#------------------------------------------------------------------------------ #$Date: 2019-11-26 03:36:25 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242520 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/25/4132560.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132560 loop_ _publ_author_name 'Wu, Pengcheng' 'Yap, Glenn P. A.' 'Theopold, Klaus H.' _publ_section_title ; Structure and Reactivity of Chromium(VI) Alkylidenes. ; _journal_issue 23 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 7088 _journal_page_last 7091 _journal_paper_doi 10.1021/jacs.8b04882 _journal_volume 140 _journal_year 2018 _chemical_formula_sum 'C32 H56 Cr N2 Si2' _chemical_formula_weight 576.96 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 101.4220(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 11.0281(6) _cell_length_b 16.9697(10) _cell_length_c 19.3066(11) _cell_measurement_reflns_used 9980 _cell_measurement_temperature 200(2) _cell_measurement_theta_max 27.05 _cell_measurement_theta_min 2.23 _cell_volume 3541.5(3) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 200(2) _diffrn_detector_area_resol_mean 8.33 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker AXS APEX diffractometer' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0476 _diffrn_reflns_av_unetI/netI 0.0304 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -22 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 53227 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.609 _diffrn_reflns_theta_min 1.612 _exptl_absorpt_coefficient_mu 0.411 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6767 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'APEX2 (Bruker, 2007)' _exptl_crystal_colour green _exptl_crystal_density_diffrn 1.082 _exptl_crystal_description block _exptl_crystal_F_000 1256 _exptl_crystal_size_max 0.413 _exptl_crystal_size_mid 0.328 _exptl_crystal_size_min 0.300 _refine_diff_density_max 0.550 _refine_diff_density_min -0.411 _refine_diff_density_rms 0.065 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.014 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 348 _refine_ls_number_reflns 8225 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.014 _refine_ls_R_factor_all 0.0572 _refine_ls_R_factor_gt 0.0422 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0589P)^2^+2.2145P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1080 _refine_ls_wR_factor_ref 0.1206 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6661 _reflns_number_total 8225 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b04882_si_002.cif _cod_data_source_block kla0695 _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 4132560 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.728 _shelx_estimated_absorpt_t_max 0.790 _shelx_res_file ; kla0695.res created by SHELXL-2014/7 TITL kla0695_a.res in P2(1)/n CELL 0.71073 11.0281 16.9697 19.3066 90.000 101.422 90.000 ZERR 4.000 0.0006 0.0010 0.0011 0.000 0.001 0.000 LATT 1 SYMM 1/2-X, 1/2+Y, 1/2-Z SFAC C H N Si Cr UNIT 128 224 8 8 4 REM Old TITL kla0695 in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.133, Rweak 0.005, Alpha 0.048, Orientation as input REM Formula found by SHELXT: C31 N3 Si2 Cr L.S. 10 BOND $H FMAP 2 PLAN 20 SIZE 0.601 0.657 0.825 ACTA TEMP -73.150 WGHT 0.058900 2.214500 FVAR 0.36318 CR1 5 0.380352 0.287405 0.258833 11.00000 0.01904 0.02417 = 0.02550 0.00549 0.00422 -0.00060 SI1 4 0.146580 0.196979 0.156023 11.00000 0.02999 0.03914 = 0.03382 0.00556 -0.00111 -0.00852 SI2 4 0.246228 0.373013 0.377115 11.00000 0.03135 0.04586 = 0.03321 -0.00328 0.01016 0.00218 N1 3 0.492752 0.263869 0.325512 11.00000 0.02251 0.02686 = 0.03115 0.00534 0.00401 -0.00195 N2 3 0.429044 0.313206 0.186457 11.00000 0.02454 0.02500 = 0.02997 0.00514 0.00697 -0.00002 C1 1 0.277482 0.189356 0.233659 11.00000 0.02602 0.02881 = 0.03117 0.00523 0.00450 -0.00382 AFIX 23 H1A 2 0.332929 0.146439 0.224354 11.00000 -1.20000 H1B 2 0.243281 0.173683 0.275319 11.00000 -1.20000 AFIX 0 C2 1 0.208671 0.199037 0.072824 11.00000 0.05625 0.09179 = 0.03253 0.00672 0.00299 -0.02070 AFIX 137 H2A 2 0.140159 0.205123 0.032264 11.00000 -1.50000 H2B 2 0.252454 0.149652 0.068216 11.00000 -1.50000 H2C 2 0.265992 0.243418 0.074321 11.00000 -1.50000 AFIX 0 C3 1 0.047298 0.107428 0.154562 11.00000 0.05304 0.06145 = 0.05413 0.00921 -0.00584 -0.02850 AFIX 137 H3A 2 0.011837 0.106289 0.197255 11.00000 -1.50000 H3B 2 0.097565 0.060094 0.152931 11.00000 -1.50000 H3C 2 -0.019540 0.108969 0.112733 11.00000 -1.50000 AFIX 0 C4 1 0.048713 0.285626 0.159763 11.00000 0.04713 0.06494 = 0.07831 0.00172 -0.01553 0.01219 AFIX 137 H4A 2 0.021725 0.286876 0.205156 11.00000 -1.50000 H4B 2 -0.023864 0.283496 0.121192 11.00000 -1.50000 H4C 2 0.096748 0.333185 0.154909 11.00000 -1.50000 AFIX 0 C5 1 0.300558 0.383152 0.291930 11.00000 0.03194 0.03020 = 0.03605 0.00182 0.00942 0.00253 AFIX 23 H5A 2 0.360557 0.427169 0.296707 11.00000 -1.20000 H5B 2 0.228826 0.398035 0.254742 11.00000 -1.20000 AFIX 0 C6 1 0.166142 0.277606 0.384363 11.00000 0.05802 0.05742 = 0.05304 0.00501 0.02975 -0.00455 AFIX 137 H6A 2 0.130669 0.277875 0.427063 11.00000 -1.50000 H6B 2 0.225672 0.234292 0.387075 11.00000 -1.50000 H6C 2 0.099950 0.270457 0.342764 11.00000 -1.50000 AFIX 0 C7 1 0.134776 0.454400 0.383306 11.00000 0.05464 0.06244 = 0.07648 -0.01057 0.02785 0.01379 AFIX 137 H7A 2 0.103063 0.448683 0.427005 11.00000 -1.50000 H7B 2 0.065825 0.451959 0.342619 11.00000 -1.50000 H7C 2 0.176981 0.505249 0.383540 11.00000 -1.50000 AFIX 0 C8 1 0.379608 0.381416 0.452748 11.00000 0.05355 0.11163 = 0.03990 -0.01206 -0.00042 0.00203 AFIX 137 H8A 2 0.417931 0.433430 0.451986 11.00000 -1.50000 H8B 2 0.440562 0.340456 0.448886 11.00000 -1.50000 H8C 2 0.350547 0.374785 0.497187 11.00000 -1.50000 AFIX 0 C9 1 0.611309 0.247355 0.361456 11.00000 0.02275 0.03027 = 0.02495 0.00115 0.00314 0.00211 C10 1 0.633556 0.172265 0.393399 11.00000 0.03125 0.02928 = 0.03094 0.00037 0.00497 0.00398 C11 1 0.752545 0.155594 0.429600 11.00000 0.03717 0.03519 = 0.04513 0.00430 0.00003 0.01257 AFIX 43 H11 2 0.769615 0.105415 0.451144 11.00000 -1.20000 AFIX 0 C12 1 0.846782 0.210371 0.435009 11.00000 0.02467 0.04826 = 0.04703 -0.00557 -0.00458 0.01133 AFIX 43 H12 2 0.927392 0.197763 0.460296 11.00000 -1.20000 AFIX 0 C13 1 0.823742 0.283179 0.403740 11.00000 0.02279 0.04350 = 0.04950 -0.00209 0.00184 -0.00022 AFIX 43 H13 2 0.889358 0.320192 0.407536 11.00000 -1.20000 AFIX 0 C14 1 0.707157 0.303780 0.366861 11.00000 0.02623 0.03609 = 0.04005 0.00475 0.00132 -0.00223 C15 1 0.529207 0.113211 0.389018 11.00000 0.03705 0.02885 = 0.04644 0.00781 0.00060 -0.00199 AFIX 13 H15 2 0.459556 0.131516 0.351087 11.00000 -1.20000 AFIX 0 C16 1 0.563459 0.031985 0.369836 11.00000 0.09094 0.04682 = 0.23223 -0.04694 0.06632 -0.02341 AFIX 137 H16A 2 0.590036 0.033477 0.324331 11.00000 -1.50000 H16B 2 0.491612 -0.002855 0.366246 11.00000 -1.50000 H16C 2 0.631182 0.012090 0.406359 11.00000 -1.50000 AFIX 0 C17 1 0.483224 0.113323 0.457791 11.00000 0.09308 0.14587 = 0.09318 -0.01713 0.04233 -0.06700 AFIX 137 H17A 2 0.547084 0.091294 0.495399 11.00000 -1.50000 H17B 2 0.408051 0.081262 0.452591 11.00000 -1.50000 H17C 2 0.464739 0.167485 0.469950 11.00000 -1.50000 AFIX 0 C18 1 0.685346 0.385407 0.334522 11.00000 0.02858 0.04732 = 0.08901 0.02914 -0.01181 -0.01289 AFIX 13 H18 2 0.596937 0.388580 0.309529 11.00000 -1.20000 AFIX 0 C19 1 0.706497 0.448733 0.393046 11.00000 0.06751 0.03562 = 0.14206 0.01096 0.02506 0.00274 AFIX 137 H19A 2 0.653689 0.437557 0.427145 11.00000 -1.50000 H19B 2 0.685785 0.500735 0.371919 11.00000 -1.50000 H19C 2 0.793449 0.448121 0.417238 11.00000 -1.50000 AFIX 0 C20 1 0.766021 0.401222 0.280690 11.00000 0.07890 0.08753 = 0.06814 0.03295 -0.00872 -0.03851 AFIX 137 H20A 2 0.853083 0.402679 0.304638 11.00000 -1.50000 H20B 2 0.743064 0.451973 0.257564 11.00000 -1.50000 H20C 2 0.753935 