#------------------------------------------------------------------------------ #$Date: 2019-11-26 03:43:09 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242529 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/25/4132580.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132580 loop_ _publ_author_name 'Dutta, Indranil' 'Yadav, Sudhir' 'Sarbajna, Abir' 'De, Subhabrata' 'H\"olscher, Markus' 'Leitner, Walter' 'Bera, Jitendra K.' _publ_section_title ; Double Dehydrogenation of Primary Amines to Nitriles by a Ruthenium Complex Featuring Pyrazole Functionality. ; _journal_issue 28 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 8662 _journal_page_last 8666 _journal_paper_doi 10.1021/jacs.8b05009 _journal_volume 140 _journal_year 2018 _chemical_formula_sum 'C26 H31 Cl3 N4 Ru' _chemical_formula_weight 606.97 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 90 _cell_angle_beta 114.5200(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 15.5162(14) _cell_length_b 11.1368(10) _cell_length_c 17.7144(16) _cell_measurement_reflns_used 9865 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 28.41 _cell_measurement_theta_min 2.28 _cell_volume 2785.0(4) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics DIAMOND _computing_publication_material ciftab _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'SHELXL-2014/7 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0245 _diffrn_reflns_av_unetI/netI 0.0178 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 23388 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 24.713 _diffrn_reflns_theta_max 24.713 _diffrn_reflns_theta_min 2.223 _diffrn_source 'fine-focus sealed tube' _exptl_absorpt_coefficient_mu 0.872 _exptl_absorpt_correction_type empirical _exptl_absorpt_process_details '(Bera et al., 2017)' _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.448 _exptl_crystal_description needle _exptl_crystal_F_000 1240 _exptl_crystal_size_max 0.200 _exptl_crystal_size_mid 0.190 _exptl_crystal_size_min 0.180 _exptl_transmission_factor_max 0.850 _exptl_transmission_factor_min 0.836 _refine_diff_density_max 0.645 _refine_diff_density_min -0.622 _refine_diff_density_rms 0.056 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.787 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 313 _refine_ls_number_reflns 4753 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 0.787 _refine_ls_R_factor_all 0.0379 _refine_ls_R_factor_gt 0.0322 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0660P)^2^+4.6582P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0873 _refine_ls_wR_factor_ref 0.0931 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4168 _reflns_number_total 4753 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b05009_si_002.cif _cod_data_source_block compound3 _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 4132580 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. Comments on CHECKCIF alerts: 'Low ’MainMol’ Ueq as Compared to Neighbors of C12..... Check' This is possibly a false alarm for the terminal t-butyl moiety. ; _shelx_estimated_absorpt_t_min 0.845 _shelx_estimated_absorpt_t_max 0.859 _exptl_absorpt_special_details SADABS _shelx_res_file ; C:\Users\user\Desktop\ANIONI~1\4may.res created by SHELXL-2014/7 REM Old TITL 4may_0m in P2(1)/n REM SHELXT solution in P2(1)/n REM R1 0.111, Rweak 0.005, Alpha 0.039, Orientation as input REM Formula found by SHELXT: C26 N5 Cl2 Ru REM indro1_0m_a.res in P2(1)/n REM R1 = 0.0354 for 4168 Fo > 4sig(Fo) and 0.0411 for all 4753 data REM 313 parameters refined using 0 restraints REM Highest difference peak 0.644, deepest hole -0.638, 1-sigma level 0.065 TITL indro1_0m_a.res in P2(1)/n CELL 0.71073 15.5162 11.1368 17.7144 90.000 114.520 90.000 ZERR 4.0000 0.0014 0.0010 0.0016 0.000 0.001 0.000 LATT 1 SYMM 0.5-X, 0.5+Y, 0.5-Z SFAC C H N CL RU UNIT 104 124 16 12 4 MERG 2 OMIT -2 50.1 SHEL 99999.00 0.85 FMAP 2 GRID PLAN 5 TEMP -173 SIZE 0.18 0.19 0.2 BOND $H L.S. 20 ACTA SAME C14 C15 WGHT 0.066000 4.658200 FVAR 0.32826 RU1 5 0.704479 0.614853 0.362737 11.00000 0.03884 0.04500 = 0.04016 -0.00057 0.01485 -0.00143 CL1 4 0.744818 0.406833 0.358366 11.00000 0.05936 0.04691 = 0.05577 -0.00071 0.01816 0.00195 CL1S 4 0.714913 0.188893 0.539766 11.00000 0.15059 0.12745 = 0.10777 0.01762 0.06392 0.00446 CL2S 4 0.536575 0.315591 0.476204 11.00000 0.09615 0.36450 = 0.14183 -0.02581 0.06324 0.00792 N3 3 0.766281 0.608464 0.489287 11.00000 0.04527 0.05305 = 0.04326 -0.00370 0.01934 -0.00437 N2 3 0.852373 0.641683 0.394466 11.00000 0.04002 0.04343 = 0.04577 0.00314 0.01775 -0.00053 N4 3 0.726954 0.603069 0.544228 11.00000 0.05314 0.06006 = 0.04788 -0.00520 0.02551 -0.00745 N1 3 0.835336 0.638638 0.258293 11.00000 0.05809 0.06364 = 0.04863 0.00757 0.02438 0.00485 C8 1 0.908707 0.643656 0.475919 11.00000 0.04365 0.04426 = 0.04513 -0.00096 0.01603 -0.00269 C9 1 0.859627 0.630722 0.528681 11.00000 0.04235 0.04852 = 0.04329 -0.00284 0.01443 -0.00219 C16 1 0.574752 0.675519 0.365960 11.00000 0.04550 0.08417 = 0.05769 0.00027 0.02297 0.01223 AFIX 43 H16 2 0.553231 0.668383 0.408751 11.00000 -1.20000 AFIX 0 C11 1 0.797943 0.621750 0.619525 11.00000 0.06309 0.05657 = 0.04530 -0.00511 0.02491 -0.00232 C7 1 1.007965 0.654051 0.507096 11.00000 0.04480 0.06261 = 0.05299 -0.00257 0.01654 -0.00632 AFIX 43 H7 2 1.045260 0.655795 0.565279 11.00000 -1.20000 AFIX 0 C5 1 0.894245 0.646555 0.339393 11.00000 0.04950 0.04441 = 0.04940 0.00418 0.02371 0.00224 C21 1 0.552745 0.584971 0.306084 11.00000 0.03924 0.07349 = 0.05371 0.00279 0.01284 -0.00619 AFIX 43 H21 2 0.519599 0.515451 0.310408 11.00000 -1.20000 AFIX 0 C19 1 0.632092 0.696927 0.236149 11.00000 0.04718 0.05532 = 0.04609 0.00970 0.01265 0.00854 AFIX 43 H19 2 0.650424 0.706647 0.191575 11.00000 -1.20000 AFIX 0 C18 1 0.658088 0.784479 0.299366 11.00000 0.05130 0.04710 = 0.06578 0.00719 0.01383 0.00429 AFIX 43 H18 2 0.696741 0.849874 0.298024 11.00000 -1.20000 AFIX 0 C4 1 0.993544 0.658666 0.368318 11.00000 0.05317 0.05403 = 0.06473 0.00418 0.03237 0.00294 C17 1 0.628482 0.777767 0.364230 11.00000 0.05689 0.05895 = 0.06205 -0.00677 0.01507 0.01401 C10 1 0.882993 0.639459 0.613418 11.00000 0.05167 0.06389 = 0.04488 -0.00691 0.01552 -0.00592 AFIX 43 H10 2 0.943494 0.654203 0.656986 11.00000 -1.20000 AFIX 0 C20 1 0.579747 0.596276 0.238487 11.00000 0.04440 0.05764 = 0.04682 0.00231 0.00800 0.00586 C6 1 1.049840 0.661514 0.454123 11.00000 0.04141 0.06945 = 0.06947 0.00145 0.02190 -0.00499 AFIX 43 H6 2 1.116728 0.668625 0.474600 11.00000 -1.20000 AFIX 0 C22 1 0.552024 0.496885 0.174639 11.00000 0.07009 0.06025 = 0.04870 -0.00290 0.00680 0.00286 AFIX 13 H22 2 0.563743 0.418849 0.205217 11.00000 -1.20000 AFIX 0 C1 1 0.874010 0.645315 0.204778 11.00000 0.07852 0.07427 = 0.05265 0.00925 0.03493 0.01163 AFIX 43 H1 2 0.833163 0.640084 0.147438 11.00000 -1.20000 AFIX 0 C12 1 0.777203 0.629512 0.696178 11.00000 0.07586 0.07920 = 0.05384 -0.01047 0.03796 -0.00246 C3 1 1.030304 0.664955 0.308014 11.00000 0.05994 0.08970 = 0.07822 0.00755 0.04161 0.00312 AFIX 43 H3 2 1.096580 0.672979 0.324295 11.00000 -1.20000 AFIX 0 C23 1 0.445599 0.505486 0.120608 11.00000 0.07281 0.11105 = 0.07465 -0.02478 -0.00220 -0.01555 AFIX 137 H23A 2 0.410878 0.499085 0.155722 11.00000 -1.50000 H23B 2 0.426400 0.440090 0.079922 11.00000 -1.50000 H23C 2 0.431343 0.582794 0.091566 11.00000 -1.50000 AFIX 0 C24 1 0.608220 0.495417 0.122783 11.00000 0.09754 0.09464 = 0.06939 -0.01959 0.02657 0.00963 AFIX 137 H24A 2 0.589793 0.564062 0.084741 11.00000 -1.50000 H24B 2 0.595479 0.420683 0.090766 11.00000 -1.50000 H24C 2 0.675948 0.500550 0.159107 11.00000 -1.50000 AFIX 0 C2 1 0.970429 0.659481 0.226336 11.00000 0.08302 0.09468 = 0.07464 0.01187 0.05479 0.01142 AFIX 43 H2 2 0.993932 0.665213 0.184758 11.00000 -1.20000 AFIX 0 C1S 1 0.654155 0.321504 0.501512 11.00000 0.11256 0.10379 = 0.12970 -0.02226 0.07868 -0.01971 AFIX 23 H1S1 2 0.682283 0.385156 0.543666 11.00000 -1.20000 H1S2 2 0.663626 0.345116 0.451607 11.00000 -1.20000 AFIX 0 C14 1 0.705696 0.535700 0.692071 11.00000 0.18974 0.14270 = 0.09744 -0.00514 0.09897 -0.04126 AFIX 137 H14A 2 0.733941 0.455760 0.697033 11.00000 -1.50000 H14B 2 0.650182 0.542009 0.638912 11.00000 -1.50000 H14C 2 0.686360 0.548186 0.737592 11.00000 -1.50000 AFIX 0 C25 1 0.656148 0.870700 0.432769 11.00000 0.11043 0.07166 = 0.08525 -0.02314 0.02578 0.01879 AFIX 137 H25A 2 0.713587 0.912526 0.437100 11.00000 -1.50000 H25B 2 0.668188 0.830858 0.485530 11.00000 -1.50000 H25C 2 0.604560 0.928809 0.419996 11.00000 -1.50000 AFIX 0 C13 1 0.730385 0.748274 0.693617 11.00000 0.31336 0.10401 = 0.16550 0.00181 0.18459 0.04450 AFIX 137 H13A 2 0.694847 0.744424 0.728160 11.00000 -1.50000 H13B 2 0.686957 0.766842 0.636279 11.00000 -1.50000 H13C 2 0.778777 0.811117 0.714739 11.00000 -1.50000 AFIX 0 C15 1 0.864703 0.612768 0.772329 11.00000 0.10016 0.47055 = 0.04173 -0.02837 0.02997 0.02898 AFIX 137 H15A 2 0.895656 0.537869 0.768257 11.00000 -1.50000 H15B 2 0.848938 0.608902 0.820420 11.00000 -1.50000 H15C 2 0.907626 0.680414 0.778882 11.00000 -1.50000 AFIX 0 HKLF 4 REM indro1_0m_a.res in P2(1)/n REM R1 = 0.0322 for 4168 Fo > 4sig(Fo) and 0.0379 for all 4753 data REM 313 parameters refined using 1 restraints END WGHT 0.0451 2.4740 REM Highest difference peak 0.645, deepest hole -0.622, 1-sigma level 0.056 Q1 1 0.6411 0.1797 0.5128 11.00000 0.05 0.65 Q2 1 0.5383 0.2079 0.4852 11.00000 0.05 0.55 Q3 1 0.7248 0.2612 0.5688 11.00000 0.05 0.48 Q4 1 0.5566 0.3410 0.4594 11.00000 0.05 0.37 Q5 1 0.7843 0.5146 0.7341 11.00000 0.05 0.31 ; _shelx_res_checksum 3740 _shelx_hkl_file ; -2 0 0 3459.35 73.29 -2 0 0 3446.26 74.79 2 0 0 3554.74 73.79 2 0 0 3555.44 73.29 2 0 0 3615.14 74.59 -2 0 0 3549.15 73.89 3 0 0 0.10 0.20 3 0 0 0.10 0.30 3 0 0 -0.10 0.30 -3 0 0 0.60 0.40 -4 0 0 755.12 16.30 4 0 0 773.12 16.10 -4 0 0 751.52 16.60 5 0 0 0.20 0.40 5 0 0 0.80 0.50 -5 0 0 0.80 0.40 -5 0 0 0.40 0.50 -6 0 0 24.70 1.70 6 0 0 28.00 1.40 -6 0 0 25.70 1.50 -7 0 0 -0.40 0.60 7 0 0 0.20 0.70 -7 0 0 0.20 0.70 8 0 0 28.70 1.80 -8 0 0 28.30 2.10 -8 0 0 27.10 1.80 -9 0 0 0.10 1.00 -9 0 0 -0.60 0.80 9 0 0 -0.50 0.90 -10 0 0 43.40 2.90 -10 0 0 45.10 2.60 10 0 0 42.20 2.40 -11 0 0 -0.50 1.00 -11 0 0 -2.10 1.20 11 0 0 0.50 1.20 12 0 0 341.77 9.00 13 0 0 -1.00 1.70 -13 0 0 0.50 1.40 13 0 0 1.00 1.90 14 0 0 73.49 4.20 -14 0 0 77.69 4.30 14 0 0 84.39 6.10 15 0 0 -2.30 2.50 -15 0 0 0.10 1.80 15 0 0 -0.70 2.40 16 0 0 1.60 2.70 -16 0 0 3.90 2.10 16 0 0 -2.30 2.90 17 0 0 2.40 3.20 -17 0 0 2.40 2.40 18 0 0 18.00 4.30 -1 -1 0 52.79 1.40 1 -1 0 65.99 1.80 -1 -1 0 59.19 1.60 1 -1 0 61.49 1.60 -1 -1 0 59.59 1.50 -1 1 0 60.79 1.50 1 1 0 61.09 1.50 -1 1 0 65.79 1.60 -2 -1 0 61.19 1.70 2 -1 0 59.99 1.60 -2 -1 0 59.39 1.60 2 -1 0 60.99 1.60 -2 1 0 59.09 1.60 -2 1 0 60.79 1.80 2 1 0 61.09 1.70 2 1 0 61.89 1.70 2 1 0 59.49 1.70 -2 1 0 61.29 1.60 2 1 0 59.69 1.60 3 -1 0 0.30 0.50 -3 -1 0 1.70 0.50 -3 -1 0 0.50 0.30 3 -1 0 0.70 0.30 -3 -1 