#------------------------------------------------------------------------------ #$Date: 2019-11-26 03:44:49 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242530 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/25/4132586.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132586 loop_ _publ_author_name 'Mokhtarzadeh, Charles C.' 'Moore, Curtis E.' 'Rheingold, Arnold L.' 'Figueroa, Joshua S.' _publ_section_title ; A Highly-Reduced Cobalt Terminal Carbyne: Divergent Metal- and \a-Carbon-Centered Reactivity. ; _journal_issue 26 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 8100 _journal_page_last 8104 _journal_paper_doi 10.1021/jacs.8b05019 _journal_volume 140 _journal_year 2018 _chemical_formula_moiety 'C54 H83 Co K N O Si, C5 H12' _chemical_formula_sum 'C59 H86 Co K N O Si' _chemical_formula_weight 951.40 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary direct _audit_creation_date 2017-04-01 _audit_creation_method ; Olex2 1.2 (compiled Jan 19 2015 12:28:14 for OlexSys, GUI svn.r4998) ; _audit_update_record ; 2017-04-01 # Formatted by publCIF ; _cell_angle_alpha 93.0540(10) _cell_angle_beta 104.8680(10) _cell_angle_gamma 110.9260(10) _cell_formula_units_Z 2 _cell_length_a 12.4898(4) _cell_length_b 12.5227(4) _cell_length_c 20.6102(6) _cell_measurement_reflns_used 9758 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 27.72 _cell_measurement_theta_min 2.18 _cell_volume 2872.39(16) _computing_cell_refinement 'SAINT v8.34A (Bruker, 2013)' _computing_data_collection 'APEX2 v2014.11-0 (Bruker, 2014)' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2008)' _computing_structure_solution 'XT (Sheldrick, 2015)' _diffrn_ambient_temperature 100 _diffrn_detector 'Bruker APEX-II CCD' _diffrn_detector_area_resol_mean 7.9 _diffrn_detector_type 'CCD Area Detector' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device 'Kappa Four-Circle Diffractometer' _diffrn_measurement_device_type 'Bruker APEX II Ultra' _diffrn_measurement_method '\w and \f scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0337 _diffrn_reflns_av_unetI/netI 0.0223 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_number 100317 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.943 _diffrn_reflns_theta_min 1.764 _diffrn_source 'sealed tube' _diffrn_source_type fine-focus _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.429 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.7139 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2014/4 (Bruker,2014) was used for absorption correction. wR2(int) was 0.0744 before and 0.0428 after correction. The Ratio of minimum to maximum transmission is 0.9575. The \l/2 correction factor is 0.00150. ; _exptl_crystal_colour 'metallic light orange' _exptl_crystal_colour_lustre metallic _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary orange _exptl_crystal_density_diffrn 1.100 _exptl_crystal_description plate _exptl_crystal_F_000 1030 _exptl_crystal_size_max 0.98 _exptl_crystal_size_mid 0.052 _exptl_crystal_size_min 0.019 _refine_diff_density_max 0.362 _refine_diff_density_min -0.285 _refine_diff_density_rms 0.047 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.029 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 635 _refine_ls_number_reflns 13771 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.029 _refine_ls_R_factor_all 0.0503 _refine_ls_R_factor_gt 0.0382 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0567P)^2^+0.9462P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1001 _refine_ls_wR_factor_ref 0.1080 _reflns_Friedel_coverage 0.000 _reflns_number_gt 11252 _reflns_number_total 13771 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b05019_si_002.cif _cod_data_source_block JFig1199 _cod_database_code 4132586 _publcif_datablock.id {d85fa9ab-89cd-403d-ac26-cbf861b2cda7} _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Uiso/Uaniso restraints and constraints Uanis(C15A) = Uanis(C15B) Uanis(C16A) = Uanis(C16B) Uanis(C17A) = Uanis(C17B) 3. Others Sof(C16B)=Sof(H16D)=Sof(H16E)=Sof(H16F)=Sof(C15B)=Sof(H15B)=Sof(C17B)= Sof(H17D)=Sof(H17E)=Sof(H17F)=1-FVAR(1) Sof(C15A)=Sof(H15A)=Sof(C16A)=Sof(H16A)=Sof(H16B)=Sof(H16C)=Sof(C17A)= Sof(H17A)=Sof(H17B)=Sof(H17C)=FVAR(1) 4.a Ternary CH refined with riding coordinates: C25(H25), C35(H35), C10(H10), C30(H30), C20(H20), C15A(H15A), C15B(H15B) 4.b Secondary CH2 refined with riding coordinates: C53(H53A,H53B), C57(H57A,H57B), C52(H52A,H52B), C56(H56A,H56B), C58(H58A,H58B) 4.c Aromatic/amide H refined with riding coordinates: C33(H33), C4(H4), C6(H6), C28(H28), C5(H5), C18(H18), C13(H13) 4.d Idealised Me refined as rotating group: C48(H48A,H48B,H48C), C36(H36A,H36B,H36C), C50(H50A,H50B,H50C), C12(H12A,H12B, H12C), C3AA(H3AA,H3AB,H3AC), C49(H49A,H49B,H49C), C45(H45A,H45B,H45C), C31(H31A,H31B,H31C), C37(H37A,H37B,H37C), C26(H26A,H26B,H26C), C46(H46A,H46B, H46C), C32(H32A,H32B,H32C), C43(H43A,H43B,H43C), C47(H47A,H47B,H47C), C22(H22A, H22B,H22C), C27(H27A,H27B,H27C), C51(H51A,H51B,H51C), C21(H21A,H21B,H21C), C16A(H16A,H16B,H16C), C55(H55A,H55B,H55C), C59(H59A,H59B,H59C), C17A(H17A,H17B, H17C), C16B(H16D,H16E,H16F), C17B(H17D,H17E,H17F) ; _shelx_res_file ; jfig1199_1_0m.res created by SHELXL-2014/7 TITL jfig1199_1_0m_a.res in P-1 REM Old TITL JFig1199_1_0m in P-1 #2 REM SHELXT solution in P-1 REM R1 0.139, Rweak 0.007, Alpha 0.038, Orientation as input REM Formula found by SHELXT: C55 N2 Si K Co CELL 0.71073 12.4898 12.5227 20.6102 93.054 104.868 110.926 ZERR 2 0.0004 0.0004 0.0006 0.001 0.001 0.001 LATT 1 SFAC C H N O Si K Co UNIT 118 172 2 2 2 2 2 EADP C15A C15B EADP C16A C16B EADP C17A C17B L.S. 10 0 0 PLAN 20 TEMP -173.15 BOND $H LIST 6 MORE -1 CONF fmap 2 53 acta OMIT 0 1 3 OMIT 2 -1 2 OMIT 0 -1 4 OMIT -1 -3 4 OMIT -1 -1 1 OMIT -3 3 8 OMIT 0 0 1 OMIT 0 -1 1 REM REM REM WGHT 0.056700 0.946200 FVAR 0.46619 0.57816 CO1 7 0.568991 0.669946 0.246690 11.00000 0.01996 0.02581 = 0.03057 0.00213 0.00733 0.00843 K1 6 0.458675 0.390439 0.161153 11.00000 0.04425 0.03687 = 0.06723 0.00055 0.02458 0.01957 SI1 5 0.506852 0.711663 0.142705 11.00000 0.02867 0.03129 = 0.03136 0.00424 0.01046 0.01262 N1 3 0.328937 0.491055 0.216108 11.00000 0.02242 0.02491 = 0.02938 0.00130 0.00748 0.00985 O1 4 0.599631 0.251122 0.193816 11.00000 0.05814 0.04484 = 0.05502 0.01251 0.01996 0.02603 C8 1 0.253399 0.614389 0.318652 11.00000 0.02588 0.02743 = 0.02526 0.00088 0.00857 0.01290 C23 1 0.156568 0.304235 0.118166 11.00000 0.02131 0.02095 = 0.02572 0.00023 0.00464 0.00651 C3 1 0.121527 0.384708 0.156995 11.00000 0.02530 0.02315 = 0.02347 0.00452 0.00735 0.01000 C7 1 0.173200 0.535090 0.253096 11.00000 0.02678 0.02351 = 0.02456 0.00479 0.00840 0.01137 C2 1 0.209437 0.473980 0.209211 11.00000 0.02210 0.02197 = 0.02357 0.00529 0.00684 0.00932 C34 1 0.153250 0.307401 0.049506 11.00000 0.02445 0.02505 = 0.02609 0.00147 0.00639 0.00833 C29 1 0.219057 0.145412 0.048555 11.00000 0.02657 0.02462 = 0.03566 -0.00269 0.00705 0.00898 C33 1 0.186525 0.229125 0.016847 11.00000 0.03194 0.03007 = 0.02748 0.00131 0.00959 0.01227 AFIX 43 H33 2 0.186941 0.233275 -0.028984 11.00000 -1.20000 AFIX 0 C4 1 0.000965 0.366011 0.144993 11.00000 0.02362 0.03071 = 0.02961 0.00017 0.00340 0.00771 AFIX 43 H4 2 -0.057921 0.307024 0.109376 11.00000 -1.20000 AFIX 0 C6 1 0.051421 0.513999 0.238519 11.00000 0.02977 0.03664 = 0.03213 0.00134 0.01125 0.01764 AFIX 43 H6 2 0.026406 0.556963 0.266629 11.00000 -1.20000 AFIX 0 C24 1 0.189337 0.219915 0.151440 11.00000 0.02880 0.02360 = 0.02690 0.00106 0.00411 0.00884 C28 1 0.219352 0.142195 0.115691 11.00000 0.03376 0.02348 = 0.03324 0.00235 0.00482 0.01260 AFIX 43 H28 2 0.240672 0.085248 0.138218 11.00000 -1.20000 AFIX 0 C1 1 0.425446 0.578099 0.232532 11.00000 0.02763 0.02655 = 0.02496 0.00329 0.00861 0.01420 C5 1 -0.034133 0.432588 0.184482 11.00000 0.02219 0.04293 = 0.03695 0.00289 0.00727 0.01440 AFIX 43 H5 2 -0.116102 0.422385 0.174522 11.00000 -1.20000 AFIX 0 C19 1 0.275333 0.566064 0.378353 11.00000 0.03517 0.03001 = 0.02786 0.00304 0.00965 0.01579 C25 1 0.185898 0.207270 0.224027 11.00000 0.05317 0.02924 = 0.02695 0.00542 0.00752 0.01850 AFIX 13 H25 2 0.184861 0.280621 0.245012 11.00000 -1.20000 AFIX 0 C9 1 0.289766 0.734747 0.322862 11.00000 0.02919 0.02839 = 0.02958 0.00263 0.01013 0.01357 C35 1 0.108897 0.389156 0.008750 11.00000 0.03531 0.03162 = 0.02676 0.00539 0.00804 0.01678 AFIX 13 H35 2 0.110235 0.451651 0.041618 11.00000 -1.20000 AFIX 0 C18 1 0.329006 0.639160 0.440966 11.00000 0.04208 0.03859 = 0.02490 0.00464 0.00796 0.01924 AFIX 43 H18 2 0.343407 0.606514 0.481299 11.00000 -1.20000 AFIX 0 C14 1 0.361976 0.758145 0.446063 11.00000 0.03525 0.03548 = 0.02897 -0.00375 0.00653 0.01583 C40 1 0.753148 0.759445 0.260808 11.00000 0.02191 0.03285 = 0.04315 0.00402 0.00768 0.00762 C13 1 0.342985 0.804011 0.386667 11.00000 0.03697 0.02706 = 0.03391 -0.00012 0.00999 0.01334 AFIX 43 H13 2 0.367031 0.885568 0.389413 11.00000 -1.20000 AFIX 0 C10 1 0.269940 0.790224 0.259217 11.00000 0.04443 0.02881 = 0.03217 0.00532 0.01166 0.01631 AFIX 13 H10 2 0.246905 0.729194 0.219237 11.00000 -1.20000 AFIX 0 C39 1 0.729345 0.642535 0.271326 11.00000 0.02207 0.03442 = 0.04315 0.00236 0.00680 0.01257 C38 1 0.677433 0.624759 0.325483 11.00000 0.02583 0.03822 = 0.03861 0.00882 0.00524 0.01241 C42 1 0.671017 0.730714 0.349201 11.00000 0.02640 0.04744 = 0.03272 -0.00177 0.00310 0.01526 C41 1 0.717744 0.813944 0.309771 11.00000 0.02602 0.03141 = 0.04543 -0.00448 0.00221 0.00958 C30 1 0.248077 0.059391 0.008232 11.00000 0.04278 0.03190 = 0.04649 -0.00244 0.01610 0.01716 AFIX 13 H30 2 0.306703 0.105062 -0.014913 11.00000 -1.20000 AFIX 0 C20 1 0.238310 0.435468 0.375842 11.00000 0.06861 0.03202 = 0.02854 0.00612 0.00991 0.02201 AFIX 13 H20 2 0.232172 0.402144 0.329219 11.00000 -1.20000 AFIX 0 PART 1 C15A 1 0.411746 0.836005 0.514070 21.00000 0.05010 0.04007 = 0.03031 -0.00613 0.00281 0.01890 AFIX 13 H15A 2 0.426575 0.916548 0.504260 21.00000 -1.20000 AFIX 0 PART 0 C48 1 0.543880 0.631628 0.075125 11.00000 0.05090 0.05593 = 0.03823 0.00274 0.01564 0.02927 AFIX 137 H48A 2 0.627047 0.637859 0.092171 11.00000 -1.50000 H48B 2 0.533802 0.666271 0.033583 11.00000 -1.50000 H48C 2 0.489729 0.549819 0.065057 11.00000 -1.50000 AFIX 0 C36 1 0.187321 0.446720 -0.035695 11.00000 0.05486 0.04538 = 0.03698 0.01718 0.01832 0.02399 AFIX 137 H36A 2 0.271684 0.480236 -0.008152 11.00000 -1.50000 H36B 2 0.163565 0.508054 -0.054274 11.00000 -1.50000 H36C 2 0.176906 0.388713 -0.073104 11.00000 -1.50000 AFIX 0 C50 1 0.341725 0.680319 0.103761 11.00000 0.03495 0.04994 = 0.03301 0.00721 