0.359210 0.245159 11.00000 -1.50000 AFIX 0 C21 1 0.511499 0.331729 0.143439 11.00000 0.02380 0.03124 = 0.02419 0.00376 0.00516 -0.00310 C22 1 0.584772 0.272601 0.120868 11.00000 0.02695 0.03440 = 0.03649 0.00497 0.01009 0.00178 C23 1 0.666330 0.294576 0.077725 11.00000 0.03374 0.04344 = 0.04468 0.00145 0.01802 0.00197 AFIX 43 H23 2 0.717664 0.255791 0.062725 11.00000 -1.20000 AFIX 0 C24 1 0.673876 0.371632 0.056403 11.00000 0.04551 0.05118 = 0.04636 0.00467 0.02647 -0.00896 AFIX 43 H24 2 0.729073 0.385214 0.026266 11.00000 -1.20000 AFIX 0 C25 1 0.601477 0.429373 0.078649 11.00000 0.05309 0.03681 = 0.04294 0.00781 0.02071 -0.00787 AFIX 43 H25 2 0.607467 0.482187 0.063355 11.00000 -1.20000 AFIX 0 C26 1 0.520381 0.411444 0.122863 11.00000 0.03394 0.03148 = 0.02857 0.00414 0.00716 -0.00357 C27 1 0.578102 0.187216 0.142907 11.00000 0.04905 0.03551 = 0.06794 0.01268 0.03637 0.01294 AFIX 13 H27 2 0.504312 0.181390 0.165376 11.00000 -1.20000 AFIX 0 C28 1 0.692687 0.165121 0.198039 11.00000 0.10939 0.05817 = 0.05414 0.01413 0.01450 0.03638 AFIX 137 H28A 2 0.765897 0.166806 0.176417 11.00000 -1.50000 H28B 2 0.682682 0.111822 0.215630 11.00000 -1.50000 H28C 2 0.702928 0.202572 0.237409 11.00000 -1.50000 AFIX 0 C29 1 0.561704 0.130957 0.079929 11.00000 0.06151 0.03759 = 0.08828 -0.00259 0.01729 -0.00289 AFIX 137 H29A 2 0.489401 0.146952 0.044546 11.00000 -1.50000 H29B 2 0.549517 0.077230 0.095869 11.00000 -1.50000 H29C 2 0.635677 0.132612 0.058988 11.00000 -1.50000 AFIX 0 C30 1 0.442999 0.473745 0.150134 11.00000 0.05001 0.02856 = 0.03517 0.00631 0.01399 0.00015 AFIX 13 H30 2 0.443473 0.461128 0.200781 11.00000 -1.20000 AFIX 0 C31 1 0.493906 0.557648 0.147841 11.00000 0.08092 0.03217 = 0.06155 0.00268 0.02636 -0.00347 AFIX 137 H31A 2 0.581023 0.558686 0.171715 11.00000 -1.50000 H31B 2 0.446338 0.593747 0.171794 11.00000 -1.50000 H31C 2 0.486871 0.574100 0.098548 11.00000 -1.50000 AFIX 0 C32 1 0.309479 0.470653 0.111035 11.00000 0.05227 0.04691 = 0.05868 0.01028 0.01185 0.01257 AFIX 137 H32A 2 0.305234 0.484028 0.061232 11.00000 -1.50000 H32B 2 0.260274 0.508496 0.132137 11.00000 -1.50000 H32C 2 0.276660 0.417438 0.114472 11.00000 -1.50000 AFIX 0 HKLF 4 REM kla0695_a.res in P2(1)/n REM R1 = 0.0422 for 6661 Fo > 4sig(Fo) and 0.0572 for all 8225 data REM 348 parameters refined using 0 restraints END WGHT 0.0528 2.2404 REM Highest difference peak 0.550, deepest hole -0.411, 1-sigma level 0.065 Q1 1 0.5326 0.0631 0.4504 11.00000 0.05 0.55 Q2 1 0.5348 0.0611 0.3229 11.00000 0.05 0.47 Q3 1 0.5788 0.0384 0.3884 11.00000 0.05 0.38 Q4 1 0.4701 0.2986 0.2953 11.00000 0.05 0.30 Q5 1 0.2208 0.1955 0.1973 11.00000 0.05 0.28 Q6 1 0.6333 0.0206 0.3466 11.00000 0.05 0.27 Q7 1 0.2806 0.3809 0.3317 11.00000 0.05 0.26 Q8 1 0.3220 0.3739 0.4176 11.00000 0.05 0.26 Q9 1 0.5139 0.3760 0.1360 11.00000 0.05 0.24 Q10 1 0.5836 0.1410 0.3907 11.00000 0.05 0.24 Q11 1 0.0115 0.2632 0.1946 11.00000 0.05 0.24 Q12 1 0.6776 0.3773 0.0353 11.00000 0.05 0.23 Q13 1 0.4615 0.3876 0.4453 11.00000 0.05 0.22 Q14 1 0.6225 0.1877 0.1874 11.00000 0.05 0.22 Q15 1 0.4951 0.4402 0.1424 11.00000 0.05 0.22 Q16 1 0.5679 0.4224 0.1026 11.00000 0.05 0.22 Q17 1 0.6250 0.3976 0.0614 11.00000 0.05 0.21 Q18 1 0.6319 0.3766 0.2983 11.00000 0.05 0.21 Q19 1 0.2188 0.3199 0.3857 11.00000 0.05 0.21 Q20 1 0.7088 0.4166 0.2922 11.00000 0.05 0.21 ; _shelx_res_checksum 10988 _shelx_hkl_file ; -1 0 0 0.00 0.10 -1 0 0 -0.10 0.20 -1 0 0 0.20 0.30 -1 0 0 0.50 0.20 1 0 0 0.30 0.20 1 0 0 0.10 0.20 1 0 0 0.20 0.20 1 0 0 1.00 0.30 -2 0 0 186.18 6.80 2 0 0 175.58 7.00 2 0 0 184.48 7.00 2 0 0 189.78 6.80 -2 0 0 178.98 7.10 -2 0 0 178.38 7.00 3 0 0 -0.70 0.50 3 0 0 0.50 0.50 -3 0 0 -0.20 0.40 3 0 0 0.20 0.40 -3 0 0 -0.90 0.90 -3 0 0 0.80 0.40 -4 0 0 46.70 2.20 4 0 0 41.00 2.00 -4 0 0 40.90 2.80 4 0 0 39.00 2.30 -4 0 0 35.10 2.30 4 0 0 40.60 2.40 5 0 0 -0.30 1.00 5 0 0 0.30 0.50 -5 0 0 0.50 1.00 5 0 0 0.50 0.90 -5 0 0 0.00 0.90 6 0 0 2.80 1.20 -6 0 0 2.60 1.20 6 0 0 4.50 0.90 6 0 0 4.40 1.40 -6 0 0 1.60 1.70 7 0 0 2.20 1.40 7 0 0 -2.00 1.20 -7 0 0 0.30 1.30 7 0 0 -1.00 0.70 -7 0 0 0.70 1.30 8 0 0 399.96 16.50 -8 0 0 395.56 17.30 -8 0 0 424.46 16.70 8 0 0 426.36 15.50 8 0 0 399.36 16.80 9 0 0 0.10 1.90 9 0 0 1.30 2.00 -9 0 0 0.00 1.80 -9 0 0 7.00 2.80 10 0 0 8.90 2.30 -10 0 0 13.60 3.10 10 0 0 14.40 2.90 11 0 0 -3.10 1.80 -11 0 0 -0.30 2.00 11 0 0 -0.70 1.60 12 0 0 11.50 2.80 -12 0 0 8.00 3.60 12 0 0 7.90 2.80 -13 0 0 10.70 4.10 13 0 0 3.40 2.80 -14 0 0 -0.80 2.70 14 0 0 -0.80 3.10 1 -1 0 1006.20 35.40 -1 -1 0 1028.30 35.50 1 -1 0 987.40 35.50 -1 -1 0 1024.80 35.60 -1 -1 0 1009.80 35.60 -1 -1 0 1021.80 35.60 1 1 0 996.80 35.50 -1 1 0 815.82 35.50 -1 1 0 998.80 35.60 -1 1 0 966.80 35.50 1 1 0 1021.40 35.60 2 -1 0 1143.89 40.50 -2 -1 0 920.81 40.20 2 -1 0 1149.08 40.30 2 -1 0 1135.39 40.40 -2 -1 0 1184.38 40.60 -2 -1 0 1161.68 40.60 -2 1 0 1159.58 40.40 2 1 0 945.21 40.10 2 1 0 1160.98 40.40 -2 1 0 1214.98 40.30 -2 1 0 1153.58 40.60 3 -1 0 439.96 16.00 3 -1 0 367.36 16.10 -3 -1 0 440.86 15.60 -3 -1 0 430.16 16.20 -3 -1 0 429.26 16.30 3 -1 0 432.16 15.90 -3 1 0 446.06 16.40 -3 1 0 436.36 16.00 3 1 0 444.16 15.60 3 1 0 442.76 16.10 4 -1 0 41.70 2.20 -4 -1 0 43.70 1.90 -4 -1 0 36.00 2.50 4 -1 0 41.10 2.60 -4 -1 0 44.90 2.80 4 -1 0 42.50 2.30 -4 1 0 40.90 2.40 4 1 0 43.30 1.90 4 1 0 38.90 2.30 4 1 0 40.50 2.50 -4 1 0 46.80 2.90 -5 -1 0 92.79 4.50 -5 -1 0 79.29 4.80 5 -1 0 90.69 4.60 -5 -1 0 92.09 3.70 5 -1 0 93.79 4.30 5 -1 0 94.49 4.10 5 1 0 92.99 4.60 -5 1 0 87.49 5.00 5 1 0 90.29 4.50 -5 1 0 97.09 4.40 5 1 0 93.79 3.80 6 -1 0 346.27 12.70 6 -1 0 341.17 13.10 6 -1 0 325.87 13.40 -6 -1 0 322.67 13.40 -6 -1 0 316.47 13.70 6 1 0 332.17 13.30 -6 1 0 328.17 13.10 6 1 0 319.17 13.30 -6 1 0 325.17 13.80 6 1 0 345.27 12.40 7 -1 0 1.70 1.30 -7 -1 0 -0.10 1.80 7 -1 0 3.90 1.10 7 -1 0 4.00 1.70 -7 -1 0 1.40 1.40 -7 1 0 2.90 1.40 -7 1 0 1.60 1.50 7 1 0 1.70 1.20 7 1 0 2.20 0.70 7 1 0 2.70 1.50 -8 -1 0 107.59 6.30 8 -1 0 109.49 5.90 -8 -1 0 105.69 5.80 8 -1 0 103.79 4.90 8 -1 0 110.89 5.70 8 1 0 102.19 5.90 -8 1 0 94.09 6.10 8 1 0 108.39 5.70 -8 1 0 110.29 5.70 8 1 0 110.49 4.50 9 -1 0 5.30 2.30 -9 -1 0 4.10 2.10 9 -1 0 2.20 1.80 -9 -1 0 5.00 2.30 9 1 0 5.70 2.20 9 1 0 4.10 2.10 -9 1 0 3.70 2.20 10 -1 0 64.89 4.70 10 -1 0 61.59 4.70 -10 -1 0 69.49 6.30 -10 -1 0 68.39 5.20 -10 1 0 75.49 6.60 10 1 0 64.79 5.10 10 1 0 71.29 5.10 11 -1 0 15.50 2.90 -11 -1 0 12.10 3.20 11 -1 0 14.20 3.20 -11 1 0 16.20 4.00 11 1 0 14.60 3.10 11 1 0 14.60 3.10 -12 -1 0 20.00 4.50 12 -1 0 18.40 3.80 -12 1 0 19.50 4.60 12 1 0 9.40 3.10 12 1 0 16.60 3.50 13 -1 0 11.40 3.50 -13 -1 0 15.10 4.50 -13 1 0 8.30 4.30 13 1 0 7.30 3.20 14 -1 0 32.20 5.20 -14 -1 0 37.30 5.70 -14 1 0 43.70 6.60 14 1 0 40.40 5.40 0 -2 0 5754.32 202.78 0 -2 0 5513.95 202.88 0 -2 0 5225.18 202.88 0 2 0 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289.57 11.30 2 -4 0 292.07 10.50 -2 -4 0 280.07 10.80 2 -4 0 282.07 11.20 -2 4 0 286.97 11.20 2 4 0 299.47 11.00 -2 4 0 293.67 10.50 2 4 0 284.17 10.80 3 -4 0 854.31 30.00 3 -4 0 793.02 29.90 -3 -4 0 821.02 30.90 3 -4 0 814.82 30.70 3 -4 0 816.92 30.70 -3 -4 0 824.52 30.70 3 4 0 839.22 30.10 -3 4 0 870.11 30.00 -3 4 0 845.82 30.90 -4 -4 0 2215.58 79.49 -4 -4 0 2177.08 80.29 -4 -4 0 2241.18 80.19 4 -4 0 2179.88 79.99 4 -4 0 2287.37 79.39 4 4 0 2184.08 79.89 4 4 0 2246.18 79.29 -4 4 0 2162.78 80.29 5 -4 0 33.80 2.00 5 -4 0 31.30 2.80 -5 -4 0 28.40 2.90 -5 -4 0 36.10 2.90 -5 -4 0 34.80 1.70 5 -4 0 29.30 2.60 5 4 0 35.40 1.70 5 4 0 32.40 1.60 -5 4 0 36.10 3.30 5 4 0 30.90 2.40 6 -4 0 72.09 3.90 6 -4 0 65.59 3.50 6 -4 0 64.99 4.20 -6 -4 0 66.79 4.50 -6 -4 0 60.99 4.30 -6 -4 0 72.19 2.90 6 4 0 73.09 2.90 6 4 0 65.69 4.30 6 4 0 64.69 3.90 -6 4 0 62.29 4.70 6 4 0 70.39 2.80 7 -4 0 347.77 14.30 7 -4 0 362.26 13.80 -7 -4 0 322.97 14.40 -7 -4 0 337.77 14.50 7 -4 0 348.77 13.40 7 4 0 344.17 12.40 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182.38 