#------------------------------------------------------------------------------ #$Date: 2019-11-26 03:44:49 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242530 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/25/4132584.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132584 loop_ _publ_author_name 'Mokhtarzadeh, Charles C.' 'Moore, Curtis E.' 'Rheingold, Arnold L.' 'Figueroa, Joshua S.' _publ_section_title ; A Highly-Reduced Cobalt Terminal Carbyne: Divergent Metal- and \a-Carbon-Centered Reactivity. ; _journal_issue 26 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 8100 _journal_page_last 8104 _journal_paper_doi 10.1021/jacs.8b05019 _journal_volume 140 _journal_year 2018 _chemical_formula_moiety 'C47 H64 Co I2 N' _chemical_formula_sum 'C47 H64 Co I2 N' _chemical_formula_weight 955.72 _space_group_crystal_system orthorhombic _space_group_IT_number 29 _space_group_name_Hall 'P 2c -2ac' _space_group_name_H-M_alt 'P c a 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2016-07-25 _audit_creation_method ; Olex2 1.2-beta (compiled 2016.07.25 svn.r3318 for OlexSys, GUI svn.r5204) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 23.0483(13) _cell_length_b 14.0290(9) _cell_length_c 27.3737(18) _cell_measurement_reflns_used 7529 _cell_measurement_temperature 100 _cell_measurement_theta_max 25.31 _cell_measurement_theta_min 2.26 _cell_volume 8851.1(10) _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_collection 'APEX2 v2013.6-2 (Bruker, 2013)' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'XT (Sheldrick, 2008)' _diffrn_ambient_temperature 100 _diffrn_detector 'Bruker APEX CCD' _diffrn_detector_area_resol_mean 8.0 _diffrn_detector_type 'CCD Area Detector' _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device 'Kappa Four-Circle Diffractometer' _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0693 _diffrn_reflns_av_unetI/netI 0.0677 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 27 _diffrn_reflns_limit_h_min -27 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 32 _diffrn_reflns_limit_l_min -32 _diffrn_reflns_number 56422 _diffrn_reflns_point_group_measured_fraction_full 0.939 _diffrn_reflns_point_group_measured_fraction_max 0.933 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.381 _diffrn_reflns_theta_min 1.451 _diffrn_source 'sealed tube' _diffrn_source_type fine-focus _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 1.814 _exptl_absorpt_correction_T_max 0.0916 _exptl_absorpt_correction_T_min 0.0650 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/5 (Bruker,2014/5) was used for absorption correction. wR2(int) was 0.1080 before and 0.0665 after correction. The Ratio of minimum to maximum transmission is 0.7096. The \l/2 correction factor is 0.00150. ; _exptl_crystal_colour 'dull dark brown' _exptl_crystal_colour_lustre dull _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary brown _exptl_crystal_density_diffrn 1.434 _exptl_crystal_description needle _exptl_crystal_F_000 3888 _exptl_crystal_size_max 0.4 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.980 _refine_diff_density_min -0.475 _refine_diff_density_rms 0.094 _refine_ls_abs_structure_details ; Flack x determined using 4538 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.348(18) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.034 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 929 _refine_ls_number_reflns 15163 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.034 _refine_ls_R_factor_all 0.0567 _refine_ls_R_factor_gt 0.0405 _refine_ls_shift/su_max 0.008 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0296P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0818 _refine_ls_wR_factor_ref 0.0897 _reflns_Friedel_coverage 0.834 _reflns_Friedel_fraction_full 0.875 _reflns_Friedel_fraction_max 0.868 _reflns_number_gt 12276 _reflns_number_total 15163 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b05019_si_002.cif _cod_data_source_block jfig1371_b _cod_database_code 4132584 _publcif_datablock.id {1065b071-05f6-4bef-907f-e95c921a87e7} _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2. Uiso/Uaniso restraints and constraints Uanis(C80) = Uanis(C78) = Uanis(C82) Uanis(C88) = Uanis(C86) = Uanis(C90) 3.a Ternary CH refined with riding coordinates: C47(H47), C35(H35), C30(H30), C57(H57), C72(H72), C62(H62), C25(H25), C67(H67), C52(H52), C15(H15), C10(H10), C20(H20) 3.b Aromatic/amide H refined with riding coordinates: C43(H43), C6(H6), C33(H33), C50(H50), C70(H70), C55(H55), C42(H42), C28(H28), C65(H65), C5(H5), C13(H13), C41(H41), C4(H4), C18(H18) 3.c Idealised Me refined as rotating group: C16(H16A,H16B,H16C), C88(H88A,H88B,H88C), C94(H94A,H94B,H94C), C48(H48A,H48B, H48C), C27(H27A,H27B,H27C), C74(H74A,H74B,H74C), C86(H86A,H86B,H86C), C26(H26A, H26B,H26C), C78(H78A,H78B,H78C), C84(H84A,H84B,H84C), C63(H63A,H63B,H63C), C32(H32A,H32B,H32C), C37(H37A,H37B,H37C), C82(H82A,H82B,H82C), C49(H49A,H49B, H49C), C21(H21A,H21B,H21C), C36(H36A,H36B,H36C), C92(H92A,H92B,H92C), C64(H64A, H64B,H64C), C31(H31A,H31B,H31C), C80(H80A,H80B,H80C), C69(H69A,H69B,H69C), C12(H12A,H12B,H12C), C17(H17A,H17B,H17C), C68(H68A,H68B,H68C), C59(H59A,H59B, H59C), C73(H73A,H73B,H73C), C76(H76A,H76B,H76C), C53(H53A,H53B,H53C), C58(H58A, H58B,H58C), C22(H22A,H22B,H22C), C90(H90A,H90B,H90C), C54(H54A,H54B,H54C), C11(H11A,H11B,H11C) ; _shelx_res_file ; jfig1371_b.res created by SHELXL-2014/7 TITL jfig1371_b_a.res in Pca2(1) REM Old TITL JFig1371_b in Pca2(1) REM SHELXT solution in Pca2(1) REM R1 0.087, Rweak 0.007, Alpha 0.014, Orientation a'=b, b'=a, c'=-c REM Flack x = 0.377 ( 0.016 ) from Parsons' quotients REM Formula found by SHELXT: C81 N15 Co2 I4 CELL 0.71073 23.0483 14.029 27.3737 90 90 90 ZERR 8 0.0013 0.0009 0.0018 0 0 0 LATT -1 SYMM -X,-Y,0.5+Z SYMM 0.5+X,-Y,+Z SYMM 0.5-X,+Y,0.5+Z SFAC C H N Co I UNIT 376 512 8 8 16 EADP C80 C78 C82 EADP C88 C86 C90 L.S. 4 PLAN 20 TEMP -173.15 BOND $H list 4 ACTA fmap 2 OMIT 0 0 -2 OMIT 0 0 2 OMIT 1 1 0 REM REM REM WGHT 0.029600 FVAR 0.08002 I3 5 0.750888 0.506843 0.663531 11.00000 0.01841 0.03050 = 0.01719 -0.00029 -0.00333 -0.00151 I4 5 0.692814 0.299855 0.592680 11.00000 0.03250 0.02030 = 0.02500 0.00044 -0.00095 0.00132 I1 5 0.504189 1.004502 0.333268 11.00000 0.01866 0.03476 = 0.01631 -0.00033 -0.00301 0.00416 I2 5 0.560763 0.801110 0.407104 11.00000 0.03402 0.02019 = 0.03181 0.00157 -0.00036 -0.00177 CO2 4 0.694688 0.483732 0.583390 11.00000 0.01265 0.02026 = 0.01354 0.00105 0.00089 -0.00116 CO1 4 0.562451 0.985698 0.412660 11.00000 0.01229 0.02079 = 0.01507 0.00028 0.00067 -0.00086 N1 3 0.672115 0.992713 0.355663 11.00000 0.01353 0.01733 = 0.01426 0.00110 0.00252 0.00153 C44 1 0.479680 0.496000 0.645145 11.00000 0.01573 0.01188 = 0.02041 0.00021 0.00565 -0.00124 C45 1 0.595460 0.514994 0.744849 11.00000 0.01863 0.02334 = 0.00889 -0.00213 0.00025 -0.00288 C43 1 0.430374 0.496217 0.674797 11.00000 0.01343 0.02948 = 0.02845 0.00492 -0.00221 -0.00482 AFIX 43 H43 2 0.393097 0.493485 0.660055 11.00000 -1.20000 AFIX 0 C6 1 0.767964 0.989749 0.247955 11.00000 0.02382 0.01987 = 0.01387 -0.00337 0.00724 0.00406 AFIX 43 H6 2 0.765394 0.990695 0.213321 11.00000 -1.20000 AFIX 0 C38 1 0.626617 0.493041 0.618488 11.00000 0.02097 0.01135 = 0.00676 0.00340 -0.00595 0.00260 C60 1 0.473283 0.500063 0.590368 11.00000 0.00544 0.02164 = 0.01184 -0.00001 0.00259 0.00256 C16 1 0.503806 1.003032 0.120286 11.00000 0.03033 0.02413 = 0.01629 0.00275 -0.00865 -0.00121 AFIX 137 H16A 2 0.520018 0.941460 0.110305 11.00000 -1.50000 H16B 2 0.530729 1.054152 0.111260 11.00000 -1.50000 H16C 2 0.466545 1.013123 0.103834 11.00000 -1.50000 AFIX 0 C29 1 0.799537 1.008571 0.506233 11.00000 0.02097 0.01860 = 0.01663 -0.00241 -0.00354 -0.00471 C47 1 0.603281 0.333452 0.750052 11.00000 0.02635 0.02481 = 0.01895 0.00583 -0.00234 0.00212 AFIX 13 H47 2 0.581003 0.337981 0.718790 11.00000 -1.20000 AFIX 0 C2 1 0.723267 0.991565 0.326142 11.00000 0.00925 0.01885 = 0.02527 -0.00109 0.00560 0.00033 C7 1 0.717254 0.991816 0.275698 11.00000 0.01948 0.01768 = 0.01204 -0.00176 -0.00194 -0.00107 C34 1 0.774284 0.916812 0.433326 11.00000 0.01362 0.01586 = 0.01593 0.00157 -0.00404 0.00032 C88 1 0.704637 0.709720 0.579423 11.00000 0.02652 0.02827 = 0.02973 0.00051 -0.00251 -0.00172 AFIX 137 H88A 2 0.666350 0.715490 0.594711 11.00000 -1.50000 H88B 2 0.710234 0.762117 0.556220 11.00000 -1.50000 H88C 2 0.734748 0.712541 0.604658 11.00000 -1.50000 AFIX 0 C40 1 0.538166 0.504385 0.719282 11.00000 0.01827 0.01660 = 0.01686 -0.00115 0.00372 -0.00049 C75 1 0.574349 0.987321 0.487940 11.00000 0.01680 0.02595 = 0.01615 -0.00038 -0.00175 -0.00462 C46 1 0.625735 0.431738 0.762023 11.00000 0.02299 0.01613 = 0.01316 0.00210 -0.00179 -0.00541 C94 1 0.647076 0.413977 0.478691 11.00000 0.02336 0.03254 = 0.01873 0.00054 -0.00455 -0.01064 AFIX 137 H94A 2 0.662830 0.349712 0.483273 11.00000 -1.50000 H94B 2 0.649502 0.431502 0.444096 11.00000 -1.50000 H94C 2 0.606433 0.415244 0.489188 11.00000 -1.50000 AFIX 0 C77 1 0.596996 1.073498 0.466755 11.00000 0.01564 0.02788 = 0.01815 -0.00797 0.00037 0.00883 C48 1 0.561055 0.296367 0.790172 11.00000 0.03330 0.03552 = 0.02813 0.00844 0.00217 -0.00140 AFIX 137 H48A 2 0.582341 0.287556 0.820833 11.00000 -1.50000 H48B 2 0.544384 0.235351 0.779837 11.00000 -1.50000 H48C 2 0.529861 0.342852 0.795099 11.00000 -1.50000 AFIX 0 C33 1 0.782156 0.924005 0.483836 11.00000 0.01390 0.02021 = 0.02328 0.00074 -0.00133 -0.00117 AFIX 43 H33 2 0.775433 0.869406 0.503569 11.00000 -1.20000 AFIX 0 C27 1 0.756925 1.224891 0.383702 11.00000 0.03057 0.01665 = 0.02510 0.01177 -0.00562 -0.00163 AFIX 137 H27A 2 0.727044 1.179282 0.373586 11.00000 -1.50000 H27B 2 0.763262 1.271438 0.357546 11.00000 -1.50000 H27C 2 0.744199 1.258031 0.413340 11.00000 -1.50000 AFIX 0 C50 1 0.675364 0.446648 0.789561 11.00000 0.02028 0.03204 = 0.01695 0.00368 -0.00648 0.00151 AFIX 43 H50 2 0.694994 0.392672 0.802445 11.00000 -1.20000 AFIX 0 C56 1 0.617251 0.605957 0.753954 11.00000 0.01543 0.01849 = 0.01592 -0.00081 0.00145 -0.00245 C35 1 0.760207 0.820223 0.410470 11.00000 0.02007 0.01832 = 0.02288 0.00397 -0.00453 -0.00111 AFIX 13 H35 2 0.736272 0.832093 0.380613 11.00000 -1.20000 AFIX 0 C70 1 0.449881 0.590015 0.518429 11.00000 0.01484 0.01914 = 0.01922 0.00739 0.00139 0.00654 AFIX 43 H70 2 0.438575 0.648424 0.503674 11.00000 -1.20000 AFIX 0 C83 1 0.513627 0.986760 0.478361 11.00000 0.02213 0.03003 = 0.01717 0.00673 0.00523 -0.00360 C55 1 0.668761 0.615594 0.781020 11.00000 0.01642 0.02782 = 0.02111 -0.00638 -0.00344 0.00146 AFIX 43 H55 2 0.684065 0.677379 0.786995 11.00000 -1.20000 AFIX 0 C30 1 0.807725 1.015523 0.560488 11.00000 0.03301 0.02787 = 0.02092 0.00269 -0.00279 -0.01510 AFIX 13 H30 2 0.828147 1.076992 0.567304 11.00000 -1.20000 AFIX 0 C87 1 0.708552 0.617122 0.553126 11.00000 0.01904 0.02595 = 0.01824 0.00377 -0.00156 -0.00761 C23 1 0.783985 0.997687 0.404028 11.00000 0.00713 0.01578 = 0.02341 0.00155 -0.00451 -0.00040 C42 1 0.434520 0.500228 0.724022 11.00000 0.01411 0.02497 = 0.03045 -0.00175 0.00927 0.00037 AFIX 43 H42 2 0.400267 0.499112 0.743317 11.00000 -1.20000 AFIX 0 C79 1 0.551071 1.120420 0.442378 11.00000 0.02333 0.02319 = 0.02425 -0.00824 0.00754 0.00188 C57 1 0.586786 0.694761 0.735099 11.00000 0.01735 0.01420 = 0.02706 -0.00567 -0.00574 0.00676 AFIX 13 H57 2 0.553698 0.673718 0.714073 11.00000 -1.20000 AFIX 0 C74 1 0.398102 0.741534 0.581597 11.00000 0.01957 0.02382 = 0.03619 -0.00391 -0.00099 0.00405 AFIX 137 H74A 2 0.407300 0.761815 0.548225 11.00000 -1.50000 H74B 2 0.395752 0.797566 0.602884 11.00000 -1.50000 H74C 2 0.360788 0.708042 0.581762 11.00000 -1.50000 AFIX 0 C24 1 0.802345 1.083842 0.425348 11.00000 0.00929 0.01760 = 0.02149 -0.00137 0.00254 -0.00015 C72 1 0.445776 0.674522 0.600250 11.00000 0.02144 0.01701 = 0.03001 0.00506 -0.00308 0.00155 AFIX 13 H72 2 0.433013 0.650879 0.632996 11.00000 -1.20000 AFIX 0 C62 1 0.497620 0.323002 0.585271 11.00000 0.01770 0.02089 = 0.01275 0.00051 -0.00424 0.00129 AFIX 13 H62 2 0.524088 0.336496 0.613379 11.00000 -1.20000 AFIX 0 C28 1 0.809560 1.087509 0.475955 11.00000 0.01706 0.01456 = 0.02098 -0.00745 -0.00258 -0.00060 AFIX 43 H28 2 0.821726 1.145714 0.490434 11.00000 -1.20000 AFIX 0 C39 1 0.533311 0.498921 0.668296 11.00000 0.00937 0.01047 = 0.01138 -0.00338 -0.00205 -0.00423 C51 1 0.697719 0.535980 0.799218 11.00000 0.01352 0.01880 = 0.01245 -0.00091 -0.00466 -0.00120 C86 1 0.601542 0.609546 0.523529 11.00000 0.02652 0.02827 = 0.02973 0.00051 -0.00251 -0.00172 AFIX 137 H86A 2 0.573419 0.557206 0.522325 11.00000 -1.50000 H86B 2 0.598981 0.646978 0.493379 11.00000 -1.50000 H86C 2 0.592984 0.650575 0.551594 11.00000 -1.50000 AFIX 0 C26 1 0.858863 1.239642 0.414197 11.00000 0.02554 0.02378 = 0.03274 0.00061 0.00613 -0.00791 AFIX 137 H26A 2 0.863565 1.293569 0.391787 11.00000 -1.50000 H26B 2 0.895944 1.206099 0.417576 11.00000 -1.50000 H26C 2 0.846357 1.263105 0.446232 11.00000 -1.50000 AFIX 0 C25 1 0.813515 1.171722 0.394053 11.00000 0.02636 0.02174 = 0.01863 -0.00179 0.00039 -0.00190 AFIX 13 H25 2 0.828397 1.148431 0.361881 11.00000 -1.20000 AFIX 0 C78 1 0.657847 1.108371 0.471911 11.00000 0.02281 0.02568 = 0.02492 -0.00260 0.00563 0.00296 AFIX 137 H78A 2 0.684426 1.053859 0.472521 11.00000 -1.50000 H78B 2 0.661617 1.144471 0.502396 11.00000 -1.50000 H78C 2 0.667465 1.149687 0.444202 11.00000 -1.50000 AFIX 0 C84 1 0.471930 0.913332 0.496493 11.00000 0.01619 0.04477 = 0.01881 0.00239 0.00614 -0.00536 AFIX 137 H84A 2 0.443398 0.899281 0.470944 11.00000 -1.50000 H84B 2 0.451934 0.937535 0.525551 11.00000 -1.50000 H84C 2 0.493101 0.855003 0.504879 11.00000 -1.50000 AFIX 0 C67 1 0.453424 0.519432 0.433118 11.00000 0.03458 0.04506 = 0.01051 0.00004 -0.00619 0.00721 AFIX 13 H67 2 0.433600 0.581091 0.425546 11.00000 -1.20000 AFIX 0 C65 1 0.476171 0.425344 0.510851 11.00000 0.01545 0.01905 = 0.01980 -0.00618 -0.00255 0.00500 AFIX 43 H65 2 0.482284 0.370698 0.491012 11.00000 -1.20000 AFIX 0 C93 1 0.681555 0.483775 0.508648 11.00000 0.01649 0.02057 = 0.00931 0.00297 0.00136 -0.00409 C71 1 0.455698 0.587090 0.568350 11.00000 0.01215 0.01528 = 0.02258 0.00324 -0.00240 -0.00176 C5 1 0.821942 0.986348 0.269951 11.00000 0.01772 0.03211 = 0.01305 -0.00877 0.00422 -0.00116 AFIX 43 H5 2 0.855949 0.983120 0.250412 11.00000 -1.20000 AFIX 0 C52 1 0.753645 0.548796 0.828271 11.00000 0.01586 0.02324 = 0.02178 -0.00059 -0.00055 0.00093 AFIX 13 H52 2 0.762521 0.618530 0.829478 11.00000 -1.20000 AFIX 0 C63 1 0.442396 0.277631 0.605873 11.00000 0.02395 0.02120 = 0.03117 0.00256 0.00988 0.00424 AFIX 137 H63A 2 0.424305 0.321443 0.629229 11.00000 -1.50000 H63B 2 0.452261 0.217868 0.622443 11.00000 -1.50000 H63C 2 0.415267 0.264536 0.579136 11.00000 -1.50000 AFIX 0 C89 1 0.759264 0.560743 0.544241 11.00000 0.01650 0.03176 = 0.01764 0.00589 0.00227 -0.00323 C81 1 0.498832 1.067074 0.450693 11.00000 0.01207 0.03555 = 0.01483 -0.00756 0.00503 -0.00213 C85 1 0.660883 0.570046 0.528504 11.00000 0.01535 0.03102 = 0.01932 0.00703 0.00419 -0.00182 C32 1 0.845355 0.934785 0.581468 11.00000 0.03362 0.07149 = 0.02521 0.00350 -0.00985 0.00972 AFIX 137 H32A 2 0.826338 0.873385 0.575544 11.00000 -1.50000 H32B 2 0.850278 0.944218 0.616698 11.00000 -1.50000 H32C 2 0.883429 0.935301 0.565533 11.00000 -1.50000 AFIX 0 C37 1 0.726262 0.752602 0.443445 11.00000 0.03661 0.01614 = 0.02753 -0.00042 0.00357 -0.01174 AFIX 137 H37A 2 0.751659 0.729172 0.469526 11.00000 -1.50000 H37B 2 0.712034 0.698609 0.424146 11.00000 -1.50000 H37C 2 0.693285 0.786583 0.457848 11.00000 -1.50000 AFIX 0 C82 1 0.439264 1.098175 0.437229 11.00000 0.02281 0.02568 = 0.02492 -0.00260 0.00563 0.00296 AFIX 137 H82A 2 0.441043 1.138762 0.408129 11.00000 -1.50000 H82B 2 0.422226 1.134159 0.464354 11.00000 -1.50000 H82C 2 0.415267 1.042103 0.430329 11.00000 -1.50000 AFIX 0 C91 1 0.743881 0.478143 0.518211 11.00000 0.01331 0.03333 = 0.02340 0.00719 0.00235 -0.00336 C1 1 0.629657 0.989621 0.376649 11.00000 0.02011 0.01793 = 0.01689 -0.00527 -0.00646 0.00241 C49 1 0.652299 0.261386 0.742401 11.00000 0.03976 0.02297 = 0.03080 -0.00337 -0.00521 -0.00005 AFIX 137 H49A 2 0.678904 0.285140 0.717267 11.00000 -1.50000 H49B 2 0.635900 0.200266 0.731920 11.00000 -1.50000 H49C 2 0.673480 0.252608 0.773115 11.00000 -1.50000 AFIX 0 C21 1 0.622218 1.232403 0.288577 11.00000 0.06180 0.04370 = 0.05845 -0.02508 0.02485 -0.02420 AFIX 137 H21A 2 0.586201 1.250486 0.271959 11.00000 -1.50000 H21B 2 0.642267 1.289896 0.299914 11.00000 -1.50000 H21C 2 0.613116 1.191628 0.316617 11.00000 -1.50000 AFIX 0 C61 1 0.483648 0.417868 0.560732 11.00000 0.00868 0.02146 = 0.01909 0.00028 0.00347 -0.00161 C13 1 0.578481 0.913043 0.214660 11.00000 0.02412 0.01957 = 0.01512 0.00109 0.00198 -0.00012 AFIX 43 H13 2 0.559319 0.855274 0.206441 11.00000 -1.20000 AFIX 0 C9 1 0.631486 0.908774 0.238639 11.00000 0.01994 0.02285 = 0.01089 0.00064 0.00372 0.00389 C36 1 0.816004 0.772601 0.394383 11.00000 0.02619 0.02751 = 0.03046 -0.00276 0.00171 0.00260 AFIX 137 H36A 2 0.836843 0.814705 0.371840 11.00000 -1.50000 H36B 2 0.806955 0.712418 0.377882 11.00000 -1.50000 H36C 2 0.840315 0.759867 0.423021 11.00000 -1.50000 AFIX 0 C15 1 0.494640 1.003598 0.175630 11.00000 0.02438 0.02838 = 0.02107 -0.00329 -0.00314 0.00184 AFIX 13 H15 2 0.476215 1.065895 0.184263 11.00000 -1.20000 AFIX 0 C92 1 0.784217 0.402143 0.499899 11.00000 0.02350 0.03529 = 0.01970 0.00085 0.00128 0.00695 AFIX 137 H92A 2 0.818057 0.398051 0.521474 11.00000 -1.50000 H92B 2 0.796953 0.418041 0.466727 11.00000 -1.50000 H92C 2 0.763981 0.340710 0.499537 11.00000 -1.50000 AFIX 0 C64 1 0.527956 0.250888 0.552175 11.00000 0.02751 0.01945 = 0.03005 0.00595 0.00384 -0.00008 AFIX 137 H64A 2 0.539948 0.195525 0.571532 11.00000 -1.50000 H64B 2 0.562187 0.280528 0.537335 11.00000 -1.50000 H64C 2 0.501195 0.230342 0.526424 11.00000 -1.50000 AFIX 0 C31 1 0.749633 1.018522 0.587164 11.00000 0.05683 0.06061 = 0.01233 -0.00432 -0.00651 0.02593 AFIX 137 H31A 2 0.727174 1.073535 0.575798 11.00000 -1.50000 H31B 2 0.756408 1.024128 0.622390 11.00000 -1.50000 H31C 2 0.728004 0.959830 0.580438 11.00000 -1.50000 AFIX 0 C80 1 0.554298 1.211323 0.413452 11.00000 0.02281 0.02568 = 0.02492 -0.00260 0.00563 0.00296 AFIX 137 H80A 2 0.594938 1.225866 0.406019 11.00000 -1.50000 H80B 2 0.537478 1.263530 0.432564 11.00000 -1.50000 H80C 2 0.532581 1.203848 0.382913 11.00000 -1.50000 AFIX 0 C69 1 0.512504 0.519296 0.407089 11.00000 0.05090 0.04784 = 0.02183 -0.00433 0.00654 -0.00463 AFIX 137 H69A 2 0.531712 0.457823 0.412341 11.00000 -1.50000 H69B 2 0.536767 0.570523 0.420320 11.00000 -1.50000 H69C 2 0.506707 0.529453 0.372006 11.00000 -1.50000 AFIX 0 C19 1 0.634406 1.082565 0.238949 11.00000 0.02325 0.02769 = 0.01126 -0.00407 0.00294 -0.00765 C41 1 0.488100 0.505940 0.746584 11.00000 0.01915 0.02984 = 0.01603 -0.00122 0.00090 0.00025 AFIX 43 H41 2 0.490324 0.510966 0.781142 11.00000 -1.20000 AFIX 0 N2 3 0.583723 0.498074 0.640169 11.00000 0.01620 0.01322 = 0.01192 -0.00122 -0.00736 -0.00176 C12 1 0.613095 0.738144 0.267657 11.00000 0.04283 0.02826 = 0.04990 0.00713 -0.01242 -0.00220 AFIX 137 H12A 2 0.589281 0.764936 0.293946 11.00000 -1.50000 H12B 2 0.633725 0.681794 0.279738 11.00000 -1.50000 H12C 2 0.588110 0.719936 0.240233 11.00000 -1.50000 AFIX 0 C17 1 0.452959 0.926143 0.190243 11.00000 0.01913 0.05264 = 0.02525 0.00082 -0.00016 -0.00611 AFIX 137 H17A 2 0.414819 0.938959 0.175846 11.00000 -1.50000 H17B 2 0.449555 0.924471 0.225919 11.00000 -1.50000 H17C 2 0.467353 0.864548 0.178483 11.00000 -1.50000 AFIX 0 C68 1 0.416305 0.438850 0.412820 11.00000 0.03704 0.08849 = 0.02486 -0.00676 -0.00884 -0.01822 AFIX 137 H68A 2 0.405476 0.453376 0.379010 11.00000 -1.50000 H68B 2 0.381163 0.432135 0.432678 11.00000 -1.50000 H68C 2 0.438387 0.379179 0.413709 11.00000 -1.50000 AFIX 0 C10 1 0.657154 0.812852 0.250536 11.00000 0.03205 0.01756 = 0.03102 -0.00593 -0.01304 0.00116 AFIX 13 H10 2 0.685005 0.822817 0.278078 11.00000 -1.20000 AFIX 0 C59 1 0.561600 0.753760 0.777589 11.00000 0.04921 0.03968 = 0.03108 -0.01153 -0.00697 0.01627 AFIX 137 H59A 2 0.537432 0.712722 0.798211 11.00000 -1.50000 H59B 2 0.537957 0.805864 0.764462 11.00000 -1.50000 H59C 2 0.593395 0.780212 0.797114 11.00000 -1.50000 AFIX 0 C73 1 0.501888 0.729444 0.608135 11.00000 0.02656 0.02132 = 0.03934 -0.00706 -0.01053 0.00409 AFIX 137 H73A 2 0.515686 0.754484 0.576798 11.00000 -1.50000 H73B 2 0.531272 0.686802 0.621991 11.00000 -1.50000 H73C 2 0.494864 0.782439 0.630698 11.00000 -1.50000 AFIX 0 C76 1 0.608299 0.918657 0.519082 11.00000 0.02706 0.03884 = 0.02084 0.00182 -0.00702 0.00070 AFIX 137 H76A 2 0.590002 0.855649 0.517810 11.00000 -1.50000 H76B 2 0.608854 0.941438 0.552922 11.00000 -1.50000 H76C 2 0.648138 0.914191 0.506783 11.00000 -1.50000 AFIX 0 C66 1 0.459712 