6.36 10 -3 8 13.74 4.96 10 3 8 5.26 3.61 10 -3 8 6.26 5.17 10 -3 8 8.30 5.37 -10 3 -8 13.95 7.84 -10 -3 -8 20.66 8.27 10 3 9 122.89 12.37 -10 -3 -9 111.20 11.45 -10 3 -9 109.97 11.94 -10 -3 -9 107.04 11.54 10 -3 9 108.02 11.71 10 3 9 96.69 10.65 10 -3 9 106.91 11.30 -10 3 -9 103.16 10.98 10 3 9 115.75 11.37 -10 -3 -9 116.24 11.59 -10 -3 -9 107.91 12.20 10 -3 9 123.95 14.26 10 -3 9 110.67 11.14 10 -3 9 106.19 11.41 10 3 9 97.18 11.37 10 -3 9 107.58 12.06 10 3 9 90.34 11.19 10 -3 9 116.30 11.95 -10 3 -9 76.16 8.67 -10 -3 -9 100.53 10.91 10 3 9 111.77 12.17 10 -3 9 103.74 10.85 10 3 9 80.50 8.73 10 -3 9 95.81 11.33 10 -3 9 87.60 9.48 -10 3 -9 88.54 13.56 -10 -3 -9 103.10 13.62 10 3 10 1.99 3.73 -10 -3 -10 0.46 3.70 -10 -3 -10 -1.17 5.80 10 -3 10 2.72 4.17 10 -3 10 0.41 3.94 10 3 10 -1.44 4.36 10 -3 10 4.19 4.76 10 3 10 -4.10 6.50 10 -3 10 4.13 4.12 -10 -3 -10 1.10 4.59 10 3 10 -1.57 5.33 10 -3 10 0.30 5.72 10 3 10 -0.45 3.23 10 -3 10 -2.27 6.25 10 -3 10 0.29 4.88 -10 3 -10 -16.06 9.81 -10 -3 -10 1.11 5.75 10 3 11 8.11 3.48 -10 -3 -11 7.31 4.23 -10 3 -11 30.22 4.75 -10 -3 -11 28.95 5.08 10 -3 11 7.14 4.11 10 -3 11 11.93 3.71 10 3 11 16.17 5.27 10 -3 11 15.66 4.32 10 3 11 16.80 6.39 10 -3 11 16.92 5.91 -10 -3 -11 14.73 4.87 10 3 11 21.50 6.15 10 -3 11 12.92 7.52 10 -3 11 14.90 4.51 10 -3 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68.45 10.15 10 -5 -10 107.59 14.72 -10 5 10 78.23 10.98 -10 5 10 86.81 12.27 -10 -5 10 82.36 12.17 10 -5 -10 86.36 12.17 10 5 -10 87.66 12.52 -10 -5 10 73.12 10.29 -10 5 10 64.36 10.98 -10 -5 10 94.35 12.74 10 -5 -10 88.85 11.68 10 5 -10 82.45 12.39 10 -5 -10 89.09 12.27 10 -5 -10 93.68 13.73 -10 5 10 78.01 10.54 -10 -5 10 76.61 10.52 -10 -5 10 87.35 13.22 -10 -5 10 66.83 9.69 10 -5 -10 77.74 10.65 -10 -5 10 77.62 13.39 10 5 -10 87.45 14.00 10 -5 -10 75.92 11.39 -10 5 10 69.36 12.95 -10 -5 10 64.87 10.59 10 -5 -10 70.61 10.60 10 -5 -9 5.43 3.67 -10 5 9 0.45 4.56 -10 -5 9 4.00 3.67 10 -5 -9 1.70 3.75 -10 -5 9 -0.19 3.23 10 5 -9 7.70 4.68 10 -5 -9 0.54 3.44 -10 5 9 -2.48 5.03 -10 -5 9 3.20 5.71 10 5 -9 -0.47 5.55 10 5 -9 1.23 3.42 10 -5 -9 1.54 7.74 -10 5 9 -2.74 5.23 -10 -5 9 0.39 3.86 -10 5 9 3.14 2.88 -10 -5 9 1.78 3.64 10 -5 -9 -2.34 3.00 10 5 -9 0.83 4.47 -10 -5 9 0.01 2.60 -10 5 9 5.34 4.40 -10 -5 9 0.27 3.81 10 -5 -9 -3.08 4.38 10 5 -9 -1.08 4.79 10 -5 -9 5.08 5.17 10 -5 -9 -2.13 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10 -5 -6 37.40 6.33 10 5 -6 50.87 9.55 -10 -5 6 31.56 6.62 -10 5 6 47.61 8.41 10 -5 -6 53.79 8.40 10 5 -6 56.24 8.86 10 -5 -6 56.01 9.34 10 -5 -6 58.19 9.39 -10 -5 6 46.85 8.69 -10 -5 6 50.46 8.33 -10 -5 6 58.80 11.24 -10 -5 6 48.80 8.32 -10 -5 6 44.25 7.31 10 -5 -6 64.61 10.98 -10 -5 6 54.54 10.67 10 5 -6 71.53 6.30 10 -5 -6 56.04 8.93 10 -5 -6 56.07 9.91 -10 5 6 73.05 5.98 -10 -5 6 63.43 10.46 10 -5 -6 68.91 6.56 10 -5 -5 0.15 3.02 10 5 -5 7.43 5.10 -10 5 5 1.38 3.83 -10 -5 5 2.89 5.86 10 -5 -5 5.19 3.71 -10 -5 5 1.34 4.11 10 5 -5 0.45 5.33 10 -5 -5 22.47 6.62 -10 5 5 15.16 5.56 -10 -5 5 0.86 5.71 10 5 -5 5.45 6.83 10 -5 -5 6.64 4.82 -10 5 5 2.34 4.52 -10 -5 5 3.29 3.84 -10 5 5 3.34 2.10 -10 -5 5 10.71 5.05 10 -5 -5 6.73 2.67 10 5 -5 -1.83 6.47 -10 -5 5 4.32 2.74 -10 5 5 5.09 3.53 -10 -5 5 1.61 3.86 10 -5 -5 3.82 3.81 10 5 -5 3.47 3.93 10 -5 -5 5.15 3.47 10 -5 -5 1.52 8.94 -10 -5 5 2.70 4.52 -10 -5 5 6.30 2.55 10 5 -5 0.08 15.05 -10 -5 5 27.06 5.97 -10 -5 5 6.54 3.89 10 -5 -5 10.48 4.85 10 5 -5 4.36 11.33 10 -5 -5 5.06 3.65 10 -5 -5 4.36 6.18 -10 5 5 2.32 3.46 -10 -5 5 3.22 4.50 10 -5 -5 4.19 5.09 10 -5 -4 9.15 3.71 10 5 -4 9.07 4.74 -10 5 4 9.72 4.25 -10 -5 4 11.47 6.37 10 -5 -4 13.80 5.50 10 5 -4 7.94 4.25 10 5 -4 6.96 8.42 10 -5 -4 7.02 3.96 -10 5 4 10.31 6.04 -10 -5 4 13.37 6.03 10 5 -4 16.18 6.03 10 -5 -4 11.51 4.90 -10 5 4 4.98 4.36 -10 -5 4 7.34 5.09 10 5 -4 2.08 3.73 -10 5 4 2.25 1.79 -10 -5 4 7.01 4.69 10 -5 -4 4.90 2.33 -10 -5 4 1.84 2.27 -10 5 4 4.23 4.00 -10 -5 4 4.22 4.41 10 -5 -4 1.44 4.46 10 5 -4 0.92 2.51 10 -5 -4 1.52 2.78 10 -5 -4 4.29 3.53 -10 -5 4 0.58 3.81 -10 -5 4 1.50 1.93 10 5 -4 2.88 4.52 -10 -5 4 1.06 3.63 -10 -5 4 -0.57 3.01 10 -5 -4 1.70 4.39 -10 -5 4 8.63 5.52 10 5 -4 -2.04 4.33 10 -5 -4 -1.72 3.00 10 -5 -4 -1.58 4.91 -10 -5 4 2.95 4.33 10 -5 -4 3.90 4.68 10 -5 -3 4.99 2.55 10 5 -3 4.32 4.46 -10 5 3 6.04 3.03 -10 -5 3 5.33 5.75 10 -5 -3 10.52 5.31 10 5 -3 8.70 4.06 10 5 -3 10.55 5.06 10 -5 -3 22.25 6.93 -10 5 3 15.93 5.28 -10 -5 3 3.93 7.31 10 5 -3 18.69 6.48 10 -5 -3 27.84 8.03 -10 5 3 5.72 4.35 -10 -5 3 13.20 6.61 10 5 -3 7.84 3.41 -10 5 3 5.87 2.18 -10 -5 3 14.52 5.08 10 -5 -3 7.03 2.36 -10 -5 3 7.70 2.59 -10 5 3 14.67 4.88 -10 -5 3 9.63 3.93 10 -5 -3 7.83 4.92 10 5 -3 5.86 2.50 10 -5 -3 8.28 3.24 10 -5 -3 3.24 4.73 -10 -5 3 9.95 6.30 -10 -5 3 5.12 2.09 10 5 -3 19.05 6.03 -10 -5 3 6.45 5.06 -10 -5 3 4.67 3.51 10 -5 -3 16.28 5.60 10 5 -3 13.48 5.20 10 5 -3 8.87 5.61 10 -5 -3 9.20 4.83 10 -5 -3 3.58 5.27 -10 -5 3 6.74 3.57 10 -5 -3 17.80 7.99 10 -5 -2 56.83 8.05 10 5 -2 64.46 9.39 -10 5 2 42.66 8.57 -10 -5 2 65.43 10.04 10 -5 -2 64.46 9.92 10 5 -2 51.19 9.77 10 5 -2 58.70 10.59 10 -5 -2 69.26 11.14 -10 5 2 76.62 11.40 -10 -5 2 79.79 11.27 10 5 -2 68.21 13.59 10 -5 -2 82.69 12.39 -10 5 2 81.13 11.74 -10 -5 2 80.04 11.28 10 5 -2 58.85 8.27 -10 -5 2 60.69 10.12 -10 -5 2 63.88 8.69 -10 5 2 62.50 8.84 -10 -5 2 89.26 11.99 10 -5 -2 79.58 11.31 10 -5 -2 89.25 11.99 10 -5 -2 82.58 11.41 -10 -5 2 110.32 11.08 10 5 -2 99.38 10.49 -10 -5 2 86.16 11.92 -10 -5 2 84.94 12.17 10 -5 -2 123.97 13.02 10 5 -2 112.88 12.70 10 5 -2 86.70 12.96 10 -5 -2 106.28 10.48 10 -5 -2 112.54 13.63 -10 -5 2 92.95 12.62 10 -5 -2 132.55 14.17 10 -5 -1 4.32 2.61 10 5 -1 5.20 3.37 -10 5 1 1.09 2.38 -10 -5 1 3.30 4.21 -10 5 1 5.51 4.93 10 5 -1 5.87 3.32 10 5 -1 8.97 4.70 10 -5 -1 6.73 4.32 -10 -5 1 8.49 4.25 10 5 -1 4.30 6.55 10 -5 -1 8.16 4.46 -10 5 1 15.85 5.78 -10 -5 1 14.08 7.14 10 5 -1 9.94 3.30 -10 -5 1 9.63 3.35 -10 -5 1 8.26 3.02 -10 5 1 18.07 5.09 -10 -5 1 16.26 4.51 10 -5 -1 18.54 5.00 10 -5 -1 17.66 5.04 10 -5 -1 20.46 5.42 -10 -5 1 20.32 6.18 -10 -5 1 13.22 4.77 -10 -5 1 21.38 5.90 10 -5 -1 26.16 7.10 10 5 -1 22.37 8.68 10 5 -1 19.64 5.89 10 -5 -1 28.80 6.59 10 -5 -1 27.63 7.02 -10 -5 1 22.80 5.22 -10 -5 1 15.96 5.31 10 -5 -1 26.75 6.85 10 -5 0 17.73 4.30 10 5 0 19.99 5.26 -10 5 0 15.71 4.32 -10 -5 0 19.04 5.55 -10 5 0 22.54 6.88 10 5 0 23.78 6.18 10 5 0 21.47 6.14 10 -5 0 24.91 7.37 -10 -5 0 15.05 4.87 10 5 0 25.77 7.71 10 -5 0 18.88 4.96 10 -5 0 20.44 7.02 -10 5 0 29.42 8.45 -10 -5 0 20.26 5.86 10 5 0 15.01 3.90 -10 -5 0 23.80 5.64 -10 -5 0 10.18 3.17 -10 -5 0 15.30 3.67 10 -5 0 18.74 4.90 10 -5 0 19.48 4.70 10 -5 0 15.25 4.35 -10 -5 0 28.14 6.70 10 5 0 22.30 6.61 10 -5 0 20.02 4.52 10 5 0 28.28 6.64 -10 -5 0 25.26 6.96 10 -5 0 34.25 6.91 10 5 0 26.34 7.69 10 5 0 20.81 7.20 10 -5 0 25.70 6.07 10 -5 0 36.49 9.42 -10 -5 0 27.11 6.93 10 -5 0 25.12 9.39 10 5 1 29.54 7.14 10 -5 1 28.10 5.84 -10 -5 -1 31.72 6.97 -10 5 -1 21.10 5.19 -10 5 -1 31.37 7.64 -10 -5 -1 31.93 6.74 10 5 1 27.75 6.54 10 5 1 27.16 6.31 10 -5 1 