0.00808 0.01731 AFIX 137 H50A 2 0.294308 0.599204 0.104616 11.00000 -1.50000 H50B 2 0.327529 0.694625 0.056618 11.00000 -1.50000 H50C 2 0.317936 0.730918 0.129906 11.00000 -1.50000 AFIX 0 C12 1 0.384129 0.888387 0.257495 11.00000 0.05458 0.03572 = 0.04512 0.01009 0.02062 0.01480 AFIX 137 H12A 2 0.407458 0.951347 0.295036 11.00000 -1.50000 H12B 2 0.369635 0.917283 0.214139 11.00000 -1.50000 H12C 2 0.448690 0.859624 0.262201 11.00000 -1.50000 AFIX 0 C3AA 1 0.166292 0.831026 0.251314 11.00000 0.05629 0.05952 = 0.05802 0.02337 0.01480 0.03468 AFIX 137 H3AA 2 0.093576 0.765695 0.251049 11.00000 -1.50000 H3AB 2 0.152300 0.861444 0.208447 11.00000 -1.50000 H3AC 2 0.186549 0.892096 0.289381 11.00000 -1.50000 AFIX 0 C49 1 0.573129 0.870230 0.132313 11.00000 0.04699 0.04015 = 0.04638 0.01331 0.01732 0.01604 AFIX 137 H49A 2 0.557807 0.917988 0.165254 11.00000 -1.50000 H49B 2 0.535793 0.879464 0.086098 11.00000 -1.50000 H49C 2 0.659849 0.894730 0.140247 11.00000 -1.50000 AFIX 0 C45 1 0.826390 0.818826 0.215992 11.00000 0.03017 0.05796 = 0.06338 0.01916 0.01831 0.01020 AFIX 137 H45A 2 0.793097 0.772926 0.170312 11.00000 -1.50000 H45B 2 0.909578 0.826274 0.235138 11.00000 -1.50000 H45C 2 0.824199 0.895957 0.213338 11.00000 -1.50000 AFIX 0 C44 1 0.765145 0.560447 0.234498 11.00000 0.03849 0.05086 = 0.06576 -0.00348 0.01209 0.02607 C31 1 0.305605 -0.011854 0.051458 11.00000 0.06436 0.04955 = 0.06935 -0.00191 0.01433 0.03904 AFIX 137 H31A 2 0.375437 0.040109 0.088185 11.00000 -1.50000 H31B 2 0.331175 -0.057336 0.023018 11.00000 -1.50000 H31C 2 0.247218 -0.064174 0.070983 11.00000 -1.50000 AFIX 0 C37 1 -0.020721 0.325253 -0.036346 11.00000 0.04078 0.05296 = 0.04415 0.00780 0.00008 0.02144 AFIX 137 H37A 2 -0.024854 0.261505 -0.067880 11.00000 -1.50000 H37B 2 -0.047467 0.379187 -0.062227 11.00000 -1.50000 H37C 2 -0.072736 0.294198 -0.007772 11.00000 -1.50000 AFIX 0 C26 1 0.294054 0.189769 0.268339 11.00000 0.06266 0.06716 = 0.03670 0.01488 0.00005 0.02595 AFIX 137 H26A 2 0.298448 0.119003 0.248679 11.00000 -1.50000 H26B 2 0.286249 0.182741 0.314193 11.00000 -1.50000 H26C 2 0.367255 0.256271 0.270738 11.00000 -1.50000 AFIX 0 C53 1 0.636387 0.207673 0.142357 11.00000 0.05124 0.04313 = 0.05896 0.00069 0.01580 0.01602 AFIX 23 H53A 2 0.596839 0.122142 0.132237 11.00000 -1.20000 H53B 2 0.724327 0.229207 0.157573 11.00000 -1.20000 AFIX 0 C46 1 0.737612 0.940291 0.321174 11.00000 0.04884 0.03486 = 0.07362 -0.00960 -0.00049 0.01450 AFIX 137 H46A 2 0.739476 0.971414 0.278665 11.00000 -1.50000 H46B 2 0.814127 0.982875 0.356239 11.00000 -1.50000 H46C 2 0.672157 0.948762 0.336036 11.00000 -1.50000 AFIX 0 C32 1 0.135920 -0.019816 -0.047094 11.00000 0.06822 0.04564 = 0.05737 -0.02044 0.00181 0.02471 AFIX 137 H32A 2 0.076027 -0.065614 -0.026152 11.00000 -1.50000 H32B 2 0.156418 -0.071889 -0.074351 11.00000 -1.50000 H32C 2 0.103055 0.027023 -0.076424 11.00000 -1.50000 AFIX 0 C43 1 0.639171 0.514150 0.354685 11.00000 0.04774 0.05524 = 0.06262 0.02741 0.01315 0.01920 AFIX 137 H43A 2 0.563553 0.501669 0.364877 11.00000 -1.50000 H43B 2 0.701184 0.519910 0.396561 11.00000 -1.50000 H43C 2 0.627902 0.448970 0.321601 11.00000 -1.50000 AFIX 0 C47 1 0.626538 0.751117 0.408250 11.00000 0.05128 0.09097 = 0.03758 -0.00482 0.00994 0.03392 AFIX 137 H47A 2 0.595157 0.812434 0.401672 11.00000 -1.50000 H47B 2 0.692897 0.774619 0.450519 11.00000 -1.50000 H47C 2 0.562631 0.679569 0.410964 11.00000 -1.50000 AFIX 0 C22 1 0.329619 0.403184 0.426123 11.00000 0.08043 0.05014 = 0.07165 0.02131 0.01669 0.03963 AFIX 137 H22A 2 0.409274 0.442884 0.420621 11.00000 -1.50000 H22B 2 0.307502 0.319229 0.417635 11.00000 -1.50000 H22C 2 0.331014 0.426603 0.472566 11.00000 -1.50000 AFIX 0 C27 1 0.070127 0.108864 0.223843 11.00000 0.06169 0.07461 = 0.04565 0.02412 0.02280 0.01602 AFIX 137 H27A 2 0.000996 0.124615 0.198347 11.00000 -1.50000 H27B 2 0.067859 0.103050 0.270740 11.00000 -1.50000 H27C 2 0.067251 0.035793 0.202324 11.00000 -1.50000 AFIX 0 C54 1 0.601955 0.258660 0.080274 11.00000 0.08728 0.06558 = 0.05788 0.00965 0.02290 0.02302 C57 1 1.029026 0.798941 0.414181 11.00000 0.06851 0.12159 = 0.06135 0.02692 0.02045 0.04344 AFIX 23 H57A 2 1.109979 0.804201 0.414087 11.00000 -1.20000 H57B 2 0.977919 0.779409 0.366315 11.00000 -1.20000 AFIX 0 C52 1 0.626601 0.204236 0.255387 11.00000 0.08180 0.05999 = 0.06468 0.02797 0.03205 0.03261 AFIX 23 H52A 2 0.594982 0.118765 0.244086 11.00000 -1.20000 H52B 2 0.584620 0.223921 0.286025 11.00000 -1.20000 AFIX 0 C51 1 0.759191 0.248118 0.292726 11.00000 0.09436 0.07806 = 0.07127 0.02741 0.00552 0.03936 AFIX 137 H51A 2 0.800557 0.222878 0.264367 11.00000 -1.50000 H51B 2 0.770858 0.216984 0.335463 11.00000 -1.50000 H51C 2 0.792070 0.332927 0.302542 11.00000 -1.50000 AFIX 0 C56 1 0.978369 0.703372 0.451347 11.00000 0.06699 0.12255 = 0.07328 0.01807 0.01471 0.03945 AFIX 23 H56A 2 1.026312 0.724541 0.499872 11.00000 -1.20000 H56B 2 0.895206 0.694054 0.448807 11.00000 -1.20000 AFIX 0 C58 1 1.038086 0.913176 0.443405 11.00000 0.09189 0.12042 = 0.08350 0.01750 0.02613 0.04768 AFIX 23 H58A 2 1.084263 0.929581 0.492148 11.00000 -1.20000 H58B 2 0.956264 0.908596 0.440791 11.00000 -1.20000 AFIX 0 C21 1 0.117101 0.379756 0.386423 11.00000 0.06454 0.04924 = 0.16950 0.04962 0.02315 0.01074 AFIX 137 H21A 2 0.121462 0.406041 0.433023 11.00000 -1.50000 H21B 2 0.092120 0.295364 0.378928 11.00000 -1.50000 H21C 2 0.058659 0.401523 0.354219 11.00000 -1.50000 AFIX 0 PART 1 C16A 1 0.534844 0.835975 0.553771 21.00000 0.06974 0.10447 = 0.06159 -0.04485 -0.02752 0.05278 AFIX 137 H16A 2 0.525859 0.757132 0.561583 21.00000 -1.50000 H16B 2 0.565211 0.887311 0.597574 21.00000 -1.50000 H16C 2 0.591525 0.863464 0.527335 21.00000 -1.50000 AFIX 0 PART 0 C55 1 0.977828 0.593870 0.423831 11.00000 0.12126 0.13500 = 0.11273 0.02614 0.03273 0.07955 AFIX 137 H55A 2 0.929868 0.572119 0.375888 11.00000 -1.50000 H55B 2 0.942991 0.533753 0.449424 11.00000 -1.50000 H55C 2 1.060262 0.601870 0.427619 11.00000 -1.50000 AFIX 0 C59 1 1.095979 1.013480 0.410224 11.00000 0.14825 0.13935 = 0.10226 0.05342 0.05477 0.05314 AFIX 137 H59A 2 1.054273 0.996701 0.361343 11.00000 -1.50000 H59B 2 1.180381 1.025467 0.417373 11.00000 -1.50000 H59C 2 1.090984 1.083591 0.430350 11.00000 -1.50000 AFIX 0 PART 1 C17A 1 0.323298 0.810280 0.555958 21.00000 0.07158 0.08770 = 0.04686 -0.02254 0.02076 0.02243 AFIX 137 H17A 2 0.250998 0.821570 0.531016 21.00000 -1.50000 H17B 2 0.360596 0.862798 0.599558 21.00000 -1.50000 H17C 2 0.301567 0.729972 0.564167 21.00000 -1.50000 AFIX 0 PART 0 H44A 2 0.722392 0.482308 0.240895 11.00000 0.05891 H44B 2 0.744732 0.559398 0.183753 11.00000 0.08210 H44C 2 0.844507 0.577631 0.250177 11.00000 0.08251 H54A 2 0.520132 0.236513 0.063946 11.00000 0.09281 H54B 2 0.640648 0.340072 0.088630 11.00000 0.08735 H54C 2 0.628312 0.237722 0.048647 11.00000 0.10081 PART 2 C16B 1 0.484619 0.791029 0.569334 -21.00000 0.06974 0.10447 = 0.06159 -0.04485 -0.02752 0.05278 AFIX 137 H16D 2 0.423507 0.725574 0.579959 -21.00000 -1.50000 H16E 2 0.528740 0.850217 0.609996 -21.00000 -1.50000 H16F 2 0.540462 0.764163 0.554439 -21.00000 -1.50000 AFIX 0 C15B 1 0.427185 0.840009 0.515540 -21.00000 0.05010 0.04007 = 0.03031 -0.00613 0.00281 0.01890 AFIX 13 H15B 2 0.492815 0.907529 0.507722 -21.00000 -1.20000 AFIX 0 C17B 1 0.343291 0.886942 0.534199 -21.00000 0.07158 0.08770 = 0.04686 -0.02254 0.02076 0.02243 AFIX 137 H17D 2 0.318049 0.930065 0.499103 -21.00000 -1.50000 H17E 2 0.383819 0.938793 0.577979 -21.00000 -1.50000 H17F 2 0.272748 0.822882 0.537803 -21.00000 -1.50000 AFIX 0 HKLF 4 REM jfig1199_1_0m_a.res in P-1 REM R1 = 0.0382 for 11252 Fo > 4sig(Fo) and 0.0503 for all 13771 data REM 635 parameters refined using 0 restraints END WGHT 0.0560 0.9646 REM Highest difference peak 0.362, deepest hole -0.285, 1-sigma level 0.047 Q1 1 1.0423 0.9219 0.3972 11.00000 0.05 0.36 Q2 1 0.5436 0.6946 0.1971 11.00000 0.05 0.35 Q3 1 0.5244 0.6349 0.2049 11.00000 0.05 0.34 Q4 1 1.0259 0.7115 0.3972 11.00000 0.05 0.33 Q5 1 0.1434 0.3533 0.1400 11.00000 0.05 0.33 Q6 1 0.2537 0.5025 0.3783 11.00000 0.05 0.33 Q7 1 0.3913 0.8008 0.4788 11.00000 0.05 0.32 Q8 1 0.4156 0.4047 0.1256 11.00000 0.05 0.32 Q9 1 0.1586 0.4222 0.1851 11.00000 0.05 0.30 Q10 1 0.2700 0.6766 0.3206 11.00000 0.05 0.30 Q11 1 0.1887 0.4868 0.2371 11.00000 0.05 0.29 Q12 1 0.5063 0.6026 0.2530 11.00000 0.05 0.29 Q13 1 0.1453 0.2968 0.0803 11.00000 0.05 0.29 Q14 1 0.2844 0.7640 0.2919 11.00000 0.05 0.28 Q15 1 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9.50 7 -3 0 256.57 9.40 7 -3 0 279.97 8.60 7 -3 0 265.77 8.90 -7 3 0 287.07 9.80 -7 3 0 268.07 9.20 -7 3 0 280.37 9.00 -7 3 0 268.77 9.40 -7 3 0 263.17 9.20 -7 3 0 265.27 9.80 6 -3 0 249.08 7.70 6 -3 0 247.48 8.50 6 -3 0 248.28 8.50 6 -3 0 258.27 8.00 6 -3 0 247.68 7.80 -6 3 0 251.37 8.20 -6 3 0 246.28 8.80 -6 3 0 254.57 8.40 -6 3 0 258.97 8.00 -6 3 0 246.68 8.70 -6 3 0 241.38 8.20 5 -3 0 17.80 1.90 5 -3 0 19.40 1.80 5 -3 0 20.00 1.90 5 -3 0 25.80 2.30 5 -3 0 15.40 1.70 5 -3 0 16.00 2.10 5 -3 0 21.20 2.60 -5 3 0 14.30 1.90 -5 3 0 18.20 2.00 -5 3 0 25.70 2.80 -5 3 0 23.70 2.00 -5 3 0 20.00 2.50 -5 3 0 19.50 1.90 -5 3 0 22.10 2.30 4 -3 0 21.10 1.70 4 -3 0 24.40 2.30 4 -3 0 19.90 2.20 4 -3 0 15.90 1.80 4 -3 0 20.80 1.70 4 -3 0 22.90 1.70 4 -3 0 19.10 1.70 4 -3 0 19.20 1.70 -4 3 0 18.40 0.80 -4 3 0 25.50 1.80 -4 3 0 23.80 2.10 -4 3 0 22.60 1.90 -4 3 0 21.50 1.60 -4 3 0 19.90 2.10 -4 3 0 16.80 1.70 -4 3 0 26.70 2.30 -4 3 0 26.50 2.40 3 -3 0 10.90 1.00 3 -3 0 8.00 1.10 3 -3 0 8.50 1.10 3 -3 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1.90 0 3 0 36.90 2.00 0 3 0 32.50 2.00 0 3 0 35.30 2.20 -1 -3 0 1531.45 36.50 -1 -3 0 1465.65 36.80 -1 -3 0 1506.15 36.00 -1 -3 0 1513.45 36.20 -1 -3 0 1480.85 36.40 -1 -3 0 1495.85 36.30 -1 -3 0 1493.85 36.80 -1 -3 0 1479.45 36.70 -1 -3 0 1455.75 36.80 1 3 0 1550.84 36.90 1 3 0 1508.45 36.80 1 3 0 1516.15 36.50 1 3 0 1482.25 36.60 1 3 0 1520.55 36.00 1 3 0 1514.75 36.60 1 3 0 1499.35 36.90 1 3 0 1522.35 36.60 1 3 0 1500.25 36.30 -2 -3 0 3026.50 73.29 -2 -3 0 3058.19 73.49 -2 -3 0 3001.10 72.79 -2 -3 0 3063.89 73.09 -2 -3 0 3123.29 72.59 -2 -3 0 3117.39 72.99 -2 -3 0 2977.30 73.09 -2 -3 0 3037.90 71.99 2 3 0 3154.98 72.99 2 3 0 2997.10 72.89 2 3 0 3135.49 73.69 2 3 0 2977.30 73.29 2 3 0 2999.20 72.99 2 3 0 2920.11 73.29 2 3 0 3078.09 72.99 2 3 0 3039.80 72.69 2 3 0 2999.00 72.99 -3 -3 0 185.98 6.30 -3 -3 0 191.18 5.50 -3 -3 0 195.38 6.70 -3 -3 0 191.38 6.60 -3 -3 0 185.38 6.80 -3 -3 0 189.88 7.30 3 3 0 194.08 6.90 3 3 0 194.38 6.80 3 3 0 185.18 5.50 3 3 0 183.28 6.50 3 3 0 191.48 6.40 3 3 0 187.68 7.20 3 3 0 