0.511807 0.488488 11.00000 0.01396 0.03005 = 0.01996 0.00087 -0.00150 0.00260 C14 1 0.552668 0.998841 0.202348 11.00000 0.01542 0.03502 = 0.01257 0.00305 0.00290 0.00056 C4 1 0.826595 0.987650 0.320964 11.00000 0.01767 0.01677 = 0.02438 0.00587 -0.00134 -0.00237 AFIX 43 H4 2 0.863921 0.986171 0.335665 11.00000 -1.20000 AFIX 0 C20 1 0.661808 1.177443 0.252636 11.00000 0.02967 0.01489 = 0.02706 0.00647 -0.00759 -0.00101 AFIX 13 H20 2 0.698964 1.163349 0.270061 11.00000 -1.20000 AFIX 0 C53 1 0.746911 0.513549 0.880929 11.00000 0.02673 0.02456 = 0.02181 -0.00226 -0.00579 0.00250 AFIX 137 H53A 2 0.715380 0.548545 0.896904 11.00000 -1.50000 H53B 2 0.783185 0.524256 0.898781 11.00000 -1.50000 H53C 2 0.737858 0.445296 0.880790 11.00000 -1.50000 AFIX 0 C18 1 0.581230 1.082575 0.214224 11.00000 0.02426 0.02461 = 0.01230 0.00553 0.00036 -0.00028 AFIX 43 H18 2 0.564229 1.141769 0.205325 11.00000 -1.20000 AFIX 0 C58 1 0.627689 0.754384 0.703464 11.00000 0.03773 0.02980 = 0.04384 0.00268 -0.00681 0.00301 AFIX 137 H58A 2 0.659833 0.777981 0.723538 11.00000 -1.50000 H58B 2 0.606386 0.808503 0.689655 11.00000 -1.50000 H58C 2 0.643061 0.714880 0.676926 11.00000 -1.50000 AFIX 0 C22 1 0.676415 1.239102 0.208746 11.00000 0.05414 0.04531 = 0.05063 0.00620 -0.00349 -0.02509 AFIX 137 H22A 2 0.640508 1.258511 0.192355 11.00000 -1.50000 H22B 2 0.700592 1.202726 0.185948 11.00000 -1.50000 H22C 2 0.697575 1.295868 0.219604 11.00000 -1.50000 AFIX 0 C8 1 0.658968 0.994522 0.250741 11.00000 0.01953 0.01393 = 0.01670 0.00070 0.00505 0.00700 C90 1 0.820144 0.588645 0.557745 11.00000 0.02652 0.02827 = 0.02973 0.00051 -0.00251 -0.00172 AFIX 137 H90A 2 0.819449 0.627043 0.587646 11.00000 -1.50000 H90B 2 0.837308 0.625960 0.531154 11.00000 -1.50000 H90C 2 0.843372 0.531125 0.563240 11.00000 -1.50000 AFIX 0 C54 1 0.804257 0.499257 0.803476 11.00000 0.01566 0.04558 = 0.02277 -0.00547 -0.00507 0.00470 AFIX 137 H54A 2 0.796548 0.430654 0.801631 11.00000 -1.50000 H54B 2 0.839748 0.510267 0.822367 11.00000 -1.50000 H54C 2 0.809149 0.524869 0.770424 11.00000 -1.50000 AFIX 0 C11 1 0.692184 0.775008 0.207617 11.00000 0.03667 0.03170 = 0.06867 -0.00896 0.00586 0.00939 AFIX 137 H11A 2 0.666731 0.767359 0.179209 11.00000 -1.50000 H11B 2 0.709111 0.713194 0.216276 11.00000 -1.50000 H11C 2 0.723278 0.820091 0.199717 11.00000 -1.50000 AFIX 0 C3 1 0.777211 0.991091 0.350652 11.00000 0.01512 0.00846 = 0.01920 -0.00068 -0.00466 -0.00031 HKLF 4 REM jfig1371_b_a.res in Pca2(1) REM R1 = 0.0405 for 12276 Fo > 4sig(Fo) and 0.0567 for all 15163 data REM 929 parameters refined using 1 restraints END WGHT 0.0296 0.0000 REM Highest difference peak 0.980, deepest hole -0.475, 1-sigma level 0.094 Q1 1 0.6792 0.7025 0.5920 11.00000 0.05 0.98 Q2 1 0.5471 1.1998 0.4018 11.00000 0.05 0.77 Q3 1 0.5770 1.1993 0.4083 11.00000 0.05 0.65 Q4 1 0.6332 0.9432 0.5903 11.00000 0.05 0.63 Q5 1 0.7174 0.7236 0.5723 11.00000 0.05 0.55 Q6 1 0.6900 1.1215 0.5895 11.00000 0.05 0.45 Q7 1 0.4299 1.0570 0.4384 11.00000 0.05 0.42 Q8 1 0.8049 1.0258 0.3313 11.00000 0.05 0.41 Q9 1 0.6668 0.5201 0.5902 11.00000 0.05 0.40 Q10 1 0.4109 0.5001 0.4219 11.00000 0.05 0.40 Q11 1 0.7597 0.9631 0.4181 11.00000 0.05 0.39 Q12 1 0.5325 0.9772 0.3246 11.00000 0.05 0.38 Q13 1 0.7584 0.9903 0.4098 11.00000 0.05 0.38 Q14 1 0.8544 0.7390 0.4079 11.00000 0.05 0.38 Q15 1 0.5878 0.5799 0.5140 11.00000 0.05 0.38 Q16 1 0.4439 0.6199 0.4307 11.00000 0.05 0.37 Q17 1 0.6180 0.4568 0.4131 11.00000 0.05 0.37 Q18 1 0.4425 0.5590 0.5799 11.00000 0.05 0.37 Q19 1 0.6936 0.9883 0.2624 11.00000 0.05 0.36 Q20 1 0.6589 1.0833 0.4841 11.00000 0.05 0.36 ; _shelx_res_checksum 90956 _shelx_hkl_file ; 0 -1 0 -6.80 0.30 0 1 0 -7.00 0.20 0 -1 0 -7.00 0.20 0 -2 0 4624.74 256.57 0 2 0 4762.42 256.47 0 -3 0 -0.90 1.60 0 -3 0 -1.30 0.80 0 3 0 -0.60 1.30 0 4 0 8881.31 513.95 0 -4 0 9999.00 514.45 0 -5 0 -2.20 2.00 0 5 0 -0.10 1.90 0 -6 0 1859.41 107.09 0 6 0 1966.40 106.89 0 7 0 2.20 2.10 0 7 0 -0.10 1.70 0 -7 0 -0.40 2.30 0 8 0 599.84 36.20 0 -8 0 581.24 36.50 0 8 0 603.44 35.50 0 9 0 1.40 2.00 0 -9 0 2.80 3.20 0 9 0 0.50 2.30 0 10 0 2910.71 162.28 0 10 0 2900.61 161.08 0 -10 0 2873.91 162.68 0 -11 0 12.50 4.80 0 11 0 17.80 4.60 0 11 0 25.10 4.90 0 12 0 478.45 29.40 0 -12 0 437.96 30.90 0 12 0 446.86 30.50 0 -13 0 16.70 6.00 0 13 0 16.60 5.20 0 14 0 345.67 26.20 0 -14 0 371.86 26.70 0 -15 0 2.60 4.70 0 15 0 1.20 3.80 0 -16 0 214.08 21.80 1 0 0 0.00 0.10 -1 0 0 0.10 0.10 1 0 0 0.00 0.10 -1 0 0 0.00 0.10 -1 0 0 0.00 0.10 1 0 0 0.00 0.10 -1 1 0 0.00 0.20 1 -1 0 -0.20 0.20 1 1 0 0.80 0.30 1 1 0 -0.20 0.30 -1 -1 0 0.20 0.30 1 -1 0 0.60 0.30 -1 2 0 51.69 3.90 -1 2 0 54.79 3.60 1 2 0 50.59 3.80 1 -2 0 59.39 3.70 -1 -2 0 54.49 4.10 1 3 0 105.89 6.90 -1 3 0 95.59 7.00 -1 -3 0 103.39 7.20 1 -4 0 215.78 14.20 -1 -4 0 218.58 14.30 1 4 0 224.88 14.00 -1 4 0 235.48 14.20 1 5 0 18.70 3.40 1 -5 0 32.60 4.50 -1 5 0 35.40 4.30 -1 -5 0 30.50 4.30 1 6 0 368.56 22.60 1 -6 0 351.66 23.00 -1 -6 0 365.46 23.30 1 6 0 377.96 22.90 -1 6 0 383.46 23.10 -1 7 0 1.60 1.60 1 7 0 1.20 1.80 1 7 0 -1.60 1.40 -1 7 0 0.40 1.60 1 -7 0 -2.00 1.70 -1 -7 0 1.70 2.30 1 -8 0 13.00 3.70 1 8 0 8.40 3.00 -1 -8 0 7.40 3.20 1 8 0 6.10 2.70 -1 8 0 4.40 2.40 -1 8 0 6.00 2.40 -1 -9 0 55.49 7.90 1 9 0 50.99 6.70 1 9 0 58.59 7.40 1 -9 0 71.79 8.60 -1 9 0 61.19 6.60 -1 9 0 54.29 7.30 1 10 0 -1.80 2.40 1 -10 0 -0.40 3.00 1 10 0 2.10 2.80 -1 -10 0 1.80 3.10 -1 10 0 2.50 2.50 -1 10 0 -2.00 2.30 1 11 0 2.30 2.90 -1 11 0 0.60 2.40 -1 11 0 -2.00 2.20 -1 -11 0 0.20 3.70 1 11 0 -1.00 2.50 1 -11 0 1.20 3.40 -1 12 0 68.39 9.80 1 -12 0 67.39 9.90 -1 -12 0 72.79 10.40 1 12 0 64.29 9.30 1 12 0 75.59 9.10 -1 13 0 14.20 4.90 1 13 0 7.40 4.10 1 -13 0 15.10 5.90 -1 -13 0 12.80 5.50 -1 -14 0 16.60 5.90 1 -14 0 18.50 6.10 1 14 0 4.00 4.00 -1 14 0 22.90 6.40 1 -15 0 1.80 4.00 1 15 0 1.00 3.90 -1 -15 0 3.90 5.20 1 -16 0 84.79 12.90 1 16 0 71.79 11.50 -1 -16 0 95.69 13.50 -2 0 0 -3.10 0.30 2 0 0 -3.30 0.20 -2 0 0 -3.20 0.30 -2 0 0 -2.20 0.30 2 0 0 -3.40 0.10 2 0 0 -3.00 0.30 -2 0 0 -2.90 0.40 2 0 0 -3.40 0.20 2 1 0 798.82 42.90 -2 -1 0 755.22 42.70 -2 2 0 -2.20 0.70 -2 2 0 -1.60 0.30 -2 -2 0 -1.40 1.00 2 2 0 -1.40 0.90 -2 -3 0 239.58 15.70 -2 3 0 251.57 15.00 2 3 0 274.27 15.50 -2 3 0 259.27 15.70 2 4 0 1.80 1.40 -2 -4 0 3.30 2.10 -2 4 0 4.30 1.80 -2 4 0 2.70 1.20 2 5 0 939.11 56.89 2 -5 0 1042.30 57.39 -2 -5 0 1059.59 57.69 -2 5 0 1000.00 57.29 2 6 0 0.10 1.70 -2 6 0 0.50 1.70 -2 -6 0 0.90 2.00 2 6 0 0.50 1.60 2 -6 0 -1.10 1.70 2 -7 0 32.40 5.10 2 7 0 33.50 4.90 -2 -7 0 29.90 5.20 -2 7 0 31.90 4.10 -2 7 0 41.40 5.60 2 7 0 29.50 4.70 2 -8 0 0.40 2.20 2 8 0 2.60 2.00 -2 8 0 2.40 2.00 -2 -8 0 0.00 2.30 2 8 0 -0.80 1.90 -2 8 0 3.50 2.10 -2 9 0 360.96 21.90 -2 9 0 338.97 23.20 2 9 0 367.96 23.30 -2 -9 0 333.47 23.50 2 9 0 346.57 22.80 2 -9 0 333.17 23.30 2 10 0 2.90 2.90 -2 10 0 7.20 2.90 -2 -10 0 6.50 3.60 2 -10 0 5.80 3.50 2 10 0 6.10 3.20 -2 10 0 4.10 2.90 -2 11 0 120.79 10.20 2 11 0 140.09 11.60 -2 -11 0 139.49 14.30 2 -11 0 126.29 13.70 2 11 0 118.59 12.70 -2 11 0 120.49 12.90 -2 12 0 8.90 4.20 -2 -12 0 11.10 4.80 2 12 0 19.60 5.20 2 -12 0 18.60 5.40 2 12 0 10.60 3.90 -2 13 0 10.60 4.90 2 -13 0 29.40 7.20 2 13 0 12.20 4.40 -2 -13 0 18.30 5.50 2 13 0 21.90 5.60 2 14 0 12.90 4.50 2 -14 0 4.30 4.40 -2 -14 0 4.00 4.30 -2 -15 0 231.68 19.90 2 -15 0 233.08 19.80 2 15 0 221.98 19.20 2 -16 0 12.50 6.20 -2 -16 0 5.10 6.00 2 16 0 9.80 5.40 -3 0 0 -0.30 0.40 3 0 0 -0.20 0.50 3 0 0 0.40 0.30 -3 0 0 0.90 0.60 -3 0 0 -0.80 0.50 -3 0 0 0.60 0.70 3 0 0 0.30 0.50 3 0 0 -0.30 0.40 3 -1 0 151.98 8.90 3 1 0 141.29 8.30 3 1 0 116.29 8.60 -3 -1 0 146.89 8.40 -3 1 0 125.79 8.30 -3 1 0 143.89 8.10 -3 -1 0 141.19 8.20 3 1 0 143.89 8.10 3 -1 0 141.19 8.10 -3 2 0 31.10 2.00 -3 2 0 22.50 2.70 -3 -2 0 27.00 3.10 3 2 0 32.10 2.80 -3 -2 0 33.50 2.20 3 -2 0 31.50 1.90 -3 -3 0 107.39 7.30 -3 3 0 99.19 6.50 3 3 0 83.49 6.50 -3 3 0 97.29 5.50 3 4 0 6.30 1.80 -3 4 0 3.90 1.40 -3 -4 0 1.50 2.00 -3 5 0 -0.30 1.00 -3 -5 0 0.80 1.70 -3 5 0 2.60 1.80 3 5 0 1.50 1.70 3 5 0 1.10 1.50 3 -5 0 0.30 1.60 -3 6 0 87.69 7.80 3 -6 0 89.79 7.80 3 6 0 92.59 8.10 -3 -6 0 86.39 8.10 3 6 0 99.49 7.60 3 7 0 72.89 6.90 -3 7 0 72.79 8.00 3 -7 0 90.89 7.60 -3 7 0 71.29 5.80 -3 -7 0 66.09 8.00 3 7 0 76.79 8.10 -3 8 0 27.00 3.70 3 8 0 23.10 4.40 -3 8 0 19.20 4.20 3 -8 0 19.10 4.20 -3 -8 0 25.40 5.10 3 8 0 21.70 4.50 -3 -9 0 70.89 9.40 -3 9 0 90.89 7.40 3 9 0 72.39 8.60 3 -9 0 93.89 9.90 3 9 0 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13.90 -4 -14 0 101.89 13.30 4 -15 0 -2.00 4.00 -4 -15 0 -0.40 4.40 4 15 0 0.90 4.00 4 -16 0 43.60 9.60 4 16 0 57.69 9.60 -4 -16 0 43.10 9.90 -5 0 0 0.40 1.00 -5 0 0 1.00 0.80 5 0 0 0.00 0.70 5 0 0 0.10 0.80 5 0 0 0.70 1.00 5 1 0 362.16 20.20 -5 -1 0 357.56 20.20 -5 -1 0 336.17 20.10 -5 1 0 356.36 20.20 -5 1 0 343.07 20.40 5 -1 0 364.26 20.30 5 1 0 341.57 20.90 -5 -2 0 46.90 3.50 5 2 0 42.70 3.70 -5 -2 0 44.70 4.10 5 2 0 49.90 5.10 5 -2 0 45.20 3.30 -5 2 0 48.10 3.40 -5 2 0 51.59 4.10 -5 3 0 52.09 4.80 -5 3 0 61.19 3.80 -5 -3 0 64.99 4.30 -5 -3 0 63.09 5.40 5 -3 0 63.49 3.70 5 3 0 61.99 4.90 5 3 0 66.29 5.90 5 4 0 167.28 11.70 -5 4 0 189.88 10.30 -5 -4 0 172.08 12.30 -5 4 0 180.28 11.60 5 4 0 200.88 13.10 5 5 0 60.09 6.80 5 5 0 55.39 5.80 -5 5 0 56.19 3.50 -5 -5 0 60.89 6.50 -5 5 0 50.29 4.60 -5 6 0 1.40 1.40 5 -6 0 -0.60 1.80 -5 6 0 0.70 0.70 -5 -6 0 3.60 2.30 5 6 0 -1.40 1.90 5 6 0 3.00 1.80 -5 7 0 205.28 12.20 5 7 0 191.78 13.70 -5 7 0 205.28 12.90 5 -7 0 209.88 14.30 5 7 0 196.58 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6 -2 0 4.70 1.20 -6 3 0 1019.60 60.49 6 3 0 1171.48 60.49 6 -3 0 1027.20 59.19 6 3 0 1055.69 61.59 -6 -3 0 1115.19 60.89 -6 3 0 1095.79 59.29 -6 -3 0 1088.09 59.79 -6 -4 0 1.00 1.60 -6 -4 0 2.10 0.90 6 4 0 -1.70 1.70 -6 4 0 0.10 1.20 -6 4 0 -0.20 0.50 6 4 0 1.90 1.30 6 5 0 162.58 10.20 -6 5 0 127.89 9.50 -6 -5 0 139.39 10.50 6 5 0 137.49 11.00 6 6 0 0.70 2.20 -6 -6 0 -1.40 2.10 -6 6 0 0.50 0.70 -6 6 0 0.90 0.60 -6 6 0 -0.30 1.30 6 6 0 -2.40 1.10 -6 -7 0 885.41 49.90 6 7 0 844.12 48.80 -6 7 0 795.12 47.80 -6 7 0 831.02 46.10 6 7 0 817.42 49.80 -6 7 0 857.21 46.50 6 -7 0 848.82 49.00 -6 -8 0 7.10 3.40 -6 8 0 5.30 1.50 6 -8 0 3.40 2.70 6 8 0 2.60 3.00 6 8 0 -0.20 1.80 6 -9 0 94.39 10.10 -6 -9 0 108.19 11.40 6 9 0 90.89 10.50 6 9 0 106.79 9.20 6 -10 0 -1.60 2.90 -6 -10 0 0.20 2.50 6 10 0 -1.90 2.10 6 10 0 4.20 3.20 -6 -11 0 59.89 9.00 6 11 0 51.49 7.80 6 -11 0 52.89 8.10 6 11 0 78.49 9.80 6 -12 0 1.70 4.20 6 12 0 7.60 4.00 6 12 0 -2.10 2.90 -6 -12 0 6.00 4.60 6 -13 0 185.38 17.00 6 13 0 194.88 17.00 6 13 0 206.78 16.80 -6 -13 0 215.58 18.00 6 14 0 0.80 4.30 6 14 0 2.40 3.30 6 -14 0 4.80 4.90 -6 -14 0 -2.70 3.80 6 15 0 -0.60 4.90 6 15 0 -2.30 3.50 -6 -15 0 -8.50 4.40 6 -15 0 -1.30 4.50 6 16 0 1.60 3.70 6 -16 0 3.00 5.10 -6 -16 0 4.60 5.10 -7 0 0 0.70 0.90 7 0 0 -0.10 0.90 7 0 0 -1.00 1.10 -7 0 0 0.00 1.10 -7 -1 0 143.69 9.60 7 -1 0 150.18 9.80 7 1 0 150.68 10.60 7 1 0 151.78 9.50 -7 1 0 149.59 9.80 -7 -1 0 151.18 9.40 -7 2 0 47.00 4.70 -7 -2 0 41.00 3.60 7 2 0 42.30 3.70 -7 -2 0 46.10 4.50 7 -2 0 43.20 3.60 7 2 0 43.70 5.20 7 -3 0 72.69 4.70 7 3 0 70.79 5.50 -7 -3 0 67.39 5.90 -7 3 0 73.29 4.80 -7 -3 0 66.79 5.00 7 3 0 60.59 7.10 -7 3 0 68.39 5.70 7 4 0 106.59 8.80 -7 4 0 79.89 7.10 7 4 0 112.29 7.60 -7 4 0 101.19 5.90 -7 -4 0 76.69 7.60 7 -4 0 100.39 5.70 -7 -4 0 100.99 6.60 7 5 0 13.00 3.80 7 5 0 16.30 3.00 -7 5 0 18.60 3.10 -7 -5 0 23.00 4.00 -7 -5 0 18.00 2.20 -7 6 0 581.24 31.60 -7 -6 0 482.65 32.40 7 6 0 532.55 33.30 7 6 0 508.75 31.70 -7 -6 0 553.04 30.20 -7 -7 0 32.90 5.40 7 -7 0 33.10 5.00 7 7 0 33.60 4.90 -7 7 0 42.30 4.90 7 7 0 33.30 5.80 7 -8 0 1.20 2.30 7 8 0 -0.40 2.30 -7 -8 0 1.70 2.60 -7 8 0 0.50 1.00 -7 8 0 1.90 1.80 7 8 0 0.90 1.90 7 -9 0 3.40 3.00 -7 -9 0 4.30 3.10 7 9 0 4.00 3.30 7 9 0 3.50 2.40 -7 -10 0 103.29 11.90 7 10 0 104.69 11.70 7 10 0 109.79 10.00 7 -10 0 111.49 11.60 7 11 0 45.50 7.20 7 11 0 31.90 6.90 7 -11 0 46.60 7.20 -7 -11 0 63.49 9.20 7 12 0 124.49 12.70 7 -12 0 89.69 11.60 7 12 0 108.19 12.80 -7 -12 0 98.49 12.50 7 -13 0 43.20 7.70 7 13 0 27.50 6.40 7 13 0 28.40 6.80 -7 -13 0 21.70 6.70 7 -14 0 -1.70 3.50 7 14 0 5.80 4.40 -7 -14 0 3.40 4.30 7 14 0 3.10 3.60 -7 -15 0 5.50 5.80 7 15 0 8.30 4.50 7 15 0 12.70 6.10 7 -15 0 2.10 5.00 -7 -16 0 97.39 13.70 7 -16 0 99.09 13.60 7 16 0 74.09 11.80 -8 0 0 377.16 22.50 -8 0 0 382.46 21.50 8 0 0 364.46 22.80 8 0 0 377.86 22.10 8 1 0 5.70 2.30 8 1 0 5.30 1.50 8 -1 0 6.00 1.70 -8 -1 0 6.30 1.80 -8 1 0 3.00 1.80 8 -1 0 2.40 1.50 -8 -1 0 4.90 1.50 -8 -2 0 1083.79 58.79 8 2 0 1040.50 60.19 8 2 0 1023.40 58.79 -8 -2 0 1055.19 58.89 8 -2 0 1057.39 58.69 -8 2 0 1045.00 59.19 -8 -3 0 -1.10 1.00 -8 -3 0 -0.20 1.50 8 3 0 0.80 2.10 8 3 0 3.20 1.70 -8 3 0 0.30 1.60 8 -3 0 0.90 1.00 8 4 0 68.09 5.70 -8 -4 0 67.29 5.20 -8 4 0 81.49 6.40 -8 -4 0 70.59 6.40 8 -4 0 69.09 4.40 8 4 0 71.19 7.90 -8 5 0 -1.30 1.40 -8 -5 0 -0.50 2.10 8 5 0 0.40 2.30 -8 -5 0 -0.30 1.10 8 5 0 -3.40 1.10 -8 6 0 1.70 1.80 8 6 0 0.10 2.40 8 6 0 1.90 2.00 -8 -6 0 2.90 1.10 -8 -6 0 3.60 2.80 8 7 0 1.10 2.90 8 -7 0 1.20 2.30 -8 7 0 -1.50 1.50 8 7 0 1.20 1.80 -8 -7 0 1.30 1.00 -8 -7 0 1.30 2.40 -8 -8 0 571.04 31.70 8 8 0 584.04 34.20 -8 8 0 536.75 33.10 8 8 0 535.75 35.50 8 -8 0 565.34 34.20 -8 -8 0 553.14 35.10 8 9 0 -0.10 2.50 -8 9 0 -0.60 1.70 -8 -9 0 0.50 2.60 8 9 0 0.20 2.10 8 -9 0 -0.80 2.50 8 -10 0 120.39 11.90 8 10 0 109.99 10.10 8 10 0 110.69 12.50 -8 -10 0 114.19 12.70 -8 -11 0 4.30 3.90 8 11 0 -0.60 2.90 8 11 0 -2.90 3.10 8 -11 0 8.00 3.90 8 -12 0 350.96 24.90 8 12 0 322.87 24.20 8 12 0 395.96 26.40 -8 -12 0 356.36 26.20 8 13 0 0.50 3.10 8 13 0 -3.30 3.80 -8 -13 0 3.90 4.90 8 -13 0 3.70 4.00 8 -14 0 8.60 4.70 8 14 0 3.60 4.00 8 14 0 2.80 5.00 -8 -14 0 3.90 4.90 -8 -15 0 6.10 5.30 8 -15 0 -1.90 4.30 8 15 0 1.20 4.30 8 15 0 -3.10 4.30 8 16 0 13.20 5.60 8 -16 0 25.60 7.10 -8 -16 0 0.40 5.20 -9 0 0 0.20 0.90 9 0 0 -1.60 1.30 -9 0 0 0.20 1.40 9 0 0 1.30 1.20 9 -1 0 20.20 3.20 -9 -1 0 16.90 2.40 9 -1 0 12.30 2.40 -9 1 0 12.60 2.60 -9 -1 0 17.10 2.80 9 1 0 17.50 2.50 9 1 0 17.00 3.40 9 -2 0 67.49 5.60 9 2 0 67.59 7.50 -9 2 0 75.29 6.20 -9 -2 0 77.99 5.90 -9 -2 0 72.19 5.80 9 2 0 74.49 5.80 9 3 0 5.50 1.80 9 -3 0 6.60 1.60 -9 -3 0 9.20 2.40 -9 -3 0 6.40 1.70 -9 3 0 12.60 2.70 9 3 0 3.60 2.70 9 4 0 77.59 8.60 9 -4 0 78.09 5.10 9 4 0 78.89 6.40 -9 4 0 81.09 6.80 -9 -4 0 79.29 5.90 -9 -4 0 77.09 6.90 -9 -5 0 2.10 2.20 -9 5 0 1.00 1.60 9 5 0 2.20 2.60 -9 -5 0 2.90 1.20 9 5 0 2.80 1.80 9 -5 0 3.10 0.60 9 6 0 345.27 21.30 -9 6 0 333.17 21.10 -9 -6 0 348.97 22.30 -9 -6 0 326.07 19.80 9 6 0 348.67 23.20 -9 7 0 120.09 9.60 9 7 0 123.79 9.90 9 -7 0 128.79 10.00 9 7 0 128.69 13.10 -9 -7 0 133.29 8.40 -9 -7 0 124.19 11.10 9 -8 0 -0.50 2.20 -9 -8 0 -1.70 2.60 -9 -8 0 1.40 1.10 9 8 0 -1.70 1.60 -9 8 0 -2.00 1.60 9 8 0 1.10 2.50 9 -9 0 7.10 3.40 -9 -9 0 10.10 4.30 9 9 0 8.70 4.00 -9 9 0 6.90 2.80 9 9 0 6.80 3.10 9 -10 0 97.59 10.50 9 10 0 88.49 9.80 -9 -10 0 103.79 11.60 9 10 0 84.29 11.20 -9 -11 0 42.30 8.00 9 11 0 38.30 7.70 9 -11 0 54.39 8.10 9 11 0 48.10 7.40 9 -12 0 82.19 10.50 9 12 0 62.39 9.90 9 12 0 65.59 9.30 -9 -12 0 99.79 12.00 9 13 0 5.10 4.70 9 -13 0 -0.10 3.40 9 13 0 1.20 3.30 -9 -13 0 7.20 4.60 9 14 0 -0.70 4.00 9 14 0 -1.10 3.60 -9 -14 0 -0.10 4.40 9 -14 0 -3.20 3.20 9 15 0 18.20 5.80 -9 -15 0 2.40 5.60 9 15 0 1.10 5.50 9 -15 0 10.20 5.70 10 0 0 0.80 1.70 -10 0 0 1.20 1.10 10 0 0 -2.00 1.00 -10 0 0 -0.10 1.50 10 -1 0 84.59 6.30 -10 -1 0 80.89 6.40 -10 1 0 86.59 6.70 -10 -1 0 73.69 5.80 10 -1 0 74.99 6.60 10 1 0 84.49 6.30 10 1 0 78.89 7.20 -10 2 0 4.90 2.00 10 -2 0 4.40 1.80 -10 -2 0 4.50 1.90 -10 -2 0 2.60 1.70 10 2 0 1.80 2.30 10 2 0 6.00 1.90 -10 -3 0 1294.17 70.59 -10 3 0 1236.48 70.69 10 3 0 1247.48 72.09 -10 -3 0 1237.48 69.99 10 3 0 1256.17 70.29 10 -3 0 1252.57 69.69 10 4 0 6.60 2.10 -10 -4 0 7.50 1.90 10 -4 0 6.50 1.40 -10 -4 0 5.90 2.50 -10 4 0 4.20 2.20 10 4 0 8.60 3.30 -10 -5 0 27.80 3.50 10 -5 0 29.80 2.10 -10 5 0 34.30 4.80 10 5 0 27.20 4.00 10 5 0 24.40 5.20 -10 -5 0 24.90 4.30 -10 -6 0 2.90 1.40 10 6 0 0.30 2.20 -10 -6 0 3.60 2.50 10 6 0 5.10 2.30 -10 6 0 3.00 1.90 10 -7 0 476.15 27.20 -10 7 0 426.86 26.70 10 7 0 397.66 26.80 -10 -7 0 445.56 25.40 10 7 0 424.86 28.90 -10 -7 0 456.35 28.30 -10 -8 0 0.20 2.60 10 8 0 2.20 2.30 10 8 0 -4.10 2.30 10 -8 0 -0.20 2.20 -10 -8 0 0.10 1.20 -10 8 0 1.80 1.90 -10 -9 0 27.10 5.80 10 9 0 25.60 5.00 10 9 0 34.60 6.70 10 -9 0 26.10 5.20 -10 9 0 20.40 4.00 -10 -10 0 5.60 4.00 10 -10 0 4.90 3.30 10 10 0 0.00 3.40 10 10 0 0.50 2.60 10 -11 0 30.70 6.30 10 11 0 36.70 7.50 -10 -11 0 42.30 7.80 10 11 0 42.50 6.70 10 -12 0 -1.60 3.60 -10 -12 0 3.10 3.50 10 12 0 0.00 3.90 10 12 0 -3.20 2.70 -10 -13 0 368.96 28.10 10 13 0 377.76 28.40 10 13 0 391.76 26.90 10 -13 0 395.96 27.30 10 -14 0 -0.60 4.40 -10 -14 0 0.00 4.40 10 14 0 -3.30 3.00 10 14 0 0.90 5.10 10 15 0 -3.50 4.10 10 -15 0 0.90 4.90 10 15 0 2.70 4.20 -10 -15 0 3.00 5.30 -11 0 0 2.90 1.80 11 0 0 -0.80 1.50 11 0 0 -0.40 1.20 -11 0 0 -0.90 0.90 -11 -1 0 241.88 14.40 11 -1 0 245.38 15.60 -11 -1 0 233.48 15.10 11 1 0 229.68 14.80 11 1 0 227.28 16.10 11 -1 0 242.68 14.90 -11 1 0 224.18 15.20 -11 -2 0 17.60 3.00 -11 2 0 11.50 2.80 11 2 0 16.10 3.80 -11 -2 0 15.60 2.70 11 2 0 14.20 2.70 11 -2 0 14.90 2.80 11 -3 0 1.40 1.30 -11 -3 0 2.30 1.60 11 3 0 5.30 2.90 11 3 0 5.20 1.90 -11 -3 0 10.20 2.50 -11 3 0 9.60 2.60 -11 -4 0 14.70 2.60 -11 4 0 9.10 2.70 11 4 0 11.20 3.60 11 4 0 9.80 2.40 11 -4 0 10.80 1.90 -11 -4 0 8.80 2.70 -11 5 0 59.49 6.40 -11 -5 0 45.90 6.50 -11 -5 0 49.60 5.00 11 5 0 51.09 5.80 11 5 0 52.99 7.50 11 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309.47 19.50 12 1 0 17.40 3.80 -12 -1 0 16.30 3.10 12 1 0 13.30 2.70 -12 1 0 11.90 2.90 12 -1 0 20.10 3.20 -12 -1 0 18.40 2.80 12 -1 0 15.30 3.30 -12 -2 0 570.44 33.40 12 2 0 581.34 33.30 12 2 0 568.04 35.10 12 -2 0 581.34 33.50 -12 2 0 536.45 33.70 -12 -2 0 581.74 33.10 12 -2 0 566.74 33.60 -12 3 0 -1.30 1.50 12 -3 0 -0.90 1.30 -12 -3 0 1.90 1.70 12 3 0 0.10 2.20 12 3 0 0.50 1.60 -12 -3 0 -0.10 1.30 -12 -4 0 332.87 21.70 -12 -4 0 348.37 20.90 -12 4 0 334.17 21.70 12 -4 0 349.47 20.30 12 4 0 356.36 23.60 12 4 0 336.37 21.20 -12 -5 0 32.20 5.10 -12 -5 0 29.00 3.80 -12 5 0 33.70 4.90 12 5 0 34.10 4.60 12 -5 0 31.00 2.70 12 5 0 26.60 5.60 12 6 0 323.37 22.50 -12 -6 0 309.27 19.00 -12 -6 0 308.27 21.00 -12 6 0 310.77 20.30 12 6 0 317.27 20.20 12 -7 0 3.00 2.50 -12 -7 0 4.10 1.80 -12 -7 0 4.50 2.90 -12 7 0 5.30 2.70 12 7 0 4.90 3.30 12 7 0 0.80 1.80 12 8 0 211.48 15.00 12 -8 0 230.78 15.10 -12 -8 0 216.38 16.30 -12 8 0 195.28 14.60 12 8 0 186.78 16.90 -12 9 0 5.90 2.80 12 -9 0 7.40 3.40 12 9 0 15.30 5.00 -12 -9 0 7.00 3.80 12 9 0 5.80 3.20 12 -10 0 33.10 5.90 12 10 0 18.40 5.90 -12 -10 0 27.30 6.40 12 10 0 27.90 5.60 -12 10 0 19.40 4.20 -12 -11 0 -1.40 4.00 12 -11 0 5.10 4.00 12 11 0 9.60 4.00 12 11 0 6.80 4.60 12 12 0 87.89 10.70 -12 -12 0 92.29 12.20 12 -12 0 109.59 11.80 12 12 0 109.99 14.00 12 13 0 0.20 5.00 -12 -13 0 2.40 4.00 12 -13 0 -2.90 4.20 12 13 0 -1.50 3.30 12 14 0 32.10 8.90 -12 -14 0 33.50 8.40 12 14 0 32.20 7.10 -12 -15 0 4.00 4.70 12 15 0 -3.50 4.10 12 15 0 -4.90 5.90 -13 0 0 1.30 1.80 13 0 0 -0.60 1.80 -13 0 0 -0.90 1.00 13 0 0 0.50 1.40 13 1 0 46.60 6.50 13 -1 0 50.89 6.20 -13 -1 0 50.59 5.80 13 1 0 51.29 5.40 13 -1 0 46.80 5.20 -13 1 0 51.09 5.90 -13 -1 0 47.50 4.70 -13 -2 0 215.38 14.70 -13 -2 0 231.38 15.20 13 -2 0 234.08 15.20 13 2 0 232.68 16.90 -13 2 0 256.37 16.00 13 -2 0 216.88 15.30 13 2 0 244.28 15.10 13 3 0 124.79 8.90 -13 -3 0 106.99 8.60 -13 -3 0 111.19 8.90 13 -3 0 109.09 8.50 13 3 0 118.89 10.60 -13 3 0 123.79 9.50 -13 4 0 5.10 2.30 -13 -4 0 0.40 1.90 13 -4 0 5.10 1.70 13 4 0 -2.00 2.10 -13 -4 0 4.70 2.00 13 4 0 1.00 1.80 13 5 0 -0.60 2.40 13 -5 0 0.00 1.00 -13 -5 0 -0.30 1.50 -13 -5 0 -0.70 2.20 13 5 0 -0.70 1.60 -13 5 0 1.50 2.30 13 6 0 172.88 14.30 13 6 0 158.08 11.70 -13 6 0 172.68 12.30 -13 -6 0 146.59 12.40 -13 -6 0 157.98 10.90 -13 -7 0 5.90 3.50 13 -7 0 6.10 2.80 -13 -7 0 10.00 2.30 13 7 0 9.40 4.30 13 7 0 13.20 3.50 -13 7 0 12.40 3.60 13 8 0 3.40 2.20 13 -8 0 1.50 2.60 -13 -8 0 0.30 2.50 -13 8 0 1.40 2.10 13 8 0 0.70 2.90 13 9 0 6.10 3.00 -13 -9 0 15.80 5.00 13 -9 0 6.70 3.40 -13 9 0 6.90 3.20 13 9 0 1.30 3.50 -13 -10 0 9.80 4.50 13 -10 0 4.10 3.50 -13 10 0 7.70 3.30 13 10 0 7.80 3.70 13 10 0 3.60 4.70 -13 -11 0 5.80 4.70 13 11 0 15.60 6.10 13 11 0 9.90 3.90 13 -11 0 11.80 4.60 -13 -12 0 115.49 14.10 13 12 0 135.49 12.20 13 12 0 115.59 14.90 -13 -13 0 5.10 4.40 13 13 0 -0.20 3.20 13 13 0 1.60 5.70 -13 -14 0 6.40 5.40 13 14 0 5.30 4.20 13 14 0 6.00 6.10 -14 0 0 4.90 1.60 -14 0 0 4.30 2.20 14 0 0 6.60 2.80 14 0 0 5.00 1.90 -14 -1 0 1265.27 69.39 14 1 0 1191.48 70.59 -14 1 0 1231.28 69.39 14 -1 0 1173.28 69.69 14 -1 0 1241.48 68.99 -14 -1 0 1215.68 67.99 14 1 0 1217.48 