8.30 -7 -5 0 172.28 8.70 -7 5 0 179.68 9.20 7 5 0 186.98 6.80 7 5 0 175.88 8.60 7 5 0 177.68 8.30 -8 -5 0 32.20 3.80 8 -5 0 34.90 2.80 8 -5 0 33.80 3.60 -8 -5 0 36.40 4.10 8 -5 0 36.20 3.30 8 5 0 34.70 3.90 8 5 0 37.40 3.30 -8 5 0 35.50 4.40 9 -5 0 74.49 4.50 9 -5 0 67.29 4.90 -9 -5 0 66.99 5.80 -9 -5 0 77.09 5.80 9 5 0 62.39 4.70 -9 5 0 68.69 6.20 9 5 0 68.09 5.40 -10 -5 0 1.40 2.60 10 -5 0 5.30 2.70 -10 -5 0 5.10 2.20 10 5 0 4.30 2.30 -10 5 0 8.80 2.90 10 5 0 7.10 2.30 11 -5 0 54.79 5.40 -11 -5 0 66.49 6.10 -11 -5 0 52.29 5.90 11 5 0 55.79 5.70 -11 5 0 51.79 6.30 11 5 0 54.29 5.20 -12 -5 0 -1.00 2.00 12 -5 0 -1.40 2.00 -12 -5 0 0.70 2.90 12 5 0 -0.10 2.80 12 5 0 0.50 2.40 -12 5 0 3.50 3.00 -13 -5 0 -3.10 2.10 13 -5 0 1.10 2.10 -13 -5 0 -0.20 2.40 13 5 0 2.50 3.00 -13 5 0 -6.30 3.30 13 5 0 -1.00 2.60 0 -6 0 27.80 1.90 0 -6 0 24.30 1.90 0 -6 0 27.70 2.10 0 -6 0 31.50 2.00 0 6 0 27.50 2.00 -1 -6 0 90.39 4.30 1 -6 0 91.39 3.90 -1 -6 0 93.19 4.20 -1 -6 0 86.59 4.10 -1 -6 0 92.19 4.30 1 -6 0 90.99 4.40 1 -6 0 95.79 4.40 1 6 0 86.89 4.20 -1 6 0 92.69 4.40 2 -6 0 438.86 17.50 -2 -6 0 461.55 17.30 -2 -6 0 457.25 17.40 -2 -6 0 461.25 17.60 -2 -6 0 468.15 17.50 2 -6 0 449.36 16.80 2 -6 0 460.75 17.70 -2 6 0 469.75 17.70 -2 6 0 460.25 16.70 2 6 0 453.95 17.30 2 6 0 456.05 17.40 3 -6 0 2521.25 94.19 -3 -6 0 2610.74 95.39 -3 -6 0 2625.84 95.09 3 -6 0 2649.33 95.29 3 -6 0 2540.95 95.29 3 6 0 2631.54 94.99 3 6 0 2634.84 94.69 -3 6 0 2860.71 94.39 -4 -6 0 1.70 1.40 -4 -6 0 -0.10 1.10 4 -6 0 -0.90 0.80 4 -6 0 -0.40 0.50 4 -6 0 -0.40 0.90 4 -6 0 0.40 0.50 -4 6 0 1.00 0.50 4 6 0 0.30 1.00 -4 6 0 3.40 1.70 4 6 0 -0.50 0.80 -5 -6 0 129.19 6.20 5 -6 0 124.89 6.20 5 -6 0 123.79 5.00 -5 -6 0 121.59 6.40 5 -6 0 122.19 6.10 5 6 0 122.39 5.90 -5 6 0 117.89 6.50 5 6 0 123.79 5.10 6 -6 0 6.10 1.80 6 -6 0 6.80 1.20 6 -6 0 11.60 1.90 -6 -6 0 8.90 2.10 -6 -6 0 7.80 2.20 6 6 0 9.70 1.00 6 6 0 8.50 2.10 -6 6 0 8.10 2.50 6 6 0 8.40 1.70 7 -6 0 -1.50 1.60 7 -6 0 -2.20 1.40 -7 -6 0 -2.20 1.20 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4.70 7 -7 0 150.38 6.70 -7 -7 0 158.38 8.30 7 -7 0 152.48 7.70 7 -7 0 157.18 7.90 -7 -7 0 147.09 7.90 -7 7 0 154.58 8.50 7 7 0 161.98 7.60 7 7 0 158.38 8.20 -8 -7 0 9.40 2.50 -8 -7 0 15.20 3.00 8 -7 0 8.90 2.30 8 -7 0 20.90 3.00 8 7 0 9.70 2.30 -8 7 0 9.20 2.60 8 7 0 9.40 2.30 9 -7 0 164.18 8.10 -9 -7 0 173.38 9.30 9 -7 0 159.98 8.80 -9 -7 0 160.18 8.70 -9 7 0 145.69 8.90 9 7 0 162.48 9.00 9 7 0 155.48 8.20 -10 -7 0 12.00 3.40 10 -7 0 11.00 2.50 10 -7 0 10.40 3.10 -10 -7 0 8.60 3.10 10 7 0 10.10 3.20 -10 7 0 6.70 2.90 10 7 0 9.90 2.70 -11 -7 0 34.70 5.00 11 -7 0 42.90 4.90 -11 -7 0 44.20 5.40 11 7 0 45.10 5.10 11 7 0 37.90 4.60 -11 7 0 43.60 5.90 -12 -7 0 11.50 3.70 -12 -7 0 0.10 2.40 12 -7 0 5.20 3.30 -12 7 0 2.00 3.90 12 7 0 4.80 3.40 12 7 0 4.40 2.70 -13 -7 0 3.20 3.10 -13 -7 0 1.80 3.70 13 -7 0 -1.20 3.10 -13 7 0 -2.70 3.90 13 7 0 2.70 3.60 0 -8 0 204.08 8.70 0 -8 0 211.18 8.70 0 -8 0 206.08 8.50 0 -8 0 211.18 8.90 0 8 0 193.28 8.80 0 8 0 210.98 8.70 1 -8 0 173.28 7.70 -1 -8 0 165.48 7.40 -1 -8 0 174.08 7.40 1 -8 0 165.68 7.50 -1 -8 0 166.28 7.30 1 -8 0 167.48 6.90 -1 -8 0 163.78 7.30 1 8 0 166.38 7.40 -1 8 0 169.28 7.50 1 8 0 178.78 7.40 2 -8 0 9.70 1.80 2 -8 0 13.20 1.30 -2 -8 0 14.60 1.90 -2 -8 0 11.20 1.60 -2 -8 0 12.90 1.80 -2 -8 0 7.70 1.70 2 -8 0 12.40 1.80 -2 8 0 12.40 2.00 2 8 0 11.00 1.60 2 8 0 12.90 1.80 -3 -8 0 106.99 5.20 3 -8 0 106.29 4.30 -3 -8 0 101.39 5.10 -3 -8 0 97.69 5.40 -3 -8 0 101.29 5.20 3 -8 0 104.89 5.40 3 -8 0 109.29 5.70 -3 8 0 118.49 5.80 3 8 0 107.79 5.10 3 8 0 109.29 5.30 4 -8 0 492.85 19.90 4 -8 0 501.55 18.40 -4 -8 0 500.55 20.10 4 -8 0 487.25 19.90 -4 -8 0 504.45 19.70 -4 8 0 511.75 20.20 -4 8 0 530.15 18.40 4 8 0 495.25 19.50 4 8 0 515.75 19.20 5 -8 0 123.69 4.70 -5 -8 0 117.29 6.40 5 -8 0 120.89 4.70 -5 -8 0 124.49 6.30 5 -8 0 114.89 6.40 5 -8 0 124.79 6.50 -5 8 0 115.49 6.40 5 8 0 120.09 5.40 5 8 0 121.19 6.00 -6 -8 0 35.70 3.50 6 -8 0 27.30 2.00 -6 -8 0 28.50 3.30 6 -8 0 32.90 3.60 6 -8 0 31.30 3.40 -6 8 0 28.90 3.70 6 8 0 32.30 2.20 6 8 0 31.80 3.40 6 8 0 30.70 3.00 7 -8 0 116.09 6.30 -7 -8 0 113.09 6.40 -7 -8 0 102.19 6.70 7 -8 0 103.19 6.20 -7 8 0 101.99 6.50 7 8 0 105.09 6.60 7 8 0 104.19 5.80 -8 -8 0 0.40 2.00 -8 -8 0 3.00 2.50 8 -8 0 -1.00 1.70 8 -8 0 -1.40 1.40 8 8 0 0.20 2.20 8 8 0 -3.20 1.50 -8 8 0 0.60 2.70 -9 -8 0 27.80 4.10 -9 -8 0 28.10 3.90 9 -8 0 29.80 4.10 9 -8 0 27.10 3.60 -9 8 0 30.80 4.30 9 8 0 20.40 3.10 9 8 0 27.60 3.70 10 -8 0 0.40 1.90 10 -8 0 3.70 2.40 -10 -8 0 0.30 2.00 -10 -8 0 1.90 2.60 10 8 0 -0.60 2.20 -10 8 0 2.40 3.40 -10 8 0 0.90 2.50 10 8 0 -0.30 2.00 11 -8 0 118.39 8.30 -11 -8 0 139.89 8.90 -11 -8 0 128.19 8.90 11 8 0 145.69 9.00 11 8 0 121.89 7.80 -11 8 0 125.69 9.50 -12 -8 0 18.10 4.60 12 -8 0 20.30 4.20 -12 -8 0 17.70 4.20 12 8 0 15.40 3.80 -12 8 0 29.00 5.70 12 8 0 12.60 4.10 13 -8 0 0.70 3.20 -13 -8 0 3.50 3.60 -13 -8 0 0.80 2.90 -13 8 0 4.40 4.60 13 8 0 2.70 2.80 0 -9 0 1.10 1.40 0 -9 0 0.30 0.90 0 -9 0 -1.40 0.70 0 9 0 -0.90 1.30 0 9 0 2.70 1.30 1 -9 0 212.58 8.60 1 -9 0 217.88 9.30 -1 -9 0 209.58 9.00 -1 -9 0 212.48 9.10 -1 -9 0 210.08 9.20 1 -9 0 209.08 9.30 -1 -9 0 209.28 9.10 1 9 0 210.18 9.30 -1 9 0 212.78 9.40 -1 9 0 211.78 9.20 1 9 0 214.28 9.10 -2 -9 0 2.00 1.30 -2 -9 0 5.20 1.40 2 -9 0 5.10 1.40 -2 -9 0 2.90 1.40 2 -9 0 4.10 0.90 2 -9 0 3.50 1.30 -2 -9 0 6.30 1.60 2 9 0 2.90 1.40 2 9 0 5.80 1.50 -2 9 0 3.50 1.40 -3 -9 0 702.93 26.30 3 -9 0 670.23 25.20 3 -9 0 677.53 26.50 -3 -9 0 704.73 26.10 3 -9 0 656.03 26.60 -3 -9 0 684.73 26.20 -3 -9 0 698.23 26.60 3 9 0 688.33 26.20 3 9 0 702.43 26.10 -3 9 0 721.53 26.70 4 -9 0 36.40 1.70 4 -9 0 33.30 3.30 4 -9 0 34.70 3.50 -4 -9 0 30.70 3.20 -4 -9 0 32.10 3.00 -4 9 0 37.30 1.70 4 9 0 37.00 2.60 -4 9 0 36.40 3.70 4 9 0 32.00 3.00 5 -9 0 248.38 11.30 5 -9 0 255.27 9.30 5 -9 0 252.57 11.30 -5 -9 0 237.48 11.20 -5 -9 0 250.77 11.00 -5 9 0 251.57 11.50 5 9 0 255.37 10.30 5 9 0 256.47 10.80 -6 -9 0 54.79 4.30 -6 -9 0 60.09 4.30 6 -9 0 55.79 4.60 6 -9 0 60.59 4.20 -6 9 0 54.79 4.50 6 9 0 58.99 4.40 6 9 0 54.99 3.80 6 9 0 61.99 3.40 7 -9 0 64.19 5.00 -7 -9 0 57.19 4.60 -7 -9 0 56.29 5.20 7 -9 0 57.79 4.30 7 9 0 54.69 4.20 7 9 0 58.39 5.20 -7 9 0 60.99 4.90 8 -9 0 97.29 6.20 -8 -9 0 92.09 6.80 -8 -9 0 102.39 6.50 8 -9 0 96.19 6.60 -8 9 0 102.59 7.30 8 9 0 106.89 6.10 8 9 0 100.99 6.90 -9 -9 0 43.90 5.30 9 -9 0 41.30 4.50 9 -9 0 45.00 4.50 -9 -9 0 45.90 4.90 9 9 0 42.50 5.00 9 9 0 47.20 4.40 -9 9 0 38.40 4.40 -9 9 0 40.60 5.40 -10 -9 0 3.20 3.10 -10 -9 0 4.30 2.30 10 -9 0 7.50 2.60 10 -9 0 9.80 3.20 -10 9 0 10.20 4.00 10 9 0 5.40 2.60 10 9 0 10.30 3.50 -10 9 0 6.70 2.80 -11 -9 0 14.50 3.60 -11 -9 0 17.40 3.80 11 -9 0 13.80 3.70 11 9 0 18.70 3.80 11 9 0 8.60 3.00 -11 9 0 11.60 4.50 12 -9 0 2.70 2.40 -12 -9 0 4.20 3.20 -12 -9 0 -6.60 3.00 -12 9 0 5.00 4.20 12 9 0 6.00 3.80 0 -10 0 980.20 34.90 0 -10 0 821.72 35.00 0 -10 0 984.90 35.50 0 10 0 935.01 35.50 0 10 0 964.30 35.10 -1 -10 0 453.05 18.60 -1 -10 0 466.65 18.70 1 -10 0 492.25 18.90 1 -10 0 487.35 18.00 -1 -10 0 469.75 18.50 -1 -10 0 484.35 18.50 1 -10 0 462.45 18.80 1 10 0 465.35 18.50 1 10 0 481.85 18.80 -1 10 0 467.65 18.90 -1 10 0 460.65 18.60 -2 -10 0 33.90 2.70 -2 -10 0 32.00 3.00 -2 -10 0 32.70 3.00 -2 -10 0 32.60 3.10 2 -10 0 32.20 2.10 2 -10 0 35.10 3.30 2 -10 0 28.90 3.20 2 10 0 31.20 3.00 2 10 0 33.20 3.10 2 10 0 25.90 2.90 -2 10 0 32.60 3.20 -3 -10 0 31.30 2.90 3 -10 0 29.90 3.30 -3 -10 0 32.20 3.10 3 -10 0 25.70 3.10 -3 -10 0 31.10 2.90 -3 -10 0 27.00 3.10 3 -10 0 31.60 1.90 3 10 0 29.80 2.80 -3 10 0 31.30 3.30 3 10 0 29.40 2.90 -4 -10 0 307.37 12.60 4 -10 0 287.67 12.90 -4 -10 0 288.67 12.90 4 -10 0 306.77 11.10 4 -10 0 299.47 13.00 -4 10 0 303.17 13.20 4 10 0 297.47 12.20 4 10 0 297.97 12.50 5 -10 0 23.90 3.00 5 -10 0 14.80 2.80 -5 -10 0 22.70 2.80 -5 -10 0 24.40 3.30 5 10 0 24.30 2.80 -5 10 0 20.70 