185.68 7.10 -4 -3 0 3.10 1.80 -4 -3 0 2.50 1.60 -4 -3 0 -0.20 2.00 -4 -3 0 0.10 1.50 -4 -3 0 -0.20 0.80 4 3 0 -3.60 1.50 4 3 0 0.00 1.60 4 3 0 -1.10 1.40 4 3 0 1.40 1.50 4 3 0 0.00 1.40 4 3 0 -0.20 1.90 -5 -3 0 538.75 15.80 -5 -3 0 541.45 16.00 -5 -3 0 556.74 14.20 -5 -3 0 553.14 16.20 -5 -3 0 539.05 16.80 5 3 0 541.85 16.00 5 3 0 543.05 15.40 5 3 0 522.65 16.50 5 3 0 519.45 15.40 5 3 0 559.04 16.10 -6 -3 0 3.90 2.50 -6 -3 0 1.60 1.10 -6 -3 0 5.80 2.80 -6 -3 0 2.70 2.20 -6 -3 0 2.50 2.10 6 3 0 2.60 2.10 6 3 0 3.60 2.00 6 3 0 1.20 2.00 6 3 0 4.20 2.50 6 3 0 5.00 2.10 -7 -3 0 678.93 20.90 -7 -3 0 665.83 21.60 -7 -3 0 669.83 20.60 -7 -3 0 694.73 20.60 7 3 0 702.03 20.00 7 3 0 723.73 20.80 7 3 0 719.83 20.20 7 3 0 731.23 21.80 7 3 0 703.43 20.80 -8 -3 0 111.59 6.80 -8 -3 0 75.19 6.00 -8 -3 0 103.59 7.70 -8 -3 0 95.49 6.60 8 3 0 100.59 6.40 8 3 0 94.79 7.20 8 3 0 90.49 5.90 8 3 0 99.89 5.90 -9 -3 0 36.90 5.90 -9 -3 0 45.60 5.50 -9 -3 0 33.80 5.20 -9 -3 0 47.70 5.50 9 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0 23.30 2.20 6 -4 0 15.60 2.20 6 -4 0 22.40 2.00 6 -4 0 17.60 2.60 6 -4 0 18.30 2.10 -6 4 0 21.40 2.10 -6 4 0 24.30 2.90 -6 4 0 17.00 2.20 -6 4 0 18.00 2.40 -6 4 0 18.50 2.20 -6 4 0 18.30 2.40 5 -4 0 277.37 8.10 5 -4 0 276.07 7.90 5 -4 0 272.27 7.90 5 -4 0 272.57 7.80 5 -4 0 266.07 9.10 5 -4 0 282.07 8.60 -5 4 0 270.07 8.30 -5 4 0 288.17 8.70 -5 4 0 280.27 8.50 -5 4 0 276.37 8.30 -5 4 0 282.17 8.00 -5 4 0 288.17 8.00 -5 4 0 277.17 8.90 -5 4 0 270.47 6.80 -5 4 0 277.27 8.80 4 -4 0 311.07 9.10 4 -4 0 320.37 8.40 4 -4 0 313.57 8.50 4 -4 0 306.67 9.80 4 -4 0 310.37 8.30 4 -4 0 313.77 8.60 4 -4 0 316.97 9.00 4 -4 0 304.37 8.60 -4 4 0 311.37 8.80 -4 4 0 321.77 9.50 -4 4 0 337.97 8.60 -4 4 0 318.37 8.90 -4 4 0 315.77 9.20 -4 4 0 305.47 9.50 -4 4 0 318.37 9.00 -4 4 0 312.87 8.70 -4 4 0 316.17 8.20 -4 4 0 316.27 8.40 3 -4 0 1745.73 41.80 3 -4 0 1736.53 42.50 3 -4 0 1727.03 42.10 3 -4 0 1733.43 41.80 3 -4 0 1775.52 42.60 3 -4 0 1733.83 42.20 3 -4 0 1693.93 43.60 -3 4 0 1790.92 42.40 -3 4 0 1779.22 42.40 -3 4 0 1807.22 42.40 -3 4 0 1769.02 42.60 -3 4 0 1802.32 42.10 -3 4 0 1800.62 42.60 -3 4 0 1752.22 43.20 -3 4 0 1831.42 42.20 -3 4 0 1801.12 43.60 2 -4 0 3441.56 81.49 2 -4 0 3585.14 82.19 2 -4 0 3391.26 81.19 2 -4 0 3374.66 81.79 2 -4 0 3400.66 82.49 2 -4 0 3563.44 81.99 -2 4 0 3616.64 82.09 -2 4 0 3346.97 83.49 -2 4 0 3309.87 83.09 -2 4 0 3451.65 80.99 -2 4 0 3587.64 83.09 -2 4 0 3352.66 82.29 -2 4 0 3299.97 82.89 -2 4 0 3322.27 81.79 1 -4 0 48.60 1.70 1 -4 0 44.70 1.70 1 -4 0 49.90 2.40 1 -4 0 46.70 2.00 1 -4 0 48.80 2.60 1 -4 0 49.50 2.40 1 -4 0 48.10 2.10 -1 4 0 52.49 2.50 -1 4 0 49.00 2.50 -1 4 0 51.69 2.30 -1 4 0 47.80 2.30 -1 4 0 50.39 2.10 -1 4 0 44.10 3.10 -1 4 0 51.39 2.90 -1 4 0 50.99 2.50 -1 4 0 47.90 2.10 0 -4 0 47.70 2.10 0 -4 0 47.40 2.40 0 -4 0 47.90 2.90 0 -4 0 47.40 2.30 0 -4 0 47.00 2.60 0 -4 0 49.00 2.30 0 -4 0 48.30 2.70 0 -4 0 53.49 2.20 0 4 0 51.39 2.80 0 4 0 50.99 2.40 0 4 0 48.40 2.40 0 4 0 48.10 2.50 0 4 0 52.19 3.00 0 4 0 48.60 2.50 0 4 0 55.49 2.80 0 4 0 50.49 2.60 0 4 0 47.80 2.30 -1 -4 0 28.00 2.50 -1 -4 0 30.40 2.20 -1 -4 0 32.90 2.90 -1 -4 0 24.40 2.00 -1 -4 0 30.90 2.00 -1 -4 0 31.10 2.00 -1 -4 0 25.10 2.10 -1 -4 0 33.50 2.80 1 4 0 30.40 2.60 1 4 0 28.50 2.30 1 4 0 28.30 2.20 1 4 0 32.00 2.50 1 4 0 30.10 1.90 1 4 0 26.90 2.40 1 4 0 28.50 2.20 1 4 0 31.40 2.50 1 4 0 26.10 2.40 -2 -4 0 90.69 4.70 -2 -4 0 85.09 3.80 -2 -4 0 90.39 3.30 -2 -4 0 84.59 4.30 2 4 0 89.19 4.10 2 4 0 85.09 3.90 2 4 0 88.79 4.60 2 4 0 82.49 4.10 2 4 0 91.99 4.20 2 4 0 93.19 3.30 2 4 0 88.69 4.10 2 4 0 86.89 4.50 2 4 0 83.19 4.20 -3 -4 0 223.28 6.60 -3 -4 0 233.08 8.50 -3 -4 0 206.78 7.50 -3 -4 0 233.88 7.80 -3 -4 0 233.38 8.10 -3 -4 0 229.08 7.40 3 4 0 230.58 8.00 3 4 0 240.28 8.00 3 4 0 219.28 8.40 3 4 0 228.68 7.60 3 4 0 228.28 6.60 3 4 0 214.98 7.70 3 4 0 242.38 8.50 -4 -4 0 5.40 2.00 -4 -4 0 7.60 2.30 -4 -4 0 11.30 2.30 -4 -4 0 11.30 1.40 -4 -4 0 6.70 2.20 4 4 0 7.90 1.90 4 4 0 10.60 2.10 4 4 0 7.90 2.10 4 4 0 8.80 2.50 4 4 0 8.80 2.10 -5 -4 0 81.99 5.10 -5 -4 0 82.19 3.50 -5 -4 0 83.79 5.30 -5 -4 0 84.59 5.50 -5 -4 0 83.29 5.00 5 4 0 73.29 4.40 5 4 0 87.69 5.30 5 4 0 87.09 4.70 5 4 0 84.69 5.80 5 4 0 89.49 5.10 -6 -4 0 442.66 12.10 -6 -4 0 423.56 14.20 -6 -4 0 455.45 15.60 -6 -4 0 439.56 14.60 -6 -4 0 477.55 14.50 6 4 0 441.36 14.50 6 4 0 451.25 15.40 6 4 0 429.66 13.70 6 4 0 434.36 14.30 6 4 0 428.16 13.70 -7 -4 0 119.39 7.20 -7 -4 0 135.99 7.30 -7 -4 0 144.49 8.30 -7 -4 0 136.39 7.50 7 4 0 145.69 6.90 7 4 0 157.18 7.80 7 4 0 123.99 6.80 7 4 0 127.89 8.10 7 4 0 145.29 7.50 -8 -4 0 12.70 3.70 -8 -4 0 22.20 4.20 -8 -4 0 30.00 5.30 -8 -4 0 19.80 3.90 8 4 0 21.30 3.60 8 4 0 24.40 4.70 8 4 0 22.80 3.60 8 4 0 21.40 3.70 -9 -4 0 199.78 10.30 -9 -4 0 194.98 11.30 -9 -4 0 170.38 9.20 9 4 0 189.38 10.40 9 4 0 185.58 9.20 9 4 0 176.38 9.30 9 4 0 177.18 8.60 -10 -4 0 1.60 3.00 -10 -4 0 -5.80 3.80 -10 -4 0 0.20 3.50 10 4 0 -3.60 2.70 10 4 0 1.40 3.20 10 4 0 -1.50 3.90 10 4 0 2.10 3.00 -11 -4 0 62.79 7.10 -11 -4 0 56.89 7.40 -11 -4 0 71.09 8.80 11 4 0 83.09 8.90 11 4 0 61.79 6.30 11 4 0 78.49 7.20 -12 -4 0 11.20 4.70 -12 -4 0 -2.90 4.40 -12 -4 0 -0.40 4.30 12 4 0 7.10 4.10 12 4 0 -1.80 4.60 12 4 0 8.60 3.70 15 -5 0 2.20 4.20 15 -5 0 4.20 3.10 -15 5 0 8.80 3.80 -15 5 0 7.90 4.30 -15 5 0 1.30 4.30 -15 5 0 4.50 3.60 -15 5 0 2.60 4.10 14 -5 0 163.68 10.10 14 -5 0 147.79 10.60 14 -5 0 143.69 7.90 -14 5 0 151.78 10.70 -14 5 0 150.28 8.90 -14 5 0 137.49 8.40 -14 5 0 145.59 9.30 -14 5 0 138.59 9.60 13 -5 0 197.58 8.70 13 -5 0 222.28 11.10 13 -5 0 196.58 10.50 -13 5 0 191.08 10.10 -13 5 0 211.08 11.40 -13 5 0 194.88 9.80 -13 5 0 211.48 10.80 -13 5 0 207.58 9.60 12 -5 0 210.28 10.70 12 -5 0 243.98 11.20 12 -5 0 242.48 9.40 -12 5 0 252.97 10.60 -12 5 0 254.47 10.90 -12 5 0 243.48 11.10 -12 5 0 246.18 11.80 -12 5 0 253.57 10.50 11 -5 0 199.08 8.00 11 -5 0 213.58 9.60 11 -5 0 195.48 9.50 -11 5 0 212.28 8.90 -11 5 0 206.18 9.60 -11 5 0 196.68 9.20 -11 5 0 191.08 8.90 -11 5 0 195.48 9.90 10 -5 0 46.60 5.10 10 -5 0 43.70 3.80 10 -5 0 32.20 4.40 -10 5 0 53.59 5.00 -10 5 0 39.80 4.50 -10 5 0 44.10 4.80 -10 5 0 35.40 4.60 -10 5 0 36.00 4.20 -10 5 0 35.30 4.00 9 -5 0 160.08 7.80 9 -5 0 177.08 6.90 9 -5 0 166.78 6.30 9 -5 0 170.08 7.60 -9 5 0 153.08 6.70 -9 5 0 154.98 7.40 -9 5 0 168.68 7.30 -9 5 0 162.38 7.20 -9 5 0 165.08 7.20 -9 5 0 161.38 8.00 8 -5 0 88.39 4.20 8 -5 0 82.79 5.30 8 -5 0 89.69 5.10 8 -5 0 84.49 6.20 8 -5 0 93.49 4.60 -8 5 0 90.99 5.10 -8 5 0 85.19 4.90 -8 5 0 76.79 5.30 -8 5 0 91.29 5.30 -8 5 0 87.49 4.40 -8 5 0 91.19 4.90 -8 5 0 87.99 5.00 7 -5 0 38.00 2.70 7 -5 0 37.00 2.60 7 -5 0 28.30 3.50 7 -5 0 38.10 3.40 7 -5 0 40.10 2.80 7 -5 0 36.30 3.10 -7 5 0 37.10 2.80 -7 5 0 35.70 3.20 -7 5 0 38.10 3.60 -7 5 0 35.30 3.40 -7 5 0 40.30 3.70 -7 5 0 35.20 3.20 -7 5 0 32.80 3.40 6 -5 0 536.05 14.10 6 -5 0 515.05 14.60 6 -5 0 518.95 13.80 6 -5 0 533.75 13.70 6 -5 0 508.75 15.50 6 -5 0 509.75 13.80 -6 5 0 507.05 12.50 -6 5 0 534.55 15.00 -6 5 0 522.75 14.30 -6 5 0 511.45 14.50 -6 5 0 519.75 14.70 -6 5 0 503.25 15.00 -6 5 0 534.75 13.90 -6 5 0 518.65 14.40 5 -5 0 1176.58 29.90 5 -5 0 1179.08 29.00 5 -5 0 1196.98 29.40 5 -5 0 1146.29 31.00 5 -5 0 1178.18 28.90 5 -5 0 1195.48 29.30 -5 5 0 1172.18 30.50 -5 5 0 1222.28 28.80 -5 5 0 1179.28 29.70 -5 5 0 1205.28 29.20 -5 5 0 1199.88 29.60 -5 5 0 1208.18 30.10 -5 5 0 1214.68 29.40 -5 5 0 1202.08 30.00 -5 5 0 1201.08 29.80 4 -5 0 295.17 8.60 4 -5 0 301.37 7.70 4 -5 0 292.17 8.60 4 -5 0 307.37 7.70 4 -5 0 299.17 8.20 -4 5 0 298.37 8.80 -4 5 0 299.97 8.10 -4 5 0 286.57 8.20 -4 5 0 302.27 8.50 -4 5 0 306.57 8.70 -4 5 0 305.17 9.40 -4 5 0 306.37 8.40 -4 5 0 302.37 8.30 -4 5 0 295.57 8.50 3 -5 0 1336.47 32.30 3 -5 0 1335.47 31.80 3 -5 0 1330.17 33.80 3 -5 0 1288.27 31.70 3 -5 0 1307.07 32.20 -3 5 0 1328.87 33.10 -3 5 0 1322.07 32.00 -3 5 0 1325.17 32.30 -3 5 0 1337.57 32.10 -3 5 0 1329.27 32.00 -3 5 0 1306.67 32.10 -3 5 0 1313.37 31.90 2 -5 0 24.40 1.50 2 -5 0 24.00 2.30 2 -5 0 26.30 1.90 2 -5 0 20.10 2.60 2 -5 0 24.40 1.60 2 -5 0 22.70 1.90 -2 5 0 25.70 2.60 -2 5 0 21.30 2.20 -2 5 0 27.10 1.80 -2 5 0 24.60 2.00 -2 5 0 25.10 1.70 -2 5 0 24.90 1.80 -2 5 0 26.70 2.90 -2 5 0 25.40 1.80 -2 5 0 26.70 2.00 1 -5 0 2.20 0.90 1 -5 0 4.80 1.20 1 -5 0 2.90 0.60 1 -5 0 3.40 0.90 1 -5 0 3.10 1.20 1 -5 0 3.60 1.30 -1 5 0 4.10 1.00 -1 5 0 2.50 1.10 -1 5 0 2.00 1.20 -1 5 0 4.10 1.60 -1 5 0 3.70 1.00 -1 5 0 2.80 1.20 -1 5 0 2.10 1.00 -1 5 0 2.80 1.10 -1 5 0 3.30 1.10 -1 5 0 2.70 1.70 0 -5 0 382.66 10.60 0 -5 0 373.46 10.00 0 -5 0 371.66 9.60 0 -5 0 347.27 10.40 0 -5 0 352.76 10.10 0 5 0 361.96 10.60 0 5 0 350.16 9.90 0 5 0 343.87 10.80 0 5 0 377.46 10.20 0 5 0 357.36 10.20 0 5 0 373.16 10.30 0 5 0 359.36 10.50 0 5 0 368.66 10.30 0 5 0 371.26 10.10 -1 -5 0 209.48 6.30 -1 -5 0 200.48 6.40 -1 -5 0 200.78 7.20 -1 -5 0 204.18 6.20 -1 -5 0 192.18 6.40 1 5 0 203.48 7.20 1 5 0 202.78 6.50 1 5 0 198.58 6.90 1 5 0 207.98 6.90 1 5 0 192.68 7.20 1 5 0 202.78 6.20 1 5 0 202.58 6.70 1 5 0 189.98 6.70 1 5 0 199.98 7.20 -2 -5 0 914.41 22.80 -2 -5 0 923.81 23.50 -2 -5 0 855.21 24.20 -2 -5 0 870.31 23.50 -2 -5 0 949.01 23.30 2 5 0 922.41 22.70 2 5 0 921.91 24.40 2 5 0 899.71 24.30 2 5 0 877.61 24.00 2 5 0 934.21 23.60 2 5 0 915.01 23.80 2 5 0 925.91 24.00 -3 -5 0 566.94 16.70 -3 -5 0 569.94 14.70 -3 -5 0 570.14 16.50 -3 -5 0 535.55 15.70 3 5 0 572.04 15.70 3 5 0 556.64 16.00 3 5 0 547.45 16.60 3 5 0 548.65 14.50 3 5 0 569.74 16.70 3 5 0 547.55 16.10 3 5 0 559.44 16.10 -4 -5 0 82.19 5.00 -4 -5 0 98.39 5.00 -4 -5 0 82.09 5.50 -4 -5 0 79.89 3.50 -4 -5 0 97.59 5.60 4 5 0 78.59 3.50 4 5 0 87.09 4.80 4 5 0 81.39 4.70 4 5 0 91.29 5.00 4 5 0 87.89 5.20 4 5 0 81.29 5.50 -5 -5 0 59.89 5.60 -5 -5 0 61.39 4.80 -5 -5 0 61.19 3.10 -5 -5 0 60.59 4.50 -5 -5 0 57.19 4.80 5 5 0 59.59 4.20 5 5 0 65.39 4.80 5 5 0 52.39 4.20 5 5 0 55.69 4.90 5 5 0 61.89 5.70 -6 -5 0 134.89 8.10 -6 -5 0 135.09 7.20 -6 -5 0 143.89 6.90 6 5 0 136.29 8.10 6 5 0 132.69 7.10 6 5 0 149.99 6.90 6 5 0 150.78 7.10 6 5 0 147.89 7.40 -7 -5 0 19.80 4.10 -7 -5 0 8.40 3.70 -7 -5 0 15.00 3.60 -7 -5 0 15.00 3.50 7 5 0 10.20 3.20 7 5 0 11.00 3.80 7 5 0 10.20 3.00 7 5 0 18.70 3.40 -8 -5 0 94.69 8.50 -8 -5 0 93.29 7.90 -8 -5 0 84.69 6.70 8 5 0 76.69 7.50 8 5 0 91.59 6.40 8 5 0 87.89 6.50 8 5 0 78.69 6.40 -9 -5 0 -4.50 3.90 -9 -5 0 1.90 3.30 -9 -5 0 4.70 3.40 9 5 0 7.90 3.70 9 5 0 2.40 2.80 9 5 0 4.00 3.10 9 5 0 1.60 3.90 -10 -5 0 13.60 4.40 -10 -5 0 10.30 4.20 -10 -5 0 20.50 5.80 10 5 0 9.10 4.50 10 5 0 10.70 4.00 10 5 0 16.90 4.30 10 5 0 10.30 4.20 -11 -5 0 26.00 5.30 -11 -5 0 31.00 5.90 -11 -5 0 23.10 6.50 11 5 