68.79 -14 -2 0 1.20 1.70 -14 -2 0 -2.00 1.40 14 -2 0 -1.10 1.80 -14 2 0 4.00 2.30 14 2 0 1.60 1.60 14 2 0 0.60 2.40 14 -2 0 2.00 1.80 -14 -3 0 603.24 34.20 -14 -3 0 560.84 34.00 14 -3 0 570.64 34.00 14 3 0 610.94 36.70 14 3 0 561.64 34.00 -14 3 0 569.14 34.80 14 4 0 6.00 2.40 14 -4 0 5.40 1.90 -14 -4 0 6.20 2.20 -14 4 0 2.30 2.20 14 4 0 5.80 3.10 -14 -4 0 5.10 2.70 14 -5 0 734.13 39.90 -14 -5 0 723.33 42.30 -14 -5 0 693.03 41.00 -14 5 0 674.73 42.10 14 5 0 708.83 41.60 14 5 0 706.83 44.30 -14 -6 0 3.40 1.90 -14 6 0 5.60 2.90 14 6 0 7.90 4.00 -14 -6 0 1.60 2.50 14 6 0 3.90 2.40 14 7 0 238.38 15.50 -14 7 0 216.18 15.40 14 7 0 177.88 16.90 14 -7 0 228.68 14.80 -14 -7 0 217.38 14.00 -14 -7 0 194.98 15.90 14 -8 0 2.00 2.70 14 8 0 2.70 2.50 -14 -8 0 3.90 3.40 -14 8 0 -0.20 1.80 14 8 0 -3.00 2.50 -14 -9 0 263.37 20.90 14 9 0 295.87 20.10 14 -9 0 295.07 23.90 -14 9 0 297.47 19.80 14 9 0 305.77 23.20 -14 -10 0 21.00 6.00 14 10 0 18.60 6.30 -14 10 0 21.80 4.40 14 10 0 19.90 4.90 14 11 0 204.68 16.50 -14 -11 0 220.88 18.00 14 11 0 236.58 19.60 -14 11 0 214.38 15.80 14 12 0 1.40 4.20 -14 -12 0 -1.60 3.90 14 12 0 1.30 3.20 14 13 0 31.40 6.70 -14 -13 0 36.50 8.30 14 13 0 43.30 9.60 -14 -14 0 0.20 4.60 14 14 0 6.40 4.60 14 14 0 -3.30 5.80 15 0 0 1.80 1.70 -15 0 0 3.40 2.20 15 0 0 0.00 2.10 15 -1 0 6.40 2.20 -15 -1 0 6.20 2.50 15 -1 0 12.50 3.50 -15 -1 0 6.30 2.00 15 1 0 8.10 2.30 15 1 0 11.80 3.80 -15 1 0 12.40 3.20 15 2 0 40.90 4.90 -15 -2 0 37.30 4.50 -15 -2 0 34.80 4.80 15 -2 0 35.30 5.20 15 2 0 28.30 5.90 15 -2 0 41.00 5.00 -15 2 0 29.00 5.00 15 3 0 0.80 2.50 -15 -3 0 3.90 2.30 15 -3 0 5.30 2.50 15 3 0 3.00 2.00 15 -3 0 5.10 2.30 -15 -3 0 4.10 2.30 -15 3 0 5.40 2.80 15 -4 0 78.19 6.50 -15 -4 0 72.89 6.70 15 4 0 77.09 7.00 -15 4 0 92.59 9.10 -15 -4 0 73.59 8.00 15 4 0 64.39 9.20 15 5 0 0.50 2.80 15 5 0 -3.70 1.30 -15 -5 0 -0.40 1.70 -15 5 0 0.10 2.40 -15 -5 0 1.60 2.70 15 6 0 85.19 7.90 -15 -6 0 97.29 7.60 -15 -6 0 87.19 9.90 -15 6 0 89.39 9.60 15 6 0 82.59 11.30 -15 7 0 2.40 2.60 15 7 0 -1.70 1.90 15 7 0 2.70 3.70 -15 -7 0 1.50 3.00 -15 -8 0 5.50 3.40 15 8 0 3.00 2.90 -15 8 0 4.10 2.90 15 8 0 6.70 4.40 -15 9 0 20.90 4.50 -15 -9 0 23.00 6.10 15 9 0 12.50 5.10 15 9 0 17.90 4.70 -15 10 0 2.70 2.80 15 10 0 4.60 4.50 -15 -10 0 5.10 4.70 15 10 0 2.40 2.90 15 11 0 1.60 2.90 15 11 0 2.20 4.40 -15 -11 0 1.10 4.00 -15 11 0 1.20 2.90 15 12 0 25.80 7.70 15 12 0 24.90 5.90 -15 -12 0 32.20 8.00 15 13 0 10.20 4.80 15 13 0 2.30 4.80 -15 -13 0 3.20 4.60 15 14 0 17.80 6.10 15 14 0 16.40 7.70 -15 -14 0 21.90 7.60 16 0 0 1823.02 106.49 -16 0 0 1806.32 105.39 16 0 0 1997.40 105.09 -16 -1 0 1.10 1.50 16 -1 0 -0.80 1.70 -16 1 0 -0.10 1.60 16 1 0 0.70 1.50 16 -1 0 -2.90 1.60 -16 -1 0 0.00 1.80 16 1 0 1.50 2.80 16 2 0 140.49 10.40 16 2 0 137.19 12.40 -16 2 0 156.28 11.50 -16 -2 0 137.19 10.00 -16 -2 0 135.19 10.70 16 -2 0 158.18 11.00 16 -2 0 128.99 11.00 16 -3 0 3.10 2.10 -16 3 0 -0.10 2.00 16 3 0 1.00 1.90 -16 -3 0 0.30 2.00 16 3 0 4.70 3.30 -16 -3 0 1.80 2.10 16 -3 0 2.70 2.00 16 4 0 884.81 55.59 16 4 0 860.01 52.59 -16 4 0 974.50 53.99 -16 -4 0 965.20 53.19 16 -4 0 881.21 52.19 -16 -4 0 930.71 52.69 -16 5 0 5.20 3.00 16 5 0 -0.80 2.00 -16 -5 0 -0.70 1.90 16 5 0 0.00 3.10 -16 -5 0 3.30 2.70 16 6 0 583.54 39.50 -16 -6 0 588.74 37.20 -16 -6 0 632.44 35.90 16 6 0 606.74 36.40 -16 6 0 611.64 37.20 -16 7 0 1.80 2.40 -16 -7 0 -1.50 2.90 16 7 0 -0.10 3.20 16 7 0 -0.90 2.10 16 8 0 41.20 8.30 16 8 0 46.90 6.60 -16 8 0 44.40 6.70 -16 -8 0 50.79 7.80 16 9 0 10.90 3.90 -16 9 0 7.10 3.60 16 9 0 3.60 4.20 -16 -9 0 5.90 4.10 16 10 0 450.35 32.80 -16 10 0 449.26 29.10 16 10 0 458.05 29.40 -16 -10 0 452.65 30.90 16 11 0 6.10 3.60 16 11 0 -2.10 4.10 -16 11 0 -2.80 2.60 -16 -11 0 -2.10 4.40 16 12 0 0.30 3.50 -16 -12 0 -0.30 3.90 16 12 0 -5.60 4.20 16 13 0 -0.30 5.20 -16 -13 0 -5.20 4.10 16 13 0 -2.50 3.70 17 0 0 2.80 2.00 -17 0 0 3.40 2.20 17 0 0 0.70 2.60 -17 -1 0 14.90 3.60 -17 1 0 15.90 3.80 17 1 0 10.60 2.90 17 -1 0 15.00 4.20 17 -1 0 14.70 3.30 17 1 0 16.70 4.60 17 2 0 5.60 3.40 17 2 0 5.80 2.40 -17 2 0 8.30 3.00 -17 -2 0 4.10 2.10 17 -2 0 3.50 2.10 17 -2 0 3.10 2.60 -17 -2 0 3.60 2.40 17 3 0 12.00 3.10 17 -3 0 9.20 2.80 -17 -3 0 9.00 2.70 -17 -3 0 7.80 2.90 17 3 0 2.80 3.20 17 -3 0 9.80 3.20 -17 3 0 4.00 2.80 17 -4 0 108.89 12.40 17 4 0 121.59 13.20 17 -4 0 115.79 9.70 -17 4 0 104.39 10.70 17 4 0 105.59 9.10 -17 -4 0 114.19 9.20 -17 -4 0 117.59 9.60 17 5 0 -2.00 1.60 -17 -5 0 -3.20 2.50 -17 5 0 1.30 2.40 17 5 0 2.20 3.60 -17 -5 0 -0.80 1.90 -17 -6 0 14.00 4.10 17 6 0 29.10 6.90 -17 6 0 24.50 5.10 17 6 0 38.90 5.50 -17 -6 0 23.40 4.10 -17 7 0 5.80 3.10 17 7 0 11.90 3.50 -17 -7 0 6.90 3.90 17 7 0 6.50 4.40 -17 -8 0 20.20 5.30 17 8 0 13.30 3.80 17 8 0 13.60 5.40 -17 8 0 22.70 5.00 -17 9 0 7.40 3.40 17 9 0 5.60 4.10 -17 -9 0 13.20 5.10 17 9 0 15.30 4.30 -17 -10 0 4.30 4.20 17 10 0 2.10 3.20 17 10 0 -0.80 4.60 -17 10 0 -1.50 3.20 17 11 0 23.00 7.20 -17 -11 0 21.90 6.60 17 11 0 14.30 4.50 -17 11 0 15.30 4.60 17 12 0 0.90 3.60 17 12 0 4.10 5.20 -17 -12 0 -3.10 4.40 -17 -13 0 0.70 5.30 17 13 0 -4.80 4.70 17 13 0 4.10 4.30 18 0 0 3.30 2.90 -18 0 0 1.00 2.20 18 0 0 0.50 2.10 -18 1 0 1029.30 59.79 18 1 0 1016.80 61.19 -18 -1 0 1031.70 59.49 18 -1 0 979.30 58.89 18 -1 0 1054.09 60.49 18 1 0 1046.50 58.99 -18 2 0 11.60 3.80 18 2 0 6.40 4.20 18 2 0 12.00 3.30 18 -2 0 12.50 3.20 -18 -2 0 14.10 3.50 18 -2 0 7.10 3.20 18 -3 0 413.76 25.40 18 3 0 380.96 24.80 -18 3 0 402.46 26.00 -18 -3 0 409.66 25.30 18 -3 0 375.96 25.20 18 3 0 440.86 28.40 18 4 0 17.20 3.90 -18 4 0 10.10 4.00 -18 -4 0 12.10 3.60 18 4 0 13.40 5.00 -18 -4 0 14.20 5.80 18 -4 0 23.00 4.40 18 5 0 1352.56 74.39 -18 5 0 1299.57 75.29 -18 -5 0 1278.17 74.49 -18 -5 0 1333.47 74.09 18 5 0 1219.18 77.39 -18 6 0 1.40 2.60 18 6 0 -0.30 2.30 -18 -6 0 -2.10 3.00 18 6 0 -1.40 3.40 -18 7 0 179.28 14.40 18 7 0 190.88 14.00 18 7 0 198.38 17.40 -18 -7 0 183.98 14.90 -18 8 0 1.80 3.00 18 8 0 -5.00 3.60 -18 -8 0 4.30 3.90 18 8 0 -0.30 2.20 18 9 0 295.67 20.40 -18 9 0 308.47 20.90 18 9 0 275.97 23.60 -18 -9 0 280.67 21.30 -18 10 0 4.40 3.30 -18 -10 0 2.20 3.90 18 10 0 -2.30 2.40 18 10 0 -6.40 3.90 18 11 0 257.27 22.40 -18 11 0 255.57 18.80 -18 -11 0 234.68 20.10 18 11 0 275.87 19.20 18 12 0 0.20 5.30 -18 -12 0 1.40 5.10 18 12 0 0.40 3.70 19 0 0 0.70 2.50 -19 0 0 -0.10 2.00 19 0 0 2.20 1.90 19 1 0 181.28 15.30 19 -1 0 178.98 13.40 19 -1 0 213.28 15.30 19 1 0 175.68 13.30 -19 -1 0 198.18 14.10 -19 1 0 192.48 14.40 19 2 0 7.50 2.90 19 -2 0 4.70 2.90 -19 -2 0 4.90 2.80 19 2 0 10.80 4.20 19 -2 0 3.50 2.50 -19 2 0 7.20 3.00 -19 -3 0 5.80 2.80 19 -3 0 7.70 2.90 19 3 0 1.30 2.20 -19 3 0 3.90 2.90 19 -3 0 1.10 2.70 19 3 0 3.50 3.70 19 4 0 13.70 3.60 19 -4 0 15.70 4.10 19 4 0 9.20 4.70 -19 -4 0 21.30 4.30 -19 4 0 7.00 3.70 19 5 0 17.10 4.40 19 -5 0 26.60 5.30 -19 5 0 36.30 6.20 19 5 0 21.60 6.20 -19 -5 0 31.70 5.10 -19 6 0 19.00 4.80 19 6 0 30.40 7.60 19 6 0 10.10 3.60 19 7 0 9.10 3.60 -19 7 0 2.70 3.10 19 7 0 4.10 4.60 -19 8 0 5.40 3.70 19 8 0 5.80 3.50 19 8 0 7.40 5.60 -19 -8 0 14.50 4.50 -19 9 0 52.39 7.50 19 9 0 48.20 7.10 19 9 0 21.90 7.50 -19 -9 0 55.79 8.80 19 10 0 1.80 3.30 -19 -10 0 -0.60 4.10 -19 10 0 2.90 3.50 19 10 0 4.60 5.20 -19 -11 0 39.90 8.20 19 11 0 61.49 8.50 19 11 0 52.29 11.10 -19 11 0 59.79 8.10 19 12 0 3.70 3.60 19 12 0 -6.50 4.70 -19 -12 0 1.60 4.50 20 0 0 507.95 31.20 20 0 0 534.15 33.40 -20 0 0 490.95 31.70 -20 -1 0 37.10 5.70 20 1 0 33.10 5.10 20 -1 0 35.90 5.30 20 -1 0 30.00 6.00 -20 1 0 29.00 5.40 20 1 0 43.00 7.60 20 -2 0 61.39 8.40 20 2 0 83.79 7.70 20 -2 0 89.29 9.00 -20 -2 0 85.19 9.10 -20 2 0 85.49 9.40 20 2 0 79.89 11.00 -20 -3 0 4.20 2.80 20 -3 0 6.00 3.00 -20 3 0 0.90 2.50 20 3 0 2.20 2.50 20 3 0 8.40 4.70 -20 -4 0 222.28 14.90 20 4 0 186.48 16.90 20 4 0 202.88 14.50 20 -4 0 183.68 14.70 -20 4 0 207.28 15.70 -20 5 0 53.79 7.60 20 5 0 53.99 9.50 -20 -5 0 58.59 7.20 20 -5 0 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142.49 14.60 -13 -7 2 120.09 12.30 13 7 -2 116.19 9.60 -13 7 2 117.99 10.00 -13 -7 -2 119.79 8.90 13 7 -2 123.99 13.60 -13 -7 -2 100.59 11.20 13 -7 2 129.19 9.60 -13 8 -2 13.90 3.60 13 8 2 16.40 5.40 -13 -8 2 22.30 5.50 13 8 2 18.60 4.20 -13 -8 -2 22.40 3.50 13 8 -2 24.20 6.10 -13 8 2 16.40 4.00 13 8 -2 23.20 4.30 13 -8 2 19.40 4.00 -13 -8 -2 17.90 4.80 -13 -9 2 3.10 3.70 13 9 2 3.30 2.80 -13 9 -2 7.30 3.10 13 9 2 3.20 4.00 13 9 -2 7.60 4.20 13 9 -2 13.10 3.80 -13 9 2 9.50 3.40 13 -9 2 3.70 3.20 -13 -9 -2 20.90 5.50 13 -10 -2 27.70 5.70 -13 -10 2 24.90 6.50 13 10 2 18.20 6.20 -13 10 -2 28.10 5.20 13 10 2 19.50 4.90 13 10 -2 14.60 5.50 -13 -10 -2 11.00 4.40 13 10 -2 23.00 5.10 13 -10 2 15.20 5.30 13 11 2 104.59 11.60 13 11 2 102.79 13.80 -13 11 -2 112.79 9.80 -13 -11 2 92.29 12.30 13 -11 -2 111.09 11.90 13 11 -2 101.09 13.40 13 11 -2 110.39 11.70 -13 -11 -2 124.29 13.60 13 12 2 6.70 4.00 -13 12 -2 4.60 3.20 13 -12 -2 4.10 4.30 13 12 2 1.90 4.90 -13 -12 2 9.60 5.40 13 12 -2 7.40 3.90 13 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147.59 10.30 -8 2 -3 126.19 8.90 -8 -2 -3 115.59 8.30 -8 -2 -3 120.49 8.20 -8 2 3 118.99 8.50 8 -2 3 119.69 8.40 8 2 -3 122.09 7.80 8 3 3 0.00 2.20 -8 3 -3 0.50 1.50 8 3 3 1.50 1.50 -8 -3 3 2.60 2.00 8 -3 -3 -1.00 0.80 -8 -3 3 0.50 0.90 8 -3 3 0.00 1.00 8 -3 3 1.40 1.00 -8 -3 -3 -1.40 1.20 8 3 -3 0.30 1.20 -8 -3 -3 0.30 1.10 -8 3 3 0.90 1.40 8 -4 -3 5.20 0.60 8 -4 -3 4.90 0.80 8 4 3 4.90 2.10 -8 -4 3 3.30 1.20 8 4 3 1.00 2.40 -8 4 -3 3.20 2.00 -8 -4 3 11.00 3.10 8 -4 3 4.20 1.60 -8 4 3 7.20 2.10 -8 -4 -3 5.20 1.60 8 4 -3 3.00 1.40 8 -4 3 3.20 1.10 -8 -4 -3 3.10 2.00 8 5 3 16.20 4.00 -8 5 -3 12.20 2.90 -8 -5 3 17.20 4.00 -8 -5 3 18.20 2.10 8 5 3 16.20 3.30 -8 -5 -3 18.50 2.70 -8 -5 -3 9.10 2.90 8 5 -3 14.80 3.00 -8 5 3 18.50 3.20 8 -5 3 19.70 2.10 8 -5 3 17.50 3.00 8 6 3 0.40 2.60 -8 6 -3 4.20 2.30 -8 -6 3 1.70 2.50 8 6 3 1.70 1.80 -8 -6 3 3.30 1.10 8 -6 3 3.60 1.10 -8 6 3 0.00 1.60 8 -6 3 0.50 1.90 8 6 -3 7.50 2.20 -8 -6 -3 3.40 2.40 8 7 3 4.80 3.20 8 7 3 7.90 2.80 -8 -7 3 5.70 1.20 -8 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5.00 8 14 3 9.60 4.70 8 -14 -3 13.10 6.10 8 14 3 13.80 6.20 -8 -14 -3 11.90 5.60 8 -14 3 8.60 5.40 8 14 -3 19.40 6.20 8 14 -3 21.00 6.40 8 15 3 5.00 4.40 8 15 3 -1.00 4.20 -8 -15 3 0.20 4.50 8 -15 -3 -2.10 4.70 8 -15 3 2.20 4.70 -8 -15 -3 3.10 5.60 8 15 -3 2.20 5.00 8 15 -3 5.30 4.60 8 -16 -3 2.80 5.50 -8 -16 3 1.70 5.00 8 16 3 3.60 4.70 8 -16 3 -4.30 4.90 -8 -16 -3 9.20 6.70 8 16 -3 2.10 5.60 8 16 -3 3.60 5.30 -9 0 -3 -0.40 1.40 9 0 3 1.00 1.20 9 0 -3 -0.20 0.80 9 0 3 -0.30 1.50 -9 0 3 1.10 1.30 -9 0 -3 0.00 0.60 -9 0 3 1.60 1.40 -9 -1 3 146.89 9.70 9 1 3 146.79 10.20 -9 -1 3 152.48 10.00 -9 1 -3 134.69 10.20 9 1 3 137.29 10.90 9 -1 -3 158.38 9.40 -9 -1 -3 137.19 10.00 9 -1 3 154.98 10.40 -9 -1 -3 142.29 9.10 -9 1 3 156.88 10.10 9 -1 3 152.58 10.50 9 1 -3 150.18 9.20 -9 -2 3 71.29 6.40 -9 2 -3 82.89 6.70 -9 -2 3 84.39 5.90 9 2 3 79.79 8.40 9 2 3 76.89 6.40 9 -2 -3 80.29 6.00 -9 -2 -3 68.39 6.00 9 2 -3 81.79 5.60 -9 2 3 81.89 6.30 -9 -2 -3 82.69 6.00 9 -2 3 68.49 6.10 9 -3 -3 42.00 3.60 -9 -3 3 35.20 4.90 9 3 3 42.90 5.00 9 3 3 34.40 5.60 -9 3 -3 47.20 5.20 -9 -3 3 46.20 3.70 9 -3 3 44.80 3.90 -9 3 3 40.00 4.80 -9 -3 -3 36.70 4.30 9 3 -3 43.10 3.70 9 -3 3 37.10 3.20 -9 -3 -3 38.00 4.50 -9 -4 3 9.60 2.90 9 -4 -3 9.90 1.40 9 4 3 15.50 3.00 9 -4 -3 10.80 1.20 -9 -4 3 11.60 1.90 9 4 3 3.00 2.60 -9 4 -3 11.70 2.80 9 4 -3 10.00 2.20 -9 -4 -3 12.10 3.00 -9 -4 -3 11.40 2.30 9 -4 3 8.70 1.70 -9 4 3 10.50 2.40 9 -4 3 13.20 2.10 9 5 3 21.40 3.90 9 5 3 20.20 4.80 -9 -5 3 17.90 4.20 -9 5 -3 18.20 3.60 -9 -5 3 23.30 2.50 -9 5 3 16.00 3.10 -9 -5 -3 21.80 4.10 9 -5 3 22.00 3.30 -9 -5 -3 21.20 2.90 9 -5 3 20.70 2.20 9 5 -3 17.00 3.00 -9 -6 3 150.18 9.30 9 6 3 155.08 12.90 9 6 3 156.78 11.50 -9 6 -3 141.19 11.00 -9 -6 3 149.39 12.10 9 -6 3 164.58 11.00 9 -6 3 150.28 9.20 -9 6 3 155.88 10.90 -9 -6 -3 160.08 10.20 -9 -6 -3 163.98 12.10 9 6 -3 142.89 10.80 -9 7 -3 51.19 6.30 -9 -7 3 58.99 8.00 9 7 3 73.89 7.70 -9 -7 3 66.29 4.60 9 7 3 66.09 8.90 -9 -7 -3 61.29 5.30 -9 7 3 68.49 6.90 9 -7 3 72.69 7.30 -9 -7 -3 56.99 7.60 9 7 -3 72.49 6.40 9 8 3 5.90 2.80 -9 -8 3 2.90 2.90 9 8 3 8.20 4.00 -9 8 -3 4.30 2.30 9 -8 3 8.00 2.90 9 8 -3 4.60 3.00 -9 -8 -3 5.40 3.20 9 8 -3 4.40 2.40 -9 9 -3 14.80 3.40 -9 -9 3 5.30 3.90 9 9 3 30.80 5.30 9 9 3 22.80 5.70 9 9 -3 8.80 4.00 9 9 -3 15.10 4.20 -9 -9 -3 25.30 5.30 9 -9 3 16.20 4.30 -9 10 -3 11.80 3.40 9 10 3 15.30 5.70 -9 -10 3 15.80 5.10 9 10 3 13.90 4.10 -9 -10 -3 16.30 5.10 9 10 -3 14.30 5.60 9 10 -3 18.10 4.60 9 -10 3 12.70 4.30 -9 -11 3 85.29 11.30 9 -11 -3 70.49 9.80 -9 11 -3 85.39 8.40 9 11 3 85.19 10.00 9 11 3 70.89 10.70 9 11 -3 78.59 10.80 -9 -11 -3 120.79 12.70 9 -11 3 86.19 10.10 9 11 -3 76.09 9.50 9 12 3 60.39 8.60 -9 -12 3 67.19 10.10 9 12 3 76.69 10.80 9 -12 -3 66.89 9.60 9 12 -3 70.59 9.40 -9 -12 -3 62.69 9.80 9 12 -3 59.49 9.90 9 -12 3 75.59 9.50 9 13 3 2.90 3.20 -9 -13 3 2.50 3.80 9 -13 -3 3.00 4.50 9 13 3 8.20 4.70 -9 -13 -3 10.10 5.30 9 13 -3 3.70 4.40 9 -13 3 -0.70 3.80 9 13 -3 0.40 2.90 -9 -14 3 2.20 3.90 9 14 3 2.50 3.40 9 14 3 0.10 4.20 9 -14 -3 1.00 4.80 9 -14 3 3.00 4.80 9 14 -3 6.50 4.20 9 14 -3 7.40 4.80 -9 -14 -3 6.80 4.60 -9 -15 3 -0.40 4.40 9 15 3 -4.50 3.80 9 -15 -3 4.10 5.70 9 15 3 0.60 3.60 9 15 -3 3.90 4.90 9 15 -3 3.30 5.40 9 -15 3 -5.80 4.20 -9 -15 -3 4.20 6.20 -10 0 -3 210.18 13.60 -10 0 3 205.98 13.00 10 0 3 181.58 13.70 -10 0 -3 201.78 11.50 -10 0 3 196.28 12.80 10 0 3 217.88 13.50 10 0 -3 203.18 12.30 -10 -1 3 239.18 15.00 10 -1 -3 244.58 14.40 10 -1 -3 242.18 15.30 10 1 3 256.27 15.40 10 1 3 236.28 16.30 -10 -1 3 237.98 14.80 -10 1 -3 253.97 15.60 -10 -1 -3 228.48 15.10 10 -1 3 225.48 15.50 10 -1 3 235.38 15.30 -10 1 3 225.68 15.00 10 1 -3 225.78 14.10 -10 -1 -3 236.88 14.10 10 2 3 66.49 5.90 -10 -2 3 81.39 6.40 -10 2 -3 67.39 6.80 10 2 3 55.19 7.20 10 -2 -3 56.49 5.40 -10 -2 3 72.39 5.40 10 -2 3 59.99 5.70 -10 -2 -3 66.99 5.40 10 2 -3 66.39 5.00 10 -2 3 70.39 6.10 -10 2 3 69.09 5.90 -10 -2 -3 63.19 5.70 10 3 3 18.50 3.40 10 3 3 22.00 4.50 10 -3 -3 28.50 3.20 -10 3 -3 14.40 3.20 -10 -3 3 26.00 4.00 -10 -3 3 26.20 3.10 -10 3 3 26.30 3.60 10 3 -3 22.70 3.00 10 -3 3 22.20 2.30 -10 -3 -3 21.40 3.30 -10 -3 -3 24.10 3.50 10 -3 3 21.50 3.10 -10 -4 3 18.70 3.90 10 -4 -3 21.70 2.30 -10 -4 3 21.00 2.70 10 4 3 20.30 3.60 10 4 3 17.60 4.60 -10 4 -3 15.80 3.30 10 -4 3 18.90 2.60 10 -4 3 19.40 2.60 -10 -4 -3 16.60 3.30 -10 -4 -3 16.30 2.80 10 4 -3 16.60 2.80 -10 4 3 21.00 3.40 10 5 3 199.08 15.40 -10 -5 3 203.18 12.20 -10 -5 3 217.98 14.60 -10 5 -3 198.28 13.80 10 5 3 198.08 13.80 -10 5 3 198.08 13.50 10 -5 3 202.88 11.90 -10 -5 -3 204.38 12.90 -10 -5 -3 201.48 14.10 10 5 -3 177.28 12.90 10 -5 3 200.28 12.80 -10 6 -3 0.40 1.80 10 6 3 0.90 2.60 -10 -6 3 4.70 1.40 -10 -6 3 0.50 2.40 10 6 3 6.30 2.60 10 -6 3 2.40 1.00 -10 -6 -3 1.70 1.50 -10 -6 -3 3.60 2.70 10 6 -3 1.50 1.60 -10 6 3 5.70 2.30 10 -6 3 0.00 1.80 -10 -7 3 11.50 3.90 10 7 3 11.00 3.20 -10 -7 3 19.00 2.20 -10 7 -3 16.10 3.60 10 7 3 14.10 4.50 -10 -7 -3 18.30 2.90 -10 -7 -3 13.50 4.10 -10 7 3 11.00 3.10 10 7 -3 14.60 4.40 10 7 -3 13.00 3.20 10 -7 3 10.00 3.20 10 8 3 3.20 3.40 -10 8 -3 6.50 2.80 -10 -8 3 7.00 4.20 10 8 3 4.70 2.70 10 -8 3 5.50 2.70 -10 -8 -3 6.70 3.40 10 8 -3 4.40 2.50 -10 -8 -3 13.30 2.50 10 8 -3 9.80 3.90 10 9 3 39.60 7.50 -10 9 -3 54.49 6.40 -10 -9 3 41.70 7.40 10 9 3 38.20 6.30 10 -9 3 52.19 6.80 10 9 -3 40.70 6.20 10 9 -3 44.20 8.10 -10 -9 -3 57.39 8.20 -10 -9 -3 50.79 5.20 -10 -10 3 6.30 3.80 10 10 3 -2.80 3.20 10 10 3 5.10 3.40 -10 10 -3 5.00 2.60 10 -10 3 4.10 3.40 -10 -10 -3 2.70 3.30 10 10 -3 7.40 4.60 10 10 -3 12.50 3.90 -10 11 -3 32.10 5.00 10 11 3 31.60 7.20 10 -11 -3 44.10 7.60 10 11 3 32.40 6.20 -10 -11 3 30.10 7.30 10 11 -3 46.40 7.20 -10 -11 -3 40.30 7.50 10 -11 3 39.10 6.60 10 11 -3 42.10 8.00 10 12 3 10.90 5.20 10 -12 -3 14.80 5.30 10 12 3 8.90 4.10 -10 -12 3 16.80 6.20 10 -12 3 16.10 5.00 -10 -12 -3 12.50 5.30 10 12 -3 9.30 4.90 10 12 -3 13.40 4.70 10 -13 -3 3.60 4.50 -10 -13 3 6.60 4.90 10 13 3 2.90 4.90 10 13 3 2.30 3.00 10 13 -3 7.80 3.80 10 -13 3 0.40 4.00 -10 -13 -3 4.40 4.80 10 13 -3 4.10 4.50 10 14 3 -0.30 4.40 10 14 3 6.30 4.80 10 -14 -3 3.20 4.70 -10 -14 3 0.20 4.60 10 14 -3 4.20 4.40 10 -14 3 0.00 4.40 10 14 -3 1.10 4.30 -10 -14 -3 9.50 6.10 10 -15 -3 31.80 8.50 10 15 3 36.10 8.80 10 15 3 35.60 7.60 -10 -15 3 40.50 9.70 10 15 -3 49.20 9.90 10 -15 3 41.20 8.50 -10 -15 -3 55.69 10.50 10 15 -3 44.90 8.20 -11 0 3 0.20 1.30 -11 0 -3 -1.80 1.40 -11 0 -3 0.60 0.70 -11 0 3 1.20 1.40 11 0 3 -2.90 1.60 11 0 3 2.00 1.70 11 0 -3 -0.60 0.90 11 0 -3 0.80 1.50 -11 -1 3 22.10 3.20 11 1 3 16.60 3.20 11 -1 -3 19.20 3.40 -11 -1 3 24.60 3.50 -11 1 -3 18.00 3.20 11 1 3 10.70 3.30 11 -1 -3 17.30 2.60 -11 -1 -3 19.00 2.40 11 -1 3 18.00 3.50 -11 -1 -3 19.50 3.40 11 -1 3 18.30 3.20 -11 1 3 22.10 3.30 11 1 -3 20.20 2.60 11 2 3 69.79 8.20 -11 -2 3 69.49 6.20 -11 2 -3 73.79 7.50 11 2 3 71.99 6.40 -11 -2 3 71.79 5.80 11 -2 -3 66.89 6.00 11 -2 3 68.49 6.20 -11 -2 -3 67.69 5.60 -11 -2 -3 68.69 6.10 11 -2 3 75.69 6.50 11 2 -3 70.89 5.40 -11 2 3 76.99 6.30 -11 -3 3 29.70 3.50 11 3 3 35.20 5.60 11 -3 -3 31.30 3.80 -11 -3 3 33.20 4.70 11 3 3 27.80 4.20 -11 3 -3 32.00 4.80 11 3 -3 30.80 3.70 -11 -3 -3 25.90 3.80 -11 3 3 30.90 4.30 11 -3 3 28.00 3.90 -11 -3 -3 28.20 4.00 11 -3 3 33.50 2.40 -11 -4 3 87.59 8.10 -11 -4 3 90.29 6.60 11 -4 -3 91.19 6.30 11 4 3 82.39 7.50 11 4 3 97.09 10.40 -11 4 -3 99.09 8.10 11 4 -3 89.89 6.90 11 -4 3 92.49 6.70 -11 4 3 91.99 7.60 11 -4 3 97.79 6.30 -11 -4 -3 94.09 7.20 -11 -4 -3 96.79 7.80 -11 -5 3 18.70 4.20 11 5 3 18.90 4.70 -11 -5 3 15.10 2.50 11 5 3 17.60 3.50 -11 5 -3 12.80 3.20 11 -5 3 15.00 2.10 -11 -5 -3 18.00 3.80 -11 -5 -3 21.60 3.30 -11 5 3 18.90 3.50 11 -5 3 24.10 3.20 11 5 -3 12.70 2.80 -11 -6 3 202.18 11.40 11 6 3 181.58 14.90 -11 6 -3 187.98 13.30 11 6 3 180.98 13.10 -11 -6 3 179.58 13.90 -11 -6 -3 175.38 13.50 -11 -6 -3 169.88 11.90 11 -6 3 187.28 12.30 11 6 -3 163.28 14.40 11 -6 3 167.18 10.70 11 6 -3 184.68 12.60 -11 6 3 198.68 13.10 11 7 3 18.70 5.20 -11 7 -3 17.40 4.10 -11 -7 3 21.60 2.70 -11 -7 3 18.80 4.80 11 7 3 20.30 4.00 -11 7 3 17.20 3.50 -11 -7 -3 24.20 3.50 -11 -7 -3 25.50 5.10 11 7 -3 17.60 4.90 11 -7 3 24.70 4.10 11 7 -3 23.50 4.10 -11 8 -3 16.70 3.90 -11 -8 3 15.60 4.40 11 8 3 10.50 4.20 11 8 3 15.50 3.90 -11 -8 -3 12.00 4.00 11 -8 3 12.30 3.40 -11 -8 -3 9.40 2.30 -11 8 3 18.10 3.80 11 8 -3 11.30 3.00 11 8 -3 6.50 3.80 11 9 3 26.00 6.20 11 9 3 41.80 6.10 -11 9 -3 20.60 4.10 -11 -9 3 25.50 5.90 11 9 -3 22.80 4.80 -11 -9 -3 29.30 6.00 -11 -9 -3 33.70 4.20 11 -9 3 33.50 5.60 11 9 -3 20.70 5.80 -11 -10 3 25.60 6.10 11 10 3 21.80 5.00 -11 10 -3 22.30 4.50 11 10 3 10.20 5.10 11 10 -3 17.00 6.00 11 -10 3 12.10 4.20 -11 -10 -3 17.50 5.50 11 10 -3 25.70 5.30 -11 11 -3 27.30 4.90 11 -11 -3 32.20 6.80 11 11 3 47.90 9.00 -11 -11 3 19.10 5.80 11 11 3 42.50 6.80 11 11 -3 39.60 8.00 -11 -11 -3 19.80 6.00 11 -11 3 41.00 6.80 11 11 -3 38.50 6.50 11 12 3 60.19 8.50 11 12 3 50.39 9.70 -11 -12 3 49.70 8.80 11 -12 -3 48.70 8.40 11 12 -3 44.90 7.60 11 12 -3 45.00 8.90 11 -12 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73.89 7.60 13 1 -3 69.99 7.90 -13 1 3 60.59 6.30 13 1 -3 66.29 5.10 -13 -1 -3 56.89 6.50 -13 -1 -3 58.69 4.60 13 -1 3 58.49 6.50 13 2 3 31.70 4.60 13 -2 -3 29.00 4.20 -13 2 -3 19.80 4.20 13 2 3 15.70 4.30 -13 -2 3 22.80 3.80 13 -2 -3 23.30 3.50 -13 -2 3 31.00 3.90 13 2 -3 31.30 3.60 13 -2 3 26.80 4.30 -13 2 3 29.40 4.50 13 -2 3 29.50 4.40 -13 -2 -3 26.00 3.50 -13 -2 -3 26.80 4.30 13 2 -3 19.60 4.80 13 3 3 1.30 1.80 13 3 3 5.70 3.30 -13 -3 3 4.80 1.90 -13 3 -3 5.60 2.60 -13 -3 3 6.40 2.50 13 -3 -3 5.40 2.10 -13 3 3 6.30 2.30 13 -3 3 7.40 2.40 -13 -3 -3 5.80 2.40 13 3 -3 4.90 3.30 13 3 -3 4.50 1.80 -13 -3 -3 7.20 2.40 -13 4 -3 39.10 5.70 13 4 3 34.20 6.50 -13 -4 3 48.30 5.00 13 -4 -3 49.40 4.40 -13 -4 3 46.40 6.20 13 4 3 48.40 5.90 13 -4 3 50.89 3.70 -13 -4 -3 50.49 5.60 -13 4 3 53.99 6.20 13 -4 3 45.70 5.00 13 4 -3 34.40 6.60 13 4 -3 46.90 5.00 -13 -4 -3 48.50 5.60 13 5 3 4.00 2.50 13 -5 -3 3.60 1.20 -13 -5 3 3.60 2.70 13 5 3 1.70 2.90 -13 5 -3 5.00 2.70 -13 -5 3 3.60 1.70 13 5 -3 6.60 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697.43 41.80 -14 -5 -3 663.93 39.10 -14 -5 -3 634.14 38.30 14 -5 3 649.64 37.30 -14 5 3 644.14 39.00 14 6 3 7.10 2.80 -14 -6 3 5.90 1.90 14 6 3 -0.60 3.00 -14 6 -3 6.90 3.20 -14 -6 3 3.40 2.90 -14 -6 -3 5.60 2.90 14 6 -3 5.90 2.40 -14 -6 -3 1.90 2.00 14 6 -3 -1.90 2.90 -14 6 3 4.70 2.60 -14 -7 3 25.30 5.40 -14 7 -3 20.90 4.60 14 7 3 22.90 4.60 14 7 3 17.90 5.80 -14 7 3 17.20 3.90 14 7 -3 27.80 4.40 14 7 -3 15.30 5.20 -14 -7 -3 17.40 3.40 -14 -7 -3 21.90 5.00 -14 8 -3 6.50 3.00 14 8 3 10.30 3.80 -14 -8 3 2.90 3.10 14 8 3 5.90 4.30 -14 8 3 14.40 3.50 14 8 -3 7.20 3.00 14 8 -3 3.30 3.90 -14 -8 -3 6.40 2.50 -14 -8 -3 3.40 3.10 -14 9 -3 74.59 8.30 14 9 3 52.39 9.10 -14 -9 3 93.19 11.20 14 9 3 74.49 8.90 14 9 -3 70.09 10.60 -14 9 3 68.89 8.20 14 9 -3 54.99 7.30 -14 -9 -3 61.29 9.00 -14 -10 3 -2.50 4.10 14 -10 -3 4.40 4.10 -14 10 -3 2.70 3.00 14 10 3 1.50 4.20 14 10 3 11.00 3.90 14 10 -3 2.20 4.10 14 10 -3 0.60 2.70 -14 -10 -3 12.20 4.80 -14 -11 3 44.70 8.80 14 11 3 58.19 8.20 14 -11 -3 51.19 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7 3 27.80 6.10 21 7 -3 24.20 7.60 -21 8 -3 -0.50 2.70 21 8 3 -1.50 4.10 21 8 3 5.90 3.30 21 8 -3 -1.30 4.50 -21 8 3 1.20 3.30 21 9 3 13.10 6.00 -21 9 -3 6.60 4.20 21 9 3 5.30 3.70 21 9 -3 3.30 5.70 -21 9 3 -0.80 3.00 21 10 3 6.90 4.10 -21 10 -3 12.30 5.00 21 10 3 18.60 6.80 -21 10 3 4.70 4.10 21 10 -3 6.40 5.10 22 0 3 2.60 3.70 -22 0 3 4.30 3.00 22 0 -3 2.10 3.50 22 0 3 4.60 2.80 -22 0 -3 9.20 3.50 -22 1 -3 124.99 11.10 22 -1 -3 117.39 12.80 -22 -1 3 110.09 11.40 22 1 3 117.59 13.60 22 1 3 143.59 11.20 22 -1 3 125.69 13.10 -22 -1 -3 122.29 12.10 22 -1 3 115.59 10.60 22 1 -3 133.39 14.20 -22 1 3 115.79 11.80 22 2 3 1.50 4.00 22 2 3 2.30 2.90 -22 2 -3 4.40 3.30 -22 -2 3 0.00 2.50 22 2 -3 2.10 3.80 22 -2 3 -0.20 2.60 -22 2 3 7.10 3.10 -22 -2 -3 10.00 3.80 22 3 3 23.80 6.60 -22 -3 3 32.80 5.40 -22 3 -3 23.50 5.40 22 3 3 28.40 5.50 22 -3 3 31.80 6.10 -22 3 3 28.30 5.70 22 3 -3 32.20 7.20 -22 -3 -3 33.90 5.90 22 4 3 -1.70 2.60 22 4 3 -2.00 3.80 -22 4 -3 2.20 3.00 -22 4 3 1.10 2.60 -22 -4 -3 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12 6 4 12.10 3.50 12 6 4 13.90 4.40 -12 -6 4 12.40 2.10 12 6 -4 10.40 2.80 -12 -6 -4 11.60 2.80 -12 6 4 12.50 3.10 12 -6 4 14.60 2.90 12 -6 4 12.90 2.00 -12 -6 -4 14.50 3.60 12 7 4 161.88 12.30 -12 -7 4 170.98 13.50 -12 7 -4 168.08 12.40 12 7 4 158.58 14.10 12 7 -4 160.08 14.10 12 -7 4 150.08 11.20 12 7 -4 163.68 11.70 -12 -7 -4 148.49 12.50 -12 7 4 149.79 11.70 -12 -7 -4 159.28 11.10 12 8 4 101.59 9.30 -12 8 -4 82.59 9.10 -12 -8 4 87.59 10.60 12 8 4 101.29 12.10 12 -8 4 99.69 8.50 12 8 -4 84.19 11.30 12 8 -4 106.79 8.70 -12 -8 -4 105.99 10.90 -12 -8 -4 95.19 7.60 12 9 4 232.08 18.50 -12 9 -4 229.68 15.90 -12 -9 4 202.08 17.30 12 9 4 227.28 16.40 -12 -9 -4 203.38 16.60 12 -9 4 256.17 16.20 -12 -9 -4 210.78 14.40 12 9 -4 201.58 15.50 12 9 -4 234.58 18.60 12 10 4 18.20 4.70 -12 10 -4 18.50 4.00 -12 -10 4 12.80 5.50 12 10 4 18.90 5.90 12 10 -4 14.80 4.20 -12 -10 -4 18.10 5.10 12 10 -4 10.40 5.10 12 -10 4 9.90 4.10 12 -11 -4 129.79 12.80 -12 -11 4 106.69 13.40 12 11 4 87.49 10.80 12 11 4 108.59 13.60 -12 11 -4 106.39 10.50 12 -11 4 105.99 11.90 12 11 -4 119.89 14.00 -12 -11 -4 109.69 13.10 12 11 -4 112.79 11.70 12 -12 -4 32.40 7.20 12 12 4 43.20 7.40 -12 -12 4 55.29 9.50 12 12 4 54.89 9.70 -12 12 -4 47.20 6.60 -12 -12 -4 56.59 9.30 12 12 -4 50.19 8.00 12 12 -4 51.09 9.70 12 13 4 21.90 6.00 12 13 4 27.10 7.50 12 -13 -4 26.00 6.90 -12 -13 4 18.70 6.60 12 13 -4 34.70 6.90 12 13 -4 30.60 7.30 -12 -13 -4 31.90 8.10 12 14 4 27.60 6.40 12 -14 -4 4.90 5.10 12 14 4 4.30 5.10 -12 -14 4 -2.40 4.90 12 14 -4 9.10 4.30 -12 -14 -4 8.20 6.40 12 14 -4 22.70 7.30 12 -15 -4 38.30 8.70 12 15 4 29.10 7.30 -12 -15 4 45.70 9.80 12 15 4 33.80 8.90 12 15 -4 46.80 10.30 12 15 -4 44.00 8.60 -12 -15 -4 52.59 9.80 -13 0 4 0.90 1.70 13 0 4 -1.80 1.70 13 0 4 -1.30 1.90 13 0 -4 -0.40 1.70 -13 0 -4 -1.00 1.50 13 0 -4 -0.80 1.00 -13 0 4 -0.10 1.60 13 1 4 99.49 8.20 13 -1 -4 92.59 8.20 -13 1 -4 83.59 7.90 13 -1 -4 90.09 6.80 -13 -1 4 95.79 7.50 13 1 4 87.99 9.80 -13 -1 4 97.19 7.60 13 1 -4 92.99 8.50 13 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13.10 2.80 -4 10 -9 346.47 22.90 -4 -10 9 362.56 26.40 4 10 9 398.86 25.60 4 10 9 413.86 26.10 4 -10 9 400.16 26.10 -4 10 9 396.06 25.80 -4 11 -9 8.60 2.50 -4 -11 9 12.00 5.10 4 11 9 3.90 3.30 4 11 9 9.40 4.00 4 -11 9 6.30 3.80 -4 11 9 10.00 4.10 4 12 9 34.00 6.60 -4 -12 9 26.50 7.20 4 12 9 40.70 6.90 4 -12 9 33.60 7.00 -4 12 9 37.70 6.90 -4 -12 -9 37.10 8.10 4 13 9 10.10 4.40 -4 -13 9 0.60 4.30 4 13 9 9.60 4.20 4 -13 9 15.10 5.80 -4 -13 -9 14.40 5.90 -4 13 9 6.50 3.80 4 -14 -9 2.70 4.30 4 14 9 9.40 4.40 -4 -14 9 5.30 5.20 -4 -14 -9 21.70 6.50 4 -14 9 10.10 5.40 -4 14 9 14.00 5.50 -4 -15 9 22.50 7.50 4 15 9 13.00 5.60 4 -15 -9 13.70 6.30 -4 15 9 20.40 6.30 4 -15 9 22.20 6.50 -4 -15 -9 19.20 7.00 -4 -16 9 8.30 6.50 4 -16 -9 15.40 6.90 4 16 9 17.80 6.60 -4 16 9 13.50 5.80 -4 -16 -9 15.90 7.40 4 -16 9 21.20 7.40 -5 0 -9 0.10 1.50 -5 0 9 -1.10 1.70 -5 0 9 -0.40 1.10 -5 0 9 -0.60 0.50 5 0 9 -0.50 1.40 5 0 9 -0.40 1.40 5 1 9 104.59 9.20 -5 -1 9 120.39 7.40 -5 1 -9 121.89 8.70 5 1 9 130.69 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6 9 24.80 5.50 9 6 9 30.10 5.00 -9 -6 9 34.20 6.20 -9 6 9 25.10 4.30 9 -6 9 28.20 4.30 9 -6 9 27.70 3.60 9 6 -9 28.20 4.10 -9 -7 9 55.59 8.30 9 7 9 47.60 6.60 -9 7 -9 54.89 6.60 9 7 9 36.70 7.00 9 -7 9 68.49 6.90 9 -7 9 48.50 5.10 9 7 -9 46.50 5.80 -9 7 9 53.19 6.60 9 8 9 35.30 5.70 -9 8 -9 29.30 4.70 9 8 9 40.40 7.10 -9 -8 9 31.40 6.40 9 8 -9 27.10 4.80 9 -8 9 28.60 5.10 -9 8 9 20.30 4.60 9 -8 9 24.10 3.60 -9 -8 -9 25.00 5.50 -9 9 -9 35.30 5.20 9 9 9 39.10 6.20 -9 -9 9 28.70 6.30 9 9 9 31.50 6.70 -9 9 9 32.40 5.70 -9 -9 -9 19.80 5.50 9 -9 9 35.60 5.70 9 9 -9 29.30 5.40 -9 10 -9 6.50 2.90 9 10 9 2.00 3.80 -9 -10 9 3.70 4.10 9 10 9 4.80 3.30 9 10 -9 3.20 3.20 9 -10 9 8.10 3.90 -9 -10 -9 6.80 4.20 9 11 9 37.80 7.20 9 11 9 14.20 4.40 -9 -11 9 24.20 6.40 -9 11 -9 30.80 5.00 -9 -11 -9 23.50 6.40 9 -11 9 18.30 5.50 9 11 -9 34.50 6.00 9 12 9 64.39 9.10 -9 12 -9 47.60 6.30 9 12 9 62.09 10.10 -9 -12 9 58.79 10.30 -9 -12 -9 43.10 8.50 9 -12 9 55.89 8.50 -9 -13 9 2.60 4.50 9 13 9 6.00 5.30 9 13 9 7.50 3.70 9 -13 9 5.30 4.30 -9 -13 -9 4.60 5.00 9 14 9 14.60 5.20 9 14 9 11.40 6.20 -9 -14 9 11.60 6.60 -9 -14 -9 13.70 6.50 9 -14 9 16.80 6.10 9 -15 -9 8.10 6.10 -9 -15 9 0.80 5.50 9 15 9 15.10 5.70 9 15 9 0.80 5.10 -9 -15 -9 13.10 6.40 9 15 -9 4.40 5.60 10 0 9 59.59 7.50 10 0 9 72.39 7.70 -10 0 9 73.59 7.60 -10 0 -9 69.69 7.00 -10 -1 9 90.09 7.80 -10 1 -9 89.09 7.60 10 1 9 68.39 8.00 10 1 9 88.39 9.30 10 -1 9 72.29 8.10 -10 -1 -9 89.99 7.50 10 -1 9 89.89 8.00 -10 -2 9 0.10 2.10 -10 2 -9 -0.80 1.60 10 2 9 4.30 2.70 -10 -2 9 0.20 0.50 10 2 9 1.50 2.00 -10 -2 -9 1.50 1.50 10 -2 9 -0.10 1.60 10 -2 9 -1.40 1.60 10 3 9 49.10 6.10 -10 -3 9 47.80 6.50 10 3 9 34.20 6.00 -10 3 -9 52.99 6.10 10 -3 9 42.80 3.70 -10 -3 -9 44.30 5.30 10 -3 9 46.20 6.20 10 -3 9 44.40 5.30 10 4 9 24.70 4.60 -10 4 -9 15.50 3.50 -10 -4 9 18.00 4.20 10 4 9 19.20 4.60 10 4 -9 19.60 2.70 -10 -4 -9 17.40 3.20 10 -4 9 19.40 2.80 10 -4 9 13.10 2.80 -10 -5 9 69.59 8.70 10 5 9 69.69 9.10 -10 5 -9 72.89 7.90 10 5 9 74.69 8.20 10 -5 9 67.29 5.90 -10 -5 -9 62.79 6.80 10 -5 9 74.59 6.00 10 5 -9 73.49 5.90 -10 -6 9 10.70 3.60 -10 6 -9 13.00 3.50 10 6 9 3.90 3.10 10 6 9 16.20 4.10 10 -6 9 10.70 2.40 10 6 -9 10.50 2.60 -10 -6 -9 12.50 3.10 10 -6 9 11.40 2.90 10 7 9 39.30 6.20 -10 7 -9 38.80 5.60 10 7 9 35.10 7.00 -10 -7 9 43.80 7.10 10 -7 9 43.80 5.70 -10 -7 -9 34.60 5.80 10 7 -9 46.20 5.40 10 -7 9 34.40 4.30 10 8 9 2.00 3.20 -10 8 -9 1.00 2.40 -10 -8 9 3.10 3.60 10 8 9 3.50 2.80 -10 -8 -9 0.00 3.10 10 -8 9 2.40 2.80 10 -8 9 2.60 1.90 10 8 -9 5.40 2.50 -10 -9 9 6.70 4.70 10 9 9 15.40 4.30 -10 9 -9 15.80 3.70 10 9 9 13.00 4.80 -10 -9 -9 9.80 4.40 10 9 -9 7.40 3.10 10 -9 9 7.00 3.50 -10 -10 9 39.50 7.80 10 10 9 41.20 7.80 10 10 9 26.50 5.70 -10 10 -9 35.30 5.70 -10 -10 -9 47.60 8.10 10 10 -9 41.50 6.50 10 -10 9 35.40 6.10 10 11 9 11.00 4.10 10 11 9 8.50 4.80 -10 11 -9 7.80 3.30 -10 -11 9 10.10 4.50 10 -11 9 1.00 3.50 -10 -11 -9 5.90 4.20 10 11 -9 1.80 2.90 10 12 9 5.10 4.20 -10 -12 9 6.10 4.60 -10 12 -9 5.40 3.10 10 12 9 11.40 4.10 10 -12 9 -2.00 3.60 10 12 -9 1.80 2.80 -10 -12 -9 9.80 5.20 10 13 9 10.90 5.50 -10 -13 9 15.70 6.00 -10 13 -9 7.00 5.60 10 13 9 8.10 4.60 -10 -13 -9 16.00 6.90 10 14 9 4.90 4.00 -10 -14 9 -7.30 4.70 10 14 9 2.40 5.20 10 14 -9 3.30 5.30 -10 -14 -9 -0.40 5.10 10 15 9 11.10 5.10 10 15 9 12.10 6.50 10 -15 -9 6.30 5.60 -10 -15 9 12.00 7.20 10 15 -9 7.30 5.90 -10 -15 -9 1.50 6.00 -11 0 -9 1.30 1.90 11 0 9 -2.30 2.00 11 0 9 1.50 1.90 -11 0 9 3.10 2.20 -11 1 -9 40.40 5.50 11 -1 -9 38.40 2.50 11 1 9 45.60 6.50 -11 -1 9 40.70 5.70 11 1 9 35.50 5.30 11 -1 -9 41.20 2.50 11 -1 9 31.80 5.10 11 -1 9 46.60 5.90 -11 -1 -9 29.30 4.70 -11 -2 9 50.89 6.70 11 2 9 51.19 7.30 -11 2 -9 69.89 7.20 11 2 9 64.69 7.20 11 -2 9 49.50 6.50 11 -2 9 46.70 6.20 -11 -2 -9 53.89 6.20 11 3 9 15.90 4.40 11 3 9 7.70 2.80 -11 -3 9 10.90 3.40 -11 3 -9 12.00 3.10 -11 -3 -9 5.70 2.40 11 -3 9 9.80 2.90 11 3 -9 10.10 1.60 11 -3 9 7.50 2.90 11 4 9 34.90 5.50 -11 -4 9 25.60 5.30 -11 4 -9 25.00 4.70 11 4 9 37.20 6.60 -11 -4 -9 36.10 5.00 11 -4 9 42.00 3.60 11 -4 9 38.40 4.70 11 4 -9 33.60 3.60 11 5 9 6.10 3.00 11 5 9 1.60 2.80 -11 5 -9 2.60 2.50 -11 -5 9 6.80 3.60 -11 -5 -9 7.50 2.40 11 5 -9 4.90 2.00 11 -5 9 9.90 2.50 11 -5 9 5.20 1.90 11 6 9 149.49 13.10 11 6 9 147.09 11.70 -11 -6 9 131.59 12.20 -11 6 -9 123.99 10.90 11 6 -9 137.99 10.10 -11 -6 -9 138.79 11.50 11 -6 9 139.59 10.10 -11 -6 -9 148.69 10.70 11 -6 9 151.48 9.90 11 7 9 3.60 3.60 11 7 9 2.50 2.70 -11 -7 9 12.90 4.60 -11 7 -9 10.30 3.30 11 7 -9 6.70 2.50 -11 -7 -9 7.00 2.50 11 -7 9 6.40 2.10 -11 -7 -9 3.40 2.90 11 -7 9 8.50 3.00 -11 -8 9 5.50 3.50 11 8 9 5.10 3.80 -11 8 -9 8.60 3.30 11 8 9 12.60 3.80 -11 -8 -9 8.20 3.50 11 -8 9 6.50 3.00 11 8 -9 8.40 3.00 11 -8 9 6.80 2.10 -11 -8 -9 7.90 2.80 -11 -9 9 24.40 6.40 11 9 9 16.10 5.70 11 9 9 24.10 5.30 -11 9 -9 23.00 4.40 -11 -9 -9 30.00 6.30 11 -9 9 26.50 5.10 11 9 -9 29.00 4.80 -11 10 -9 12.30 3.70 11 10 9 0.30 3.30 -11 -10 9 11.40 5.00 11 10 9 7.30 3.70 11 10 -9 8.60 3.70 -11 -10 -9 12.20 5.00 11 -10 9 4.60 3.60 11 11 9 8.40 5.20 11 11 9 11.90 4.30 -11 11 -9 8.30 3.70 -11 -11 9 18.20 5.60 -11 -11 -9 15.70 5.10 11 11 -9 9.70 3.90 11 12 9 62.79 10.10 11 12 9 52.09 8.50 -11 -12 9 47.70 9.40 -11 12 -9 52.29 7.00 11 12 -9 56.69 8.40 -11 -12 -9 43.10 8.70 11 13 9 11.60 6.10 -11 -13 9 11.90 5.60 -11 13 -9 4.80 3.10 11 13 9 6.90 4.80 -11 -13 -9 11.40 6.00 -11 -14 9 4.70 5.90 11 14 9 5.20 3.90 11 14 9 5.10 5.30 11 14 -9 3.80 4.90 -11 -14 -9 0.60 5.30 12 0 9 448.96 28.40 -12 0 -9 482.55 28.30 12 0 9 445.26 28.80 -12 0 9 437.66 28.10 -12 -1 9 90.49 9.20 12 1 9 97.59 10.10 12 1 9 87.39 9.20 12 -1 -9 84.69 5.20 -12 1 -9 90.19 5.40 12 -1 -9 85.29 5.10 -12 1 -9 76.29 8.20 12 -1 9 96.59 8.50 12 -1 9 94.79 9.50 -12 -1 -9 88.09 8.80 12 2 9 35.30 5.50 -12 2 -9 39.00 5.70 12 2 9 39.70 6.60 -12 -2 9 46.50 6.40 12 -2 9 46.20 5.80 12 -2 9 42.50 5.90 -12 -2 -9 21.40 4.20 12 3 9 27.50 4.80 -12 -3 9 28.50 5.10 12 3 9 23.10 5.20 -12 3 -9 17.90 4.20 12 -3 9 31.20 5.10 12 -3 9 25.00 4.20 -12 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5.20 12 9 -9 31.10 5.40 -12 -9 -9 26.70 6.00 -12 -10 9 154.98 16.70 -12 10 -9 162.18 12.70 12 10 9 176.78 13.80 12 10 9 125.79 15.10 -12 -10 -9 158.98 15.80 12 10 -9 138.09 12.20 -12 -10 -9 163.48 12.00 12 11 9 16.50 4.80 12 11 9 24.50 6.70 -12 -11 9 17.00 6.40 -12 11 -9 16.50 4.40 -12 -11 -9 23.50 6.90 12 11 -9 19.30 4.90 -12 -12 9 35.90 8.40 12 12 9 27.50 6.20 -12 12 -9 46.60 6.50 12 12 9 36.40 8.00 -12 -12 -9 36.50 8.20 12 12 -9 39.90 7.20 12 13 9 6.00 4.90 12 13 9 4.80 4.50 -12 -13 9 4.30 4.90 -12 13 -9 6.90 3.70 -12 -13 -9 5.40 4.80 12 13 -9 6.30 4.50 12 13 -9 5.50 4.70 -12 -14 9 30.20 7.90 12 14 9 27.50 8.40 12 14 9 21.80 6.30 12 14 -9 18.60 7.40 -12 -14 -9 12.20 6.40 13 0 9 1.00 2.00 -13 0 -9 0.60 2.00 13 0 9 -0.20 2.30 -13 0 -9 0.30 0.90 13 1 9 50.09 6.60 13 -1 -9 44.50 3.00 13 1 9 34.50 6.10 -13 1 -9 30.60 5.20 -13 -1 9 47.10 6.20 13 -1 9 33.40 5.50 13 -1 9 48.60 6.50 -13 -1 -9 46.60 3.90 -13 -1 -9 43.90 5.90 -13 2 -9 22.30 4.40 13 -2 -9 33.70 2.90 13 2 9 40.60 5.80 13 2 9 31.10 6.10 -13 -2 9 29.40 5.30 -13 -2 -9 28.70 4.70 13 2 -9 29.90 2.20 13 -2 9 24.10 4.50 13 -2 9 28.90 5.10 -13 -2 -9 30.80 3.80 13 3 9 2.80 3.10 13 3 9 5.70 2.60 -13 3 -9 15.30 3.80 -13 -3 9 3.70 2.70 13 -3 9 6.60 2.50 -13 -3 -9 6.50 2.30 13 3 -9 9.00 1.50 13 -3 9 8.00 3.30 -13 -3 -9 11.30 3.10 13 4 9 35.90 6.70 13 4 9 53.19 6.80 -13 4 -9 44.80 6.30 -13 -4 9 34.90 5.90 13 -4 9 40.10 5.40 13 -4 9 54.89 7.20 -13 -4 -9 49.80 5.90 13 4 -9 51.79 4.10 -13 -4 -9 44.00 6.00 -13 -5 9 4.90 3.30 13 5 9 10.40 3.60 13 5 9 7.60 4.00 -13 5 -9 4.30 3.00 -13 -5 -9 4.80 2.80 13 5 -9 9.00 2.20 -13 -5 -9 8.30 2.80 13 -5 9 9.20 2.50 -13 -6 9 60.19 8.40 -13 6 -9 73.49 8.30 13 6 9 68.89 8.20 13 6 9 41.00 7.80 13 6 -9 54.79 5.90 -13 -6 -9 48.30 7.10 13 -6 9 63.79 5.60 -13 -6 -9 67.59 7.20 13 7 9 38.70 7.50 -13 -7 9 33.00 6.60 13 7 9 41.40 6.40 -13 7 -9 33.30 5.60 -13 -7 -9 45.00 6.70 13 -7 9 43.70 4.70 -13 -7 -9 32.40 4.90 13 7 -9 33.70 4.90 -13 -8 9 3.30 3.90 13 8 9 5.60 3.10 13 8 9 4.80 4.10 -13 8 -9 5.50 3.30 -13 -8 -9 6.40 3.40 13 8 -9 7.60 2.90 -13 -8 -9 14.20 3.30 -13 -9 9 18.20 5.60 13 9 9 10.80 5.00 -13 9 -9 14.20 3.90 13 9 9 14.10 4.30 -13 -9 -9 13.60 4.60 13 9 -9 9.00 3.40 -13 -9 -9 15.10 3.70 13 10 9 29.60 7.40 -13 -10 9 30.90 7.20 13 10 9 45.70 7.60 -13 10 -9 46.10 6.60 13 10 -9 33.60 5.60 -13 -10 -9 38.70 5.60 -13 -10 -9 28.00 7.10 13 11 9 69.79 10.80 13 11 9 58.99 8.60 -13 11 -9 42.90 6.70 -13 -11 9 52.59 9.60 -13 -11 -9 79.59 10.80 13 11 -9 49.60 8.30 13 12 9 48.40 7.90 -13 12 -9 37.60 6.30 -13 -12 9 41.50 8.90 13 12 9 42.50 8.50 -13 -12 -9 24.20 7.50 -13 -13 9 -5.70 4.00 13 13 9 -1.30 4.10 -13 13 -9 -3.10 2.90 13 13 9 1.90 4.70 13 13 -9 9.30 5.10 -13 -13 -9 10.70 6.00 -13 -14 9 8.40 6.90 13 14 9 19.60 7.70 13 14 9 22.10 6.00 13 14 -9 14.70 7.30 -13 -14 -9 2.80 6.00 -14 0 -9 110.99 8.80 14 0 9 83.79 9.60 14 0 9 76.19 9.00 -14 -1 9 187.58 13.30 14 1 9 175.48 13.40 14 1 9 196.68 14.60 -14 1 -9 154.58 12.90 -14 -1 -9 158.08 12.80 14 -1 9 180.98 13.60 14 -1 9 177.88 13.50 -14 2 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0 -10 2258.97 128.79 8 0 10 2285.17 129.39 -8 0 10 2192.48 129.39 -8 -1 10 52.79 6.50 8 -1 -10 51.49 3.30 8 1 10 44.00 5.90 -8 1 -10 55.99 6.20 8 1 10 55.69 7.00 -8 -1 -10 56.99 6.00 8 -1 10 56.19 6.40 8 -1 10 53.99 6.40 8 2 10 62.99 7.00 8 2 10 62.69 7.50 -8 -2 10 62.49 3.80 -8 -2 10 58.49 7.00 -8 2 -10 50.19 5.90 8 -2 10 50.09 6.00 -8 -2 -10 67.89 6.70 -8 2 10 64.39 4.40 8 -2 10 56.39 6.70 8 3 10 211.58 15.30 -8 -3 10 201.48 14.80 -8 3 -10 210.28 13.90 8 3 10 195.28 14.20 8 -3 10 195.18 14.30 8 -3 10 203.18 13.60 8 -3 10 198.58 12.80 -8 -3 -10 204.88 13.60 -8 3 10 203.08 12.50 -8 -4 10 561.54 35.80 8 4 10 579.34 35.30 8 4 10 560.24 36.20 -8 4 -10 638.34 35.10 8 -4 10 544.95 33.80 8 -4 10 629.34 34.20 -8 4 10 579.04 33.80 -8 5 -10 1.30 1.80 -8 -5 10 2.90 3.00 8 5 10 3.30 3.10 8 5 10 5.10 2.50 8 -5 10 3.10 1.80 -8 5 10 3.70 2.00 8 5 -10 3.10 0.90 8 -5 10 6.40 2.20 -8 5 10 3.90 1.40 -8 6 -10 345.27 21.70 8 6 10 338.77 22.40 -8 -6 10 324.47 23.00 8 6 10 341.17 23.50 -8 6 10 338.67 21.40 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10 23.80 6.10 -9 -13 10 22.90 6.70 -9 -13 -10 21.40 7.20 9 -13 10 15.00 5.30 9 14 10 9.70 4.60 9 14 10 11.30 5.50 -9 -14 10 23.00 7.50 -9 -14 -10 18.60 6.70 9 15 10 15.20 6.40 -9 -15 10 22.30 7.80 9 -15 -10 10.60 5.80 9 15 10 19.20 6.10 -9 -15 -10 21.80 8.00 9 15 -10 24.50 7.40 -10 0 -10 11.40 2.90 10 0 10 11.30 3.20 10 0 10 8.30 3.00 -10 0 10 6.60 2.80 -10 1 -10 397.16 25.10 -10 -1 10 386.46 25.40 10 1 10 428.06 26.50 10 1 10 380.46 25.50 10 -1 10 445.66 25.80 10 -1 10 416.56 25.70 -10 -1 -10 384.16 24.90 10 2 10 252.77 17.60 -10 2 -10 229.38 16.20 -10 -2 10 227.28 16.50 10 2 10 259.97 16.90 -10 -2 -10 235.18 15.90 10 -2 10 254.97 16.40 10 -2 10 225.58 16.50 -10 -3 10 64.79 7.70 10 3 10 73.59 7.80 -10 3 -10 68.39 7.50 10 3 10 69.39 8.80 10 -3 10 54.49 7.20 -10 -3 -10 77.69 7.40 10 -3 10 58.59 6.50 -10 -4 10 41.40 6.20 10 4 10 36.20 5.60 -10 4 -10 31.40 5.00 10 4 10 45.20 6.90 -10 -4 -10 32.80 4.70 10 -4 10 48.60 4.60 10 -4 10 31.00 4.40 10 5 10 707.53 41.20 -10 -5 10 637.84 40.10 -10 5 -10 656.83 39.00 10 5 10 657.03 39.50 10 -5 10 629.14 37.70 -10 -5 -10 659.83 38.40 10 -5 10 636.24 37.50 -10 6 -10 45.80 6.40 10 6 10 44.20 6.50 -10 -6 10 50.89 7.60 10 6 10 44.10 7.40 10 -6 10 39.10 5.20 10 -6 10 49.20 5.20 -10 -7 10 1.10 2.80 -10 7 -10 2.70 2.60 10 7 10 3.00 2.80 10 7 10 0.00 2.60 10 -7 10 3.60 2.40 10 -7 10 -1.00 1.40 -10 8 -10 169.78 12.40 10 8 10 167.28 13.10 -10 -8 10 161.38 13.90 10 8 10 158.08 14.50 10 -8 10 151.88 10.70 10 -8 10 155.68 12.20 -10 -8 -10 146.19 13.20 10 9 10 111.99 13.10 10 9 10 97.49 10.80 -10 9 -10 96.09 9.80 -10 -9 10 104.29 12.20 10 -9 10 101.49 10.30 -10 -9 -10 92.89 11.30 10 10 10 17.30 5.50 10 10 10 20.30 5.10 -10 -10 10 8.60 4.80 -10 10 -10 15.40 3.90 -10 -10 -10 17.80 5.50 10 -10 10 11.30 4.30 10 11 10 69.19 9.30 10 11 10 49.00 8.90 -10 11 -10 63.19 7.60 -10 -11 10 44.10 8.80 -10 -11 -10 68.09 10.20 10 -11 10 52.39 8.30 10 12 10 73.79 9.70 -10 -12 10 85.99 12.20 -10 12 -10 60.39 7.60 10 12 10 70.99 10.90 -10 -12 -10 73.59 10.90 10 13 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10 104.79 9.50 11 -6 10 107.79 7.80 11 -6 10 94.59 7.80 -11 -6 -10 97.79 8.50 11 6 -10 103.69 8.00 11 7 10 17.70 4.50 11 7 10 11.80 4.60 -11 7 -10 14.60 3.90 -11 -7 10 14.00 4.80 -11 -7 -10 15.80 3.60 11 -7 10 13.90 2.80 -11 -7 -10 11.30 4.20 11 7 -10 15.70 3.40 11 -7 10 20.40 3.80 -11 -8 10 31.60 6.90 11 8 10 31.20 5.70 -11 8 -10 37.40 5.60 11 8 10 30.10 6.70 11 -8 10 29.30 5.10 11 8 -10 34.50 5.30 11 -8 10 35.20 4.40 -11 -8 -10 41.00 6.90 11 9 10 92.19 10.40 -11 -9 10 104.39 12.40 -11 9 -10 87.79 9.30 11 9 10 83.09 11.40 -11 -9 -10 75.49 10.30 11 9 -10 99.19 8.90 11 -9 10 96.69 10.00 11 10 10 58.99 9.70 -11 10 -10 48.60 7.00 11 10 10 65.19 8.60 -11 -10 10 40.20 8.80 11 10 -10 61.19 7.90 -11 -10 -10 71.99 9.80 -11 11 -10 80.59 9.10 11 11 10 89.29 10.70 -11 -11 10 86.09 11.70 11 11 10 84.79 12.00 -11 -11 -10 82.89 11.30 -11 12 -10 113.39 10.00 -11 -12 10 104.69 14.20 11 12 10 122.99 14.40 11 12 10 115.99 12.70 -11 -12 -10 95.49 12.60 -11 -13 10 14.20 6.80 11 13 10 18.90 6.00 11 13 10 2.10 4.70 -11 -13 -10 19.80 7.00 11 14 10 6.10 4.20 11 14 10 13.20 6.60 -11 -14 10 1.70 5.00 -11 -14 -10 8.60 6.60 -12 0 -10 468.75 28.40 12 0 10 439.96 28.80 12 0 10 463.55 29.30 -12 -1 10 100.09 8.80 12 1 10 88.49 9.60 -12 1 -10 108.59 8.90 12 1 10 83.99 10.00 -12 -1 -10 103.89 8.60 12 -1 10 103.49 9.00 12 -1 10 95.89 8.90 -12 2 -10 154.38 12.10 12 2 10 144.09 13.00 12 2 10 163.38 12.40 -12 -2 10 150.08 12.10 12 -2 10 169.28 12.30 12 -2 10 158.18 12.40 -12 -2 -10 162.28 11.80 12 3 10 163.18 14.40 -12 3 -10 174.68 13.50 12 3 10 176.78 13.50 -12 -3 10 186.78 14.00 12 -3 10 193.08 13.20 -12 -3 -10 169.78 12.90 12 -3 10 204.98 14.30 -12 4 -10 301.17 20.00 -12 -4 10 303.27 20.80 12 4 10 267.47 21.00 12 4 10 322.57 20.50 12 -4 10 303.57 19.20 12 -4 10 298.17 17.50 12 -4 10 286.87 20.30 -12 -4 -10 295.07 19.40 12 5 10 92.09 11.20 -12 5 -10 96.19 9.90 -12 -5 10 101.79 11.10 12 5 10 97.19 10.10 12 -5 10 101.39 7.50 12 5 -10 93.79 7.10 12 -5 10 86.49 7.60 -12 -5 -10 99.69 8.30 -12 -6 10 197.48 16.50 12 6 10 240.58 16.50 12 6 10 225.28 17.70 -12 6 -10 210.08 15.80 12 -6 10 207.58 14.00 12 6 -10 213.78 14.20 -12 -6 -10 229.28 16.10 -12 -6 -10 228.88 15.30 12 7 10 183.08 15.80 -12 -7 10 192.08 15.50 12 7 10 171.48 14.10 -12 7 -10 176.28 13.90 12 7 -10 188.28 12.90 -12 -7 -10 185.48 14.30 -12 -7 -10 154.68 12.90 12 -7 10 209.78 12.50 12 8 10 27.90 6.50 -12 -8 10 26.60 5.90 -12 8 -10 41.90 6.00 12 8 10 25.40 5.20 12 8 -10 30.70 4.90 -12 -8 -10 38.70 6.80 -12 -8 -10 22.90 4.60 -12 -9 10 43.70 8.10 12 9 10 64.69 8.50 12 9 10 52.59 9.00 -12 9 -10 59.29 7.50 -12 -9 -10 61.19 8.80 12 9 -10 53.99 7.00 -12 -9 -10 60.79 7.20 12 10 10 140.09 15.10 12 10 10 143.09 12.30 -12 -10 10 134.99 14.50 -12 10 -10 91.99 10.80 -12 -10 -10 120.89 10.40 -12 -10 -10 129.89 13.90 12 10 -10 129.99 11.10 -12 -11 10 64.29 10.70 -12 11 -10 63.09 8.20 12 11 10 70.19 9.30 12 11 10 74.49 10.90 12 11 -10 62.29 8.40 -12 -11 -10 69.89 10.20 -12 -11 -10 70.29 8.90 -12 -12 10 24.10 7.30 12 12 10 16.10 5.20 12 12 10 33.50 8.20 -12 12 -10 34.60 5.80 -12 -12 -10 18.30 6.60 12 13 10 49.80 9.90 -12 13 -10 46.00 6.70 12 13 10 45.30 8.10 -12 -13 10 22.20 8.00 -12 -13 -10 28.50 7.50 -12 -14 10 44.10 9.70 12 14 10 42.10 9.30 12 14 10 50.89 9.00 12 14 -10 38.80 9.20 -12 -14 -10 47.30 10.20 13 0 10 2.60 2.30 13 0 10 -3.00 1.60 -13 0 -10 3.10 2.20 -13 -1 10 37.10 5.40 -13 1 -10 34.70 5.40 13 1 10 22.50 5.10 13 1 10 33.50 5.40 -13 -1 -10 28.60 5.10 13 -1 10 37.80 5.90 13 -1 10 36.70 5.80 13 -2 -10 24.20 2.40 13 2 10 28.20 5.20 -13 -2 10 23.90 4.80 13 2 10 26.40 5.50 -13 2 -10 28.20 5.10 13 -2 10 23.10 4.80 13 -2 10 20.60 4.20 -13 -2 -10 29.90 4.80 13 3 10 4.60 2.50 -13 3 -10 5.60 2.90 13 3 10 -3.00 2.10 -13 -3 10 2.10 2.50 -13 -3 -10 0.10 1.70 -13 -3 -10 4.60 2.60 13 -3 10 1.20 2.10 13 -3 10 3.10 2.60 13 4 10 66.29 9.10 -13 -4 10 59.29 8.20 13 4 10 53.99 7.70 -13 4 -10 86.39 