37.80 7.84 -10 -5 -1 29.14 6.07 10 5 1 31.64 7.51 10 -5 1 27.37 6.06 10 -5 1 26.86 6.45 -10 5 -1 36.24 6.84 -10 -5 -1 36.38 7.24 10 5 1 28.45 6.12 -10 -5 -1 32.86 3.09 -10 -5 -1 22.24 4.88 -10 -5 -1 29.35 5.97 10 -5 1 28.10 7.06 10 -5 1 28.92 6.10 10 -5 1 29.02 6.72 -10 5 -1 27.96 7.36 -10 -5 -1 36.19 6.44 10 5 1 34.75 6.37 10 -5 1 33.40 5.93 10 5 1 34.15 6.25 -10 -5 -1 44.24 8.46 10 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-3 8.63 2.60 10 5 3 4.52 2.41 10 -5 3 4.35 3.23 10 -5 3 3.44 4.10 10 -5 3 4.79 3.60 -10 5 -3 6.94 3.66 -10 -5 -3 5.42 3.23 10 5 3 0.36 6.15 10 -5 3 6.79 3.67 10 5 3 5.33 5.20 -10 -5 -3 2.72 4.88 10 -5 3 5.83 5.04 10 5 3 2.09 4.93 10 -5 3 1.81 3.46 10 5 3 7.31 3.46 10 -5 3 5.19 4.09 10 -5 3 3.36 4.35 -10 -5 -3 5.28 5.56 10 -5 3 -1.17 6.19 10 5 4 5.00 5.39 -10 -5 -4 7.37 4.65 -10 5 -4 8.65 5.83 -10 -5 -4 10.27 4.46 10 5 4 13.57 3.72 10 5 4 13.43 4.70 10 -5 4 8.84 4.40 10 5 4 12.28 6.94 10 -5 4 13.80 4.30 10 -5 4 14.46 5.97 -10 5 -4 13.78 6.42 -10 -5 -4 11.27 6.41 10 5 4 7.12 2.57 -10 -5 -4 7.17 2.97 10 5 4 14.79 2.88 -10 -5 -4 18.29 3.88 10 -5 4 10.20 3.83 10 -5 4 13.65 4.03 10 -5 4 12.11 4.29 -10 -5 -4 10.85 3.36 10 5 4 12.38 4.29 10 -5 4 7.86 4.25 10 5 4 7.07 4.73 -10 -5 -4 14.21 4.81 10 5 4 16.62 7.11 10 -5 4 7.83 3.47 10 5 4 6.38 3.34 10 -5 4 9.36 4.53 10 -5 4 12.45 6.38 -10 -5 -4 12.58 6.83 10 -5 4 7.18 6.00 10 5 5 19.53 4.87 -10 -5 -5 17.04 4.64 -10 5 -5 20.17 6.31 -10 -5 -5 22.01 4.85 10 -5 5 13.77 4.40 10 5 5 15.39 7.35 10 -5 5 14.42 4.23 10 -5 5 14.52 4.04 -10 5 -5 13.90 4.41 -10 -5 -5 16.00 4.68 10 5 5 14.21 2.78 -10 -5 -5 17.22 3.66 10 5 5 11.77 3.58 -10 -5 -5 11.75 3.13 10 -5 5 17.09 4.64 10 -5 5 11.57 2.90 10 -5 5 15.68 4.05 -10 -5 -5 12.16 3.89 10 5 5 12.05 4.23 10 -5 5 13.62 3.37 10 5 5 11.87 4.99 -10 5 -5 23.44 7.86 -10 -5 -5 21.85 6.90 10 5 5 12.84 5.50 10 -5 5 12.99 3.83 10 5 5 7.51 4.52 10 -5 5 15.87 5.54 10 -5 5 9.44 4.52 -10 -5 -5 28.48 8.86 10 -5 5 18.47 10.23 10 5 6 89.51 13.82 -10 -5 -6 88.41 13.51 -10 5 -6 66.78 10.53 -10 -5 -6 77.54 11.37 10 -5 6 66.72 10.61 10 5 6 69.69 10.94 10 -5 6 77.33 11.33 10 -5 6 75.98 11.57 -10 -5 -6 64.19 9.95 10 5 6 78.36 11.41 -10 -5 -6 80.95 11.76 10 5 6 64.34 9.31 -10 -5 -6 82.85 11.77 10 -5 6 87.35 12.85 10 -5 6 84.90 11.82 10 -5 6 89.07 13.68 -10 -5 -6 79.17 11.30 10 5 6 74.06 12.99 10 -5 6 93.42 13.24 10 5 6 92.02 13.57 -10 5 -6 71.16 11.37 -10 -5 -6 83.97 13.11 10 5 6 93.13 13.98 10 -5 6 96.24 13.76 10 5 6 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179.16 14.08 10 6 2 153.26 13.71 10 -6 2 165.76 12.69 10 6 2 160.47 13.69 -10 -6 -2 145.20 13.88 10 -6 2 188.51 15.65 10 6 2 152.33 13.90 10 6 2 143.39 11.87 10 -6 2 151.61 12.05 10 -6 2 168.74 13.90 -10 -6 -2 194.66 16.75 10 -6 2 172.88 15.45 10 6 3 -1.72 3.46 -10 -6 -3 -5.45 4.06 -10 6 -3 1.80 5.91 -10 -6 -3 1.31 2.85 10 6 3 2.32 5.15 10 6 3 2.68 4.00 10 -6 3 2.76 4.13 10 6 3 -0.98 6.59 10 -6 3 1.99 3.63 10 -6 3 0.41 6.02 -10 6 -3 1.96 5.32 -10 -6 -3 -0.81 4.33 10 6 3 2.67 2.45 -10 -6 -3 0.35 2.54 10 6 3 4.07 2.82 10 -6 3 3.52 3.88 10 -6 3 0.16 3.23 10 -6 3 6.02 3.41 -10 6 -3 3.90 4.47 -10 -6 -3 0.31 4.34 10 6 3 1.40 4.27 10 -6 3 3.09 3.59 10 6 3 -1.09 5.17 -10 -6 -3 0.80 5.74 10 -6 3 6.56 4.47 10 6 3 2.08 6.12 10 -6 3 1.37 2.50 10 6 3 4.98 4.18 10 -6 3 -0.35 3.88 10 -6 3 2.31 6.20 -10 -6 -3 3.87 4.46 10 -6 3 2.48 5.89 10 6 4 10.03 3.34 -10 -6 -4 8.26 4.07 -10 6 -4 4.62 5.35 -10 -6 -4 12.04 3.44 10 6 4 6.84 3.29 10 -6 4 12.24 4.73 10 6 4 0.85 7.31 10 -6 4 9.83 4.32 10 -6 4 5.69 3.69 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-6 24.57 8.44 10 -7 6 12.28 7.05 10 7 7 14.96 4.63 -10 -7 -7 6.31 4.27 -10 7 -7 2.76 5.67 10 -7 7 4.12 3.70 10 7 7 6.32 6.71 10 -7 7 2.61 3.89 10 -7 7 5.44 4.27 -10 -7 -7 1.58 5.35 10 7 7 6.64 3.51 -10 -7 -7 5.68 3.51 10 7 7 0.21 3.55 -10 -7 -7 -3.75 4.40 10 -7 7 -5.02 5.81 10 -7 7 2.85 5.26 10 -7 7 -0.97 4.73 -10 -7 -7 2.60 4.07 10 7 7 4.97 4.71 10 -7 7 -0.07 5.63 10 7 7 2.88 7.40 -10 7 -7 -6.06 6.62 -10 -7 -7 -1.10 7.75 10 7 7 5.75 9.45 10 -7 7 0.45 4.17 10 -7 7 10.15 5.71 10 -7 7 0.19 5.37 -10 -7 -7 1.91 5.45 10 -7 7 0.30 9.63 10 7 8 123.34 12.50 -10 -7 -8 124.94 12.64 10 7 8 113.28 12.40 -10 -7 -8 156.54 15.68 10 -7 8 148.10 16.39 10 -7 8 149.40 15.18 10 -7 8 135.73 15.29 -10 -7 -8 126.65 12.58 10 7 8 131.23 15.11 10 -7 8 143.38 14.70 10 7 8 131.77 15.07 -10 -7 -8 137.48 14.61 10 7 8 135.22 14.32 10 -7 8 159.86 15.97 10 -7 8 128.72 13.37 10 -7 8 144.59 15.92 -10 7 -8 99.49 15.57 -10 -7 -8 154.43 17.22 10 7 9 71.37 8.29 -10 -7 -9 62.26 7.52 10 7 9 47.90 6.84 -10 -7 -9 65.34 8.10 10 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132.87 15.77 11 -3 -3 127.64 12.85 -11 3 3 184.99 18.82 -11 -3 3 190.01 18.64 11 3 -3 155.84 15.64 11 -3 -3 135.76 13.25 -11 -3 3 118.21 14.83 11 -3 -3 151.10 15.66 11 3 -3 142.53 13.95 11 3 -3 133.28 14.09 11 -3 -3 140.83 13.80 11 -3 -3 111.75 11.94 -11 -3 3 103.42 10.14 -11 -3 3 91.67 12.64 11 -3 -3 136.80 14.66 11 3 -2 36.31 6.30 -11 -3 2 36.00 6.43 -11 3 2 44.73 7.65 11 3 -2 30.40 7.90 11 -3 -2 38.21 11.58 -11 3 2 38.12 6.82 -11 -3 2 41.47 7.87 11 3 -2 53.18 9.27 11 -3 -2 48.23 7.93 11 -3 -2 48.75 8.49 -11 3 2 87.34 11.68 -11 -3 2 67.86 6.38 11 -3 -2 39.49 6.02 11 3 -2 49.36 7.66 -11 3 2 38.72 6.37 -11 -3 2 58.82 9.23 -11 3 2 85.59 10.07 -11 -3 2 68.59 3.83 11 -3 -2 70.23 3.99 11 3 -2 69.03 4.17 11 -3 -2 79.88 9.88 11 -3 -2 64.30 10.38 -11 -3 2 112.79 13.48 11 3 -2 115.37 14.12 11 -3 -2 87.63 10.39 11 3 -2 75.13 9.30 11 -3 -2 103.48 12.82 11 3 -2 121.09 14.30 11 3 -2 101.54 12.47 11 -3 -2 112.99 13.88 11 -3 -2 123.95 15.33 11 -3 -2 127.89 15.89 11 -3 -1 4.51 2.91 11 3 -1 -0.36 4.12 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1 9.45 4.23 11 -3 1 11.41 4.42 11 -3 1 3.25 6.00 -11 -3 -1 3.64 5.22 11 -3 1 5.68 6.37 11 3 2 22.81 7.53 11 -3 2 25.41 5.40 -11 -3 -2 24.75 6.32 -11 3 -2 20.77 5.80 -11 3 -2 28.13 8.13 -11 -3 -2 28.05 6.37 11 3 2 33.03 6.43 11 -3 2 39.27 7.31 11 3 2 38.62 7.41 11 -3 2 37.86 6.78 11 -3 2 38.46 7.80 -11 3 -2 35.78 7.49 -11 -3 -2 48.89 10.12 11 3 2 40.33 6.94 11 -3 2 37.07 5.75 -11 -3 -2 43.26 7.31 -11 3 -2 33.87 5.61 -11 -3 -2 52.35 8.33 11 -3 2 54.73 3.81 11 3 2 40.08 6.53 11 -3 2 53.26 8.51 11 -3 2 53.53 8.73 -11 3 -2 52.36 8.99 -11 -3 -2 67.64 9.89 11 3 2 47.90 9.48 11 -3 2 66.00 8.90 11 3 2 60.87 8.84 -11 3 -2 73.50 13.14 -11 -3 -2 74.03 11.81 11 3 2 66.33 9.59 11 -3 2 67.58 9.39 11 3 2 71.29 10.96 11 -3 2 65.42 9.26 11 -3 2 64.90 9.25 -11 -3 -2 52.25 10.62 11 -3 2 77.72 11.82 11 -3 3 210.98 16.52 11 3 3 200.92 16.60 -11 3 -3 173.04 14.89 -11 -3 -3 206.53 17.59 -11 3 -3 189.96 17.49 -11 -3 -3 186.32 15.37 11 3 3 193.02 16.35 11 -3 3 218.45 17.18 11 3 3 208.55 16.81 11 -3 3 230.22 18.38 11 -3 3 214.96 16.58 -11 3 -3 192.11 15.82 -11 -3 -3 240.50 19.23 11 -3 3 199.87 15.16 11 3 3 201.20 15.83 -11 3 -3 165.97 13.94 -11 -3 -3 210.55 16.95 -11 -3 -3 222.28 18.55 11 -3 3 228.57 18.00 11 -3 3 202.76 15.54 11 -3 3 212.77 16.74 -11 3 -3 213.89 17.14 -11 -3 -3 228.01 17.70 11 3 3 218.32 17.41 11 -3 3 236.59 18.40 11 3 3 203.57 16.62 -11 3 -3 200.03 