0 29.60 5.00 11 5 0 20.20 4.70 11 5 0 39.20 6.80 -12 -5 0 0.20 4.20 -12 -5 0 -6.00 4.70 12 5 0 1.60 3.70 12 5 0 -7.60 3.90 12 5 0 -0.80 3.90 15 -6 0 146.19 9.90 15 -6 0 117.29 7.30 -15 6 0 146.49 10.80 -15 6 0 141.19 8.90 -15 6 0 140.69 8.90 -15 6 0 155.38 10.30 -15 6 0 147.59 9.60 14 -6 0 79.99 8.20 14 -6 0 84.49 5.90 -14 6 0 87.09 7.60 -14 6 0 80.39 7.10 -14 6 0 78.79 7.90 -14 6 0 77.09 8.20 -14 6 0 89.39 7.40 13 -6 0 18.10 4.40 13 -6 0 14.80 3.10 13 -6 0 12.10 3.70 -13 6 0 14.50 3.70 -13 6 0 9.30 3.90 -13 6 0 9.90 4.20 -13 6 0 9.80 3.50 -13 6 0 12.30 3.70 12 -6 0 146.39 6.80 12 -6 0 145.59 8.30 12 -6 0 131.09 8.40 -12 6 0 145.29 8.10 -12 6 0 132.29 8.80 -12 6 0 151.68 7.70 -12 6 0 153.08 8.50 -12 6 0 133.49 8.00 11 -6 0 4.50 2.60 11 -6 0 10.10 2.40 11 -6 0 7.60 3.30 -11 6 0 8.40 2.90 -11 6 0 4.70 3.00 -11 6 0 10.30 3.10 -11 6 0 9.20 3.50 -11 6 0 7.80 2.80 10 -6 0 79.69 6.40 10 -6 0 96.89 5.90 10 -6 0 78.19 4.50 -10 6 0 97.89 6.00 -10 6 0 82.09 5.80 -10 6 0 88.19 6.50 -10 6 0 87.49 5.60 -10 6 0 85.39 5.10 -10 6 0 86.79 5.60 9 -6 0 43.50 3.20 9 -6 0 41.00 4.60 9 -6 0 47.20 3.60 9 -6 0 44.00 4.20 -9 6 0 42.50 3.90 -9 6 0 47.30 4.40 -9 6 0 34.20 4.00 -9 6 0 43.00 4.30 -9 6 0 53.89 3.80 -9 6 0 35.80 3.80 -9 6 0 46.80 4.40 8 -6 0 259.47 8.00 8 -6 0 265.87 8.50 8 -6 0 263.77 9.20 8 -6 0 250.77 8.10 8 -6 0 242.78 9.90 -8 6 0 267.07 9.50 -8 6 0 257.37 9.60 -8 6 0 242.18 8.90 -8 6 0 252.67 8.40 -8 6 0 254.27 9.50 -8 6 0 260.07 9.20 -8 6 0 254.57 8.90 7 -6 0 474.25 12.90 7 -6 0 470.05 12.70 7 -6 0 466.55 12.50 7 -6 0 485.95 13.10 7 -6 0 445.16 14.80 7 -6 0 448.36 13.60 -7 6 0 472.45 11.30 -7 6 0 456.55 13.80 -7 6 0 473.55 13.50 -7 6 0 468.65 13.50 -7 6 0 463.05 14.40 -7 6 0 478.35 13.80 -7 6 0 466.65 14.20 -7 6 0 466.25 12.90 -7 6 0 471.15 11.40 6 -6 0 85.39 3.20 6 -6 0 76.49 3.90 6 -6 0 84.79 3.50 6 -6 0 81.79 3.10 6 -6 0 85.59 3.60 6 -6 0 86.09 5.10 -6 6 0 83.49 3.90 -6 6 0 82.69 3.00 -6 6 0 80.29 3.40 -6 6 0 77.29 4.30 -6 6 0 87.69 4.70 -6 6 0 85.19 4.20 -6 6 0 80.59 4.00 -6 6 0 77.99 3.90 5 -6 0 100.79 5.60 5 -6 0 105.49 4.40 5 -6 0 107.29 3.20 5 -6 0 105.59 3.90 5 -6 0 110.19 3.20 -5 6 0 105.99 5.10 -5 6 0 104.89 4.20 -5 6 0 115.99 4.50 -5 6 0 113.99 4.10 -5 6 0 116.19 4.00 -5 6 0 99.39 4.20 -5 6 0 111.19 4.70 -5 6 0 111.99 4.50 -5 6 0 104.19 3.80 4 -6 0 164.88 5.50 4 -6 0 162.78 4.90 4 -6 0 163.98 6.90 4 -6 0 151.88 5.40 -4 6 0 161.38 5.10 -4 6 0 164.38 6.30 -4 6 0 166.98 5.30 -4 6 0 164.18 4.90 -4 6 0 157.28 5.50 -4 6 0 156.28 5.20 -4 6 0 160.88 5.50 -4 6 0 159.38 5.30 -4 6 0 163.38 5.50 3 -6 0 2.70 1.90 3 -6 0 0.50 1.00 3 -6 0 2.10 1.00 3 -6 0 1.00 0.80 -3 6 0 -0.70 0.90 -3 6 0 0.80 1.00 -3 6 0 1.00 1.50 -3 6 0 2.00 1.20 -3 6 0 0.90 0.90 -3 6 0 2.00 1.00 -3 6 0 1.60 1.00 2 -6 0 176.68 5.20 2 -6 0 162.08 5.50 2 -6 0 176.08 5.80 -2 6 0 179.08 5.40 -2 6 0 175.48 6.80 -2 6 0 174.68 5.90 -2 6 0 179.18 5.50 -2 6 0 180.48 5.70 -2 6 0 180.98 6.30 -2 6 0 177.48 5.60 -2 6 0 178.68 5.80 1 -6 0 9.90 1.70 1 -6 0 9.90 1.40 1 -6 0 9.20 1.60 1 -6 0 9.90 1.80 1 -6 0 9.50 0.90 1 -6 0 10.30 0.90 -1 6 0 11.90 2.40 -1 6 0 9.30 1.50 -1 6 0 8.70 1.50 -1 6 0 12.20 1.80 -1 6 0 9.40 1.80 -1 6 0 9.60 1.50 -1 6 0 9.00 1.40 -1 6 0 7.60 1.50 -1 6 0 10.70 1.80 0 -6 0 7.10 1.70 0 -6 0 5.40 1.00 0 6 0 9.80 1.70 0 6 0 7.80 1.70 0 6 0 4.90 1.40 0 6 0 9.20 1.50 0 6 0 6.20 1.40 0 6 0 3.80 1.30 0 6 0 6.00 1.90 0 6 0 7.50 1.50 -1 -6 0 16.90 2.00 -1 -6 0 20.20 2.00 -1 -6 0 26.30 2.90 -1 -6 0 22.80 2.20 -1 -6 0 21.60 1.90 1 6 0 18.40 2.70 1 6 0 21.60 2.30 1 6 0 19.60 2.00 1 6 0 21.70 2.50 1 6 0 22.20 2.60 1 6 0 17.40 2.40 1 6 0 20.30 2.80 -2 -6 0 3.00 1.30 -2 -6 0 6.80 2.10 -2 -6 0 2.50 1.20 -2 -6 0 4.10 1.50 -2 -6 0 2.90 1.60 2 6 0 0.70 1.60 2 6 0 2.20 1.90 2 6 0 4.70 1.70 2 6 0 1.30 1.70 2 6 0 0.40 1.50 2 6 0 1.00 1.60 2 6 0 3.30 1.20 -3 -6 0 38.20 2.60 -3 -6 0 47.40 3.60 -3 -6 0 40.30 3.60 -3 -6 0 35.80 3.90 3 6 0 46.40 3.70 3 6 0 35.60 3.80 3 6 0 49.50 4.60 3 6 0 40.30 3.80 3 6 0 41.90 2.60 3 6 0 33.80 3.50 3 6 0 35.40 3.40 -4 -6 0 26.30 2.30 -4 -6 0 28.70 4.10 -4 -6 0 23.50 3.50 -4 -6 0 24.90 3.30 4 6 0 28.30 3.50 4 6 0 28.40 4.00 4 6 0 28.10 2.40 4 6 0 25.90 3.30 4 6 0 24.90 3.20 4 6 0 32.20 3.60 -5 -6 0 4.50 2.40 -5 -6 0 -2.00 1.80 -5 -6 0 -2.10 2.10 -5 -6 0 2.50 2.90 5 6 0 -0.60 2.30 5 6 0 1.60 2.00 5 6 0 -2.80 2.40 5 6 0 -0.90 2.40 5 6 0 1.00 2.20 -6 -6 0 72.69 6.80 -6 -6 0 59.19 5.20 -6 -6 0 65.39 6.20 6 6 0 79.49 6.50 6 6 0 61.89 5.20 6 6 0 64.49 5.10 6 6 0 63.39 6.20 -7 -6 0 53.39 6.80 -7 -6 0 44.90 5.50 -7 -6 0 34.60 4.60 7 6 0 44.70 4.90 7 6 0 32.70 4.50 7 6 0 39.80 4.70 7 6 0 40.50 5.90 -8 -6 0 176.18 10.70 -8 -6 0 175.18 9.30 -8 -6 0 172.58 10.00 8 6 0 189.38 9.90 8 6 0 199.78 9.20 8 6 0 177.48 9.00 8 6 0 186.68 10.70 -9 -6 0 35.30 5.60 -9 -6 0 46.90 7.00 -9 -6 0 39.80 5.40 9 6 0 42.20 5.60 9 6 0 51.59 5.60 9 6 0 40.40 5.60 9 6 0 37.70 6.20 -10 -6 0 -4.20 4.30 -10 -6 0 1.60 3.60 10 6 0 0.40 3.30 10 6 0 -0.40 3.80 10 6 0 -0.40 4.20 10 6 0 6.10 3.60 -11 -6 0 22.40 6.70 -11 -6 0 16.60 5.00 11 6 0 18.60 5.80 11 6 0 28.20 5.10 11 6 0 20.30 5.00 15 -7 0 1.90 4.10 -15 7 0 -1.90 3.30 -15 7 0 2.30 3.90 -15 7 0 -1.80 4.10 -15 7 0 -3.00 2.90 -15 7 0 3.70 3.40 14 -7 0 43.90 4.50 14 -7 0 43.30 6.50 -14 7 0 34.50 5.20 -14 7 0 30.70 4.70 -14 7 0 29.20 5.70 -14 7 0 28.80 5.10 -14 7 0 34.20 5.60 13 -7 0 2.70 2.30 13 -7 0 5.70 3.90 -13 7 0 6.50 3.70 -13 7 0 3.30 3.70 -13 7 0 6.00 3.00 -13 7 0 2.50 2.90 -13 7 0 7.20 3.10 12 -7 0 29.60 4.60 12 -7 0 20.10 4.90 12 -7 0 28.10 3.30 -12 7 0 28.20 4.80 -12 7 0 20.90 3.70 -12 7 0 21.10 3.90 -12 7 0 18.70 4.00 -12 7 0 26.40 4.40 11 -7 0 434.96 14.80 11 -7 0 420.36 12.80 11 -7 0 422.26 16.00 -11 7 0 425.96 15.40 -11 7 0 429.36 13.80 -11 7 0 423.06 14.50 -11 7 0 422.36 14.80 -11 7 0 434.06 14.90 10 -7 0 122.39 7.80 10 -7 0 116.69 6.60 10 -7 0 119.59 5.20 -10 7 0 124.69 6.90 -10 7 0 120.89 7.30 -10 7 0 120.89 7.20 -10 7 0 117.19 5.80 -10 7 0 124.09 6.50 -10 7 0 134.99 6.90 9 -7 0 293.37 9.00 9 -7 0 281.97 11.60 9 -7 0 284.87 9.00 9 -7 0 313.87 10.60 9 -7 0 301.17 9.60 -9 7 0 290.97 9.50 -9 7 0 291.17 10.30 -9 7 0 294.27 10.70 -9 7 0 291.77 10.50 -9 7 0 284.87 11.00 -9 7 0 305.67 11.10 -9 7 0 284.47 10.20 8 -7 0 394.26 11.40 8 -7 0 399.36 12.20 8 -7 0 377.06 13.60 8 -7 0 397.76 10.70 8 -7 0 371.06 10.70 -8 7 0 395.06 12.30 -8 7 0 367.66 11.80 -8 7 0 399.46 11.30 -8 7 0 373.66 12.30 -8 7 0 369.76 11.90 -8 7 0 379.36 13.00 -8 7 0 389.26 12.60 7 -7 0 338.57 9.80 7 -7 0 343.37 9.90 7 -7 0 339.07 9.10 7 -7 0 314.67 12.00 7 -7 0 335.97 10.50 7 -7 0 347.67 9.10 -7 7 0 335.77 10.50 -7 7 0 346.57 10.60 -7 7 0 341.17 10.80 -7 7 0 343.77 11.60 -7 7 0 347.07 9.80 -7 7 0 342.77 9.00 -7 7 0 333.67 10.40 -7 7 0 326.67 10.90 6 -7 0 49.80 2.70 6 -7 0 43.30 4.40 6 -7 0 44.30 3.00 -6 7 0 46.80 2.50 -6 7 0 45.20 2.50 -6 7 0 48.70 3.40 -6 7 0 45.60 3.00 -6 7 0 48.40 3.30 -6 7 0 48.30 3.10 -6 7 0 50.39 3.10 -6 7 0 52.39 4.00 5 -7 0 43.90 2.80 5 -7 0 48.80 2.40 5 -7 0 41.30 4.30 -5 7 0 42.60 2.30 -5 7 0 47.50 3.10 -5 7 0 41.20 2.80 -5 7 0 43.10 2.80 -5 7 0 57.09 4.40 -5 7 0 47.10 2.80 -5 7 0 44.90 2.50 -5 7 0 48.40 2.80 -5 7 0 46.90 2.90 4 -7 0 79.19 2.90 4 -7 0 72.99 4.80 4 -7 0 76.49 3.50 -4 7 0 77.69 3.40 -4 7 0 79.99 3.50 -4 7 0 79.09 4.60 -4 7 0 81.89 3.90 -4 7 0 72.49 3.00 -4 7 0 72.99 3.70 -4 7 0 72.49 3.30 -4 7 0 78.99 3.30 -4 7 0 81.19 3.40 3 -7 0 456.75 12.70 3 -7 0 477.95 12.00 -3 7 0 458.05 12.70 -3 7 0 464.05 14.30 -3 7 0 469.85 12.50 -3 7 0 461.85 12.70 -3 7 0 468.15 13.70 -3 7 0 480.35 13.00 -3 7 0 483.55 12.50 -3 7 0 476.45 12.70 2 -7 0 49.10 2.90 2 -7 0 45.30 2.20 -2 7 0 44.20 2.50 -2 7 0 39.30 3.80 -2 7 0 43.90 2.70 -2 7 0 41.30 2.60 -2 7 0 47.30 3.10 -2 7 0 47.90 3.10 -2 7 0 44.60 2.60 -2 7 0 36.40 2.60 -2 7 0 40.60 2.70 1 -7 0 98.09 4.40 1 -7 0 92.29 3.60 1 -7 0 97.99 2.80 -1 7 0 99.39 4.20 -1 7 0 98.59 4.00 -1 7 0 91.19 5.00 -1 7 0 96.39 4.30 -1 7 0 93.39 4.20 -1 7 0 94.09 4.10 -1 7 0 92.19 4.40 -1 7 0 89.39 4.20 -1 7 0 90.49 4.00 0 -7 0 67.19 4.00 0 -7 0 70.89 2.80 0 -7 0 71.49 3.40 0 -7 0 68.99 3.00 0 7 0 71.29 3.90 0 7 0 70.59 4.40 0 7 0 67.49 4.00 0 7 0 64.89 3.50 0 7 0 69.69 3.80 0 7 0 73.39 4.30 0 7 0 69.89 3.60 -1 -7 0 33.10 2.30 -1 -7 0 30.50 2.60 -1 -7 0 31.60 3.30 -1 -7 0 29.40 2.60 1 7 0 30.30 3.00 1 7 0 40.30 3.80 1 7 0 33.90 3.20 1 7 0 34.90 3.70 1 7 0 31.30 2.90 1 7 0 35.40 3.60 1 7 0 37.20 2.50 -2 -7 0 286.87 9.20 -2 -7 0 292.57 10.40 -2 -7 0 290.87 9.40 -2 -7 0 297.07 8.90 2 7 0 295.87 8.80 2 7 0 297.67 10.50 2 7 0 295.87 10.40 2 7 0 282.97 9.90 2 7 0 286.87 10.00 2 7 0 279.57 9.50 2 7 0 289.27 10.50 -3 -7 0 87.39 5.80 -3 -7 0 78.39 4.70 -3 -7 0 81.39 4.60 3 7 0 80.69 5.20 3 7 0 81.39 4.80 3 7 0 87.39 5.10 3 7 0 79.69 5.60 3 7 0 93.69 5.70 3 7 0 84.79 3.80 -4 -7 0 203.28 8.20 -4 -7 0 196.98 8.10 -4 -7 0 215.58 9.50 4 7 0 201.98 6.90 4 7 0 212.98 8.90 4 7 0 194.78 9.20 4 7 0 216.48 8.50 4 7 0 211.58 8.80 4 7 0 216.58 8.80 -5 -7 0 62.59 6.20 -5 -7 0 74.89 5.30 5 7 0 80.29 5.80 5 7 0 73.89 5.10 5 7 0 70.89 5.40 5 7 0 77.09 6.30 -6 -7 0 0.60 3.10 -6 -7 0 1.70 2.60 6 7 0 -1.80 2.50 6 7 0 -3.30 2.40 6 7 0 2.70 3.10 6 7 0 4.20 2.80 -7 -7 0 6.80 3.30 -7 -7 0 3.40 3.90 7 7 0 5.00 3.40 7 7 0 2.80 3.20 7 7 0 8.90 3.80 7 7 0 3.30 3.00 -8 -7 0 12.00 3.90 -8 -7 0 14.10 4.90 8 7 0 22.30 4.70 8 7 0 17.90 3.90 8 7 0 13.70 4.60 8 7 0 10.60 3.70 -9 -7 0 9.40 3.90 -9 -7 0 1.00 4.60 9 7 0 1.00 3.30 9 7 0 4.20 3.60 9 7 0 0.10 3.60 9 7 0 0.60 3.70 -10 -7 0 4.70 4.00 -10 -7 0 -5.20 4.90 10 7 0 -5.40 3.60 10 7 0 -0.40 4.40 10 7 0 2.30 3.60 10 7 0 1.60 3.60 15 -8 0 85.09 9.10 -15 8 0 80.69 7.60 -15 8 0 77.39 8.20 -15 8 0 87.29 7.90 -15 8 0 65.29 7.40 14 -8 0 56.99 7.40 -14 8 0 52.79 5.60 -14 8 0 45.50 6.40 -14 8 0 52.99 6.10 -14 8 0 53.19 6.10 -14 8 0 48.70 6.20 13 -8 0 180.48 7.30 13 -8 0 167.98 10.60 -13 8 0 177.58 9.20 -13 8 0 179.08 10.10 -13 8 0 177.88 9.50 -13 8 0 182.58 8.50 -13 8 0 173.78 9.70 12 -8 0 271.27 9.10 12 -8 0 271.87 12.50 -12 8 0 255.07 10.00 -12 8 0 265.47 11.30 -12 8 0 262.87 11.80 -12 8 0 265.47 11.40 -12 8 0 259.67 10.80 11 -8 0 97.39 7.60 11 -8 0 94.69 4.60 -11 8 0 93.79 6.30 -11 8 0 99.69 6.70 -11 8 0 96.39 6.70 -11 8 0 102.99 5.60 -11 8 0 95.19 6.00 10 -8 0 8.20 1.70 10 -8 0 7.70 2.50 10 -8 0 5.90 3.40 -10 8 0 9.70 2.90 -10 8 0 6.70 2.40 -10 8 0 5.50 2.10 -10 8 0 9.30 3.00 -10 8 0 6.60 2.60 9 -8 0 751.02 18.90 9 -8 0 771.82 20.90 9 -8 0 743.03 21.00 9 -8 0 738.53 23.10 -9 8 0 720.83 20.80 -9 8 0 754.32 20.80 -9 8 0 718.93 19.90 -9 8 0 728.83 21.10 -9 8 0 752.52 23.10 -9 8 0 720.73 21.40 -9 8 0 749.62 22.00 8 -8 0 79.89 3.70 8 -8 0 74.79 5.70 8 -8 0 71.59 2.70 8 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8 0 55.09 3.10 -3 