8.90 -13 -4 -10 78.19 8.20 -13 -4 -10 79.49 7.80 13 -4 10 66.09 8.50 13 -4 10 77.19 7.00 13 5 10 11.30 3.90 13 5 10 13.80 4.80 -13 5 -10 25.90 5.00 -13 -5 10 14.60 4.40 -13 -5 -10 15.80 3.70 13 -5 10 15.00 3.20 -13 -5 -10 20.20 4.10 13 6 10 17.00 4.30 -13 -6 10 23.20 5.50 13 6 10 8.20 4.60 -13 6 -10 9.40 3.40 13 -6 10 13.20 2.90 -13 -6 -10 12.00 3.80 -13 -6 -10 26.40 4.50 13 7 10 73.49 9.10 -13 -7 10 94.39 10.90 13 7 10 81.29 11.00 -13 7 -10 100.29 9.90 13 -7 10 61.49 6.20 -13 -7 -10 79.09 9.30 -13 -7 -10 77.29 8.20 13 8 10 -2.00 2.20 -13 -8 10 4.30 3.60 -13 8 -10 5.80 3.00 13 8 10 8.30 4.40 -13 -8 -10 13.00 4.30 -13 -8 -10 10.50 3.10 -13 -9 10 6.40 4.90 13 9 10 5.40 3.50 13 9 10 5.40 4.00 -13 9 -10 6.60 3.50 -13 -9 -10 1.40 3.20 -13 -9 -10 8.00 3.00 13 10 10 5.40 4.20 -13 10 -10 -0.50 2.80 13 10 10 0.00 3.00 -13 -10 10 -0.20 3.50 -13 -10 -10 -0.40 3.10 -13 -10 -10 -0.40 2.40 13 11 10 99.29 13.00 13 11 10 86.29 10.80 -13 11 -10 89.19 9.80 -13 -11 10 94.29 12.80 -13 -11 -10 84.89 11.60 -13 -12 10 11.70 6.00 -13 12 -10 14.40 4.40 13 12 10 17.50 6.50 13 12 10 14.50 5.00 -13 -12 -10 7.80 5.40 -13 -13 10 -6.60 4.00 13 13 10 5.90 5.80 13 13 10 23.40 5.90 -13 13 -10 16.40 4.60 -13 -13 -10 7.00 5.80 13 14 10 20.10 6.20 14 0 10 496.35 33.00 14 0 10 588.94 33.10 -14 0 -10 480.45 32.00 14 1 10 35.40 6.00 14 1 10 50.39 7.40 -14 1 -10 64.79 7.50 -14 -1 10 39.50 6.00 14 -1 10 52.29 6.90 -14 -1 -10 54.89 7.00 14 -1 10 52.79 7.20 14 2 10 194.98 13.70 14 2 10 155.08 13.90 -14 -2 10 165.78 13.10 -14 2 -10 156.08 12.90 -14 -2 -10 176.68 11.50 14 -2 10 183.08 13.30 14 -2 10 162.18 13.30 -14 -2 -10 160.38 12.70 -14 3 -10 53.99 7.30 14 3 10 67.59 9.10 -14 -3 10 58.49 7.90 14 3 10 66.29 8.10 14 -3 10 66.49 8.30 -14 -3 -10 70.49 6.80 14 -3 10 80.29 8.00 -14 -3 -10 62.59 7.40 -14 -4 10 303.87 20.70 14 4 10 302.87 22.00 -14 4 -10 286.37 20.10 14 4 10 244.18 19.70 -14 -4 -10 299.77 19.00 -14 -4 -10 321.87 19.90 14 -4 10 307.97 19.30 14 -4 10 283.17 20.40 14 5 10 0.40 3.00 -14 -5 10 4.10 3.00 14 5 10 -1.30 2.40 -14 5 -10 -1.80 2.40 -14 -5 -10 1.10 2.20 14 -5 10 1.50 2.00 14 -5 10 -2.30 2.70 -14 -5 -10 -0.10 2.40 14 6 10 154.48 13.10 -14 6 -10 189.58 13.70 -14 -6 10 169.78 14.20 14 6 10 157.08 14.60 -14 -6 -10 169.48 12.50 -14 -6 -10 151.48 12.50 14 -6 10 161.08 11.40 14 7 10 34.50 7.40 -14 7 -10 32.70 5.90 14 7 10 32.70 6.20 -14 -7 10 49.99 8.00 -14 -7 -10 44.30 6.20 -14 -7 -10 38.90 6.50 14 8 10 111.89 11.90 -14 8 -10 103.89 11.00 14 8 10 109.69 13.30 -14 -8 10 109.59 12.90 -14 -8 -10 125.59 12.40 -14 -8 -10 111.99 9.50 -14 -9 10 10.80 4.80 -14 9 -10 2.40 3.00 14 9 10 0.90 3.00 14 9 10 1.10 3.90 -14 -9 -10 1.00 3.40 -14 -9 -10 5.60 2.90 14 10 10 159.18 13.00 -14 10 -10 111.39 12.30 -14 -10 10 139.59 15.80 14 10 10 117.19 15.00 -14 -10 -10 127.69 11.00 -14 -10 -10 148.09 14.80 -14 11 -10 18.70 4.90 -14 -11 10 5.00 4.40 14 11 10 9.40 4.50 14 11 10 14.50 5.70 -14 -11 -10 1.90 3.90 14 12 10 48.20 9.60 -14 12 -10 50.69 7.40 -14 -12 10 48.70 9.80 14 12 10 48.60 8.50 -14 -12 -10 65.59 10.50 -14 -13 10 53.39 10.00 14 13 10 25.60 7.80 14 13 10 37.80 7.40 -14 13 -10 47.60 7.10 -14 -13 -10 32.50 8.00 14 13 -10 38.20 9.00 15 0 10 -1.10 2.20 15 0 10 -1.00 2.40 -15 0 -10 1.50 2.20 15 1 10 14.80 4.50 -15 -1 10 19.30 4.30 -15 1 -10 25.90 5.20 15 1 10 15.10 4.40 15 -1 10 22.90 4.80 -15 -1 -10 22.40 4.90 15 -1 10 17.60 4.40 15 2 10 35.40 6.00 15 2 10 28.50 6.20 -15 -2 10 21.60 5.00 -15 2 -10 30.90 5.70 -15 -2 -10 43.90 6.10 15 -2 10 36.50 5.80 15 -2 10 36.50 6.10 -15 -3 10 1.30 2.90 15 3 10 2.80 3.70 -15 3 -10 -0.70 2.10 15 3 10 2.70 2.50 15 -3 10 4.90 2.70 15 -3 10 1.40 2.20 -15 -3 -10 7.60 3.20 -15 -4 10 39.30 6.60 -15 4 -10 33.20 5.90 15 4 10 31.60 5.80 15 4 10 26.80 6.20 15 -4 10 36.30 6.30 15 -4 10 25.90 4.60 -15 -4 -10 32.60 5.50 -15 -4 -10 28.90 5.40 15 5 10 10.10 4.70 -15 5 -10 12.30 4.20 15 5 10 9.70 3.80 -15 -5 10 9.20 3.90 -15 -5 -10 14.50 3.80 15 -5 10 12.40 3.10 -15 -5 -10 9.00 3.30 15 -5 10 14.10 4.50 -15 -6 10 73.79 10.00 -15 6 -10 81.09 9.70 15 6 10 79.69 11.10 15 6 10 79.99 9.60 -15 -6 -10 90.19 9.40 15 -6 10 94.59 7.40 -15 -6 -10 82.39 9.30 15 7 10 15.60 4.60 15 7 10 7.80 4.70 -15 -7 10 20.40 5.30 -15 7 -10 15.40 4.30 -15 -7 -10 28.00 5.60 -15 -7 -10 15.80 3.90 15 8 10 6.90 4.80 -15 8 -10 5.60 3.50 -15 -8 10 4.70 4.30 15 8 10 2.50 3.20 -15 -8 -10 7.20 3.20 -15 -8 -10 6.30 4.10 15 9 10 0.50 3.80 15 9 10 -0.60 2.90 -15 9 -10 8.50 3.70 -15 -9 10 0.30 3.70 -15 -9 -10 9.10 3.50 -15 -9 -10 0.20 3.50 -15 10 -10 1.20 3.30 -15 -10 10 11.40 4.90 15 10 10 9.50 4.30 15 10 10 6.10 4.50 -15 -10 -10 9.20 5.40 -15 -10 -10 8.00 4.80 -15 11 -10 7.10 3.70 15 11 10 5.20 4.70 -15 -11 10 7.30 5.70 15 11 10 1.50 3.50 -15 -11 -10 3.10 4.70 15 12 10 46.40 9.40 15 12 10 22.20 6.20 -15 12 -10 35.40 6.30 -15 -12 10 26.00 7.80 -15 -12 -10 42.00 8.70 15 12 -10 45.00 9.80 -15 13 -10 9.20 3.90 -15 -13 10 5.30 5.40 15 13 10 -1.40 4.60 15 13 10 2.40 3.90 15 13 -10 1.80 4.60 -15 -13 -10 8.30 5.60 -16 0 -10 110.79 10.50 16 0 10 135.89 12.00 16 0 10 132.49 11.20 16 1 10 426.06 26.70 -16 1 -10 462.75 27.00 -16 -1 10 388.36 25.90 16 1 10 378.26 27.10 16 -1 10 401.86 26.70 -16 -1 -10 386.96 26.00 16 -1 10 387.56 26.40 -16 -2 10 321.97 20.70 16 2 10 321.37 22.30 16 2 10 312.67 20.90 -16 2 -10 285.87 20.40 16 -2 10 264.37 20.00 -16 -2 -10 294.97 20.30 16 -2 10 291.27 20.80 -16 -3 10 90.69 10.10 16 3 10 89.59 9.80 -16 3 -10 77.69 9.30 16 3 10 101.59 11.80 16 -3 10 68.69 9.10 -16 -3 -10 96.89 9.60 16 -3 10 98.49 8.80 16 4 10 26.10 6.30 -16 -4 10 31.10 6.20 -16 4 -10 15.20 4.20 16 4 10 17.70 4.70 16 -4 10 24.90 5.50 -16 -4 -10 20.10 4.40 16 -4 10 22.70 4.50 16 5 10 330.17 24.30 -16 5 -10 301.47 22.10 16 5 10 335.37 22.50 -16 -5 10 326.47 22.90 16 -5 10 342.57 23.00 -16 -5 -10 330.97 21.70 16 -5 10 311.87 20.70 16 6 10 8.00 3.60 -16 -6 10 9.30 4.30 -16 6 -10 1.20 2.60 16 6 10 14.90 5.30 16 -6 10 17.40 5.10 -16 -6 -10 9.10 3.40 -16 7 -10 55.79 7.70 16 7 10 56.89 8.30 -16 -7 10 55.29 8.80 16 7 10 33.80 8.00 -16 -7 -10 44.30 6.50 -16 -7 -10 42.00 7.00 -16 8 -10 85.19 9.90 16 8 10 64.49 10.50 16 8 10 77.89 9.90 -16 -8 10 72.09 10.80 -16 -8 -10 75.09 8.80 -16 -8 -10 90.19 10.50 -16 9 -10 89.99 10.20 16 9 10 114.89 13.90 -16 -9 10 106.09 13.00 16 9 10 95.09 11.20 -16 -9 -10 97.69 11.50 -16 -9 -10 95.29 10.00 16 10 10 17.60 6.30 -16 10 -10 19.00 5.20 -16 -10 10 12.00 4.70 16 10 10 30.90 6.40 -16 -10 -10 13.80 5.20 16 11 10 104.29 12.20 16 11 10 107.89 14.30 -16 -11 10 105.09 13.60 -16 11 -10 96.49 11.10 -16 -11 -10 95.59 12.30 16 12 10 60.59 9.50 16 12 10 53.29 10.70 -16 -12 10 40.80 9.40 -16 12 -10 62.69 8.20 -16 -12 -10 44.10 8.40 16 12 -10 53.79 10.40 17 0 10 -1.10 2.40 17 0 10 -0.60 2.80 -17 0 -10 2.10 2.50 -17 1 -10 22.90 4.80 17 1 10 25.30 5.40 17 1 10 19.70 5.00 -17 -1 10 18.20 4.50 17 -1 10 22.60 5.20 17 -1 10 28.80 5.50 -17 -1 -10 22.10 5.00 17 2 10 24.90 6.20 -17 2 -10 21.90 4.70 -17 -2 10 23.90 5.10 17 2 10 19.00 4.90 17 -2 10 27.50 5.40 17 -2 10 15.70 4.60 -17 -2 -10 15.80 4.20 17 3 10 8.40 4.40 17 3 10 18.40 4.40 -17 -3 10 7.60 3.60 -17 3 -10 15.30 4.60 17 -3 10 5.90 3.60 -17 -3 -10 9.40 3.50 17 -3 10 12.90 4.20 17 4 10 24.80 5.70 17 4 10 18.80 5.60 -17 4 -10 19.40 4.80 -17 -4 10 26.70 5.70 17 -4 10 22.20 4.50 17 -4 10 34.00 6.40 -17 -4 -10 20.60 4.70 17 5 10 -2.20 2.40 -17 5 -10 0.60 2.80 -17 -5 10 7.60 3.80 17 5 10 5.00 4.50 17 -5 10 2.90 2.30 17 -5 10 2.20 3.30 -17 -5 -10 3.20 2.80 17 6 10 82.19 10.20 17 6 10 84.79 12.10 -17 -6 10 99.69 11.50 -17 6 -10 87.99 10.40 17 -6 10 118.79 12.50 -17 -6 -10 107.09 10.70 17 7 10 10.60 4.10 -17 7 -10 14.50 4.40 -17 -7 10 7.90 4.80 17 7 10 10.30 4.80 -17 -7 -10 13.80 3.70 17 8 10 0.00 4.30 17 8 10 1.40 3.40 -17 -8 10 4.50 4.00 -17 8 -10 -1.80 2.80 -17 -8 -10 3.60 2.90 -17 -9 10 8.70 5.50 17 9 10 12.80 4.90 -17 9 -10 14.00 4.30 17 9 10 15.90 5.70 -17 -9 -10 10.70 3.50 -17 -10 10 13.40 6.20 17 10 10 6.90 5.10 17 10 10 17.50 5.30 -17 10 -10 10.40 4.60 -17 -11 10 18.70 6.30 17 11 10 29.50 6.60 17 11 10 11.70 6.50 -17 11 -10 12.80 4.80 17 11 -10 18.60 6.50 -17 -12 10 32.90 8.20 17 12 10 36.20 7.50 -17 12 -10 31.00 6.40 17 12 10 23.30 7.90 -17 -12 -10 39.00 9.80 17 12 -10 37.00 10.10 18 0 10 476.65 29.70 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12 14 164.28 14.50 6 12 14 116.89 13.90 6 -12 14 175.58 15.00 -6 12 14 162.48 14.20 6 13 14 16.80 6.10 6 13 14 15.10 5.30 -6 -13 14 9.70 6.50 -6 13 14 7.90 4.70 6 -13 14 21.10 6.30 -6 -13 -14 16.40 6.90 -6 -14 14 0.50 5.20 6 14 14 7.90 4.40 6 -14 14 10.90 5.90 -6 -14 -14 4.10 5.80 -6 14 14 7.80 5.00 7 0 14 -0.40 1.90 7 0 14 -1.30 1.80 -7 0 14 0.30 0.80 -7 0 -14 -0.40 1.40 -7 1 -14 99.49 8.30 7 1 14 92.39 9.90 -7 -1 14 111.69 9.50 -7 -1 14 98.29 6.20 7 1 14 103.99 8.80 -7 1 14 97.99 6.40 -7 1 14 100.89 7.90 -7 -1 -14 95.19 8.00 7 -1 14 97.09 8.60 7 -1 14 87.19 8.50 -7 -2 14 59.99 7.90 -7 -2 14 52.79 3.80 7 2 14 38.10 6.30 7 2 14 46.90 6.40 -7 2 -14 47.30 5.70 7 -2 14 46.30 5.90 -7 2 14 47.10 3.90 -7 2 14 48.30 5.20 7 -2 14 45.90 6.40 -7 -3 14 1.80 2.50 -7 3 -14 4.60 2.20 7 3 14 3.70 2.50 7 3 14 5.40 2.30 7 -3 14 4.90 2.30 -7 3 14 4.50 2.00 7 -3 14 5.30 2.10 -7 3 14 3.20 1.50 7 -3 14 2.50 2.30 -7 4 -14 5.50 2.50 -7 -4 14 3.80 3.30 7 4 14 3.90 2.70 7 4 14 3.50 2.50 7 -4 14 3.50 2.80 -7 4 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33.80 7.80 7 12 14 53.29 9.00 7 12 14 38.50 7.30 -7 12 14 36.80 7.40 7 -12 14 49.30 8.60 7 13 14 -1.20 3.50 -7 -13 14 0.10 3.80 7 13 14 1.70 3.80 -7 13 14 2.70 3.60 7 -13 14 1.30 4.10 -7 -13 -14 4.00 5.00 7 14 14 7.10 4.30 -7 -14 14 9.20 5.90 -7 -14 -14 7.40 5.60 7 -14 14 9.10 5.50 -7 14 14 10.70 4.60 -8 0 -14 312.47 20.00 -8 0 14 312.77 17.30 8 0 14 319.97 21.00 8 0 14 301.07 20.70 -8 1 -14 19.90 4.00 8 1 14 17.70 4.10 -8 -1 14 18.20 4.50 -8 -1 14 17.00 1.40 8 1 14 20.40 4.60 -8 -1 14 17.20 1.50 8 -1 14 21.40 4.20 -8 -1 -14 16.10 3.30 8 -1 14 20.10 4.00 -8 1 14 18.80 1.90 -8 -2 14 514.05 28.30 -8 2 -14 481.85 30.70 8 2 14 560.94 32.50 -8 -2 14 481.45 31.90 8 2 14 524.35 31.60 8 -2 14 491.15 31.50 8 -2 14 499.45 31.00 -8 -2 -14 535.95 30.90 -8 2 14 490.15 28.70 -8 -3 14 334.07 18.80 -8 -3 14 322.77 22.20 8 3 14 364.36 21.80 8 3 14 327.17 22.30 -8 3 -14 316.57 20.90 8 -3 14 312.77 20.20 8 -3 14 305.27 21.50 -8 3 14 333.17 19.20 8 -3 14 278.97 20.40 -8 3 14 334.67 20.00 -8 4 -14 124.39 10.30 8 4 14 162.28 12.40 8 4 14 135.79 11.00 -8 -4 14 138.79 11.90 -8 4 14 129.59 9.30 -8 4 14 134.29 9.20 8 -4 14 123.99 9.90 8 -4 14 124.09 9.90 8 -4 14 128.79 11.20 8 5 14 97.59 8.60 8 5 14 74.69 9.60 -8 5 -14 97.09 8.00 -8 -5 14 85.39 10.20 -8 5 14 72.49 6.20 -8 5 14 79.39 6.70 8 -5 14 63.69 7.20 8 -5 14 83.79 7.40 8 6 14 40.10 6.50 -8 -6 14 51.59 8.20 8 6 14 40.90 7.20 -8 6 -14 50.09 6.30 8 -6 14 55.09 6.70 -8 6 14 55.39 6.30 -8 6 14 48.30 5.00 8 -6 14 63.29 6.60 -8 7 -14 459.25 28.90 8 7 14 427.16 29.70 8 7 14 500.35 31.40 -8 -7 14 417.96 30.70 8 -7 14 489.95 28.40 -8 7 14 470.15 28.90 8 -7 14 491.75 29.50 8 8 14 164.88 13.50 8 8 14 168.58 14.70 -8 -8 14 162.48 14.70 -8 8 -14 176.48 12.70 8 -8 14 169.68 13.30 -8 8 14 151.48 12.50 8 -8 14 163.08 11.90 -8 -9 14 5.90 4.70 8 9 14 5.70 3.90 -8 9 -14 0.80 2.40 8 9 14 5.40 3.30 -8 9 14 5.20 3.20 8 -9 14 9.20 4.00 -8 -10 14 24.10 6.20 8 10 14 17.00 4.80 8 10 14 28.40 6.40 -8 10 -14 13.90 3.90 -8 10 14 26.60 5.80 8 -10 14 36.30 6.40 -8 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4.60 -9 -4 14 9.70 3.80 -9 4 14 18.30 2.90 9 -4 14 24.80 4.10 9 -4 14 16.10 4.20 9 -4 14 20.50 3.60 -9 -5 14 22.30 5.40 -9 5 -14 18.80 4.20 9 5 14 25.00 5.10 9 5 14 17.50 4.90 -9 5 14 30.90 4.20 9 -5 14 28.70 4.50 9 -5 14 26.20 4.30 -9 5 14 30.40 3.80 9 6 14 50.89 7.10 9 6 14 46.20 7.60 -9 -6 14 46.40 7.80 -9 6 -14 48.90 6.70 -9 6 14 53.09 6.10 9 -6 14 55.09 6.00 9 -6 14 59.29 6.80 -9 6 14 51.89 5.30 9 7 14 62.39 8.50 9 7 14 63.49 9.70 -9 -7 14 103.79 11.60 -9 7 -14 74.69 8.40 9 -7 14 82.49 8.60 -9 7 14 83.29 8.40 9 -7 14 82.19 7.20 9 8 14 2.10 2.80 9 8 14 7.30 3.90 -9 -8 14 8.50 4.60 -9 8 -14 5.30 3.00 9 -8 14 6.60 2.60 9 -8 14 12.10 3.80 -9 8 14 5.60 3.00 9 9 14 12.20 4.20 -9 9 -14 6.00 3.10 -9 -9 14 8.60 4.80 9 9 14 2.70 3.90 -9 9 14 4.60 3.30 9 -9 14 14.70 4.50 9 -9 14 8.50 3.10 -9 -10 14 -3.70 3.40 -9 10 -14 1.70 2.70 9 10 14 3.90 3.30 9 10 14 1.20 3.80 -9 10 14 5.80 3.30 9 -10 14 4.80 3.50 -9 -11 14 108.69 14.30 9 11 14 122.19 13.10 -9 11 -14 130.39 10.80 9 11 14 131.69 14.60 9 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14 32.10 4.00 10 -4 14 35.70 5.10 10 5 14 16.90 5.00 10 5 14 6.60 2.90 -10 5 -14 11.70 3.70 -10 -5 14 15.00 4.70 10 -5 14 13.00 3.10 10 -5 14 19.30 3.70 -10 5 14 12.60 2.80 10 6 14 30.90 6.50 -10 6 -14 29.50 5.20 -10 -6 14 34.00 6.80 10 6 14 33.50 5.90 10 -6 14 35.60 5.20 -10 6 14 24.00 4.20 10 -6 14 25.80 4.20 -10 7 -14 63.79 7.70 10 7 14 68.99 9.80 -10 -7 14 62.69 9.20 10 7 14 57.79 8.20 -10 7 14 57.39 7.00 10 -7 14 65.99 6.90 10 -7 14 70.69 7.90 -10 -8 14 349.77 24.90 10 8 14 303.97 23.10 10 8 14 359.56 25.20 -10 8 -14 337.17 22.60 10 -8 14 333.37 21.40 -10 8 14 336.77 22.30 10 -8 14 366.46 22.70 10 9 14 9.10 3.90 10 9 14 11.70 4.90 -10 9 -14 9.70 3.60 -10 -9 14 5.00 4.30 10 -9 14 10.60 3.10 -10 9 14 7.40 3.40 10 -9 14 12.10 6.70 -10 10 -14 -2.80 2.50 10 10 14 6.10 3.50 -10 -10 14 2.40 4.30 10 10 14 4.40 4.00 -10 10 14 2.60 3.30 -10 11 -14 5.90 3.20 -10 -11 14 2.80 5.00 10 11 14 0.50 3.10 10 11 14 4.50 4.50 -10 -11 -14 2.30 4.20 -10 11 14 2.70 3.40 10 12 14 149.29 15.80 -10 -12 14 175.08 18.10 10 12 14 172.38 17.90 -10 -12 -14 161.38 17.00 -10 12 14 152.58 14.20 -10 -13 14 24.80 7.30 10 13 14 27.90 6.50 10 13 14 23.20 6.80 -10 -13 -14 32.40 8.40 10 14 14 16.80 5.90 -11 0 -14 -0.50 1.70 11 0 14 0.50 2.20 11 0 14 -0.70 2.20 -11 1 -14 15.60 3.60 11 1 14 9.00 3.30 11 1 14 19.40 4.90 -11 -1 14 12.70 4.30 11 -1 14 13.80 3.80 11 -1 14 10.00 3.30 -11 -1 -14 12.00 3.30 11 2 14 90.09 10.30 -11 -2 14 87.99 9.90 11 2 14 81.99 9.50 -11 2 -14 101.19 8.60 -11 -2 -14 77.09 8.40 11 -2 14 76.09 9.20 11 -2 14 86.39 9.20 -11 3 -14 9.00 3.00 11 3 14 6.20 3.40 11 3 14 10.00 3.50 -11 -3 14 11.90 3.90 11 -3 14 10.50 3.10 11 -3 14 13.80 4.10 -11 -3 -14 10.80 3.20 11 4 14 58.89 7.70 -11 -4 14 51.79 7.80 11 4 14 40.30 7.50 -11 4 -14 40.50 6.30 11 -4 14 70.19 8.30 11 -4 14 52.39 6.50 -11 -4 -14 62.79 7.30 -11 -5 14 -1.20 2.80 11 5 14 5.40 3.70 -11 5 -14 2.20 2.60 11 5 14 1.90 2.60 -11 -5 -14 -0.70 1.90 11 -5 14 -0.90 2.40 11 -5 14 -0.80 1.80 11 -5 14 -0.80 1.80 11 6 14 184.68 14.60 -11 6 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175.18 13.30 -12 -2 14 61.39 8.30 -12 2 -14 85.69 9.00 12 2 14 68.49 9.20 12 2 14 54.49 7.90 12 -2 14 77.69 9.20 -12 -2 -14 71.39 7.90 12 -2 14 76.19 8.50 -12 3 -14 211.68 16.40 12 3 14 228.08 17.10 -12 -3 14 253.17 17.90 12 3 14 236.18 18.10 -12 -3 -14 231.98 16.40 12 -3 14 278.07 17.00 12 -3 14 203.28 16.80 12 4 14 65.99 9.40 -12 -4 14 107.39 11.70 12 4 14 86.39 10.90 -12 4 -14 96.59 10.20 -12 -4 -14 104.59 9.00 12 -4 14 113.39 8.80 12 -4 14 111.19 11.50 12 5 14 75.99 10.50 12 5 14 73.79 9.40 -12 5 -14 107.19 9.10 -12 -5 14 79.39 10.20 12 -5 14 94.49 10.80 -12 -5 -14 84.89 9.00 12 -5 14 103.59 8.20 -12 6 -14 37.70 6.10 12 6 14 42.40 7.80 12 6 14 44.90 7.00 -12 -6 14 30.70 6.60 -12 -6 -14 48.00 6.40 12 -6 14 40.90 5.40 12 7 14 222.58 17.10 12 7 14 209.08 18.00 -12 -7 14 247.68 18.40 -12 7 -14 229.58 16.30 12 -7 14 200.68 14.70 -12 -7 -14 231.28 16.20 12 8 14 39.70 6.90 -12 8 -14 23.30 5.10 12 8 14 31.80 7.20 -12 -8 14 45.20 8.10 -12 -8 -14 33.20 5.80 12 -8 14 43.70 5.40 -12 9 -14 96.89 10.30 -12 -9 14 91.59 12.40 12 9 14 89.89 10.90 12 9 14 87.49 12.10 -12 -9 -14 106.19 12.30 12 10 14 14.70 4.80 -12 -10 14 15.30 5.90 -12 10 -14 17.10 5.00 12 10 14 27.30 7.20 -12 -10 -14 8.20 5.00 -12 -11 14 43.40 9.10 12 11 14 53.99 10.20 12 11 14 50.49 8.40 -12 11 -14 69.79 8.30 -12 -11 -14 55.19 9.60 12 12 14 25.00 6.30 12 12 14 21.10 7.20 -12 -12 14 16.80 6.60 -12 12 -14 19.60 6.90 -12 -12 -14 21.90 7.20 12 13 14 46.50 8.50 -12 -13 14 32.90 8.50 12 13 14 47.40 9.40 -12 -13 -14 35.80 8.30 -13 0 -14 0.10 2.20 13 0 14 -1.70 2.30 13 0 14 -1.80 2.00 13 1 14 74.29 9.10 -13 1 -14 68.79 8.20 -13 -1 14 60.49 8.30 13 1 14 82.09 9.80 -13 -1 -14 78.59 8.80 13 -1 14 72.49 8.90 13 -1 14 79.49 9.40 13 2 14 10.60 3.80 13 2 14 12.40 4.40 -13 2 -14 16.20 4.30 -13 -2 14 15.90 4.70 -13 -2 -14 12.30 3.80 13 -2 14 16.60 4.20 13 -2 14 19.90 4.80 13 3 14 5.60 3.60 -13 3 -14 5.00 2.90 13 3 14 2.30 2.40 -13 -3 14 4.20 3.40 13 -3 14 7.40 3.00 13 -3 14 1.90 2.70 -13 -3 -14 1.90 2.40 13 4 14 14.50 4.30 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8.90 -4 5 -21 210.98 14.50 4 5 21 201.28 15.80 -4 -5 21 207.48 17.10 -4 -5 21 223.48 16.20 4 5 21 202.18 15.30 4 -5 21 191.78 14.90 -4 5 21 197.88 14.20 4 -5 21 224.68 16.10 -4 5 21 199.18 14.70 4 -5 21 181.98 15.50 4 6 21 60.39 8.20 -4 6 -21 49.70 6.50 4 6 21 57.99 8.00 -4 -6 21 42.90 8.40 4 -6 21 53.19 8.20 4 -6 21 64.49 7.90 4 -6 21 56.39 8.20 -4 6 21 65.59 7.50 -4 6 21 60.89 7.20 4 7 21 40.20 7.00 -4 -7 21 37.10 7.60 4 7 21 34.80 6.30 -4 7 -21 28.30 5.00 -4 7 21 40.30 5.80 4 -7 21 51.29 6.90 4 -7 21 31.00 6.40 -4 7 21 31.90 5.10 4 8 21 2.90 3.40 -4 -8 21 0.20 4.00 4 8 21 4.70 3.40 4 -8 21 2.20 2.90 -4 8 21 3.10 2.90 4 -8 21 7.10 4.50 4 9 21 18.60 5.00 -4 -9 21 19.60 6.60 4 9 21 26.40 6.00 4 -9 21 18.10 5.40 -4 9 21 11.00 3.90 4 10 21 54.99 8.50 -4 -10 21 63.59 10.70 4 10 21 44.90 7.90 -4 10 21 55.29 7.90 4 -10 21 60.49 9.80 -4 -11 21 16.70 7.00 4 11 21 5.10 3.60 4 11 21 11.70 4.90 4 -11 21 18.50 6.30 -4 11 21 12.40 4.60 4 12 21 -0.60 3.60 -4 -12 21 -2.40 3.50 4 -12 21 -2.00 4.30 -4 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46.00 8.50 5 7 21 51.59 7.90 -5 7 -21 43.00 6.10 5 7 21 45.40 7.30 -5 7 21 50.09 6.60 5 -7 21 43.20 6.40 -5 7 21 46.70 6.40 5 -7 21 43.50 7.50 5 8 21 13.20 4.40 -5 -8 21 -2.00 4.10 5 8 21 11.10 4.40 5 -8 21 5.50 3.50 -5 8 21 11.00 3.80 5 -8 21 5.40 4.20 -5 -9 21 38.70 8.20 5 9 21 53.49 8.20 5 9 21 50.19 7.50 -5 9 21 48.80 7.00 5 -9 21 31.70 7.40 -5 -10 21 7.70 5.60 5 10 21 3.20 3.80 5 10 21 10.30 4.20 -5 10 21 8.80 3.60 5 -10 21 8.30 4.70 5 11 21 17.80 5.40 5 11 21 14.10 4.80 -5 -11 21 15.30 6.60 -5 11 21 16.30 4.90 5 -11 21 8.40 5.60 5 12 21 13.40 4.60 -5 -12 21 3.60 5.00 5 12 21 16.30 6.60 5 -12 21 9.60 5.70 -5 12 21 17.60 5.70 -6 0 -21 196.48 15.10 -6 0 21 223.58 15.60 6 0 21 232.48 16.40 6 0 21 214.18 16.20 -6 1 -21 46.70 6.50 -6 -1 21 56.59 7.30 6 1 21 54.79 7.40 6 1 21 50.29 7.10 -6 1 21 44.90 6.40 6 -1 21 54.89 7.50 6 -1 21 46.60 7.00 6 2 21 48.60 7.10 -6 -2 21 40.60 7.70 6 2 21 50.19 7.30 -6 2 -21 55.09 6.90 6 -2 21 57.29 7.70 6 -2 21 49.70 6.90 -6 2 21 44.10 6.20 6 3 21 2.60 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4.00 6 -11 21 14.80 6.10 6 12 21 19.50 6.00 6 12 21 9.00 5.70 -6 -12 21 25.90 7.70 6 -12 21 18.10 6.70 7 0 21 0.30 2.40 -7 0 21 1.40 2.30 7 0 21 1.90 2.80 -7 0 -21 0.80 2.20 -7 1 -21 2.90 2.70 7 1 21 4.80 3.00 7 1 21 5.00 3.20 7 -1 21 4.30 2.80 -7 -1 -21 1.20 2.60 7 -1 21 0.80 2.80 -7 1 21 5.60 2.90 -7 -2 21 26.80 6.00 7 2 21 33.70 5.80 -7 2 -21 23.70 4.80 7 2 21 26.70 5.60 7 -2 21 31.80 5.50 7 -2 21 24.90 5.50 -7 2 21 30.90 4.90 -7 -3 21 22.20 5.60 7 3 21 22.70 4.90 7 3 21 23.50 5.30 -7 3 -21 25.30 4.90 7 -3 21 18.10 4.60 -7 3 21 26.40 4.90 7 -3 21 21.00 5.30 7 4 21 46.70 7.70 -7 4 -21 42.70 6.30 7 4 21 62.89 8.10 -7 -4 21 59.39 9.10 7 -4 21 45.50 6.70 -7 4 21 50.89 6.60 7 -4 21 50.19 7.70 7 5 21 6.00 4.00 -7 -5 21 1.40 3.40 7 5 21 6.90 3.60 -7 5 -21 8.20 3.10 7 -5 21 10.30 3.90 -7 5 21 4.10 2.50 7 -5 21 7.50 3.00 7 -5 21 5.60 3.50 -7 6 -21 75.99 8.50 7 6 21 75.29 9.80 -7 -6 21 89.79 11.60 7 6 21 72.69 9.30 7 -6 21 70.59 9.00 -7 6 21 63.79 7.60 7 -6 21 74.89 10.00 7 -6 21 63.49 8.00 7 7 21 19.80 5.50 -7 -7 21 24.70 6.80 7 7 21 29.50 5.80 -7 7 -21 20.50 4.50 7 -7 21 16.10 5.00 7 -7 21 19.20 4.70 7 -7 21 12.90 5.00 7 8 21 22.30 5.70 -7 8 -21 11.80 3.90 -7 -8 21 24.40 7.20 7 8 21 11.90 4.20 7 -8 21 24.90 5.00 7 -8 21 26.10 6.30 7 9 21 0.50 3.70 7 9 21 0.60 3.20 -7 -9 21 3.90 4.40 7 -9 21 0.90 3.20 7 -9 21 -3.50 3.60 -7 -10 21 2.10 4.70 7 10 21 0.40 3.10 7 10 21 1.70 4.30 7 -10 21 1.90 4.50 7 11 21 32.70 7.70 7 11 21 37.30 7.20 -7 -11 21 35.80 8.70 -7 -12 21 7.40 6.20 7 12 21 12.20 4.90 7 12 21 10.10 5.80 -8 0 -21 23.60 4.70 8 0 21 33.80 6.20 8 0 21 28.40 5.70 8 1 21 10.00 3.70 8 1 21 12.10 4.00 -8 1 -21 5.90 3.10 8 -1 21 14.90 4.60 -8 -1 -21 9.80 3.90 8 -1 21 9.40 3.60 -8 1 21 7.10 2.90 -8 2 -21 13.40 4.00 8 2 21 11.00 4.30 8 2 21 6.60 3.90 -8 -2 21 8.80 4.40 8 -2 21 15.70 4.20 -8 -2 -21 7.60 3.40 -8 2 21 9.30 3.30 8 -2 21 11.20 4.20 -8 3 -21 8.90 3.30 -8 -3 21 14.20 5.10 8 3 21 10.50 3.90 8 3 21 8.40 3.90 8 -3 21 7.70 3.20 8 -3 21 6.40 3.70 -8 3 21 15.30 3.80 8 4 21 7.00 3.60 -8 4 -21 7.60 3.30 8 4 21 8.80 4.20 -8 -4 21 11.20 5.10 8 -4 21 8.90 3.80 8 -4 21 11.00 4.40 -8 4 21 8.20 3.00 -8 5 -21 64.99 8.40 8 