3.20 5 10 0 21.10 2.20 -6 -10 0 23.30 3.20 -6 -10 0 24.60 3.10 6 -10 0 23.60 3.10 6 -10 0 26.90 3.50 6 10 0 25.30 2.40 6 10 0 24.10 3.50 -6 10 0 18.00 3.10 6 10 0 27.90 3.00 7 -10 0 113.69 6.40 -7 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7 -11 0 2.90 1.90 7 -11 0 4.60 2.40 7 11 0 1.90 2.00 -7 11 0 -0.40 2.10 7 11 0 4.50 2.80 -7 11 0 3.40 2.60 -8 -11 0 77.09 5.80 -8 -11 0 58.79 6.00 8 -11 0 64.19 6.10 8 -11 0 81.09 5.90 8 11 0 82.19 6.40 8 11 0 68.09 5.20 -8 11 0 68.59 6.70 -8 11 0 74.49 5.90 -9 -11 0 108.49 7.30 -9 -11 0 102.09 7.90 9 -11 0 111.79 7.20 9 -11 0 100.59 7.40 9 11 0 97.69 6.60 -9 11 0 103.69 8.10 -9 11 0 109.89 7.40 9 11 0 113.19 8.00 10 -11 0 56.29 6.20 -10 -11 0 51.59 6.40 -10 -11 0 67.09 6.40 10 -11 0 60.19 5.80 10 11 0 60.29 5.50 -10 11 0 61.29 6.60 -10 11 0 50.89 5.60 10 11 0 59.89 6.50 -11 -11 0 0.20 2.90 11 -11 0 3.10 2.50 -11 -11 0 0.80 3.50 11 11 0 -3.50 3.20 -11 11 0 -1.00 3.70 -12 -11 0 28.60 5.10 -12 -11 0 35.40 5.90 12 -11 0 26.70 4.70 12 11 0 27.40 5.40 -12 11 0 27.40 6.10 0 -12 0 1284.27 54.99 0 -12 0 1562.94 55.59 0 -12 0 1512.75 54.69 0 12 0 1574.04 55.69 0 12 0 1508.45 55.09 -1 -12 0 65.09 4.30 -1 -12 0 69.99 4.50 -1 -12 0 69.49 4.70 1 -12 0 64.69 3.90 -1 -12 0 61.19 4.30 1 -12 0 75.49 4.90 1 -12 0 79.09 5.10 -1 12 0 68.69 4.70 1 12 0 69.79 4.70 -1 12 0 64.99 5.00 1 12 0 60.59 4.40 2 -12 0 162.18 8.30 2 -12 0 169.98 7.20 -2 -12 0 172.18 8.00 2 -12 0 163.08 8.40 -2 -12 0 175.08 8.10 -2 -12 0 164.58 8.20 -2 -12 0 158.78 8.00 -2 12 0 160.38 8.40 2 12 0 161.48 8.20 -2 12 0 170.18 8.30 2 12 0 172.58 8.10 2 12 0 164.78 8.00 -3 -12 0 41.00 3.70 3 -12 0 41.80 4.10 -3 -12 0 30.20 3.60 3 -12 0 43.10 2.50 3 -12 0 39.60 3.90 -3 -12 0 43.40 3.90 -3 -12 0 43.70 3.60 3 12 0 36.10 3.60 -3 12 0 37.40 3.80 3 12 0 41.30 3.70 -3 12 0 39.00 4.00 -4 -12 0 181.48 9.30 4 -12 0 177.18 9.40 -4 -12 0 186.78 8.70 4 -12 0 183.78 9.30 4 12 0 184.38 8.80 -4 12 0 192.38 9.70 4 12 0 180.28 8.50 -4 12 0 183.78 9.40 -5 -12 0 43.00 4.00 5 -12 0 42.50 4.60 -5 -12 0 39.50 4.20 5 -12 0 42.50 4.50 -5 12 0 50.19 5.00 5 12 0 46.40 3.40 -5 12 0 38.90 4.50 5 12 0 48.40 4.30 -6 -12 0 -2.10 1.40 6 -12 0 0.10 2.30 6 -12 0 0.20 1.70 -6 -12 0 -2.10 1.90 6 12 0 2.00 1.40 6 12 0 -0.70 1.70 -6 12 0 -2.70 2.50 -6 12 0 1.50 2.40 6 12 0 -0.30 1.90 7 -12 0 8.80 3.10 -7 -12 0 4.40 3.00 7 -12 0 11.70 3.10 -7 -12 0 8.60 2.60 7 12 0 9.00 2.60 -7 12 0 11.30 3.30 7 12 0 10.70 2.60 -7 12 0 9.70 3.50 -8 -12 0 15.60 3.20 8 -12 0 15.60 3.50 -8 -12 0 16.40 3.70 8 -12 0 13.50 3.10 -8 12 0 12.90 3.50 -8 12 0 11.90 3.20 8 12 0 12.20 3.70 8 12 0 11.10 3.00 -9 -12 0 115.69 8.20 9 -12 0 99.49 7.10 -9 -12 0 104.59 7.60 9 -12 0 120.49 7.70 -9 12 0 108.89 7.80 -9 12 0 91.69 7.40 9 12 0 105.89 6.90 9 12 0 104.89 8.10 10 -12 0 24.80 4.60 -10 -12 0 21.10 4.10 10 -12 0 19.00 4.00 -10 -12 0 25.10 4.90 -10 12 0 18.30 4.80 -10 12 0 17.00 3.80 10 12 0 20.40 3.70 10 12 0 23.00 4.60 -11 -12 0 10.20 3.70 -11 -12 0 13.20 4.40 11 -12 0 7.40 3.70 -11 12 0 5.30 4.40 11 12 0 10.30 4.30 0 -13 0 1.70 1.70 0 -13 0 0.20 2.00 0 -13 0 0.40 1.90 0 13 0 0.20 1.60 0 13 0 -0.10 1.90 1 -13 0 1.10 1.30 -1 -13 0 2.10 1.50 -1 -13 0 -1.90 1.10 1 -13 0 0.20 2.10 1 -13 0 0.30 1.40 -1 -13 0 2.10 1.90 -1 -13 0 0.00 1.40 -1 13 0 -1.40 2.10 1 13 0 -0.30 1.90 1 13 0 -0.20 1.40 -1 13 0 -1.00 1.90 -2 -13 0 94.99 5.70 -2 -13 0 97.29 5.90 -2 -13 0 92.99 5.80 2 -13 0 108.79 6.60 -2 -13 0 92.69 5.70 2 -13 0 106.89 6.40 2 -13 0 100.39 5.00 2 13 0 99.49 6.00 -2 13 0 102.99 6.10 -2 13 0 94.39 6.50 2 13 0 96.59 5.80 2 13 0 109.19 6.10 3 -13 0 323.07 14.10 -3 -13 0 302.47 13.30 -3 -13 0 312.07 13.20 3 -13 0 298.37 13.70 -3 -13 0 315.97 13.50 -3 -13 0 315.37 13.70 3 13 0 298.37 13.30 -3 13 0 306.37 14.10 3 13 0 307.17 13.30 -3 13 0 305.47 13.70 3 13 0 296.37 13.30 -4 -13 0 16.30 2.80 -4 -13 0 15.60 2.70 -4 -13 0 10.30 2.60 4 -13 0 19.60 3.10 4 -13 0 16.70 3.40 4 13 0 20.30 2.80 -4 13 0 22.70 3.70 4 13 0 20.00 2.70 -4 13 0 17.50 3.10 5 -13 0 21.70 3.70 -5 -13 0 34.40 3.70 -5 -13 0 26.90 3.80 5 -13 0 36.00 4.30 -5 13 0 26.50 4.10 5 13 0 21.30 3.00 -5 13 0 27.00 4.10 5 13 0 29.10 3.50 6 -13 0 235.38 11.40 -6 -13 0 213.08 10.50 6 -13 0 210.98 10.90 -6 -13 0 223.08 11.30 6 13 0 223.68 11.20 6 13 0 219.58 10.50 -6 13 0 212.58 11.00 -6 13 0 205.88 10.90 7 -13 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5.50 1 -10 4 23.20 2.70 1 -10 4 31.40 3.30 -1 -10 -4 25.70 2.90 -1 -10 -4 22.90 2.90 1 10 4 24.10 3.00 1 10 4 23.40 2.90 1 10 4 27.10 2.10 -1 10 -4 32.20 2.00 -1 10 -4 31.00 3.30 -2 -10 -4 4.10 1.60 2 -10 4 6.90 1.80 2 -10 4 1.90 1.30 -2 -10 -4 4.80 1.20 -2 -10 -4 9.20 2.30 2 10 4 7.00 1.90 2 10 4 5.30 1.60 2 10 4 3.70 1.20 -2 10 -4 6.90 0.90 -2 10 -4 8.90 2.00 3 -10 4 189.68 9.20 -3 -10 -4 182.18 7.80 3 -10 4 175.78 8.60 -3 -10 -4 192.98 9.10 -3 10 -4 188.48 9.30 3 10 4 182.78 8.60 3 10 4 185.98 8.80 4 -10 4 -0.20 1.40 -4 -10 -4 4.10 2.10 -4 -10 -4 -0.80 1.10 4 -10 4 -0.80 1.20 4 10 4 -0.60 1.80 -4 10 -4 -2.30 1.50 4 10 4 2.70 1.60 5 -10 4 481.05 19.90 -5 -10 -4 487.05 20.30 5 -10 4 469.85 19.90 -5 -10 -4 480.15 18.90 5 10 4 488.85 19.00 -5 10 -4 464.35 20.20 5 10 4 487.15 19.60 -6 -10 -4 196.68 10.30 6 -10 4 175.68 9.50 6 -10 4 188.88 9.90 -6 -10 -4 208.88 9.20 6 10 4 195.68 9.70 -6 10 -4 192.18 10.20 6 10 4 196.58 8.80 7 -10 4 76.29 5.50 -7 -10 -4 79.49 5.40 7 -10 4 83.19 5.80 -7 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8 -11 -4 8.90 2.70 -8 -11 4 8.20 3.10 -8 -11 4 2.30 2.30 -8 11 4 10.80 3.30 -8 11 4 8.80 2.90 8 11 -4 5.30 2.10 8 11 -4 8.40 2.60 -7 -11 4 45.90 4.70 7 -11 -4 47.10 4.70 7 -11 -4 45.30 4.80 -7 -11 4 39.40 4.40 7 11 -4 48.10 3.80 -7 11 4 42.40 4.70 7 11 -4 37.30 4.30 -7 11 4 44.10 4.80 -6 -11 4 41.30 4.00 6 -11 -4 39.30 4.40 -6 -11 4 46.80 4.50 6 -11 -4 41.20 4.40 -6 -11 4 44.50 4.60 -6 11 4 46.80 4.50 -6 11 4 42.10 4.60 6 11 -4 41.80 4.20 6 11 -4 44.10 3.30 6 11 -4 43.90 3.20 -5 -11 4 32.10 3.70 -5 -11 4 30.60 3.70 5 -11 -4 28.40 3.60 -5 -11 4 32.40 2.90 5 -11 -4 33.00 2.80 5 -11 -4 31.40 3.80 -5 11 4 40.50 3.80 -5 11 4 27.10 3.70 5 11 -4 31.50 2.90 5 11 -4 36.20 2.80 5 11 -4 28.40 3.60 -4 -11 4 2.50 1.50 4 -11 -4 0.00 1.30 4 -11 -4 0.90 2.00 -4 -11 4 3.40 1.60 -4 -11 4 0.90 1.40 -4 -11 4 -1.20 1.20 4 -11 -4 1.00 1.20 -4 11 4 0.70 1.50 -4 11 4 0.40 1.90 4 11 -4 1.20 1.30 4 11 -4 2.50 1.40 4 11 -4 -0.80 1.10 3 -11 -4 175.18 8.90 -3 -11 4 169.08 8.30 -3 -11 4 191.38 8.70 -3 -11 4 190.48 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2.60 9 11 4 1.70 2.70 10 -11 4 18.00 3.80 10 -11 4 13.80 4.00 -10 -11 -4 10.50 4.10 10 11 4 9.70 3.50 10 11 4 12.00 3.50 -10 11 -4 5.40 4.40 -11 -11 -4 -0.40 3.50 11 -11 4 8.20 3.90 -11 11 -4 5.30 4.60 11 11 4 8.00 3.60 11 11 4 4.50 3.90 -12 -12 4 51.19 6.50 12 -12 -4 33.10 5.10 -12 12 4 37.50 6.40 12 12 -4 43.80 6.60 -11 -12 4 9.90 3.80 11 -12 -4 13.70 3.90 -11 -12 4 0.10 2.80 -11 12 4 5.10 3.10 11 12 -4 14.00 3.70 10 -12 -4 19.10 3.60 10 -12 -4 14.00 3.50 -10 -12 4 12.70 4.20 -10 -12 4 12.00 3.30 -10 12 4 21.20 4.00 10 12 -4 11.40 4.30 -10 12 4 13.40 4.40 9 -12 -4 24.80 3.90 -9 -12 4 20.00 3.90 9 -12 -4 25.50 4.00 -9 -12 4 30.90 4.80 -9 12 4 32.40 4.60 9 12 -4 29.80 4.40 -9 12 4 24.70 4.40 -8 -12 4 155.58 9.70 8 -12 -4 182.28 9.90 -8 -12 4 196.98 10.50 8 -12 -4 183.28 10.10 8 12 -4 191.48 10.10 -8 12 4 188.68 10.20 -8 12 4 182.08 10.20 7 -12 -4 3.30 2.50 -7 -12 4 1.60 2.00 7 -12 -4 2.00 1.90 -7 -12 4 8.10 2.70 -7 12 4 0.80 2.00 7 12 -4 1.90 2.10 7 12 -4 2.10 2.00 -7 12 4 2.20 2.60 6 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6.50 -4 -12 -4 133.39 7.90 4 -12 4 128.39 7.30 4 -12 4 134.29 7.90 4 12 4 135.79 7.10 4 12 4 132.59 7.30 -4 12 -4 136.49 8.20 5 -12 4 38.10 4.30 5 -12 4 33.00 4.30 -5 -12 -4 35.20 3.40 -5 -12 -4 34.70 4.20 5 12 4 39.50 3.90 5 12 4 33.90 4.00 -5 12 -4 34.90 4.80 -6 -12 -4 16.20 3.30 6 -12 4 12.90 3.20 6 -12 4 9.70 3.10 6 12 4 13.40 3.10 6 12 4 9.80 2.30 -6 12 -4 13.10 3.40 7 -12 4 60.69 5.90 7 -12 4 