20.03 -11 -3 -3 192.80 18.99 11 3 3 207.34 16.38 11 -3 3 211.67 16.68 11 3 3 180.92 14.44 11 -3 3 197.79 15.54 11 -3 3 176.91 13.94 11 -3 3 191.73 16.86 11 3 4 83.28 8.39 11 -3 4 80.26 7.71 -11 -3 -4 78.74 7.76 -11 3 -4 66.91 10.43 -11 3 -4 67.47 12.14 -11 -3 -4 69.63 10.81 11 3 4 61.92 10.62 11 -3 4 76.14 12.05 11 3 4 64.38 10.70 11 -3 4 73.48 11.29 -11 3 -4 43.66 9.44 -11 -3 -4 65.55 11.87 11 3 4 71.30 10.50 11 -3 4 62.50 9.19 -11 -3 -4 66.36 9.90 -11 3 -4 40.96 6.66 -11 -3 -4 31.69 6.85 11 -3 4 63.84 9.85 11 -3 4 44.52 7.41 11 -3 4 49.26 8.45 -11 -3 -4 43.63 7.31 11 3 4 53.21 9.09 11 -3 4 52.65 8.61 11 3 4 51.19 9.67 -11 3 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17.18 5.09 12 -6 -5 19.75 5.00 12 6 -5 16.23 3.57 12 -6 -5 21.48 5.04 12 -6 -5 15.96 8.75 -12 -6 5 25.06 7.78 12 6 -5 22.86 7.68 -12 -6 5 10.77 4.61 -12 -6 5 13.45 4.19 12 -6 -5 13.40 5.54 12 6 -5 18.83 8.86 12 6 -5 25.44 6.77 12 -6 -5 16.54 4.23 12 -6 -5 19.15 7.78 -12 -6 5 10.15 7.23 12 -6 -5 13.88 8.40 12 6 -4 67.25 11.25 -12 -6 4 62.89 10.27 12 -6 -4 62.07 10.49 12 6 -4 62.78 10.65 12 -6 -4 64.13 10.46 -12 -6 4 59.61 9.80 12 6 -4 70.70 11.43 12 -6 -4 50.32 9.09 -12 6 4 38.55 8.32 -12 -6 4 68.01 11.45 12 6 -4 51.18 8.42 -12 -6 4 59.52 9.81 -12 6 4 58.59 9.66 -12 -6 4 41.81 7.05 12 -6 -4 60.92 10.54 12 -6 -4 47.21 8.09 12 -6 -4 40.76 7.43 -12 -6 4 39.38 8.11 12 6 -4 43.97 8.68 -12 -6 4 33.28 7.30 -12 -6 4 18.08 6.18 12 -6 -4 43.47 8.20 12 6 -4 35.84 7.95 12 6 -4 43.65 9.08 12 -6 -4 38.64 6.88 12 -6 -4 33.17 8.17 -12 -6 4 38.72 7.77 12 -6 -4 29.12 8.42 12 6 -3 1.50 4.01 -12 -6 3 0.62 4.41 -12 6 3 2.36 7.65 12 6 -3 -2.28 5.10 12 -6 -3 4.04 5.35 -12 -6 3 4.86 5.91 12 6 -3 4.12 5.85 12 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2 18.96 4.79 12 -6 2 15.58 5.43 12 -6 2 6.65 8.03 -12 -6 -2 23.32 7.61 12 -6 2 18.36 11.71 12 6 3 -0.56 3.72 -12 -6 -3 -1.14 5.00 -12 6 -3 0.17 6.93 12 -6 3 -2.56 4.83 12 6 3 2.19 5.12 12 -6 3 1.32 4.23 -12 6 -3 5.09 7.17 -12 -6 -3 2.91 5.91 12 6 3 5.54 3.17 -12 -6 -3 2.39 3.52 12 -6 3 -3.25 5.49 12 -6 3 1.51 6.02 12 -6 3 0.19 4.74 -12 -6 -3 -4.51 4.79 12 6 3 4.45 8.92 12 -6 3 -0.92 3.06 12 6 3 -6.93 5.25 -12 6 -3 2.57 9.77 -12 -6 -3 1.67 9.50 12 6 3 -1.97 7.32 12 6 3 3.84 5.55 12 -6 3 -1.64 3.83 12 -6 3 1.54 7.40 -12 -6 -3 -0.28 5.35 12 -6 3 -3.87 7.94 12 6 4 60.71 9.88 -12 -6 -4 60.07 10.12 -12 6 -4 46.35 8.39 12 -6 4 58.45 9.28 12 6 4 48.77 8.97 12 -6 4 52.04 8.61 -12 6 -4 39.40 6.91 -12 -6 -4 54.01 9.50 12 6 4 48.42 7.69 -12 -6 -4 45.36 7.75 12 -6 4 53.26 9.23 12 -6 4 53.57 9.30 12 -6 4 55.36 10.46 -12 -6 -4 61.26 10.31 12 6 4 57.03 11.76 12 -6 4 62.76 9.78 12 6 4 51.84 9.77 -12 6 -4 49.03 10.98 -12 -6 -4 64.32 12.24 12 6 4 50.83 9.61 12 -6 4 49.34 7.80 12 6 4 44.70 8.12 12 -6 4 57.22 9.37 12 -6 4 52.66 9.16 -12 -6 -4 63.94 12.45 12 -6 4 53.07 10.56 12 6 5 3.84 2.82 -12 -6 -5 6.49 3.84 12 -6 5 7.88 4.76 12 -6 5 5.84 5.05 12 -6 5 9.33 5.66 -12 -6 -5 3.25 5.00 12 6 5 13.31 5.64 12 -6 5 5.71 3.95 12 6 5 13.27 5.67 -12 6 -5 3.76 6.60 -12 -6 -5 5.77 6.48 12 6 5 3.63 6.04 12 -6 5 7.83 3.59 12 6 5 2.77 4.19 12 -6 5 4.22 7.86 12 -6 5 11.49 6.56 -12 -6 -5 8.11 6.14 12 -6 5 -0.81 8.56 12 6 6 1.40 2.74 -12 -6 -6 0.11 3.08 12 -6 6 5.44 5.08 12 -6 6 6.67 5.17 12 -6 6 4.71 4.50 -12 -6 -6 5.81 3.86 12 6 6 6.32 5.19 12 -6 6 7.12 4.13 12 6 6 -1.80 5.39 -12 6 -6 5.40 6.29 -12 -6 -6 -1.84 6.33 12 6 6 1.06 7.46 12 -6 6 -0.68 4.45 12 -6 6 4.88 4.80 12 -6 6 6.32 7.51 -12 -6 -6 -4.54 6.22 12 -6 6 7.68 8.09 12 6 7 -2.45 2.63 -12 -6 -7 1.52 2.66 12 -6 7 1.69 4.58 12 -6 7 2.54 4.30 12 -6 7 4.44 4.74 -12 -6 -7 -1.14 3.63 12 6 7 2.67 6.95 12 -6 7 -1.27 3.70 12 6 7 1.72 5.67 -12 6 -7 4.00 4.91 -12 -6 -7 -2.65 7.69 12 6 7 2.78 8.30 12 -6 7 0.40 4.29 12 -6 7 0.22 4.77 12 -6 7 -4.38 5.33 -12 6 -7 -1.85 8.74 -12 -6 -7 -4.87 6.70 12 6 8 3.01 2.60 -12 -6 -8 3.89 2.65 -12 -6 -8 -0.57 3.87 12 -6 8 6.43 4.21 12 -6 8 3.05 3.48 12 -6 8 -1.14 4.77 12 6 8 2.48 4.06 12 -6 8 1.09 5.87 12 6 8 -4.25 4.82 -12 -6 -8 8.75 5.29 12 6 8 1.83 6.01 12 -6 8 -0.39 4.56 12 -6 8 0.35 5.27 12 -6 8 -5.44 6.41 -12 6 -8 -7.13 10.69 -12 -6 -8 -5.55 6.97 12 6 9 0.56 3.46 -12 -6 -9 -0.48 2.55 -12 -6 -9 -1.64 4.22 12 -6 9 2.28 4.11 12 -6 9 -4.61 3.48 12 -6 9 1.38 5.37 12 6 9 -2.63 5.19 12 -6 9 0.87 3.90 12 6 9 -1.99 5.09 -12 -6 -9 -3.14 4.86 12 6 9 1.70 5.34 12 -6 9 3.23 4.53 12 -6 9 6.00 5.51 12 -6 9 0.18 5.03 -12 6 -9 5.84 7.53 -12 -6 -9 5.26 7.77 12 6 10 73.44 10.10 -12 -6 -10 65.55 9.20 -12 6 -10 36.72 6.10 -12 -6 -10 47.66 7.13 12 -6 10 61.40 8.82 12 -6 10 48.77 7.47 12 6 10 35.54 3.87 12 -6 10 61.35 9.68 12 6 10 37.24 7.16 -12 -6 -10 49.28 7.68 12 6 10 46.77 8.47 12 -6 10 55.93 8.85 12 -6 10 51.67 9.04 12 -6 10 44.60 8.03 -12 6 -10 16.72 8.44 -12 -6 -10 47.39 8.34 12 6 11 -0.07 2.62 -12 -6 -11 1.73 2.57 -12 6 -11 1.14 4.19 -12 -6 -11 2.19 3.95 12 -6 11 -0.99 3.01 12 -6 11 -5.50 4.59 12 6 11 0.51 2.83 12 -6 11 -2.62 4.44 12 6 11 -0.71 6.44 -12 -6 -11 1.37 4.19 12 6 11 3.31 4.12 12 -6 11 -2.38 4.27 12 -6 11 2.96 4.19 12 -6 11 3.37 4.06 -12 6 -11 -4.30 5.61 -12 -6 -11 -4.90 7.05 -12 -6 -12 55.59 10.32 -12 6 -12 28.03 6.73 -12 -6 -12 52.53 10.02 12 -6 12 47.08 8.69 12 -6 12 36.71 7.35 12 6 12 24.75 4.41 12 -6 12 44.05 8.88 12 6 12 25.60 6.35 -12 -6 -12 40.36 8.23 12 6 12 28.74 6.89 12 -6 12 47.03 9.22 12 -6 12 40.61 8.12 12 -6 12 40.21 8.16 -12 6 -12 19.07 5.55 -12 -6 -12 38.63 9.39 12 -7 -20 3.60 3.93 -12 -7 20 4.03 3.29 -12 7 20 -3.05 3.95 12 7 -20 3.08 6.01 12 -7 -20 1.66 5.34 -12 7 20 3.94 3.87 -12 -7 20 0.52 4.07 12 7 -20 4.07 6.32 12 -7 -20 2.57 5.12 -12 7 20 -1.10 9.21 -12 -7 20 2.86 4.99 12 -7 -19 2.85 4.56 -12 -7 19 1.37 4.24 -12 7 19 0.66 4.64 12 7 -19 4.57 6.84 12 -7 -19 0.27 4.99 -12 7 19 -2.13 5.21 -12 -7 19 -4.48 4.69 12 7 -19 -7.32 5.04 12 7 -19 4.52 7.20 12 -7 -19 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16.52 4.38 15 -7 -4 23.90 4.94 -15 7 4 18.57 6.88 -15 -7 4 20.50 6.90 15 7 -4 22.53 5.85 15 7 -4 14.24 3.98 -15 -7 4 11.78 5.23 15 -7 -4 19.58 7.08 15 7 -4 15.42 9.19 15 7 -4 21.31 8.40 15 -7 -4 10.44 4.69 15 -7 -4 8.53 7.78 15 -7 -4 15.48 6.30 15 7 -3 13.95 4.44 -15 -7 3 9.63 5.08 -15 -7 3 8.44 4.85 15 -7 -3 11.07 3.69 15 -7 -3 13.61 5.92 15 -7 -3 0.17 6.51 -15 7 3 16.27 7.70 -15 -7 3 11.08 4.85 15 7 -3 10.23 8.35 15 7 -3 10.08 5.57 -15 -7 3 7.83 5.10 15 -7 -3 16.54 7.75 15 7 -3 15.35 6.64 15 7 -3 16.34 9.15 15 -7 -3 12.15 5.09 15 -7 -3 24.10 9.05 15 -7 -3 19.75 7.17 15 7 -2 12.12 3.47 -15 -7 2 14.07 3.92 -15 -7 2 10.98 4.13 15 -7 -2 10.06 6.33 15 -7 -2 8.81 3.59 15 -7 -2 7.61 5.37 -15 7 2 7.63 9.98 -15 -7 2 15.74 4.58 15 7 -2 19.12 5.50 15 7 -2 12.80 4.86 -15 -7 2 14.09 4.92 15 7 -2 6.50 9.22 15 7 -2 14.20 7.65 15 -7 -2 8.17 6.26 15 -7 -2 5.93 6.25 15 -7 -2 12.58 6.42 15 7 -1 82.47 9.69 -15 -7 1 75.75 10.49 -15 -7 1 61.06 7.22 15 -7 -1 81.58 10.09 15 -7 -1 75.74 9.63 15 -7 -1 74.20 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2.08 5.12 15 8 -15 -6.72 5.11 15 8 -15 7.95 7.82 15 -8 -15 12.73 6.60 -15 8 15 -4.11 8.04 -15 -8 15 -0.50 6.00 -15 -8 14 14.12 3.42 -15 8 14 38.90 9.28 -15 -8 14 16.31 3.53 15 