5 21 78.39 9.70 -8 -5 21 84.89 11.60 8 5 21 74.99 10.20 8 -5 21 86.89 10.20 -8 5 21 73.39 8.30 8 -5 21 87.79 9.20 8 -5 21 74.79 9.00 -8 -6 21 0.80 3.30 -8 6 -21 4.10 3.10 8 6 21 4.20 3.40 8 6 21 2.60 3.30 8 -6 21 10.40 4.00 8 -6 21 8.60 3.60 8 -6 21 3.90 3.60 -8 -7 21 7.90 4.60 8 7 21 12.40 5.00 -8 7 -21 8.00 3.60 8 7 21 5.50 4.20 8 -7 21 14.40 5.20 8 -7 21 13.60 4.90 8 -7 21 12.90 4.00 8 8 21 1.30 4.00 -8 -8 21 4.90 4.60 8 8 21 3.60 3.70 -8 8 -21 -1.30 2.80 8 -8 21 0.00 2.70 8 -8 21 1.20 3.30 -8 -9 21 1.70 4.60 8 9 21 2.20 4.20 8 9 21 -1.40 3.20 8 -9 21 12.10 4.10 -8 -10 21 6.80 5.50 8 10 21 11.30 4.40 8 10 21 16.40 5.60 8 11 21 5.70 4.40 -8 -11 21 8.00 6.00 8 11 21 6.30 4.10 -8 -12 21 15.40 6.50 8 12 21 21.00 6.40 8 12 21 10.50 4.70 9 0 21 1.30 2.90 9 0 21 -0.70 2.70 -9 0 -21 5.40 3.00 9 1 21 14.20 4.20 9 1 21 13.50 4.10 -9 1 -21 13.10 4.20 9 -1 21 11.00 3.70 9 -1 21 10.80 3.90 -9 -1 -21 13.80 4.10 -9 -2 21 22.60 6.00 9 2 21 27.90 5.90 -9 2 -21 23.50 5.00 9 2 21 34.70 6.30 9 -2 21 26.30 5.40 9 -2 21 33.10 6.20 -9 -2 -21 26.10 5.00 9 3 21 14.80 4.60 9 3 21 11.70 4.90 -9 3 -21 12.90 3.90 -9 -3 21 9.90 4.70 -9 3 21 14.00 3.70 9 -3 21 15.50 4.80 -9 -3 -21 8.60 3.20 9 -3 21 10.60 3.70 9 4 21 19.30 4.90 9 4 21 13.60 4.70 -9 -4 21 10.20 5.00 -9 4 -21 14.10 4.50 9 -4 21 12.20 3.80 9 -4 21 11.40 4.60 -9 4 21 25.50 4.60 -9 -5 21 6.80 4.30 9 5 21 9.70 4.00 9 5 21 3.00 3.60 -9 5 -21 11.30 4.20 -9 5 21 5.00 2.60 9 -5 21 5.00 3.90 9 -5 21 3.80 3.20 9 6 21 44.80 7.20 9 6 21 46.60 8.20 -9 -6 21 49.99 9.20 -9 6 -21 36.00 6.10 9 -6 21 37.00 7.20 9 -6 21 39.80 9.60 9 -6 21 34.40 6.00 9 7 21 14.60 4.90 9 7 21 9.80 5.20 -9 7 -21 2.00 3.30 -9 -7 21 11.40 5.00 9 -7 21 7.90 3.60 9 -7 21 9.90 4.70 -9 8 -21 10.90 4.10 9 8 21 2.70 4.00 9 8 21 3.00 3.80 -9 -8 21 2.00 4.00 9 -8 21 8.00 4.70 9 -8 21 11.50 3.80 9 9 21 12.70 5.20 9 9 21 22.50 5.50 -9 -9 21 5.40 5.10 9 -9 21 5.90 3.30 9 10 21 -3.10 3.90 9 10 21 -0.50 3.10 -9 -10 21 5.70 5.40 9 11 21 7.30 5.40 9 11 21 12.20 5.30 -9 -11 21 7.70 6.20 10 0 21 307.07 22.20 10 0 21 307.17 22.00 -10 0 -21 319.77 21.50 -10 1 -21 4.30 3.10 10 1 21 10.60 4.20 10 1 21 9.30 4.30 -10 -1 -21 9.60 3.60 10 -1 21 1.80 2.90 10 -1 21 1.10 3.00 10 2 21 14.30 4.50 -10 2 -21 21.60 4.60 10 2 21 9.90 4.20 10 -2 21 15.40 4.60 -10 -2 -21 5.90 3.00 10 -2 21 16.20 4.50 10 3 21 20.00 5.20 10 3 21 16.60 4.50 -10 3 -21 16.00 4.20 -10 -3 21 11.40 5.00 -10 -3 -21 18.30 4.30 10 -3 21 19.90 4.60 10 -3 21 17.40 5.10 -10 4 -21 54.09 7.50 10 4 21 63.89 8.80 10 4 21 52.69 8.50 -10 -4 21 60.59 9.40 10 -4 21 53.89 7.20 10 -4 21 73.59 9.50 -10 -4 -21 46.10 7.20 10 5 21 3.20 3.10 10 5 21 3.80 4.00 -10 5 -21 3.70 3.30 -10 -5 21 -1.20 3.60 10 -5 21 2.10 2.90 10 -5 21 6.10 3.80 10 6 21 38.80 7.10 -10 6 -21 34.60 6.30 10 6 21 34.60 7.20 -10 -6 21 44.10 8.80 10 -6 21 32.20 7.50 10 -6 21 45.10 6.50 -10 -7 21 1.20 4.00 10 7 21 8.70 4.60 10 7 21 7.20 4.00 -10 7 -21 1.60 2.80 10 -7 21 1.30 4.10 10 -7 21 4.40 3.40 10 8 21 -3.60 3.00 -10 -8 21 6.20 4.70 10 8 21 2.30 3.60 -10 8 -21 5.90 3.60 10 -8 21 0.20 3.70 10 -8 21 4.60 2.70 -10 9 -21 0.60 2.90 -10 -9 21 16.00 6.40 10 9 21 2.80 3.50 10 9 21 1.20 3.80 10 -9 21 4.80 3.40 10 10 21 100.79 13.00 -10 -10 21 123.79 15.20 10 10 21 95.39 12.00 10 11 21 6.40 4.70 -10 -11 21 6.30 5.80 10 11 21 5.40 3.90 -11 0 -21 -3.70 2.00 11 0 21 1.00 3.20 11 0 21 0.70 3.00 -11 1 -21 49.20 7.30 11 1 21 35.00 6.70 11 1 21 41.60 7.40 -11 -1 -21 47.50 6.90 11 -1 21 45.40 7.20 11 -1 21 50.99 7.90 -11 2 -21 10.30 3.90 11 2 21 -0.40 3.30 11 2 21 5.00 3.90 11 -2 21 1.90 2.70 -11 -2 -21 6.00 3.20 11 -2 21 4.70 3.60 -11 3 -21 18.20 4.90 -11 -3 21 25.60 6.30 11 3 21 16.60 4.60 11 3 21 20.60 5.50 11 -3 21 16.00 4.50 -11 -3 -21 15.40 4.10 11 -3 21 22.80 5.70 -11 4 -21 5.80 3.40 -11 -4 21 2.30 4.30 11 4 21 7.70 4.00 11 4 21 12.00 4.80 11 -4 21 -1.50 2.60 11 -4 21 8.50 3.90 -11 -4 -21 -0.70 2.70 11 5 21 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62.59 8.40 12 -2 21 59.39 8.90 12 -2 21 64.39 8.50 12 3 21 52.39 8.50 -12 -3 21 27.80 6.70 -12 3 -21 33.50 6.30 12 3 21 22.70 5.40 -12 -3 -21 36.90 6.00 12 -3 21 20.60 4.90 12 -3 21 34.20 6.70 12 4 21 60.19 9.20 -12 -4 21 43.70 8.60 -12 4 -21 46.10 7.30 12 4 21 69.99 9.30 12 -4 21 58.99 9.20 -12 -4 -21 58.09 8.40 12 -4 21 54.69 7.50 -12 5 -21 135.09 12.00 12 5 21 138.19 15.20 12 5 21 119.19 13.30 -12 -5 21 160.98 16.60 -12 -5 -21 141.29 12.10 12 -5 21 140.89 14.90 12 -5 21 121.39 11.20 -12 -6 21 53.79 9.50 12 6 21 50.59 8.10 -12 6 -21 37.70 6.70 12 6 21 38.70 8.10 12 -6 21 33.00 6.00 -12 -6 -21 53.09 7.80 12 -6 21 52.29 8.50 12 7 21 42.10 8.40 -12 -7 21 28.10 7.30 12 7 21 52.89 8.30 -12 7 -21 34.90 6.70 -12 -7 -21 30.50 6.20 12 -7 21 49.50 8.90 12 -7 21 44.10 6.60 12 8 21 21.40 6.60 12 8 21 9.30 4.40 -12 8 -21 13.80 4.80 -12 -8 21 7.30 5.00 12 -8 21 5.60 4.90 12 -8 21 11.70 3.80 -12 -8 -21 3.90 3.70 12 9 21 -1.90 3.10 12 9 21 11.80 5.40 -12 -9 21 9.70 5.80 -12 9 -21 6.20 4.10 12 -9 21 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4.20 -14 -4 -27 -0.40 4.00 14 -4 27 2.70 4.70 14 -4 27 2.90 3.60 -15 0 -27 1.40 4.10 15 0 27 -0.90 3.40 15 0 27 1.60 4.40 15 1 27 -4.90 3.70 15 1 27 -1.60 3.60 -15 1 -27 -1.30 4.10 15 -1 27 3.80 3.90 -15 -1 -27 -1.80 3.00 15 -1 27 -0.80 3.90 -15 2 -27 12.90 4.90 15 2 27 12.20 5.60 15 2 27 18.50 5.30 15 -2 27 10.30 4.50 15 -2 27 1.60 4.70 -15 -2 -27 11.30 4.70 -15 3 -27 1.20 4.40 15 3 27 -3.70 3.60 15 3 27 -3.80 3.60 -15 -3 -27 1.40 3.70 15 -3 27 6.70 5.00 15 -3 27 2.90 3.60 0 0 28 424.06 28.30 0 -1 28 29.60 6.10 0 1 28 29.40 5.70 0 -2 28 73.29 9.50 0 2 28 77.19 9.50 0 3 28 1.20 2.70 0 -3 28 1.70 3.20 0 3 -28 2.60 3.00 0 4 28 216.78 16.80 0 -4 28 221.58 17.20 0 -5 28 67.89 9.40 0 5 28 63.09 8.70 0 6 28 151.58 12.50 0 -6 28 128.69 15.50 0 -6 28 136.89 14.50 0 -7 28 -0.20 4.20 0 7 28 -0.30 3.10 0 -8 28 8.80 5.70 0 8 28 3.20 3.30 1 0 28 -0.60 3.00 1 0 28 0.30 3.10 -1 0 28 -1.10 2.70 -1 -1 28 10.50 4.30 1 1 28 12.00 4.30 1 1 28 3.50 3.40 -1 1 28 16.50 4.80 1 -1 28 9.90 3.90 1 -1 28 11.70 6.00 1 2 28 10.50 3.90 1 2 28 8.50 3.80 -1 2 -28 3.50 3.00 -1 -2 28 3.10 2.90 -1 2 28 4.70 3.30 1 -2 28 5.20 3.60 -1 -3 28 34.70 6.40 1 3 28 38.60 6.30 1 3 28 27.70 5.70 -1 3 -28 27.20 5.40 -1 3 28 27.30 5.70 1 -3 28 24.00 5.80 1 3 -28 32.70 5.50 -1 -4 28 31.50 6.90 1 4 28 32.90 6.30 -1 4 -28 35.20 6.70 1 4 28 53.79 7.30 -1 4 28 40.30 7.00 1 -4 28 37.00 7.00 1 5 28 2.20 3.30 1 5 28 5.60 3.20 -1 -5 28 1.80 3.60 -1 5 28 6.00 3.50 1 -5 28 6.90 3.60 1 6 28 18.90 5.20 1 6 28 25.60 5.50 -1 -6 28 26.10 7.40 1 -6 28 7.50 5.10 -1 6 28 21.80 5.20 1 -6 28 17.60 5.30 1 7 28 -1.30 2.80 -1 -7 28 -0.50 4.10 1 7 28 3.70 3.10 1 -7 28 -1.60 3.70 -1 7 28 0.20 2.80 1 8 28 13.10 4.80 1 8 28 13.80 4.90 -1 -8 28 11.10 5.70 -1 8 28 6.20 3.90 1 -8 28 5.40 5.40 2 0 28 67.19 9.20 2 0 28 94.59 10.10 -2 0 28 83.09 10.00 -2 -1 28 288.47 19.80 2 1 28 226.38 18.40 2 1 28 238.48 19.10 -2 1 28 308.77 20.10 2 -1 28 259.97 19.40 2 -1 28 268.97 19.10 2 2 28 0.50 2.70 -2 2 -28 3.60 3.20 -2 -2 28 -0.70 3.10 2 2 28 5.60 3.60 -2 2 28 3.60 3.40 2 -2 28 4.60 4.10 2 -2 28 5.90 3.70 2 3 28 89.69 10.10 -2 -3 28 76.09 10.00 2 3 28 90.99 10.70 -2 3 -28 87.69 9.40 2 -3 28 100.29 11.30 2 -3 28 87.69 10.30 -2 3 28 81.79 9.90 2 4 28 38.50 6.80 -2 4 -28 44.00 6.60 -2 -4 28 41.90 7.30 2 4 28 31.80 6.10 2 -4 28 48.10 7.50 2 -4 28 39.40 7.00 -2 4 28 40.90 6.70 2 5 28 336.17 23.70 2 5 28 320.27 23.00 -2 -5 28 316.57 25.50 2 -5 28 338.37 23.70 2 -5 28 360.06 24.60 -2 5 28 340.57 23.20 -2 -6 28 44.50 9.30 2 6 28 29.60 6.40 2 6 28 19.20 5.60 2 -6 28 27.10 6.20 -2 6 28 49.20 7.30 2 -6 28 59.69 12.60 2 -6 28 38.70 8.20 -2 -7 28 38.10 8.70 2 7 28 51.99 8.10 2 7 28 48.00 7.60 -2 7 28 61.09 8.30 2 -7 28 63.99 10.60 2 -7 28 53.79 8.20 -2 -8 28 3.30 5.70 2 8 28 8.30 4.20 2 8 28 3.00 3.30 2 -8 28 4.90 4.40 -3 0 28 2.00 3.20 3 0 28 0.40 2.40 3 0 28 0.20 3.10 3 1 28 28.80 5.60 -3 1 -28 14.10 4.40 3 1 28 28.60 5.90 -3 -1 28 14.80 4.90 -3 1 28 24.10 5.30 3 -1 28 40.80 6.90 3 -1 28 19.30 5.20 -3 -2 28 13.90 4.40 3 2 28 2.80 3.10 3 2 28 8.00 3.60 -3 2 -28 9.20 3.70 3 -2 28 3.90 3.90 3 -2 28 7.50 3.90 -3 2 28 3.50 3.30 3 3 28 2.50 3.00 -3 -3 28 3.30 3.30 3 3 28 0.80 2.80 -3 3 -28 10.00 3.50 3 -3 28 12.10 4.60 -3 3 28 4.70 3.60 3 -3 28 8.90 4.10 -3 4 -28 16.10 4.60 3 4 28 19.10 5.30 3 4 28 19.90 5.00 -3 -4 28 12.40 4.50 3 -4 28 21.30 5.40 -3 4 28 20.00 4.90 3 -4 28 17.90 5.30 -3 -5 28 -3.00 4.00 3 5 28 0.60 3.10 3 5 28 4.40 3.40 -3 5 28 5.80 3.30 3 -5 28 -1.10 3.40 3 -5 28 3.50 4.00 3 6 28 10.70 4.50 -3 -6 28 3.40 4.40 3 6 28 9.70 4.20 3 -6 28 20.20 6.20 3 -6 28 7.30 4.20 3 -6 28 8.10 3.90 -3 6 28 8.70 4.00 -3 -7 28 26.60 7.70 3 7 28 21.90 5.50 3 7 28 29.30 6.30 3 -7 28 25.00 6.00 -3 7 28 25.00 5.70 3 -7 28 23.40 6.40 3 -7 28 18.80 5.80 -3 -8 28 7.20 5.50 3 8 28 13.40 4.70 3 8 28 11.80 4.80 3 -8 28 33.80 7.70 3 -8 28 12.90 5.40 -4 0 28 132.99 12.10 4 0 28 140.89 12.40 -4 0 -28 132.69 11.50 4 0 28 111.99 12.70 4 1 28 80.49 9.70 4 1 28 67.29 9.10 -4 1 -28 60.79 8.20 -4 -1 28 74.99 9.70 4 -1 28 86.49 9.80 -4 1 28 59.69 8.50 4 -1 28 67.59 9.30 -4 2 -28 67.29 8.20 4 2 28 69.59 9.30 -4 -2 28 63.19 8.70 4 2 28 58.69 8.80 -4 2 28 76.09 9.50 4 -2 28 62.29 8.90 4 -2 28 87.69 10.30 -4 3 -28 80.89 9.20 4 3 28 77.39 10.10 -4 -3 28 80.29 10.20 4 3 28 68.09 8.90 4 -3 28 62.89 9.10 -4 3 28 88.59 10.00 4 -3 28 79.69 10.30 -4 4 -28 66.19 8.70 4 4 28 77.59 10.00 4 4 28 68.69 9.50 4 -4 28 75.59 10.00 4 -4 28 73.69 9.70 -4 4 28 87.39 10.00 -4 5 -28 69.29 12.30 4 5 28 63.29 8.90 -4 -5 28 43.10 8.90 4 5 28 59.19 8.80 4 -5 28 46.80 8.00 -4 5 28 75.69 9.20 4 -5 28 55.99 8.70 4 6 28 85.19 10.80 4 6 28 95.69 11.30 -4 -6 28 106.69 13.90 -4 6 28 100.79 10.60 4 -6 28 93.99 11.70 4 -6 28 74.69 10.20 4 7 28 66.59 9.10 -4 -7 28 68.59 11.10 4 7 28 45.80 7.90 4 -7 28 58.69 8.60 4 -7 28 43.40 8.00 4 -7 28 32.00 8.10 4 8 28 28.80 6.60 -4 -8 28 43.60 9.60 4 8 28 27.80 6.60 4 -8 28 26.90 6.50 4 -8 28 24.40 6.60 4 -8 28 34.30 7.80 5 0 28 -0.40 2.90 5 0 28 -0.50 2.60 -5 0 28 2.10 2.90 -5 0 -28 -2.20 2.40 -5 -1 28 32.30 6.20 5 1 28 21.40 5.30 -5 1 -28 19.20 4.80 5 1 28 31.10 6.10 -5 1 28 41.40 7.00 5 -1 28 22.40 5.40 5 -1 28 23.00 5.60 5 2 28 0.50 3.20 5 2 28 3.00 3.20 -5 2 -28 -3.30 2.60 -5 -2 28 -2.10 2.80 5 -2 28 1.40 3.90 5 -2 28 2.20 2.80 -5 2 28 -2.00 2.90 5 3 28 -3.20 2.90 -5 3 -28 -2.20 2.70 5 3 28 -0.70 3.10 5 -3 28 4.10 4.00 5 -3 28 -2.70 2.60 -5 3 28 -0.80 2.60 -5 4 -28 20.60 5.40 5 4 28 36.80 7.00 5 4 28 43.80 7.40 5 -4 28 40.90 7.10 5 -4 28 39.90 7.50 -5 4 28 21.80 5.30 -5 5 -28 7.30 3.60 5 5 28 0.40 3.30 5 5 28 2.70 3.50 -5 -5 28 4.90 4.40 5 -5 28 -0.10 3.30 5 -5 28 1.00 3.70 -5 5 28 4.90 3.40 -5 -6 28 11.20 5.70 5 6 28 12.50 4.40 5 6 28 2.10 3.40 -5 6 28 6.20 3.80 5 -6 28 5.10 3.80 5 -6 28 9.30 5.20 -5 -7 28 18.80 6.50 5 7 28 21.70 6.00 5 7 28 14.60 5.30 5 -7 28 30.10 7.10 5 -7 28 17.10 5.10 5 -7 28 14.10 6.20 -5 -8 28 4.70 5.10 5 8 28 8.10 4.30 5 8 28 8.60 4.70 5 -8 28 8.10 4.70 5 -8 28 4.00 4.70 5 -8 28 9.30 5.30 -6 0 28 79.89 9.70 6 0 28 73.69 9.90 -6 0 -28 69.39 8.80 6 0 28 70.29 9.60 -6 1 -28 8.40 3.90 6 1 28 17.30 5.10 -6 -1 28 10.50 4.30 6 1 28 15.90 4.80 -6 -1 -28 17.40 4.80 6 -1 28 16.70 5.20 6 -1 28 8.80 4.10 -6 1 28 9.70 3.90 -6 2 -28 176.48 13.70 6 2 28 141.89 13.80 6 2 28 162.48 14.10 -6 2 28 172.08 14.00 6 -2 28 160.78 14.20 6 -2 28 158.28 14.10 -6 3 -28 82.69 9.80 6 3 28 77.69 10.10 6 3 28 76.69 10.20 6 -3 28 99.29 11.60 6 -3 28 109.19 11.50 -6 3 28 83.39 10.10 -6 4 -28 81.69 10.20 6 4 28 124.49 13.40 6 4 28 125.89 12.80 6 -4 28 109.29 12.90 -6 4 28 112.29 11.60 6 -4 28 110.39 12.20 6 5 28 5.10 3.80 -6 -5 28 0.50 5.10 6 5 28 6.30 4.10 -6 5 -28 0.80 3.30 6 -5 28 8.70 4.90 -6 5 28 3.70 3.40 6 -5 28 7.40 4.10 6 6 28 103.79 12.00 -6 -6 28 102.99 14.00 6 6 28 104.49 12.50 6 -6 28 121.29 12.50 6 -6 28 117.29 13.30 6 7 28 23.30 6.00 6 7 28 38.10 7.70 -6 -7 28 26.90 7.80 6 -7 28 33.80 6.50 6 -7 28 49.00 8.70 -6 -8 28 95.29 13.50 6 8 28 94.39 12.30 6 8 28 110.99 12.50 6 -8 28 116.09 13.40 6 -8 28 108.39 12.10 -7 0 28 -1.00 2.60 7 0 28 1.30 3.30 7 0 28 5.60 3.40 -7 0 -28 1.60 3.00 -7 1 -28 8.70 3.40 7 1 28 28.80 6.40 7 1 28 11.70 4.70 -7 -1 -28 24.20 5.60 7 -1 28 13.70 4.90 7 -1 28 15.40 4.90 -7 1 28 17.50 5.10 7 2 28 1.10 3.10 7 2 28 7.30 4.30 -7 2 -28 12.20 4.60 7 -2 28 10.80 4.30 -7 -2 -28 8.30 3.80 -7 2 28 13.50 4.40 7 -2 28 4.20 4.00 7 3 28 16.10 5.20 -7 3 -28 11.30 4.60 7 3 28 16.90 5.60 -7 3 28 16.40 4.90 7 -3 28 9.30 4.70 7 -3 28 12.60 4.70 7 4 28 24.90 5.80 -7 4 -28 32.70 6.30 7 4 28 29.10 6.50 7 -4 28 16.70 5.50 -7 4 28 32.70 6.40 7 -4 28 19.20 5.30 -7 5 -28 -8.00 2.90 7 5 28 2.10 3.50 7 5 28 4.20 3.90 -7 -5 28 9.20 5.50 7 -5 28 -0.70 3.30 7 -5 28 2.20 3.40 -7 5 28 -1.80 2.30 7 6 28 19.80 5.80 7 6 28 34.90 7.20 -7 -6 28 28.90 7.70 7 -6 28 27.50 5.90 7 -6 28 23.50 6.80 -7 -7 28 0.80 4.00 7 7 28 7.40 4.00 7 7 28 5.90 3.90 7 -7 28 5.20 4.20 7 -7 28 -1.10 4.60 8 0 28 8.60 4.50 -8 0 -28 -2.70 2.50 8 0 28 4.50 3.60 -8 1 -28 67.19 9.00 8 1 28 92.69 11.00 8 1 28 68.39 9.80 -8 1 28 67.19 9.30 8 -1 28 77.19 10.00 -8 -1 -28 71.99 9.50 8 -1 28 82.39 10.70 -8 2 -28 109.39 11.50 8 2 28 96.19 11.60 8 2 28 99.79 11.70 8 -2 28 105.39 11.70 8 -2 28 96.29 11.80 -8 -2 -28 71.79 9.60 -8 2 28 84.39 10.40 8 3 28 250.67 19.80 8 3 28 246.98 19.50 -8 3 -28 290.57 19.60 8 -3 28 269.97 20.20 -8 3 28 229.68 18.30 8 -3 28 243.38 19.10 -8 -3 -28 259.47 19.20 8 4 28 21.30 5.80 8 4 28 13.60 5.00 -8 4 -28 9.40 4.40 -8 4 28 10.80 4.20 8 -4 28 18.10 5.80 8 -4 28 6.00 3.90 8 5 28 71.19 10.20 -8 -5 28 69.79 11.90 8 5 28 59.09 9.30 -8 5 -28 62.49 9.00 8 -5 28 85.19 10.50 8 -5 28 84.99 11.30 -8 6 -28 -1.20 3.60 8 6 28 8.40 4.50 -8 -6 28 1.70 4.20 8 6 28 5.50 4.70 8 -6 28 7.60 5.30 8 -6 28 6.40 3.80 8 7 28 204.28 16.80 -8 -7 28 178.88 19.70 8 7 28 178.78 16.70 8 -7 28 189.88 17.40 8 -7 28 218.98 16.40 9 0 28 1.10 2.90 -9 0 -28 -0.70 2.30 9 0 28 1.40 3.40 -9 1 -28 9.50 4.20 9 1 28 7.10 3.90 9 1 28 16.60 5.30 9 -1 28 13.10 4.60 -9 -1 -28 12.30 4.50 9 -1 28 7.50 4.30 9 2 28 5.00 3.70 -9 2 -28 -1.30 2.80 9 2 28 5.90 3.90 9 -2 28 3.90 4.10 9 -2 28 9.10 4.50 -9 -2 -28 2.90 3.50 -9 3 -28 19.60 5.30 9 3 28 13.70 5.20 9 3 28 8.30 4.30 9 -3 28 20.10 5.70 9 -3 28 11.60 5.10 -9 3 28 14.30 4.90 -9 -3 -28 6.90 4.00 9 4 28 20.60 5.70 -9 4 -28 17.30 4.90 9 4 28 16.20 5.40 -9 4 28 8.60 4.00 9 -4 28 5.60 4.50 -9 -4 -28 11.00 4.90 9 -4 28 27.70 6.30 -9 -5 28 3.70 5.00 -9 5 -28 1.50 3.50 9 5 28 -4.10 3.10 9 5 28 3.90 4.00 9 -5 28 3.40 3.30 9 -5 28 3.80 3.80 -9 6 -28 36.70 7.00 9 6 28 27.80 7.40 9 6 28 35.30 7.30 -9 -6 28 35.90 9.20 9 -6 28 40.10 8.00 9 -6 28 48.40 7.90 9 7 28 4.40 4.30 9 7 28 4.80 4.50 9 -7 28 4.30 4.90 9 -7 28 3.20 4.00 10 0 28 48.90 7.90 -10 0 -28 47.40 7.50 10 0 28 37.70 7.70 10 1 28 4.80 3.90 10 1 28 5.10 4.20 -10 1 -28 2.20 4.10 -10 -1 -28 5.20 3.20 10 -1 28 -0.70 3.30 10 -1 28 2.40 3.80 10 2 28 154.58 14.10 10 2 28 163.68 14.50 -10 2 -28 155.68 13.80 10 -2 28 141.09 15.50 -10 -2 -28 156.38 13.90 10 -2 28 149.59 13.60 10 3 28 101.39 12.40 -10 3 -28 106.09 11.50 10 3 28 111.29 12.70 10 -3 28 76.79 10.50 10 -3 28 98.39 12.20 -10 -3 -28 88.79 10.80 -10 4 -28 78.39 10.50 10 4 28 116.09 13.10 10 4 28 92.89 11.90 -10 -4 -28 81.19 10.80 10 -4 28 103.89 11.50 10 -4 28 103.29 12.50 10 5 28 8.80 4.60 10 5 28 0.30 3.70 -10 5 -28 6.60 4.40 -10 -5 28 0.50 4.10 -10 -5 -28 1.80 3.40 10 -5 28 3.40 4.20 10 -5 28 3.10 4.00 10 6 28 70.69 9.80 -10 6 -28 57.59 8.60 10 6 28 49.30 9.30 -10 -6 28 52.29 10.20 -10 -6 -28 57.79 8.90 10 -6 28 66.09 10.30 10 -6 28 67.79 9.50 11 0 28 -0.80 3.00 -11 0 -28 2.70 3.30 11 0 28 4.00 4.20 -11 1 -28 13.00 5.10 11 1 28 17.40 5.40 11 1 28 14.10 5.60 11 -1 28 20.40 5.70 11 -1 28 32.00 7.40 -11 -1 -28 13.60 4.70 11 2 28 5.90 4.10 11 2 28 6.50 4.00 -11 2 -28 0.40 3.70 -11 -2 -28 2.10 3.50 11 -2 28 1.10 3.10 11 -2 28 8.40 4.70 -11 3 -28 20.20 5.80 11 3 28 12.00 5.30 11 3 28 20.50 6.00 -11 -3 -28 7.10 4.00 11 -3 28 19.70 6.40 11 -3 28 13.20 4.60 11 4 28 23.30 6.10 11 4 28 9.40 4.80 -11 4 -28 11.10 4.70 11 -4 28 7.80 5.10 11 -4 28 10.00 4.30 -11 -4 -28 9.00 4.70 -11 5 -28 -2.50 4.00 11 5 28 -3.40 3.40 -11 -5 28 5.30 5.80 11 5 28 4.70 4.40 11 -5 28 -2.10 3.20 -11 -5 -28 3.80 4.70 11 -5 28 2.70 4.10 12 0 28 2.90 4.00 -12 0 -28 0.30 3.90 12 0 28 3.90 3.90 12 1 28 85.29 11.90 12 1 28 95.19 11.80 -12 1 -28 79.39 10.50 12 -1 28 93.69 12.20 12 -1 28 90.49 11.30 -12 -1 -28 92.99 11.50 -12 2 -28 40.90 7.80 12 2 28 44.20 8.10 12 2 28 49.00 8.20 12 -2 28 39.10 7.70 -12 -2 -28 40.80 7.70 12 -2 28 49.50 8.90 12 3 28 93.49 12.10 -12 3 -28 72.59 10.30 12 3 28 72.29 10.80 12 -3 28 65.89 9.60 12 -3 28 86.89 11.40 -12 -3 -28 86.99 10.80 -12 4 -28 16.60 5.70 12 4 28 26.30 6.40 12 4 28 5.90 5.00 12 -4 28 20.60 5.50 -12 -4 -28 20.30 6.20 12 -4 28 10.00 5.10 -12 -5 28 30.90 8.80 -12 5 -28 26.30 6.50 12 5 28 35.00 7.80 12 5 28 31.30 7.30 -12 -5 -28 34.40 7.20 12 -5 28 30.10 6.70 12 -5 28 36.20 8.10 13 0 28 -0.30 3.60 -13 0 -28 -2.60 3.50 13 0 28 -0.90 3.40 13 1 28 9.60 5.00 13 1 28 3.80 4.60 -13 1 -28 22.20 6.10 13 -1 28 11.40 5.20 13 -1 28 1.80 3.90 -13 -1 -28 7.10 5.10 -13 2 -28 1.80 3.60 13 2 28 2.70 4.10 13 2 28 16.70 5.30 13 -2 28 12.40 5.80 13 -2 28 7.30 4.00 -13 -2 -28 4.50 4.30 13 3 28 7.20 4.90 13 3 28 0.20 3.70 -13 3 -28 6.90 4.10 -13 -3 -28 4.80 4.30 13 -3 28 5.90 4.10 13 -3 28 7.70 4.90 -13 4 -28 -3.10 4.10 13 4 28 2.60 4.30 13 4 28 3.40 4.10 13 -4 28 7.00 4.90 -13 -4 -28 3.60 3.40 13 -4 28 1.90 3.50 -14 0 -28 67.19 9.60 14 0 28 64.29 10.30 14 0 28 68.09 10.60 14 1 28 84.09 11.50 -14 1 -28 67.29 9.80 14 1 28 75.79 11.40 14 -1 28 84.29 11.70 14 -1 28 106.99 12.20 -14 -1 -28 80.39 11.10 -14 2 -28 4.90 4.90 14 2 28 29.60 7.00 14 2 28 19.10 6.50 -14 -2 -28 12.00 5.40 14 -2 28 18.50 6.00 14 -2 28 15.70 5.70 0 0 29 0.20 3.40 0 -1 29 3.90 3.40 0 1 29 -2.10 2.40 0 2 29 1.50 3.00 0 -2 29 -1.30 3.00 0 3 -29 1.20 3.00 0 3 29 -0.20 2.80 0 -3 29 0.90 3.30 0 4 29 1.40 3.30 0 -4 29 1.40 2.90 0 -5 29 -1.50 2.80 0 5 29 -0.40 3.10 0 -6 29 -1.30 3.40 0 -6 29 0.20 5.10 0 6 29 -2.00 2.80 0 -7 29 1.70 4.60 0 7 29 0.80 2.70 0 8 29 -3.60 2.90 -1 0 29 2.60 3.50 1 0 29 -1.00 2.90 -1 -1 29 8.90 4.10 1 1 29 10.20 4.50 1 -1 29 13.50 5.20 -1 1 29 19.10 5.00 1 2 29 7.30 3.70 -1 -2 29 11.00 4.40 -1 2 -29 13.50 4.20 -1 2 29 8.80 3.70 1 -2 29 10.80 4.70 1 3 29 17.40 5.00 -1 3 -29 28.40 5.40 -1 -3 29 22.00 5.40 -1 3 29 9.50 4.10 1 -3 29 32.30 6.20 -1 -4 29 10.30 4.50 1 4 29 13.60 4.50 1 -4 29 10.10 4.40 -1 4 29 7.80 4.10 1 5 29 -0.20 2.70 -1 -5 29 0.40 2.80 1 -5 29 1.60 3.50 -1 5 29 -2.00 3.00 -1 -6 29 34.30 8.40 1 6 29 19.20 5.40 -1 6 29 26.90 5.90 1 -6 29 19.70 5.70 1 -6 29 33.10 7.70 1 7 29 0.20 3.30 -1 -7 29 0.40 4.60 -1 7 29 -1.60 3.10 1 -7 29 0.60 4.70 2 0 29 59.79 8.70 -2 0 29 57.29 8.60 2 0 29 67.49 8.80 2 1 29 -0.90 3.10 2 1 29 3.70 3.60 -2 -1 29 6.70 3.60 2 -1 29 -2.10 2.80 2 -1 29 3.60 4.30 -2 1 29 1.90 3.00 2 2 29 9.80 4.20 -2 -2 29 10.10 4.20 2 2 29 14.60 4.30 -2 2 -29 12.10 4.20 2 -2 29 5.70 3.90 -2 2 29 7.00 3.70 2 3 29 38.90 6.70 -2 -3 29 27.10 6.00 2 3 29 32.00 6.10 -2 3 -29 31.30 5.70 -2 3 29 33.10 6.50 2 -3 29 22.60 5.90 2 4 29 2.90 3.20 -2 -4 29 7.30 4.10 2 4 29 5.60 3.80 2 -4 29 -0.40 3.20 -2 4 29 5.30 3.40 2 5 29 15.50 5.00 2 5 29 9.20 4.50 -2 5 29 18.70 4.80 2 -5 29 19.90 5.30 2 6 29 5.00 3.90 2 6 29 5.10 4.00 -2 -6 29 12.90 6.30 2 -6 29 8.80 3.90 -2 6 29 8.10 4.10 -2 -7 29 28.40 8.20 2 7 29 22.70 5.40 2 7 29 14.40 4.70 -2 7 29 32.90 6.20 2 -7 29 20.30 6.00 2 -7 29 30.40 7.90 -3 0 29 -1.40 2.50 3 0 29 -0.10 3.00 3 0 29 2.90 3.20 3 1 29 4.50 3.20 -3 -1 29 8.10 3.80 3 1 29 -1.00 3.20 -3 1 -29 2.10 3.30 3 -1 29 7.30 3.80 3 -1 29 11.90 4.20 -3 1 29 5.80 3.80 -3 2 -29 7.20 3.90 -3 -2 29 8.10 3.80 3 2 29 13.50 4.50 3 2 29 13.20 4.70 3 -2 29 3.60 3.50 -3 2 29 12.20 4.70 3 -2 29 1.10 3.70 -3 -3 29 6.10 4.20 -3 3 -29 10.00 3.80 3 3 29 6.40 3.90 3 3 29 4.40 3.50 -3 3 29 5.10 3.50 3 -3 29 5.00 3.50 3 -3 29 2.00 3.80 3 4 29 54.69 8.00 -3 -4 29 54.59 8.80 3 4 29 45.20 7.80 -3 4 -29 55.69 7.60 3 -4 29 49.20 8.30 -3 4 29 57.29 8.30 3 -4 29 42.30 7.50 3 5 29 5.00 3.50 3 5 29 3.40 3.30 3 -5 29 6.40 4.10 3 -5 29 7.30 4.00 -3 5 29 1.70 3.20 3 6 29 4.80 3.80 -3 -6 29 7.40 5.40 3 6 29 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1.60 3.30 -7 1 -30 29.90 6.40 7 1 30 34.50 6.70 7 1 30 25.50 6.20 -7 1 30 26.20 6.20 -7 -1 -30 26.50 6.40 7 -1 30 30.60 7.00 7 -1 30 33.10 7.20 7 2 30 0.60 3.30 7 2 30 -0.20 3.90 -7 2 -30 0.40 3.30 -7 -2 -30 3.30 3.20 -7 2 30 3.80 3.70 7 -2 30 -1.60 3.60 7 -2 30 -3.70 2.60 7 3 30 4.40 3.70 -7 3 -30 -2.60 3.70 7 3 30 2.00 4.20 7 -3 30 6.70 4.30 -7 -3 -30 3.70 3.70 -7 3 30 2.00 3.30 7 -3 30 6.50 5.00 -7 4 -30 13.40 4.50 7 4 30 11.20 5.30 7 4 30 16.90 5.50 7 -4 30 12.80 5.10 7 -4 30 5.20 5.20 -7 4 30 3.80 3.60 7 5 30 -2.90 3.20 -7 5 -30 -1.10 3.60 7 5 30 1.30 3.60 7 -5 30 0.60 4.10 7 -5 30 -1.90 3.10 8 0 30 80.99 10.80 8 0 30 65.89 9.50 -8 0 -30 68.19 9.50 8 1 30 -3.80 3.10 8 