0 0.90 0.30 3 1 0 1.10 0.40 -3 1 0 1.00 0.50 -3 1 0 1.30 0.40 -3 1 0 0.10 0.30 3 1 0 0.30 0.40 3 1 0 0.50 0.30 -4 -1 0 154.48 3.70 -4 -1 0 151.28 4.00 4 -1 0 133.19 3.60 -4 -1 0 151.98 3.90 4 -1 0 151.88 3.70 4 1 0 146.59 3.60 -4 1 0 142.29 3.70 -4 1 0 151.58 4.20 -4 1 0 143.79 3.70 -5 -1 0 460.65 10.30 5 -1 0 481.25 10.40 -5 -1 0 470.45 10.90 -5 -1 0 460.05 10.60 -5 1 0 464.05 10.40 -5 1 0 462.85 11.00 6 -1 0 351.76 8.00 -6 -1 0 332.17 8.60 -6 -1 0 348.47 7.90 -6 -1 0 348.37 8.20 -6 1 0 341.67 8.70 -6 1 0 336.17 8.10 -7 -1 0 1865.41 39.40 -7 -1 0 1865.21 38.90 7 -1 0 1876.11 39.10 -7 -1 0 1833.62 39.90 -7 1 0 1828.82 40.00 -7 1 0 1873.61 39.20 8 -1 0 151.38 4.30 -8 -1 0 144.49 4.90 -8 -1 0 144.49 4.10 -8 -1 0 140.59 4.40 -8 1 0 144.99 4.60 -8 1 0 143.69 5.00 -9 -1 0 6.00 1.20 9 -1 0 4.70 1.10 -9 1 0 5.60 1.40 -9 1 0 4.50 1.10 10 -1 0 29.40 2.10 -10 -1 0 26.80 2.20 -10 1 0 25.80 2.10 -10 1 0 29.90 2.60 10 1 0 27.50 2.20 11 -1 0 2.60 1.30 -11 -1 0 2.60 1.20 -11 1 0 0.90 1.60 11 1 0 2.00 1.30 -11 1 0 2.70 1.20 11 1 0 0.00 1.50 12 -1 0 5.70 1.60 -12 -1 0 5.70 1.50 -12 1 0 6.50 1.50 -12 1 0 9.90 2.20 12 1 0 7.50 1.90 12 1 0 4.70 1.70 13 -1 0 43.60 3.20 -13 -1 0 42.80 3.00 13 1 0 36.80 3.30 -13 1 0 39.80 3.10 13 1 0 47.20 3.80 14 -1 0 81.19 4.30 -14 -1 0 97.19 4.50 14 1 0 82.79 4.30 -14 1 0 93.79 4.50 14 1 0 79.59 5.30 15 -1 0 57.09 5.20 15 -1 0 65.89 4.60 -15 -1 0 54.39 4.30 15 1 0 62.99 5.00 -15 1 0 57.79 4.30 15 1 0 58.69 5.10 16 -1 0 61.39 5.20 -16 -1 0 64.39 4.50 16 -1 0 76.09 5.90 -16 1 0 62.19 4.80 16 1 0 64.09 5.50 16 1 0 58.09 5.60 17 -1 0 21.30 4.60 -17 -1 0 21.60 3.30 -17 1 0 27.20 4.10 17 1 0 30.70 5.50 -18 -1 0 10.40 3.10 18 -1 0 7.90 4.00 -18 1 0 15.00 3.40 0 -2 0 842.12 17.70 0 -2 0 835.32 17.60 0 2 0 805.32 17.60 0 2 0 816.02 17.70 -1 -2 0 8923.91 185.58 1 -2 0 8668.03 185.48 1 -2 0 8979.80 183.78 1 -2 0 8689.93 183.28 1 2 0 8997.40 184.48 1 2 0 8832.82 186.98 -1 2 0 8508.15 183.48 1 2 0 8920.81 183.68 -1 2 0 9130.59 184.18 -2 -2 0 49.50 1.60 -2 -2 0 51.79 1.50 2 -2 0 52.79 1.70 2 -2 0 53.69 1.60 -2 -2 0 46.20 1.60 2 -2 0 56.79 1.60 -2 2 0 53.59 1.70 2 2 0 49.80 1.60 2 2 0 48.50 1.40 -2 2 0 54.99 1.60 2 2 0 49.00 1.70 -3 -2 0 235.98 5.50 3 -2 0 222.28 5.20 3 -2 0 232.88 5.30 -3 -2 0 225.18 5.30 3 2 0 213.08 5.50 -3 2 0 232.38 5.60 -3 2 0 223.78 5.20 3 2 0 218.38 5.30 3 2 0 232.78 5.30 4 -2 0 97.49 2.70 -4 -2 0 93.89 2.80 -4 -2 0 86.99 2.60 -4 2 0 88.09 3.00 4 2 0 95.69 2.80 -4 2 0 93.19 2.60 -5 -2 0 110.09 3.30 -5 -2 0 114.69 3.20 5 -2 0 113.69 3.20 -5 2 0 110.49 3.70 5 2 0 109.99 3.40 -5 2 0 110.89 3.10 6 -2 0 362.96 8.30 -6 -2 0 363.66 8.20 -6 -2 0 336.97 8.40 -6 2 0 345.77 8.30 -6 2 0 350.76 9.00 6 2 0 343.57 8.60 -7 -2 0 8.10 1.10 -7 -2 0 8.20 1.20 7 -2 0 9.50 1.20 -7 2 0 10.10 1.20 7 2 0 7.90 1.30 -7 2 0 10.00 1.50 -8 -2 0 51.69 2.50 8 -2 0 56.89 2.30 -8 -2 0 54.69 2.30 8 2 0 58.49 2.80 -8 2 0 53.49 2.40 -8 2 0 57.09 3.10 -9 -2 0 889.01 20.50 -9 -2 0 928.71 20.10 9 -2 0 924.81 20.10 9 2 0 910.11 21.00 -9 2 0 920.71 20.40 -9 2 0 900.81 21.40 -10 -2 0 3.00 1.10 -10 -2 0 3.60 1.00 10 -2 0 3.80 1.10 -10 2 0 2.10 1.20 10 2 0 2.50 1.30 11 -2 0 565.84 13.00 -11 -2 0 536.55 12.80 -11 2 0 542.55 13.20 11 2 0 547.35 15.20 -11 2 0 527.45 14.50 12 -2 0 1.20 1.40 -12 -2 0 0.10 1.20 12 2 0 -1.30 1.60 -12 2 0 1.40 1.60 -12 2 0 -0.30 1.30 -13 -2 0 319.47 9.20 13 -2 0 318.47 8.60 13 2 0 316.37 10.00 -13 2 0 313.07 10.40 -13 2 0 316.47 9.00 13 2 0 304.67 8.80 14 -2 0 1.10 2.00 -14 -2 0 0.50 1.70 -14 2 0 0.40 1.60 14 2 0 3.10 2.20 14 2 0 -0.70 2.10 15 -2 0 77.79 4.40 15 -2 0 81.49 6.00 -15 -2 0 78.59 4.70 -15 2 0 78.49 4.60 15 2 0 84.19 5.50 15 2 0 71.49 4.60 -16 -2 0 1.80 2.20 16 -2 0 -0.10 2.50 16 -2 0 2.40 3.00 16 2 0 2.50 3.00 16 2 0 3.30 2.90 -16 2 0 3.70 2.40 -17 -2 0 -1.10 2.30 17 -2 0 6.50 3.50 17 2 0 -4.00 3.00 -17 2 0 -0.30 2.60 18 -2 0 -2.70 3.80 -18 -2 0 -0.20 2.90 18 2 0 4.70 3.90 -18 2 0 0.90 2.90 0 -3 0 1.00 0.40 0 -3 0 0.90 0.30 0 3 0 0.70 0.30 1 -3 0 2751.82 59.79 1 -3 0 2875.51 59.39 -1 -3 0 2852.61 59.59 -1 3 0 2891.01 60.39 1 3 0 2922.71 60.79 -1 3 0 2653.13 59.49 2 -3 0 3.90 0.60 -2 -3 0 3.30 0.60 2 -3 0 3.60 0.60 -2 -3 0 4.40 0.50 -2 3 0 4.70 0.70 -2 3 0 3.70 0.70 2 3 0 3.60 0.70 -3 -3 0 10.40 0.80 3 -3 0 11.10 0.90 -3 -3 0 11.00 0.90 -3 -3 0 9.80 0.90 -3 3 0 10.10 1.00 3 3 0 8.90 0.70 -3 3 0 11.50 0.80 -4 -3 0 263.07 6.40 4 -3 0 272.07 6.40 -4 -3 0 271.07 6.60 -4 3 0 264.97 6.30 4 3 0 260.77 6.40 4 3 0 260.07 6.30 -4 3 0 265.97 6.80 -5 -3 0 111.69 3.50 5 -3 0 112.99 3.30 -5 -3 0 112.39 3.30 -5 3 0 110.79 3.20 5 3 0 112.49 3.30 -5 3 0 105.29 4.00 6 -3 0 1677.93 36.70 -6 -3 0 1763.72 36.70 -6 -3 0 1751.82 37.00 -6 3 0 1746.23 37.60 6 3 0 1744.53 36.90 -6 3 0 1743.43 36.70 -7 -3 0 431.66 10.00 7 -3 0 418.26 10.00 -7 -3 0 423.86 10.30 -7 3 0 432.66 11.00 7 3 0 422.86 10.30 -7 3 0 416.56 10.00 -8 -3 0 287.47 7.60 8 -3 0 284.57 7.20 -8 -3 0 284.97 7.20 -8 3 0 282.87 7.30 8 3 0 284.47 7.70 -8 3 0 273.27 8.20 -9 -3 0 0.70 1.00 -9 -3 0 0.30 1.00 9 -3 0 0.20 0.90 -9 3 0 0.50 1.10 -9 3 0 0.00 0.90 9 3 0 1.40 1.20 -10 -3 0 1.00 1.10 -10 -3 0 0.00 0.90 10 -3 0 2.30 1.10 10 3 0 1.60 1.30 -10 3 0 -1.00 1.30 -10 3 0 1.30 1.10 -11 -3 0 8.40 1.50 -11 -3 0 5.00 1.40 11 -3 0 6.60 1.50 -11 3 0 6.50 1.50 11 3 0 6.50 1.70 -11 3 0 5.60 1.90 12 -3 0 35.00 2.90 -12 -3 0 30.00 2.70 -12 -3 0 33.50 2.70 -12 3 0 27.00 2.70 12 3 0 37.80 3.30 -12 3 0 41.40 3.60 -13 -3 0 19.70 2.60 -13 -3 0 25.10 2.70 13 -3 0 25.20 3.00 13 3 0 22.90 3.00 -13 3 0 24.10 2.80 -13 3 0 21.70 3.50 14 -3 0 79.59 4.30 -14 -3 0 69.99 4.30 14 3 0 76.49 4.70 14 3 0 68.59 5.00 -14 3 0 77.09 4.10 -14 3 0 79.09 5.40 -15 -3 0 35.40 3.80 15 3 0 40.20 4.80 -15 3 0 37.80 3.70 -16 -3 0 56.09 4.60 16 -3 0 54.29 4.70 16 -3 0 68.19 6.20 16 3 0 44.40 6.20 16 3 0 59.29 5.70 -16 3 0 56.49 4.50 -17 -3 0 19.50 3.40 -17 3 0 28.90 4.80 17 3 0 20.60 4.30 -18 -3 0 22.90 3.70 18 -3 0 31.70 5.40 18 3 0 28.90 5.00 -18 3 0 27.30 3.90 0 -4 0 9912.21 206.98 0 -4 0 9999.00 204.18 0 4 0 9744.12 204.48 0 4 0 9871.51 207.68 -1 -4 0 18.00 1.20 1 -4 0 20.00 1.20 1 -4 0 17.00 1.00 -1 4 0 16.00 1.00 1 4 0 17.20 1.30 -1 4 0 16.50 1.30 2 -4 0 1777.62 37.30 -2 -4 0 1733.23 37.30 -2 4 0 1816.12 37.20 -2 4 0 1751.82 37.10 2 4 0 1769.82 37.60 -3 -4 0 36.20 1.40 -3 -4 0 33.50 1.70 3 -4 0 32.20 1.60 3 4 0 33.50 1.20 -3 4 0 30.30 1.60 -3 4 0 31.60 1.60 4 -4 0 382.76 9.10 -4 -4 0 388.66 9.20 -4 -4 0 395.46 9.20 4 4 0 395.96 8.70 -4 4 0 388.96 9.00 -4 4 0 379.06 9.40 -5 -4 0 1.20 0.70 5 -4 0 1.10 0.70 -5 -4 0 2.80 0.80 -5 4 0 2.60 0.90 5 4 0 1.50 0.60 -5 4 0 2.30 0.70 -6 -4 0 0.00 0.60 -6 -4 0 0.30 0.80 6 -4 0 -0.10 0.60 -6 4 0 1.00 0.80 6 4 0 -0.10 0.70 -6 4 0 0.80 0.90 -7 -4 0 343.77 8.80 7 -4 0 333.17 8.40 -7 -4 0 338.17 8.40 -7 4 0 330.97 8.30 7 4 0 342.17 8.50 -7 4 0 337.87 9.30 8 -4 0 24.70 1.90 -8 -4 0 24.10 2.10 -8 -4 0 25.50 1.90 -8 4 0 24.60 2.00 8 4 0 27.60 2.00 -8 4 0 27.60 2.40 9 -4 0 25.40 2.10 -9 -4 0 23.30 2.20 -9 -4 0 27.30 2.00 -9 4 0 24.20 2.70 -9 4 0 23.00 2.10 9 4 0 25.10 2.20 -10 -4 0 215.38 6.70 10 -4 0 224.08 6.40 -10 -4 0 220.38 6.30 -10 4 0 212.68 7.40 -10 4 0 214.98 6.40 10 4 0 223.08 6.80 -11 -4 0 29.00 2.50 -11 -4 0 29.40 2.50 11 -4 0 30.10 2.70 11 4 0 34.00 3.00 -11 4 0 31.50 3.20 -11 4 0 30.50 2.80 -12 -4 0 104.49 4.30 12 -4 0 99.69 4.30 -12 -4 0 103.99 4.50 -12 4 0 105.99 4.50 -12 4 0 101.89 5.30 12 4 0 99.99 4.80 13 -4 0 21.70 3.00 -13 -4 0 27.70 3.00 -13 -4 0 21.90 2.90 13 4 0 21.50 3.50 -13 4 0 26.90 3.00 -13 4 0 25.40 3.90 14 -4 0 46.70 4.20 -14 -4 0 50.29 3.80 -14 -4 0 59.19 4.30 -14 4 0 49.90 4.90 -14 4 0 52.99 3.60 14 4 0 48.20 4.50 15 -4 0 3.30 2.10 -15 4 0 2.90 2.10 15 4 0 1.30 2.90 -15 4 0 5.60 2.80 16 -4 0 -0.60 2.60 -16 -4 0 -3.10 2.10 -16 4 0 0.80 2.40 16 4 0 1.00 3.80 16 4 0 -2.30 3.00 -17 -4 0 0.50 2.40 17 -4 0 1.40 3.80 17 4 0 9.00 3.60 -17 4 0 1.50 2.80 18 -4 0 16.60 5.20 -18 -4 0 9.00 3.20 18 4 0 7.20 4.20 0 -5 0 -0.30 0.40 0 -5 0 -0.20 0.60 0 5 0 0.40 0.50 1 -5 0 4.00 0.90 1 5 0 6.00 1.20 -1 5 0 3.60 0.70 2 -5 0 411.86 10.00 -2 -5 0 429.76 10.10 -2 5 0 403.46 9.90 2 5 0 444.46 10.40 -2 5 0 412.66 9.70 3 -5 0 260.97 6.80 -3 -5 0 252.67 6.80 -3 5 0 283.57 6.80 3 5 0 243.98 7.10 -3 5 0 269.37 6.80 4 -5 0 3.80 0.90 -4 -5 0 3.00 0.90 -4 5 0 3.20 0.90 -4 5 0 2.20 0.90 4 5 0 3.40 1.10 4 5 0 3.80 0.60 5 -5 0 1020.80 22.40 -5 -5 0 987.50 22.40 5 5 0 1048.50 21.80 -5 5 0 1022.90 22.20 -5 5 0 1008.10 22.80 -6 -5 0 353.66 9.10 6 -5 0 354.76 8.90 -6 -5 0 355.46 9.00 -6 5 0 363.86 8.80 -6 5 0 368.46 9.60 6 5 0 352.86 8.50 -7 -5 0 621.24 14.70 7 -5 0 622.74 14.60 -7 -5 0 623.54 14.90 -7 5 0 642.44 15.70 -7 5 0 637.54 14.50 7 5 0 647.34 14.40 -8 -5 0 41.00 2.50 8 -5 0 38.20 2.40 -8 -5 0 41.50 2.50 -8 5 0 43.00 2.40 -8 5 0 42.70 3.00 8 5 0 42.80 2.40 9 -5 0 162.38 5.20 -9 -5 0 170.38 5.40 -9 -5 0 163.78 5.50 -9 5 0 159.48 6.10 -9 5 0 169.08 5.30 9 5 0 168.38 5.30 -10 -5 0 4.30 1.30 10 -5 0 4.20 1.30 -10 -5 0 2.70 1.10 -10 5 0 3.60 1.50 -10 5 0 3.50 1.70 10 5 0 3.60 1.60 -11 -5 0 1.50 1.40 11 -5 0 0.00 1.30 -11 -5 0 0.20 1.10 -11 5 0 1.70 1.70 -11 5 0 0.00 2.00 11 5 0 0.60 1.70 -12 -5 0 5.90 1.80 12 -5 0 5.20 1.60 -12 -5 0 5.40 1.60 -12 5 0 6.60 2.50 -12 5 0 7.10 1.90 12 5 0 4.20 2.00 -13 -5 0 12.40 2.10 -13 -5 0 10.90 2.10 13 -5 0 17.50 2.90 -13 5 0 12.80 3.10 13 5 0 11.60 2.50 -13 5 0 12.00 2.10 -14 -5 0 14.80 2.50 -14 -5 0 17.30 3.20 14 -5 0 19.30 3.30 -14 5 0 17.60 3.70 14 5 0 14.70 3.00 -14 5 0 15.00 2.40 -15 -5 0 44.10 3.90 -15 -5 0 37.30 3.80 15 -5 0 44.80 3.80 -15 5 0 36.60 3.80 15 5 0 28.10 3.80 -15 5 0 34.70 5.60 -16 -5 0 12.30 2.70 16 -5 0 10.50 3.60 -16 5 0 15.30 3.20 16 5 0 10.70 3.50 17 -5 0 26.10 4.90 17 5 0 26.10 4.40 0 -6 0 74.99 3.00 0 -6 0 70.89 2.30 0 6 0 73.79 3.10 0 6 0 83.19 2.40 -1 -6 0 1571.04 33.70 1 -6 0 1562.94 33.70 -1 6 0 1538.95 33.60 1 6 0 1544.75 33.80 -1 6 0 1607.64 33.10 -2 -6 0 1179.18 25.50 2 -6 0 1142.29 25.30 -2 6 0 1160.58 24.90 -2 6 0 1140.99 25.30 2 6 0 1158.18 25.70 -3 -6 0 52.79 2.50 3 -6 0 53.19 2.50 3 6 0 53.79 2.90 -3 6 0 53.09 2.60 -3 6 0 49.80 2.40 -4 -6 0 239.08 6.70 4 -6 0 233.38 6.50 -4 6 0 239.58 6.60 4 6 0 235.58 7.10 -4 6 0 231.08 6.30 5 -6 0 17.90 1.70 -5 -6 0 21.30 1.90 5 6 0 14.30 2.10 -5 6 0 19.10 1.70 -5 6 0 17.40 1.90 5 6 0 16.70 1.20 -6 -6 0 133.59 4.60 6 -6 0 134.29 4.50 -6 6 0 134.29 4.90 6 6 0 140.79 5.20 6 6 0 143.09 3.90 -6 6 0 125.39 4.20 7 -6 0 52.89 2.80 -7 -6 0 57.19 2.90 -7 6 0 48.00 2.70 -7 6 0 55.79 3.30 7 6 0 48.60 2.30 8 -6 0 4.20 1.30 -8 -6 0 3.60 1.30 -8 -6 0 2.90 1.10 8 6 0 1.30 1.00 -8 6 0 3.00 1.60 -8 6 0 3.40 1.20 -9 -6 0 165.08 5.60 9 -6 0 163.98 5.40 -9 -6 0 162.68 5.60 9 6 0 166.78 5.30 -9 6 0 170.68 5.50 -9 6 0 161.48 6.30 -10 -6 0 2.40 1.50 10 -6 0 3.00 1.40 -10 -6 0 3.50 1.10 -10 6 0 3.50 1.90 10 6 0 0.70 1.40 -10 6 0 4.70 1.50 -11 -6 0 190.48 6.40 11 -6 0 192.38 6.30 -11 -6 0 195.88 6.60 11 6 0 192.88 6.60 -11 6 0 196.58 6.40 -11 6 0 198.58 7.50 -12 -6 0 -0.60 1.70 12 -6 0 -0.20 1.60 -12 -6 0 0.70 1.40 12 6 0 2.70 2.30 -12 6 0 1.50 1.70 -12 6 0 1.80 2.30 -13 -6 0 91.39 