8 -14 21.79 4.01 15 -8 -14 21.33 5.81 -15 8 14 20.22 7.13 -15 -8 14 17.37 3.43 15 8 -14 30.82 7.19 15 8 -14 22.13 5.20 15 8 -14 35.87 8.85 15 -8 -14 22.18 6.66 -15 8 14 23.52 6.77 -15 -8 14 12.43 6.27 15 8 -13 2.07 2.55 -15 -8 13 0.40 3.69 -15 8 13 -3.49 7.01 -15 -8 13 -0.77 3.96 15 -8 -13 4.75 3.31 15 8 -13 7.08 4.41 15 -8 -13 3.61 2.78 15 -8 -13 1.28 4.27 -15 8 13 8.32 8.52 -15 -8 13 3.66 3.96 15 8 -13 0.66 6.62 15 -8 -13 5.39 5.52 15 8 -13 5.00 5.89 15 8 -13 1.15 9.28 15 -8 -13 11.95 8.68 -15 8 13 5.96 7.65 -15 -8 13 2.77 6.02 15 8 -12 -2.53 3.06 -15 -8 12 -0.97 3.63 -15 8 12 -3.53 5.48 -15 -8 12 -4.13 4.81 15 -8 -12 1.58 3.69 15 8 -12 1.12 4.87 15 -8 -12 -1.58 2.82 15 -8 -12 -6.76 5.81 -15 8 12 -7.30 8.76 -15 -8 12 0.59 3.40 -15 -8 12 -2.05 4.21 15 8 -12 -0.02 5.84 15 -8 -12 -5.92 6.95 15 8 -12 -3.86 7.46 15 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5.98 3.64 15 -8 -5 3.65 3.51 15 -8 -5 1.80 3.65 15 -8 -5 1.04 5.39 -15 8 5 0.51 7.64 -15 -8 5 6.00 5.15 15 8 -5 1.52 6.58 15 8 -5 1.35 4.67 -15 -8 5 -0.44 5.44 15 -8 -5 3.49 8.61 15 8 -5 -0.85 6.77 15 -8 -5 2.57 8.39 -15 -8 5 -0.40 3.66 15 -8 -5 1.96 9.28 15 8 -4 14.37 2.86 -15 -8 4 10.88 3.53 -15 -8 4 13.32 3.65 15 -8 -4 12.41 4.01 15 -8 -4 14.87 3.84 15 -8 -4 6.68 4.07 -15 8 4 12.50 8.16 -15 -8 4 16.38 5.06 15 8 -4 14.89 5.25 15 8 -4 11.66 5.79 -15 -8 4 6.49 4.63 15 -8 -4 14.35 5.95 15 8 -4 9.57 8.91 15 8 -4 14.92 6.33 15 -8 -4 11.16 3.26 15 -8 -4 7.06 5.22 15 -8 -4 14.90 8.96 15 8 -3 -0.44 3.94 -15 -8 3 2.90 3.70 -15 -8 3 -0.66 5.00 15 -8 -3 0.33 5.32 15 -8 -3 6.21 5.09 15 -8 -3 -3.93 4.46 -15 8 3 1.70 6.87 -15 -8 3 2.03 5.73 15 8 -3 -0.40 7.52 15 8 -3 1.75 4.58 -15 -8 3 4.35 5.35 15 -8 -3 9.31 5.54 15 8 -3 2.77 6.93 15 8 -3 5.58 6.76 15 -8 -3 2.30 3.80 15 -8 -3 -0.62 7.12 15 -8 -3 -4.54 9.79 15 8 -2 20.20 3.32 -15 -8 2 12.55 3.38 -15 -8 2 19.76 3.75 15 -8 -2 20.55 4.18 15 -8 -2 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-20 -1 3 2.26 4.04 -20 1 3 2.80 5.81 -20 -1 3 -1.23 4.50 20 1 -3 4.47 4.41 20 -1 -3 1.17 4.63 20 -2 -10 9.20 1.99 20 2 -10 10.62 2.93 -20 2 10 6.65 3.01 -20 -2 10 7.07 3.46 -20 2 10 5.19 3.59 -20 -2 10 6.49 3.71 20 2 -10 6.10 3.15 20 -2 -10 3.70 3.13 -20 2 10 3.17 5.80 -20 -2 10 5.42 4.67 20 2 -10 2.70 5.71 20 -2 -10 4.77 3.37 20 2 -9 13.30 3.18 20 -2 -9 13.09 1.83 -20 -2 9 7.93 3.28 -20 2 9 7.61 2.68 -20 2 9 11.18 3.26 -20 -2 9 6.08 2.97 20 -2 -9 5.96 3.11 20 2 -9 4.96 3.14 -20 2 9 2.50 5.77 -20 -2 9 3.61 5.64 20 2 -9 7.54 4.93 20 -2 -9 5.12 3.66 20 2 -8 -2.15 3.40 20 -2 -8 1.39 2.10 -20 -2 8 -2.61 3.44 -20 2 8 -4.10 2.88 -20 -2 8 -0.35 3.05 20 -2 -8 -1.04 2.73 20 2 -8 1.43 2.54 -20 2 8 -0.57 5.25 -20 -2 8 -1.93 5.95 20 2 -8 -2.41 5.04 20 -2 -8 0.71 3.14 20 -2 -7 5.15 1.92 20 2 -7 4.59 2.93 -20 2 7 8.23 2.94 -20 -2 7 3.81 3.22 20 2 -7 6.66 3.01 20 -2 -7 4.50 2.82 -20 2 7 8.01 4.69 -20 -2 7 3.54 4.52 -20 2 7 4.46 4.22 -20 -2 7 -1.14 3.92 20 2 -7 0.92 4.80 20 -2 -7 1.67 3.80 20 -2 -6 6.13 1.97 20 2 -6 7.55 2.31 -20 2 6 2.08 2.76 -20 -2 6 5.05 2.84 20 2 -6 6.13 2.55 20 -2 -6 6.33 2.99 -20 2 6 -0.48 4.69 -20 -2 6 12.88 5.17 -20 2 6 5.16 4.56 -20 -2 6 4.28 4.47 20 2 -6 7.76 4.54 20 -2 -6 -0.21 3.81 20 -2 -5 2.12 1.90 20 2 -5 3.07 2.76 -20 2 5 2.65 2.44 -20 -2 5 1.96 3.06 20 -2 -5 2.39 2.68 -20 2 5 1.33 4.81 -20 -2 5 -1.83 3.93 -20 2 5 -3.20 5.73 -20 -2 5 1.03 3.77 20 2 -5 -1.68 4.10 20 -2 -5 -0.56 4.30 20 2 -4 3.01 2.18 -20 -2 4 0.75 2.18 20 -2 -4 1.20 2.88 -20 2 4 3.80 4.29 -20 -2 4 -1.79 3.84 20 2 -4 2.84 2.93 -20 2 4 2.60 5.50 -20 -2 4 3.07 4.25 20 2 -4 1.74 4.67 20 -2 -4 -0.75 4.16 20 3 -9 6.93 2.50 -20 -3 9 4.82 2.73 -20 -3 9 4.19 3.31 20 3 -9 3.98 2.72 20 -3 -9 4.35 3.17 -20 3 9 2.89 5.86 -20 -3 9 1.72 5.22 20 3 -9 8.09 5.61 20 3 -8 0.04 2.27 -20 -3 8 -2.38 2.74 -20 -3 8 0.92 3.44 20 -3 -8 -0.35 3.30 -20 3 8 -0.56 4.41 -20 -3 8 0.51 5.54 -20 3 8 -6.00 4.09 20 3 -8 -1.92 5.44 20 -3 -8 -0.06 2.76 20 3 -7 10.56 2.74 -20 -3 7 6.66 2.57 20 -3 -7 8.79 2.79 -20 3 7 12.30 5.98 -20 -3 7 8.67 4.74 -20 3 7 6.66 4.41 20 3 -7 9.39 5.35 20 -3 -7 2.61 3.34 20 3 -6 24.56 4.98 -20 -3 6 13.39 3.41 20 -3 -6 15.46 3.29 -20 3 6 11.47 4.98 -20 -3 6 18.05 4.65 -20 3 6 10.54 4.62 -20 -3 6 9.83 4.03 20 3 -6 9.20 4.86 20 -3 -6 12.49 3.30 20 3 -5 14.34 2.47 -20 -3 5 5.15 2.73 20 -3 -5 7.93 3.06 -20 3 5 9.66 4.88 -20 -3 5 9.59 4.45 20 3 -5 12.37 2.78 -20 3 5 10.48 4.93 -20 -3 5 15.04 5.08 20 3 -5 8.45 4.32 20 -3 -5 10.29 2.97 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 44565 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp Fe1 Fe 0.85223(4) 0.66105(5) 0.60785(4) 0.0526(3) Uani 1 1 d . . N11 N 0.9579(2) 0.6942(3) 0.59187(19) 0.0535(10) Uani 1 1 d . . N21 N 0.9058(2) 0.5887(2) 0.68514(18) 0.0444(8) Uani 1 1 d . . C11 C 1.1042(4) 0.7009(5) 0.6156(4) 0.095(2) Uani 1 1 d . . H11A H 1.0921 0.7187 0.5676 0.143 Uiso 1 1 calc R U H11B H 1.1453 0.6592 0.6248 0.143 Uiso 1 1 calc R U H11C H 1.1235 0.7464 0.6465 0.143 Uiso 1 1 calc R U C21 C 1.0290(3) 0.6673(3) 0.6278(3) 0.0597(13) Uani 1 1 d . . C31 C 1.0397(3) 0.6102(3) 0.6802(2) 0.0549(12) Uani 1 1 d . . H31 H 1.0936 0.5944 0.7008 0.066 Uiso 1 1 calc R U C41 C 0.9850(3) 0.5729(3) 0.7071(2) 0.0477(10) Uani 1 1 d . . C51 C 1.0182(3) 0.5119(3) 0.7622(3) 0.0567(12) Uani 1 1 d . . H51A H 0.9814 0.5047 0.7897 0.085 Uiso 1 1 calc R U H51B H 1.0701 0.5303 0.7920 0.085 Uiso 1 1 calc R U H51C H 1.0251 0.4608 0.7409 0.085 Uiso 1 1 calc R U C12 C 0.9530(3) 0.7487(4) 0.5362(2) 0.0603(13) Uani 1 1 d . . C22 C 0.9375(4) 0.7171(4) 0.4690(3) 0.0696(15) Uani 1 1 d . . C32 C 0.9256(4) 0.7716(5) 0.4143(3) 0.0818(19) Uani 1 1 d . . H32 H 0.9157 0.7512 0.3689 0.098 Uiso 1 1 calc R U C42 C 0.9276(5) 0.8520(5) 0.4233(3) 0.088(2) Uani 1 1 d . . H42 H 0.9187 0.8868 0.3848 0.105 Uiso 1 1 calc R U C52 C 0.9429(4) 0.8832(4) 0.4900(3) 0.0819(19) Uani 1 1 d . . H52 H 0.9440 0.9396 0.4968 0.098 Uiso 1 1 calc R U C62 C 0.9567(4) 0.8319(4) 0.5462(3) 0.0690(16) Uani 1 1 d . . C72 C 0.9359(4) 0.6280(4) 0.4572(3) 0.0814(18) Uani 1 1 d . . H72 H 0.9161 0.6034 0.4939 0.098 Uiso 1 1 calc R U C82 C 1.0191(7) 0.5918(7) 0.4658(6) 0.154(5) Uani 1 1 d . . H82A H 1.0472 0.6241 0.4400 0.231 Uiso 1 1 calc R U H82B H 1.0133 0.5368 0.4482 0.231 Uiso 1 1 calc R U H82C H 1.0499 0.5916 0.5148 0.231 Uiso 1 1 calc R U C92 C 0.8771(8) 0.6026(6) 0.3882(4) 0.156(5) Uani 1 1 d . . H92A H 0.8227 0.6169 0.3875 0.234 Uiso 1 1 calc R U H92B H 0.8806 0.5445 0.3826 0.234 Uiso 1 1 calc R U H92C H 0.8905 0.6300 0.3505 0.234 Uiso 1 1 calc R U C102 C 0.9784(5) 0.8687(4) 0.6184(3) 0.083(2) Uani 1 1 d . . H102 H 0.9900 0.8240 0.6527 0.100 Uiso 1 1 calc R U C112 C 1.0514(5) 0.9202(5) 0.6326(3) 0.093(2) Uani 1 1 d . . H11D H 1.0953 0.8891 0.6249 0.139 Uiso 1 1 calc R U H11E H 1.0665 0.9386 0.6806 0.139 Uiso 1 1 calc R U H11F H 1.0401 0.9666 0.6017 0.139 Uiso 1 1 calc R U C122 C 0.9120(6) 0.9188(8) 0.6302(6) 0.161(5) Uani 1 1 d . . H12A H 0.8893 0.9532 0.5900 0.241 Uiso 1 1 calc R U H12B H 0.9332 0.9521 0.6713 0.241 Uiso 1 1 calc R U H12C H 0.8702 0.8835 0.6369 0.241 Uiso 1 1 calc R U C13 C 0.8548(3) 0.5496(3) 0.7178(2) 0.0462(10) Uani 