1 30 1.40 3.80 -8 1 -30 -2.20 3.30 8 -1 30 -2.20 2.80 -8 -1 -30 1.20 3.50 8 -1 30 0.50 3.60 -8 2 -30 181.28 15.60 8 2 30 195.98 16.20 8 2 30 183.58 16.00 -8 -2 -30 187.58 15.60 8 -2 30 186.28 15.80 8 -2 30 199.98 16.90 -8 2 30 173.48 15.50 -8 3 -30 57.59 8.40 8 3 30 58.39 9.20 8 3 30 50.49 8.80 8 -3 30 77.99 11.10 -8 3 30 57.79 8.70 -8 -3 -30 53.59 8.30 8 -3 30 63.99 9.30 8 4 30 71.89 10.40 -8 4 -30 85.09 10.50 8 4 30 87.69 11.30 -8 4 30 98.59 11.00 8 -4 30 85.29 11.60 -8 -4 -30 77.79 10.40 8 -4 30 93.59 11.50 8 5 30 18.30 5.70 8 5 30 26.30 6.80 -8 5 -30 28.30 6.20 8 -5 30 18.50 6.30 8 -5 30 34.50 7.10 -9 0 -30 -1.80 3.60 9 0 30 -2.20 3.60 9 0 30 0.60 3.60 9 1 30 16.70 5.40 -9 1 -30 17.10 5.10 9 1 30 25.20 6.40 9 -1 30 26.10 6.40 9 -1 30 10.90 5.20 -9 -1 -30 16.30 5.30 9 2 30 0.60 4.30 9 2 30 6.90 4.10 -9 2 -30 7.80 4.80 9 -2 30 3.50 4.10 9 -2 30 8.10 5.30 -9 -2 -30 15.80 4.70 9 3 30 10.70 4.70 9 3 30 5.90 4.20 -9 3 -30 7.80 4.40 9 -3 30 12.80 5.30 -9 -3 -30 11.90 4.90 -9 3 30 9.30 4.40 9 -3 30 10.10 4.70 -9 4 -30 3.30 3.70 9 4 30 9.50 5.30 9 4 30 7.90 4.80 9 -4 30 8.70 4.50 9 -4 30 5.80 4.80 -9 -4 -30 1.50 3.60 10 0 30 21.70 5.80 -10 0 -30 12.30 4.50 10 0 30 29.00 7.00 -10 1 -30 152.48 16.00 10 1 30 163.78 14.90 10 1 30 167.88 15.40 10 -1 30 192.28 15.40 10 -1 30 179.38 15.80 -10 -1 -30 149.49 15.40 10 2 30 69.79 10.40 10 2 30 85.99 11.20 -10 2 -30 70.29 9.60 -10 -2 -30 78.69 10.50 10 -2 30 69.79 10.20 10 -2 30 81.49 11.30 10 3 30 150.88 16.10 -10 3 -30 162.88 14.30 10 3 30 177.28 15.10 -10 -3 -30 151.38 15.40 10 -3 30 140.19 16.00 10 -3 30 153.38 14.10 -11 0 -30 2.50 4.20 11 0 30 -1.40 3.30 11 0 30 3.30 4.60 11 1 30 -1.10 3.50 -11 1 -30 -4.10 3.50 11 1 30 0.40 4.10 11 -1 30 4.20 4.00 -11 -1 -30 4.40 3.70 11 -1 30 2.50 4.30 -11 2 -30 13.20 5.50 11 2 30 8.90 5.20 11 2 30 2.60 4.40 -11 -2 -30 8.30 4.10 11 -2 30 8.20 5.20 0 0 31 0.00 3.00 0 -1 31 2.30 3.40 0 1 31 1.30 2.90 0 -2 31 -2.90 3.00 0 2 -31 -0.60 3.20 0 2 31 -1.00 2.90 0 3 31 -2.00 2.80 0 -3 31 3.30 3.30 0 -4 31 -0.60 3.00 0 4 31 1.80 3.20 0 -5 31 2.60 4.00 0 5 31 3.60 3.50 1 0 31 0.70 3.30 -1 0 31 2.80 3.30 -1 -1 31 17.20 5.30 1 1 31 11.30 4.50 -1 1 31 13.70 4.90 1 -1 31 6.50 4.20 -1 2 -31 -0.80 3.20 -1 -2 31 1.30 3.70 1 2 31 3.30 3.10 -1 2 31 4.00 3.80 1 -2 31 1.00 3.60 -1 -3 31 5.80 3.90 1 3 31 11.30 4.90 -1 3 31 6.40 4.00 1 -3 31 14.80 4.90 -1 -4 31 22.40 5.90 1 4 31 7.70 4.20 -1 4 31 22.10 5.30 1 -4 31 22.00 5.80 -1 -5 31 -2.00 2.90 1 5 31 -1.10 2.90 -1 5 31 0.50 3.20 1 -5 31 3.70 3.70 2 0 31 8.20 4.30 -2 0 31 6.30 3.90 2 1 31 22.70 5.90 -2 -1 31 25.50 6.40 -2 1 -31 9.80 4.50 2 -1 31 18.10 5.40 -2 1 31 21.70 5.70 -2 2 -31 26.10 5.90 -2 -2 31 30.70 6.40 2 2 31 26.30 6.30 2 -2 31 20.60 5.50 -2 2 31 23.60 6.00 -2 -3 31 18.30 5.60 2 3 31 5.50 3.90 -2 3 -31 6.90 4.00 -2 3 31 7.90 3.70 2 -3 31 5.00 4.00 -2 -4 31 -0.80 3.80 2 4 31 7.40 4.00 -2 4 31 0.00 3.20 2 -4 31 8.20 4.30 2 5 31 30.10 6.60 -2 5 31 38.80 6.90 2 -5 31 28.70 6.40 3 0 31 -1.00 3.30 -3 0 -31 -0.10 3.10 -3 0 31 3.50 3.40 -3 -1 31 16.40 5.20 -3 1 -31 11.90 4.40 3 1 31 13.50 4.90 -3 1 31 16.60 5.10 3 -1 31 14.40 4.70 3 2 31 5.60 3.90 -3 -2 31 4.80 3.70 -3 2 -31 4.20 3.50 3 -2 31 2.10 3.50 -3 2 31 0.50 2.80 3 3 31 19.40 5.60 -3 -3 31 10.10 4.70 -3 3 -31 16.90 4.70 3 -3 31 8.80 4.40 -3 3 31 13.50 4.90 3 4 31 13.80 4.90 3 -4 31 7.30 4.40 -3 4 31 5.90 4.20 3 5 31 0.10 3.30 3 -5 31 3.40 3.50 -3 5 31 2.90 3.40 4 0 31 69.59 9.20 -4 0 31 65.69 9.40 4 0 31 56.79 9.10 -4 0 -31 63.49 8.70 -4 1 -31 -1.50 3.30 4 1 31 -0.10 3.10 -4 -1 31 1.60 4.00 4 1 31 3.50 4.00 4 -1 31 1.70 3.80 4 -1 31 0.70 2.80 -4 1 31 -2.30 3.00 4 2 31 4.60 4.10 -4 -2 31 -0.30 3.90 4 2 31 5.60 3.60 -4 2 -31 2.60 3.70 4 -2 31 2.00 3.70 4 -2 31 17.00 8.70 -4 2 31 1.70 3.30 4 3 31 24.00 5.90 4 3 31 35.40 6.90 -4 -3 31 35.60 7.50 -4 3 -31 37.90 6.80 4 -3 31 33.10 6.90 -4 3 31 33.10 6.70 4 4 31 20.50 5.60 4 4 31 22.50 5.80 4 -4 31 17.40 5.60 -4 4 31 14.60 4.90 4 5 31 17.40 5.50 4 5 31 7.10 4.40 4 -5 31 18.00 5.60 -4 5 31 14.60 5.10 5 0 31 -2.50 3.30 -5 0 31 0.30 3.20 -5 0 -31 0.80 3.90 5 0 31 -1.50 3.50 -5 -1 31 14.10 5.00 5 1 31 4.60 3.90 -5 1 -31 18.10 4.50 5 1 31 14.00 5.10 -5 1 31 15.30 4.70 -5 -1 -31 10.90 4.40 5 -1 31 10.90 4.50 5 -1 31 18.20 5.40 5 2 31 8.00 4.10 -5 -2 31 9.40 4.90 5 2 31 11.50 4.70 -5 2 -31 8.40 4.60 5 -2 31 13.20 5.00 5 -2 31 4.60 4.00 -5 2 31 12.20 4.60 -5 3 -31 7.30 4.40 5 3 31 10.10 4.30 5 3 31 14.70 4.90 -5 3 31 7.80 4.20 5 -3 31 15.00 5.60 5 -3 31 19.20 5.60 -5 4 -31 15.90 5.30 5 4 31 9.20 4.40 5 4 31 1.70 3.60 -5 4 31 13.20 4.80 5 -4 31 12.90 4.80 5 -4 31 7.70 4.50 -6 0 31 5.30 3.50 6 0 31 -2.70 3.90 -6 0 -31 1.50 3.30 6 0 31 4.10 3.60 6 1 31 2.60 3.40 -6 1 -31 1.40 3.60 -6 -1 31 4.60 4.10 6 1 31 9.10 4.60 -6 -1 -31 2.20 3.40 6 -1 31 0.90 3.50 -6 1 31 5.50 4.10 6 -1 31 0.10 4.00 -6 2 -31 15.10 5.10 6 2 31 28.10 6.40 6 2 31 40.50 7.80 -6 2 31 44.90 7.30 6 -2 31 30.10 6.60 -6 -2 -31 29.80 6.80 6 -2 31 43.50 7.50 6 3 31 18.90 5.70 6 3 31 28.70 6.40 -6 3 -31 15.30 5.00 6 -3 31 14.80 5.70 6 -3 31 5.60 4.80 -6 3 31 15.60 4.90 -6 4 -31 -2.10 2.90 6 4 31 3.40 4.40 6 4 31 -1.00 3.30 6 -4 31 2.00 3.80 -6 4 31 2.40 3.90 6 -4 31 4.20 4.40 -7 0 31 -2.40 3.10 7 0 31 3.00 3.90 -7 0 -31 -2.10 3.30 7 0 31 -0.10 4.20 7 1 31 9.60 4.60 7 1 31 13.50 4.70 -7 1 -31 11.00 4.60 -7 -1 -31 14.90 5.10 7 -1 31 6.60 4.20 -7 1 31 3.50 3.80 7 -1 31 2.90 3.60 -7 2 -31 2.90 4.00 7 2 31 3.30 4.20 7 2 31 4.60 4.30 7 -2 31 -1.10 3.30 -7 -2 -31 4.00 4.00 -7 2 31 5.70 3.90 7 -2 31 6.50 4.60 7 3 31 3.20 3.90 7 3 31 -5.60 3.10 -7 3 -31 0.90 3.70 7 -3 31 2.80 3.80 -7 -3 -31 -0.50 3.50 7 -3 31 5.20 4.90 -7 3 31 0.20 3.20 8 0 31 2.80 4.50 -8 0 -31 14.60 4.70 8 0 31 5.80 4.40 -8 1 -31 -1.40 3.20 8 1 31 5.20 4.20 8 1 31 7.40 4.00 -8 -1 -31 2.70 3.70 8 -1 31 9.30 4.60 8 -1 31 6.70 4.90 -8 2 -31 10.90 4.80 8 2 31 10.10 4.50 8 2 31 12.20 5.30 8 -2 31 12.20 5.20 -8 -2 -31 10.40 4.50 -8 2 31 3.90 4.20 8 -2 31 6.40 4.30 -8 3 -31 -0.10 3.60 8 3 31 10.40 5.10 8 3 31 0.50 3.30 8 -3 31 1.40 3.80 -8 3 31 1.30 4.00 -8 -3 -31 4.50 3.50 8 -3 31 -2.50 3.80 9 0 31 1.20 3.30 -9 0 -31 -1.60 3.20 9 0 31 -1.80 4.00 -9 1 -31 -0.20 4.00 9 1 31 3.30 3.80 9 1 31 4.20 4.60 -9 -1 -31 3.00 4.10 9 -1 31 -1.30 3.20 9 -1 31 9.90 5.20 0 0 32 30.60 7.00 0 1 32 19.00 5.80 0 -1 32 34.80 6.90 0 2 -32 62.19 9.30 0 2 32 69.19 9.60 0 -2 32 63.89 9.50 0 -3 32 29.80 6.90 0 3 32 43.90 7.30 0 -4 32 2.00 3.80 0 4 32 6.10 3.80 1 0 32 -1.10 3.40 -1 0 32 3.90 3.70 -1 1 -32 11.00 4.40 1 1 32 5.40 4.00 -1 -1 32 10.50 4.70 -1 1 32 -1.70 3.30 1 -1 32 2.80 3.90 1 2 32 5.40 3.90 -1 2 -32 3.50 3.90 -1 -2 32 11.50 5.00 1 -2 32 4.10 3.70 -1 2 32 2.80 4.20 -1 -3 32 4.50 3.90 1 3 32 3.30 3.80 -1 3 32 0.70 3.50 1 -3 32 3.90 4.40 -2 0 32 50.79 8.40 2 0 32 43.00 7.90 -2 1 -32 2.60 3.60 2 1 32 11.50 4.90 -2 -1 32 6.60 4.20 2 -1 32 2.40 3.90 -2 1 32 2.70 3.40 -2 2 -32 47.50 7.70 2 2 32 72.39 9.80 -2 -2 32 50.49 8.30 2 -2 32 59.89 9.10 -2 2 32 53.19 8.50 2 3 32 86.49 11.10 -2 -3 32 94.19 11.70 2 -3 32 97.49 11.80 -2 3 32 82.69 10.80 -3 0 32 -1.70 3.60 -3 0 -32 -0.80 3.20 3 0 32 0.00 3.50 -3 1 -32 10.00 4.80 -3 -1 32 21.10 5.50 3 1 32 6.90 4.70 3 -1 32 12.50 4.70 -3 1 32 21.50 5.70 -3 2 -32 7.50 3.80 -3 -2 32 3.80 3.70 3 2 32 0.70 3.70 3 -2 32 5.30 4.60 -3 2 32 -1.50 3.50 3 3 32 1.00 3.40 -3 3 -32 -1.10 3.80 -3 -3 32 2.70 4.20 3 -3 32 2.10 3.90 -3 3 32 -1.00 3.00 -4 0 -32 -2.00 3.20 4 0 32 2.00 4.00 -4 0 32 8.10 4.10 -4 1 -32 80.29 10.00 -4 -1 32 75.09 10.50 4 1 32 71.09 9.90 -4 -1 -32 61.89 8.70 4 -1 32 69.69 10.00 -4 1 32 79.89 10.20 -4 2 -32 6.30 4.00 -4 -2 32 3.90 4.30 4 2 32 3.40 3.90 -4 2 32 8.80 4.50 4 -2 32 3.10 3.80 4 3 32 104.39 12.40 -4 3 -32 91.29 10.80 4 -3 32 102.69 12.40 -4 3 32 114.49 12.50 -5 0 -32 -1.70 3.50 -5 0 32 -2.90 3.70 5 0 32 4.50 4.10 5 0 32 0.40 3.40 -5 1 -32 14.70 4.90 5 1 32 14.70 5.60 -5 -1 32 15.30 5.40 5 1 32 14.10 5.40 5 -1 32 7.50 4.80 5 -1 32 18.90 5.70 -5 -1 -32 19.90 5.90 -5 1 32 12.00 4.70 5 2 32 9.30 5.00 5 2 32 11.20 4.90 -5 2 -32 12.40 4.80 -5 -2 32 8.20 4.70 -5 2 32 -0.20 3.00 5 -2 32 10.70 4.50 6 0 32 171.98 15.00 6 0 32 174.48 15.20 -6 0 32 172.68 14.90 -6 0 -32 132.89 14.50 6 1 32 35.30 7.60 6 1 32 47.30 8.10 -6 1 -32 34.30 6.90 -6 1 32 41.20 7.60 6 -1 32 26.10 6.50 6 -1 32 40.00 7.50 -6 -1 -32 32.10 6.80 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 45893 _shelx_shelxl_version_number 2014/7 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x+1/2, -y, z' '-x+1/2, y, z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn I3 I 0.75089(2) 0.50684(4) 0.66353(3) 0.0220(2) Uani 1 1 d . I4 I 0.69281(3) 0.29985(5) 0.59268(4) 0.02593(16) Uani 1 1 d . I1 I 0.50419(3) 1.00450(5) 0.33327(3) 0.0232(2) Uani 1 1 d . I2 I 0.56076(3) 0.80111(5) 0.40710(4) 0.02867(17) Uani 1 1 d . Co2 Co 0.69469(5) 0.48373(9) 0.58339(5) 0.0155(3) Uani 1 1 d . Co1 Co 0.56245(5) 0.98570(9) 0.41266(6) 0.0161(3) Uani 1 1 d . N1 N 0.6721(3) 0.9927(5) 0.3557(4) 0.015(2) Uani 1 1 d . C44 C 0.4797(4) 0.4960(6) 0.6451(4) 0.016(2) Uani 1 1 d . C45 C 0.5955(4) 0.5150(7) 0.7448(4) 0.017(2) Uani 1 1 d . C43 C 0.4304(4) 0.4962(7) 0.6748(5) 0.024(3) Uani 1 1 d . H43 H 0.3931 0.4935 0.6601 0.029 Uiso 1 1 calc R C6 C 0.7680(4) 0.9897(6) 0.2480(5) 0.019(2) Uani 1 1 d . H6 H 0.7654 0.9907 0.2133 0.023 Uiso 1 1 calc R C38 C 0.6266(4) 0.4930(6) 0.6185(4) 0.013(2) Uani 1 1 d . C60 C 0.4733(4) 0.5001(5) 0.5904(4) 0.013(2) Uani 1 1 d . C16 C 0.5038(4) 1.0030(6) 0.1203(5) 0.024(3) Uani 1 1 d . H16A H 0.5200 0.9415 0.1103 0.035 Uiso 1 1 calc GR H16B H 0.5307 1.0542 0.1113 0.035 Uiso 1 1 calc GR H16C H 0.4665 1.0131 0.1038 0.035 Uiso 1 1 calc GR C29 C 0.7995(4) 1.0086(6) 0.5062(4) 0.019(2) Uani 1 1 d . C47 C 0.6033(4) 0.3335(7) 0.7501(4) 0.023(2) Uani 1 1 d . H47 H 0.5810 0.3380 0.7188 0.028 Uiso 1 1 calc R C2 C 0.7233(4) 0.9916(6) 0.3261(5) 0.018(3) Uani 1 1 d . C7 C 0.7173(4) 0.9918(6) 0.2757(4) 0.016(2) Uani 1 1 d . C34 C 0.7743(3) 0.9168(6) 0.4333(3) 0.015(2) Uani 1 1 d . C88 C 0.7046(4) 0.7097(7) 0.5794(4) 0.0282(13) Uani 1 1 d . H88A H 0.6663 0.7155 0.5947 0.042 Uiso 1 1 calc GR H88B H 0.7102 0.7621 0.5562 0.042 Uiso 1 1 calc GR H88C H 0.7347 0.7125 0.6047 0.042 Uiso 1 1 calc GR C40 C 0.5382(4) 0.5044(6) 0.7193(4) 0.017(3) Uani 1 1 d . C75 C 0.5743(4) 0.9873(7) 0.4879(4) 0.020(2) Uani 1 1 d . C46 C 0.6257(4) 0.4317(7) 0.7620(3) 0.017(2) Uani 1 1 d . C94 C 0.6471(3) 0.4140(7) 0.4787(3) 0.025(2) Uani 1 1 d . H94A H 0.6628 0.3497 0.4833 0.037 Uiso 1 1 calc GR H94B H 0.6495 0.4315 0.4441 0.037 Uiso 1 1 calc GR H94C H 0.6064 0.4152 0.4892 0.037 Uiso 1 1 calc GR C77 C 0.5970(3) 1.0735(7) 0.4668(3) 0.021(2) Uani 1 1 d . C48 C 0.5611(4) 0.2964(8) 0.7902(4) 0.032(3) Uani 1 1 d . H48A H 0.5823 0.2876 0.8208 0.048 Uiso 1 1 calc GR H48B H 0.5444 0.2354 0.7798 0.048 Uiso 1 1 calc GR H48C H 0.5299 0.3429 0.7951 0.048 Uiso 1 1 calc GR C33 C 0.7822(3) 0.9240(7) 0.4838(3) 0.019(2) Uani 1 1 d . H33 H 0.7754 0.8694 0.5036 0.023 Uiso 1 1 calc R C27 C 0.7569(4) 1.2249(6) 0.3837(4) 0.024(2) Uani 1 1 d . H27A H 0.7270 1.1793 0.3736 0.036 Uiso 1 1 calc GR H27B H 0.7633 1.2714 0.3575 0.036 Uiso 1 1 calc GR H27C H 0.7442 1.2580 0.4133 0.036 Uiso 1 1 calc GR C50 C 0.6754(4) 0.4466(7) 0.7896(3) 0.023(2) Uani 1 1 d . H50 H 0.6950 0.3927 0.8024 0.028 Uiso 1 1 calc R C56 C 0.6173(3) 0.6060(7) 0.7540(3) 0.017(2) Uani 1 1 d . C35 C 0.7602(3) 0.8202(6) 0.4105(4) 0.0204(19) Uani 1 1 d . H35 H 0.7363 0.8321 0.3806 0.025 Uiso 1 1 calc R C70 C 0.4499(4) 0.5900(7) 0.5184(3) 0.018(2) Uani 1 1 d . H70 H 0.4386 0.6484 0.5037 0.021 Uiso 1 1 calc R C83 C 0.5136(5) 0.9868(7) 0.4784(5) 0.023(2) Uani 1 1 d . C55 C 0.6688(3) 0.6156(7) 0.7810(3) 0.022(2) Uani 1 1 d . H55 H 0.6841 0.6774 0.7870 0.026 Uiso 1 1 calc R C30 C 0.8077(4) 1.0155(7) 0.5605(4) 0.027(3) Uani 1 1 d . H30 H 0.8281 1.0770 0.5673 0.033 Uiso 1 1 calc R C87 C 0.7086(4) 0.6171(7) 0.5531(3) 0.021(2) Uani 1 1 d . C23 C 0.7840(3) 0.9977(5) 0.4040(5) 0.015(2) Uani 1 1 d . C42 C 0.4345(4) 0.5002(6) 0.7240(5) 0.023(3) Uani 1 1 d . H42 H 0.4003 0.4991 0.7433 0.028 Uiso 1 1 calc R C79 C 0.5511(4) 1.1204(7) 0.4424(3) 0.024(2) Uani 1 1 d . C57 C 0.5868(4) 0.6948(7) 0.7351(4) 0.020(2) Uani 1 1 d . H57 H 0.5537 0.6737 0.7141 0.023 Uiso 1 1 calc R C74 C 0.3981(3) 0.7415(7) 0.5816(4) 0.027(2) Uani 1 1 d . H74A H 0.4073 0.7618 0.5482 0.040 Uiso 1 1 calc GR H74B H 0.3958 0.7976 0.6029 0.040 Uiso 1 1 calc GR H74C H 0.3608 0.7080 0.5818 0.040 Uiso 1 1 calc GR C24 C 0.8023(3) 1.0838(6) 0.4253(3) 0.0161(18) Uani 1 1 d . C72 C 0.4458(3) 0.6745(6) 0.6003(4) 0.023(2) Uani 1 1 d . H72 H 0.4330 0.6509 0.6330 0.027 Uiso 1 1 calc R C62 C 0.4976(3) 0.3230(6) 0.5853(3) 0.017(2) Uani 1 1 d . H62 H 0.5241 0.3365 0.6134 0.021 Uiso 1 1 calc R C28 C 0.8096(3) 1.0875(6) 0.4760(3) 0.0175(19) Uani 1 1 d . H28 H 0.8217 1.1457 0.4904 0.021 Uiso 1 1 calc R C39 C 0.5333(4) 0.4989(5) 0.6683(4) 0.010(2) Uani 1 1 d . C51 C 0.6977(3) 0.5360(7) 0.7992(3) 0.015(2) Uani 1 1 d . C86 C 0.6015(3) 0.6095(7) 0.5235(3) 0.0282(13) Uani 1 1 d . H86A H 0.5734 0.5572 0.5223 0.042 Uiso 1 1 calc GR H86B H 0.5990 0.6470 0.4934 0.042 Uiso 1 1 calc GR H86C H 0.5930 0.6506 0.5516 0.042 Uiso 1 1 calc GR C26 C 0.8589(3) 1.2396(6) 0.4142(4) 0.027(2) Uani 1 1 d . H26A H 0.8636 1.2936 0.3918 0.041 Uiso 1 1 calc GR H26B H 0.8959 1.2061 0.4176 0.041 Uiso 1 1 calc GR H26C H 0.8464 1.2631 0.4462 0.041 Uiso 1 1 calc GR C25 C 0.8135(4) 1.1717(6) 0.3941(3) 0.022(2) Uani 1 1 d . H25 H 0.8284 1.1484 0.3619 0.027 Uiso 1 1 calc R C78 C 0.6578(3) 1.1084(6) 0.4719(3) 0.0245(13) Uani 1 1 d . H78A H 0.6844 1.0539 0.4725 0.037 Uiso 1 1 calc GR H78B H 0.6616 1.1445 0.5024 0.037 Uiso 1 1 calc GR H78C H 0.6675 1.1497 0.4442 0.037 Uiso 1 1 calc GR C84 C 0.4719(3) 0.9133(7) 0.4965(3) 0.027(2) Uani 1 1 d . H84A H 0.4434 0.8993 0.4709 0.040 Uiso 1 1 calc GR H84B H 0.4519 0.9375 0.5256 0.040 Uiso 1 1 calc GR H84C H 0.4931 0.8550 0.5049 0.040 Uiso 1 1 calc GR C67 C 0.4534(4) 0.5194(8) 0.4331(4) 0.030(2) Uani 1 1 d . H67 H 0.4336 0.5811 0.4255 0.036 Uiso 1 1 calc R C65 C 0.4762(3) 0.4253(6) 0.5109(3) 0.018(2) Uani 1 1 d . H65 H 0.4823 0.3707 0.4910 0.022 Uiso 1 1 calc R C93 C 0.6816(4) 0.4838(7) 0.5086(4) 0.015(2) Uani 1 1 d . C71 C 0.4557(3) 0.5871(6) 0.5684(3) 0.017(2) Uani 1 1 d . C5 C 0.8219(4) 0.9863(7) 0.2700(4) 0.021(2) Uani 1 1 d . H5 H 0.8559 0.9831 0.2504 0.025 Uiso 1 1 calc R C52 C 0.7536(3) 0.5488(7) 0.8283(3) 0.020(2) Uani 1 1 d . H52 H 0.7625 0.6185 0.8295 0.024 Uiso 1 1 calc R C63 C 0.4424(4) 0.2776(7) 0.6059(4) 0.025(2) Uani 1 1 d . H63A H 0.4243 0.3214 0.6292 0.038 Uiso 1 1 calc GR H63B H 0.4523 0.2179 0.6224 0.038 Uiso 1 1 calc GR H63C H 0.4153 0.2645 0.5791 0.038 Uiso 1 1 calc GR C89 C 0.7593(3) 0.5607(7) 0.5442(3) 0.022(2) Uani 1 1 d . C81 C 0.4988(3) 1.0671(7) 0.4507(3) 0.021(2) Uani 1 1 d . C85 C 0.6609(3) 0.5700(7) 0.5285(3) 0.022(2) Uani 1 1 d . C32 C 0.8454(4) 0.9348(9) 0.5815(3) 0.043(3) Uani 1 1 d . H32A H 0.8263 0.8734 0.5755 0.065 Uiso 1 1 calc GR H32B H 0.8503 0.9442 0.6167 0.065 Uiso 1 1 calc GR H32C H 0.8834 0.9353 0.5655 0.065 Uiso 1 1 calc GR C37 C 0.7263(4) 0.7526(7) 0.4434(3) 0.027(2) Uani 1 1 d . H37A H 0.7517 0.7292 0.4695 0.040 Uiso 1 1 calc GR H37B H 0.7120 0.6986 0.4241 0.040 Uiso 1 1 calc GR H37C H 0.6933 0.7866 0.4578 0.040 Uiso 1 1 calc GR C82 C 0.4393(3) 1.0982(6) 0.4372(3) 0.0245(13) Uani 1 1 d . H82A H 0.4410 1.1388 0.4081 0.037 Uiso 1 1 calc GR H82B H 0.4222 1.1342 0.4644 0.037 Uiso 1 1 calc GR H82C H 0.4153 1.0421 0.4303 0.037 Uiso 1 1 calc GR C91 C 0.7439(4) 0.4781(8) 0.5182(5) 0.023(2) Uani 1 1 d . C1 C 0.6297(4) 0.9896(6) 0.3766(4) 0.018(2) Uani 1 1 d . C49 C 0.6523(4) 0.2614(7) 0.7424(4) 0.031(2) Uani 1 1 d . H49A H 0.6789 0.2851 0.7173 0.047 Uiso 1 1 calc GR H49B H 0.6359 0.2003 0.7319 0.047 Uiso 1 1 calc GR H49C H 0.6735 0.2526 0.7731 0.047 Uiso 1 1 calc GR C21 C 0.6222(5) 1.2324(8) 0.2886(5) 0.055(4) Uani 1 1 d . H21A H 0.5862 1.2505 0.2720 0.082 Uiso 1 1 calc GR H21B H 0.6423 1.2899 0.2999 0.082 Uiso 1 1 calc GR H21C H 0.6131 1.1916 0.3166 0.082 Uiso 1 1 calc GR C61 C 0.4836(3) 0.4179(6) 0.5607(3) 0.0164(19) Uani 1 1 d . C13 C 0.5785(4) 0.9130(7) 0.2147(3) 0.020(2) Uani 1 1 d . H13 H 0.5593 0.8553 0.2064 0.024 Uiso 1 1 calc R C9 C 0.6315(3) 0.9088(7) 0.2386(4) 0.018(2) Uani 1 1 d . C36 C 0.8160(4) 0.7726(7) 0.3944(4) 0.028(2) Uani 1 1 d . H36A H 0.8368 0.8147 0.3718 0.042 Uiso 1 1 calc GR H36B H 0.8070 0.7124 0.3779 0.042 Uiso 1 1 calc GR H36C H 0.8403 0.7599 0.4230 0.042 Uiso 1 1 calc GR C15 C 0.4946(4) 1.0036(6) 0.1756(4) 0.025(2) Uani 1 1 d . H15 H 0.4762 1.0659 0.1843 0.030 Uiso 1 1 calc R C92 C 0.7842(4) 0.4021(7) 0.4999(3) 0.026(2) Uani 1 1 d . H92A H 0.8181 0.3981 0.5215 0.039 Uiso 1 1 calc GR H92B H 0.7970 0.4180 0.4667 0.039 Uiso 1 1 calc GR H92C H 0.7640 0.3407 0.4995 0.039 Uiso 1 1 calc GR C64 C 0.5280(4) 0.2509(7) 0.5522(3) 0.026(2) Uani 1 1 d . H64A H 0.5399 0.1955 0.5715 0.039 Uiso 1 1 calc GR H64B H 0.5622 0.2805 0.5373 0.039 Uiso 1 1 calc GR H64C H 0.5012 0.2303 0.5264 0.039 Uiso 1 1 calc GR C31 C 0.7496(4) 1.0185(8) 0.5872(5) 0.043(3) Uani 1 1 d . H31A H 0.7272 1.0735 0.5758 0.065 Uiso 1 1 calc GR H31B H 0.7564 1.0241 0.6224 0.065 Uiso 1 1 calc GR H31C H 0.7280 0.9598 0.5804 0.065 Uiso 1 1 calc GR C80 C 0.5543(4) 1.2113(7) 0.4135(4) 0.0245(13) Uani 1 1 d . H80A H 0.5949 1.2259 0.4060 0.037 Uiso 1 1 calc GR H80B H 0.5375 1.2635 0.4326 0.037 Uiso 1 1 calc GR H80C H 0.5326 1.2038 0.3829 0.037 Uiso 1 1 calc GR C69 C 0.5125(5) 0.5193(8) 0.4071(5) 0.040(3) Uani 1 1 d . H69A H 0.5317 0.4578 0.4123 0.060 Uiso 1 1 calc GR H69B H 0.5368 0.5705 0.4203 0.060 Uiso 1 1 calc GR H69C H 0.5067 0.5295 0.3720 0.060 Uiso 1 1 calc GR C19 C 0.6344(3) 1.0826(7) 0.2389(4) 0.021(2) Uani 1 1 d . C41 C 0.4881(4) 0.5059(6) 0.7466(5) 0.022(3) Uani 1 1 d . H41 H 0.4903 0.5110 0.7811 0.026 Uiso 1 1 calc R N2 N 0.5837(3) 0.4981(5) 0.6402(3) 0.014(2) Uani 1 1 d . C12 C 0.6131(4) 0.7381(7) 0.2677(4) 0.040(3) Uani 1 1 d . H12A H 0.5893 0.7649 0.2939 0.060 Uiso 1 1 calc GR H12B H 0.6337 0.6818 0.2797 0.060 Uiso 1 1 calc GR H12C H 0.5881 0.7199 0.2402 0.060 Uiso 1 1 calc GR C17 C 0.4530(4) 0.9261(7) 0.1902(3) 0.032(2) Uani 1 1 d . H17A H 0.4148 0.9390 0.1758 0.049 Uiso 1 1 calc GR H17B H 0.4496 0.9245 0.2259 0.049 Uiso 1 1 calc GR H17C H 0.4674 0.8645 0.1785 0.049 Uiso 1 1 calc GR C68 C 0.4163(4) 0.4389(9) 0.4128(4) 0.050(3) Uani 1 1 d . H68A H 0.4055 0.4534 0.3790 0.075 Uiso 1 1 calc GR H68B H 0.3812 0.4321 0.4327 0.075 Uiso 1 1 calc GR H68C H 0.4384 0.3792 0.4137 0.075 Uiso 1 1 calc GR C10 C 0.6572(4) 0.8129(7) 0.2505(4) 0.027(2) Uani 1 1 d . H10 H 0.6850 0.8228 0.2781 0.032 Uiso 1 1 calc R C59 C 0.5616(4) 0.7538(8) 0.7776(4) 0.040(3) Uani 1 1 d . H59A H 0.5374 0.7127 0.7982 0.060 Uiso 1 1 calc GR H59B H 0.5380 0.8059 0.7645 0.060 Uiso 1 1 calc GR H59C H 0.5934 0.7802 0.7971 0.060 Uiso 1 1 calc GR C73 C 0.5019(3) 0.7294(7) 0.6081(4) 0.029(2) Uani 1 1 d . H73A H 0.5157 0.7545 0.5768 0.044 Uiso 1 1 calc GR H73B H 0.5313 0.6868 0.6220 0.044 Uiso 1 1 calc GR H73C H 0.4949 0.7824 0.6307 0.044 Uiso 1 1 calc GR C76 C 0.6083(4) 0.9187(7) 0.5191(3) 0.029(2) Uani 1 1 d . H76A H 0.5900 0.8556 0.5178 0.043 Uiso 1 1 calc GR H76B H 0.6089 0.9414 0.5529 0.043 Uiso 1 1 calc GR H76C H 0.6481 0.9142 0.5068 0.043 Uiso 1 1 calc GR C66 C 0.4597(4) 0.5118(7) 0.4885(4) 0.021(2) Uani 1 1 d . C14 C 0.5527(4) 0.9988(6) 0.2023(4) 0.021(3) Uani 1 1 d . C4 C 0.8266(4) 0.9876(7) 0.3210(5) 0.020(2) Uani 1 1 d . H4 H 0.8639 0.9862 0.3357 0.024 Uiso 1 1 calc R C20 C 0.6618(4) 1.1774(7) 0.2526(4) 0.024(2) Uani 1 1 d . H20 H 0.6990 1.1633 0.2701 0.029 Uiso 1 1 calc R C53 C 0.7469(4) 0.5135(7) 0.8809(5) 0.024(3) Uani 1 1 d . H53A H 0.7154 0.5485 0.8969 0.037 Uiso 1 1 calc GR H53B H 0.7832 0.5243 0.8988 0.037 Uiso 1 1 calc GR H53C H 0.7379 0.4453 0.8808 0.037 Uiso 1 1 calc GR C18 C 0.5812(4) 1.0826(7) 0.2142(3) 0.020(2) Uani 1 1 d . H18 H 0.5642 1.1418 0.2053 0.024 Uiso 1 1 calc R C58 C 0.6277(4) 0.7544(7) 0.7035(4) 0.037(3) Uani 1 1 d . H58A H 0.6598 0.7780 0.7235 0.056 Uiso 1 1 calc GR H58B H 0.6064 0.8085 0.6897 0.056 Uiso 1 1 calc GR H58C H 0.6431 0.7149 0.6769 0.056 Uiso 1 1 calc GR C22 C 0.6764(5) 1.2391(9) 0.2087(4) 0.050(3) Uani 1 1 d . H22A H 0.6405 1.2585 0.1924 0.075 Uiso 1 1 calc GR H22B H 0.7006 1.2027 0.1859 0.075 Uiso 1 1 calc GR H22C H 0.6976 1.2959 0.2196 0.075 Uiso 1 1 calc GR C8 C 0.6590(4) 0.9945(6) 0.2507(4) 0.017(2) Uani 1 1 d . C90 C 0.8201(3) 0.5886(7) 0.5577(3) 0.0282(13) Uani 1 1 d . H90A H 0.8194 0.6270 0.5876 0.042 Uiso 1 1 calc GR H90B H 0.8373 0.6260 0.5312 0.042 Uiso 1 1 calc GR H90C H 0.8434 0.5311 0.5632 0.042 Uiso 1 1 calc GR C54 C 0.8043(4) 0.4993(7) 0.8035(3) 0.028(2) Uani 1 1 d . H54A H 0.7965 0.4307 0.8016 0.042 Uiso 1 1 calc GR H54B H 0.8397 0.5103 0.8224 0.042 Uiso 1 1 calc GR H54C H 0.8091 0.5249 0.7704 0.042 Uiso 1 1 calc GR C11 C 0.6922(4) 0.7750(8) 0.2076(5) 0.046(3) Uani 1 1 d . H11A H 0.6667 0.7674 0.1792 0.069 Uiso 1 1 calc GR H11B H 0.7091 0.7132 0.2163 0.069 Uiso 1 1 calc GR H11C H 0.7233 0.8201 0.1997 0.069 Uiso 1 1 calc GR C3 C 0.7772(4) 0.9911(6) 0.3507(4) 0.014(2) Uani 1 1 d . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 I3 0.0184(3) 0.0305(5) 0.0172(5) -0.0003(3) -0.0033(3) -0.0015(3) I4 0.0325(3) 0.0203(4) 0.0250(3) 0.0004(3) -0.0010(3) 0.0013(3) I1 0.0187(3) 0.0348(5) 0.0163(5) -0.0003(3) -0.0030(3) 0.0042(2) I2 0.0340(3) 0.0202(3) 0.0318(4) 0.0016(4) -0.0004(3) -0.0018(3) Co2 0.0126(6) 0.0203(7) 0.0135(8) 0.0010(6) 0.0009(5) -0.0012(5) Co1 0.0123(6) 0.0208(7) 0.0151(8) 0.0003(7) 0.0007(5) -0.0009(5) N1 0.014(4) 0.017(5) 0.014(5) 0.001(3) 0.003(4) 0.002(3) C44 0.016(5) 0.012(6) 0.020(6) 0.000(4) 0.006(4) -0.001(4) C45 0.019(5) 0.023(6) 0.009(5) -0.002(4) 0.000(4) -0.003(4) C43 0.013(5) 0.029(7) 0.028(7) 0.005(4) -0.002(5) -0.005(4) C6 0.024(5) 0.020(6) 0.014(6) -0.003(4) 0.007(5) 0.004(4) C38 0.021(5) 0.011(5) 0.007(5) 0.003(3) -0.006(4) 0.003(4) C60 0.005(4) 0.022(7) 0.012(5) 0.000(4) 0.003(4) 0.003(3) C16 0.030(6) 0.024(7) 0.016(7) 0.003(4) -0.009(4) -0.001(4) C29 0.021(5) 0.019(6) 0.017(5) -0.002(4) -0.004(4) -0.005(4) C47 0.026(5) 0.025(6) 0.019(5) 0.006(4) -0.002(4) 0.002(4) C2 0.009(4) 0.019(6) 0.025(7) -0.001(4) 0.006(5) 0.000(3) C7 0.019(5) 0.018(6) 0.012(6) -0.002(4) -0.002(4) -0.001(4) C34 0.014(4) 0.016(5) 0.016(5) 0.002(4) -0.004(4) 0.000(4) C88 0.027(3) 0.028(3) 0.030(3) 0.001(3) -0.003(2) -0.002(2) C40 0.018(5) 0.017(6) 0.017(6) -0.001(4) 0.004(4) 0.000(4) C75 0.017(4) 0.026(6) 0.016(6) 0.000(4) -0.002(4) -0.005(4) C46 0.023(4) 0.016(5) 0.013(5) 0.002(4) -0.002(4) -0.005(4) C94 0.023(5) 0.033(6) 0.019(5) 0.001(4) -0.005(4) -0.011(4) C77 0.016(4) 0.028(6) 0.018(5) -0.008(4) 0.000(4) 0.009(4) C48 0.033(6) 0.036(7) 0.028(6) 0.008(5) 0.002(4) -0.001(5) C33 0.014(4) 0.020(5) 0.023(5) 0.001(4) -0.001(4) -0.001(4) C27 0.031(5) 0.017(5) 0.025(5) 0.012(4) -0.006(4) -0.002(4) C50 0.020(5) 0.032(6) 0.017(5) 0.004(5) -0.006(4) 0.002(4) C56 0.015(4) 0.018(5) 0.016(5) -0.001(4) 0.001(4) -0.002(4) C35 0.020(4) 0.018(5) 0.023(5) 0.004(5) -0.005(4) -0.001(4) C70 0.015(4) 0.019(5) 0.019(5) 0.007(4) 0.001(4) 0.007(4) C83 0.022(5) 0.030(6) 0.017(6) 0.007(5) 0.005(5) -0.004(4) C55 0.016(4) 0.028(6) 0.021(5) -0.006(4) -0.003(4) 0.001(4) C30 0.033(6) 0.028(6) 0.021(6) 0.003(5) -0.003(4) -0.015(5) C87 0.019(4) 0.026(6) 0.018(5) 0.004(4) -0.002(4) -0.008(4) C23 0.007(4) 0.016(6) 0.023(6) 0.002(4) -0.005(4) 0.000(3) C42 0.014(5) 0.025(6) 0.030(7) -0.002(4) 0.009(5) 0.000(4) C79 0.023(5) 0.023(6) 0.024(5) -0.008(4) 0.008(4) 0.002(4) C57 0.017(4) 0.014(5) 0.027(5) -0.006(4) -0.006(4) 0.007(4) C74 0.020(5) 0.024(6) 0.036(6) -0.004(5) -0.001(4) 0.004(4) C24 0.009(4) 0.018(5) 0.021(4) -0.001(4) 0.003(3) 0.000(3) C72 0.021(4) 0.017(5) 0.030(5) 0.005(5) -0.003(5) 0.002(4) C62 0.018(4) 0.021(5) 0.013(5) 0.001(4) -0.004(4) 0.001(4) C28 0.017(4) 0.015(5) 0.021(5) -0.007(4) -0.003(4) -0.001(4) C39 0.009(4) 0.010(5) 0.011(5) -0.003(3) -0.002(4) -0.004(3) C51 0.014(4) 0.019(5) 0.012(4) -0.001(4) -0.005(4) -0.001(4) C86 0.027(3) 0.028(3) 0.030(3) 0.001(3) -0.003(2) -0.002(2) C26 0.026(5) 0.024(5) 0.033(6) 0.001(5) 0.006(5) -0.008(4) C25 0.026(5) 0.022(5) 0.019(5) -0.002(4) 0.000(4) -0.002(4) C78 0.023(3) 0.026(3) 0.025(3) -0.003(3) 0.006(2) 0.003(2) C84 0.016(4) 0.045(7) 0.019(5) 0.002(5) 0.006(4) -0.005(4) C67 0.035(5) 0.045(7) 0.011(5) 0.000(5) -0.006(4) 0.007(5) C65 0.015(4) 0.019(5) 0.020(5) -0.006(4) -0.003(4) 0.005(4) C93 0.016(4) 0.021(5) 0.009(5) 0.003(4) 0.001(4) -0.004(4) C71 0.012(4) 0.015(5) 0.023(5) 0.003(4) -0.002(4) -0.002(4) C5 0.018(5) 0.032(6) 0.013(6) -0.009(4) 0.004(4) -0.001(4) C52 0.016(4) 0.023(6) 0.022(5) -0.001(4) -0.001(4) 0.001(4) C63 0.024(5) 0.021(6) 0.031(6) 0.003(5) 0.010(4) 0.004(4) C89 0.016(4) 0.032(6) 0.018(5) 0.006(4) 0.002(4) -0.003(4) C81 0.012(4) 0.036(6) 0.015(5) -0.008(4) 0.005(4) -0.002(4) C85 0.015(4) 0.031(6) 0.019(5) 0.007(4) 0.004(4) -0.002(4) C32 0.034(5) 0.071(9) 0.025(6) 0.003(6) -0.010(5) 0.010(6) C37 0.037(5) 0.016(5) 0.028(5) 0.000(4) 0.004(4) -0.012(4) C82 0.023(3) 0.026(3) 0.025(3) -0.003(3) 0.006(2) 0.003(2) C91 0.013(5) 0.033(6) 0.023(6) 0.007(5) 0.002(4) -0.003(4) C1 0.020(5) 0.018(6) 0.017(6) -0.005(4) -0.006(5) 0.002(4) C49 0.040(5) 0.023(5) 0.031(5) -0.003(5) -0.005(5) 0.000(4) C21 0.062(8) 0.044(7) 0.058(8) -0.025(6) 0.025(7) -0.024(6) C61 0.009(4) 0.021(5) 0.019(5) 0.000(4) 0.003(4) -0.002(4) C13 0.024(5) 0.020(5) 0.015(5) 0.001(4) 0.002(4) 0.000(4) C9 0.020(4) 0.023(6) 0.011(5) 0.001(4) 0.004(4) 0.004(4) C36 0.026(5) 0.028(6) 0.030(6) -0.003(5) 0.002(5) 0.003(4) C15 0.024(5) 0.028(6) 0.021(5) -0.003(4) -0.003(4) 0.002(4) C92 0.024(5) 0.035(6) 0.020(5) 0.001(4) 0.001(4) 0.007(4) C64 0.028(5) 0.019(5) 0.030(5) 0.006(4) 0.004(4) 0.000(4) C31 0.057(8) 0.061(8) 0.012(6) -0.004(6) -0.007(5) 0.026(6) C80 0.023(3) 0.026(3) 0.025(3) -0.003(3) 0.006(2) 0.003(2) C69 0.051(6) 0.048(7) 0.022(7) -0.004(6) 0.007(6) -0.005(5) C19 0.023(5) 0.028(6) 0.011(5) -0.004(4) 0.003(4) -0.008(4) C41 0.019(5) 0.030(7) 0.016(6) -0.001(4) 0.001(5) 0.000(4) N2 0.016(4) 0.013(5) 0.012(5) -0.001(3) -0.007(4) -0.002(3) C12 0.043(6) 0.028(6) 0.050(7) 0.007(5) -0.012(5) -0.002(5) C17 0.019(5) 0.053(7) 0.025(5) 0.001(5) 0.000(4) -0.006(5) C68 0.037(6) 0.088(10) 0.025(6) -0.007(7) -0.009(5) -0.018(6) C10 0.032(5) 0.018(5) 0.031(6) -0.006(5) -0.013(5) 0.001(4) C59 0.049(7) 0.040(7) 0.031(6) -0.012(5) -0.007(5) 0.016(5) C73 0.027(5) 0.021(6) 0.039(6) -0.007(5) -0.011(4) 0.004(4) C76 0.027(5) 0.039(7) 0.021(5) 0.002(5) -0.007(4) 0.001(4) C66 0.014(5) 0.030(6) 0.020(6) 0.001(4) -0.002(4) 0.003(4) C14 0.015(4) 0.035(8) 0.013(5) 0.003(4) 0.003(4) 0.001(4) C4 0.018(5) 0.017(5) 0.024(7) 0.006(4) -0.001(4) -0.002(4) C20 0.030(5) 0.015(5) 0.027(5) 0.006(4) -0.008(4) -0.001(4) C53 0.027(6) 0.025(6) 0.022(7) -0.002(4) -0.006(4) 0.003(4) C18 0.024(5) 0.025(6) 0.012(4) 0.006(4) 0.000(4) 0.000(4) C58 0.038(6) 0.030(6) 0.044(7) 0.003(5) -0.007(5) 0.003(5) C22 0.054(7) 0.045(8) 0.051(8) 0.006(6) -0.003(6) -0.025(6) C8 0.020(5) 0.014(6) 0.017(6) 0.001(4) 0.005(4) 0.007(4) C90 0.027(3) 0.028(3) 0.030(3) 0.001(3) -0.003(2) -0.002(2) C54 0.016(4) 0.046(7) 0.023(5) -0.005(4) -0.005(4) 0.005(4) C11 0.037(6) 0.032(7) 0.069(9) -0.009(6) 0.006(6) 0.009(5) C3 0.015(5) 0.008(5) 0.019(6) -0.001(4) -0.005(4) 0.000(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' I I -0.4742 1.8119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle I3 Co2 I4 92.88(5) C38 Co2 I3 88.6(3) C38 Co2 I4 90.3(2) C38 Co2 C87 106.0(3) C38 Co2 C93 113.0(4) C38 Co2 C89 145.2(4) C38 Co2 C85 90.9(4) C38 Co2 C91 153.9(4) C87 Co2 I3 98.6(2) C87 Co2 I4 160.2(3) C87 Co2 C89 39.8(3) C87 Co2 C85 40.8(3) C87 Co2 C91 67.3(4) C93 Co2 I3 156.7(2) C93 Co2 I4 95.4(3) C93 Co2 C87 68.1(4) C93 Co2 C89 66.7(4) C93 Co2 C85 39.7(3) C93 Co2 C91 40.9(4) C89 Co2 I3 90.8(3) C89 Co2 I4 124.5(3) C85 Co2 I3 137.1(3) C85 Co2 I4 130.1(3) C85 Co2 C89 66.6(3) C85 Co2 C91 67.3(4) C91 Co2 I3 117.1(3) C91 Co2 I4 93.1(3) C91 Co2 C89 38.7(4) I1 Co1 I2 92.58(5) C75 Co1 I1 155.0(3) C75 Co1 I2 94.1(3) C75 Co1 C77 40.4(3) C75 Co1 C83 39.6(4) C75 Co1 C81 66.5(4) C77 Co1 I1 137.8(3) C77 Co1 I2 129.6(3) C77 Co1 C83 66.2(4) C77 Co1 C81 66.4(3) C83 Co1 I1 116.1(3) C83 Co1 I2 92.8(3) C83 Co1 C81 38.4(4) C79 Co1 I1 99.9(3) C79 Co1 I2 158.5(3) C79 Co1 C75 67.5(4) C79 Co1 C77 39.8(3) C79 Co1 C83 66.1(4) C79 Co1 C81 39.9(3) C81 Co1 I1 89.9(2) C81 Co1 I2 123.6(3) C1 Co1 I1 89.1(3) C1 Co1 I2 90.6(3) C1 Co1 C75 114.9(4) C1 Co1 C77 92.4(4) C1 Co1 C83 154.4(5) C1 Co1 C79 106.8(4) C1 Co1 C81 145.8(4) C1 N1 C2 175.1(10) C43 C44 C60 119.9(9) C39 C44 C43 117.3(11) C39 C44 C60 122.6(9) C46 C45 C40 119.9(8) C56 C45 C40 119.4(8) C56 C45 C46 120.7(8) C44 C43 H43 119.3 C42 C43 C44 121.5(10) C42 C43 H43 119.3 C7 C6 H6 119.4 C5 C6 H6 119.4 C5 C6 C7 121.2(11) N2 C38 Co2 179.2(9) C71 C60 C44 118.8(8) C71 C60 C61 120.0(10) C61 C60 C44 121.2(8) H16A C16 H16B 109.5 H16A C16 H16C 109.5 H16B C16 H16C 109.5 C15 C16 H16A 109.5 C15 C16 H16B 109.5 C15 C16 H16C 109.5 C33 C29 C30 121.8(9) C33 C29 C28 117.3(10) C28 C29 C30 120.9(8) C46 C47 H47 107.7 C46 C47 C48 111.5(8) C46 C47 C49 112.3(7) C48 C47 H47 107.7 C49 C47 H47 107.7 C49 C47 C48 109.7(8) C7 C2 N1 118.7(9) C7 C2 C3 124.1(10) C3 C2 N1 117.2(11) C6 C7 C8 120.0(10) C2 C7 C6 117.3(9) C2 C7 C8 122.7(9) C33 C34 C35 119.8(9) C33 C34 C23 119.0(9) C23 C34 C35 121.0(9) H88A C88 H88B 109.5 H88A C88 H88C 109.5 H88B C88 H88C 109.5 C87 C88 H88A 109.5 C87 C88 H88B 109.5 C87 C88 H88C 109.5 C39 C40 C45 122.6(9) C41 C40 C45 118.9(11) C41 C40 C39 118.4(10) C77 C75 Co1 70.0(6) C77 C75 C76 125.3(8) C83 C75 Co1 71.8(7) C83 C75 C77 106.7(8) C83 C75 C76 127.7(9) C76 C75 Co1 128.5(7) C45 C46 C47 120.3(8) C50 C46 C45 117.1(9) C50 C46 C47 122.6(8) H94A C94 H94B 109.5 H94A C94 H94C 109.5 H94B C94 H94C 109.5 C93 C94 H94A 109.5 C93 C94 H94B 109.5 C93 C94 H94C 109.5 C75 C77 Co1 69.6(6) C75 C77 C78 125.3(8) C79 C77 Co1 69.7(5) C79 C77 C75 108.0(8) C79 C77 C78 126.6(9) C78 C77 Co1 128.3(6) C47 C48 H48A 109.5 C47 C48 H48B 109.5 C47 C48 H48C 109.5 H48A C48 H48B 109.5 H48A C48 H48C 109.5 H48B C48 H48C 109.5 C29 C33 C34 122.2(10) C29 C33 H33 118.9 C34 C33 H33 118.9 H27A C27 H27B 109.5 H27A C27 H27C 109.5 H27B C27 H27C 109.5 C25 C27 H27A 109.5 C25 C27 H27B 109.5 C25 C27 H27C 109.5 C46 C50 H50 118.3 C51 C50 C46 123.3(9) C51 C50 H50 118.3 C45 C56 C55 119.1(9) C45 C56 C57 121.5(8) C55 C56 C57 119.3(8) C34 C35 H35 107.7 C37 C35 C34 114.7(8) C37 C35 H35 107.7 C36 C35 C34 109.3(7) C36 C35 H35 107.7 C36 C35 C37 109.5(8) C71 C70 H70 118.4 C71 C70 C66 123.2(9) C66 C70 H70 118.4 C75 C83 Co1 68.6(6) C75 C83 C84 125.1(10) C84 C83 Co1 128.2(8) C81 C83 Co1 71.1(6) C81 C83 C75 109.5(8) C81 C83 C84 125.3(9) C56 C55 H55 119.5 C51 C55 C56 121.1(9) C51 C55 H55 119.5 C29 C30 H30 107.5 C29 C30 C32 113.1(9) C29 C30 C31 111.4(9) C32 C30 H30 107.5 C31 C30 H30 107.5 C31 C30 C32 109.7(9) C88 C87 Co2 125.9(7) C89 C87 Co2 72.2(5) C89 C87 C88 127.9(8) C89 C87 C85 106.8(8) C85 C87 Co2 69.9(5) C85 C87 C88 125.3(8) C34 C23 C24 120.3(10) C34 C23 C3 119.9(8) C24 C23 C3 119.8(8) C43 C42 H42 119.7 C43 C42 C41 120.7(10) C41 C42 H42 119.6 C77 C79 Co1 70.5(5) C77 C79 C81 108.1(8) C77 C79 C80 127.3(8) C81 C79 Co1 72.1(5) C81 C79 C80 124.6(8) C80 C79 Co1 124.1(7) C56 C57 H57 107.8 C56 C57 C59 111.0(8) C56 C57 C58 110.8(7) C59 C57 H57 107.8 C58 C57 H57 107.8 C58 C57 C59 111.5(8) H74A C74 H74B 109.5 H74A C74 H74C 109.5 H74B C74 H74C 109.5 C72 C74 H74A 109.5 C72 C74 H74B 109.5 C72 C74 H74C 109.5 C23 C24 C25 120.8(8) C28 C24 C23 118.6(9) C28 C24 C25 120.5(8) C74 C72 H72 106.9 C71 C72 C74 114.2(8) C71 C72 H72 106.9 C73 C72 C74 110.2(8) C73 C72 H72 106.9 C73 C72 C71 111.2(7) C63 C62 H62 107.6 C61 C62 H62 107.6 C61 C62 C63 110.5(7) C61 C62 C64 114.4(7) C64 C62 H62 107.6 C64 C62 C63 108.9(7) C29 C28 H28 118.7 C24 C28 C29 122.5(8) C24 C28 H28 118.7 C44 C39 C40 121.8(10) C44 C39 N2 119.3(11) N2 C39 C40 118.9(9) C50 C51 C55 118.7(8) C50 C51 C52 121.5(9) C55 C51 C52 119.8(8) H86A C86 H86B 109.5 H86A C86 H86C 109.5 H86B C86 H86C 109.5 C85 C86 H86A 109.5 C85 C86 H86B 109.5 C85 C86 H86C 109.5 H26A C26 H26B 109.5 H26A C26 H26C 109.5 H26B C26 H26C 109.5 C25 C26 H26A 109.5 C25 C26 H26B 109.5 C25 C26 H26C 109.5 C27 C25 H25 106.8 C24 C25 C27 110.8(7) C24 C25 H25 106.8 C26 C25 C27 110.4(8) C26 C25 C24 114.8(8) C26 C25 H25 106.8 C77 C78 H78A 109.5 C77 C78 H78B 109.5 C77 C78 H78C 109.5 H78A C78 H78B 109.5 H78A C78 H78C 109.5 H78B C78 H78C 109.5 C83 C84 H84A 109.5 C83 C84 H84B 109.5 C83 C84 H84C 109.5 H84A C84 H84B 109.5 H84A C84 H84C 109.5 H84B C84 H84C 109.5 C69 C67 H67 108.0 C68 C67 H67 108.0 C68 C67 C69 109.1(9) C68 C67 C66 111.3(9) C66 C67 H67 108.0 C66 C67 C69 112.1(9) C61 C65 H65 119.1 C61 C65 C66 121.9(9) C66 C65 H65 119.1 C94 C93 Co2 128.1(7) C85 C93 Co2 70.6(6) C85 C93 C94 126.2(8) C85 C93 C91 108.0(9) C91 C93 Co2 71.3(7) C91 C93 C94 125.5(9) C60 C71 C72 119.5(8) C70 C71 C60 118.4(9) C70 C71 C72 122.1(9) C6 C5 H5 119.9 C6 C5 C4 120.2(10) C4 C5 H5 119.9 C51 C52 H52 107.8 C51 C52 C53 111.5(7) C53 C52 H52 107.8 C54 C52 C51 111.2(7) C54 C52 H52 107.8 C54 C52 C53 110.5(7) C62 C63 H63A 109.5 C62 C63 H63B 109.5 C62 C63 H63C 109.5 H63A C63 H63B 109.5 H63A C63 H63C 109.5 H63B C63 H63C 109.5 C87 C89 Co2 67.9(5) C87 C89 C90 125.2(9) C91 C89 Co2 70.2(6) C91 C89 C87 109.6(8) C91 C89 C90 125.1(8) C90 C89 Co2 131.4(6) C83 C81 Co1 70.4(6) C83 C81 C79 107.5(8) C83 C81 C82 126.5(8) C79 C81 Co1 68.0(5) C79 C81 C82 125.6(9) C82 C81 Co1 132.2(6) C87 C85 Co2 69.2(5) C87 C85 C86 124.9(9) C86 C85 Co2 129.0(6) C93 C85 Co2 69.7(6) C93 C85 C87 108.3(7) C93 C85 C86 126.7(8) C30 C32 H32A 109.5 C30 C32 H32B 109.5 C30 C32 H32C 109.5 H32A C32 H32B 109.5 H32A C32 H32C 109.5 H32B C32 H32C 109.5 C35 C37 H37A 109.5 C35 C37 H37B 109.5 C35 C37 H37C 109.5 H37A C37 H37B 109.5 H37A C37 H37C 109.5 H37B C37 H37C 109.5 C81 C82 H82A 109.5 C81 C82 H82B 109.5 C81 C82 H82C 109.5 H82A C82 H82B 109.5 H82A C82 H82C 109.5 H82B C82 H82C 109.5 C93 C91 Co2 67.8(6) C93 C91 C92 126.0(10) C89 C91 Co2 71.2(6) C89 C91 C93 107.1(9) C89 C91 C92 126.8(8) C92 C91 Co2 129.8(8) N1 C1 Co1 177.9(10) C47 C49 H49A 109.5 C47 C49 H49B 109.5 C47 C49 H49C 109.5 H49A C49 H49B 109.5 H49A C49 H49C 109.5 H49B C49 H49C 109.5 H21A C21 H21B 109.5 H21A C21 H21C 109.5 H21B C21 H21C 109.5 C20 C21 H21A 109.5 C20 C21 H21B 109.5 C20 C21 H21C 109.5 C60 C61 C62 119.3(8) C65 C61 C60 118.6(8) C65 C61 C62 121.9(8) C9 C13 H13 119.0 C14 C13 H13 119.0 C14 C13 C9 122.1(9) C13 C9 C10 119.1(8) C13 C9 C8 118.2(9) C8 C9 C10 122.6(8) C35 C36 H36A 109.5 C35 C36 H36B 109.5 C35 C36 H36C 109.5 H36A C36 H36B 109.5 H36A C36 H36C 109.5 H36B C36 H36C 109.5 C16 C15 H15 107.3 C17 C15 C16 110.4(7) C17 C15 H15 107.3 C17 C15 C14 113.6(8) C14 C15 C16 110.7(7) C14 C15 H15 107.3 C91 C92 H92A 109.5 C91 C92 H92B 109.5 C91 C92 H92C 109.5 H92A C92 H92B 109.5 H92A C92 H92C 109.5 H92B C92 H92C 109.5 C62 C64 H64A 109.5 C62 C64 H64B 109.5 C62 C64 H64C 109.5 H64A C64 H64B 109.5 H64A C64 H64C 109.5 H64B C64 H64C 109.5 C30 C31 H31A 109.5 C30 C31 H31B 109.5 C30 C31 H31C 109.5 H31A C31 H31B 109.5 H31A C31 H31C 109.5 H31B C31 H31C 109.5 C79 C80 H80A 109.5 C79 C80 H80B 109.5 C79 C80 H80C 109.5 H80A C80 H80B 109.5 H80A C80 H80C 109.5 H80B C80 H80C 109.5 C67 C69 H69A 109.5 C67 C69 H69B 109.5 C67 C69 H69C 109.5 H69A C69 H69B 109.5 H69A C69 H69C 109.5 H69B C69 H69C 109.5 C18 C19 C20 118.9(9) C8 C19 C20 123.3(8) C8 C19 C18 117.8(9) C40 C41 C42 120.4(12) C40 C41 H41 119.8 C42 C41 H41 119.8 C38 N2 C39 176.0(9) H12A C12 H12B 109.5 H12A C12 H12C 109.5 H12B C12 H12C 109.5 C10 C12 H12A 109.5 C10 C12 H12B 109.5 C10 C12 H12C 109.5 C15 C17 H17A 109.5 C15 C17 H17B 109.5 C15 C17 H17C 109.5 H17A C17 H17B 109.5 H17A C17 H17C 109.5 H17B C17 H17C 109.5 C67 C68 H68A 109.5 C67 C68 H68B 109.5 C67 C68 H68C 109.5 H68A C68 H68B 109.5 H68A C68 H68C 109.5 H68B C68 H68C 109.5 C9 C10 C12 114.6(8) C9 C10 H10 106.9 C9 C10 C11 110.7(9) C12 C10 H10 106.9 C11 C10 C12 110.4(9) C11 C10 H10 106.9 C57 C59 H59A 109.5 C57 C59 H59B 109.5 C57 C59 H59C 109.5 H59A C59 H59B 109.5 H59A C59 H59C 109.5 H59B C59 H59C 109.5 C72 C73 H73A 109.5 C72 C73 H73B 109.5 C72 C73 H73C 109.5 H73A C73 H73B 109.5 H73A C73 H73C 109.5 H73B C73 H73C 109.5 C75 C76 H76A 109.5 C75 C76 H76B 109.5 C75 C76 H76C 109.5 H76A C76 H76B 109.5 H76A C76 H76C 109.5 H76B C76 H76C 109.5 C70 C66 C67 121.0(9) C70 C66 C65 117.9(10) C65 C66 C67 121.1(9) C13 C14 C15 122.1(8) C13 C14 C18 118.4(9) C18 C14 C15 119.5(8) C5 C4 H4 119.4 C3 C4 C5 121.1(10) C3 C4 H4 119.4 C21 C20 H20 107.5 C19 C20 C21 110.4(8) C19 C20 H20 107.5 C22 C20 C21 110.5(9) C22 C20 C19 113.3(8) C22 C20 H20 107.5 C52 C53 H53A 109.5 C52 C53 H53B 109.5 C52 C53 H53C 109.5 H53A C53 H53B 109.5 H53A C53 H53C 109.5 H53B C53 H53C 109.5 C19 C18 H18 119.0 C14 C18 C19 122.0(9) C14 C18 H18 119.0 C57 C58 H58A 109.5 C57 C58 H58B 109.5 C57 C58 H58C 109.5 H58A C58 H58B 109.5 H58A C58 H58C 109.5 H58B C58 H58C 109.5 C20 C22 H22A 109.5 C20 C22 H22B 109.5 C20 C22 H22C 109.5 H22A C22 H22B 109.5 H22A C22 H22C 109.5 H22B C22 H22C 109.5 C9 C8 C7 119.3(8) C19 C8 C7 119.2(8) C19 C8 C9 121.5(9) C89 C90 H90A 109.5 C89 C90 H90B 109.5 C89 C90 H90C 109.5 H90A C90 H90B 109.5 H90A C90 H90C 109.5 H90B C90 H90C 109.5 C52 C54 H54A 109.5 C52 C54 H54B 109.5 C52 C54 H54C 109.5 H54A C54 H54B 109.5 H54A C54 H54C 109.5 H54B C54 H54C 109.5 C10 C11 H11A 109.5 C10 C11 H11B 109.5 C10 C11 H11C 109.5 H11A C11 H11B 109.5 H11A C11 H11C 109.5 H11B C11 H11C 109.5 C2 C3 C23 124.4(10) C4 C3 C2 116.1(11) C4 C3 C23 119.5(9) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance I3 Co2 2.5682(17) I4 Co2 2.5925(14) I1 Co1 2.5682(18) I2 Co1 2.5944(14) Co2 C38 1.844(10) Co2 C87 2.071(9) Co2 C93 2.068(11) Co2 C89 2.129(9) Co2 C85 2.081(9) Co2 C91 2.115(12) Co1 C75 2.079(11) Co1 C77 2.084(9) Co1 C83 2.122(12) Co1 C79 2.074(9) Co1 C81 2.130(8) Co1 C1 1.837(11) N1 C2 1.429(13) N1 C1 1.136(12) C44 C43 1.397(15) C44 C60 1.508(16) C44 C39 1.390(13) C45 C40 1.502(14) C45 C46 1.439(13) C45 C56 1.394(13) C43 H43 0.9500 C43 C42 1.352(18) C6 H6 0.9500 C6 C7 1.394(14) C6 C5 1.383(15) C38 N2 1.155(12) C60 C71 1.421(12) C60 C61 1.430(12) C16 H16A 0.9800 C16 H16B 0.9800 C16 H16C 0.9800 C16 C15 1.530(17) C29 C33 1.394(13) C29 C30 1.500(16) C29 C28 1.402(13) C47 H47 1.0000 C47 C46 1.509(13) C47 C48 1.557(13) C47 C49 1.530(12) C2 C7 1.388(16) C2 C3 1.413(14) C7 C8 1.508(14) C34 C33 1.398(13) C34 C35 1.527(12) C34 C23 1.407(13) C88 H88A 0.9800 C88 H88B 0.9800 C88 H88C 0.9800 C88 C87 1.488(13) C40 C39 1.402(16) C40 C41 1.375(14) C75 C77 1.439(13) C75 C83 1.424(14) C75 C76 1.506(13) C46 C50 1.386(11) C94 H94A 0.9800 C94 H94B 0.9800 C94 H94C 0.9800 C94 C93 1.504(13) C77 C79 1.414(12) C77 C78 1.492(11) C48 H48A 0.9800 C48 H48B 0.9800 C48 H48C 0.9800 C33 H33 0.9500 C27 H27A 0.9800 C27 H27B 0.9800 C27 H27C 0.9800 C27 C25 1.529(12) C50 H50 0.9500 C50 C51 1.381(13) C56 C55 1.406(11) C56 C57 1.520(12) C35 H35 1.0000 C35 C37 1.525(12) C35 C36 1.515(12) C70 H70 0.9500 C70 C71 1.374(13) C70 C66 1.388(13) C83 C84 1.494(12) C83 C81 1.400(14) C55 H55 0.9500 C55 C51 1.393(12) C30 H30 1.0000 C30 C32 1.538(14) C30 C31 1.526(14) C87 C89 1.432(12) C87 C85 1.448(12) C23 C24 1.407(12) C23 C3 1.472(16) C42 H42 0.9500 C42 C41 1.383(15) C79 C81 1.436(12) C79 C80 1.503(14) C57 H57 1.0000 C57 C59 1.541(13) C57 C58 1.529(13) C74 H74A 0.9800 C74 H74B 0.9800 C74 H74C 0.9800 C74 C72 1.534(11) C24 C28 1.396(12) C24 C25 1.523(12) C72 H72 1.0000 C72 C71 1.523(13) C72 C73 1.521(11) C62 H62 1.0000 C62 C63 1.531(11) C62 C61 1.525(12) C62 C64 1.527(12) C28 H28 0.9500 C39 N2 1.394(13) C51 C52 1.525(11) C86 H86A 0.9800 C86 H86B 0.9800 C86 H86C 0.9800 C86 C85 1.482(11) C26 H26A 0.9800 C26 H26B 0.9800 C26 H26C 0.9800 C26 C25 1.518(11) C25 H25 1.0000 C78 H78A 0.9800 C78 H78B 0.9800 C78 H78C 0.9800 C84 H84A 0.9800 C84 H84B 0.9800 C84 H84C 0.9800 C67 H67 1.0000 C67 C69 1.537(14) C67 C68 1.523(14) C67 C66 1.526(15) C65 H65 0.9500 C65 C61 1.380(12) C65 C66 1.411(13) C93 C85 1.410(13) C93 C91 1.462(12) C5 H5 0.9500 C5 C4 1.401(16) C52 H52 1.0000 C52 C53 1.532(16) C52 C54 1.518(11) C63 H63A 0.9800 C63 H63B 0.9800 C63 H63C 0.9800 C89 C91 1.406(15) C89 C90 1.503(11) C81 C82 1.487(11) C32 H32A 0.9800 C32 H32B 0.9800 C32 H32C 0.9800 C37 H37A 0.9800 C37 H37B 0.9800 C37 H37C 0.9800 C82 H82A 0.9800 C82 H82B 0.9800 C82 H82C 0.9800 C91 C92 1.501(13) C49 H49A 0.9800 C49 H49B 0.9800 C49 H49C 0.9800 C21 H21A 0.9800 C21 H21B 0.9800 C21 H21C 0.9800 C21 C20 1.548(14) C13 H13 0.9500 C13 C9 1.388(12) C13 C14 1.384(12) C9 C10 1.506(13) C9 C8 1.399(13) C36 H36A 0.9800 C36 H36B 0.9800 C36 H36C 0.9800 C15 H15 1.0000 C15 C17 1.505(12) C15 C14 1.526(12) C92 H92A 0.9800 C92 H92B 0.9800 C92 H92C 0.9800 C64 H64A 0.9800 C64 H64B 0.9800 C64 H64C 0.9800 C31 H31A 0.9800 C31 H31B 0.9800 C31 H31C 0.9800 C80 H80A 0.9800 C80 H80B 0.9800 C80 H80C 0.9800 C69 H69A 0.9800 C69 H69B 0.9800 C69 H69C 0.9800 C19 C20 1.520(13) C19 C18 1.400(12) C19 C8 1.397(12) C41 H41 0.9500 C12 H12A 0.9800 C12 H12B 0.9800 C12 H12C 0.9800 C12 C10 1.533(14) C17 H17A 0.9800 C17 H17B 0.9800 C17 H17C 0.9800 C68 H68A 0.9800 C68 H68B 0.9800 C68 H68C 0.9800 C10 H10 1.0000 C10 C11 1.521(15) C59 H59A 0.9800 C59 H59B 0.9800 C59 H59C 0.9800 C73 H73A 0.9800 C73 H73B 0.9800 C73 H73C 0.9800 C76 H76A 0.9800 C76 H76B 0.9800 C76 H76C 0.9800 C14 C18 1.385(12) C4 H4 0.9500 C4 C3 1.399(14) C20 H20 1.0000 C20 C22 1.518(14) C53 H53A 0.9800 C53 H53B 0.9800 C53 H53C 0.9800 C18 H18 0.9500 C58 H58A 0.9800 C58 H58B 0.9800 C58 H58C 0.9800 C22 H22A 0.9800 C22 H22B 0.9800 C22 H22C 0.9800 C90 H90A 0.9800 C90 H90B 0.9800 C90 H90C 0.9800 C54 H54A 0.9800 C54 H54B 0.9800 C54 H54C 0.9800 C11 H11A 0.9800 C11 H11B 0.9800 C11 H11C 0.9800 loop_ _publcif_info_datablock.id _publcif_info_datablock.publ_exptl _publcif_info_datablock.publ_geom _publcif_info_datablock.structure {1065b071-05f6-4bef-907f-e95c921a87e7} y y y