4.50 13 -6 0 82.79 4.30 -13 -6 0 81.79 4.50 -13 6 0 76.89 4.30 -13 6 0 84.79 5.90 13 6 0 87.19 4.90 -14 -6 0 2.50 2.00 -14 -6 0 3.10 2.20 14 -6 0 0.50 2.00 -14 6 0 3.10 2.20 14 6 0 -0.10 2.40 -14 6 0 0.20 2.80 -15 -6 0 16.00 3.20 -15 -6 0 29.40 3.80 15 -6 0 21.60 3.80 15 6 0 20.90 3.50 -15 6 0 34.90 6.00 -15 6 0 19.10 3.10 -16 -6 0 1.20 2.40 16 6 0 -3.00 3.20 -17 -6 0 1.60 2.90 17 -6 0 -5.00 4.10 17 6 0 0.50 3.80 0 -7 0 6.10 1.30 0 7 0 4.90 1.30 -1 -7 0 158.98 5.10 1 7 0 163.58 5.20 -1 7 0 156.98 4.40 -1 7 0 148.39 5.10 -2 -7 0 158.28 5.20 2 -7 0 163.68 5.20 2 7 0 153.88 6.00 -2 7 0 165.78 4.70 -2 7 0 172.68 5.30 -3 -7 0 -0.30 0.90 3 -7 0 0.80 0.90 -3 7 0 0.30 0.90 -3 7 0 1.80 1.10 3 7 0 0.90 0.90 -4 -7 0 358.96 9.50 4 -7 0 366.36 9.50 -4 7 0 364.96 9.30 4 7 0 339.17 9.80 -4 7 0 360.86 9.30 5 -7 0 50.99 2.70 -5 -7 0 49.40 2.90 -5 7 0 48.60 2.90 -5 7 0 48.60 2.70 5 7 0 49.00 3.70 6 -7 0 383.86 9.80 -6 -7 0 369.56 9.90 6 7 0 377.66 10.70 6 7 0 371.66 8.60 -6 7 0 378.26 10.20 -6 7 0 355.16 9.50 -7 -7 0 81.69 3.80 7 -7 0 84.09 3.70 -7 7 0 85.49 4.20 7 7 0 84.89 3.00 -7 7 0 82.09 3.70 7 7 0 82.89 4.30 -8 -7 0 129.39 5.80 8 -7 0 134.09 5.70 -8 7 0 149.39 5.30 -8 7 0 140.79 5.80 8 7 0 154.88 4.50 8 7 0 148.59 6.00 9 -7 0 0.10 1.40 -9 -7 0 2.20 1.50 9 7 0 1.30 1.40 -9 7 0 -0.30 1.60 -9 7 0 1.80 1.60 9 7 0 3.40 1.70 10 -7 0 5.90 1.70 -10 -7 0 5.90 1.80 -10 7 0 5.20 1.80 10 7 0 6.50 1.70 -10 7 0 6.80 2.30 11 -7 0 2.20 1.60 -11 -7 0 1.30 1.70 11 7 0 -1.60 1.90 -11 7 0 0.00 1.80 -11 7 0 0.30 2.30 12 -7 0 21.80 3.20 -12 -7 0 15.60 2.50 -12 7 0 17.80 3.60 -12 7 0 18.10 3.20 -13 -7 0 10.10 2.60 13 -7 0 13.40 2.50 -13 7 0 10.20 3.40 -13 7 0 13.20 2.50 13 7 0 7.60 2.50 -14 -7 0 45.00 4.50 14 -7 0 33.90 4.10 -14 7 0 39.60 4.10 14 7 0 40.10 4.50 -14 7 0 36.10 6.10 -15 -7 0 7.20 4.60 15 -7 0 7.50 2.90 15 7 0 5.20 3.20 -15 7 0 8.10 4.00 16 7 0 41.20 5.80 0 -8 0 796.12 19.70 0 8 0 828.32 19.00 1 -8 0 0.40 1.00 -1 -8 0 1.30 1.20 1 8 0 -0.60 1.20 -2 8 0 338.47 8.50 2 8 0 331.97 9.40 -2 8 0 337.27 9.20 3 -8 0 16.70 2.70 -3 -8 0 16.90 3.20 -3 8 0 15.00 2.20 -3 8 0 16.20 2.00 -4 -8 0 11.60 2.00 4 -8 0 13.00 2.00 -4 8 0 12.30 1.80 -4 8 0 14.30 2.30 4 8 0 14.50 2.20 -5 -8 0 23.90 2.40 5 -8 0 20.30 2.30 -5 8 0 24.20 2.50 5 8 0 23.80 2.70 -5 8 0 22.60 2.50 6 -8 0 4.40 1.50 -6 -8 0 3.40 1.40 6 8 0 0.70 1.30 -6 8 0 2.90 1.40 -6 8 0 2.80 1.60 -7 -8 0 86.49 4.30 7 -8 0 93.79 4.10 -7 8 0 97.19 5.10 7 8 0 90.89 4.60 8 -8 0 50.39 3.10 -8 -8 0 46.70 3.40 -8 8 0 45.80 3.80 8 8 0 45.90 2.70 8 8 0 42.40 4.00 -8 8 0 51.49 3.40 -9 -8 0 90.09 4.60 9 -8 0 90.69 4.30 9 8 0 90.69 3.60 9 8 0 84.29 5.30 -9 8 0 90.69 4.60 -9 8 0 93.49 5.20 10 -8 0 97.09 4.80 -10 -8 0 105.69 5.10 10 8 0 104.59 4.20 10 8 0 106.19 5.90 -10 8 0 102.59 4.40 -10 8 0 106.59 5.70 11 -8 0 55.69 4.10 -11 -8 0 52.49 4.30 11 8 0 57.59 3.70 -11 8 0 60.59 3.70 11 8 0 54.49 5.10 -11 8 0 60.49 5.10 12 -8 0 67.39 4.80 -12 -8 0 70.19 4.90 12 8 0 83.59 5.90 -12 8 0 81.89 4.40 12 8 0 84.49 4.70 -12 8 0 79.89 6.00 13 -8 0 48.50 4.60 -13 8 0 50.19 4.40 13 8 0 52.49 5.90 13 8 0 50.49 5.60 -13 8 0 51.29 6.20 -14 -8 0 16.50 3.20 14 -8 0 20.00 3.30 -14 8 0 19.70 4.60 14 8 0 20.00 4.20 15 8 0 12.50 4.30 -15 8 0 8.90 4.30 16 8 0 8.10 6.20 0 -9 0 -0.20 1.10 0 9 0 -1.20 1.30 1 -9 0 98.79 4.40 -1 -9 0 91.19 4.40 -1 9 0 104.29 3.60 1 9 0 93.99 4.40 2 -9 0 62.19 3.50 -2 -9 0 60.49 3.50 -2 9 0 56.29 3.80 -2 9 0 59.99 3.10 2 9 0 65.69 3.70 -3 -9 0 34.50 2.90 3 -9 0 38.50 3.00 3 9 0 34.90 3.00 -3 9 0 39.60 4.00 -3 9 0 37.40 2.70 4 -9 0 33.60 2.80 -4 -9 0 29.40 2.90 4 9 0 34.30 3.20 -4 9 0 26.90 2.80 -4 9 0 36.40 3.30 -5 -9 0 242.28 7.90 5 -9 0 262.17 7.90 -5 9 0 263.87 7.90 5 9 0 244.58 8.40 -5 9 0 263.57 8.00 -6 -9 0 69.69 3.80 6 -9 0 62.59 3.70 6 9 0 63.39 4.20 -6 9 0 67.29 4.10 7 -9 0 180.28 6.30 -7 -9 0 181.38 6.60 7 9 0 174.58 7.00 -7 9 0 179.38 6.70 -7 9 0 162.38 6.60 8 -9 0 5.90 2.00 -8 -9 0 5.20 2.10 -8 9 0 8.80 2.40 8 9 0 6.30 2.30 -8 9 0 7.30 1.90 9 -9 0 73.09 4.30 -9 -9 0 58.19 4.50 9 9 0 61.39 4.80 -9 9 0 51.19 3.80 -9 9 0 63.99 4.80 -10 -9 0 1.00 2.40 10 -9 0 0.00 1.80 -10 9 0 -3.10 1.80 10 9 0 0.70 2.10 -10 9 0 1.40 2.80 11 -9 0 -1.90 2.00 -11 -9 0 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5.20 2.40 -11 9 3 8.10 2.70 11 9 -3 10.60 2.70 -11 9 3 5.00 2.90 -10 -9 3 110.39 5.60 10 -9 -3 104.69 5.30 -10 9 3 116.69 6.10 10 9 -3 113.29 6.10 -10 9 3 99.59 4.50 -9 -9 3 1.20 1.90 9 -9 -3 -1.00 1.70 9 9 -3 0.70 1.90 -9 9 3 3.40 2.00 -9 9 3 0.50 1.60 -8 -9 3 143.99 5.80 8 -9 -3 132.99 5.50 8 9 -3 129.09 5.90 -8 9 3 130.19 4.90 -8 9 3 139.19 5.90 -7 -9 3 12.00 2.20 7 -9 -3 7.70 1.90 7 9 -3 6.80 2.20 -7 9 3 9.90 1.90 -7 9 3 9.10 2.20 6 -9 -3 51.79 3.20 -6 -9 3 47.40 3.40 -6 9 3 49.99 3.20 -6 9 3 46.00 3.40 6 9 -3 42.20 3.40 5 -9 -3 11.30 1.90 -5 -9 3 16.60 2.40 -5 9 3 15.20 2.60 5 9 -3 14.40 2.50 -5 9 3 15.00 2.10 4 -9 -3 -0.30 1.30 -4 -9 3 0.40 1.50 -4 9 3 -0.60 1.30 4 9 -3 0.50 1.40 -4 9 3 4.40 1.70 3 -9 -3 8.20 1.60 -3 -9 3 5.70 1.60 -3 9 3 10.40 1.80 3 9 -3 8.40 1.90 -3 9 3 10.30 2.00 -2 -9 3 97.69 4.50 2 -9 -3 93.29 4.20 2 9 -3 96.09 4.60 -2 9 3 100.09 4.40 -2 9 3 102.19 3.90 1 -9 -3 21.60 2.40 -1 -9 3 15.20 2.30 -1 9 3 14.10 2.00 1 9 -3 15.50 2.30 -1 9 3 16.00 2.30 0 -9 -3 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9.10 2.20 0 11 3 7.50 2.20 0 11 -3 5.20 2.20 0 11 3 4.20 1.80 -1 -11 -3 95.89 5.00 1 -11 3 93.89 5.00 1 11 3 87.99 3.90 1 11 3 94.59 5.10 -1 11 -3 91.09 5.30 -2 -11 -3 1.20 1.80 2 -11 3 -0.50 1.90 2 11 3 -2.70 1.80 -2 11 -3 1.60 2.10 -3 -11 -3 86.09 5.00 3 -11 3 76.89 4.90 3 11 3 88.19 5.30 -3 11 -3 85.79 4.90 4 -11 3 3.90 2.10 4 -11 3 3.90 2.30 -4 -11 -3 5.60 2.30 -4 11 -3 5.30 2.20 4 11 3 4.70 2.40 5 -11 3 25.70 4.10 -5 -11 -3 25.00 4.00 -5 11 -3 25.20 3.70 5 11 3 26.80 4.30 6 -11 3 2.30 2.40 -6 -11 -3 3.70 2.50 6 -11 3 1.70 2.50 -6 11 -3 0.80 2.10 6 11 3 3.90 2.70 7 -11 3 2.90 2.40 -7 -11 -3 -2.10 2.60 7 -11 3 -2.90 2.60 7 11 3 0.20 2.70 -7 11 -3 5.80 2.30 8 -11 3 7.20 2.70 -8 -11 -3 7.60 3.10 8 -11 3 6.70 3.20 -8 11 -3 2.20 2.70 8 11 3 5.20 3.10 9 -11 3 19.30 4.00 9 -11 3 20.40 3.50 -9 -11 -3 20.30 3.80 9 11 3 15.30 4.90 -9 11 -3 15.00 3.30 10 -11 3 6.50 3.20 10 -11 3 7.60 3.80 -10 -11 -3 6.10 3.60 10 11 3 9.50 3.80 -10 11 -3 4.50 3.20 11 -11 3 24.10 5.10 -11 -11 -3 25.60 4.70 11 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7.50 10 -4 4 299.67 9.70 10 -4 4 296.57 7.50 -10 4 -4 300.47 8.80 10 4 4 291.67 8.90 -11 -4 -4 55.19 3.00 11 -4 4 50.99 4.30 -11 -4 -4 50.79 3.50 11 -4 4 50.49 2.90 11 4 4 52.49 3.90 -11 4 -4 50.49 3.70 -12 -4 -4 107.19 5.20 12 -4 4 101.29 4.10 12 -4 4 102.99 5.90 -12 4 -4 109.29 5.20 12 4 4 108.29 5.70 13 -4 4 25.90 4.10 -13 -4 -4 19.90 3.40 13 4 4 20.10 3.30 -13 4 -4 15.40 2.70 14 -4 4 8.00 3.10 -14 -4 -4 8.00 2.50 -14 4 -4 10.90 2.80 14 4 4 6.90 3.00 15 -4 4 0.90 4.40 -15 -4 -4 0.70 2.60 -15 4 -4 -1.00 2.50 15 4 4 0.70 3.20 16 -4 4 1.60 4.10 -16 -4 -4 2.40 2.90 16 4 4 7.40 3.80 -16 4 -4 7.40 3.10 19 5 -4 19.00 5.40 18 -5 -4 11.50 3.40 18 5 -4 17.10 4.00 18 5 -4 19.50 4.20 -18 5 4 15.80 4.70 -17 -5 4 30.10 4.90 17 -5 -4 25.10 3.70 -17 5 4 28.10 4.60 17 5 -4 34.80 5.80 17 5 -4 26.00 4.00 16 -5 -4 10.70 2.60 -16 -5 4 8.30 2.60 16 5 -4 10.80 3.10 16 5 -4 13.40 3.40 -16 5 4 11.60 3.30 15 -5 -4 45.90 4.10 -15 -5 4 38.00 4.00 15 5 -4 49.20 4.30 15 5 -4 53.89 5.20 -15 5 4 49.99 5.00 14 -5 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8.40 3.30 -14 5 -4 0.10 2.50 14 5 4 2.50 2.90 -15 -5 -4 25.50 4.50 15 -5 4 18.90 4.60 15 5 4 24.40 4.10 -15 5 -4 32.40 5.30 -16 -5 -4 4.10 3.20 16 -5 4 -0.50 4.50 -16 5 -4 4.60 3.40 16 5 4 6.10 4.10 18 -6 -4 -1.50 3.30 -18 -6 4 5.40 3.40 18 6 -4 -3.80 4.30 -18 6 4 3.60 4.40 17 -6 -4 3.20 2.80 -17 -6 4 -1.70 2.90 17 6 -4 -0.20 3.90 -17 6 4 4.20 4.00 -16 -6 4 1.30 2.80 16 -6 -4 5.40 2.60 16 6 -4 -0.40 3.40 -16 6 4 0.90 3.20 16 6 -4 2.70 3.10 -15 -6 4 27.70 4.40 15 -6 -4 27.20 4.00 15 6 -4 28.10 4.20 -15 6 4 37.00 5.10 15 6 -4 23.90 3.30 14 -6 -4 1.30 2.10 -14 -6 4 0.70 2.20 14 6 -4 4.30 2.70 14 6 -4 -0.50 2.40 -14 6 4 2.00 2.80 13 -6 -4 164.88 6.30 -13 -6 4 168.78 6.30 13 6 -4 159.78 6.00 13 6 -4 165.78 7.20 -13 6 4 164.08 5.40 -13 6 4 166.28 7.40 -12 -6 4 2.50 1.60 12 -6 -4 1.20 1.60 12 6 -4 0.60 1.70 -12 6 4 1.40 1.40 12 6 -4 4.90 1.80 -12 6 4 3.60 2.10 -11 -6 4 333.27 9.60 11 -6 -4 327.17 9.40 -11 6 4 330.27 10.30 11 6 -4 337.07 8.70 11 6 -4 325.37 9.90 -11 6 4 336.37 8.30 -10 -6 4 1.40 1.20 10 -6 -4 2.50 1.40 -10 6 4 1.10 1.00 10 6 -4 0.20 1.20 -10 6 4 0.80 1.40 10 6 -4 1.60 1.40 -9 -6 4 189.58 6.30 9 -6 -4 190.58 6.20 -9 6 4 201.88 5.30 9 6 -4 188.88 6.60 -9 6 4 199.58 6.80 -8 -6 4 3.00 1.20 8 -6 -4 1.60 1.20 -8 6 4 2.10 0.90 -8 6 4 1.80 1.30 -7 -6 4 32.20 2.40 7 -6 -4 34.60 2.40 7 6 -4 29.00 2.70 -7 6 4 35.90 1.80 -7 6 4 35.70 2.50 6 -6 -4 4.90 1.20 -6 -6 4 2.90 1.10 -6 6 4 5.20 1.30 6 6 -4 5.50 1.50 -6 6 4 3.40 0.90 -5 -6 4 30.20 2.20 5 -6 -4 25.00 1.90 -5 6 4 24.20 1.90 -5 6 4 23.30 1.70 4 -6 -4 111.69 4.00 -4 -6 4 111.59 4.00 -4 6 4 112.09 3.90 4 6 -4 112.19 4.20 -4 6 4 114.29 3.60 -3 -6 4 524.35 12.60 3 -6 -4 517.95 12.50 -3 6 4 492.85 12.00 -3 6 4 521.35 12.20 3 6 -4 535.75 12.70 2 -6 -4 464.75 11.30 -2 -6 4 479.25 11.40 -2 6 4 463.85 11.00 -2 6 4 429.36 10.90 2 6 -4 480.45 11.60 -1 -6 4 741.53 16.70 1 -6 -4 709.73 16.50 1 6 -4 708.53 16.70 -1 6 4 715.43 16.50 -1 6 4 737.43 17.40 0 -6 4 251.87 6.90 0 -6 4 259.27 6.20 0 -6 -4 254.57 6.90 0 6 -4 247.68 7.10 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6.50 2.00 12 7 -4 5.00 1.80 -12 7 4 4.50 1.70 -12 7 4 2.60 2.40 12 7 -4 4.70 2.30 11 -7 -4 4.50 1.60 -11 -7 4 4.00 1.80 11 7 -4 3.90 2.00 -11 7 4 3.50 1.50 11 7 -4 4.50 1.60 -10 -7 4 111.59 4.80 10 -7 -4 107.29 4.60 -10 7 4 98.89 5.10 10 7 -4 106.39 5.20 -10 7 4 102.89 3.80 9 -7 -4 10.60 1.90 -9 -7 4 8.60 1.80 -9 7 4 7.50 1.40 9 7 -4 7.80 1.80 -9 7 4 8.10 2.00 -8 -7 4 200.38 6.60 8 -7 -4 208.78 6.60 -8 7 4 215.78 5.70 -8 7 4 191.18 7.70 8 7 -4 209.58 7.10 -7 -7 4 39.50 2.80 7 -7 -4 39.00 2.70 -7 7 4 39.10 2.80 7 7 -4 40.60 3.00 -7 7 4 38.90 2.30 -6 -7 4 223.18 8.00 6 -7 -4 233.58 7.90 -6 7 4 251.97 7.30 -6 7 4 245.28 6.40 -5 -7 4 139.89 5.00 5 -7 -4 141.19 4.90 -5 7 4 135.09 4.90 -5 7 4 148.49 4.50 5 7 -4 136.09 5.30 4 -7 -4 312.57 8.40 -4 -7 4 297.57 8.40 -4 7 4 307.47 8.20 -4 7 4 311.37 7.90 4 7 -4 294.87 8.60 -3 -7 4 17.60 1.90 3 -7 -4 14.90 1.90 3 7 -4 15.30 2.30 -3 7 4 16.00 1.70 -3 7 4 15.00 1.90 -2 -7 4 7.00 1.50 2 -7 -4 8.00 1.40 2 7 -4 7.30 1.40 -2 7 4 10.90 1.70 -2 7 4 10.00 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1.60 -1 8 4 4.50 1.30 1 8 -4 6.80 1.80 -1 8 4 5.00 1.40 0 8 4 398.66 10.60 0 8 4 423.86 9.80 0 8 -4 364.06 11.30 1 -8 4 -0.40 1.00 1 8 4 0.60 1.00 1 8 4 1.00 1.40 -1 8 -4 -0.80 1.20 2 -8 4 144.09 4.70 2 8 4 146.49 4.50 -2 8 -4 138.29 5.30 3 -8 4 6.50 1.50 -3 8 -4 6.20 1.50 3 8 4 9.50 1.40 3 8 4 6.50 1.80 4 -8 4 -0.10 1.50 -4 -8 -4 -0.50 1.40 4 -8 4 1.10 1.50 4 8 4 2.20 1.50 -4 8 -4 2.60 1.30 4 8 4 0.70 1.10 5 -8 4 60.79 3.80 -5 -8 -4 57.99 3.50 5 -8 4 60.79 