56.59 5.70 -7 -12 -4 59.89 6.10 7 12 4 60.19 5.60 -7 12 -4 40.60 5.30 -8 -12 -4 33.30 4.70 8 -12 4 44.90 5.20 8 -12 4 36.50 4.90 8 12 4 31.60 4.20 -8 12 -4 34.30 5.00 9 -12 4 -3.70 2.70 9 -12 4 -0.60 2.60 -9 -12 -4 -3.30 2.90 -9 12 -4 0.60 3.70 9 12 4 -3.60 2.60 10 -12 4 143.49 9.80 -10 -12 -4 148.69 9.60 10 -12 4 149.29 9.20 10 12 4 138.19 9.30 -10 12 -4 149.79 10.70 10 12 4 132.09 9.10 11 -12 4 7.50 3.90 -11 -12 -4 2.80 4.10 11 12 4 6.60 4.20 11 12 4 6.30 3.70 -11 12 -4 5.10 3.70 -11 -13 4 8.10 3.70 11 -13 -4 7.80 3.60 -11 -13 4 12.60 4.20 11 13 -4 9.80 3.50 -11 13 4 7.90 4.50 -10 -13 4 74.79 7.70 10 -13 -4 67.29 6.60 -10 -13 4 65.49 7.10 10 -13 -4 85.79 6.50 -10 13 4 63.39 6.80 10 13 -4 70.29 7.40 -10 13 4 77.79 7.20 9 -13 -4 8.10 3.20 -9 -13 4 4.80 2.80 -9 -13 4 8.60 3.50 9 -13 -4 4.80 2.60 -9 13 4 2.90 3.50 -9 13 4 10.00 3.90 9 13 -4 10.20 3.30 -8 -13 4 44.30 5.30 -8 -13 4 35.90 4.70 8 -13 -4 34.90 4.90 8 -13 -4 39.30 4.60 -8 13 4 43.20 5.30 -8 13 4 39.40 5.10 8 13 -4 34.10 4.60 7 -13 -4 3.90 2.80 -7 -13 4 2.50 1.90 7 -13 -4 4.60 2.20 -7 -13 4 1.40 2.10 -7 13 4 5.70 2.90 7 13 -4 -2.20 1.90 -7 13 4 8.90 3.40 7 13 -4 -0.60 1.80 -6 -13 4 124.79 7.40 6 -13 -4 118.19 7.70 6 -13 -4 123.19 7.80 -6 -13 4 114.69 7.50 -6 13 4 128.49 8.00 6 13 -4 123.69 6.50 6 13 -4 122.69 7.30 -6 13 4 130.49 7.60 -5 -13 4 4.60 2.30 -5 -13 4 4.60 1.80 -5 -13 4 1.00 2.40 5 -13 -4 4.90 2.70 5 -13 -4 2.70 2.00 5 13 -4 2.40 2.30 5 13 -4 2.30 1.80 -5 13 4 1.60 2.60 5 13 -4 3.40 1.90 -5 13 4 1.40 2.20 4 -13 -4 6.40 1.80 -4 -13 4 7.20 2.50 -4 -13 4 1.90 1.80 -4 -13 4 2.80 2.30 -4 -13 4 3.50 1.70 4 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39.50 5.70 9 15 -5 44.50 6.10 -9 15 5 36.80 5.00 -8 -15 5 19.20 4.60 8 -15 -5 34.00 4.60 -8 -15 5 22.70 4.30 8 -15 -5 31.20 5.00 8 15 -5 28.80 5.00 -8 15 5 29.80 4.90 -8 15 5 18.90 4.50 -7 -15 5 21.70 4.00 -7 -15 5 25.50 4.40 7 -15 -5 19.20 4.40 7 -15 -5 25.90 4.20 -7 15 5 22.70 4.10 -7 15 5 24.90 4.20 7 15 -5 27.40 4.20 6 -15 -5 37.00 4.70 -6 -15 5 31.90 4.70 -6 -15 5 52.79 5.70 6 -15 -5 32.00 4.40 -6 15 5 34.80 4.70 6 15 -5 40.10 4.90 -6 15 5 34.30 4.50 5 -15 -5 105.69 7.40 5 -15 -5 103.49 7.50 -5 -15 5 104.89 7.00 -5 -15 5 103.39 6.20 -5 -15 5 99.39 6.70 5 15 -5 111.09 7.00 5 15 -5 99.69 6.90 -5 15 5 80.59 6.60 5 15 -5 87.59 6.00 -5 15 5 104.09 6.50 5 15 -5 101.69 6.10 -4 -15 5 12.00 2.70 -4 -15 5 14.00 3.20 -4 -15 5 12.90 2.90 4 -15 -5 9.40 3.30 -4 -15 5 14.70 2.90 4 -15 -5 13.50 3.20 4 15 -5 12.90 2.90 -4 15 5 6.40 3.10 4 15 -5 13.30 3.00 4 15 -5 18.30 2.90 4 15 -5 11.50 3.00 -4 15 5 9.10 2.80 -3 -15 5 38.90 4.30 3 -15 -5 38.20 4.80 -3 -15 5 47.60 4.20 -3 -15 5 38.60 4.80 -3 -15 5 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13.70 4.10 11 3 8 11.90 3.30 -12 -3 -8 12.40 4.00 12 -3 8 10.10 4.20 -12 3 -8 5.40 3.60 12 3 8 9.20 4.20 14 4 -8 -1.70 3.50 -13 -4 8 7.00 3.90 13 4 -8 2.40 2.60 -13 4 8 -0.30 2.50 12 -4 -8 87.39 6.60 -12 -4 8 90.49 8.40 -12 4 8 94.49 7.30 12 4 -8 91.79 6.90 11 -4 -8 5.70 2.30 -11 -4 8 5.90 3.40 11 -4 -8 4.60 2.60 11 4 -8 10.30 3.00 -11 4 8 5.60 2.60 10 -4 -8 20.40 3.30 -10 -4 8 15.10 3.50 10 -4 -8 18.00 2.90 10 4 -8 18.10 3.70 -10 4 8 22.50 4.00 9 -4 -8 193.18 9.30 -9 -4 8 192.98 10.10 9 -4 -8 183.58 8.70 -9 4 8 182.88 10.00 9 4 -8 177.48 9.70 -9 4 8 189.78 10.00 -8 -4 8 37.90 4.70 8 -4 -8 51.99 3.90 8 -4 -8 46.80 4.20 -8 4 8 57.79 3.80 8 4 -8 53.99 5.00 -8 4 8 62.59 4.90 7 -4 -8 36.00 3.40 -7 -4 8 23.70 3.50 7 -4 -8 34.20 3.00 -7 -4 8 33.30 2.10 7 4 -8 34.10 2.00 7 4 -8 29.90 3.70 -7 4 8 33.20 3.00 -7 4 8 33.80 3.70 6 -4 -8 52.49 3.20 6 -4 -8 41.60 3.60 -6 -4 8 49.30 3.80 -6 -4 8 49.50 2.70 -6 -4 8 44.50 2.10 6 4 -8 44.80 2.10 -6 4 8 42.00 3.80 6 4 -8 43.10 4.10 -6 4 8 42.90 3.30 6 4 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10 13.30 3.40 10 -8 -10 -1.90 2.00 -10 -8 10 3.30 3.20 -10 8 10 -0.10 2.60 10 8 -10 -3.40 3.10 9 -8 -10 43.30 4.40 -9 -8 10 40.80 5.00 9 -8 -10 36.10 4.10 -9 8 10 36.80 4.20 9 8 -10 44.60 5.30 -9 8 10 39.30 4.70 8 -8 -10 9.80 2.70 8 -8 -10 5.20 2.30 -8 -8 10 5.10 2.40 -8 8 10 1.50 2.10 -8 8 10 2.40 2.30 8 8 -10 -0.20 2.80 7 -8 -10 53.19 4.20 -7 -8 10 47.30 5.30 7 -8 -10 48.90 4.50 -7 8 10 45.70 4.50 7 8 -10 50.09 4.80 -7 8 10 51.19 4.50 6 -8 -10 23.10 3.20 -6 -8 10 23.70 2.60 6 -8 -10 19.30 2.90 -6 -8 10 24.00 3.80 -6 8 10 25.10 3.40 6 8 -10 25.40 3.30 -6 8 10 20.00 3.00 5 -8 -10 239.78 11.10 5 -8 -10 241.98 11.20 -5 -8 10 258.97 12.00 -5 -8 10 262.87 10.90 -5 8 10 240.88 10.60 5 8 -10 245.78 11.40 -5 8 10 251.07 11.30 4 -8 -10 125.39 6.60 -4 -8 10 118.19 6.90 -4 -8 10 122.49 6.30 4 -8 -10 119.29 6.50 -4 8 10 125.09 6.70 4 8 -10 114.99 6.60 4 8 -10 120.59 5.20 -4 8 10 124.89 5.80 3 -8 -10 24.80 2.90 -3 -8 10 21.30 2.80 -3 -8 10 23.40 1.80 -3 -8 10 22.10 3.10 3 -8 -10 18.60 2.90 -3 8 10 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11 10 70.99 6.30 7 11 -10 64.49 6.20 6 -11 -10 56.39 5.20 -6 -11 10 55.19 5.80 6 -11 -10 57.59 4.60 -6 11 10 61.69 5.70 6 11 -10 64.59 5.60 -6 11 10 49.70 4.30 5 -11 -10 24.60 3.50 -5 -11 10 33.50 4.20 5 -11 -10 23.20 3.60 -5 -11 10 30.40 3.40 -5 11 10 29.80 3.80 5 11 -10 28.50 3.90 4 -11 -10 152.68 8.20 4 -11 -10 156.08 8.30 -4 -11 10 165.68 9.00 -4 -11 10 165.18 8.20 -4 11 10 149.39 8.50 4 11 -10 163.18 8.40 -3 -11 10 1.70 2.00 -3 -11 10 -1.20 2.50 3 -11 -10 0.70 2.00 3 -11 -10 1.70 1.50 -3 11 10 0.90 1.40 3 11 -10 -2.20 2.40 -3 11 10 -0.80 2.30 3 11 -10 -2.40 1.70 2 -11 -10 -1.20 1.50 -2 -11 10 -1.40 1.20 -2 -11 10 -4.30 2.20 2 -11 -10 -1.00 1.90 -2 -11 10 -0.50 1.90 2 11 -10 -6.20 2.20 2 11 -10 -0.50 1.50 -2 11 10 -0.10 1.50 -2 11 10 -0.60 1.70 1 -11 -10 19.10 3.10 -1 -11 10 16.60 3.50 1 -11 -10 17.20 3.30 -1 -11 10 20.50 3.10 -1 -11 10 18.20 2.50 -1 11 10 14.10 3.00 1 11 -10 17.40 2.60 -1 11 10 10.30 3.10 1 11 -10 11.40 3.40 0 -11 -10 294.17 13.90 0 -11 10 309.37 12.80 0 -11 -10 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65.69 6.80 8 11 10 59.99 6.30 -8 11 -10 64.19 7.60 9 -11 10 7.80 3.60 9 -11 10 10.50 4.20 -9 -11 -10 14.70 4.60 9 11 10 6.60 3.90 -9 11 -10 6.10 4.70 11 -12 -10 1.70 3.00 -11 -12 10 5.90 3.60 11 12 -10 8.90 3.60 -11 12 10 6.50 3.50 10 -12 -10 24.50 4.30 -10 -12 10 14.80 4.50 -10 12 10 27.50 4.50 10 12 -10 26.10 5.30 -10 12 10 22.30 4.70 -9 -12 10 8.10 3.10 9 -12 -10 9.10 3.20 9 12 -10 5.80 3.10 -9 12 10 6.40 3.20 -9 12 10 7.80 3.60 -8 -12 10 159.98 10.20 8 -12 -10 161.98 9.50 -8 12 10 181.38 10.00 8 12 -10 164.28 9.50 -7 -12 10 6.40 3.20 7 -12 -10 7.00 2.30 7 12 -10 9.40 3.40 -7 12 10 7.10 3.30 6 -12 -10 62.69 5.90 6 -12 -10 63.69 5.00 -6 -12 10 70.79 6.60 6 12 -10 60.09 5.50 -6 12 10 69.39 5.50 -5 -12 10 31.40 3.50 -5 -12 10 33.80 4.50 5 -12 -10 33.10 3.90 5 -12 -10 34.40 4.30 5 12 -10 36.20 4.20 -5 12 10 36.70 4.60 -4 -12 10 262.97 11.50 4 -12 -10 234.88 11.40 4 -12 -10 253.17 11.80 -4 -12 10 235.28 12.00 4 12 -10 247.48 12.40 4 12 -10 213.28 11.10 -4 12 10 246.98 12.10 -3 -12 10 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7.60 3.30 6 -4 14 20.50 4.00 -6 -4 -14 22.60 4.00 6 -4 14 22.80 3.80 6 4 14 13.40 3.20 6 4 14 21.60 3.70 -6 4 -14 25.40 4.40 7 -4 14 6.80 3.00 -7 -4 -14 11.80 3.20 7 -4 14 9.80 3.50 7 4 14 6.00 2.90 7 4 14 8.40 3.40 -7 4 -14 9.10 3.90 -8 -4 -14 6.10 3.30 8 -4 14 11.60 3.90 8 -4 14 9.60 3.20 8 4 14 8.00 3.80 -8 4 -14 14.60 4.40 8 4 14 17.20 3.60 -9 -4 -14 5.60 3.40 9 -4 14 2.90 3.30 9 -4 14 6.40 3.90 9 4 14 6.60 3.30 -9 4 -14 3.90 4.10 -12 -5 14 20.60 4.70 12 -5 -14 23.80 4.40 12 5 -14 26.00 4.70 -12 5 14 24.40 4.70 11 -5 -14 8.30 3.40 -11 -5 14 2.10 2.80 -11 5 14 5.30 3.10 11 5 -14 1.20 3.40 -10 -5 14 15.60 4.20 10 -5 -14 12.90 3.00 -10 5 14 11.70 3.00 10 5 -14 5.10 2.90 -9 -5 14 -0.40 2.00 9 -5 -14 4.70 2.80 -9 5 14 3.80 2.40 9 5 -14 1.80 3.00 -8 -5 14 25.50 4.00 8 -5 -14 17.80 3.20 -8 5 14 23.30 3.40 8 5 -14 26.60 4.30 -8 5 14 23.30 3.70 7 -5 -14 34.40 4.10 7 -5 -14 37.20 3.90 -7 -5 14 44.60 4.90 7 5 -14 42.40 4.60 -7 5 14 35.10 3.80 -7 