1 1 d . . C23 C 0.8240(3) 0.4729(3) 0.6965(3) 0.0597(13) Uani 1 1 d . . C33 C 0.7664(4) 0.4413(3) 0.7235(4) 0.0756(17) Uani 1 1 d . . H33 H 0.7449 0.3898 0.7090 0.091 Uiso 1 1 calc R U C43 C 0.7401(4) 0.4824(4) 0.7705(4) 0.0806(18) Uani 1 1 d . . H43 H 0.6996 0.4603 0.7872 0.097 Uiso 1 1 calc R U C53 C 0.7729(4) 0.5570(3) 0.7939(3) 0.0658(14) Uani 1 1 d . . H53 H 0.7556 0.5850 0.8276 0.079 Uiso 1 1 calc R U C63 C 0.8304(3) 0.5904(3) 0.7684(2) 0.0486(10) Uani 1 1 d . . C73 C 0.8517(3) 0.4229(3) 0.6454(3) 0.0673(15) Uani 1 1 d . . H73 H 0.8914 0.4548 0.6299 0.081 Uiso 1 1 calc R U C83 C 0.8922(4) 0.3448(3) 0.6794(4) 0.0830(19) Uani 1 1 d . . H83A H 0.9358 0.3579 0.7210 0.124 Uiso 1 1 calc R U H83B H 0.9138 0.3158 0.6469 0.124 Uiso 1 1 calc R U H83C H 0.8529 0.3111 0.6919 0.124 Uiso 1 1 calc R U C93 C 0.7823(4) 0.4020(4) 0.5827(4) 0.093(2) Uani 1 1 d . . H93A H 0.7413 0.3735 0.5974 0.140 Uiso 1 1 calc R U H93B H 0.8013 0.3677 0.5517 0.140 Uiso 1 1 calc R U H93C H 0.7596 0.4513 0.5585 0.140 Uiso 1 1 calc R U C103 C 0.8676(3) 0.6705(3) 0.7962(2) 0.0482(11) Uani 1 1 d . . H103 H 0.8845 0.6965 0.7585 0.058 Uiso 1 1 calc R U C113 C 0.9419(4) 0.6612(3) 0.8570(3) 0.0669(15) Uani 1 1 d . . H11G H 0.9278 0.6358 0.8953 0.100 Uiso 1 1 calc R U H11H H 0.9652 0.7141 0.8713 0.100 Uiso 1 1 calc R U H11I H 0.9807 0.6277 0.8436 0.100 Uiso 1 1 calc R U C123 C 0.8101(4) 0.7280(3) 0.8152(3) 0.0759(17) Uani 1 1 d . . H12D H 0.7656 0.7401 0.7740 0.114 Uiso 1 1 calc R U H12E H 0.8382 0.7776 0.8336 0.114 Uiso 1 1 calc R U H12F H 0.7894 0.7032 0.8501 0.114 Uiso 1 1 calc R U C14 C 0.7613(3) 0.7434(4) 0.6210(3) 0.0669(14) Uani 1 1 d D . H14 H 0.765(4) 0.785(3) 0.654(3) 0.08(2) Uiso 1 1 d D . C24 C 0.7807(3) 0.7535(4) 0.5584(3) 0.0699(16) Uani 1 1 d D . H24 H 0.802(4) 0.803(3) 0.548(4) 0.11(2) Uiso 1 1 d D . C34 C 0.7726(4) 0.6889(5) 0.5129(3) 0.0763(17) Uani 1 1 d D . H34 H 0.786(4) 0.693(4) 0.4702(19) 0.077(18) Uiso 1 1 d D . C44 C 0.7451(4) 0.6155(5) 0.5301(3) 0.0790(18) Uani 1 1 d D . H44 H 0.735(4) 0.565(2) 0.507(3) 0.081(19) Uiso 1 1 d D . C54 C 0.7062(4) 0.6126(5) 0.5826(4) 0.0838(19) Uani 1 1 d D . H54 H 0.676(3) 0.568(2) 0.592(3) 0.070(16) Uiso 1 1 d D . C64 C 0.7139(4) 0.6762(4) 0.6278(3) 0.0735(16) Uani 1 1 d D . H64 H 0.691(3) 0.678(3) 0.665(2) 0.060(15) Uiso 1 1 d D . K1 K 0.60236(7) 0.75600(7) 0.48037(5) 0.0616(3) Uani 1 1 d . . O10 O 0.6599(4) 0.9180(3) 0.4935(3) 0.1034(17) Uani 1 1 d . . C20 C 0.6836(6) 0.9509(5) 0.4415(5) 0.114(3) Uani 1 1 d . . H20A H 0.7281 0.9888 0.4608 0.137 Uiso 1 1 calc R U H20B H 0.6388 0.9811 0.4101 0.137 Uiso 1 1 calc R U C30 C 0.7101(6) 0.8865(5) 0.4022(4) 0.122(4) Uani 1 1 d . . H30A H 0.7298 0.9113 0.3661 0.146 Uiso 1 1 calc R U H30B H 0.7549 0.8566 0.4338 0.146 Uiso 1 1 calc R U O40 O 0.6492(3) 0.8338(3) 0.3717(3) 0.0959(15) Uani 1 1 d . . C50 C 0.6718(5) 0.7724(6) 0.3326(4) 0.116(3) Uani 1 1 d . . H50A H 0.7158 0.7405 0.3631 0.140 Uiso 1 1 calc R U H50B H 0.6915 0.7971 0.2964 0.140 Uiso 1 1 calc R U C60 C 0.6033(6) 0.7191(5) 0.3000(3) 0.100(2) Uani 1 1 d . . H60A H 0.5569 0.7513 0.2735 0.120 Uiso 1 1 calc R U H60B H 0.6177 0.6816 0.2679 0.120 Uiso 1 1 calc R U O70 O 0.5834(3) 0.6752(3) 0.3537(2) 0.0922(14) Uani 1 1 d . . C80 C 0.5262(6) 0.6220(4) 0.3345(5) 0.108(3) Uani 1 1 d . . H80A H 0.5412 0.5828 0.3039 0.130 Uiso 1 1 calc R U H80B H 0.4772 0.6496 0.3068 0.130 Uiso 1 1 calc R U C90 C 0.5072(5) 0.5777(4) 0.3901(3) 0.087(2) Uani 1 1 d . . H90A H 0.4665 0.5360 0.3709 0.104 Uiso 1 1 calc R U H90B H 0.5557 0.5516 0.4205 0.104 Uiso 1 1 calc R U O100 O 0.4770(3) 0.6367(2) 0.4280(2) 0.0801(12) Uani 1 1 d . . C110 C 0.4610(5) 0.6068(4) 0.4840(3) 0.089(2) Uani 1 1 d . . H11J H 0.5113 0.5873 0.5169 0.106 Uiso 1 1 calc R U H11K H 0.4246 0.5604 0.4700 0.106 Uiso 1 1 calc R U C120 C 0.4253(4) 0.6638(4) 0.5180(3) 0.0742(16) Uani 1 1 d . . H12G H 0.4063 0.6369 0.5536 0.089 Uiso 1 1 calc R U H12H H 0.3791 0.6896 0.4843 0.089 Uiso 1 1 calc R U O130 O 0.4842(3) 0.7224(3) 0.5491(2) 0.0842(12) Uani 1 1 d . . C140 C 0.4618(7) 0.7830(5) 0.5806(5) 0.122(3) Uani 1 1 d . . H14A H 0.4393 0.7619 0.6164 0.147 Uiso 1 1 calc R U H14B H 0.4190 0.8131 0.5468 0.147 Uiso 1 1 calc R U C150 C 0.5265(5) 0.8371(4) 0.6125(3) 0.086(2) Uani 1 1 d . . H15A H 0.5098 0.8749 0.6431 0.103 Uiso 1 1 calc R U H15B H 0.5731 0.8064 0.6407 0.103 Uiso 1 1 calc R U O160 O 0.5471(3) 0.8791(3) 0.5614(2) 0.0938(14) Uani 1 1 d . . C170 C 0.6079(6) 0.9306(5) 0.5886(4) 0.108(3) Uani 1 1 d . . H17A H 0.6548 0.9011 0.6178 0.129 Uiso 1 1 calc R U H17B H 0.5917 0.9708 0.6176 0.129 Uiso 1 1 calc R U C180 C 0.6296(6) 0.9726(4) 0.5288(5) 0.106(3) Uani 1 1 d . . H18A H 0.5813 0.9978 0.4974 0.127 Uiso 1 1 calc R U H18B H 0.6695 1.0151 0.5474 0.127 Uiso 1 1 calc R U O190 O 0.2304(4) 0.8619(4) 0.5761(3) 0.117(2) Uani 1 1 d . . C200 C 0.2896(10) 0.8774(11) 0.6975(6) 0.235(10) Uani 1 1 d . . H20C H 0.2934 0.9357 0.6939 0.353 Uiso 1 1 calc R U H20D H 0.3368 0.8572 0.7328 0.353 Uiso 1 1 calc R U H20E H 0.2415 0.8639 0.7104 0.353 Uiso 1 1 calc R U C210 C 0.2852(8) 0.8422(10) 0.6342(7) 0.178(6) Uani 1 1 d . . H21A H 0.3377 0.8509 0.6265 0.214 Uiso 1 1 calc R U H21B H 0.2802 0.7837 0.6401 0.214 Uiso 1 1 calc R U C220 C 0.2196(7) 0.8280(6) 0.5169(6) 0.126(3) Uani 1 1 d . . H22A H 0.2115 0.7702 0.5233 0.151 Uiso 1 1 calc R U H22B H 0.2704 0.8329 0.5054 0.151 Uiso 1 1 calc R U C230 C 0.1582(8) 0.8525(7) 0.4580(5) 0.141(4) Uani 1 1 d . . H23A H 0.1065 0.8349 0.4621 0.212 Uiso 1 1 calc R U H23B H 0.1668 0.8285 0.4167 0.212 Uiso 1 1 calc R U H23C H 0.1586 0.9110 0.4542 0.212 Uiso 1 1 calc R U O240 O 0.5763(3) 0.4101(3) 0.3054(3) 0.0883(13) Uani 1 1 d . . C250 C 0.5181(5) 0.3676(4) 0.2545(3) 0.087(2) Uani 1 1 d . . H25A H 0.5349 0.3111 0.2538 0.105 Uiso 1 1 calc R U H25B H 0.5126 0.3912 0.2087 0.105 Uiso 1 1 calc R U C260 C 0.4417(5) 0.3709(5) 0.2688(5) 0.110(3) Uani 1 1 d . . H26A H 0.4500 0.3614 0.3180 0.165 Uiso 1 1 calc R U H26B H 0.4061 0.3298 0.2418 0.165 Uiso 1 1 calc R U H26C H 0.4177 0.4239 0.2563 0.165 Uiso 1 1 calc R U C270 C 0.6525(6) 0.4117(5) 0.2960(5) 0.110(3) Uani 1 1 d . . H27A H 0.6492 0.4355 0.2506 0.132 Uiso 1 1 calc R U H27B H 0.6735 0.3565 0.2973 0.132 Uiso 1 1 calc R U C280 C 0.7066(7) 0.4604(11) 0.3521(9) 0.209(7) Uani 1 1 d . . H28A H 0.6831 0.5135 0.3531 0.314 Uiso 1 1 calc R U H28B H 0.7585 0.4663 0.3436 0.314 Uiso 1 1 calc R U H28C H 0.7139 0.4336 0.3964 0.314 Uiso 1 1 calc R U loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0528(5) 0.0655(5) 0.0379(4) -0.0003(3) 0.0112(3) -0.0116(3) N11 0.058(2) 0.070(3) 0.0350(19) -0.0073(18) 0.0180(17) -0.009(2) N21 0.051(2) 0.045(2) 0.0390(18) -0.0074(15) 0.0149(16) -0.0083(16) C11 0.075(4) 0.126(6) 0.106(5) 0.025(5) 0.058(4) 0.006(4) C21 0.059(3) 0.080(4) 0.047(3) -0.009(2) 0.026(2) -0.003(3) C31 0.050(3) 0.068(3) 0.049(3) -0.012(2) 0.019(2) -0.001(2) C41 0.052(3) 0.050(3) 0.042(2) -0.0152(19) 0.014(2) -0.002(2) C51 0.060(3) 0.050(3) 0.059(3) -0.007(2) 0.018(2) 0.001(2) C12 0.067(3) 0.081(4) 0.042(3) -0.001(2) 0.030(2) -0.006(3) C22 0.081(4) 0.090(4) 0.047(3) -0.007(3) 