3.40 5 8 4 57.09 2.90 -5 8 -4 62.19 3.50 -6 -8 -4 37.90 2.90 -6 -8 -4 33.40 2.90 6 -8 4 33.90 3.80 6 -8 4 35.40 3.00 -6 8 -4 31.30 3.00 6 8 4 34.60 2.60 7 -8 4 100.09 5.10 -7 -8 -4 107.19 4.60 -7 -8 -4 103.89 5.20 7 -8 4 103.49 4.50 -7 8 -4 112.79 4.90 7 8 4 104.59 4.20 -8 -8 -4 104.29 4.80 8 -8 4 111.19 5.60 8 -8 4 98.69 4.60 -8 -8 -4 93.79 4.70 8 8 4 107.29 6.10 -8 8 -4 115.99 5.10 -9 -8 -4 117.59 5.30 -9 -8 -4 112.79 5.20 9 -8 4 119.29 6.20 9 -8 4 113.39 5.50 -9 8 -4 115.49 5.40 9 8 4 115.99 5.10 10 -8 4 96.29 4.80 10 -8 4 84.19 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4 19.90 2.80 -2 9 -4 19.10 2.80 2 9 4 17.90 2.20 3 -9 4 236.88 7.20 3 -9 4 248.48 7.70 -3 -9 -4 242.38 7.70 3 9 4 239.38 8.10 -3 9 -4 249.68 7.90 3 9 4 246.28 6.70 4 -9 4 20.70 2.60 4 -9 4 13.20 2.30 -4 -9 -4 15.40 2.60 4 9 4 14.10 2.70 4 9 4 15.40 2.30 -4 9 -4 13.70 2.30 5 -9 4 196.68 6.80 5 -9 4 195.48 6.60 -5 -9 -4 198.48 7.00 5 9 4 212.18 7.90 5 9 4 198.58 5.90 -5 9 -4 197.88 6.90 6 -9 4 10.70 2.00 6 -9 4 11.20 2.20 -6 -9 -4 9.50 2.00 6 9 4 7.50 2.40 6 9 4 10.30 2.70 -6 9 -4 15.60 2.70 7 -9 4 81.59 4.40 7 -9 4 82.79 4.80 -7 -9 -4 71.99 4.50 7 9 4 86.89 5.40 -7 9 -4 73.09 4.60 7 9 4 76.69 3.70 8 -9 4 8.20 2.10 8 -9 4 7.80 2.70 -8 -9 -4 11.00 2.50 8 9 4 10.10 2.70 8 9 4 10.10 2.00 -8 9 -4 6.20 2.20 -9 -9 -4 13.60 2.90 9 -9 4 10.60 3.30 9 -9 4 12.00 2.50 9 9 4 13.90 2.30 -9 9 -4 8.90 2.60 -10 -9 -4 -1.20 2.60 10 -9 4 -5.80 3.10 10 -9 4 1.40 2.20 10 9 4 0.20 2.10 -10 9 -4 1.60 2.40 11 -9 4 6.90 3.70 -11 -9 -4 3.80 2.80 -11 9 -4 10.70 2.80 11 9 4 5.80 2.50 12 -9 4 -0.80 3.70 -12 9 -4 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35.20 4.00 4 -10 -4 125.89 5.40 -4 -10 4 127.59 5.70 -4 10 4 134.59 7.60 -4 10 4 128.59 5.50 4 10 -4 122.59 5.70 -3 -10 4 135.59 5.60 3 -10 -4 136.49 5.40 3 10 -4 119.89 5.70 -3 10 4 128.79 5.00 -2 -10 4 109.39 5.10 2 -10 -4 112.39 5.00 2 10 -4 99.59 5.20 -2 10 4 110.29 5.00 -2 10 4 101.89 4.30 1 -10 -4 126.69 5.40 -1 -10 4 123.89 5.40 -1 10 4 128.89 4.80 1 10 -4 127.89 5.60 -1 10 4 125.79 5.40 0 -10 -4 97.49 4.70 0 -10 4 100.59 4.80 0 10 4 97.19 4.90 0 10 4 97.19 4.20 0 10 -4 93.19 5.00 -1 -10 -4 110.19 5.10 1 -10 4 113.29 5.00 1 10 4 113.59 5.20 1 10 4 114.89 4.20 -1 10 -4 109.09 5.10 -2 -10 -4 31.50 3.40 2 -10 4 28.10 2.60 2 -10 4 35.80 3.20 2 10 4 34.30 2.60 -2 10 -4 31.10 3.50 2 10 4 32.20 3.70 -3 -10 -4 47.40 3.80 3 -10 4 43.70 3.30 3 -10 4 46.90 3.80 3 10 4 45.40 3.00 -3 10 -4 42.80 3.80 3 10 4 49.00 4.20 4 -10 4 7.80 2.20 -4 -10 -4 4.30 2.20 4 -10 4 8.40 2.10 4 10 4 8.90 1.80 -4 10 -4 6.70 2.10 4 10 4 9.00 2.40 5 -10 4 3.90 2.50 -5 -10 -4 -3.30 2.00 5 -10 4 1.40 2.00 -5 10 -4 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21.70 4.00 9 -11 -4 -1.20 2.20 -9 -11 4 -1.90 2.60 9 11 -4 0.30 2.40 -9 11 4 1.50 2.80 -8 -11 4 69.09 5.30 8 -11 -4 63.79 4.70 -8 11 4 65.69 5.40 -8 11 4 57.19 4.10 8 11 -4 62.79 5.10 -7 -11 4 7.40 2.50 7 -11 -4 -3.70 2.10 -7 11 4 1.30 1.90 7 11 -4 1.30 2.40 -7 11 4 2.00 2.40 6 -11 -4 96.19 5.30 -6 -11 4 102.39 5.60 -6 11 4 94.89 5.20 -6 11 4 95.79 4.90 6 11 -4 97.39 5.80 -5 -11 4 2.20 2.20 5 -11 -4 2.60 1.90 -5 11 4 1.80 2.10 -5 11 4 1.50 2.10 5 11 -4 1.30 2.30 4 -11 -4 81.29 4.70 -4 -11 4 67.39 4.70 4 11 -4 64.29 4.80 -4 11 4 75.49 4.50 -4 11 4 76.69 4.50 3 -11 -4 2.70 1.80 -3 -11 4 6.50 2.30 3 11 -4 -1.40 2.10 -3 11 4 2.00 1.90 -3 11 4 2.90 3.90 2 -11 -4 1.80 1.90 -2 -11 4 4.00 2.00 -2 11 4 4.70 2.00 2 11 -4 3.20 2.10 -2 11 4 5.60 2.10 -1 -11 4 1.10 1.90 1 -11 -4 1.20 2.00 -1 11 4 1.00 1.80 1 11 -4 2.60 2.10 -1 11 4 -0.40 1.80 0 -11 -4 14.20 2.50 0 -11 4 12.40 2.70 0 11 -4 16.10 2.90 0 11 4 15.80 2.80 0 11 4 11.90 2.30 -1 -11 -4 -1.40 1.90 1 -11 4 3.00 2.10 1 11 4 -0.30 1.90 1 11 4 2.90 1.70 -1 11 -4 4.30 2.00 -2 -11 -4 54.89 4.40 2 -11 4 59.29 4.30 2 11 4 50.99 3.30 -2 11 -4 56.69 4.60 2 11 4 56.29 4.50 3 -11 4 1.90 2.00 -3 -11 -4 5.60 2.20 3 11 4 -0.70 2.10 -3 11 -4 2.70 2.20 -4 -11 -4 71.99 5.20 4 -11 4 73.79 5.00 4 -11 4 67.99 5.00 -4 11 -4 80.39 5.00 4 11 4 79.09 5.30 -5 -11 -4 2.10 2.40 5 -11 4 -0.90 2.20 5 -11 4 -1.00 2.30 -5 11 -4 1.40 2.10 5 11 4 -0.60 2.60 -6 -11 -4 48.60 5.00 6 -11 4 51.59 4.80 6 -11 4 47.80 4.70 6 11 4 53.59 5.30 -6 11 -4 52.89 4.60 7 -11 4 -2.40 2.90 7 -11 4 0.30 3.00 -7 -11 -4 0.60 2.70 -7 11 -4 5.50 2.50 7 11 4 -2.20 2.90 8 -11 4 9.70 3.10 -8 -11 -4 9.30 3.20 8 -11 4 0.80 3.10 8 11 4 9.90 3.20 -8 11 -4 8.30 2.90 9 -11 4 10.10 3.30 -9 -11 -4 9.40 3.70 9 -11 4 6.10 3.70 -9 11 -4 9.30 3.00 9 11 4 1.50 3.20 10 -11 4 4.90 3.30 -10 -11 -4 5.50 3.70 10 -11 4 3.40 3.80 -10 11 -4 2.80 3.20 10 11 4 1.60 3.90 12 -12 -4 28.50 4.90 -12 -12 4 44.10 6.90 12 12 -4 25.00 5.40 -12 12 4 24.20 5.80 -11 -12 4 25.90 4.50 11 -12 -4 13.90 4.30 -11 12 4 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36.80 4.90 -14 -9 5 29.40 4.10 14 9 -5 33.00 5.60 -14 9 5 39.70 6.70 -13 -9 5 0.80 2.60 13 -9 -5 3.20 2.50 -13 9 5 5.20 3.20 13 9 -5 5.80 2.90 -12 -9 5 20.60 3.20 12 -9 -5 18.10 3.10 12 9 -5 24.60 4.40 -12 9 5 18.70 3.70 11 -9 -5 0.30 2.00 -11 -9 5 -2.90 2.10 11 9 -5 -0.90 2.10 -11 9 5 4.60 2.70 10 -9 -5 0.80 1.90 -10 -9 5 2.60 2.10 -10 9 5 -0.60 2.30 10 9 -5 -0.20 2.10 9 -9 -5 10.00 2.20 -9 -9 5 9.50 2.30 -9 9 5 12.30 2.60 9 9 -5 7.80 2.30 -9 9 5 7.70 1.70 8 -9 -5 36.70 3.40 -8 -9 5 34.60 3.60 8 9 -5 33.70 3.40 -8 9 5 32.80 3.40 -8 9 5 36.40 2.90 -7 -9 5 13.30 2.50 7 -9 -5 12.70 2.20 -7 9 5 13.20 2.50 7 9 -5 9.50 2.00 -7 9 5 12.40 2.50 -6 -9 5 215.28 7.30 6 -9 -5 199.78 7.00 -6 9 5 211.88 7.30 6 9 -5 214.18 7.50 -6 9 5 202.18 6.40 -5 -9 5 18.20 2.60 5 -9 -5 15.20 2.40 5 9 -5 11.10 2.20 -5 9 5 12.10 2.20 -5 9 5 12.80 2.10 -4 -9 5 290.67 8.90 4 -9 -5 295.57 8.70 -4 9 5 302.47 8.50 -4 9 5 298.97 8.40 4 9 -5 289.47 9.10 -3 -9 5 14.30 2.40 3 -9 -5 15.20 2.20 -3 9 5 20.30 3.10 3 9 -5 13.90 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5.50 -3 2 9 197.78 5.70 -2 -2 9 622.84 14.10 2 -2 -9 640.14 14.20 -2 -2 9 641.34 14.30 2 -2 -9 619.64 14.10 -2 2 9 622.74 14.50 2 2 -9 626.94 14.40 1 -2 -9 122.49 3.90 -1 -2 9 123.99 3.60 1 -2 -9 124.89 3.70 -1 -2 9 126.89 4.00 -1 2 9 127.19 4.10 1 2 -9 121.39 4.00 0 -2 -9 437.66 10.50 0 -2 9 426.26 10.50 0 -2 -9 441.96 9.80 0 -2 9 429.96 9.80 0 2 9 423.06 10.60 0 2 -9 432.56 10.60 -1 -2 -9 22.00 1.30 -1 -2 -9 23.00 1.80 1 -2 9 23.10 1.30 1 -2 9 25.30 1.90 -1 2 -9 25.60 2.00 1 2 9 23.90 1.90 2 -2 9 95.79 3.80 -2 -2 -9 102.69 3.90 -2 2 -9 98.89 3.90 2 2 9 101.19 3.90 3 -2 9 149.19 5.20 -3 -2 -9 158.18 5.60 -3 2 -9 150.88 5.40 3 2 9 156.18 5.20 4 2 9 1.00 1.40 -4 2 -9 2.50 1.10 -5 -2 -9 2.20 1.10 5 -2 9 0.30 1.10 5 2 9 0.70 1.30 -5 2 -9 2.10 1.10 6 -2 9 26.30 2.80 -6 -2 -9 25.60 2.40 6 2 9 26.70 2.60 -6 2 -9 23.20 2.50 -7 -2 -9 0.90 1.20 7 -2 9 1.80 1.60 -7 2 -9 1.40 1.30 7 2 9 0.80 1.40 -8 -2 -9 211.48 7.40 8 -2 9 207.48 7.70 8 2 9 209.78 7.40 -8 2 -9 206.38 7.50 9 -2 9 -0.50 2.10 -9 -2 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9 189.08 7.60 14 3 -9 204.08 6.80 -13 -3 9 110.09 4.70 -13 -3 9 103.79 4.70 13 -3 -9 106.69 5.00 -13 3 9 108.69 5.30 13 3 -9 108.49 4.80 -12 -3 9 24.20 2.60 -12 -3 9 23.20 2.50 12 -3 -9 26.40 2.80 -12 3 9 23.00 2.90 12 3 -9 25.50 2.70 -11 -3 9 28.90 2.50 -11 -3 9 28.30 2.60 11 -3 -9 31.10 2.80 -11 3 9 30.40 2.90 11 3 -9 25.00 2.60 -10 -3 9 2.10 1.30 10 -3 -9 0.00 1.20 -10 -3 9 -1.30 1.00 -10 3 9 0.40 1.10 10 3 -9 2.00 1.30 9 -3 -9 21.00 2.30 -9 -3 9 20.80 2.00 -9 -3 9 17.80 1.90 -9 3 9 19.50 2.10 9 3 -9 21.50 2.10 -8 -3 9 63.79 2.70 8 -3 -9 61.69 4.20 -8 -3 9 61.89 3.10 -8 3 9 62.79 3.30 8 3 -9 62.69 2.90 7 -3 -9 123.29 4.40 -7 -3 9 117.19 4.20 -7 -3 9 122.89 3.80 -7 3 9 124.89 4.50 7 3 -9 120.99 4.10 6 -3 -9 113.59 4.10 -6 -3 9 117.59 3.60 -6 -3 9 113.29 4.20 6 3 -9 113.99 3.90 -6 3 9 118.49 4.30 -5 -3 9 395.06 9.80 -5 -3 9 391.66 9.30 5 -3 -9 395.96 10.10 5 3 -9 395.86 9.70 -5 3 9 390.16 10.00 -4 -3 9 217.38 5.60 4 -3 -9 207.18 6.00 -4 -3 9 216.08 6.00 4 -3 -9 212.28 5.20 -4 3 9 218.08 6.20 4 3 -9 211.78 5.90 3 -3 -9 320.27 7.70 -3 -3 9 319.07 8.10 -3 -3 9 327.77 7.90 3 -3 -9 317.37 8.10 3 3 -9 322.07 8.30 -3 3 9 328.97 8.40 2 -3 -9 549.95 12.70 -2 -3 9 564.54 12.80 2 -3 -9 559.04 12.90 -2 -3 9 554.54 12.80 2 3 -9 575.64 13.30 -2 3 9 552.14 13.20 1 -3 -9 49.70 2.20 -1 -3 9 48.20 2.10 -1 -3 9 49.00 2.30 1 -3 -9 46.30 2.20 1 3 -9 48.60 2.40 -1 3 9 47.80 2.40 0 -3 -9 61.99 2.70 0 -3 9 65.19 2.40 0 -3 9 63.49 2.80 0 -3 -9 63.39 2.40 0 3 9 65.59 2.80 0 3 -9 61.79 2.90 -1 -3 -9 1.30 0.90 1 -3 9 2.50 0.80 1 -3 9 0.50 0.90 -1 -3 -9 1.60 0.70 -1 3 -9 2.50 1.00 1 3 9 1.10 0.80 2 -3 9 44.50 1.80 -2 -3 -9 42.70 1.80 -2 -3 -9 41.40 2.50 2 -3 9 39.60 2.40 -2 3 -9 39.90 2.50 2 3 9 45.90 2.60 3 -3 9 82.29 3.80 -3 -3 -9 82.19 3.60 3 3 9 85.79 3.60 -4 -3 -9 78.29 3.60 4 3 9 75.19 3.50 -4 3 -9 81.49 3.70 -5 -3 -9 172.38 6.00 5 -3 9 168.08 6.10 5 3 9 179.28 6.10 -5 3 -9 165.78 5.90 6 -3 9 163.58 6.20 -6 -3 -9 163.88 5.90 -6 3 -9 156.58 5.80 6 3 9 163.08 6.00 7 -3 9 80.49 4.50 -7 -3 -9 85.19 4.10 7 3 9 81.49 4.30 -7 3 -9 79.49 4.20 8 -3 9 13.40 2.60 -8 -3 -9 8.60 1.90 8 3 9 13.10 2.40 -8 3 -9 10.30 2.00 9 -3 9 10.40 2.60 -9 -3 -9 10.80 2.20 9 3 9 7.70 2.40 -9 3 -9 12.30 2.40 10 -3 9 8.70 2.90 -10 -3 -9 7.70 2.50 -10 3 -9 8.90 2.30 10 3 9 10.70 2.80 11 -3 9 0.70 2.70 -11 -3 -9 0.60 2.40 -11 3 -9 -0.30 2.10 11 3 9 3.70 2.70 -12 -3 -9 -1.80 2.70 12 -3 9 3.60 3.50 12 3 9 4.10 3.10 -12 3 -9 1.60 2.50 13 -3 9 8.50 3.70 13 3 9 12.60 3.90 -13 3 -9 16.70 3.40 20 -4 -9 -3.80 4.40 20 4 -9 9.90 5.80 19 -4 -9 28.10 4.20 -19 -4 9 20.10 4.50 -19 4 9 27.70 5.40 19 4 -9 25.50 4.80 19 4 -9 30.10 5.80 -18 -4 9 2.10 3.40 18 -4 -9 4.70 3.30 18 4 -9 8.80 3.10 -18 4 9 12.80 3.70 -17 -4 9 8.70 3.10 17 -4 -9 2.90 3.00 -17 -4 9 5.80 2.80 -17 4 9 5.70 3.00 17 4 -9 7.50 2.70 -16 -4 9 11.90 2.70 -16 -4 9 12.20 2.80 16 -4 -9 12.90 2.80 16 4 -9 6.20 2.40 -16 4 9 9.00 3.10 -15 -4 9 12.10 2.70 -15 -4 9 12.20 2.60 15 -4 -9 12.90 2.70 15 4 -9 17.80 3.40 -15 4 9 15.70 3.00 14 -4 -9 3.60 2.00 -14 -4 9 2.80 2.10 -14 -4 9 1.10 1.80 14 4 -9 2.80 1.90 -14 4 9 -0.30 2.00 -13 -4 9 1.30 1.50 -13 -4 9 3.40 1.80 13 -4 -9 2.70 1.70 13 4 -9 -0.60 2.10 -13 4 9 1.30 1.70 12 -4 -9 166.08 6.20 -12 -4 9 164.08 6.00 -12 -4 9 166.88 5.70 -12 4 9 163.58 6.60 12 4 -9 172.98 6.00 11 -4 -9 118.69 5.00 -11 -4 9 122.99 4.90 -11 -4 9 118.89 4.50 -11 4 9 119.09 5.30 10 -4 -9 78.59 3.80 -10 -4 9 75.29 3.30 -10 -4 9 74.69 3.70 10 4 -9 78.79 3.70 -10 4 9 76.29 4.00 -9 -4 9 272.97 7.20 -9 -4 9 263.77 7.90 9 -4 -9 272.37 8.00 -9 4 9 268.57 8.30 9 4 -9 279.27 7.70 8 -4 -9 20.50 2.10 -8 -4 9 20.80 1.70 -8 -4 9 22.00 2.10 8 4 -9 21.90 2.40 -8 4 9 21.20 2.20 -7 -4 9 126.59 5.10 7 -4 -9 132.09 5.70 -7 -4 9 127.79 3.90 7 4 -9 125.89 4.50 -7 4 9 129.49 4.70 -6 -4 9 45.00 2.60 6 -4 -9 44.40 2.60 -6 -4 9 44.40 2.00 6 4 -9 46.20 2.50 -6 4 9 45.90 2.60 -5 -4 9 387.56 9.00 -5 -4 9 390.76 9.90 5 -4 -9 376.36 9.80 5 -4 -9 382.46 8.50 -5 4 9 374.36 9.90 5 4 -9 393.26 9.80 4 -4 -9 11.10 1.60 4 -4 -9 9.30 1.10 -4 -4 9 9.60 1.30 -4 -4 9 10.40 1.50 4 4 -9 9.70 1.60 -4 4 9 9.60 1.50 3 -4 -9 605.44 14.20 -3 -4 9 604.64 14.20 -3 -4 9 637.34 13.70 3 -4 -9 605.74 13.60 3 4 -9 607.14 14.50 -3 4 9 600.34 14.40 2 -4 -9 2.20 0.90 -2 -4 9 0.90 0.90 -2 -4 9 0.20 0.80 2 -4 -9 1.70 0.80 2 4 -9 1.60 0.90 -2 4 9 1.60 0.90 1 -4 -9 945.31 20.70 1 -4 -9 939.81 20.60 -1 -4 9 938.61 20.70 -1 -4 9 930.61 20.60 1 4 -9 949.01 21.30 -1 4 9 914.41 21.10 0 -4 9 3.10 1.00 0 -4 9 4.60 1.20 0 -4 -9 4.60 1.10 0 -4 -9 3.70 1.00 0 4 9 3.60 1.00 0 4 -9 4.10 1.20 -1 -4 -9 529.15 12.20 1 -4 9 526.15 12.80 1 -4 9 530.25 12.10 -1 -4 -9 526.85 12.80 -1 4 -9 528.95 13.10 1 4 9 541.25 13.00 -2 -4 -9 31.30 1.80 -2 -4 -9 30.40 2.20 2 -4 9 34.80 1.90 2 -4 9 32.80 2.30 2 4 9 32.80 2.20 3 -4 9 211.68 5.50 3 -4 9 221.08 7.00 -3 -4 -9 208.98 5.40 -3 -4 -9 199.78 7.10 -3 4 -9 206.48 6.50 3 4 9 210.88 8.70 -4 -4 -9 5.90 1.30 4 -4 9 7.10 1.90 -4 4 -9 5.50 1.40 4 4 9 4.60 1.40 -5 -4 -9 64.09 3.50 5 -4 9 63.19 3.80 -5 4 -9 66.69 3.60 5 4 9 61.39 3.40 6 -4 9 21.60 2.90 -6 -4 -9 18.20 2.50 -6 4 -9 19.60 2.50 6 4 9 17.10 2.50 7 -4 9 5.20 2.00 -7 -4 -9 7.90 2.70 -7 4 -9 6.60 1.70 -8 -4 -9 20.20 3.10 8 -4 9 25.70 3.50 -8 4 -9 28.00 3.20 8 4 9 20.70 3.40 -9 -4 -9 92.99 5.10 9 -4 9 93.79 5.60 9 4 9 89.89 5.30 -9 4 -9 93.29 5.20 -10 -4 -9 17.20 2.90 10 -4 9 20.70 3.60 -10 4 -9 18.20 3.00 10 4 9 18.90 3.40 11 -4 9 37.90 5.30 -11 -4 -9 32.40 4.20 11 4 9 36.50 5.20 -11 4 -9 46.10 4.90 -12 -4 -9 9.10 2.80 12 -4 9 8.00 4.40 12 4 9 4.70 3.40 -12 4 -9 7.70 2.90 13 -4 9 22.80 4.80 13 4 9 14.90 4.30 -13 4 -9 18.20 3.70 19 -5 -9 1.40 3.80 19 5 -9 6.30 3.60 -19 5 9 5.20 4.50 18 -5 -9 26.20 4.10 -18 -5 9 16.90 3.80 18 5 -9 32.20 5.20 -18 5 9 28.10 4.90 -17 -5 9 17.20 3.60 17 -5 -9 23.90 3.70 -17 -5 9 30.80 4.60 17 5 -9 26.70 4.70 -17 5 9 20.40 4.20 -16 -5 9 82.29 5.50 -16 -5 9 86.59 5.50 16 -5 -9 81.79 5.70 16 5 -9 90.49 5.50 -16 5 9 91.59 6.60 -15 -5 9 39.80 4.60 15 -5 -9 42.40 4.20 15 5 -9 42.50 4.30 -15 5 9 43.60 4.70 14 -5 -9 68.49 4.50 -14 -5 9 64.89 4.40 -14 -5 9 72.99 4.50 14 5 -9 60.69 4.40 -14 5 9 59.69 4.80 13 -5 -9 40.80 3.50 -13 -5 9 39.00 3.50 -13 -5 9 31.60 3.40 13 5 -9 39.60 3.50 -13 5 9 38.40 3.90 -12 -5 9 51.99 3.50 -12 -5 9 57.09 3.80 12 -5 -9 61.09 3.80 -12 5 9 62.99 4.20 12 5 -9 56.09 3.60 -11 -5 9 9.20 1.80 11 -5 -9 13.00 2.30 -11 -5 9 7.50 1.60 11 5 -9 10.50 1.80 -11 5 9 7.30 2.00 -10 -5 9 2.30 1.30 10 -5 -9 3.50 1.40 -10 -5 9 1.30 1.30 -10 5 9 3.40 1.40 10 5 -9 4.70 1.90 -9 -5 9 1.80 1.20 9 -5 -9 1.20 1.10 -9 -5 9 0.80 1.30 9 5 -9 2.30 1.50 -9 5 9 1.30 1.30 8 -5 -9 102.59 4.30 -8 -5 9 102.79 4.20 -8 -5 9 107.49 3.40 -8 5 9 104.09 4.50 8 5 -9 101.79 4.40 -7 -5 9 10.20 1.40 7 -5 -9 12.80 2.20 -7 -5 9 13.30 2.30 -7 5 9 12.20 1.80 7 5 -9 13.90 2.20 -6 -5 9 128.89 4.60 6 -5 -9 128.49 4.60 6 5 -9 119.79 4.50 -6 5 9 127.79 4.70 -5 -5 9 68.39 3.20 -5 -5 9 67.89 2.40 5 -5 -9 74.19 3.30 5 5 -9 73.29 3.40 -5 5 9 67.89 3.30 -5 5 9 72.59 2.60 -4 -5 9 156.78 4.20 4 -5 -9 154.98 5.10 -4 -5 9 159.68 5.10 4 -5 -9 155.88 4.20 -4 5 9 157.48 5.20 4 5 -9 150.28 5.20 3 -5 -9 104.39 3.90 -3 -5 9 103.59 3.80 -3 -5 9 105.59 3.20 3 -5 -9 103.89 3.30 3 5 -9 101.29 4.10 -3 5 9 103.39 3.90 2 -5 -9 98.49 4.30 -2 -5 9 94.79 3.60 -2 -5 9 90.99 3.10 2 -5 -9 91.29 3.50 2 5 -9 93.59 3.90 -2 5 9 100.89 3.80 1 -5 -9 25.60 1.90 1 -5 -9 24.50 1.90 -1 -5 9 25.10 1.80 -1 -5 9 24.90 1.90 1 5 -9 23.70 2.20 -1 5 9 25.80 2.00 0 -5 -9 6.70 1.20 0 -5 9 5.30 1.20 0 -5 9 6.80 1.20 0 -5 -9 4.30 1.10 0 5 9 5.50 1.30 0 5 -9 3.70 1.30 1 -5 9 0.50 1.00 1 -5 9 0.20 0.90 -1 -5 -9 0.70 1.00 -1 -5 -9 2.30 1.00 1 5 9 -0.10 0.90 -1 5 -9 0.80 0.90 2 -5 9 48.30 2.40 -2 -5 -9 46.10 2.40 -2 -5 -9 46.20 2.70 2 -5 9 52.29 2.90 2 5 9 49.80 2.70 -2 5 -9 48.90 2.90 -3 -5 -9 29.10 2.10 3 -5 9 34.50 2.10 -3 -5 -9 30.70 2.50 3 -5 9 36.00 2.70 3 5 9 32.90 2.60 -3 5 -9 31.20 2.60 4 -5 9 209.68 5.80 -4 -5 -9 213.38 5.80 4 -5 9 215.88 7.00 -4 -5 -9 210.18 6.80 -4 5 -9 206.78 6.90 4 5 9 211.88 6.80 5 -5 9 50.59 3.60 5 -5 9 50.39 2.50 -5 -5 -9 48.40 2.50 -5 -5 -9 50.29 3.20 -5 5 -9 49.10 3.30 5 5 9 49.90 3.20 -6 -5 -9 176.08 6.50 6 -5 9 176.68 6.70 -6 5 -9 181.38 6.60 6 5 9 181.88 6.40 -7 -5 -9 27.60 3.00 7 -5 9 21.40 3.40 7 5 9 26.50 2.90 -7 5 -9 30.70 3.10 8 -5 9 58.49 4.60 -8 -5 -9 51.09 3.90 8 5 9 62.19 4.10 -8 5 -9 64.49 4.30 9 -5 9 7.00 2.70 -9 -5 -9 5.90 2.00 9 5 9 3.90 2.30 -9 5 -9 6.30 2.20 10 -5 9 7.40 3.10 -10 5 -9 7.50 2.70 10 5 9 8.30 2.90 -11 -5 -9 -0.20 2.30 11 -5 9 -0.90 3.00 11 5 9 -4.10 2.80 -11 5 -9 2.10 2.70 12 -5 9 0.40 3.40 -12 -5 -9 2.10 2.70 12 5 9 -3.30 3.20 13 -5 9 1.00 4.30 13 5 9 -3.90 3.60 -19 -6 9 13.80 4.20 19 -6 -9 8.60 3.50 19 6 -9 9.00 4.20 -18 -6 9 -0.90 3.00 18 -6 -9 -3.20 3.40 18 6 -9 8.10 3.70 -18 6 9 5.80 4.20 -17 -6 9 0.70 3.00 17 -6 -9 1.10 3.10 17 6 -9 7.00 3.80 -17 6 9 5.00 3.90 16 -6 -9 -0.10 2.80 -16 -6 9 -0.10 2.90 -16 6 9 3.30 3.40 16 6 -9 6.40 3.00 -15 -6 9 6.60 2.80 15 -6 -9 4.30 2.70 15 6 -9 6.00 2.60 -15 6 9 12.30 3.10 -14 -6 9 28.20 3.90 -14 -6 9 24.70 3.90 14 -6 -9 23.50 3.70 14 6 -9 25.60 4.00 -14 6 9 17.60 3.40 -13 -6 9 20.70 3.30 -13 -6 9 17.20 3.10 13 -6 -9 15.70 2.80 -13 6 9 18.00 3.10 13 6 -9 18.00 3.40 12 -6 -9 79.29 4.50 -12 -6 9 79.69 4.40 -12 -6 9 71.09 3.60 12 6 -9 79.99 4.60 -12 6 9 80.59 5.50 -11 -6 9 -1.10 1.40 11 -6 -9 0.80 1.50 11 6 -9 1.50 1.50 -11 6 9 0.20 1.90 10 -6 -9 314.67 9.40 -10 -6 9 317.97 9.50 10 6 -9 313.97 9.30 -10 6 9 327.67 9.90 -9 -6 9 10.30 2.00 9 -6 -9 10.90 1.90 -9 6 9 9.90 2.10 9 6 -9 9.70 2.00 8 -6 -9 162.58 5.70 -8 -6 9 157.88 5.70 -8 6 9 163.38 6.00 8 6 -9 162.88 5.80 -7 -6 9 96.79 4.30 7 -6 -9 95.19 4.20 7 6 -9 102.79 4.40 -7 6 9 100.19 4.40 6 -6 -9 2.40 1.20 -6 -6 9 3.00 1.10 -5 -6 9 18.80 2.40 -5 6 9 15.80 1.80 -5 6 9 19.50 2.00 -4 -6 9 63.29 3.10 4 -6 -9 60.69 3.10 -4 6 9 61.29 3.10 -4 6 9 56.59 2.80 -3 -6 9 166.18 5.40 3 -6 -9 159.88 5.20 -3 -6 9 167.48 4.40 3 -6 -9 150.88 4.50 -3 6 9 152.78 5.30 2 -6 -9 198.88 5.70 -2 -6 9 210.28 5.50 2 -6 -9 197.78 6.10 -2 -6 9 208.38 6.20 -2 6 9 212.48 6.40 2 6 -9 207.28 6.60 -1 -6 9 195.18 5.50 -1 -6 9 204.08 6.00 1 -6 -9 199.68 5.80 1 -6 -9 199.88 6.10 -1 6 9 197.68 6.20 1 6 -9 193.38 6.30 0 -6 -9 308.57 8.30 0 -6 9 321.17 8.40 0 -6 9 319.77 8.20 0 -6 -9 319.37 8.40 0 6 9 307.37 8.50 0 6 -9 315.17 9.00 -1 -6 -9 146.09 5.00 1 -6 9 140.19 4.80 -1 -6 -9 146.19 4.80 1 -6 9 141.29 4.80 -1 6 -9 139.29 5.20 1 6 9 141.99 4.90 2 -6 9 149.88 4.90 -2 -6 -9 148.39 4.90 2 -6 9 150.98 5.20 -2 -6 -9 151.68 5.20 -2 6 -9 149.29 5.40 -3 -6 -9 153.78 5.00 3 -6 9 160.48 5.00 -3 -6 -9 149.29 5.40 3 -6 9 150.28 5.50 -3 6 -9 155.08 5.70 3 6 9 154.28 5.30 -4 -6 -9 35.50 2.80 4 -6 9 43.30 3.30 4 -6 9 37.70 2.60 -4 -6 -9 43.70 3.00 -4 6 -9 45.30 3.30 4 6 9 41.70 3.00 -5 -6 -9 18.70 2.50 5 -6 9 20.50 3.00 -5 -6 -9 24.70 2.70 5 -6 9 21.80 2.20 5 6 9 24.50 2.70 -5 6 -9 21.50 2.70 6 -6 9 -1.20 1.30 6 -6 9 0.10 1.80 -6 -6 -9 -0.10 1.40 -6 -6 -9 -1.00 1.50 -6 6 -9 2.20 1.60 6 6 9 0.90 1.60 -7 -6 -9 1.80 1.60 7 -6 9 0.70 1.50 7 -6 9 3.80 2.30 7 6 9 2.70 2.00 -7 6 -9 2.20 1.80 -8 -6 -9 69.79 4.50 8 -6 9 79.19 5.30 -8 6 -9 72.79 5.00 8 6 9 61.19 4.50 9 -6 9 -0.80 2.50 -9 -6 -9 -1.90 1.80 9 6 9 1.40 2.30 -9 6 -9 4.50 2.30 -10 -6 -9 78.99 5.10 10 -6 9 86.79 6.50 10 6 9 79.49 5.50 -10 6 -9 73.19 5.80 -11 -6 -9 1.60 2.50 11 -6 9 4.00 3.60 11 6 9 2.50 3.00 -11 6 -9 1.40 2.90 -12 -6 -9 32.90 5.20 12 -6 9 45.50 6.80 12 6 9 38.50 5.50 -12 6 -9 43.00 5.60 -18 -7 9 -3.30 3.50 18 -7 -9 5.20 3.60 18 7 -9 -3.10 3.90 -18 7 9 15.40 5.10 17 -7 -9 37.90 5.50 -17 -7 9 40.50 5.90 -17 7 9 46.10 7.00 17 7 -9 47.20 6.20 16 -7 -9 9.80 3.00 -16 -7 9 5.10 3.20 -16 7 9 8.00 3.70 16 7 -9 11.50 3.40 15 -7 -9 80.39 5.50 -15 -7 9 94.39 6.00 -15 7 9 94.19 6.80 15 7 -9 82.39 5.80 14 -7 -9 83.29 5.30 -14 -7 9 86.39 5.50 14 7 -9 79.09 5.50 -14 7 9 99.19 6.30 13 -7 -9 60.49 4.50 -13 -7 9 60.09 4.40 13 7 -9 58.89 4.80 -13 7 9 56.69 5.10 -12 -7 9 4.60 2.10 12 -7 -9 4.40 2.20 12 7 -9 7.60 2.30 -12 7 9 -1.00 2.50 11 -7 -9 24.90 3.10 -11 -7 9 21.00 3.30 -11 7 9 23.70 3.70 11 7 -9 16.30 2.70 -10 -7 9 17.40 2.80 10 -7 -9 8.50 2.10 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3.80 16 -8 -9 9.90 3.20 -16 8 9 8.40 4.30 16 8 -9 1.60 3.70 15 -8 -9 4.60 2.70 -15 -8 9 4.60 2.90 -15 8 9 2.70 3.50 15 8 -9 3.40 3.20 -14 -8 9 9.90 3.00 14 -8 -9 12.90 2.70 14 8 -9 9.60 3.20 -14 8 9 11.10 3.50 -13 -8 9 15.20 3.00 13 -8 -9 15.80 2.80 13 8 -9 16.00 3.10 -13 8 9 16.70 3.40 12 -8 -9 63.29 4.50 -12 -8 9 51.69 4.50 -12 8 9 50.59 5.00 12 8 -9 54.49 5.00 11 -8 -9 92.49 5.10 -11 -8 9 98.49 5.20 11 8 -9 88.99 5.50 -11 8 9 98.69 5.70 -10 -8 9 33.90 3.40 10 -8 -9 40.40 3.40 10 8 -9 27.90 3.90 -10 8 9 31.90 4.00 9 -8 -9 145.19 5.90 -9 -8 9 155.88 6.20 9 8 -9 145.99 6.20 -9 8 9 153.28 6.50 -8 -8 9 27.50 3.10 8 -8 -9 25.60 2.90 8 8 -9 28.70 3.10 -8 8 9 29.50 3.40 7 -8 -9 29.30 2.90 -7 -8 9 26.20 3.10 -7 8 9 23.10 3.00 7 8 -9 24.40 3.20 6 -8 -9 35.10 2.90 -6 -8 9 37.30 3.10 -6 8 9 34.30 3.20 6 8 -9 33.50 3.10 -6 8 9 31.70 2.50 5 -8 -9 19.00 2.50 -5 -8 9 14.50 2.50 5 8 -9 23.80 2.90 -5 8 9 14.00 2.60 -5 8 9 18.20 2.50 4 -8 -9 17.40 2.40 -4 -8 9 10.20 2.00 -4 8 9 14.60 2.50 -4 8 9 14.50 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-4 10 48.50 3.90 -14 -4 10 43.20 3.70 14 -4 -10 46.10 3.90 -14 4 10 46.70 4.10 14 4 -10 47.90 3.60 -13 -4 10 4.70 1.90 -13 -4 10 5.00 1.90 13 -4 -10 6.70 2.00 -13 4 10 9.20 2.10 13 4 -10 4.30 2.10 -12 -4 10 -0.80 1.50 12 -4 -10 2.80 1.70 -12 -4 10 1.80 1.40 -12 4 10 -1.50 1.60 12 4 -10 1.70 1.60 11 -4 -10 25.80 2.70 -11 -4 10 23.30 2.60 -11 -4 10 31.00 2.70 -11 4 10 31.00 3.00 11 4 -10 33.20 3.10 10 -4 -10 199.98 6.80 -10 -4 10 200.68 6.70 -10 -4 10 204.28 6.10 10 4 -10 220.68 6.60 -10 4 10 205.08 7.10 -9 -4 10 82.69 3.30 9 -4 -10 83.49 4.00 -9 -4 10 84.39 3.80 9 4 -10 82.79 3.80 -9 4 10 84.79 4.10 -8 -4 10 498.15 11.50 -8 4 10 456.55 13.50 8 4 -10 498.75 12.10 7 -4 -10 20.70 2.20 -7 -4 10 25.40 1.80 -7 -4 10 23.70 2.10 -7 4 10 22.00 2.20 7 4 -10 27.10 2.30 -6 -4 10 77.49 2.90 6 -4 -10 75.69 3.40 -6 -4 10 75.99 3.40 6 4 -10 74.09 3.30 -6 4 10 71.89 3.40 5 -4 -10 161.38 4.20 -5 -4 10 167.28 5.30 5 -4 -10 161.08 5.30 -5 -4 10 163.58 4.70 5 4 -10 168.28 5.30 -5 4 10 171.18 6.80 -4 -4 10 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10 26.60 4.50 15 5 -10 27.30 4.00 -14 -5 10 81.29 6.40 14 -5 -10 75.89 4.80 -14 -5 10 71.99 4.60 -14 5 10 70.69 5.10 14 5 -10 73.19 4.50 -13 -5 10 21.20 3.10 13 -5 -10 24.80 3.20 -13 -5 10 22.20 3.20 -13 5 10 26.90 3.30 13 5 -10 22.80 3.10 -12 -5 10 19.20 2.90 12 -5 -10 21.30 2.90 -12 -5 10 18.20 2.70 -12 5 10 19.10 3.20 12 5 -10 22.50 3.00 -11 -5 10 7.50 2.30 -11 -5 10 7.60 1.80 11 -5 -10 8.50 1.90 -11 5 10 6.50 1.90 11 5 -10 7.60 1.90 -10 -5 10 7.10 1.50 -10 -5 10 8.50 1.80 10 -5 -10 7.10 1.70 -10 5 10 8.40 1.90 9 -5 -10 92.89 4.30 -9 -5 10 98.29 3.50 -9 -5 10 90.69 4.20 9 5 -10 103.29 4.30 -9 5 10 87.99 4.50 8 -5 -10 -0.10 1.20 -8 -5 10 -1.10 0.90 -8 -5 10 -1.40 1.00 -8 5 10 0.40 1.20 8 5 -10 0.60 1.30 7 -5 -10 439.66 11.60 -7 -5 10 444.46 10.30 -7 -5 10 447.56 11.60 7 5 -10 447.56 11.40 -7 5 10 447.76 