8 0 63.79 3.50 -3 8 0 53.69 4.20 -3 8 0 58.69 3.00 2 -8 0 20.90 1.80 2 -8 0 19.20 2.20 -2 8 0 17.40 2.30 -2 8 0 18.10 2.20 -2 8 0 21.00 3.20 -2 8 0 21.00 2.10 -2 8 0 18.20 2.10 -2 8 0 16.30 2.30 -2 8 0 18.40 2.10 -2 8 0 18.70 2.20 1 -8 0 13.10 2.10 1 -8 0 12.30 1.50 -1 8 0 10.30 2.40 -1 8 0 11.30 1.90 -1 8 0 11.40 1.90 -1 8 0 8.20 1.80 -1 8 0 12.80 2.00 -1 8 0 11.10 2.20 -1 8 0 9.90 2.00 0 -8 0 1.40 1.00 0 -8 0 1.30 0.90 0 -8 0 2.70 1.70 0 -8 0 2.60 1.20 0 8 0 0.50 1.60 0 8 0 1.50 1.80 0 8 0 2.30 1.60 0 8 0 2.70 1.50 0 8 0 1.60 1.50 0 8 0 2.80 2.00 0 8 0 2.60 1.50 -1 -8 0 2.60 1.90 -1 -8 0 1.60 1.30 -1 -8 0 0.30 1.00 -1 -8 0 -0.70 1.20 1 8 0 2.00 1.40 1 8 0 -3.00 1.40 1 8 0 0.20 1.50 1 8 0 2.10 1.60 1 8 0 -1.70 1.80 1 8 0 0.60 1.70 1 8 0 1.90 1.90 -2 -8 0 2.80 1.70 -2 -8 0 7.70 1.60 -2 -8 0 5.80 2.50 -2 -8 0 7.70 1.90 2 8 0 2.40 1.90 2 8 0 8.00 2.20 2 8 0 3.50 2.40 2 8 0 2.50 2.30 2 8 0 7.50 1.70 2 8 0 7.60 2.40 2 8 0 6.60 2.40 -3 -8 0 35.20 3.40 -3 -8 0 38.60 4.50 3 8 0 34.20 4.30 3 8 0 28.00 3.50 3 8 0 28.00 3.90 3 8 0 33.50 3.80 3 8 0 24.80 3.50 3 8 0 25.90 2.60 -4 -8 0 148.89 7.00 -4 -8 0 146.19 8.10 4 8 0 148.89 7.60 4 8 0 150.28 8.30 4 8 0 148.09 5.80 4 8 0 158.08 7.40 4 8 0 164.78 7.90 -5 -8 0 6.20 2.60 -5 -8 0 1.40 2.90 5 8 0 3.20 2.70 5 8 0 -1.80 2.90 5 8 0 2.80 3.00 5 8 0 1.70 1.70 5 8 0 2.40 2.80 -6 -8 0 0.40 3.20 -6 -8 0 -0.70 2.50 6 8 0 4.00 3.30 6 8 0 -3.90 2.70 6 8 0 -0.30 2.80 6 8 0 -1.90 2.30 -7 -8 0 53.49 5.60 -7 -8 0 64.59 7.60 7 8 0 50.29 5.90 7 8 0 53.79 5.80 7 8 0 62.49 6.40 7 8 0 43.70 6.20 -8 -8 0 79.69 7.00 8 8 0 55.59 7.30 8 8 0 66.19 6.60 8 8 0 60.09 6.40 8 8 0 59.69 6.90 -9 -8 0 10.50 4.00 9 8 0 9.90 4.30 9 8 0 11.90 4.70 9 8 0 9.30 3.80 9 8 0 13.80 4.30 15 -9 0 56.79 7.50 -15 9 0 40.20 5.80 -15 9 0 36.20 5.40 -15 9 0 40.50 6.20 -15 9 0 38.90 6.40 14 -9 0 28.50 6.00 -14 9 0 24.00 4.90 -14 9 0 28.90 5.50 -14 9 0 23.60 5.00 -14 9 0 22.90 4.50 13 -9 0 85.39 8.30 -13 9 0 81.79 6.40 -13 9 0 75.79 6.90 -13 9 0 94.89 8.00 -13 9 0 74.79 7.10 12 -9 0 43.70 6.20 -12 9 0 43.30 5.10 -12 9 0 42.70 4.60 -12 9 0 55.79 6.20 -12 9 0 43.50 5.40 -12 9 0 44.10 4.30 11 -9 0 28.70 5.40 -11 9 0 24.40 4.20 -11 9 0 16.80 3.60 -11 9 0 21.40 3.00 -11 9 0 17.70 3.80 -11 9 0 20.00 3.40 10 -9 0 20.30 4.60 -10 9 0 12.60 2.30 -10 9 0 21.80 3.50 -10 9 0 23.30 3.40 -10 9 0 17.60 3.40 -10 9 0 18.10 3.80 9 -9 0 12.20 2.50 9 -9 0 11.90 3.80 -9 9 0 13.70 2.00 -9 9 0 10.90 1.40 -9 9 0 8.90 2.60 -9 9 0 7.50 2.30 -9 9 0 8.90 2.50 -9 9 0 9.70 3.10 -9 9 0 10.70 2.50 8 -9 0 515.35 14.70 8 -9 0 493.85 17.30 -8 9 0 493.75 14.70 -8 9 0 487.25 15.00 -8 9 0 490.15 14.50 -8 9 0 501.45 13.30 -8 9 0 491.05 13.60 -8 9 0 468.75 16.10 -8 9 0 504.05 15.00 -8 9 0 518.95 15.30 7 -9 0 29.60 2.80 7 -9 0 31.30 4.60 -7 9 0 28.60 4.00 -7 9 0 21.40 2.60 -7 9 0 24.10 2.80 -7 9 0 21.30 2.80 -7 9 0 20.40 2.70 -7 9 0 23.80 2.60 -7 9 0 20.60 2.00 -7 9 0 21.50 3.50 6 -9 0 24.00 2.50 6 -9 0 26.00 4.30 -6 9 0 22.60 2.60 -6 9 0 16.10 2.20 -6 9 0 23.30 3.70 -6 9 0 22.60 2.40 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50.59 5.10 8 7 -9 127.79 7.00 8 7 -9 120.59 7.40 8 7 -9 113.99 7.00 8 7 -9 114.09 7.90 -8 -7 9 112.19 6.30 7 7 -9 30.50 4.60 7 7 -9 45.30 4.50 7 7 -9 33.80 4.30 7 7 -9 29.40 4.10 -7 -7 9 34.40 3.60 6 7 -9 35.80 3.90 6 7 -9 37.70 4.00 6 7 -9 30.80 3.90 6 7 -9 32.10 4.30 -6 -7 9 31.70 4.20 -6 -7 9 36.70 3.20 5 7 -9 44.10 4.20 5 7 -9 50.09 4.30 5 7 -9 50.39 4.50 5 7 -9 43.10 4.40 5 7 -9 41.40 3.90 -5 -7 9 52.79 3.10 -5 -7 9 58.19 5.10 4 7 -9 9.40 2.40 4 7 -9 9.90 2.30 4 7 -9 14.50 2.70 4 7 -9 10.00 2.30 4 7 -9 14.90 2.50 4 7 -9 12.10 2.50 -4 -7 9 13.30 1.20 -4 -7 9 13.90 2.60 3 7 -9 80.59 4.40 3 7 -9 75.89 4.10 3 7 -9 87.89 4.70 3 7 -9 81.39 2.90 3 7 -9 85.39 4.70 3 7 -9 76.19 4.50 3 7 -9 76.09 4.30 -3 -7 9 83.19 4.50 2 7 -9 59.39 3.20 2 7 -9 57.79 3.50 2 7 -9 51.59 3.30 2 7 -9 55.89 2.80 2 7 -9 58.59 3.50 2 7 -9 57.39 3.70 2 7 -9 67.79 5.00 2 7 -9 52.69 3.40 1 7 -9 34.80 2.40 1 7 -9 29.80 2.30 1 7 -9 29.00 2.40 1 7 -9 32.60 2.50 1 7 -9 30.40 2.40 1 7 -9 30.10 3.00 1 7 -9 24.00 3.30 1 7 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118.89 4.70 -6 7 -9 110.29 6.20 -6 7 -9 115.29 5.40 6 -7 9 114.39 7.10 -7 7 -9 7.30 2.30 -7 7 -9 10.70 2.90 -7 7 -9 8.70 1.70 -7 7 -9 13.20 2.40 -7 7 -9 6.40 2.10 -7 7 -9 7.70 2.50 7 -7 9 4.70 2.90 -8 7 -9 62.89 4.70 -8 7 -9 52.99 4.90 -8 7 -9 58.59 3.00 -8 7 -9 59.89 4.60 -8 7 -9 58.19 4.50 -8 7 -9 66.89 5.00 8 -7 9 56.79 5.90 -9 7 -9 1.40 2.60 -9 7 -9 0.50 2.40 -9 7 -9 3.30 2.70 -9 7 -9 -1.00 2.30 9 -7 9 -2.50 2.80 -10 7 -9 8.30 3.40 -10 7 -9 13.20 3.50 -10 7 -9 12.20 3.40 -10 7 -9 14.50 3.60 10 -7 9 14.00 4.10 -11 7 -9 10.50 3.60 -11 7 -9 9.00 3.80 -11 7 -9 5.30 3.40 11 -7 9 12.80 4.20 -12 7 -9 -1.90 3.10 -12 7 -9 2.30 3.70 -12 7 -9 -3.50 3.20 -12 7 -9 3.50 3.20 12 -7 9 4.70 4.10 -13 7 -9 45.20 6.70 -13 7 -9 39.40 6.00 -13 7 -9 35.40 5.70 -13 7 -9 33.70 6.00 13 -7 9 37.80 6.40 12 6 -9 18.30 4.30 12 6 -9 17.30 5.20 12 6 -9 16.80 5.10 12 6 -9 22.90 4.40 12 6 -9 19.70 4.60 -12 -6 9 21.40 4.70 11 6 -9 28.20 5.10 11 6 -9 30.90 5.00 11 6 -9 26.80 5.40 11 6 -9 24.30 4.40 11 6 -9 22.40 4.80 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117.59 5.80 -8 6 -9 15.40 3.00 -8 6 -9 9.30 2.60 -8 6 -9 3.60 2.50 -8 6 -9 7.90 1.50 -8 6 -9 9.90 2.80 -8 6 -9 9.90 3.20 8 -6 9 8.50 1.10 8 -6 9 14.90 4.90 8 -6 9 5.70 3.00 -9 6 -9 36.60 4.60 -9 6 -9 44.90 4.80 -9 6 -9 42.60 4.60 -9 6 -9 36.20 4.80 9 -6 9 48.00 5.90 -10 6 -9 52.89 5.60 -10 6 -9 49.10 5.40 -10 6 -9 50.59 5.30 -10 6 -9 53.59 6.10 10 -6 9 53.19 6.20 -11 6 -9 23.10 4.70 -11 6 -9 19.00 4.10 -11 6 -9 20.70 4.70 -11 6 -9 24.50 5.10 11 -6 9 27.50 5.40 -12 6 -9 37.40 6.20 -12 6 -9 46.10 5.90 -12 6 -9 51.99 6.50 -12 6 -9 29.00 5.10 12 -6 9 46.30 6.40 -13 6 -9 34.60 6.40 -13 6 -9 31.60 6.30 -13 6 -9 29.90 5.60 -13 6 -9 23.50 5.00 13 -6 9 39.30 6.50 12 5 -9 60.09 6.20 12 5 -9 60.59 6.30 12 5 -9 62.29 7.30 12 5 -9 59.09 6.50 12 5 -9 67.19 7.80 -12 -5 9 55.29 6.60 11 5 -9 3.50 3.30 11 5 -9 4.90 3.10 11 5 -9 -0.20 3.10 11 5 -9 -1.10 3.30 11 5 -9 2.70 3.10 -11 -5 9 2.50 4.10 -11 -5 9 8.60 3.60 10 5 -9 26.90 4.40 10 5 -9 24.20 4.00 10 5 -9 25.80 4.50 10 5 -9 25.10 4.40 10 5 -9 22.30 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366.66 10.40 1 4 -9 385.16 10.50 1 4 -9 370.56 11.40 1 4 -9 390.96 10.60 1 4 -9 366.76 10.70 1 4 -9 382.26 10.90 1 4 -9 389.96 10.30 1 4 -9 376.16 10.90 -1 -4 9 391.66 10.10 -1 -4 9 372.36 10.70 0 4 -9 198.48 6.10 0 4 -9 205.28 6.00 0 4 -9 193.08 6.10 0 4 -9 206.28 5.90 0 4 -9 191.18 6.40 0 4 -9 205.88 7.00 0 4 -9 207.58 6.20 0 4 -9 206.78 6.40 0 4 -9 203.08 6.60 0 -4 9 204.68 5.60 0 -4 9 203.88 6.90 0 -4 9 196.18 6.10 -1 4 -9 70.99 3.50 -1 4 -9 72.39 2.90 -1 4 -9 70.69 3.20 -1 4 -9 74.49 3.50 -1 4 -9 74.29 3.20 -1 4 -9 73.29 4.50 -1 4 -9 74.19 3.80 -1 4 -9 77.39 3.00 -1 4 -9 74.79 3.20 1 -4 9 79.49 3.90 1 -4 9 69.09 3.00 1 -4 9 76.59 2.60 -2 4 -9 42.80 2.70 -2 4 -9 41.30 2.50 -2 4 -9 46.80 2.90 -2 4 -9 46.30 2.60 -2 4 -9 46.20 3.50 -2 4 -9 47.30 2.70 -2 4 -9 45.80 2.50 -2 4 -9 48.80 3.00 -2 4 -9 42.20 2.80 -2 4 -9 41.80 2.90 2 -4 9 44.50 3.40 2 -4 9 44.50 2.80 2 -4 9 50.19 2.20 -3 4 -9 11.20 1.70 -3 4 -9 11.80 1.80 -3 4 -9 16.70 1.90 -3 4 -9 12.20 2.40 -3 4 -9 14.10 2.00 -3 4 -9 13.40 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13.30 2.20 -8 4 -9 11.30 3.30 -8 4 -9 14.60 3.30 -8 4 -9 8.40 3.10 8 -4 9 8.50 2.10 8 -4 9 13.40 3.60 8 -4 9 15.20 3.30 -9 4 -9 2.40 2.70 -9 4 -9 -0.60 2.70 -9 4 -9 6.30 2.90 -9 4 -9 3.60 3.20 9 -4 9 4.30 2.90 9 -4 9 -2.40 3.00 9 -4 9 3.70 2.00 -10 4 -9 9.90 3.60 -10 4 -9 0.50 2.90 -10 4 -9 2.10 3.80 -10 4 -9 2.60 2.90 10 -4 9 5.60 2.30 10 -4 9 7.80 3.40 10 -4 9 1.50 4.00 -11 4 -9 93.29 8.80 -11 4 -9 87.79 8.00 -11 4 -9 102.99 7.70 -11 4 -9 97.79 8.20 11 -4 9 87.99 5.60 11 -4 9 109.59 8.20 -12 4 -9 89.09 8.30 -12 4 -9 96.89 9.80 -12 4 -9 84.79 8.20 12 -4 9 88.49 8.50 12 -4 9 88.69 5.90 -13 4 -9 34.10 6.70 -13 4 -9 17.90 5.10 -13 4 -9 17.00 5.30 -13 4 -9 16.10 5.00 13 -4 9 22.60 5.60 14 3 -9 -2.20 3.70 14 3 -9 2.70 3.30 14 3 -9 -4.10 3.70 -14 -3 9 -5.30 4.00 -14 -3 9 5.40 4.30 13 3 -9 1.50 3.60 13 3 -9 -1.30 3.60 13 3 -9 7.20 3.20 -13 -3 9 9.00 4.20 -13 -3 9 -1.50 4.00 12 3 -9 19.80 4.00 12 3 -9 15.90 4.30 12 3 -9 15.20 3.50 12 3 -9 13.40 4.10 12 3 -9 11.00 4.70 -12 -3 9 12.40 4.60 -12 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213.48 8.50 -5 -3 9 212.78 8.40 -5 -3 9 205.08 7.60 -5 -3 9 215.98 7.00 -5 -3 9 221.98 7.60 4 3 -9 56.79 3.50 4 3 -9 59.29 3.60 4 3 -9 64.79 2.90 4 3 -9 69.79 4.30 4 3 -9 63.19 2.20 4 3 -9 51.69 3.60 4 3 -9 61.69 4.00 4 3 -9 55.39 3.40 -4 -3 9 62.09 4.10 -4 -3 9 65.79 3.00 -4 -3 9 62.69 3.10 -4 -3 9 61.99 3.40 -4 -3 9 62.49 3.50 3 3 -9 99.69 4.40 3 3 -9 105.79 4.70 3 3 -9 102.79 4.70 3 3 -9 100.49 4.80 3 3 -9 96.79 3.40 3 3 -9 96.69 3.30 3 3 -9 98.29 4.30 3 3 -9 104.39 4.30 -3 -3 9 98.19 3.60 -3 -3 9 95.89 3.90 -3 -3 9 98.09 3.70 -3 -3 9 104.89 4.30 -3 -3 9 105.99 4.90 2 3 -9 32.10 2.20 2 3 -9 34.20 2.80 2 3 -9 28.90 1.90 2 3 -9 33.10 2.90 2 3 -9 26.20 2.40 2 3 -9 27.80 2.70 2 3 -9 29.00 1.60 2 3 -9 30.10 2.50 2 3 -9 33.70 2.40 2 3 -9 29.90 2.30 -2 -3 9 33.40 2.70 -2 -3 9 32.40 2.00 -2 -3 9 29.70 1.80 -2 -3 9 34.10 2.40 1 3 -9 848.02 22.60 1 3 -9 869.81 21.70 1 3 -9 897.61 22.40 1 3 -9 876.81 21.90 1 3 -9 865.51 22.00 1 3 -9 859.71 21.10 1 3 -9 877.91 22.40 1 3 -9 842.12 22.00 1 3 -9 874.11 21.80 1 3 -9 872.51 21.70 -1 -3 9 868.21 21.10 -1 -3 9 875.81 21.00 -1 -3 9 849.72 21.70 -1 -3 9 865.31 22.40 0 3 -9 7.20 1.30 0 3 -9 7.70 1.30 0 3 -9 6.20 1.50 0 3 -9 7.70 1.40 0 3 -9 8.60 1.50 0 3 -9 8.30 1.40 0 3 -9 6.10 1.50 0 3 -9 4.30 1.30 0 3 -9 8.60 2.10 0 3 -9 8.20 1.70 0 -3 9 9.20 1.30 0 -3 9 7.20 1.50 0 -3 9 8.80 1.60 0 -3 9 7.60 0.80 0 -3 9 8.00 0.80 0 -3 9 8.30 1.60 -1 3 -9 0.30 1.10 -1 3 -9 0.40 1.10 -1 3 -9 0.40 1.60 -1 3 -9 0.80 1.20 -1 3 -9 -0.60 1.20 -1 3 -9 -1.00 1.10 -1 3 -9 -0.80 1.30 -1 3 -9 -0.80 0.80 -1 3 -9 1.30 1.00 -1 3 -9 1.00 1.00 1 -3 9 -0.80 1.20 1 -3 9 -0.30 0.60 1 -3 9 0.00 0.60 1 -3 9 -0.40 1.00 1 -3 9 -0.90 1.30 -2 3 -9 -1.10 1.20 -2 3 -9 -0.40 1.20 -2 3 -9 2.30 1.30 -2 3 -9 -1.00 1.00 -2 3 -9 0.50 1.00 -2 3 -9 -2.10 1.10 -2 3 -9 0.90 1.40 -2 3 -9 1.00 1.10 -2 3 -9 0.40 1.50 2 -3 9 -0.40 1.00 2 -3 9 0.30 0.70 2 -3 9 -0.40 1.30 2 -3 9 -1.10 1.20 2 -3 9 -0.10 0.70 -3 3 -9 16.50 2.40 -3 3 -9 13.60 1.80 -3 3 -9 10.80 1.80 -3 3 -9 10.10 2.20 -3 3 -9 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8 -10 -1.20 2.70 6 8 -10 -1.20 2.20 5 8 -10 19.20 3.20 5 8 -10 26.20 3.50 5 8 -10 25.50 3.40 5 8 -10 20.50 3.50 4 8 -10 3.90 2.00 4 8 -10 2.30 2.10 4 8 -10 3.70 2.10 4 8 -10 3.30 2.70 4 8 -10 2.40 2.10 4 8 -10 6.50 2.20 3 8 -10 239.08 8.10 3 8 -10 240.18 8.50 3 8 -10 239.08 8.90 3 8 -10 239.08 10.20 3 8 -10 236.58 8.40 3 8 -10 230.68 8.60 3 8 -10 245.98 6.70 2 8 -10 2.30 1.60 2 8 -10 5.70 1.40 2 8 -10 5.50 1.70 2 8 -10 2.80 1.60 2 8 -10 6.40 2.10 2 8 -10 6.10 1.70 2 8 -10 6.60 1.80 2 8 -10 1.40 2.80 -2 -8 10 3.80 2.00 1 8 -10 149.09 7.20 1 8 -10 150.48 6.40 1 8 -10 160.48 5.80 1 8 -10 153.18 5.50 1 8 -10 138.99 5.10 1 8 -10 147.29 5.20 1 8 -10 148.09 5.30 1 8 -10 146.39 5.40 0 8 -10 25.50 1.90 0 8 -10 29.50 2.10 0 8 -10 28.90 3.10 0 8 -10 46.30 4.60 0 8 -10 26.40 1.80 0 8 -10 28.50 2.10 0 8 -10 35.70 3.10 0 8 -10 28.60 2.10 0 8 -10 31.00 2.00 -1 8 -10 136.49 4.00 -1 8 -10 128.49 6.40 -1 8 -10 126.89 4.00 -1 8 -10 130.09 5.90 -1 8 -10 128.09 4.10 -1 8 -10 127.19 3.80 -2 8 -10 13.40 2.40 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1.60 -6 7 -10 5.70 1.80 -6 7 -10 5.20 2.00 -6 7 -10 1.80 1.70 -6 7 -10 3.70 1.70 6 -7 10 -0.80 2.60 -7 7 -10 49.60 4.90 -7 7 -10 57.79 4.20 -7 7 -10 58.49 3.30 -7 7 -10 62.09 4.30 -7 7 -10 57.49 4.60 -7 7 -10 57.99 4.30 7 -7 10 53.99 5.70 -8 7 -10 3.10 2.40 -8 7 -10 6.40 2.40 -8 7 -10 5.60 1.50 -8 7 -10 2.10 2.40 -8 7 -10 5.10 2.70 8 -7 10 7.80 3.40 -9 7 -10 85.69 5.90 -9 7 -10 81.19 6.40 -9 7 -10 75.89 5.80 -9 7 -10 76.49 5.70 9 -7 10 78.29 7.30 -10 7 -10 155.78 9.00 -10 7 -10 171.28 8.60 -10 7 -10 162.98 8.40 -10 7 -10 175.18 9.20 10 -7 10 170.98 10.00 -11 7 -10 89.09 7.90 -11 7 -10 85.29 7.50 -11 7 -10 86.99 7.40 -11 7 -10 92.49 7.00 11 -7 10 83.19 8.30 -12 7 -10 57.89 7.10 -12 7 -10 65.39 7.20 -12 7 -10 58.69 6.90 -12 7 -10 50.19 6.10 12 -7 10 55.39 7.30 -13 7 -10 35.80 6.20 -13 7 -10 35.70 5.90 -13 7 -10 28.90 5.80 -13 7 -10 35.40 5.80 13 -7 10 34.70 6.60 12 6 -10 2.00 3.60 12 6 -10 8.30 4.00 12 6 -10 5.10 4.30 12 6 -10 3.50 3.40 12 6 -10 7.40 3.50 -12 -6 10 9.00 4.10 11 6 -10 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4 6 -10 6.60 2.00 4 6 -10 6.40 1.90 4 6 -10 6.30 2.60 4 6 -10 9.40 2.20 -4 -6 10 7.00 1.20 -4 -6 10 8.20 1.30 -4 -6 10 6.80 2.20 -4 -6 10 7.70 1.60 3 6 -10 18.40 1.40 3 6 -10 19.70 2.50 3 6 -10 18.30 2.40 3 6 -10 13.50 2.00 3 6 -10 18.30 2.60 3 6 -10 18.70 1.50 3 6 -10 15.60 2.20 3 6 -10 16.00 2.30 3 6 -10 17.80 3.40 -3 -6 10 18.00 2.50 2 6 -10 0.00 0.90 2 6 -10 0.00 1.10 2 6 -10 0.40 1.40 2 6 -10 1.10 1.40 2 6 -10 -1.40 1.90 2 6 -10 0.80 1.20 2 6 -10 0.60 1.20 2 6 -10 0.40 1.20 -2 -6 10 0.30 1.20 1 6 -10 11.80 1.70 1 6 -10 9.60 1.50 1 6 -10 9.20 1.70 1 6 -10 11.70 1.70 1 6 -10 13.60 2.70 1 6 -10 12.40 1.50 1 6 -10 10.50 1.50 1 6 -10 11.50 1.70 -1 -6 10 6.40 1.30 0 6 -10 127.79 4.20 0 6 -10 121.89 4.30 0 6 -10 126.29 5.00 0 6 -10 128.29 4.00 0 6 -10 115.69 4.20 0 6 -10 115.29 5.50 0 6 -10 119.39 4.30 0 6 -10 113.29 4.30 0 -6 10 118.89 4.10 0 -6 10 126.69 4.00 -1 6 -10 86.19 3.10 -1 6 -10 83.39 3.30 -1 6 -10 87.29 3.00 -1 6 -10 85.79 4.60 -1 6 -10 82.29 4.90 -1 6 -10 85.09 3.30 -1 6 -10 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3.40 6 -6 10 42.70 3.50 6 -6 10 41.30 4.80 -7 6 -10 304.97 10.80 -7 6 -10 312.77 9.40 -7 6 -10 309.17 11.30 -7 6 -10 315.77 11.60 -7 6 -10 306.37 10.80 -7 6 -10 314.37 10.80 7 -6 10 331.27 12.50 7 -6 10 309.87 11.10 -8 6 -10 97.59 5.90 -8 6 -10 99.29 4.30 -8 6 -10 98.49 6.00 -8 6 -10 86.19 6.00 -8 6 -10 81.59 6.20 8 -6 10 89.69 6.90 -9 6 -10 38.00 4.70 -9 6 -10 33.30 4.30 -9 6 -10 40.70 5.00 -9 6 -10 35.30 4.90 9 -6 10 30.90 4.90 -10 6 -10 20.90 4.00 -10 6 -10 21.10 4.10 -10 6 -10 13.80 4.20 -10 6 -10 16.90 4.30 10 -6 10 18.50 4.80 -11 6 -10 2.80 3.20 -11 6 -10 3.60 3.30 -11 6 -10 1.10 3.80 -11 6 -10 0.20 3.10 11 -6 10 3.00 3.70 -12 6 -10 2.50 3.90 -12 6 -10 7.10 4.40 -12 6 -10 -0.20 3.40 12 -6 10 2.00 4.00 -13 6 -10 4.50 4.10 -13 6 -10 3.80 4.00 -13 6 -10 1.80 4.20 -13 6 -10 -3.90 4.10 13 -6 10 4.20 4.30 12 5 -10 9.60 4.50 12 5 -10 6.50 3.70 12 5 -10 10.20 3.90 12 5 -10 16.70 4.10 12 5 -10 11.70 3.80 -12 -5 10 12.30 4.00 11 5 -10 1.20 3.00 11 5 -10 3.50 3.80 11 5 -10 7.00 3.40 11 5 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2.20 1.80 4 5 -10 1.60 1.30 4 5 -10 2.60 1.90 4 5 -10 0.40 1.50 4 5 -10 0.90 1.60 4 5 -10 -1.00 1.90 -4 -5 10 1.50 1.20 -4 -5 10 3.90 1.10 -4 -5 10 2.70 1.40 -4 -5 10 2.40 1.80 3 5 -10 144.19 6.60 3 5 -10 141.69 5.10 3 5 -10 138.49 4.30 3 5 -10 137.59 6.00 3 5 -10 141.59 5.60 3 5 -10 139.89 5.90 3 5 -10 141.49 5.60 3 5 -10 152.98 5.50 -3 -5 10 145.89 5.20 -3 -5 10 141.59 5.90 -3 -5 10 136.19 5.30 -3 -5 10 146.49 4.30 -3 -5 10 150.18 4.20 2 5 -10 397.56 12.60 2 5 -10 395.16 11.00 2 5 -10 395.36 11.00 2 5 -10 385.26 11.20 2 5 -10 397.56 11.70 2 5 -10 397.46 11.30 2 5 -10 387.86 11.50 2 5 -10 385.26 12.40 2 5 -10 405.76 10.70 -2 -5 10 402.56 10.70 -2 -5 10 401.46 11.50 1 5 -10 210.28 6.80 1 5 -10 213.48 6.20 1 5 -10 200.38 7.10 1 5 -10 196.38 6.60 1 5 -10 211.08 6.40 1 5 -10 198.58 6.40 1 5 -10 197.78 6.40 1 5 -10 203.48 6.40 1 5 -10 193.38 7.50 0 5 -10 37.30 2.10 0 5 -10 44.00 2.60 0 5 -10 38.50 2.50 0 5 -10 35.20 2.70 0 5 -10 37.60 2.20 0 5 -10 38.00 2.40 0 5 -10 40.40 2.60 0 5 -10 37.30 2.40 0 5 -10 32.70 3.20 0 -5 10 38.70 2.30 -1 5 -10 77.29 3.30 -1 5 -10 76.69 3.50 -1 5 -10 78.79 3.10 -1 5 -10 72.99 4.80 -1 5 -10 79.39 3.10 -1 5 -10 79.89 3.40 -1 5 -10 76.99 3.30 -1 5 -10 71.49 3.90 1 -5 10 79.49 3.30 1 -5 10 73.99 4.30 -2 5 -10 37.80 2.70 -2 5 -10 37.50 2.50 -2 5 -10 34.40 3.60 -2 5 -10 32.90 2.20 -2 5 -10 39.10 2.30 -2 5 -10 32.90 2.40 -2 5 -10 39.00 2.60 -2 5 -10 29.60 2.70 2 -5 10 38.10 2.30 2 -5 10 33.50 3.40 -3 5 -10 33.30 2.70 -3 5 -10 35.20 3.80 -3 5 -10 34.40 2.60 -3 5 -10 31.10 2.70 -3 5 -10 30.70 2.50 -3 5 -10 31.10 2.30 -3 5 -10 35.10 2.90 -3 5 -10 31.40 2.80 3 -5 10 35.20 3.60 -4 5 -10 24.60 2.60 -4 5 -10 32.30 2.80 -4 5 -10 32.00 3.80 -4 5 -10 27.20 2.50 -4 5 -10 24.80 2.50 -4 5 -10 27.50 2.80 -4 5 -10 32.30 3.10 4 -5 10 30.30 2.70 4 -5 10 30.50 3.50 -5 5 -10 22.70 2.80 -5 5 -10 27.30 3.00 -5 5 -10 23.90 2.70 -5 5 -10 26.10 2.50 -5 5 -10 26.70 3.10 -5 5 -10 19.70 3.20 -5 5 -10 24.60 3.10 5 -5 10 19.30 3.20 5 -5 10 25.90 2.90 -6 5 -10 61.99 3.50 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-4 10 354.56 13.10 -7 -4 10 348.47 11.90 -7 -4 10 344.07 11.60 6 4 -10 382.76 12.40 6 4 -10 375.16 12.40 6 4 -10 378.26 12.80 6 4 -10 362.56 10.90 6 4 -10 343.57 12.00 6 4 -10 367.56 11.80 -6 -4 10 364.76 11.50 -6 -4 10 370.96 11.80 -6 -4 10 378.76 13.00 5 4 -10 198.28 7.80 5 4 -10 181.08 6.30 5 4 -10 196.28 8.20 5 4 -10 187.58 7.90 5 4 -10 189.78 7.10 5 4 -10 194.58 7.50 5 4 -10 183.38 7.30 -5 -4 10 192.28 6.90 -5 -4 10 194.98 7.10 -5 -4 10 182.18 6.40 -5 -4 10 196.58 8.00 4 4 -10 244.48 8.90 4 4 -10 250.57 8.50 4 4 -10 251.37 7.50 4 4 -10 254.77 8.20 4 4 -10 242.28 8.40 4 4 -10 246.78 8.90 4 4 -10 256.57 9.20 4 4 -10 253.07 6.50 -4 -4 10 257.47 7.90 -4 -4 10 255.97 9.00 -4 -4 10 255.77 8.20 -4 -4 10 245.08 7.80 -4 -4 10 260.57 7.60 3 4 -10 203.88 5.90 3 4 -10 207.38 6.80 3 4 -10 189.58 7.50 3 4 -10 216.68 7.20 3 4 -10 209.68 7.10 3 4 -10 202.58 7.50 3 4 -10 203.38 7.10 3 4 -10 204.28 7.40 3 4 -10 212.28 6.20 -3 -4 10 203.68 6.80 -3 -4 10 206.08 6.20 -3 -4 10 209.48 6.50 -3 -4 10 204.08 7.40 -3 -4 10 208.08 6.00 2 4 -10 7.30 1.60 2 4 -10 10.20 1.40 2 4 -10 8.20 1.20 2 4 -10 11.40 2.20 2 4 -10 13.10 1.70 2 4 -10 10.70 1.90 2 4 -10 12.80 2.00 2 4 -10 12.30 1.80 2 4 -10 10.40 1.70 -2 -4 10 12.40 1.00 -2 -4 10 11.20 1.50 -2 -4 10 11.60 1.90 -2 -4 10 10.50 1.10 1 4 -10 233.08 7.10 1 4 -10 242.58 7.30 1 4 -10 223.88 6.90 1 4 -10 225.18 7.30 1 4 -10 223.78 7.50 1 4 -10 228.68 7.20 1 4 -10 241.18 7.20 1 4 -10 233.18 7.50 1 4 -10 229.58 6.60 1 4 -10 232.98 8.10 -1 -4 10 227.98 7.40 -1 -4 10 235.48 6.80 0 4 -10 63.19 3.00 0 4 -10 75.89 3.30 0 4 -10 69.89 3.10 0 4 -10 73.49 3.90 0 4 -10 69.79 3.60 0 4 -10 69.19 3.30 0 4 -10 72.39 3.50 0 4 -10 67.79 3.30 0 4 -10 68.59 3.00 0 -4 10 69.49 3.60 0 -4 10 72.49 3.50 0 -4 10 68.99 2.80 -1 4 -10 268.47 8.60 -1 4 -10 270.07 8.30 -1 4 -10 273.07 7.80 -1 4 -10 261.27 8.00 -1 4 -10 241.68 9.10 -1 4 -10 261.87 7.80 -1 4 -10 274.47 8.20 -1 4 -10 268.97 8.10 1 -4 10 277.27 7.40 1 -4 10 258.57 8.10 1 -4 10 271.67 8.60 -2 4 -10 571.84 15.00 -2 4 -10 563.84 15.60 -2 4 -10 570.24 16.60 -2 4 -10 562.74 15.30 -2 4 -10 573.84 15.10 -2 4 -10 575.84 14.90 -2 4 -10 565.54 15.50 -2 4 -10 551.44 15.60 -2 4 -10 544.15 15.30 2 -4 10 566.34 15.40 2 -4 10 585.14 16.10 2 -4 10 580.64 14.60 -3 4 -10 328.07 10.30 -3 4 -10 337.87 10.10 -3 4 -10 345.57 10.70 -3 4 -10 336.57 10.20 -3 4 -10 335.37 10.30 -3 4 -10 349.57 11.50 -3 4 -10 359.86 10.80 3 -4 10 350.76 11.00 3 -4 10 345.27 9.60 3 -4 10 342.07 10.50 -4 4 -10 204.98 7.50 -4 4 -10 201.88 7.40 -4 4 -10 190.68 8.00 -4 4 -10 211.28 8.00 -4 4 -10 211.18 7.60 -4 4 -10 210.58 7.00 -4 4 -10 212.88 7.90 4 -4 10 201.08 5.80 4 -4 10 209.48 5.90 4 -4 10 198.18 8.00 4 -4 10 218.98 6.90 4 -4 10 225.58 7.80 -5 4 -10 141.09 5.40 -5 4 -10 147.19 6.30 -5 4 -10 147.09 6.30 -5 4 -10 154.68 6.90 -5 4 -10 132.89 6.50 -5 4 -10 144.59 6.30 -5 4 -10 138.89 6.80 5 -4 10 133.69 6.70 5 -4 10 138.49 4.80 5 -4 10 146.29 6.40 5 -4 10 143.99 5.60 5 -4 10 139.69 4.70 -6 4 -10 38.60 3.80 -6 4 -10 35.70 4.10 -6 4 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12 -4 10 29.70 4.20 -13 4 -10 47.20 7.20 -13 4 -10 51.09 7.60 -13 4 -10 40.10 6.60 -13 4 -10 34.20 7.20 13 -4 10 43.10 6.70 14 3 -10 2.20 3.50 -14 -3 10 2.40 5.10 -14 -3 10 -1.90 3.70 13 3 -10 2.20 3.60 13 3 -10 3.20 4.10 13 3 -10 -2.70 3.50 13 3 -10 0.20 3.10 -13 -3 10 -1.20 3.70 -13 -3 10 -3.10 3.80 12 3 -10 -3.10 3.30 12 3 -10 0.60 2.50 12 3 -10 -0.80 3.00 12 3 -10 2.40 3.30 12 3 -10 -1.10 2.50 -12 -3 10 3.20 4.00 -12 -3 10 -6.30 3.00 11 3 -10 7.80 3.60 11 3 -10 3.00 3.30 11 3 -10 10.20 3.50 11 3 -10 9.60 3.10 11 3 -10 6.50 2.90 -11 -3 10 2.70 3.60 -11 -3 10 10.80 3.70 10 3 -10 11.00 3.80 10 3 -10 6.60 2.90 10 3 -10 6.90 2.70 10 3 -10 8.20 2.90 10 3 -10 3.90 2.90 -10 -3 10 7.40 3.10 -10 -3 10 12.90 4.20 9 3 -10 59.69 6.10 9 3 -10 62.09 4.60 9 3 -10 58.59 5.50 9 3 -10 65.29 4.60 9 3 -10 51.79 4.90 -9 -3 10 62.69 5.50 -9 -3 10 66.99 6.80 8 3 -10 199.78 8.30 8 3 -10 202.58 8.30 8 3 -10 205.18 8.80 8 3 -10 206.78 9.50 8 3 -10 190.68 7.40 -8 -3 10 192.38 9.60 -8 -3 10 192.98 8.50 -8 -3 10 213.48 8.70 7 3 -10 379.06 11.50 7 3 -10 392.06 12.60 7 3 -10 390.76 12.60 7 3 -10 401.16 13.20 7 3 -10 407.16 13.10 7 3 -10 384.96 13.60 -7 -3 10 388.76 13.90 -7 -3 10 376.26 12.60 6 3 -10 25.90 3.20 6 3 -10 34.20 2.80 6 3 -10 35.20 3.50 6 3 -10 30.00 3.50 6 3 -10 26.60 3.50 6 3 -10 27.50 3.40 -6 -3 10 36.90 4.20 -6 -3 10 34.60 3.40 5 3 -10 104.79 5.00 5 3 -10 93.89 5.60 5 3 -10 107.59 5.70 5 3 -10 107.09 3.00 5 3 -10 