5 14 42.50 4.40 -6 -5 14 126.89 7.80 6 -5 -14 117.49 7.50 6 -5 -14 123.39 6.40 -6 -5 14 119.39 6.70 6 5 -14 120.69 7.60 -6 5 14 137.09 6.90 -6 5 14 129.49 6.50 -6 5 14 120.79 7.10 5 -5 -14 33.60 3.20 -5 -5 14 29.20 3.80 -5 -5 14 29.10 3.30 5 -5 -14 35.80 4.20 -5 5 14 29.10 3.70 5 5 -14 32.00 3.70 -5 5 14 35.20 3.30 -5 5 14 33.20 3.10 -4 -5 14 13.20 3.00 -4 -5 14 15.00 2.60 4 -5 -14 22.60 3.20 4 -5 -14 21.20 2.70 -4 5 14 20.30 2.40 -4 5 14 19.40 2.90 -4 5 14 19.30 2.50 4 5 -14 21.00 3.30 3 -5 -14 20.90 3.10 -3 -5 14 24.20 3.20 -3 -5 14 21.30 3.10 -3 5 14 22.10 2.20 -3 5 14 23.80 3.10 -3 5 14 20.10 2.60 3 5 -14 18.10 2.70 3 5 -14 19.50 3.10 -2 -5 14 7.50 1.30 2 -5 -14 6.90 2.20 2 -5 -14 6.80 1.60 -2 -5 14 14.60 2.70 -2 -5 14 4.80 2.30 2 5 -14 6.30 2.20 -2 5 14 9.20 1.40 2 5 -14 6.20 2.20 -2 5 14 7.30 2.20 -2 5 14 11.60 2.20 1 -5 -14 212.78 10.70 -1 -5 14 223.58 10.50 -1 -5 14 225.88 10.70 -1 -5 14 213.78 9.10 -1 5 14 214.48 9.80 1 5 -14 222.98 10.10 -1 5 14 218.08 10.30 1 5 -14 209.48 10.70 0 -5 14 63.99 4.90 0 -5 -14 71.09 5.10 0 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33.50 5.30 8 -5 14 50.59 6.00 -8 -5 -14 41.20 5.60 -8 5 -14 41.60 5.90 8 5 14 38.90 5.50 -9 -5 -14 100.79 8.10 9 -5 14 106.69 7.80 9 -5 14 88.89 8.00 -9 5 -14 107.89 9.50 9 5 14 85.09 7.90 12 -6 -14 0.20 2.90 -12 -6 14 1.50 2.80 -12 6 14 4.80 3.20 12 6 -14 -0.60 3.90 -11 -6 14 31.30 5.40 11 -6 -14 21.70 4.20 -11 6 14 26.50 4.50 11 6 -14 21.20 4.90 10 -6 -14 1.20 2.80 -10 -6 14 -1.90 2.10 -10 6 14 -2.30 2.40 10 6 -14 2.80 2.60 9 -6 -14 130.69 8.00 -9 -6 14 115.29 8.10 -9 6 14 130.39 7.80 -9 6 14 119.39 7.40 9 6 -14 113.49 8.20 8 -6 -14 9.40 2.60 -8 -6 14 14.40 3.20 -8 6 14 10.50 2.80 8 6 -14 16.00 3.70 -8 6 14 15.80 3.30 7 -6 -14 10.50 2.70 7 -6 -14 12.20 2.20 -7 -6 14 15.00 3.50 7 6 -14 16.60 3.60 -7 6 14 18.60 3.20 -7 6 14 17.60 3.00 6 -6 -14 19.20 3.60 -6 -6 14 22.50 3.00 -6 -6 14 19.50 3.50 6 -6 -14 13.60 2.30 6 6 -14 22.40 3.80 -6 6 14 20.00 2.70 -6 6 14 17.10 3.30 -6 6 14 14.40 2.60 -5 -6 14 338.27 16.40 5 -6 -14 387.36 15.60 5 -6 -14 374.06 16.50 -5 -6 14 376.56 15.80 5 6 -14 390.16 16.50 -5 6 14 386.76 16.30 -5 6 14 393.16 15.40 -5 6 14 359.96 15.50 -4 -6 14 41.30 4.70 -4 -6 14 48.60 4.30 4 -6 -14 49.40 4.70 4 -6 -14 40.60 3.70 -4 6 14 40.30 4.40 -4 6 14 47.00 3.30 -4 6 14 41.70 3.70 4 6 -14 42.60 4.40 -3 -6 14 60.09 5.50 3 -6 -14 61.89 5.40 -3 -6 14 63.29 4.80 3 6 -14 57.09 5.60 -3 6 14 55.89 4.10 -3 6 14 64.49 5.40 3 6 -14 59.79 4.70 -2 -6 14 12.40 2.80 2 -6 -14 6.80 2.70 -2 -6 14 9.20 2.50 -2 6 14 17.30 3.20 -2 6 14 12.20 2.30 2 6 -14 12.10 2.80 2 6 -14 13.40 2.60 1 -6 -14 265.67 12.80 -1 -6 14 278.37 11.30 -1 -6 14 285.07 13.00 -1 -6 14 277.37 12.80 1 6 -14 284.67 13.30 -1 6 14 284.67 12.30 1 6 -14 274.07 12.20 -1 6 14 287.27 12.90 0 -6 14 29.20 2.90 0 -6 -14 21.10 3.40 0 -6 14 34.70 4.20 0 6 14 25.20 3.10 0 6 14 26.60 3.80 0 6 -14 27.10 3.10 0 6 -14 21.40 3.70 1 -6 14 41.10 3.60 1 -6 14 36.70 4.60 -1 -6 -14 44.70 4.90 -1 6 -14 45.30 3.60 1 6 14 37.20 4.00 1 6 14 37.00 4.00 -1 6 -14 41.80 4.70 2 -6 14 3.60 2.20 2 -6 14 3.80 1.90 -2 -6 -14 2.50 2.60 -2 6 -14 6.00 1.80 -2 6 -14 5.30 2.70 2 6 14 2.50 1.80 2 6 14 4.30 1.90 3 -6 14 0.80 2.70 3 -6 14 6.20 2.30 -3 -6 -14 4.40 2.80 3 6 14 0.10 2.30 -3 6 -14 2.00 2.80 -3 6 -14 7.70 2.00 3 6 14 3.60 1.90 4 -6 14 22.60 3.50 4 -6 14 23.70 3.80 -4 -6 -14 18.80 3.40 4 6 14 19.70 3.20 -4 6 -14 14.40 3.70 4 6 14 27.50 3.80 5 -6 14 1.10 2.10 -5 -6 -14 0.70 2.80 5 -6 14 0.50 2.50 5 6 14 -2.80 1.50 -5 6 -14 5.30 3.30 5 6 14 -4.90 2.50 -6 -6 -14 16.80 4.00 6 -6 14 7.70 2.70 6 -6 14 11.50 3.90 6 6 14 15.60 3.40 6 6 14 18.40 4.00 -6 6 -14 9.90 4.10 7 -6 14 4.10 3.20 7 -6 14 6.10 3.50 -7 -6 -14 0.90 2.30 7 6 14 3.70 2.70 -7 6 -14 2.00 3.60 7 6 14 3.90 3.30 8 -6 14 -0.50 3.10 -8 -6 -14 1.50 2.20 8 -6 14 2.70 2.50 8 6 14 4.40 3.70 -8 6 -14 -3.50 2.50 9 -6 14 48.70 6.50 -9 -6 -14 40.10 5.50 9 -6 14 32.90 5.40 9 6 14 38.10 5.90 -9 6 -14 35.90 6.20 -12 -7 14 5.40 3.90 -12 7 14 3.40 3.00 12 7 -14 -4.40 3.40 11 -7 -14 8.40 3.40 -11 -7 14 14.90 4.60 -11 7 14 8.80 3.30 11 7 -14 13.30 4.40 -10 -7 14 9.40 3.30 10 -7 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15 82.69 7.90 -7 -10 -15 79.09 8.10 7 -10 15 59.89 6.80 -7 10 -15 80.09 8.60 7 10 15 62.99 6.80 -10 -11 15 44.10 6.60 10 11 -15 46.70 6.00 -9 -11 15 18.10 4.90 -9 11 15 13.70 4.00 9 11 -15 22.00 4.90 -8 -11 15 0.40 3.30 8 -11 -15 0.40 2.60 8 -11 -15 -2.00 2.40 8 11 -15 -1.30 2.30 -8 11 15 1.40 3.10 -7 -11 15 57.99 6.70 7 -11 -15 56.89 5.40 7 -11 -15 59.79 5.90 -7 11 15 45.20 5.00 7 11 -15 42.40 5.50 -7 11 15 44.40 5.20 6 -11 -15 5.60 2.60 6 -11 -15 4.80 2.40 -6 -11 15 6.20 2.90 -6 11 15 7.30 3.50 6 11 -15 6.30 3.10 -6 11 15 10.20 3.00 5 -11 -15 1.80 2.70 -5 -11 15 -1.20 2.80 -5 -11 15 1.40 2.30 5 -11 -15 2.40 2.50 -5 11 15 1.40 2.50 -5 11 15 1.50 2.40 5 11 -15 1.50 2.00 5 11 -15 -1.40 3.00 -4 -11 15 18.10 3.90 4 -11 -15 29.30 4.50 -4 -11 15 33.20 4.40 4 -11 -15 24.80 3.90 4 11 -15 30.80 4.80 -4 11 15 29.70 4.10 4 11 -15 27.70 4.00 -4 11 15 32.60 4.70 -3 -11 15 128.19 8.00 3 -11 -15 133.19 7.80 -3 -11 15 118.39 8.20 3 -11 -15 130.09 8.00 3 11 -15 124.89 8.60 -3 11 15 123.09 7.70 -3 11 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7.10 -5 12 -15 38.90 6.00 5 12 15 38.20 5.80 5 12 15 47.60 5.50 6 -12 15 2.30 3.20 -6 -12 -15 4.20 4.30 6 -12 15 15.60 4.60 6 12 15 8.90 4.30 6 12 15 11.70 3.60 -6 12 -15 2.40 3.60 -9 -13 15 8.30 3.60 9 13 -15 5.70 4.20 -9 13 15 7.90 3.90 8 -13 -15 5.60 3.00 -8 -13 15 3.10 3.70 8 13 -15 1.70 3.60 -8 13 15 5.70 3.30 -8 13 15 4.00 2.90 7 -13 -15 48.50 5.40 -7 -13 15 29.50 5.70 7 -13 -15 39.50 5.20 7 13 -15 39.60 5.50 -7 13 15 36.00 4.90 -7 13 15 29.60 4.70 6 -13 -15 15.40 3.80 -6 -13 15 16.20 4.50 6 -13 -15 19.00 3.80 6 13 -15 12.40 3.80 -6 13 15 6.80 3.70 -6 13 15 13.00 3.60 6 13 -15 12.20 4.30 5 -13 -15 -2.40 2.10 5 -13 -15 -3.30 2.20 -5 -13 15 0.40 3.30 -5 13 15 -0.30 2.40 5 13 -15 3.30 3.70 5 13 -15 -1.40 2.60 -5 13 15 0.80 2.50 4 -13 -15 3.10 2.60 -4 -13 15 1.40 2.50 -4 -13 15 2.40 2.60 4 -13 -15 3.00 2.90 -4 13 15 2.20 3.30 -4 13 15 -1.20 2.50 4 13 -15 0.80 2.70 4 13 -15 4.10 2.80 3 -13 -15 50.69 5.80 -3 -13 15 51.59 5.70 -3 -13 15 50.79 6.40 3 -13 -15 44.20 5.30 3 13 -15 52.19 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-23 2.00 4.00 -4 8 23 2.00 2.60 4 8 -23 8.30 3.90 -3 -8 23 -3.00 3.50 -3 -8 23 -1.70 3.30 3 -8 -23 -2.30 3.70 3 8 -23 -4.30 3.00 -3 8 23 3.50 3.50 3 8 -23 5.60 4.30 2 -8 -23 2.70 4.30 -2 -8 23 -0.50 3.50 -2 8 23 0.00 2.60 2 8 -23 -0.70 2.90 -1 -8 23 -3.30 3.60 1 -8 -23 -1.00 2.60 1 8 -23 -2.90 3.40 -1 8 23 -1.50 3.30 -6 0 24 23.50 4.90 6 0 -24 24.50 5.70 -5 0 24 0.30 3.50 5 0 -24 -3.20 2.50 -4 0 24 -2.10 3.10 4 0 -24 3.20 3.80 -3 0 24 -4.80 2.10 3 0 -24 1.50 3.70 -2 0 24 124.09 9.10 2 0 -24 138.49 9.80 1 0 -24 -0.40 3.20 -1 0 24 0.60 2.70 0 0 -24 5.70 3.60 0 0 24 -1.10 2.80 1 0 24 3.00 3.90 -1 0 -24 4.40 3.60 -6 -1 24 26.70 4.90 6 -1 -24 27.50 5.10 6 1 -24 33.70 6.00 -6 1 24 30.20 5.10 -5 -1 24 -1.40 2.40 5 -1 -24 1.70 3.90 -5 1 24 -2.00 2.10 5 1 -24 -1.60 3.60 4 -1 -24 8.10 3.50 -4 -1 24 9.60 3.40 4 1 -24 8.40 4.40 -4 1 24 15.90 4.50 -3 -1 24 0.30 3.70 3 -1 -24 4.00 3.70 -3 1 24 3.50 2.80 3 1 -24 -1.70 3.60 2 -1 -24 7.20 3.20 -2 -1 24 7.70 4.00 2 1 -24 12.60 4.20 -2 1 24 6.50 4.00 1 -1 -24 10.30 4.40 -1 -1 24 2.40 3.10 -1 1 24 17.40 4.90 1 1 -24 8.80 3.30 0 -1 24 -5.60 3.30 0 -1 -24 -2.00 2.20 0 1 24 1.10 2.90 0 1 -24 2.60 3.40 -1 -1 -24 10.90 4.00 1 -1 24 7.50 4.50 -1 1 -24 16.70 4.40 1 1 24 15.10 4.90 -6 -2 24 36.40 5.60 6 -2 -24 46.00 6.60 -6 2 24 41.90 6.00 6 2 -24 40.90 5.80 -5 -2 24 -4.10 3.10 5 -2 -24 -3.00 3.60 -5 2 24 1.00 3.30 5 2 -24 5.30 3.90 -4 -2 24 1.00 3.50 4 -2 -24 -2.90 3.60 4 2 -24 -0.80 2.40 -4 2 24 -2.90 2.30 3 -2 -24 27.10 5.40 -3 -2 24 26.70 4.80 -3 2 24 19.90 5.00 3 2 -24 28.50 4.80 -2 -2 24 71.79 7.80 2 -2 -24 71.19 7.90 2 2 -24 76.19 7.70 -2 2 24 83.69 8.10 -1 -2 24 11.20 4.30 1 -2 -24 2.60 3.80 1 2 -24 3.00 2.70 -1 2 24 11.60 4.30 0 -2 -24 -0.20 2.50 0 -2 24 0.60 3.80 0 2 -24 1.50 3.20 0 2 24 -1.50 2.70 1 -2 24 17.10 5.00 -1 -2 -24 12.50 4.50 -1 2 -24 9.10 3.70 1 2 24 13.30 4.90 -6 -3 24 10.00 4.00 6 -3 -24 19.60 4.80 6 3 -24 10.70 4.60 -6 3 24 17.10 4.50 -5 -3 24 1.50 3.30 5 -3 -24 -0.60 3.90 -5 3 24 1.10 3.40 5 3 -24 -8.40 3.20 -4 -3 24 7.90 3.80 4 -3 -24 5.20 3.20 4 3 -24 2.00 3.00 -4 3 24 2.40 3.50 3 -3 -24 18.60 4.90 -3 -3 24 20.20 4.80 -3 3 24 17.50 4.80 3 3 -24 20.60 4.30 2 -3 -24 -1.60 3.50 -2 -3 24 1.30 2.90 -2 3 24 2.30 3.80 2 3 -24 2.70 3.50 1 -3 -24 37.20 6.10 -1 -3 24 45.80 6.50 -1 3 24 48.30 6.70 1 3 -24 32.50 5.40 0 -3 24 6.80 4.10 0 -3 -24 -0.70 3.30 0 3 24 0.40 2.80 0 3 -24 2.50 3.10 1 -3 24 62.09 7.40 -1 -3 -24 70.19 7.80 1 3 24 69.59 8.00 -1 3 -24 58.29 6.80 -6 -4 24 44.50 7.50 6 -4 -24 59.19 7.70 6 4 -24 75.89 10.10 6 4 -24 44.30 6.60 -6 4 24 45.50 5.70 5 -4 -24 18.00 4.40 -5 -4 24 15.20 4.20 5 4 -24 5.20 3.30 -5 4 24 16.70 4.40 -4 -4 24 15.20 4.40 4 -4 -24 21.90 5.30 -4 4 24 16.30 4.60 4 4 -24 13.70 4.50 -3 -4 24 0.30 2.50 3 -4 -24 -1.00 2.70 -3 4 24 4.00 3.70 3 4 -24 2.60 2.80 -2 -4 24 2.90 3.80 2 -4 -24 1.20 2.70 -2 4 24 -0.30 3.50 2 4 -24 0.60 3.40 1 -4 -24 16.20 4.10 -1 -4 24 9.10 3.60 1 4 -24 11.20 3.80 -1 4 24 4.40 4.00 0 -4 -24 1.50 3.70 0 -4 24 4.40 3.10 0 4 24 0.90 2.90 0 4 -24 7.20 3.60 5 -5 -24 43.30 6.70 -5 -5 24 36.30 5.70 -5 -5 24 32.00 5.70 5 5 -24 33.50 5.40 -5 5 24 39.20 5.90 5 5 -24 43.20 6.30 4 -5 -24 17.00 4.40 -4 -5 24 6.80 4.10 -4 -5 24 15.90 4.50 4 5 -24 18.20 4.90 4 5 -24 9.70 4.30 -4 5 24 8.60 4.20 -3 -5 24 36.30 7.30 -3 -5 24 30.00 5.60 3 -5 -24 36.50 6.20 3 5 -24 29.90 4.80 -3 5 24 34.90 5.80 2 -5 -24 4.30 3.90 -2 -5 24 2.90 3.00 -2 5 24 -2.70 3.50 2 5 -24 0.10 3.40 -1 -5 24 56.69 7.30 1 -5 -24 68.19 7.90 1 5 -24 56.99 6.50 -1 5 24 62.59 7.30 0 -5 -24 -1.70 3.40 0 -5 24 -3.20 3.80 0 5 24 2.10 3.80 4 -6 -24 2.40 4.10 -4 -6 24 11.10 4.10 -4 -6 24 4.70 3.70 -4 6 24 4.50 3.00 4 6 -24 1.20 3.00 4 6 -24 6.20 4.00 3 -6 -24 4.10 3.00 -3 -6 24 2.80 3.70 3 6 -24 4.30 3.50 3 6 -24 2.60 3.50 -3 6 24 2.50 3.80 2 -6 -24 5.10 3.20 -2 -6 24 -2.20 3.50 -2 6 24 0.30 2.70 2 6 -24 -0.80 3.30 2 6 -24 1.30 3.50 1 -6 -24 9.50 3.50 -1 -6 24 -3.10 2.50 -1 6 24 2.00 2.90 -4 0 25 -5.50 3.10 4 0 -25 -3.00 2.50 -3 0 25 10.00 4.40 3 0 -25 10.70 3.80 -2 0 25 -0.30 2.90 2 0 -25 0.40 2.50 4 -1 -25 -3.40 3.70 -4 -1 25 -1.50 3.40 4 1 -25 0.10 3.70 -4 1 25 -6.50 3.20 -3 -1 25 43.10 6.60 3 -1 -25 36.40 6.20 3 1 -25 48.90 6.70 -3 1 25 46.20 6.20 2 -1 -25 12.10 4.40 -2 -1 25 13.20 4.70 -2 1 25 21.70 5.20 2 1 -25 17.50 4.20 3 -2 -25 1.60 4.00 -3 -2 25 4.50 3.00 3 2 -25 0.30 3.80 -3 2 25 2.40 3.00 2 -2 -25 39.10 6.10 -2 -2 25 31.10 5.80 -2 2 25 29.20 5.60 2 2 -25 17.90 4.80 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 62770 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp Cr1 Cr 0.38035(2) 0.28741(2) 0.25883(2) 0.02293(9) Uani 1 1 d . . Si1 Si 0.14658(5) 0.19698(3) 0.15602(3) 0.03534(14) Uani 1 1 d . . Si2 Si 0.24623(5) 0.37301(4) 0.37712(3) 0.03629(14) Uani 1 1 d . . N1 N 0.49275(13) 0.26387(9) 0.32551(8) 0.0270(3) Uani 1 1 d . . N2 N 0.42904(13) 0.31321(9) 0.18646(8) 0.0263(3) Uani 1 1 d . . C1 C 0.27748(16) 0.18936(11) 0.23366(10) 0.0288(4) Uani 1 1 d . . H1A H 0.3329 0.1464 0.2244 0.035 Uiso 1 1 calc R U H1B H 0.2433 0.1737 0.2753 0.035 Uiso 1 1 calc R U C2 C 0.2087(3) 0.19904(19) 0.07282(12) 0.0610(7) Uani 1 1 d . . H2A H 0.1402 0.2051 0.0323 0.091 Uiso 1 1 calc R U H2B H 0.2525 0.1497 0.0682 0.091 Uiso 1 1 calc R U H2C H 0.2660 0.2434 0.0743 0.091 Uiso 1 1 calc R U C3 C 0.0473(2) 0.10743(16) 0.15456(14) 0.0585(7) Uani 1 1 d . . H3A H 0.0118 0.1063 0.1973 0.088 Uiso 1 1 calc R U H3B H 0.0976 0.0601 0.1529 0.088 Uiso 1 1 calc R U H3C H -0.0195 0.1090 0.1127 0.088 Uiso 1 1 calc R U C4 C 0.0487(3) 0.28563(17) 0.15976(17) 0.0673(8) Uani 1 1 d . . H4A H 0.0217 0.2869 0.2052 0.101 Uiso 1 1 calc R U H4B H -0.0239 0.2835 0.1212 0.101 Uiso 1 1 calc R U H4C H 0.0967 0.3332 0.1549 0.101 Uiso 1 1 calc R U C5 C 0.30056(18) 0.38315(11) 0.29193(10) 0.0324(4) Uani 1 1 d . . H5A H 0.3606 0.4272 0.2967 0.039 Uiso 1 1 calc R U H5B H 0.2288 0.3980 0.2547 0.039 Uiso 1 1 calc R U C6 C 0.1661(3) 0.27761(15) 0.38436(14) 0.0536(6) Uani 1 1 d . . H6A H 0.1307 0.2779 0.4271 0.080 Uiso 1 1 calc R U H6B H 0.2257 0.2343 0.3871 0.080 Uiso 1 1 calc R U H6C H 0.0999 0.2705 0.3428 0.080 Uiso 1 1 calc R U C7 C 0.1348(3) 0.45440(17) 0.38331(16) 0.0625(7) Uani 1 1 d . . H7A H 0.1031 0.4487 0.4270 0.094 Uiso 1 1 calc R U H7B H 0.0658 0.4520 0.3426 0.094 Uiso 1 1 calc R U H7C H 0.1770 0.5052 0.3835 0.094 Uiso 1 1 calc R U C8 C 0.3796(3) 0.3814(2) 0.45275(14) 0.0697(8) Uani 1 1 d . . H8A H 0.4179 0.4334 0.4520 0.105 Uiso 1 1 calc R U H8B H 0.4406 0.3405 0.4489 0.105 Uiso 1 1 calc R U H8C H 0.3505 0.3748 0.4972 0.105 Uiso 1 1 calc R U C9 C 0.61131(16) 0.24736(10) 0.36146(9) 0.0262(4) Uani 1 1 d . . C10 C 0.63356(17) 0.17227(11) 0.39340(10) 0.0307(4) Uani 1 1 d . . C11 C 0.75254(19) 0.15559(12) 0.42960(12) 0.0403(5) Uani 1 1 d . . H11 H 0.7696 0.1054 0.4511 0.048 Uiso 1 1 calc R U C12 C 0.84678(19) 0.21037(13) 0.43501(12) 0.0416(5) Uani 1 1 d . . H12 H 0.9274 0.1978 0.4603 0.050 Uiso 1 1 calc R U C13 C 0.82374(18) 0.28318(13) 0.40374(12) 0.0393(5) Uani 1 1 d . . H13 H 0.8894 0.3202 0.4075 0.047 Uiso 1 1 calc R U C14 C 0.70716(18) 0.30378(12) 0.36686(11) 0.0348(4) Uani 1 1 d . . C15 C 0.5292(2) 0.11321(11) 0.38902(12) 0.0385(5) Uani 1 1 d . . H15 H 0.4596 0.1315 0.3511 0.046 Uiso 1 1 calc R U C16 C 0.5635(4) 0.03199(19) 0.3698(3) 0.1186(18) Uani 1 1 d . . H16A H 0.5900 0.0335 0.3243 0.178 Uiso 1 1 calc R U H16B H 0.4916 -0.0029 0.3662 0.178 Uiso 1 1 calc R U H16C H 0.6312 0.0121 0.4064 0.178 Uiso 1 1 calc R U C17 C 0.4832(4) 0.1133(3) 0.4578(2) 0.1074(15) Uani 1 1 d . . H17A H 0.5471 0.0913 0.4954 0.161 Uiso 1 1 calc R U H17B H 0.4081 0.0813 0.4526 0.161 Uiso 1 1 calc R U H17C H 0.4647 0.1675 0.4699 0.161 Uiso 1 1 calc R U C18 C 0.6853(2) 0.38541(14) 0.33452(16) 0.0582(7) Uani 1 1 d . . H18 H 0.5969 0.3886 0.3095 0.070 Uiso 1 1 calc R U C19 C 0.7065(3) 0.44873(16) 0.3930(2) 0.0811(10) Uani 1 1 d . . H19A H 0.6537 0.4376 0.4271 0.122 Uiso 1 1 calc R U H19B H 0.6858 0.5007 0.3719 0.122 Uiso 1 1 calc R U H19C H 0.7934 0.4481 0.4172 0.122 Uiso 1 1 calc R U C20 C 0.7660(3) 0.4012(2) 0.28069(17) 0.0814(10) Uani 1 1 d . . H20A H 0.8531 0.4027 0.3046 0.122 Uiso 1 1 calc R U H20B H 0.7431 0.4520 0.2576 0.122 Uiso 1 1 calc R U H20C H 0.7539 0.3592 0.2452 0.122 Uiso 1 1 calc R U C21 C 0.51150(16) 0.33173(11) 0.14344(9) 0.0264(4) Uani 1 1 d . . C22 C 0.58477(17) 0.27260(11) 0.12087(10) 0.0321(4) Uani 1 1 d . . C23 C 0.66633(19) 0.29458(13) 0.07773(12) 0.0392(5) Uani 1 1 d . . H23 H 0.7177 0.2558 0.0627 0.047 Uiso 1 1 calc R U C24 C 0.6739(2) 0.37163(14) 0.05640(12) 0.0453(5) Uani 1 1 d . . H24 H 0.7291 0.3852 0.0263 0.054 Uiso 1 1 calc R U C25 C 0.6015(2) 0.42937(13) 0.07865(12) 0.0427(5) Uani 1 1 d . . H25 H 0.6075 0.4822 0.0634 0.051 Uiso 1 1 calc R U C26 C 0.52038(18) 0.41144(11) 0.12286(10) 0.0312(4) Uani 1 1 d . . C27 C 0.5781(2) 0.18722(13) 0.14291(14) 0.0474(6) Uani 1 1 d . . H27 H 0.5043 0.1814 0.1654 0.057 Uiso 1 1 calc R U C28 C 0.6927(3) 0.16512(18) 0.19804(15) 0.0741(9) Uani 1 1 d . . H28A H 0.7659 0.1668 0.1764 0.111 Uiso 1 1 calc R U H28B H 0.6827 0.1118 0.2156 0.111 Uiso 1 1 calc R U H28C H 0.7029 0.2026 0.2374 0.111 Uiso 1 1 calc R U C29 C 0.5617(3) 0.13096(15) 0.07993(17) 0.0621(7) Uani 1 1 d . . H29A H 0.4894 0.1470 0.0445 0.093 Uiso 1 1 calc R U H29B H 0.5495 0.0772 0.0959 0.093 Uiso 1 1 calc R U H29C H 0.6357 0.1326 0.0590 0.093 Uiso 1 1 calc R U C30 C 0.4430(2) 0.47375(11) 0.15013(11) 0.0371(4) Uani 1 1 d . . H30 H 0.4435 0.4611 0.2008 0.045 Uiso 1 1 calc R U C31 C 0.4939(3) 0.55765(13) 0.14784(14) 0.0565(6) Uani 1 1 d . . H31A H 0.5810 0.5587 0.1717 0.085 Uiso 1 1 calc