11.80 6 -5 -10 55.69 3.10 -6 -5 10 59.29 3.00 -6 -5 10 51.29 2.30 6 5 -10 58.79 3.20 5 -5 -10 284.57 6.80 -5 -5 10 286.37 7.10 5 -5 -10 290.27 8.10 -5 -5 10 299.87 8.10 -5 5 10 284.97 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2.00 1.60 -4 -5 -10 0.80 1.20 -4 -5 -10 1.50 1.30 4 -5 10 1.80 1.20 -4 5 -10 -0.60 1.30 4 5 10 -0.10 1.40 5 -5 10 131.69 4.20 -5 -5 -10 122.59 5.20 5 -5 10 143.59 5.60 -5 5 -10 126.39 5.40 5 5 10 135.09 5.40 6 -5 10 9.50 2.40 -6 -5 -10 5.90 1.90 6 5 10 9.00 2.10 -6 5 -10 6.00 1.70 7 -5 10 85.39 5.20 -7 -5 -10 87.29 4.90 -7 5 -10 87.89 5.00 7 5 10 91.09 4.90 -8 -5 -10 42.90 3.90 8 -5 10 44.70 4.60 8 5 10 47.50 4.00 -8 5 -10 50.99 4.30 -9 -5 -10 77.59 4.80 9 -5 10 76.39 5.90 -9 5 -10 69.79 5.30 9 5 10 75.99 5.00 10 -5 10 12.80 3.70 -10 5 -10 10.00 3.00 10 5 10 9.90 3.00 -11 -5 -10 28.20 4.40 11 -5 10 30.50 6.10 11 5 10 30.00 4.00 12 -5 10 -4.10 4.00 -12 -5 -10 -1.70 2.90 -12 5 -10 4.00 3.30 12 5 10 0.10 3.20 19 6 -10 37.30 6.90 18 -6 -10 12.20 7.40 -18 6 10 15.40 4.70 18 6 -10 15.90 3.90 17 -6 -10 33.70 4.50 -17 -6 10 29.10 4.00 17 6 -10 34.60 5.40 16 -6 -10 7.80 3.00 -16 -6 10 4.90 3.10 16 6 -10 8.30 3.00 -16 6 10 13.40 3.60 -15 -6 10 31.30 4.50 15 -6 -10 29.60 4.20 -15 6 10 30.70 4.90 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145.79 7.00 12 7 -10 157.78 6.70 11 -7 -10 0.30 1.60 -11 -7 10 0.60 1.70 -11 7 10 -0.50 2.20 11 7 -10 0.90 1.80 -10 -7 10 9.10 2.20 10 -7 -10 9.60 2.00 -10 7 10 5.80 2.20 10 7 -10 3.80 2.00 -9 -7 10 -0.30 1.50 9 -7 -10 1.00 1.60 9 7 -10 2.80 1.80 -9 7 10 0.20 1.50 8 -7 -10 29.60 2.80 -8 -7 10 30.20 2.90 -8 7 10 29.50 2.90 8 7 -10 30.50 3.10 -7 -7 10 3.40 1.50 7 -7 -10 1.60 1.30 7 7 -10 1.10 1.30 -7 7 10 2.70 1.50 -6 -7 10 98.39 4.50 6 -7 -10 98.49 4.40 -6 7 10 97.09 3.50 -6 7 10 99.99 4.60 6 7 -10 99.89 4.50 5 -7 -10 34.10 2.80 -5 -7 10 31.00 2.80 -5 7 10 29.90 2.90 5 7 -10 33.20 2.90 -5 7 10 31.70 2.40 -4 -7 10 207.78 6.70 4 -7 -10 207.68 6.60 4 7 -10 202.38 6.90 -4 7 10 204.58 6.80 -4 7 10 208.88 6.30 3 -7 -10 4.30 1.50 -3 -7 10 5.40 1.60 3 7 -10 3.80 1.50 -3 7 10 4.30 1.50 -2 -7 10 144.39 5.30 2 -7 -10 151.08 4.70 -2 -7 10 138.69 4.30 2 -7 -10 146.39 5.20 -2 7 10 143.89 5.30 2 7 -10 139.69 5.50 -1 -7 10 24.70 2.10 1 -7 -10 28.20 2.20 -1 7 10 28.00 2.60 1 7 -10 25.70 2.60 0 -7 10 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10 35.00 5.60 -10 -7 -10 39.00 4.90 -10 7 -10 45.50 6.00 10 7 10 33.20 4.30 11 -7 10 3.50 4.30 17 -8 -10 4.30 3.60 -17 -8 10 3.10 3.90 17 8 -10 4.30 3.80 -17 8 10 -2.30 4.70 -16 -8 10 19.60 6.90 -16 8 10 13.30 4.20 16 8 -10 14.30 3.80 -15 -8 10 3.90 3.00 15 -8 -10 2.00 2.80 -15 8 10 3.70 3.50 15 8 -10 3.70 3.30 -14 -8 10 29.40 4.50 14 -8 -10 25.10 4.20 14 8 -10 16.50 3.60 -14 8 10 17.10 4.00 -13 -8 10 23.20 3.30 13 -8 -10 24.90 3.90 13 8 -10 21.20 3.70 -13 8 10 19.60 3.70 -12 -8 10 4.90 2.30 12 -8 -10 4.20 2.30 -12 8 10 10.70 2.90 12 8 -10 6.00 2.60 11 -8 -10 9.00 2.30 -11 -8 10 7.40 2.30 -11 8 10 1.50 2.40 11 8 -10 5.30 2.30 -10 -8 10 123.19 5.80 10 -8 -10 109.89 5.50 10 8 -10 120.39 5.80 -10 8 10 130.49 6.10 -9 -8 10 45.90 3.80 9 -8 -10 49.00 3.50 -9 8 10 42.60 4.00 9 8 -10 40.10 4.00 -8 -8 10 182.68 7.00 8 -8 -10 175.38 6.60 -8 8 10 178.48 7.00 8 8 -10 177.28 6.90 -7 -8 10 66.99 4.20 7 -8 -10 73.69 4.00 -7 8 10 69.49 4.30 7 8 -10 69.39 4.20 -6 -8 10 168.48 6.40 6 -8 -10 167.48 6.10 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65.59 3.50 -1 -2 14 5.30 1.40 1 -2 -14 8.10 1.40 -1 2 14 5.00 1.40 1 2 -14 4.30 1.30 1 2 -14 5.50 1.40 0 -2 14 4.80 1.50 0 -2 -14 7.60 1.60 0 -2 -14 6.30 1.20 0 2 -14 6.90 1.60 0 2 14 8.90 1.80 0 2 -14 6.40 1.40 1 -2 14 82.69 4.10 -1 -2 -14 80.69 4.00 1 2 14 73.69 4.00 -1 2 -14 77.59 4.00 2 -2 14 16.50 2.60 -2 -2 -14 9.90 2.00 -2 2 -14 14.80 2.50 2 2 14 9.00 1.90 3 -2 14 158.38 6.20 -3 -2 -14 153.88 6.10 -3 2 -14 153.58 6.20 3 2 14 148.19 6.10 -4 -2 -14 3.00 1.90 4 -2 14 0.20 1.60 4 2 14 1.20 1.60 -4 2 -14 1.10 1.70 5 -2 14 10.30 2.70 -5 -2 -14 17.40 3.30 5 2 14 11.20 2.40 -5 2 -14 16.40 3.20 -6 -2 -14 20.70 3.50 6 -2 14 15.10 2.90 -6 2 -14 13.90 2.70 6 2 14 12.30 2.60 7 -2 14 0.10 2.40 -7 -2 -14 5.50 2.20 7 2 14 2.30 2.10 -7 2 -14 -0.20 2.10 -8 -2 -14 1.90 3.80 8 -2 14 0.50 3.40 8 2 14 3.30 3.20 -9 -2 -14 26.30 5.00 9 2 14 29.60 4.80 -9 2 -14 25.40 4.90 19 -3 -14 7.30 3.90 -19 -3 14 0.20 4.20 19 3 -14 15.10 4.80 -19 3 14 8.10 4.30 18 -3 -14 18.80 4.80 -18 -3 14 20.60 4.20 -18 3 14 28.70 5.00 18 3 -14 28.50 5.60 17 -3 -14 8.30 3.20 -17 -3 14 3.80 3.20 17 3 -14 6.40 3.70 -17 3 14 3.00 3.20 -16 -3 14 53.79 5.00 16 -3 -14 58.59 5.40 16 3 -14 56.09 4.40 -16 3 14 66.39 5.80 16 3 -14 60.59 5.70 -15 -3 14 40.20 4.40 15 -3 -14 47.50 4.70 -15 3 14 38.60 4.90 15 3 -14 39.50 4.60 -14 -3 14 109.49 5.60 -14 -3 14 116.29 5.40 14 -3 -14 113.39 6.10 -14 3 14 118.69 6.20 14 3 -14 113.99 5.20 -13 -3 14 29.60 3.50 -13 -3 14 24.80 3.20 13 -3 -14 32.40 3.80 -13 3 14 31.70 3.80 13 3 -14 33.90 3.40 12 -3 -14 63.19 4.40 -12 -3 14 62.99 3.80 -12 -3 14 67.99 4.00 12 3 -14 58.29 4.10 -12 3 14 60.19 4.70 11 -3 -14 -0.40 1.70 -11 -3 14 2.30 1.60 -11 -3 14 -0.20 1.60 -11 3 14 -0.50 1.80 11 3 -14 0.90 1.70 -10 -3 14 23.00 2.70 10 -3 -14 17.50 2.60 -10 -3 14 21.80 2.50 10 3 -14 20.30 2.80 -10 3 14 23.50 3.00 -9 -3 14 4.80 1.70 -9 -3 14 7.10 1.90 9 -3 -14 3.50 1.60 -9 3 14 9.70 2.00 9 3 -14 6.70 1.70 8 -3 -14 3.40 1.60 -8 -3 14 7.80 1.60 8 3 -14 8.90 1.70 -8 3 14 5.90 1.70 7 -3 -14 103.29 3.40 -7 -3 14 106.69 4.50 -7 -3 14 110.39 4.40 7 -3 -14 106.79 4.60 -7 3 14 104.79 4.80 7 3 -14 114.29 4.50 -6 -3 14 56.09 4.50 6 -3 -14 57.49 2.60 6 3 -14 62.29 3.40 -6 3 14 57.99 3.50 5 -3 -14 64.59 3.40 5 -3 -14 67.19 2.90 -5 -3 14 71.09 3.40 -5 -3 14 68.09 3.40 -5 3 14 59.29 3.70 4 -3 -14 203.68 6.00 -4 -3 14 213.08 6.30 -4 -3 14 201.68 6.30 4 -3 -14 198.98 6.20 4 3 -14 197.58 6.30 -4 3 14 196.18 6.70 -3 -3 14 259.47 7.10 3 -3 -14 254.57 7.20 -3 -3 14 239.38 8.10 3 -3 -14 244.38 7.10 3 3 -14 249.58 7.50 -3 3 14 243.88 7.60 -2 -3 14 43.60 2.80 2 -3 -14 41.90 2.90 2 -3 -14 41.90 2.70 -2 -3 14 44.20 2.60 2 3 -14 44.10 2.90 -2 3 14 43.90 3.00 -1 -3 14 18.60 2.30 1 -3 -14 21.70 2.50 -1 -3 14 21.00 2.00 1 -3 -14 14.50 1.90 1 3 -14 17.20 2.30 -1 3 14 18.20 2.20 0 -3 14 0.30 1.30 0 -3 -14 -0.60 1.20 0 -3 14 2.30 1.20 0 -3 -14 0.40 1.20 0 3 14 0.10 1.20 0 3 -14 -0.10 1.10 1 -3 14 13.80 2.40 -1 -3 -14 16.30 2.40 -1 3 -14 17.30 2.60 1 3 14 18.70 2.50 -2 -3 -14 29.20 3.00 2 -3 14 30.90 3.00 -2 3 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14 4 -14 3.00 1.90 -14 4 14 -0.10 2.20 13 -4 -14 28.10 3.70 -13 -4 14 27.00 3.30 -13 -4 14 25.40 3.40 13 4 -14 20.50 3.30 -13 4 14 29.40 3.90 -12 -4 14 29.70 3.20 -12 -4 14 30.80 3.40 12 -4 -14 31.90 3.40 12 4 -14 29.30 3.30 -12 4 14 34.40 3.90 11 -4 -14 28.30 3.80 -11 -4 14 24.80 2.80 -11 -4 14 23.40 3.10 11 4 -14 30.40 3.10 -11 4 14 26.10 3.40 -10 -4 14 196.38 6.90 -10 -4 14 186.48 6.30 10 -4 -14 192.18 7.00 10 4 -14 185.08 8.10 -10 4 14 203.98 7.30 -9 -4 14 18.40 2.40 -9 -4 14 23.50 2.60 9 -4 -14 19.70 2.80 -9 4 14 23.20 3.10 9 4 -14 19.30 2.60 -8 -4 14 283.37 8.50 -8 -4 14 272.57 8.30 8 -4 -14 282.97 8.50 -8 4 14 273.67 8.80 8 4 -14 287.37 8.20 -7 -4 14 22.40 2.30 -7 -4 14 22.90 2.50 7 -4 -14 15.40 2.50 7 4 -14 17.80 2.40 -7 4 14 22.30 2.60 -6 -4 14 55.09 3.30 6 -4 -14 56.99 3.30 -6 -4 14 56.29 3.30 6 -4 -14 56.59 2.60 -6 4 14 61.79 3.60 6 4 -14 49.00 3.20 -5 -4 14 137.39 4.80 5 -4 -14 125.79 4.20 -5 4 14 127.99 5.20 5 4 -14 122.59 4.90 -4 -4 14 27.90 2.80 -4 -4 14 31.20 2.50 4 -4 -14 29.40 2.20 4 -4 -14 34.50 2.80 -4 4 14 26.50 2.70 4 4 -14 28.40 2.60 3 -4 -14 11.10 1.70 -3 -4 14 11.60 2.00 3 -4 -14 9.30 1.80 -3 -4 14 8.70 1.70 -3 4 14 8.80 1.80 3 4 -14 8.90 1.80 -2 -4 14 6.90 1.50 2 -4 -14 6.50 1.50 2 -4 -14 6.60 1.60 -2 -4 14 4.60 1.70 -2 4 14 7.40 1.70 2 4 -14 4.90 1.50 1 -4 -14 -1.90 1.20 1 -4 -14 -0.20 1.20 -1 -4 14 0.40 1.20 -1 -4 14 1.40 1.40 -1 4 14 1.80 1.30 1 4 -14 0.70 1.30 0 -4 14 156.28 4.90 0 -4 -14 162.88 5.70 0 -4 -14 154.08 5.00 0 -4 14 160.38 5.80 0 4 -14 160.68 6.10 0 4 14 152.78 5.80 1 -4 14 12.90 2.10 -1 -4 -14 17.70 2.60 1 -4 14 17.20 2.70 -1 -4 -14 15.60 2.10 1 4 14 14.40 2.50 -1 4 -14 19.00 2.60 2 -4 14 257.87 8.30 -2 -4 -14 258.57 8.30 2 4 14 259.57 8.40 -2 4 -14 258.47 8.60 3 -4 14 -0.50 1.80 -3 -4 -14 1.10 1.60 -3 4 -14 0.50 1.50 3 4 14 1.20 1.70 -4 -4 -14 171.18 6.70 4 -4 14 158.78 6.70 4 4 14 155.48 6.50 -4 4 -14 158.18 6.70 -5 -4 -14 -0.40 1.90 5 -4 14 -4.00 2.10 5 4 14 1.00 2.00 -5 4 -14 0.70 1.90 -6 -4 -14 30.50 3.90 6 -4 14 23.50 3.70 -6 4 -14 23.70 3.60 6 4 14 20.40 3.20 -7 -4 -14 3.90 2.40 7 -4 14 -0.40 2.80 7 4 14 -2.30 2.50 -7 4 -14 2.40 2.50 -8 -4 -14 2.20 2.70 8 -4 14 8.40 4.00 -8 4 -14 -2.10 2.60 8 4 14 -3.20 2.90 9 -4 14 3.30 3.80 -9 -4 -14 1.40 3.20 -9 4 -14 2.70 3.10 9 4 14 2.50 3.30 -18 -5 14 1.60 3.60 18 -5 -14 7.00 3.80 18 5 -14 5.70 4.40 -18 5 14 3.40 4.10 -17 5 14 25.00 6.10 17 5 -14 19.60 3.60 -16 -5 14 17.40 3.10 16 -5 -14 8.50 3.40 16 5 -14 11.00 3.00 -15 -5 14 57.69 4.80 -15 -5 14 49.10 5.90 15 -5 -14 50.29 5.00 -15 5 14 57.79 5.80 15 5 -14 51.49 4.70 -14 -5 14 18.00 3.00 14 -5 -14 15.60 3.10 -14 -5 14 19.40 4.30 -14 5 14 19.00 3.40 14 5 -14 24.40 3.80 13 -5 -14 72.49 5.00 -13 -5 14 60.99 4.80 -13 -5 14 77.29 4.50 -13 5 14 82.99 5.30 13 5 -14 77.49 4.60 -12 -5 14 7.90 2.30 -12 -5 14 5.80 2.10 12 -5 -14 3.90 2.20 -12 5 14 3.60 2.40 12 5 -14 3.40 2.00 -11 -5 14 12.60 2.50 -11 -5 14 13.10 2.10 11 -5 -14 14.60 2.50 11 5 -14 12.80 2.20 -11 5 14 13.80 2.70 -10 -5 14 -0.90 1.50 10 -5 -14 1.00 1.80 -10 -5 14 -0.70 1.60 10 5 -14 4.00 1.80 -10 5 14 -1.90 1.50 -9 -5 14 -1.10 1.40 9 -5 -14 -0.10 1.80 -9 -5 14 2.10 1.50 9 5 -14 0.00 1.50 -9 5 14 2.50 1.90 -8 -5 14 7.30 1.50 8 -5 -14 8.10 1.90 -8 -5 14 7.40 1.90 8 5 -14 7.90 1.80 -8 5 14 5.40 1.80 -7 -5 14 9.10 1.70 -7 -5 14 10.30 1.90 7 -5 -14 8.60 1.90 -7 5 14 8.90 1.90 7 5 -14 9.20 1.80 -6 -5 14 5.70 1.60 -6 -5 14 5.30 1.60 6 -5 -14 4.60 1.10 6 -5 -14 3.00 1.70 -6 5 14 3.90 1.80 6 5 -14 3.40 1.50 5 -5 -14 95.49 3.50 -5 -5 14 92.99 4.20 5 -5 -14 89.19 4.20 -5 -5 14 93.69 3.90 -5 5 14 90.79 4.60 5 5 -14 94.19 4.30 -4 -5 14 200.78 6.10 4 -5 -14 190.78 6.30 -4 -5 14 192.38 6.30 4 -5 -14 188.58 5.70 4 5 -14 200.58 6.60 -4 5 14 189.18 6.90 3 -5 -14 99.79 4.10 -3 -5 14 96.19 4.00 3 -5 -14 94.39 4.30 -3 -5 14 96.69 4.20 -3 5 14 96.29 4.60 3 5 -14 96.89 4.40 -2 -5 14 40.00 2.80 2 -5 -14 34.40 2.80 2 -5 -14 39.70 2.90 -2 5 14 39.30 3.20 2 5 -14 39.40 3.10 1 -5 -14 54.19 3.30 -1 -5 14 56.19 3.30 1 -5 -14 58.99 3.20 -1 -5 14 57.89 3.10 -1 5 14 56.99 3.60 1 5 -14 55.09 3.70 0 -5 14 0.90 1.30 0 -5 -14 0.10 1.30 0 -5 -14 -0.30 1.50 0 -5 14 -1.90 1.40 0 5 14 0.70 1.50 0 5 -14 0.20 1.40 1 -5 14 1.60 1.40 -1 -5 -14 -1.60 1.50 -1 -5 -14 1.20 1.40 1 -5 14 1.80 1.70 -1 5 -14 -1.10 1.40 1 5 14 0.30 1.50 2 -5 14 29.10 3.20 2 -5 14 27.70 2.50 -2 -5 -14 28.40 3.30 2 5 14 26.10 3.30 -2 5 -14 28.30 3.20 -3 -5 -14 27.80 3.50 3 -5 14 23.60 3.50 -3 5 -14 28.90 3.40 3 5 14 28.40 3.30 -4 -5 -14 4.50 2.20 4 -5 14 4.00 2.40 -4 5 -14 6.20 2.20 4 5 14 3.30 2.10 -5 -5 -14 43.40 4.30 5 -5 14 42.10 4.80 -5 5 -14 48.00 4.50 5 5 14 53.19 4.50 -6 -5 -14 16.30 3.00 6 -5 14 12.60 3.50 -6 5 -14 19.10 3.30 6 5 14 23.50 4.10 7 -5 14 44.70 5.50 -7 -5 -14 32.70 6.10 -7 5 -14 39.50 5.10 7 5 14 35.90 4.70 8 -5 14 4.70 3.40 -8 -5 -14 1.40 2.70 -8 5 -14 2.70 3.20 8 5 14 6.20 3.20 18 -6 -14 10.00 4.20 -18 -6 14 11.60 3.90 18 6 -14 6.90 3.80 -18 6 14 0.10 4.80 17 -6 -14 15.50 3.90 -17 -6 14 3.20 3.60 17 6 -14 1.40 3.30 -17 6 14 8.30 4.30 -16 -6 14 0.60 3.60 16 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14 23.00 2.90 5 6 -14 19.40 2.80 4 -6 -14 2.60 1.40 -4 -6 14 5.30 1.60 4 -6 -14 5.40 1.70 -4 -6 14 3.70 1.60 -4 6 14 6.10 1.90 4 6 -14 4.10 1.70 3 -6 -14 0.00 1.40 -3 -6 14 0.30 1.50 -3 -6 14 -1.40 1.40 3 -6 -14 0.10 1.30 -3 6 14 0.90 1.70 3 6 -14 -0.40 1.50 2 -6 -14 67.79 4.10 -2 -6 14 64.99 3.50 -2 -6 14 67.39 3.70 2 -6 -14 70.09 3.70 -2 6 14 78.79 4.30 2 6 -14 74.49 4.10 1 -6 -14 19.40 2.50 -1 -6 14 16.00 2.60 1 -6 -14 17.60 2.70 -1 -6 14 16.40 2.60 1 6 -14 18.00 2.80 -1 6 14 14.30 2.30 0 -6 14 72.19 4.00 0 -6 14 82.59 3.90 0 -6 -14 73.79 4.30 0 -6 -14 82.89 4.00 0 6 14 82.69 4.40 0 6 -14 84.29 4.60 -1 -6 -14 81.49 4.00 -1 -6 -14 81.69 4.40 1 -6 14 84.79 4.40 1 -6 14 87.09 4.00 -1 6 -14 84.09 4.80 1 6 14 83.39 4.50 2 -6 14 41.30 3.40 -2 -6 -14 35.60 3.50 2 -6 14 34.20 3.50 2 6 14 36.60 3.60 -2 6 -14 36.20 3.70 3 -6 14 108.29 5.60 -3 -6 -14 112.49 5.50 -3 6 -14 118.89 5.80 3 6 14 117.69 5.60 -4 -6 -14 22.50 3.60 4 -6 14 15.60 3.10 4 6 14 19.00 3.10 -4 6 -14 24.80 3.90 -5 -6 -14 20.60 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3.70 5 3 -21 10.10 2.60 -4 -3 21 1.10 2.70 4 -3 -21 5.40 2.40 4 3 -21 7.60 2.60 -4 3 21 -1.70 2.90 3 -3 -21 4.60 2.40 -3 -3 21 1.90 2.70 -3 3 21 1.60 2.90 3 3 -21 2.60 2.70 2 -3 -21 1.30 2.40 -2 -3 21 0.90 3.20 2 3 -21 2.50 2.70 -2 3 21 -2.40 2.60 1 -3 -21 5.70 2.70 -1 3 21 4.20 2.80 1 3 -21 3.00 2.70 0 -3 21 -2.20 3.20 0 -3 -21 2.60 3.10 0 3 21 -0.60 3.00 0 3 -21 -4.20 2.80 14 -4 -21 7.80 3.80 14 4 -21 -2.60 4.30 -14 4 21 8.20 4.30 13 -4 -21 30.30 4.70 -13 -4 21 39.80 5.60 13 4 -21 30.10 4.80 -13 4 21 45.90 6.20 -12 -4 21 -1.00 3.10 12 -4 -21 -2.10 3.40 -12 4 21 11.80 3.50 12 4 -21 3.20 3.70 12 4 -21 1.70 2.40 -11 -4 21 18.50 3.70 11 -4 -21 27.10 4.20 -11 4 21 25.90 4.60 11 4 -21 16.50 3.20 10 -4 -21 -2.50 3.00 -10 -4 21 -1.10 2.80 10 4 -21 -2.80 2.30 -10 4 21 7.90 3.30 10 4 -21 0.80 3.10 -9 -4 21 0.00 3.00 9 -4 -21 -0.30 3.00 -9 4 21 2.60 3.60 9 4 -21 0.10 2.30 9 4 -21 3.40 3.20 8 -4 -21 -1.90 2.90 -8 -4 21 4.10 2.90 8 4 -21 3.80 2.20 -8 4 21 3.80 4.90 8 4 -21 -0.10 3.00 -7 -4 21 8.70 2.90 7 -4 -21 -2.10 2.80 -7 4 21 11.00 5.20 7 4 -21 1.80 3.10 7 4 -21 4.90 2.50 6 -4 -21 -0.10 2.60 -6 -4 21 1.90 2.50 6 4 -21 0.60 2.30 6 4 -21 -0.70 2.60 -6 4 21 5.20 3.20 -5 -4 21 32.70 4.60 -5 4 21 33.30 4.50 5 4 -21 40.30 4.50 4 -4 -21 5.90 2.40 -4 -4 21 1.70 2.80 4 4 -21 4.40 2.60 -4 4 21 4.50 3.10 -3 -4 21 55.49 5.40 3 -4 -21 61.09 4.90 3 4 -21 61.69 5.20 -3 4 21 63.69 5.50 2 -4 -21 9.60 2.60 -2 -4 21 2.80 3.00 2 4 -21 4.00 3.00 -2 4 21 1.00 3.20 1 -4 -21 14.80 3.60 1 4 -21 13.40 3.30 -1 4 21 9.30 3.70 13 -5 -21 -1.60 3.60 -13 5 21 -3.30 3.80 13 5 -21 -1.10 2.70 12 -5 -21 4.40 3.60 -12 5 21 2.00 3.70 12 5 -21 7.40 2.90 -11 -5 21 7.40 3.30 11 -5 -21 8.40 3.60 11 5 -21 -1.30 2.60 -11 5 21 0.40 3.70 -10 -5 21 6.50 3.30 10 -5 -21 8.70 3.40 10 5 -21 8.90 2.90 -10 5 21 12.60 3.80 -9 -5 21 5.60 3.00 -9 -5 21 0.10 3.00 9 -5 -21 0.40 2.90 9 5 -21 -2.30 2.60 -9 5 21 7.60 3.40 -8 -5 21 4.80 3.00 -8 -5 21 5.50 3.10 8 -5 -21 12.80 3.20 8 5 -21 1.80 2.70 -8 5 21 7.80 3.50 7 -5 -21 4.20 2.80 -7 -5 21 8.60 3.00 7 5 -21 3.00 2.50 -7 5 21 8.30 3.20 -6 -5 21 10.10 3.20 6 -5 -21 4.80 2.80 6 5 -21 3.90 2.70 -6 5 21 1.80 3.30 -5 -5 21 1.10 2.90 -5 5 21 -3.00 2.80 5 5 -21 -3.00 2.40 -4 -5 21 0.20 2.90 -4 5 21 0.00 3.50 -3 -5 21 6.80 3.10 3 5 -21 4.60 2.80 2 -5 -21 11.60 3.20 -2 -5 21 15.00 3.40 -2 5 21 13.00 3.50 2 5 -21 10.80 3.10 12 -6 -21 18.60 4.30 -12 -6 21 25.30 4.30 -11 -6 21 2.90 3.20 11 -6 -21 5.80 3.60 -11 6 21 -4.90 3.60 11 6 -21 1.30 2.90 -10 -6 21 14.10 3.30 10 -6 -21 10.40 3.90 10 6 -21 4.00 3.10 -10 6 21 10.40 3.90 9 -6 -21 1.00 3.30 -9 -6 21 4.20 3.00 -9 6 21 1.10 3.40 9 6 -21 1.10 2.70 8 -6 -21 -0.70 3.10 -8 -6 21 3.00 2.90 -8 6 21 4.00 3.50 -7 -6 21 4.10 2.80 7 -6 -21 -1.40 3.10 -7 6 21 4.90 3.40 7 6 -21 -2.40 2.60 6 -6 -21 9.30 3.40 -6 -6 21 9.00 2.90 -6 6 21 9.30 3.50 5 6 -21 7.50 3.00 -5 6 21 5.10 3.80 -4 -6 21 37.10 5.30 4 6 -21 31.30 5.10 -4 6 21 41.20 6.30 15 0 -22 -9.10 4.40 -15 0 22 -2.20 4.30 14 0 -22 30.90 5.20 -14 0 22 23.10 6.40 -13 0 22 0.60 3.80 12 0 -22 43.40 6.60 -12 0 22 43.30 6.10 -11 0 22 1.80 3.10 11 0 -22 -0.70 3.20 -10 0 22 13.20 3.80 10 0 -22 16.10 3.70 -9 0 22 4.60 3.20 9 0 -22 -4.60 2.90 8 0 -22 3.30 3.10 8 0 -22 4.10 2.30 -8 0 22 5.30 3.30 7 0 -22 0.80 2.30 7 0 -22 1.10 2.70 -7 0 22 0.20 2.90 -6 0 22 12.20 3.30 6 0 -22 2.10 2.30 -5 0 22 2.40 4.70 5 0 -22 -0.80 2.10 -4 0 22 31.40 4.60 4 0 -22 32.30 4.40 -3 0 22 -1.70 2.80 3 0 -22 0.80 2.40 2 0 -22 28.40 4.60 -2 0 22 24.00 3.80 1 0 -22 -3.80 2.80 -1 0 22 0.20 2.90 15 -1 -22 12.80 5.00 15 1 -22 15.50 5.20 14 -1 -22 14.10 4.20 -14 -1 22 16.10 4.70 -14 1 22 14.60 4.80 14 1 -22 15.50 4.60 -13 -1 22 4.10 3.90 -13 1 22 2.10 3.60 -12 -1 22 -2.60 3.30 12 -1 -22 0.70 4.10 12 1 -22 0.20 4.00 11 -1 -22 -2.70 3.10 -11 -1 22 0.20 3.00 -11 1 22 0.60 3.30 11 1 -22 0.60 3.30 10 -1 -22 3.00 3.20 -10 -1 22 0.50 3.20 10 1 -22 -6.00 3.20 -10 1 22 0.60 3.30 -9 -1 22 10.40 3.40 9 -1 -22 6.00 3.10 -9 1 22 11.80 3.40 9 1 -22 8.70 2.40 9 1 -22 2.40 3.20 -8 -1 22 29.40 5.30 8 -1 -22 24.00 3.70 8 1 -22 30.90 4.20 8 1 -22 35.20 4.10 -8 1 22 41.00 5.60 7 -1 -22 36.60 4.60 -7 -1 22 28.50 4.90 7 -1 -22 37.30 3.90 7 1 -22 32.60 4.10 7 1 -22 27.20 4.70 -7 1 22 32.80 5.60 6 -1 -22 23.70 3.90 6 1 -22 22.90 4.30 5 -1 -22 9.50 2.70 -5 1 22 9.60 3.40 5 1 -22 14.70 3.00 4 -1 -22 14.60 3.30 4 1 -22 14.50 3.10 -4 1 22 12.90 3.30 3 -1 -22 14.20 3.00 -3 -1 22 22.00 3.60 -3 1 22 18.70 3.60 3 1 -22 16.40 3.20 -2 -1 22 7.40 3.30 2 -1 -22 9.60 2.90 -2 1 22 15.80 3.60 2 1 -22 11.60 3.10 -14 -2 22 1.70 3.90 14 -2 -22 1.00 3.70 -14 2 22 -4.60 4.30 14 2 -22 7.40 4.30 13 -2 -22 35.40 4.70 -13 -2 22 35.10 6.30 -13 2 22 50.59 6.70 13 2 -22 54.89 7.10 12 -2 -22 -0.80 3.50 -12 -2 22 -3.00 3.30 -12 2 22 1.70 3.50 12 2 -22 6.10 4.30 11 -2 -22 57.49 5.90 -11 -2 22 50.69 5.70 -11 2 22 65.59 6.20 11 2 -22 61.99 6.70 10 -2 -22 4.90 3.00 -10 -2 22 -1.40 3.10 10 2 -22 -2.10 3.40 10 2 -22 3.20 2.90 -10 2 22 -2.30 3.70 9 -2 -22 17.00 3.40 -9 -2 22 22.50 3.90 -9 2 22 17.90 4.80 9 2 -22 18.40 2.90 9 2 -22 22.50 3.80 8 -2 -22 0.10 3.00 -8 -2 22 -2.30 3.20 8 2 -22 0.70 3.20 -8 2 22 1.80 3.50 -7 -2 22 13.90 3.30 7 -2 -22 3.50 3.10 7 2 -22 9.40 3.30 7 2 -22 8.80 2.80 -7 2 22 10.50 3.60 -6 -2 22 4.70 2.80 6 -2 -22 5.50 2.60 -6 2 22 1.60 2.90 6 2 -22 0.00 2.50 -5 -2 22 9.70 3.50 5 -2 -22 8.60 2.60 -5 2 22 7.50 2.90 5 2 -22 7.50 2.70 4 -2 -22 3.00 2.60 -4 -2 22 3.10 3.10 -4 2 22 -3.10 2.60 4 2 -22 0.60 2.50 3 -2 -22 8.50 2.90 -3 -2 22 14.60 3.50 3 2 -22 10.00 3.30 -3 2 22 9.50 3.60 2 -2 -22 3.20 2.80 -2 -2 22 4.60 3.20 2 2 -22 2.80 3.20 -2 2 22 2.90 3.30 14 -3 -22 2.10 3.80 14 3 -22 3.50 4.70 13 -3 -22 2.00 3.80 -13 -3 22 2.00 3.60 13 3 -22 -6.50 4.20 -13 3 22 -4.20 3.70 -12 -3 22 -1.80 3.20 -12 3 22 4.90 3.50 11 -3 -22 -1.90 3.30 -11 -3 22 0.70 3.20 11 3 -22 -4.10 3.70 -11 3 22 5.00 3.60 -10 -3 22 9.30 3.50 10 -3 -22 5.30 3.30 10 3 -22 1.40 2.60 10 3 -22 2.60 3.60 -10 3 22 2.80 3.40 -9 -3 22 11.00 3.40 9 -3 -22 2.60 3.20 -9 3 22 4.00 3.20 9 3 -22 7.40 2.50 9 3 -22 1.50 3.60 -8 -3 22 37.40 5.50 8 -3 -22 31.00 5.20 -8 3 22 32.30 5.60 8 3 -22 35.00 5.70 8 3 -22 33.00 4.30 -7 -3 22 13.60 3.50 7 -3 -22 15.60 3.50 7 3 -22 15.90 3.10 7 3 -22 17.20 3.70 -7 3 22 14.50 4.00 -6 -3 22 55.99 5.30 6 3 -22 47.50 4.80 -6 3 22 51.69 5.70 5 -3 -22 10.00 4.10 -5 -3 22 7.70 3.10 -5 3 22 13.60 3.70 5 3 -22 9.10 3.00 -4 -3 22 32.80 5.20 4 3 -22 29.00 5.00 -4 3 22 27.40 4.30 -3 -3 22 21.10 4.60 3 -3 -22 31.20 4.90 -3 3 22 11.20 3.40 13 -4 -22 -4.80 3.90 13 4 -22 3.00 4.10 -12 -4 22 17.30 3.90 12 -4 -22 26.70 4.70 -12 4 22 16.30 4.40 12 4 -22 17.80 4.40 -11 -4 22 1.00 3.40 11 -4 -22 0.00 3.50 -11 4 22 -0.30 3.60 11 4 -22 -0.20 3.70 11 4 -22 2.30 2.80 10 -4 -22 8.50 3.70 -10 -4 22 11.60 3.60 10 4 -22 12.00 2.80 -10 4 22 10.50 3.90 10 4 -22 6.80 3.70 -9 -4 22 9.70 3.60 9 -4 -22 10.50 3.70 -9 4 22 9.50 3.80 9 4 -22 6.80 3.60 9 4 -22 4.90 2.70 -8 -4 22 5.30 3.10 8 -4 -22 -5.50 3.10 8 4 -22 6.70 3.40 8 4 -22 1.10 2.70 -8 4 22 6.70 3.50 7 -4 -22 2.80 2.90 -7 -4 22 4.10 3.20 7 4 -22 7.30 3.40 7 4 -22 -0.60 2.40 -7 4 22 2.20 3.10 -6 -4 22 6.20 3.20 6 4 -22 1.40 2.70 -6 4 22 5.00 3.50 -5 -4 22 0.80 3.00 5 4 -22 3.20 3.00 -5 4 22 -1.00 3.50 -4 -4 22 32.00 5.40 -4 4 22 45.30 5.70 4 4 -22 56.69 6.90 11 -5 -22 1.80 3.60 11 5 -22 -1.30 4.20 -11 5 22 4.50 4.10 10 -5 -22 -7.20 3.40 -10 5 22 -5.90 3.20 10 5 -22 -5.00 4.20 10 5 -22 0.60 2.80 9 -5 -22 9.30 3.40 9 5 -22 5.20 3.90 9 5 -22 4.10 2.90 -9 5 22 10.70 4.20 -8 -5 22 9.00 3.60 8 -5 -22 5.80 3.50 8 5 -22 11.50 3.10 8 5 -22 13.10 3.90 -8 5 22 11.00 4.20 7 -5 -22 24.70 3.90 -7 -5 22 24.80 3.90 -7 5 22 28.70 4.80 7 5 -22 23.80 3.80 7 5 -22 26.50 4.30 -6 -5 22 3.00 3.50 -6 5 22 1.80 3.90 -5 -5 22 24.20 4.00 -5 5 22 26.30 4.80 5 5 -22 26.70 4.80 13 0 -23 16.40 4.50 -12 0 23 5.90 4.00 11 0 -23 21.40 4.50 -11 0 23 30.80 4.30 10 0 -23 3.20 3.60 -10 0 23 4.10 3.70 9 0 -23 27.10 4.30 8 0 -23 3.80 3.30 -8 0 23 3.60 3.40 7 0 -23 17.50 3.10 -7 0 23 25.70 4.20 6 0 -23 -1.40 2.50 -6 0 23 -1.60 3.40 5 0 -23 2.90 2.60 -4 0 23 -3.00 3.30 4 0 -23 1.80 2.60 12 -1 -23 5.60 4.90 -12 -1 23 3.10 5.10 -12 1 23 3.10 4.10 12 1 -23 1.70 5.30 11 -1 -23 10.40 3.90 11 1 -23 18.60 4.40 -11 1 23 12.00 4.00 10 -1 -23 6.20 3.50 -10 1 23 4.30 3.60 10 1 -23 2.60 4.00 9 -1 -23 -3.00 3.20 9 1 -23 -5.30 3.40 -9 1 23 2.50 3.30 8 -1 -23 4.80 3.20 8 1 -23 1.30 3.50 -8 1 23 6.60 3.30 8 1 -23 0.00 2.80 -7 -1 23 2.20 3.20 -7 1 23 6.70 3.50 7 1 -23 -1.10 2.70 -6 -1 23 15.10 3.70 6 -1 -23 10.60 2.90 6 1 -23 6.70 2.90 -6 1 23 -0.70 3.70 -5 -1 23 9.60 3.50 5 -1 -23 4.90 2.70 5 1 -23 7.30 3.00 -5 1 23 5.10 3.30 -4 -1 23 14.40 4.20 -4 1 23 18.70 3.90 -12 -2 23 47.80 7.30 12 -2 -23 53.79 6.40 12 2 -23 61.19 7.50 -12 2 23 45.60 7.30 -11 -2 23 1.60 3.50 11 -2 -23 5.00 3.70 -11 2 23 5.00 3.60 11 2 -23 3.60 4.40 -10 -2 23 42.40 6.60 10 -2 -23 37.10 5.90 10 2 -23 31.80 4.90 -10 2 23 47.10 6.80 -9 -2 23 5.30 3.70 9 -2 -23 0.00 3.30 9 2 -23 -2.20 2.90 9 2 -23 1.10 3.40 -9 2 23 1.20 3.60 8 -2 -23 47.80 6.20 -8 -2 23 66.09 6.50 -8 2 23 63.59 6.30 8 2 -23 64.59 5.50 8 2 -23 56.69 6.50 7 2 -23 3.40 2.70 -7 2 23 3.60 3.40 -6 -2 23 20.90 4.10 6 2 -23 21.10 3.50 -6 2 23 17.60 4.20 5 -2 -23 -2.90 3.30 -5 -2 23 3.00 3.20 5 2 -23 5.90 3.00 -5 2 23 4.30 3.40 10 -3 -23 -2.50 3.50 -10 -3 23 2.10 3.80 -10 3 23 2.90 3.90 10 3 -23 2.50 3.50 10 3 -23 4.50 3.90 -9 -3 23 4.70 3.50 9 -3 -23 0.30 3.40 -9 3 23 -0.70 3.70 9 3 -23 2.50 2.60 -8 -3 23 -1.40 3.40 8 -3 -23 4.00 3.60 8 3 -23 3.60 3.70 -8 3 23 0.50 3.50 8 3 -23 -0.30 2.80 -7 -3 23 6.70 3.60 -7 3 23 6.50 4.00 6 3 -23 -1.60 3.10 -6 3 23 0.00 3.50 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 9004 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp Ru1 Ru 0.70448(2) 0.61485(2) 0.36274(2) 0.04185(10) Uani 1 1 d D . Cl1 Cl 0.74482(6) 0.40683(7) 0.35837(5) 0.0559(2) Uani 1 1 d D . Cl1S Cl 0.71491(13) 0.18889(16) 0.53977(10) 0.1252(5) Uani 1 1 d . . Cl2S Cl 0.53658(13) 0.3156(3) 0.47620(13) 0.1962(12) Uani 1 1 d . . N3 N 0.76628(18) 0.6085(2) 0.48929(15) 0.0469(6) Uani 1 1 d . . N2 N 0.85237(17) 0.6417(2) 0.39447(15) 0.0431(5) Uani 1 1 d . . N4 N 0.72695(19) 0.6031(2) 0.54423(16) 0.0522(6) Uani 1 1 d . . N1 N 0.8353(2) 0.6386(3) 0.25829(17) 0.0560(7) Uani 1 1 d . . C8 C 0.9087(2) 0.6437(3) 0.47592(18) 0.0451(6) Uani 1 1 d . . C9 C 0.8596(2) 0.6307(3) 0.52868(18) 0.0458(7) Uani 1 1 d . . C16 C 0.5748(2) 0.6755(4) 0.3660(2) 0.0619(9) Uani 1 1 d . . H16 H 0.5532 0.6684 0.4088 0.074 Uiso 1 1 calc R U C11 C 0.7979(2) 0.6217(3) 0.6195(2) 0.0542(8) Uani 1 1 d . . C7 C 1.0080(2) 0.6541(3) 0.5071(2) 0.0547(8) Uani 1 1 d . . H7 H 1.0453 0.6558 0.5653 0.066 Uiso 1 1 calc R U C5 C 0.8942(2) 0.6466(3) 0.33939(19) 0.0467(7) Uani 1 1 d . . C21 C 0.5527(2) 0.5850(3) 0.3061(2) 0.0576(8) Uani 1 1 d . . H21 H 0.5196 0.5155 0.3104 0.069 Uiso 1 1 calc R U C19 C 0.6321(2) 0.6969(3) 0.23615(19) 0.0518(7) Uani 1 1 d . . H19 H 0.6504 0.7066 0.1916 0.062 Uiso 1 1 calc R U C18 C 0.6581(2) 0.7845(3) 0.2994(2) 0.0582(8) Uani 1 1 d . . H18 H 0.6967 0.8499 0.2980 0.070 Uiso 1 1 calc R U C4 C 0.9935(2) 0.6587(3) 0.3683(2) 0.0547(8) Uani 1 1 d . . C17 C 0.6285(2) 0.7778(3) 0.3642(2) 0.0625(9) Uani 1 1 d . . C10 C 0.8830(2) 0.6395(3) 0.6134(2) 0.0550(8) Uani 1 1 d . . H10 H 0.9435 0.6542 0.6570 0.066 Uiso 1 1 calc R U C20 C 0.5797(2) 0.5963(3) 0.2385(2) 0.0533(8) Uani 1 1 d . . C6 C 1.0498(2) 0.6615(3) 0.4541(2) 0.0605(8) Uani 1 1 d . . H6 H 1.1167 0.6686 0.4746 0.073 Uiso 1 1 calc R U C22 C 0.5520(3) 0.4969(3) 0.1746(2) 0.0656(9) Uani 1 1 d . . H22 H 0.5637 0.4188 0.2052 0.079 Uiso 1 1 calc R U C1 C 0.8740(3) 0.6453(3) 0.2048(2) 0.0659(9) Uani 1 1 d . . H1 H 0.8332 0.6401 0.1474 0.079 Uiso 1 1 calc R U C12 C 0.7772(3) 0.6295(4) 0.6962(2) 0.0659(10) Uani 1 1 d . . C3 C 1.0303(3) 0.6650(4) 0.3080(3) 0.0716(10) Uani 1 1 d . . H3 H 1.0966 0.6730 0.3243 0.086 Uiso 1 1 calc R U C23 C 0.4456(3) 0.5055(5) 0.1206(3) 0.0971(15) Uani 1 1 d . . H23A H 0.4109 0.4991 0.1557 0.146 Uiso 1 1 calc R U H23B H 0.4264 0.4401 0.0799 0.146 Uiso 1 1 calc R U H23C H 0.4313 0.5828 0.0916 0.146 Uiso 1 1 calc R U C24 C 0.6082(3) 0.4954(4) 0.1228(3) 0.0899(13) Uani 1 1 d . . H24A H 0.5898 0.5641 0.0847 0.135 Uiso 1 1 calc R U H24B H 0.5955 0.4207 0.0908 0.135 Uiso 1 1 calc R U H24C H 0.6759 0.5005 0.1591 0.135 Uiso 1 1 calc R U C2 C 0.9704(3) 0.6595(4) 0.2263(3) 0.0767(11) Uani 1 1 d . . H2 H 0.9939 0.6652 0.1848 0.092 Uiso 1 1 calc R U C1S C 0.6542(4) 0.3215(5) 0.5015(4) 0.1059(16) Uani 1 1 d . . H1S1 H 0.6823 0.3852 0.5437 0.127 Uiso 1 1 calc R U H1S2 H 0.6636 0.3451 0.4516 0.127 Uiso 1 1 calc R U C14 C 0.7057(5) 0.5357(6) 0.6921(3) 0.130(2) Uani 1 1 d D . H14A H 0.7339 0.4558 0.6970 0.195 Uiso 1 1 calc R U H14B H 0.6502 0.5420 0.6389 0.195 Uiso 1 1 calc R U H14C H 0.6864 0.5482 0.7376 0.195 Uiso 1 1 calc R U C25 C 0.6561(4) 0.8707(4) 0.4328(3) 0.0941(15) Uani 1 1 d . . H25A H 0.7136 0.9125 0.4371 0.141 Uiso 1 1 calc R U H25B H 0.6682 0.8309 0.4855 0.141 Uiso 1 1 calc R U H25C H 0.6046 0.9288 0.4200 0.141 Uiso 1 1 calc R U C13 C 0.7304(6) 0.7483(6) 0.6936(4) 0.166(4) Uani 1 1 d . . H13A H 0.6948 0.7444 0.7282 0.249 Uiso 1 1 calc R U H13B H 0.6870 0.7668 0.6363 0.249 Uiso 1 1 calc R U H13C H 0.7788 0.8111 0.7147 0.249 Uiso 1 1 calc R U C15 C 0.8647(4) 0.6128(10) 0.7723(3) 0.204(5) Uani 1 1 d D . H15A H 0.8957 0.5379 0.7683 0.306 Uiso 1 1 calc R U H15B H 0.8489 0.6089 0.8204 0.306 Uiso 1 1 calc R U H15C H 0.9076 0.6804 0.7789 0.306 Uiso 1 1 calc R U loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.03884(15) 0.04500(16) 0.04016(15) -0.00057(9) 0.01485(11) -0.00143(9) Cl1 0.0594(5) 0.0469(4) 0.0558(4) -0.0007(3) 0.0182(4) 0.0019(3) Cl1S 0.1506(14) 0.1274(12) 0.1078(10) 0.0176(9) 0.0639(10) 0.0045(10) Cl2S 0.0961(11) 0.364(4) 0.1418(15) -0.026(2) 0.0632(11) 0.0079(17) N3 0.0453(14) 0.0530(15) 0.0433(13) -0.0037(11) 0.0193(11) -0.0044(11) N2 0.0400(12) 0.0434(13) 0.0458(13) 0.0031(10) 0.0178(11) -0.0005(10) N4 0.0531(15) 0.0601(16) 0.0479(15) -0.0052(12) 0.0255(13) -0.0075(12) N1 0.0581(16) 0.0636(17) 0.0486(15) 0.0076(12) 0.0244(13) 0.0048(13) C8 0.0436(15) 0.0443(15) 0.0451(16) -0.0010(12) 0.0160(13) -0.0027(13) C9 0.0424(16) 0.0485(17) 0.0433(16) -0.0028(12) 0.0144(13) -0.0022(12) C16 0.0455(17) 0.084(3) 0.0577(19) 0.0003(18) 0.0230(15) 0.0122(17) C11 0.063(2) 0.057(2) 0.0453(17) -0.0051(13) 0.0249(16) -0.0023(15) C7 0.0448(16) 0.063(2) 0.0530(18) -0.0026(15) 0.0165(14) -0.0063(15) C5 0.0495(16) 0.0444(15) 0.0494(17) 0.0042(13) 0.0237(14) 0.0022(13) C21 0.0392(16) 0.073(2) 0.0537(19) 0.0028(16) 0.0128(14) -0.0062(15) C19 0.0472(17) 0.0553(18) 0.0461(16) 0.0097(14) 0.0127(14) 0.0085(14) C18 0.0513(18) 0.0471(18) 0.066(2) 0.0072(15) 0.0138(16) 0.0043(14) C4 0.0532(18) 0.0540(18) 0.065(2) 0.0042(15) 0.0324(16) 0.0029(15) C17 0.057(2) 0.059(2) 0.062(2) -0.0068(16) 0.0151(17) 0.0140(16) C10 0.0517(18) 0.064(2) 0.0449(17) -0.0069(14) 0.0155(14) -0.0059(15) C20 0.0444(16) 0.0576(19) 0.0468(17) 0.0023(14) 0.0080(14) 0.0059(14) C6 0.0414(16) 0.069(2) 0.069(2) 0.0014(18) 0.0219(16) -0.0050(15) C22 0.070(2) 0.060(2) 0.0487(19) -0.0029(15) 0.0068(17) 0.0029(17) C1 0.079(2) 0.074(2) 0.0527(19) 0.0093(17) 0.0349(19) 0.0116(19) C12 0.076(2) 0.079(2) 0.054(2) -0.0105(17) 0.0380(19) -0.0025(19) C3 0.060(2) 0.090(3) 0.078(3) 0.008(2) 0.042(2) 0.003(2) C23 0.073(3) 0.111(4) 0.075(3) -0.025(3) -0.002(2) -0.016(3) C24 0.098(3) 0.095(3) 0.069(3) -0.020(2) 0.027(2) 0.010(3) C2 0.083(3) 0.095(3) 0.075(3) 0.012(2) 0.055(2) 0.011(2) C1S 0.113(4) 0.104(4) 0.130(4) -0.022(3) 0.079(4) -0.020(3) C14 0.190(6) 0.143(5) 0.097(4) -0.005(4) 0.099(4) -0.041(5) C25 0.110(4) 0.072(3) 0.085(3) -0.023(2) 0.026(3) 0.019(2) C13 0.313(11) 0.104(4) 0.165(6) 0.002(4) 0.185(7) 0.044(5) C15 0.100(4) 0.471(17) 0.042(3) -0.028(5) 0.030(3) 0.029(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N3 Ru1 N2 75.71(10) N3 Ru1 C16 90.00(12) N2 Ru1 C16 149.58(13) N3 Ru1 C18 120.27(12) N2 Ru1 C18 95.96(11) C16 Ru1 C18 67.98(14) N3 Ru1 C21 115.34(12) N2 Ru1 C21 168.79(11) C16 Ru1 C21 37.85(14) C18 Ru1 C21 80.22(13) N3 Ru1 C17 91.48(12) N2 Ru1 C17 114.08(12) C16 Ru1 C17 38.38(14) C18 Ru1 C17 37.85(13) C21 Ru1 C17 69.07(14) N3 Ru1 C19 157.52(11) N2 Ru1 C19 104.03(10) C16 Ru1 C19 79.18(13) C18 Ru1 C19 37.31(12) C21 Ru1 C19 66.60(12) C17 Ru1 C19 67.82(13) N3 Ru1 C20 152.81(12) N2 Ru1 C20 131.24(11) C16 Ru1 C20 67.72(13) C18 Ru1 C20 66.92(12) C21 Ru1 C20 37.60(12) C17 Ru1 C20 80.69(12) C19 Ru1 C20 36.10(12) N3 Ru1 Cl1 89.53(7) N2 Ru1 Cl1 83.02(7) C16 Ru1 Cl1 124.23(11) C18 Ru1 Cl1 149.12(10) C21 Ru1 Cl1 94.83(10) C17 Ru1 Cl1 162.57(11) C19 Ru1 Cl1 112.86(9) C20 Ru1 Cl1 90.55(9) N4 N3 C9 110.3(2) N4 N3 Ru1 130.4(2) C9 N3 Ru1 118.5(2) C8 N2 C5 118.2(2) C8 N2 Ru1 115.65(19) C5 N2 Ru1 125.9(2) N3 N4 C11 106.2(3) C1 N1 C5 116.9(3) N2 C8 C7 122.8(3) N2 C8 C9 114.4(3) C7 C8 C9 122.8(3) N3 C9 C10 108.3(3) N3 C9 C8 115.4(3) C10 C9 C8 136.2(3) C21 C16 C17 121.5(3) C21 C16 Ru1 71.91(19) C17 C16 Ru1 71.71(19) C21 C16 H16 119.2 C17 C16 H16 119.2 Ru1 C16 H16 129.7 N4 C11 C10 111.1(3) N4 C11 C12 120.2(3) C10 C11 C12 128.6(3) C6 C7 C8 119.8(3) C6 C7 H7 120.1 C8 C7 H7 120.1 N1 C5 N2 116.2(3) N1 C5 C4 123.2(3) N2 C5 C4 120.6(3) C16 C21 C20 120.5(3) C16 C21 Ru1 70.24(18) C20 C21 Ru1 74.61(18) C16 C21 H21 119.7 C20 C21 H21 119.7 Ru1 C21 H21 127.4 C20 C19 C18 120.6(3) C20 C19 Ru1 72.49(18) C18 C19 Ru1 68.21(18) C20 C19 H19 119.7 C18 C19 H19 119.7 Ru1 C19 H19 132.7 C17 C18 C19 121.9(3) C17 C18 Ru1 71.36(19) C19 C18 Ru1 74.48(18) C17 C18 H18 119.0 C19 C18 H18 119.0 Ru1 C18 H18 127.2 C6 C4 C3 123.7(3) C6 C4 C5 119.3(3) C3 C4 C5 117.0(3) C18 C17 C16 117.0(3) C18 C17 C25 122.6(4) C16 C17 C25 120.3(4) C18 C17 Ru1 70.78(19) C16 C17 Ru1 69.91(19) C25 C17 Ru1 127.3(3) C11 C10 C9 104.1(3) C11 C10 H10 127.9 C9 C10 H10 127.9 C19 C20 C21 118.2(3) C19 C20 C22 123.7(3) C21 C20 C22 118.1(3) C19 C20 Ru1 71.41(17) C21 C20 Ru1 67.79(17) C22 C20 Ru1 131.2(2) C7 C6 C4 119.3(3) C7 C6 H6 120.4 C4 C6 H6 120.4 C20 C22 C24 114.0(3) C20 C22 C23 108.7(3) C24 C22 C23 111.5(4) C20 C22 H22 107.4 C24 C22 H22 107.4 C23 C22 H22 107.4 N1 C1 C2 124.6(4) N1 C1 H1 117.7 C2 C1 H1 117.7 C15 C12 C13 112.9(6) C15 C12 C11 110.7(4) C13 C12 C11 107.6(3) C15 C12 C14 109.7(5) C13 C12 C14 105.8(5) C11 C12 C14 110.0(3) C2 C3 C4 119.6(3) C2 C3 H3 120.2 C4 C3 H3 120.2 C22 C23 H23A 109.5 C22 C23 H23B 109.5 H23A C23 H23B 109.5 C22 C23 H23C 109.5 H23A C23 H23C 109.5 H23B C23 H23C 109.5 C22 C24 H24A 109.5 C22 C24 H24B 109.5 H24A C24 H24B 109.5 C22 C24 H24C 109.5 H24A C24 H24C 109.5 H24B C24 H24C 109.5 C3 C2 C1 118.7(3) C3 C2 H2 120.7 C1 C2 H2 120.7 Cl2S C1S Cl1S 115.0(3) Cl2S C1S H1S1 108.5 Cl1S C1S H1S1 108.5 Cl2S C1S H1S2 108.5 Cl1S C1S H1S2 108.5 H1S1 C1S H1S2 107.5 C12 C14 H14A 109.5 C12 C14 H14B 109.5 H14A C14 H14B 109.5 C12 C14 H14C 109.5 H14A C14 H14C 109.5 H14B C14 H14C 109.5 C17 C25 H25A 109.5 C17 C25 H25B 109.5 H25A C25 H25B 109.5 C17 C25 H25C 109.5 H25A C25 H25C 109.5 H25B C25 H25C 109.5 C12 C13 H13A 109.5 C12 C13 H13B 109.5 H13A C13 H13B 109.5 C12 C13 H13C 109.5 H13A C13 H13C 109.5 H13B C13 H13C 109.5 C12 C15 H15A 109.5 C12 C15 H15B 109.5 H15A C15 H15B 109.5 C12 C15 H15C 109.5 H15A C15 H15C 109.5 H15B C15 H15C 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Ru1 N3 2.041(3) Ru1 N2 2.145(2) Ru1 C16 2.146(3) Ru1 C18 2.162(3) Ru1 C21 2.168(3) Ru1 C17 2.170(3) Ru1 C19 2.244(3) Ru1 C20 2.258(3) Ru1 Cl1 2.4094(8) Cl1S C1S 1.732(6) Cl2S C1S 1.690(5) N3 N4 1.348(4) N3 C9 1.344(4) N2 C8 1.342(4) N2 C5 1.379(4) N4 C11 1.348(4) N1 C1 1.318(4) N1 C5 1.348(4) C8 C7 1.409(4) C8 C9 1.437(4) C9 C10 1.394(4) C16 C21 1.399(5) C16 C17 1.419(5) C16 H16 0.9500 C11 C10 1.382(5) C11 C12 1.522(4) C7 C6 1.347(5) C7 H7 0.9500 C5 C4 1.414(4) C21 C20 1.429(5) C21 H21 0.9500 C19 C20 1.395(5) C19 C18 1.412(5) C19 H19 0.9500 C18 C17 1.405(5) C18 H18 0.9500 C4 C6 1.404(5) C4 C3 1.406(5) C17 C25 1.516(5) C10 H10 0.9500 C20 C22 1.512(5) C6 H6 0.9500 C22 C24 1.506(6) C22 C23 1.530(5) C22 H22 1.0000 C1 C2 1.391(6) C1 H1 0.9500 C12 C15 1.476(7) C12 C13 1.501(7) C12 C14 1.504(7) C3 C2 1.358(6) C3 H3 0.9500 C23 H23A 0.9800 C23 H23B 0.9800 C23 H23C 0.9800 C24 H24A 0.9800 C24 H24B 0.9800 C24 H24C 0.9800 C2 H2 0.9500 C1S H1S1 0.9900 C1S H1S2 0.9900 C14 H14A 0.9800 C14 H14B 0.9800 C14 H14C 0.9800 C25 H25A 0.9800 C25 H25B 0.9800 C25 H25C 0.9800 C13 H13A 0.9800 C13 H13B 0.9800 C13 H13C 0.9800 C15 H15A 0.9800 C15 H15B 0.9800 C15 H15C 0.9800