0.033(3) -0.005(3) C32 0.093(4) 0.120(6) 0.043(3) -0.002(3) 0.037(3) -0.008(4) C42 0.117(6) 0.104(5) 0.054(3) 0.011(3) 0.043(4) -0.026(4) C52 0.113(5) 0.084(4) 0.062(4) 0.003(3) 0.046(3) -0.039(4) C62 0.091(4) 0.078(4) 0.050(3) -0.004(3) 0.039(3) -0.028(3) C72 0.100(5) 0.101(5) 0.048(3) -0.012(3) 0.029(3) 0.020(4) C82 0.175(10) 0.151(9) 0.176(11) -0.013(8) 0.114(9) 0.049(8) C92 0.252(14) 0.094(6) 0.078(5) -0.030(5) -0.018(7) 0.007(7) C102 0.129(6) 0.079(4) 0.053(3) -0.010(3) 0.043(4) -0.045(4) C112 0.109(5) 0.105(5) 0.062(4) 0.001(3) 0.023(4) -0.042(4) C122 0.118(7) 0.255(14) 0.126(8) -0.115(9) 0.063(6) -0.047(8) C13 0.051(2) 0.041(2) 0.048(2) -0.0041(19) 0.017(2) -0.0055(19) C23 0.059(3) 0.045(3) 0.079(4) -0.015(2) 0.026(3) -0.008(2) C33 0.081(4) 0.046(3) 0.115(5) -0.011(3) 0.051(4) -0.017(3) C43 0.080(4) 0.063(4) 0.117(5) 0.009(3) 0.058(4) -0.006(3) C53 0.079(4) 0.056(3) 0.078(4) 0.007(3) 0.047(3) 0.009(3) C63 0.059(3) 0.039(2) 0.051(3) 0.0032(19) 0.022(2) 0.005(2) C73 0.066(3) 0.055(3) 0.082(4) -0.029(3) 0.023(3) -0.009(2) C83 0.086(4) 0.057(3) 0.108(5) -0.026(3) 0.032(4) -0.005(3) C93 0.083(4) 0.086(5) 0.100(5) -0.047(4) 0.010(4) -0.006(4) C103 0.064(3) 0.041(2) 0.040(2) -0.0006(18) 0.016(2) 0.003(2) C113 0.087(4) 0.049(3) 0.056(3) -0.006(2) 0.008(3) 0.008(3) C123 0.083(4) 0.056(3) 0.081(4) -0.020(3) 0.011(3) 0.017(3) C14 0.053(3) 0.082(4) 0.062(3) 0.011(3) 0.012(3) 0.002(3) C24 0.056(3) 0.089(4) 0.058(3) 0.024(3) 0.007(2) -0.004(3) C34 0.063(3) 0.109(5) 0.046(3) 0.006(3) 0.000(3) -0.018(3) C44 0.067(3) 0.104(5) 0.055(3) -0.010(3) 0.002(3) -0.024(3) C54 0.076(4) 0.090(5) 0.072(4) 0.015(4) 0.002(3) -0.021(3) C64 0.076(4) 0.080(4) 0.064(4) 0.019(3) 0.019(3) 0.003(3) K1 0.0698(7) 0.0619(7) 0.0429(6) 0.0000(5) 0.0013(5) -0.0124(5) O10 0.142(5) 0.078(3) 0.071(3) -0.002(3) 0.002(3) -0.018(3) C20 0.138(7) 0.096(6) 0.099(6) 0.019(5) 0.022(5) -0.041(5) C30 0.150(8) 0.092(5) 0.078(5) 0.019(4) -0.035(5) -0.048(5) O40 0.103(4) 0.098(4) 0.079(3) 0.021(3) 0.015(3) -0.004(3) C50 0.086(5) 0.165(8) 0.091(5) -0.047(6) 0.015(4) 0.030(5) C60 0.146(7) 0.111(6) 0.050(3) 0.000(4) 0.039(4) -0.010(5) O70 0.122(4) 0.085(3) 0.063(3) 0.000(2) 0.017(3) 0.010(3) C80 0.145(7) 0.049(4) 0.155(8) -0.003(4) 0.082(6) -0.007(4) C90 0.135(6) 0.060(3) 0.064(4) -0.020(3) 0.027(4) -0.008(4) O100 0.104(3) 0.063(2) 0.072(3) 0.003(2) 0.024(2) -0.001(2) C110 0.126(6) 0.076(4) 0.059(4) 0.017(3) 0.021(4) 0.025(4) C120 0.088(4) 0.067(4) 0.066(4) -0.006(3) 0.020(3) -0.022(3) O130 0.089(3) 0.089(3) 0.068(3) -0.011(2) 0.013(2) 0.007(2) C140 0.176(9) 0.072(5) 0.092(5) -0.021(4) -0.001(6) -0.002(5) C150 0.129(6) 0.069(4) 0.051(3) -0.009(3) 0.015(4) -0.003(4) O160 0.121(4) 0.072(3) 0.074(3) -0.010(2) 0.007(3) -0.007(3) C170 0.158(8) 0.071(4) 0.082(5) -0.010(4) 0.019(5) -0.019(5) C180 0.129(6) 0.063(4) 0.112(6) -0.007(4) 0.013(5) -0.027(4) O190 0.146(5) 0.109(4) 0.073(3) 0.008(3) -0.002(3) -0.060(4) C200 0.277(19) 0.30(2) 0.086(7) 0.028(10) -0.006(9) -0.197(17) C210 0.126(9) 0.275(18) 0.133(10) 0.084(11) 0.039(8) -0.012(9) C220 0.133(8) 0.132(8) 0.128(8) 0.031(7) 0.063(7) 0.017(6) C230 0.169(10) 0.139(8) 0.095(6) -0.034(6) 0.009(7) -0.035(7) O240 0.087(3) 0.089(3) 0.094(3) -0.019(3) 0.035(3) -0.011(2) C250 0.126(6) 0.078(4) 0.068(4) -0.011(3) 0.045(4) -0.005(4) C260 0.098(5) 0.101(6) 0.128(7) -0.035(5) 0.028(5) -0.017(4) C270 0.119(7) 0.098(6) 0.127(7) 0.002(5) 0.060(6) 0.004(5) C280 0.088(7) 0.260(17) 0.269(18) -0.089(15) 0.037(9) -0.021(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Fe Fe -1.1336 3.1974 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.3868 1.0657 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 N21 Fe1 N11 92.99(16) . . N21 Fe1 C24 157.2(2) . . N11 Fe1 C24 99.7(2) . . N21 Fe1 C34 154.8(2) . . N11 Fe1 C34 100.5(2) . . C24 Fe1 C34 39.7(3) . . N21 Fe1 C14 118.56(19) . . N11 Fe1 C14 125.3(2) . . C24 Fe1 C14 39.1(2) . . C34 Fe1 C14 70.0(3) . . N21 Fe1 C44 117.5(2) . . N11 Fe1 C44 126.7(2) . . C24 Fe1 C44 69.0(3) . . C34 Fe1 C44 38.1(3) . . C14 Fe1 C44 78.8(3) . . C21 N11 C12 118.4(4) . . C21 N11 Fe1 124.7(3) . . C12 N11 Fe1 116.9(3) . . C41 N21 C13 118.9(4) . . C41 N21 Fe1 125.4(3) . . C13 N21 Fe1 115.7(3) . . C21 C11 H11A 109.5 . . C21 C11 H11B 109.5 . . H11A C11 H11B 109.5 . . C21 C11 H11C 109.5 . . H11A C11 H11C 109.5 . . H11B C11 H11C 109.5 . . N11 C21 C31 122.8(5) . . N11 C21 C11 120.5(5) . . C31 C21 C11 116.7(5) . . C41 C31 C21 130.9(5) . . C41 C31 H31 114.6 . . C21 C31 H31 114.6 . . N21 C41 C31 123.1(4) . . N21 C41 C51 120.9(4) . . C31 C41 C51 116.0(4) . . C41 C51 H51A 109.5 . . C41 C51 H51B 109.5 . . H51A C51 H51B 109.5 . . C41 C51 H51C 109.5 . . H51A C51 H51C 109.5 . . H51B C51 H51C 109.5 . . C62 C12 C22 119.8(5) . . C62 C12 N11 121.6(4) . . C22 C12 N11 118.3(5) . . C32 C22 C12 117.6(6) . . C32 C22 C72 121.6(5) . . C12 C22 C72 120.8(5) . . C42 C32 C22 123.0(6) . . C42 C32 H32 118.5 . . C22 C32 H32 118.5 . . C32 C42 C52 119.3(6) . . C32 C42 H42 120.3 . . C52 C42 H42 120.3 . . C62 C52 C42 120.1(6) . . C62 C52 H52 119.9 . . C42 C52 H52 119.9 . . C52 C62 C12 120.1(5) . . C52 C62 C102 118.2(5) . . C12 C62 C102 121.6(5) . . C22 C72 C92 113.3(6) . . C22 C72 C82 113.3(7) . . C92 C72 C82 110.6(8) . . C22 C72 H72 106.3 . . C92 C72 H72 106.3 . . C82 C72 H72 106.3 . . C72 C82 H82A 109.5 . . C72 C82 H82B 109.5 . . H82A C82 H82B 109.5 . . C72 C82 H82C 109.5 . . H82A C82 H82C 109.5 . . H82B C82 H82C 109.5 . . C72 C92 H92A 109.5 . . C72 C92 H92B 109.5 . . H92A C92 H92B 109.5 . . C72 C92 H92C 109.5 . . H92A C92 H92C 109.5 . . H92B C92 H92C 109.5 . . C112 C102 C122 107.9(7) . . C112 C102 C62 111.7(5) . . C122 C102 C62 113.0(7) . . C112 C102 H102 108.0 . . C122 C102 H102 108.0 . . C62 C102 H102 108.0 . . C102 C112 H11D 109.5 . . C102 C112 H11E 109.5 . . H11D C112 H11E 109.5 . . C102 C112 H11F 109.5 . . H11D C112 H11F 109.5 . . H11E C112 H11F 109.5 . . C102 C122 H12A 109.5 . . C102 C122 H12B 109.5 . . H12A C122 H12B 109.5 . . C102 C122 H12C 109.5 . . H12A C122 H12C 109.5 . . H12B C122 H12C 109.5 . . C63 C13 C23 119.6(4) . . C63 C13 N21 119.4(4) . . C23 C13 N21 120.8(4) . . C33 C23 C13 118.8(5) . . C33 C23 C73 118.7(5) . . C13 C23 C73 122.6(5) . . C43 C33 C23 121.6(5) . . C43 C33 H33 119.2 . . C23 C33 H33 119.2 . . C33 C43 C53 119.8(5) . . C33 C43 H43 120.1 . . C53 C43 H43 120.1 . . C63 C53 C43 120.3(5) . . C63 C53 H53 119.8 . . C43 C53 H53 119.8 . . C53 C63 C13 119.7(4) . . C53 C63 C103 119.7(4) . . C13 C63 C103 120.5(4) . . C93 C73 C23 111.1(5) . . C93 C73 C83 109.2(5) . . C23 C73 C83 110.9(5) . . C93 C73 H73 108.5 . . C23 C73 H73 108.5 . . C83 C73 H73 108.5 . . C73 C83 H83A 109.5 . . C73 C83 H83B 109.5 . . H83A C83 H83B 109.5 . . C73 C83 H83C 109.5 . . H83A C83 H83C 109.5 . . H83B C83 H83C 109.5 . . C73 C93 H93A 109.5 . . C73 C93 H93B 109.5 . . H93A C93 H93B 109.5 . . C73 C93 H93C 109.5 . . H93A C93 H93C 109.5 . . H93B C93 H93C 109.5 . . C113 C103 C63 112.6(4) . . C113 C103 C123 109.5(4) . . C63 C103 C123 113.8(4) . . C113 C103 H103 106.9 . . C63 C103 H103 106.9 . . C123 C103 H103 106.9 . . C103 C113 K1 150.4(3) . 