R U H31B H 0.4463 0.5937 0.1718 0.085 Uiso 1 1 calc R U H31C H 0.4869 0.5741 0.0985 0.085 Uiso 1 1 calc R U C32 C 0.3095(2) 0.47065(15) 0.11103(14) 0.0525(6) Uani 1 1 d . . H32A H 0.3052 0.4840 0.0612 0.079 Uiso 1 1 calc R U H32B H 0.2603 0.5085 0.1321 0.079 Uiso 1 1 calc R U H32C H 0.2767 0.4174 0.1145 0.079 Uiso 1 1 calc R U loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cr1 0.01904(14) 0.02417(14) 0.02550(15) 0.00549(10) 0.00422(10) -0.00060(10) Si1 0.0300(3) 0.0391(3) 0.0338(3) 0.0056(2) -0.0011(2) -0.0085(2) Si2 0.0313(3) 0.0459(3) 0.0332(3) -0.0033(2) 0.0102(2) 0.0022(2) N1 0.0225(7) 0.0269(7) 0.0311(8) 0.0053(6) 0.0040(6) -0.0019(6) N2 0.0245(7) 0.0250(7) 0.0300(8) 0.0051(6) 0.0070(6) 0.0000(6) C1 0.0260(9) 0.0288(9) 0.0312(9) 0.0052(7) 0.0045(7) -0.0038(7) C2 0.0563(15) 0.092(2) 0.0325(12) 0.0067(12) 0.0030(11) -0.0207(14) C3 0.0530(14) 0.0615(16) 0.0541(15) 0.0092(12) -0.0058(12) -0.0285(12) C4 0.0471(15) 0.0649(17) 0.078(2) 0.0017(14) -0.0155(14) 0.0122(12) C5 0.0319(10) 0.0302(9) 0.0361(10) 0.0018(8) 0.0094(8) 0.0025(7) C6 0.0580(15) 0.0574(15) 0.0530(14) 0.0050(11) 0.0298(12) -0.0046(12) C7 0.0546(15) 0.0624(16) 0.0765(18) -0.0106(14) 0.0278(14) 0.0138(13) C8 0.0535(16) 0.112(3) 0.0399(13) -0.0121(15) -0.0004(12) 0.0020(16) C9 0.0227(8) 0.0303(9) 0.0250(8) 0.0011(7) 0.0031(7) 0.0021(7) C10 0.0313(9) 0.0293(9) 0.0309(9) 0.0004(7) 0.0050(8) 0.0040(7) C11 0.0372(11) 0.0352(10) 0.0451(12) 0.0043(9) 0.0000(9) 0.0126(8) C12 0.0247(9) 0.0483(12) 0.0470(12) -0.0056(10) -0.0046(9) 0.0113(9) C13 0.0228(9) 0.0435(11) 0.0495(12) -0.0021(9) 0.0018(8) -0.0002(8) C14 0.0262(9) 0.0361(10) 0.0400(11) 0.0048(8) 0.0013(8) -0.0022(8) C15 0.0371(11) 0.0289(9) 0.0464(12) 0.0078(8) 0.0006(9) -0.0020(8) C16 0.091(3) 0.0468(17) 0.232(5) -0.047(3) 0.066(3) -0.0234(17) C17 0.093(3) 0.146(4) 0.093(3) -0.017(2) 0.042(2) -0.067(3) C18 0.0286(11) 0.0473(13) 0.0890(19) 0.0291(13) -0.0118(11) -0.0129(9) C19 0.0675(19) 0.0356(13) 0.142(3) 0.0110(17) 0.025(2) 0.0027(13) C20 0.079(2) 0.088(2) 0.0681(19) 0.0329(17) -0.0087(16) -0.0385(18) C21 0.0238(8) 0.0312(9) 0.0242(8) 0.0038(7) 0.0052(7) -0.0031(7) C22 0.0270(9) 0.0344(10) 0.0365(10) 0.0050(8) 0.0101(8) 0.0018(7) C23 0.0337(10) 0.0434(11) 0.0447(12) 0.0015(9) 0.0180(9) 0.0020(9) C24 0.0455(12) 0.0512(13) 0.0464(12) 0.0047(10) 0.0265(10) -0.0090(10) C25 0.0531(13) 0.0368(11) 0.0429(12) 0.0078(9) 0.0207(10) -0.0079(9) C26 0.0339(10) 0.0315(9) 0.0286(9) 0.0041(7) 0.0072(8) -0.0036(8) C27 0.0490(13) 0.0355(11) 0.0679(15) 0.0127(10) 0.0364(12) 0.0129(9) C28 0.109(3) 0.0582(17) 0.0541(16) 0.0141(13) 0.0145(16) 0.0364(17) C29 0.0615(16) 0.0376(12) 0.088(2) -0.0026(13) 0.0173(15) -0.0029(11) C30 0.0500(12) 0.0286(9) 0.0352(10) 0.0063(8) 0.0140(9) 0.0002(8) C31 0.0809(18) 0.0322(11) 0.0615(15) 0.0027(10) 0.0264(14) -0.0035(11) C32 0.0523(14) 0.0469(13) 0.0587(15) 0.0103(11) 0.0119(12) 0.0126(11) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N1 Cr1 N2 113.85(7) N1 Cr1 C5 104.84(8) N2 Cr1 C5 106.89(8) N1 Cr1 C1 106.74(7) N2 Cr1 C1 106.03(8) C5 Cr1 C1 118.82(8) C4 Si1 C2 109.42(15) C4 Si1 C1 112.75(11) C2 Si1 C1 109.56(10) C4 Si1 C3 108.37(14) C2 Si1 C3 108.40(13) C1 Si1 C3 108.24(10) C8 Si2 C6 108.69(14) C8 Si2 C5 110.03(11) C6 Si2 C5 112.71(10) C8 Si2 C7 108.71(14) C6 Si2 C7 108.06(13) C5 Si2 C7 108.56(11) C9 N1 Cr1 158.57(13) C21 N2 Cr1 158.45(13) Si1 C1 Cr1 116.38(9) Si1 C1 H1A 108.2 Cr1 C1 H1A 108.2 Si1 C1 H1B 108.2 Cr1 C1 H1B 108.2 H1A C1 H1B 107.3 Si1 C2 H2A 109.5 Si1 C2 H2B 109.5 H2A C2 H2B 109.5 Si1 C2 H2C 109.5 H2A C2 H2C 109.5 H2B C2 H2C 109.5 Si1 C3 H3A 109.5 Si1 C3 H3B 109.5 H3A C3 H3B 109.5 Si1 C3 H3C 109.5 H3A C3 H3C 109.5 H3B C3 H3C 109.5 Si1 C4 H4A 109.5 Si1 C4 H4B 109.5 H4A C4 H4B 109.5 Si1 C4 H4C 109.5 H4A C4 H4C 109.5 H4B C4 H4C 109.5 Si2 C5 Cr1 116.26(10) Si2 C5 H5A 108.2 Cr1 C5 H5A 108.2 Si2 C5 H5B 108.2 Cr1 C5 H5B 108.2 H5A C5 H5B 107.4 Si2 C6 H6A 109.5 Si2 C6 H6B 109.5 H6A C6 H6B 109.5 Si2 C6 H6C 109.5 H6A C6 H6C 109.5 H6B C6 H6C 109.5 Si2 C7 H7A 109.5 Si2 C7 H7B 109.5 H7A C7 H7B 109.5 Si2 C7 H7C 109.5 H7A C7 H7C 109.5 H7B C7 H7C 109.5 Si2 C8 H8A 109.5 Si2 C8 H8B 109.5 H8A C8 H8B 109.5 Si2 C8 H8C 109.5 H8A C8 H8C 109.5 H8B C8 H8C 109.5 N1 C9 C14 121.23(16) N1 C9 C10 117.80(16) C14 C9 C10 120.97(16) C11 C10 C9 117.89(18) C11 C10 C15 121.66(18) C9 C10 C15 120.44(16) C12 C11 C10 121.49(19) C12 C11 H11 119.3 C10 C11 H11 119.3 C13 C12 C11 119.97(18) C13 C12 H12 120.0 C11 C12 H12 120.0 C12 C13 C14 121.58(19) C12 C13 H13 119.2 C14 C13 H13 119.2 C13 C14 C9 118.09(18) C13 C14 C18 119.78(18) C9 C14 C18 122.12(17) C16 C15 C17 111.3(3) C16 C15 C10 113.4(2) C17 C15 C10 109.5(2) C16 C15 H15 107.5 C17 C15 H15 107.5 C10 C15 H15 107.5 C15 C16 H16A 109.5 C15 C16 H16B 109.5 H16A C16 H16B 109.5 C15 C16 H16C 109.5 H16A C16 H16C 109.5 H16B C16 H16C 109.5 C15 C17 H17A 109.5 C15 C17 H17B 109.5 H17A C17 H17B 109.5 C15 C17 H17C 109.5 H17A C17 H17C 109.5 H17B C17 H17C 109.5 C14 C18 C20 112.1(2) C14 C18 C19 110.2(2) C20 C18 C19 110.7(2) C14 C18 H18 107.9 C20 C18 H18 107.9 C19 C18 H18 107.9 C18 C19 H19A 109.5 C18 C19 H19B 109.5 H19A C19 H19B 109.5 C18 C19 H19C 109.5 H19A C19 H19C 109.5 H19B C19 H19C 109.5 C18 C20 H20A 109.5 C18 C20 H20B 109.5 H20A C20 H20B 109.5 C18 C20 H20C 109.5 H20A C20 H20C 109.5 H20B C20 H20C 109.5 N2 C21 C22 120.58(16) N2 C21 C26 118.34(16) C22 C21 C26 121.08(16) C23 C22 C21 118.15(18) C23 C22 C27 119.79(18) C21 C22 C27 122.05(17) C24 C23 C22 121.14(19) C24 C23 H23 119.4 C22 C23 H23 119.4 C23 C24 C25 120.40(19) C23 C24 H24 119.8 C25 C24 H24 119.8 C24 C25 C26 121.15(19) C24 C25 H25 119.4 C26 C25 H25 119.4 C25 C26 C21 118.05(18) C25 C26 C30 122.44(18) C21 C26 C30 119.51(16) C22 C27 C29 112.2(2) C22 C27 C28 110.5(2) C29 C27 C28 110.6(2) C22 C27 H27 107.8 C29 C27 H27 107.8 C28 C27 H27 107.8 C27 C28 H28A 109.5 C27 C28 H28B 109.5 H28A C28 H28B 109.5 C27 C28 H28C 109.5 H28A C28 H28C 109.5 H28B C28 H28C 109.5 C27 C29 H29A 109.5 C27 C29 H29B 109.5 H29A C29 H29B 109.5 C27 C29 H29C 109.5 H29A C29 H29C 109.5 H29B C29 H29C 109.5 C32 C30 C26 111.14(18) C32 C30 C31 110.03(19) C26 C30 C31 113.74(18) C32 C30 H30 107.2 C26 C30 H30 107.2 C31 C30 H30 107.2 C30 C31 H31A 109.5 C30 C31 H31B 109.5 H31A C31 H31B 109.5 C30 C31 H31C 109.5 H31A C31 H31C 109.5 H31B C31 H31C 109.5 C30 C32 H32A 109.5 C30 C32 H32B 109.5 H32A C32 H32B 109.5 C30 C32 H32C 109.5 H32A C32 H32C 109.5 H32B C32 H32C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Cr1 N1 1.6496(15) Cr1 N2 1.6522(15) Cr1 C5 2.0113(19) Cr1 C1 2.0182(18) Si1 C4 1.861(3) Si1 C2 1.867(3) Si1 C1 1.8683(18) Si1 C3 1.870(2) Si2 C8 1.862(3) Si2 C6 1.863(3) Si2 C5 1.866(2) Si2 C7 1.868(2) N1 C9 1.382(2) N2 C21 1.384(2) C1 H1A 0.9900 C1 H1B 0.9900 C2 H2A 0.9800 C2 H2B 0.9800 C2 H2C 0.9800 C3 H3A 0.9800 C3 H3B 0.9800 C3 H3C 0.9800 C4 H4A 0.9800 C4 H4B 0.9800 C4 H4C 0.9800 C5 H5A 0.9900 C5 H5B 0.9900 C6 H6A 0.9800 C6 H6B 0.9800 C6 H6C 0.9800 C7 H7A 0.9800 C7 H7B 0.9800 C7 H7C 0.9800 C8 H8A 0.9800 C8 H8B 0.9800 C8 H8C 0.9800 C9 C14 1.415(3) C9 C10 1.416(3) C10 C11 1.388(3) C10 C15 1.516(3) C11 C12 1.383(3) C11 H11 0.9500 C12 C13 1.377(3) C12 H12 0.9500 C13 C14 1.386(3) C13 H13 0.9500 C14 C18 1.519(3) C15 C16 1.495(4) C15 C17 1.512(4) C15 H15 1.0000 C16 H16A 0.9800 C16 H16B 0.9800 C16 H16C 0.9800 C17 H17A 0.9800 C17 H17B 0.9800 C17 H17C 0.9800 C18 C20 1.520(4) C18 C19 1.543(4) C18 H18 1.0000 C19 H19A 0.9800 C19 H19B 0.9800 C19 H19C 0.9800 C20 H20A 0.9800 C20 H20B 0.9800 C20 H20C 0.9800 C21 C22 1.410(3) C21 C26 1.419(2) C22 C23 1.392(3) C22 C27 1.516(3) C23 C24 1.378(3) C23 H23 0.9500 C24 C25 1.385(3) C24 H24 0.9500 C25 C26 1.387(3) C25 H25 0.9500 C26 C30 1.517(3) C27 C29 1.528(4) C27 C28 1.529(4) C27 H27 1.0000 C28 H28A 0.9800 C28 H28B 0.9800 C28 H28C 0.9800 C29 H29A 0.9800 C29 H29B 0.9800 C29 H29C 0.9800 C30 C32 1.517(3) C30 C31 1.534(3) C30 H30 1.0000 C31 H31A 0.9800 C31 H31B 0.9800 C31 H31C 0.9800 C32 H32A 0.9800 C32 H32B 0.9800 C32 H32C 0.9800