4_676 C103 C113 H11G 109.5 . . K1 C113 H11G 86.5 4_676 . C103 C113 H11H 109.5 . . K1 C113 H11H 41.0 4_676 . H11G C113 H11H 109.5 . . C103 C113 H11I 109.5 . . K1 C113 H11I 86.9 4_676 . H11G C113 H11I 109.5 . . H11H C113 H11I 109.5 . . C103 C123 H12D 109.5 . . C103 C123 H12E 109.5 . . H12D C123 H12E 109.5 . . C103 C123 H12F 109.5 . . H12D C123 H12F 109.5 . . H12E C123 H12F 109.5 . . C24 C14 C64 118.8(6) . . C24 C14 Fe1 65.6(3) . . C64 C14 Fe1 89.2(4) . . C24 C14 K1 65.8(3) . . C64 C14 K1 76.8(3) . . Fe1 C14 K1 112.8(2) . . C24 C14 H14 124(4) . . C64 C14 H14 115(4) . . Fe1 C14 H14 130(4) . . K1 C14 H14 115(4) . . C34 C24 C14 119.7(6) . . C34 C24 Fe1 70.8(4) . . C14 C24 Fe1 75.4(3) . . C34 C24 K1 77.3(3) . . C14 C24 K1 89.1(3) . . Fe1 C24 K1 130.2(3) . . C34 C24 H24 119(5) . . C14 C24 H24 121(5) . . Fe1 C24 H24 123(5) . . K1 C24 H24 106(5) . . C44 C34 C24 119.0(6) . . C44 C34 Fe1 76.0(4) . . C24 C34 Fe1 69.5(3) . . C44 C34 K1 89.3(4) . . C24 C34 K1 76.3(4) . . Fe1 C34 K1 128.7(3) . . C44 C34 H34 119(4) . . C24 C34 H34 122(4) . . Fe1 C34 H34 125(4) . . K1 C34 H34 105(4) . . C34 C44 C54 119.5(7) . . C34 C44 Fe1 66.0(3) . . C54 C44 Fe1 88.3(4) . . C34 C44 K1 66.1(4) . . C54 C44 K1 76.6(4) . . Fe1 C44 K1 112.1(3) . . C34 C44 H44 133(4) . . C54 C44 H44 106(4) . . Fe1 C44 H44 131(4) . . K1 C44 H44 117(4) . . C64 C54 C44 119.8(6) . . C64 C54 K1 77.9(4) . . C44 C54 K1 78.7(4) . . C64 C54 H54 115(4) . . C44 C54 H54 125(4) . . K1 C54 H54 117(4) . . C54 C64 C14 118.8(6) . . C54 C64 K1 78.1(4) . . C14 C64 K1 78.5(3) . . C54 C64 H64 125(3) . . C14 C64 H64 116(3) . . K1 C64 H64 115(3) . . O70 K1 O10 118.37(16) . . O70 K1 O130 116.18(15) . . O10 K1 O130 114.99(17) . . O70 K1 O40 60.14(16) . . O10 K1 O40 58.32(16) . . O130 K1 O40 150.43(14) . . O70 K1 O100 58.23(15) . . O10 K1 O100 151.78(15) . . O130 K1 O100 58.09(13) . . O40 K1 O100 112.50(14) . . O70 K1 O160 149.63(14) . . O10 K1 O160 57.36(17) . . O130 K1 O160 57.64(14) . . O40 K1 O160 109.13(15) . . O100 K1 O160 109.80(14) . . O70 K1 C24 106.82(18) . . O10 K1 C24 71.79(17) . . O130 K1 C24 121.26(14) . . O40 K1 C24 85.56(15) . . O100 K1 C24 136.27(16) . . O160 K1 C24 100.02(17) . . O70 K1 C34 82.26(17) . . O10 K1 C34 91.78(19) . . O130 K1 C34 128.24(15) . . O40 K1 C34 81.28(16) . . O100 K1 C34 114.09(17) . . O160 K1 C34 126.13(16) . . C24 K1 C34 26.41(18) . . O70 K1 C64 120.32(16) . . O10 K1 C64 101.38(16) . . O130 K1 C64 78.47(15) . . O40 K1 C64 130.12(16) . . O100 K1 C64 103.40(15) . . O160 K1 C64 88.79(16) . . C24 K1 C64 44.92(16) . . C34 K1 C64 52.25(17) . . O70 K1 C54 96.81(17) . . O10 K1 C54 120.44(16) . . O130 K1 C54 84.06(16) . . O40 K1 C54 124.96(18) . . O100 K1 C54 87.15(15) . . O160 K1 C54 111.04(17) . . C24 K1 C54 51.83(16) . . C34 K1 C54 44.61(18) . . C64 K1 C54 23.97(17) . . O70 K1 C14 125.91(16) . . O10 K1 C14 78.46(15) . . O130 K1 C14 96.32(13) . . O40 K1 C14 109.09(15) . . O100 K1 C14 127.75(14) . . O160 K1 C14 84.06(15) . . C24 K1 C14 25.09(15) . . C34 K1 C14 44.38(16) . . C64 K1 C14 24.67(15) . . C54 K1 C14 42.44(16) . . O70 K1 C44 79.40(15) . . O10 K1 C44 114.80(17) . . O130 K1 C44 107.35(15) . . O40 K1 C44 100.80(16) . . O100 K1 C44 92.69(14) . . O160 K1 C44 130.78(14) . . C24 K1 C44 43.82(17) . . C34 K1 C44 24.59(17) . . C64 K1 C44 42.67(17) . . C54 K1 C44 24.66(17) . . C14 K1 C44 48.97(16) . . C180 O10 C20 113.4(7) . . C180 O10 K1 119.8(5) . . C20 O10 K1 119.2(5) . . O10 C20 C30 110.0(7) . . O10 C20 H20A 109.7 . . C30 C20 H20A 109.7 . . O10 C20 H20B 109.7 . . C30 C20 H20B 109.7 . . H20A C20 H20B 108.2 . . O40 C30 C20 112.0(9) . . O40 C30 H30A 109.2 . . C20 C30 H30A 109.2 . . O40 C30 H30B 109.2 . . C20 C30 H30B 109.2 . . H30A C30 H30B 107.9 . . C30 O40 C50 113.7(8) . . C30 O40 K1 107.6(5) . . C50 O40 K1 107.1(5) . . O40 C50 C60 110.9(7) . . O40 C50 H50A 109.5 . . C60 C50 H50A 109.5 . . O40 C50 H50B 109.5 . . C60 C50 H50B 109.5 . . H50A C50 H50B 108.0 . . O70 C60 C50 108.3(6) . . O70 C60 H60A 110.0 . . C50 C60 H60A 110.0 . . O70 C60 H60B 110.0 . . C50 C60 H60B 110.0 . . H60A C60 H60B 108.4 . . C80 O70 C60 117.1(6) . . C80 O70 K1 117.7(5) . . C60 O70 K1 117.1(4) . . O70 C80 C90 116.1(8) . . O70 C80 H80A 108.3 . . C90 C80 H80A 108.3 . . O70 C80 H80B 108.3 . . C90 C80 H80B 108.3 . . H80A C80 H80B 107.4 . . O100 C90 C80 105.7(5) . . O100 C90 H90A 110.6 . . C80 C90 H90A 110.6 . . O100 C90 H90B 110.6 . . C80 C90 H90B 110.6 . . H90A C90 H90B 108.7 . . C110 O100 C90 113.6(5) . . C110 O100 K1 105.5(4) . . C90 O100 K1 107.6(4) . . O100 C110 C120 113.2(5) . . O100 C110 K1 52.9(4) . . C120 C110 K1 87.2(4) . . O100 C110 H11J 108.9 . . C120 C110 H11J 108.9 . . K1 C110 H11J 75.9 . . O100 C110 H11K 108.9 . . C120 C110 H11K 108.9 . . K1 C110 H11K 160.4 . . H11J C110 H11K 107.7 . . C110 C120 O130 108.0(6) . . C110 C120 H12G 110.1 . . O130 C120 H12G 110.1 . . C110 C120 H12H 110.1 . . O130 C120 H12H 110.1 . . H12G C120 H12H 108.4 . . C140 O130 C120 117.4(6) . . C140 O130 K1 116.6(6) . . C120 O130 K1 116.7(4) . . O130 C140 C150 112.9(9) . . O130 C140 H14A 109.0 . . C150 C140 H14A 109.0 . . O130 C140 H14B 109.0 . . C150 C140 H14B 109.0 . . H14A C140 H14B 107.8 . . O160 C150 C140 109.1(6) . . O160 C150 H15A 109.9 . . C140 C150 H15A 109.9 . . O160 C150 H15B 109.9 . . C140 C150 H15B 109.9 . . H15A C150 H15B 108.3 . . C170 O160 C150 111.4(5) . . C170 O160 K1 108.5(5) . . C150 O160 K1 105.4(4) . . O160 C170 C180 108.4(6) . . O160 C170 H17A 110.0 . . C180 C170 H17A 110.0 . . O160 C170 H17B 110.0 . . C180 C170 H17B 110.0 . . H17A C170 H17B 108.4 . . O10 C180 C170 109.7(6) . . O10 C180 H18A 109.7 . . C170 C180 H18A 109.7 . . O10 C180 H18B 109.7 . . C170 C180 H18B 109.7 . . H18A C180 H18B 108.2 . . C220 O190 C210 126.1(11) . . C210 C200 H20C 109.5 . . C210 C200 H20D 109.5 . . H20C C200 H20D 109.5 . . C210 C200 H20E 109.5 . . H20C C200 H20E 109.5 . . H20D C200 H20E 109.5 . . O190 C210 C200 123.0(15) . . O190 C210 H21A 106.6 . . C200 C210 H21A 106.6 . . O190 C210 H21B 106.6 . . C200 C210 H21B 106.6 . . H21A C210 H21B 106.5 . . O190 C220 C230 121.8(10) . . O190 C220 H22A 106.9 . . C230 C220 H22A 106.9 . . O190 C220 H22B 106.9 . . C230 C220 H22B 106.9 . . H22A C220 H22B 106.7 . . C220 C230 H23A 109.5 . . C220 C230 H23B 109.5 . . H23A C230 H23B 109.5 . . C220 C230 H23C 109.5 . . H23A C230 H23C 109.5 . . H23B C230 H23C 109.5 . . C270 O240 C250 114.9(6) . . O240 C250 C260 110.1(6) . . O240 C250 H25A 109.6 . . C260 C250 H25A 109.6 . . O240 C250 H25B 109.6 . . C260 C250 H25B 109.6 . . H25A C250 H25B 108.2 . . C250 C260 H26A 109.5 . . C250 C260 H26B 109.5 . . H26A C260 H26B 109.5 . . C250 C260 H26C 109.5 . . H26A C260 H26C 109.5 . . H26B C260 H26C 109.5 . . O240 C270 C280 108.8(8) . . O240 C270 H27A 109.9 . . C280 C270 H27A 109.9 . . O240 C270 H27B 109.9 . . C280 C270 H27B 109.9 . . H27A C270 H27B 108.3 . . C270 C280 H28A 109.5 . . C270 C280 H28B 109.5 . . H28A C280 H28B 109.5 . . C270 C280 H28C 109.5 . . H28A C280 H28C 109.5 . . H28B C280 H28C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Fe1 N21 1.982(4) . Fe1 N11 2.051(4) . Fe1 C24 2.053(6) . Fe1 C34 2.070(6) . Fe1 C14 2.182(6) . Fe1 C44 2.199(6) . N11 C21 1.323(7) . N11 C12 1.434(7) . N21 C41 1.351(6) . N21 C13 1.423(6) . C11 C21 1.519(8) . C11 H11A 0.9800 . C11 H11B 0.9800 . C11 H11C 0.9800 . C21 C31 1.399(8) . C31 C41 1.387(7) . C31 H31 0.9500 . C41 C51 1.497(7) . C51 H51A 0.9800 . C51 H51B 0.9800 . C51 H51C 0.9800 . C12 C62 1.402(8) . C12 C22 1.414(7) . C22 C32 1.403(9) . C22 C72 1.505(10) . C32 C42 1.352(10) . C32 H32 0.9500 . C42 C52 1.402(9) . C42 H42 0.9500 . C52 C62 1.390(8) . C52 H52 0.9500 . C62 C102 1.531(8) . C72 C92 1.532(10) . C72 C82 1.541(12) . C72 H72 1.0000 . C82 H82A 0.9800 . C82 H82B 0.9800 . C82 H82C 0.9800 . C92 H92A 0.9800 . C92 H92B 0.9800 . C92 H92C 0.9800 . C102 C112 1.497(9) . C102 C122 1.510(13) . C102 H102 1.0000 . C112 H11D 0.9800 . C112 H11E 0.9800 . C112 H11F 0.9800 . C122 H12A 0.9800 . C122 H12B 0.9800 . C122 H12C 0.9800 . C13 C63 1.402(6) . C13 C23 1.407(7) . C23 C33 1.389(8) . C23 C73 1.520(7) . C33 C43 1.362(9) . C33 H33 0.9500 . C43 C53 1.395(9) . C43 H43 0.9500 . C53 C63 1.380(7) . C53 H53 0.9500 . C63 C103 1.521(6) . C73 C93 1.518(8) . C73 C83 1.546(9) . C73 H73 1.0000 . C83 H83A 0.9800 . C83 H83B 0.9800 . C83 H83C 0.9800 . C93 H93A 0.9800 . C93 H93B 0.9800 . C93 H93C 0.9800 . C103 C113 1.512(7) . C103 C123 1.523(7) . C103 H103 1.0000 . C113 K1 3.452(6) 4_676 C113 H11G 0.9800 . C113 H11H 0.9800 . C113 H11I 0.9800 . C123 H12D 0.9800 . C123 H12E 0.9800 . C123 H12F 0.9800 . C14 C24 1.422(8) . C14 C64 1.428(9) . C14 K1 3.352(6) . C14 H14 0.96(2) . C24 C34 1.400(10) . C24 K1 3.058(6) . C24 H24 0.95(2) . C34 C44 1.398(10) . C34 K1 3.071(7) . C34 H34 0.96(2) . C44 C54 1.429(10) . C44 K1 3.359(8) . C44 H44 0.96(2) . C54 C64 1.383(10) . C54 K1 3.332(7) . C54 H54 0.97(2) . C64 K1 3.330(6) . C64 H64 0.96(2) . K1 O70 2.837(5) . K1 O10 2.871(5) . K1 O130 2.879(5) . K1 O40 2.884(5) . K1 O100 2.923(5) . K1 O160 2.971(5) . O10 C180 1.362(10) . O10 C20 1.362(9) . C20 C30 1.493(14) . C20 H20A 0.9900 . C20 H20B 0.9900 . C30 O40 1.381(9) . C30 H30A 0.9900 . C30 H30B 0.9900 . O40 C50 1.423(9) . C50 C60 1.483(12) . C50 H50A 0.9900 . C50 H50B 0.9900 . C60 O70 1.441(8) . C60 H60A 0.9900 . C60 H60B 0.9900 . O70 C80 1.309(10) . C80 C90 1.471(10) . C80 H80A 0.9900 . C80 H80B 0.9900 . C90 O100 1.444(8) . C90 H90A 0.9900 . C90 H90B 0.9900 . O100 C110 1.348(8) . C110 C120 1.424(9) . C110 H11J 0.9900 . C110 H11K 0.9900 . C120 O130 1.426(7) . C120 H12G 0.9900 . C120 H12H 0.9900 . O130 C140 1.319(9) . C140 C150 1.444(11) . C140 H14A 0.9900 . C140 H14B 0.9900 . C150 O160 1.387(8) . C150 H15A 0.9900 . C150 H15B 0.9900 . O160 C170 1.353(9) . C170 C180 1.545(12) . C170 H17A 0.9900 . C170 H17B 0.9900 . C180 H18A 0.9900 . C180 H18B 0.9900 . O190 C220 1.292(12) . O190 C210 1.323(13) . C200 C210 1.40(2) . C200 H20C 0.9800 . C200 H20D 0.9800 . C200 H20E 0.9800 . C210 H21A 0.9900 . C210 H21B 0.9900 . C220 C230 1.411(14) . C220 H22A 0.9900 . C220 H22B 0.9900 . C230 H23A 0.9800 . C230 H23B 0.9800 . C230 H23C 0.9800 . O240 C270 1.405(9) . O240 C250 1.409(8) . C250 C260 1.454(11) . C250 H25A 0.9900 . C250 H25B 0.9900 . C260 H26A 0.9800 . C260 H26B 0.9800 . C260 H26C 0.9800 . C270 C280 1.489(15) . C270 H27A 0.9900 . C270 H27B 0.9900 . C280 H28A 0.9800 . C280 H28B 0.9800 . C280 H28C 0.9800 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_4 C12 N11 C21 C31 -175.9(5) . Fe1 N11 C21 C31 2.2(7) . C12 N11 C21 C11 6.9(8) . Fe1 N11 C21 C11 -175.0(5) . N11 C21 C31 C41 -2.4(9) . C11 C21 C31 C41 174.9(6) . C13 N21 C41 C31 -177.6(4) . Fe1 N21 C41 C31 4.3(6) . C13 N21 C41 C51 3.4(6) . Fe1 N21 C41 C51 -174.8(3) . C21 C31 C41 N21 -1.1(8) . C21 C31 C41 C51 178.0(5) . C21 N11 C12 C62 -90.9(7) . Fe1 N11 C12 C62 90.9(6) . C21 N11 C12 C22 94.4(6) . Fe1 N11 C12 C22 -83.8(5) . C62 C12 C22 C32 -0.6(9) . N11 C12 C22 C32 174.3(5) . C62 C12 C22 C72 178.0(6) . N11 C12 C22 C72 -7.1(8) . C12 C22 C32 C42 -0.6(10) . C72 C22 C32 C42 -179.3(7) . C22 C32 C42 C52 0.6(11) . C32 C42 C52 C62 0.6(11) . C42 C52 C62 C12 -1.8(10) . C42 C52 C62 C102 176.2(7) . C22 C12 C62 C52 1.8(9) . N11 C12 C62 C52 -172.9(5) . C22 C12 C62 C102 -176.1(6) . N11 C12 C62 C102 9.2(9) . C32 C22 C72 C92 -33.5(10) . C12 C22 C72 C92 147.9(8) . C32 C22 C72 C82 93.6(8) . C12 C22 C72 C82 -85.0(8) . C52 C62 C102 C112 -57.4(9) . C12 C62 C102 C112 120.6(7) . C52 C62 C102 C122 64.5(9) . C12 C62 C102 C122 -117.5(8) . C41 N21 C13 C63 99.3(5) . Fe1 N21 C13 C63 -82.4(4) . C41 N21 C13 C23 -85.3(5) . Fe1 N21 C13 C23 93.0(5) . C63 C13 C23 C33 3.6(8) . N21 C13 C23 C33 -171.8(5) . C63 C13 C23 C73 -175.9(5) . N21 C13 C23 C73 8.7(8) . C13 C23 C33 C43 -0.8(10) . C73 C23 C33 C43 178.8(6) . C23 C33 C43 C53 -1.9(11) . C33 C43 C53 C63 1.7(10) . C43 C53 C63 C13 1.1(8) . C43 C53 C63 C103 -177.9(5) . C23 C13 C63 C53 -3.8(7) . N21 C13 C63 C53 171.6(5) . C23 C13 C63 C103 175.2(4) . N21 C13 C63 C103 -9.3(7) . C33 C23 C73 C93 58.9(8) . C13 C23 C73 C93 -121.6(6) . C33 C23 C73 C83 -62.7(7) . C13 C23 C73 C83 116.7(6) . C53 C63 C103 C113 90.7(6) . C13 C63 C103 C113 -88.3(6) . C53 C63 C103 C123 -34.6(7) . C13 C63 C103 C123 146.4(5) . C63 C103 C113 K1 177.4(6) 4_676 C123 C103 C113 K1 -55.0(9) 4_676 C64 C14 C24 C34 -17.1(8) . Fe1 C14 C24 C34 57.3(5) . K1 C14 C24 C34 -74.9(5) . C64 C14 C24 Fe1 -74.4(5) . K1 C14 C24 Fe1 -132.2(2) . C64 C14 C24 K1 57.7(5) . Fe1 C14 C24 K1 132.2(2) . C14 C24 C34 C44 0.2(9) . Fe1 C24 C34 C44 59.8(5) . K1 C24 C34 C44 -81.4(5) . C14 C24 C34 Fe1 -59.6(5) . K1 C24 C34 Fe1 -141.2(2) . C14 C24 C34 K1 81.6(5) . Fe1 C24 C34 K1 141.2(2) . C24 C34 C44 C54 16.6(9) . Fe1 C34 C44 C54 73.2(5) . K1 C34 C44 C54 -57.2(5) . C24 C34 C44 Fe1 -56.5(5) . K1 C34 C44 Fe1 -130.4(3) . C24 C34 C44 K1 73.8(5) . Fe1 C34 C44 K1 130.4(3) . C34 C44 C54 C64 -16.7(9) . Fe1 C44 C54 C64 44.3(7) . K1 C44 C54 C64 -68.9(6) . C34 C44 C54 K1 52.2(5) . Fe1 C44 C54 K1 113.2(2) . C44 C54 C64 C14 -0.4(9) . K1 C54 C64 C14 -69.7(5) . C44 C54 C64 K1 69.3(6) . C24 C14 C64 C54 17.0(9) . Fe1 C14 C64 C54 -44.3(6) . K1 C14 C64 C54 69.4(5) . C24 C14 C64 K1 -52.4(5) . Fe1 C14 C64 K1 -113.7(2) . C180 O10 C20 C30 -175.7(7) . K1 O10 C20 C30 -26.1(9) . O10 C20 C30 O40 61.8(9) . C20 C30 O40 C50 178.8(7) . C20 C30 O40 K1 -62.8(7) . C30 O40 C50 C60 -178.7(7) . K1 O40 C50 C60 62.6(7) . O40 C50 C60 O70 -67.5(10) . C50 C60 O70 C80 -177.0(7) . C50 C60 O70 K1 34.9(8) . C60 O70 C80 C90 179.8(7) . K1 O70 C80 C90 -32.3(9) . O70 C80 C90 O100 64.7(9) . C80 C90 O100 C110 -176.2(7) . C80 C90 O100 K1 -59.7(7) . C90 O100 C110 C120 -175.4(6) . K1 O100 C110 C120 67.0(7) . C90 O100 C110 K1 117.6(6) . O100 C110 C120 O130 -69.5(8) . K1 C110 C120 O130 -22.2(4) . C110 C120 O130 C140 176.9(6) . C110 C120 O130 K1 31.2(6) . C120 O130 C140 C150 177.8(6) . K1 O130 C140 C150 -36.5(8) . O130 C140 C150 O160 70.9(9) . C140 C150 O160 C170 -179.8(7) . C140 C150 O160 K1 -62.2(7) . C150 O160 C170 C180 177.8(7) . K1 O160 C170 C180 62.2(7) . C20 O10 C180 C170 -177.4(7) . K1 O10 C180 C170 33.2(8) . O160 C170 C180 O10 -66.1(9) . C220 O190 C210 C200 -174.9(11) . C210 O190 C220 C230 178.7(10) . C270 O240 C250 C260 -179.1(7) . C250 O240 C270 C280 178.3(10) .