105.89 5.20 5 3 -10 102.59 4.00 5 3 -10 97.79 5.00 5 3 -10 103.69 5.30 -5 -3 10 105.89 5.70 -5 -3 10 104.79 4.30 -5 -3 10 111.19 5.00 -5 -3 10 96.49 4.70 4 3 -10 86.39 4.80 4 3 -10 85.29 4.70 4 3 -10 80.39 3.20 4 3 -10 81.69 4.40 4 3 -10 77.89 4.00 4 3 -10 79.59 2.80 4 3 -10 80.69 4.20 4 3 -10 79.09 4.20 -4 -3 10 84.49 3.90 -4 -3 10 79.59 4.10 -4 -3 10 79.09 3.60 -4 -3 10 81.69 3.30 -4 -3 10 75.29 4.60 3 3 -10 6.80 1.40 3 3 -10 8.10 2.00 3 3 -10 5.30 1.60 3 3 -10 3.90 1.00 3 3 -10 4.40 1.50 3 3 -10 4.20 0.90 3 3 -10 6.70 1.60 3 3 -10 7.00 1.90 3 3 -10 5.00 1.80 -3 -3 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-1 3 -10 89.89 3.20 -1 3 -10 87.29 4.10 -1 3 -10 89.29 3.80 -1 3 -10 93.29 4.10 -1 3 -10 84.89 4.70 -1 3 -10 82.49 3.80 1 -3 10 87.09 4.30 1 -3 10 90.79 3.80 1 -3 10 95.99 3.00 1 -3 10 89.39 3.00 1 -3 10 94.29 4.10 -2 3 -10 162.58 6.60 -2 3 -10 183.58 6.70 -2 3 -10 177.38 6.20 -2 3 -10 163.48 6.00 -2 3 -10 183.58 6.40 -2 3 -10 171.88 6.30 -2 3 -10 173.18 7.00 -2 3 -10 180.88 5.60 2 -3 10 173.28 6.30 2 -3 10 180.58 5.20 2 -3 10 166.88 6.50 2 -3 10 175.18 5.90 2 -3 10 174.38 5.20 -3 3 -10 332.57 10.60 -3 3 -10 314.47 10.10 -3 3 -10 332.57 9.80 -3 3 -10 328.47 10.20 -3 3 -10 315.97 10.60 -3 3 -10 331.27 10.80 -3 3 -10 323.77 10.10 3 -3 10 324.17 10.50 3 -3 10 317.57 9.00 3 -3 10 322.57 8.90 3 -3 10 331.87 10.30 3 -3 10 319.77 9.70 -4 3 -10 155.28 6.60 -4 3 -10 172.98 6.10 -4 3 -10 171.68 6.80 -4 3 -10 164.78 7.20 -4 3 -10 170.08 6.80 -4 3 -10 162.68 7.10 -4 3 -10 174.28 7.20 4 -3 10 167.78 6.90 4 -3 10 171.68 6.30 4 -3 10 172.68 5.70 4 -3 10 162.78 5.50 4 -3 10 170.68 7.10 -5 3 -10 9.40 2.40 -5 3 -10 7.10 2.10 -5 3 -10 10.80 2.70 -5 3 -10 12.80 2.00 -5 3 -10 9.90 2.40 -5 3 -10 8.20 2.50 -5 3 -10 10.40 2.60 5 -3 10 7.90 1.70 5 -3 10 9.30 1.80 5 -3 10 8.70 2.40 5 -3 10 12.30 2.80 5 -3 10 11.00 2.20 -6 3 -10 34.20 3.80 -6 3 -10 32.40 3.70 -6 3 -10 32.50 3.90 -6 3 -10 38.80 3.30 -6 3 -10 36.70 4.40 -6 3 -10 40.60 4.60 6 -3 10 44.10 4.60 6 -3 10 42.80 3.20 6 -3 10 42.30 3.80 6 -3 10 43.00 4.50 -7 3 -10 128.49 7.50 -7 3 -10 120.79 7.20 -7 3 -10 114.39 6.70 -7 3 -10 134.39 5.60 -7 3 -10 118.39 6.80 7 -3 10 140.69 7.50 7 -3 10 123.29 5.50 7 -3 10 115.99 6.90 -8 3 -10 23.80 4.30 -8 3 -10 31.10 3.30 -8 3 -10 25.30 4.20 -8 3 -10 20.10 3.70 -8 3 -10 36.50 5.20 8 -3 10 28.50 3.30 8 -3 10 18.10 3.90 8 -3 10 40.30 5.20 -9 3 -10 262.77 12.30 -9 3 -10 275.47 11.60 -9 3 -10 304.47 12.10 -9 3 -10 262.97 11.50 9 -3 10 261.77 11.90 9 -3 10 290.67 12.00 9 -3 10 259.47 9.70 -10 3 -10 152.98 10.00 -10 3 -10 128.99 8.50 -10 3 -10 134.29 8.40 -10 3 -10 158.48 9.30 10 -3 10 131.19 8.90 10 -3 10 133.49 8.40 10 -3 10 145.09 7.00 -11 3 -10 4.20 4.70 -11 3 -10 5.10 4.00 -11 3 -10 10.60 4.30 -11 3 -10 10.30 3.90 11 -3 10 12.30 4.40 11 -3 10 5.10 2.80 -12 3 -10 54.89 6.80 -12 3 -10 62.29 8.60 -12 3 -10 56.39 7.00 12 -3 10 56.69 6.80 12 -3 10 47.40 5.10 14 2 -10 4.40 3.50 14 2 -10 -3.10 3.80 -14 -2 10 4.90 4.20 -14 -2 10 4.20 4.70 13 2 -10 -3.80 3.20 13 2 -10 -5.80 3.00 -13 -2 10 1.90 3.70 -13 -2 10 5.30 4.30 12 2 -10 -0.30 2.20 12 2 -10 4.10 2.60 12 2 -10 3.30 3.70 12 2 -10 -1.30 2.60 12 2 -10 0.10 2.80 -12 -2 10 1.70 2.90 -12 -2 10 2.40 4.00 11 2 -10 5.20 3.20 11 2 -10 3.10 3.50 11 2 -10 7.10 2.60 11 2 -10 1.90 2.90 11 2 -10 6.00 2.80 -11 -2 10 5.00 3.30 -11 -2 10 3.40 3.60 10 2 -10 0.60 2.70 10 2 -10 1.70 2.20 10 2 -10 2.60 2.30 10 2 -10 2.10 3.00 10 2 -10 -0.40 2.50 -10 -2 10 0.20 2.80 -10 -2 10 -2.20 2.80 9 2 -10 44.10 4.00 9 2 -10 44.40 4.30 9 2 -10 52.59 5.00 9 2 -10 42.50 4.50 9 2 -10 44.60 5.30 -9 -2 10 35.10 5.00 -9 -2 10 50.59 5.50 -9 -2 10 41.00 4.70 8 2 -10 40.60 4.90 8 2 -10 46.30 3.60 8 2 -10 47.70 4.20 8 2 -10 37.30 4.10 8 2 -10 42.10 4.40 8 2 -10 51.89 4.50 -8 -2 10 43.40 5.20 -8 -2 10 40.60 4.20 -8 -2 10 46.00 4.40 7 2 -10 50.39 3.90 7 2 -10 57.49 4.20 7 2 -10 50.09 4.30 7 2 -10 52.89 3.30 7 2 -10 48.50 3.70 7 2 -10 43.30 4.50 -7 -2 10 49.40 4.30 -7 -2 10 62.69 5.60 -7 -2 10 46.70 4.30 -7 -2 10 48.50 1.90 6 2 -10 36.80 3.40 6 2 -10 28.70 1.60 6 2 -10 28.80 3.20 6 2 -10 34.50 4.00 6 2 -10 32.40 2.50 6 2 -10 26.40 3.10 6 2 -10 31.00 3.30 -6 -2 10 29.40 3.20 -6 -2 10 32.40 2.50 -6 -2 10 34.90 3.40 -6 -2 10 34.10 4.00 -6 -2 10 32.40 1.60 5 2 -10 257.57 8.70 5 2 -10 270.17 9.00 5 2 -10 264.67 7.20 5 2 -10 253.67 9.40 5 2 -10 266.17 9.60 5 2 -10 270.97 8.90 5 2 -10 249.88 8.80 5 2 -10 251.97 7.50 -5 -2 10 265.57 7.70 -5 -2 10 273.57 8.90 -5 -2 10 261.97 9.70 -5 -2 10 257.07 7.10 4 2 -10 1382.36 33.40 4 2 -10 1399.76 33.70 4 2 -10 1383.36 35.10 4 2 -10 1354.76 35.10 4 2 -10 1411.96 34.90 4 2 -10 1415.56 35.90 4 2 -10 1402.76 35.70 4 2 -10 1364.56 35.10 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3.50 5 -8 14 37.80 5.10 -6 8 -14 8.20 2.30 -6 8 -14 1.80 2.90 -6 8 -14 12.80 2.60 -6 8 -14 8.60 2.30 6 -8 14 3.30 3.10 -7 8 -14 20.00 2.80 -7 8 -14 13.30 2.80 -7 8 -14 13.20 3.00 -7 8 -14 15.90 4.00 7 -8 14 10.60 3.80 -8 8 -14 32.20 4.00 -8 8 -14 30.50 4.90 -8 8 -14 26.20 4.00 8 -8 14 33.00 5.20 -9 8 -14 41.60 5.70 -9 8 -14 33.20 5.00 -9 8 -14 34.10 4.40 9 -8 14 38.00 6.00 -10 8 -14 -2.10 2.50 -10 8 -14 -2.90 3.30 -10 8 -14 -2.20 3.00 10 -8 14 -2.40 3.40 -11 8 -14 -2.50 2.90 -11 8 -14 6.10 4.00 -11 8 -14 0.80 3.60 11 -8 14 4.60 4.10 10 7 -14 42.10 6.30 10 7 -14 33.70 5.10 10 7 -14 47.60 5.70 10 7 -14 33.90 5.20 9 7 -14 63.99 6.30 9 7 -14 69.09 7.00 9 7 -14 82.89 7.60 9 7 -14 75.19 6.70 8 7 -14 82.39 8.00 8 7 -14 76.79 7.30 8 7 -14 80.19 6.40 8 7 -14 79.29 6.20 8 7 -14 71.79 7.00 7 7 -14 48.60 5.00 7 7 -14 41.70 3.90 7 7 -14 61.79 6.00 7 7 -14 56.99 5.10 7 7 -14 54.29 6.00 6 7 -14 102.69 5.90 6 7 -14 109.19 6.90 6 7 -14 111.59 6.80 6 7 -14 101.59 6.20 6 7 -14 105.09 5.20 5 7 -14 71.29 4.90 5 7 -14 74.09 5.00 5 7 -14 69.79 5.30 5 7 -14 72.39 6.40 5 7 -14 65.39 4.00 4 7 -14 9.90 2.30 4 7 -14 2.30 2.90 4 7 -14 3.60 1.70 4 7 -14 5.40 2.20 4 7 -14 6.20 2.30 4 7 -14 1.40 2.10 3 7 -14 165.98 6.90 3 7 -14 180.38 6.90 3 7 -14 175.78 8.40 3 7 -14 161.48 6.80 3 7 -14 186.18 7.40 3 7 -14 179.98 6.30 2 7 -14 22.50 2.60 2 7 -14 26.10 4.00 2 7 -14 16.50 2.60 2 7 -14 16.20 2.20 2 7 -14 18.50 2.40 2 7 -14 22.70 2.60 1 7 -14 127.59 5.20 1 7 -14 124.99 5.50 1 7 -14 132.79 5.20 1 7 -14 139.29 5.40 1 7 -14 131.09 7.00 1 7 -14 122.69 5.30 0 7 -14 212.78 9.40 0 7 -14 210.88 7.30 0 7 -14 211.48 7.20 0 7 -14 213.78 7.30 0 7 -14 200.58 7.20 0 7 -14 230.98 8.90 0 7 -14 219.18 7.20 0 7 -14 215.08 7.00 -1 7 -14 13.80 2.10 -1 7 -14 10.40 1.80 -1 7 -14 17.70 2.10 -1 7 -14 14.90 3.40 -1 7 -14 16.50 2.10 -1 7 -14 14.90 2.10 -1 7 -14 20.20 2.50 -1 7 -14 15.90 3.00 1 -7 14 16.10 3.00 -2 7 -14 309.37 9.40 -2 7 -14 293.37 10.50 -2 7 -14 307.27 11.80 -2 7 -14 312.07 11.50 -2 7 -14 303.67 9.50 -2 7 -14 303.77 9.40 2 -7 14 315.97 11.30 -3 7 -14 56.49 5.70 -3 7 -14 72.69 4.00 -3 7 -14 62.09 4.50 -3 7 -14 64.99 4.00 -3 7 -14 64.69 4.00 -3 7 -14 66.69 3.90 3 -7 14 73.09 5.40 -4 7 -14 66.49 4.20 -4 7 -14 72.39 4.40 -4 7 -14 70.49 4.40 -4 7 -14 70.99 4.60 -4 7 -14 76.79 5.80 -4 7 -14 79.39 4.50 4 -7 14 75.39 5.60 -5 7 -14 247.28 9.00 -5 7 -14 257.77 9.10 -5 7 -14 264.67 9.30 -5 7 -14 247.28 10.70 -5 7 -14 256.27 9.10 -5 7 -14 245.08 9.10 5 -7 14 253.67 10.70 -6 7 -14 84.49 6.60 -6 7 -14 95.69 5.00 -6 7 -14 88.09 5.30 -6 7 -14 83.89 5.40 -6 7 -14 88.79 5.60 6 -7 14 92.09 6.70 -7 7 -14 3.30 2.00 -7 7 -14 8.90 2.70 -7 7 -14 4.10 2.60 -7 7 -14 0.70 2.40 -7 7 -14 8.10 3.60 7 -7 14 6.30 3.40 -8 7 -14 2.50 2.60 -8 7 -14 10.40 3.60 -8 7 -14 9.20 3.20 -8 7 -14 5.60 2.90 8 -7 14 2.90 3.40 -9 7 -14 3.90 2.90 -9 7 -14 4.80 3.40 -9 7 -14 -0.60 2.90 -9 7 -14 -3.40 2.90 9 -7 14 1.80 3.60 -10 7 -14 12.30 4.30 -10 7 -14 6.80 4.10 -10 7 -14 9.20 3.60 -10 7 -14 1.60 3.70 10 -7 14 7.70 4.20 -11 7 -14 2.90 3.70 -11 7 -14 -3.30 3.00 -11 7 -14 3.30 4.00 11 -7 14 -0.70 3.10 11 6 -14 17.20 4.50 11 6 -14 29.10 5.80 11 6 -14 22.60 4.80 11 6 -14 15.40 4.00 10 6 -14 3.00 3.40 10 6 -14 -0.20 3.20 10 6 -14 -2.90 3.00 10 6 -14 -2.20 2.70 9 6 -14 2.90 2.90 9 6 -14 1.70 2.80 9 6 -14 7.20 3.30 9 6 -14 6.00 3.20 9 6 -14 5.20 3.30 -9 -6 14 8.40 2.70 8 6 -14 10.10 3.70 8 6 -14 11.10 3.30 8 6 -14 5.50 3.30 8 6 -14 9.10 2.50 8 6 -14 10.10 3.30 -8 -6 14 9.40 2.40 7 6 -14 2.00 2.70 7 6 -14 -0.20 2.30 7 6 -14 2.50 2.60 7 6 -14 1.10 2.40 7 6 -14 -1.90 1.80 -7 -6 14 1.00 1.70 6 6 -14 51.29 4.70 6 6 -14 54.79 5.30 6 6 -14 55.09 3.70 6 6 -14 54.49 5.30 6 6 -14 62.59 4.70 -6 -6 14 48.90 3.20 5 6 -14 58.69 4.30 5 6 -14 64.29 4.70 5 6 -14 68.29 5.10 5 6 -14 61.29 3.50 5 6 -14 69.79 6.00 -5 -6 14 59.89 2.80 4 6 -14 301.27 10.50 4 6 -14 297.87 11.40 4 6 -14 330.67 11.20 4 6 -14 310.67 10.60 4 6 -14 313.87 9.10 4 6 -14 317.37 10.30 -4 -6 14 305.87 10.70 3 6 -14 14.50 1.80 3 6 -14 14.20 2.30 3 6 -14 9.70 2.80 3 6 -14 13.80 2.30 3 6 -14 13.70 2.60 3 6 -14 11.40 2.20 2 6 -14 146.39 7.40 2 6 -14 149.69 5.90 2 6 -14 154.38 6.20 2 6 -14 150.48 6.50 2 6 -14 147.29 6.10 2 6 -14 152.98 5.20 2 6 -14 157.48 6.60 -2 -6 14 164.48 6.40 1 6 -14 0.70 2.40 1 6 -14 5.40 1.90 1 6 -14 1.20 1.50 1 6 -14 2.70 1.20 1 6 -14 2.50 1.60 1 6 -14 3.30 1.70 1 6 -14 4.70 1.60 0 6 -14 1.10 1.20 0 6 -14 -0.60 1.30 0 6 -14 -1.20 2.20 0 6 -14 -0.60 1.50 0 6 -14 -0.50 1.30 0 6 -14 -1.00 1.40 0 6 -14 -1.30 1.20 0 6 -14 -4.80 2.20 -1 6 -14 449.86 15.20 -1 6 -14 474.75 12.90 -1 6 -14 475.55 12.40 -1 6 -14 452.45 13.30 -1 6 -14 434.16 13.00 -1 6 -14 441.56 13.10 -1 6 -14 447.86 12.80 -1 6 -14 448.76 13.00 -1 6 -14 455.85 14.10 1 -6 14 443.56 13.90 -2 6 -14 11.70 2.00 -2 6 -14 12.40 2.70 -2 6 -14 14.00 2.10 -2 6 -14 10.90 2.20 -2 6 -14 12.00 2.10 -2 6 -14 16.40 3.30 -2 6 -14 12.90 2.20 2 -6 14 13.80 2.80 -3 6 -14 6.20 1.90 -3 6 -14 9.50 2.40 -3 6 -14 6.60 2.80 -3 6 -14 6.10 2.20 -3 6 -14 11.70 2.30 -3 6 -14 7.80 2.00 3 -6 14 9.40 2.70 -4 6 -14 27.00 3.20 -4 6 -14 24.30 3.00 -4 6 -14 24.80 3.00 -4 6 -14 21.90 3.00 -4 6 -14 25.60 4.20 -4 6 -14 22.60 3.20 4 -6 14 35.20 4.30 -5 6 -14 8.10 2.60 -5 6 -14 7.70 2.40 -5 6 -14 11.60 3.60 -5 6 -14 8.30 2.30 -5 6 -14 7.30 2.40 -5 6 -14 10.50 2.50 5 -6 14 3.70 2.90 -6 6 -14 3.20 2.40 -6 6 -14 2.20 2.00 -6 6 -14 -2.30 2.50 -6 6 -14 3.90 2.30 -6 6 -14 6.00 2.50 6 -6 14 3.10 2.80 -7 6 -14 26.70 3.90 -7 6 -14 25.20 4.00 -7 6 -14 25.80 3.20 -7 6 -14 21.80 4.10 -7 6 -14 34.00 4.30 7 -6 14 29.40 4.70 -8 6 -14 59.59 5.60 -8 6 -14 72.09 7.00 -8 6 -14 57.99 5.80 -8 6 -14 66.09 6.40 8 -6 14 70.49 7.20 -9 6 -14 22.60 4.70 -9 6 -14 24.00 4.20 -9 6 -14 30.80 4.80 -9 6 -14 24.80 4.70 9 -6 14 31.80 5.40 -10 6 -14 8.80 3.70 -10 6 -14 3.50 3.90 -10 6 -14 7.50 4.20 -10 6 -14 5.90 3.30 10 -6 14 8.40 4.20 -11 6 -14 -6.00 3.00 -11 6 -14 2.70 3.90 -11 6 -14 -6.70 3.70 -11 6 -14 6.20 3.70 11 -6 14 -1.30 3.60 12 5 -14 -2.40 3.60 12 5 -14 -0.90 3.40 12 5 -14 -1.20 3.10 12 5 -14 -0.50 3.60 -12 -5 14 -1.70 3.10 11 5 -14 21.80 4.20 11 5 -14 20.90 4.40 11 5 -14 25.20 5.20 11 5 -14 25.00 4.80 -11 -5 14 17.00 3.90 10 5 -14 50.79 6.00 10 5 -14 48.60 6.40 10 5 -14 43.30 5.30 10 5 -14 39.20 4.60 10 5 -14 52.29 5.80 -10 -5 14 49.60 5.00 9 5 -14 138.49 8.00 9 5 -14 132.39 7.70 9 5 -14 140.19 7.90 9 5 -14 139.59 6.50 9 5 -14 135.29 8.60 -9 -5 14 133.19 6.90 8 5 -14 130.79 7.50 8 5 -14 121.79 5.70 8 5 -14 119.09 7.10 8 5 -14 116.39 6.80 8 5 -14 106.09 7.40 -8 -5 14 129.39 13.30 -8 -5 14 132.39 6.40 7 5 -14 41.30 5.00 7 5 -14 39.80 3.30 7 5 -14 41.80 4.70 7 5 -14 38.90 4.20 7 5 -14 34.40 4.40 -7 -5 14 40.10 3.80 -7 -5 14 35.00 4.70 6 5 -14 10.00 3.00 6 5 -14 9.20 3.20 6 5 -14 10.20 2.70 6 5 -14 9.70 2.00 6 5 -14 11.70 2.70 -6 -5 14 10.80 2.10 -6 -5 14 10.60 2.90 5 5 -14 55.39 5.00 5 5 -14 44.70 4.00 5 5 -14 57.49 4.50 5 5 -14 56.89 4.80 5 5 -14 58.79 3.10 5 5 -14 54.39 4.30 -5 -5 14 59.09 3.40 -5 -5 14 63.49 4.90 4 5 -14 157.38 6.70 4 5 -14 156.78 6.70 4 5 -14 147.39 4.90 4 5 -14 148.19 7.20 4 5 -14 146.99 7.10 4 5 -14 142.39 4.90 4 5 -14 155.08 6.40 4 5 -14 135.49 6.80 -4 -5 14 147.79 6.80 -4 -5 14 153.08 4.90 -4 -5 14 142.89 6.20 -4 -5 14 149.79 6.00 3 5 -14 5.20 2.10 3 5 -14 4.50 1.80 3 5 -14 5.60 1.10 3 5 -14 5.60 2.10 3 5 -14 4.80 1.80 3 5 -14 2.30 1.70 3 5 -14 0.90 2.50 3 5 -14 3.70 1.50 3 5 -14 4.90 1.60 -3 -5 14 5.40 2.00 2 5 -14 13.50 2.00 2 5 -14 10.00 2.10 2 5 -14 11.30 1.20 2 5 -14 10.50 2.30 2 5 -14 6.00 2.40 2 5 -14 11.40 2.10 2 5 -14 10.00 2.30 2 5 -14 9.00 2.00 -2 -5 14 9.40 2.20 1 5 -14 14.10 2.10 1 5 -14 16.00 2.20 1 5 -14 13.20 2.40 1 5 -14 15.10 1.50 1 5 -14 11.50 2.80 1 5 -14 13.60 2.20 1 5 -14 13.40 1.90 1 5 -14 15.80 2.50 -1 -5 14 14.30 2.20 0 5 -14 23.40 2.70 0 5 -14 20.70 2.30 0 5 -14 21.10 2.40 0 5 -14 12.70 3.00 0 5 -14 16.70 1.80 0 5 -14 19.30 2.70 0 5 -14 21.00 1.70 0 5 -14 20.60 2.60 0 5 -14 21.90 2.60 0 5 -14 18.90 3.10 0 -5 14 20.70 2.60 0 -5 14 22.50 2.80 -1 5 -14 -0.60 1.80 -1 5 -14 -0.60 1.70 -1 5 -14 -0.70 0.90 -1 5 -14 -1.90 1.20 -1 5 -14 2.20 1.60 -1 5 -14 3.50 1.60 -1 5 -14 1.40 1.40 -1 5 -14 1.60 2.30 1 -5 14 1.10 1.50 1 -5 14 -2.40 1.50 -2 5 -14 99.69 4.10 -2 5 -14 107.79 5.00 -2 5 -14 93.49 6.30 -2 5 -14 96.99 5.00 -2 5 -14 92.99 4.90 -2 5 -14 96.69 5.30 -2 5 -14 92.29 4.90 2 -5 14 97.59 5.30 2 -5 14 104.29 5.10 -3 5 -14 14.90 2.60 -3 5 -14 11.30 2.40 -3 5 -14 10.80 2.30 -3 5 -14 9.50 2.30 -3 5 -14 12.30 2.60 -3 5 -14 8.20 3.00 -3 5 -14 9.90 2.20 3 -5 14 9.90 2.20 3 -5 14 13.10 2.80 -4 5 -14 24.40 3.90 -4 5 -14 26.70 3.30 -4 5 -14 22.60 3.10 -4 5 -14 21.00 3.30 -4 5 -14 23.50 3.10 -4 5 -14 26.20 3.40 4 -5 14 25.50 3.60 4 -5 14 22.00 3.00 -5 5 -14 298.67 10.80 -5 5 -14 288.27 10.00 -5 5 -14 311.17 11.10 -5 5 -14 305.37 10.90 -5 5 -14 290.07 11.60 -5 5 -14 302.27 11.30 5 -5 14 297.57 11.30 -6 5 -14 7.00 2.20 -6 5 -14 4.00 2.70 -6 5 -14 10.60 2.80 -6 5 -14 10.90 3.20 -6 5 -14 11.20 3.30 6 -5 14 7.80 3.00 -7 5 -14 79.09 6.30 -7 5 -14 82.39 6.50 -7 5 -14 90.19 6.50 -7 5 -14 76.09 6.10 -7 5 -14 96.09 5.20 7 -5 14 91.59 6.90 -8 5 -14 30.50 4.90 -8 5 -14 36.50 4.70 -8 5 -14 38.60 5.10 -8 5 -14 31.90 5.00 8 -5 14 40.20 5.40 -9 5 -14 1.90 3.60 -9 5 -14 1.50 2.90 -9 5 -14 3.90 3.50 -9 5 -14 1.80 3.30 9 -5 14 13.60 4.20 -10 5 -14 10.10 3.70 -10 5 -14 3.00 3.80 -10 5 -14 8.00 4.30 -10 5 -14 6.00 3.80 10 -5 14 8.30 4.10 -11 5 -14 0.90 3.40 -11 5 -14 5.80 3.90 -11 5 -14 3.80 4.60 -11 5 -14 -1.20 3.70 11 -5 14 0.40 3.20 13 4 -14 21.00 5.20 13 4 -14 39.10 6.80 13 4 -14 24.70 4.60 13 4 -14 14.00 4.50 -13 -4 14 26.40 5.00 12 4 -14 31.60 5.40 12 4 -14 27.50 5.20 12 4 -14 39.80 5.10 12 4 -14 39.00 6.50 -12 -4 14 30.20 5.00 11 4 -14 162.68 10.10 11 4 -14 138.79 7.90 11 4 -14 152.78 8.60 11 4 -14 149.99 9.10 11 4 -14 156.08 8.80 -11 -4 14 161.38 8.70 10 4 -14 34.00 4.90 10 4 -14 37.20 5.00 10 4 -14 38.60 4.90 10 4 -14 41.10 5.70 10 4 -14 42.90 4.20 -10 -4 14 47.40 5.00 -10 -4 14 33.70 5.40 9 4 -14 16.20 4.00 9 4 -14 19.00 3.50 9 4 -14 19.50 3.90 9 4 -14 23.30 3.00 9 4 -14 21.80 3.90 -9 -4 14 25.60 4.80 -9 -4 14 20.60 3.60 8 4 -14 75.79 5.60 8 4 -14 63.99 6.10 8 4 -14 84.09 6.00 8 4 -14 74.59 4.40 8 4 -14 77.79 5.80 -8 -4 14 77.89 6.60 -8 -4 14 82.79 5.40 7 4 -14 42.80 4.50 7 4 -14 40.00 4.30 7 4 -14 43.70 4.90 7 4 -14 38.30 4.30 7 4 -14 40.40 3.10 -7 -4 14 40.70 4.00 -7 -4 14 44.20 5.10 6 4 -14 24.90 3.50 6 4 -14 28.70 4.00 6 4 -14 27.00 2.30 6 4 -14 23.90 3.60 6 4 -14 23.10 3.30 -6 -4 14 30.60 4.10 -6 -4 14 25.60 3.00 5 4 -14 10.00 2.40 5 4 -14 5.20 2.60 5 4 -14 7.80 2.70 5 4 -14 5.00 2.20 5 4 -14 7.40 2.20 5 4 -14 6.20 1.20 5 4 -14 8.50 1.40 5 4 -14 5.90 1.70 5 4 -14 6.20 2.50 -5 -4 14 12.90 2.40 -5 -4 14 6.60 1.30 -5 -4 14 10.90 2.70 -5 -4 14 8.50 1.70 -5 -4 14 4.60 1.80 4 4 -14 107.59 5.90 4 4 -14 88.99 5.50 4 4 -14 101.89 5.70 4 4 -14 95.79 3.90 4 4 -14 94.99 3.10 4 4 -14 87.19 4.80 4 4 -14 91.19 4.10 4 4 -14 87.79 5.10 4 4 -14 92.19 5.00 -4 -4 14 99.29 4.20 -4 -4 14 97.69 5.50 -4 -4 14 94.39 4.70 -4 -4 14 93.49 3.90 3 4 -14 117.39 6.00 3 4 -14 134.09 5.70 3 4 -14 116.09 6.00 3 4 -14 117.99 6.10 3 4 -14 118.69 4.40 3 4 -14 116.89 5.60 3 4 -14 113.29 5.30 -3 -4 14 117.29 4.10 -3 -4 14 125.09 4.40 -3 -4 14 112.39 5.00 -3 -4 14 115.29 5.90 2 4 -14 112.69 5.70 2 4 -14 120.29 5.10 2 4 -14 118.39 5.40 2 4 -14 114.89 5.60 2 4 -14 111.29 4.20 2 4 -14 119.99 5.80 2 4 -14 118.79 5.40 -2 -4 14 111.99 3.80 -2 -4 14 113.49 3.90 -2 -4 14 117.69 4.90 -2 -4 14 121.09 5.80 1 4 -14 33.50 3.30 1 4 -14 34.50 3.20 1 4 -14 36.10 2.30 1 4 -14 32.10 3.40 1 4 -14 41.50 3.20 1 4 -14 37.30 3.20 1 4 -14 34.70 4.00 1 4 -14 29.70 3.50 -1 -4 14 36.20 1.70 -1 -4 14 35.10 3.50 -1 -4 14 31.30 1.70 -1 -4 14 34.00 2.80 0 4 -14 12.20 3.20 0 4 -14 15.30 2.30 0 4 -14 18.40 2.70 0 4 -14 16.30 1.30 0 4 -14 18.20 1.50 0 4 -14 16.70 2.40 0 4 -14 18.00 2.50 0 4 -14 17.10 2.90 0 4 -14 17.80 2.60 0 -4 14 17.40 2.10 0 -4 14 17.50 1.20 0 -4 14 20.60 2.40 0 -4 14 17.50 2.60 -1 4 -14 504.35 14.80 -1 4 -14 499.15 14.60 -1 4 -14 495.35 14.80 -1 4 -14 464.65 15.60 -1 4 -14 495.95 14.70 -1 4 -14 508.85 12.90 -1 4 -14 494.05 14.50 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21 17.60 5.70 -4 7 21 14.30 4.60 -4 7 21 12.40 4.20 3 -7 -21 3.50 4.00 3 -7 -21 0.60 3.50 3 -7 -21 5.50 4.80 -3 7 21 1.10 4.10 -3 7 21 -0.90 3.20 -3 7 21 -3.70 3.20 2 -7 -21 -2.30 3.90 2 -7 -21 2.30 3.50 2 -7 -21 -3.80 3.80 -2 7 21 -4.80 3.70 -2 7 21 -1.10 3.40 -2 7 21 3.50 4.40 1 -7 -21 81.39 8.60 1 -7 -21 79.19 9.60 1 -7 -21 61.69 7.40 -1 7 21 61.59 7.10 -1 7 21 86.49 10.10 -1 7 21 73.99 7.60 0 -7 -21 107.79 9.70 0 -7 -21 112.99 9.90 0 -7 -21 96.79 11.00 0 7 21 85.79 8.30 0 7 21 93.29 10.50 0 7 21 90.79 8.60 11 -8 -21 3.50 3.50 11 -8 -21 4.40 3.80 11 -8 -21 -1.50 3.90 -11 8 21 3.50 4.10 -11 8 21 7.00 4.90 -11 8 21 0.20 3.50 10 -8 -21 93.79 10.00 10 -8 -21 92.39 8.40 10 -8 -21 94.89 8.30 -10 8 21 80.09 9.50 -10 8 21 85.49 8.30 -10 8 21 87.99 7.70 9 -8 -21 66.79 7.30 9 -8 -21 44.60 7.40 9 -8 -21 61.69 6.80 -9 8 21 55.29 7.90 -9 8 21 58.19 7.00 -9 8 21 67.89 6.80 8 -8 -21 3.00 3.30 8 -8 -21 6.50 3.90 8 -8 -21 11.80 4.90 -8 8 21 8.30 4.00 -8 8 21 2.80 4.30 -8 8 21 3.90 3.60 7 -8 -21 5.70 3.70 7 -8 -21 3.20 3.50 7 -8 -21 3.40 4.00 -7 8 21 -0.30 3.10 -7 8 21 -0.10 3.60 -7 8 21 3.60 4.40 6 -8 -21 25.40 6.10 6 -8 -21 19.30 5.20 6 -8 -21 37.60 6.10 -6 8 21 24.00 6.00 -6 8 21 31.60 5.40 -6 8 21 41.40 5.90 5 -8 -21 -6.50 2.90 5 -8 -21 0.60 3.90 5 -8 -21 -3.90 2.90 -5 8 21 -0.10 3.20 -5 8 21 -3.40 2.90 -5 8 21 3.10 4.70 4 -8 -21 3.10 4.60 4 -8 -21 1.20 3.30 4 -8 -21 -0.20 3.50 -4 8 21 -1.50 3.40 -4 8 21 1.90 3.40 -4 8 21 4.40 4.60 3 -8 -21 18.40 5.10 3 -8 -21 20.90 6.00 3 -8 -21 26.40 5.90 -3 8 21 18.50 5.70 -3 8 21 25.00 5.40 -3 8 21 25.00 5.00 2 -8 -21 14.10 4.80 2 -8 -21 7.80 4.60 2 -8 -21 25.00 6.20 -2 8 21 12.70 4.90 -2 8 21 10.90 5.20 -2 8 21 16.30 5.20 10 -9 -21 103.39 9.00 10 -9 -21 97.89 8.60 10 -9 -21 88.49 9.80 -10 9 21 82.79 8.40 -10 9 21 81.89 9.70 -10 9 21 70.59 7.20 9 -9 -21 14.40 4.80 9 -9 -21 10.40 4.00 9 -9 -21 8.10 5.00 -9 9 21 9.30 4.80 -9 9 21 6.80 5.10 -9 9 21 6.60 3.90 8 -9 -21 0.30 3.70 8 -9 -21 1.20 4.30 8 -9 -21 5.00 3.60 -8 9 21 2.80 3.60 -8 9 21 12.40 5.40 -8 9 21 -2.50 3.60 7 -9 -21 27.30 5.40 7 -9 -21 27.70 5.70 7 -9 -21 23.00 6.10 -7 9 21 24.10 6.20 -7 9 21 21.10 5.10 -7 9 21 14.80 4.40 6 -9 -21 18.10 5.80 6 -9 -21 28.70 6.10 6 -9 -21 22.30 5.10 -6 9 21 21.80 4.80 -6 9 21 25.10 5.50 -6 9 21 13.30 5.50 5 -9 -21 50.39 7.10 5 -9 -21 38.50 6.20 5 -9 -21 38.30 6.90 -5 9 21 49.50 6.70 -5 9 21 45.40 7.70 -5 9 21 45.00 6.70 4 -9 -21 14.00 5.20 4 -9 -21 2.50 4.10 4 -9 -21 3.80 4.90 -4 9 21 7.40 5.10 -4 9 21 7.20 4.50 -4 9 21 7.20 4.30 2 10 -22 7.80 4.30 2 10 -22 2.60 2.40 2 10 -22 8.40 4.30 1 10 -22 1.80 2.30 1 10 -22 3.00 3.80 1 10 -22 -2.50 3.40 0 10 -22 -1.60 3.40 0 10 -22 2.90 3.80 0 10 -22 1.30 2.20 -1 10 -22 0.40 3.10 -1 10 -22 2.40 2.20 -1 10 -22 -4.60 3.20 -2 10 -22 4.90 4.00 -2 10 -22 5.50 3.40 -2 10 -22 5.00 2.40 4 9 -22 3.10 3.50 4 9 -22 2.10 2.50 4 9 -22 1.50 2.50 3 9 -22 36.80 5.40 3 9 -22 34.70 4.30 3 9 -22 32.10 4.10 3 9 -22 33.00 5.90 2 9 -22 10.20 4.20 2 9 -22 7.50 2.80 2 9 -22 12.70 4.90 1 9 -22 4.00 2.50 1 9 -22 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14.20 3.30 -4 8 -22 39.60 4.60 -4 8 -22 28.70 4.10 -4 8 -22 49.10 5.40 -4 8 -22 39.50 6.10 7 7 -22 -2.10 3.50 7 7 -22 0.50 2.70 7 7 -22 2.10 3.20 6 7 -22 -1.40 3.70 6 7 -22 -0.50 2.80 6 7 -22 -1.30 2.80 5 7 -22 5.10 3.50 5 7 -22 3.60 2.80 5 7 -22 3.60 3.00 4 7 -22 2.50 3.20 4 7 -22 0.90 2.40 4 7 -22 -1.50 3.00 4 7 -22 2.00 2.80 3 7 -22 1.70 2.60 3 7 -22 -1.30 2.90 3 7 -22 -0.60 2.40 3 7 -22 3.00 3.40 2 7 -22 7.70 3.00 2 7 -22 4.90 3.60 2 7 -22 11.30 3.60 2 7 -22 12.00 3.00 1 7 -22 4.10 3.40 1 7 -22 4.10 2.50 1 7 -22 6.50 3.90 1 7 -22 2.70 2.50 0 7 -22 0.10 2.30 0 7 -22 -2.60 2.90 0 7 -22 -1.80 2.90 0 7 -22 1.60 2.30 -1 7 -22 3.20 2.70 -1 7 -22 2.20 2.50 -1 7 -22 1.00 3.30 -1 7 -22 -0.40 2.50 -2 7 -22 72.59 7.60 -2 7 -22 84.29 6.60 -2 7 -22 83.19 6.30 -2 7 -22 83.39 6.20 -3 7 -22 22.80 4.10 -3 7 -22 33.90 5.70 -3 7 -22 31.80 4.60 -3 7 -22 33.50 4.30 -4 7 -22 10.70 3.40 -4 7 -22 13.20 4.40 -4 7 -22 6.80 3.30 -4 7 -22 15.60 3.70 -5 7 -22 16.40 3.90 -5 7 -22 14.80 3.80 -5 7 -22 10.30 3.50 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-1 -25 -2.80 3.40 8 -1 -25 -0.10 3.00 8 -1 -25 0.80 3.40 -8 1 25 4.10 3.30 7 -1 -25 3.40 3.20 7 -1 -25 -3.00 3.40 7 -1 -25 3.40 3.80 7 -1 -25 -2.60 3.50 7 -1 -25 -0.50 2.90 -7 1 25 -1.90 3.10 -7 1 25 -0.80 2.90 6 -1 -25 11.00 4.00 6 -1 -25 13.50 4.40 6 -1 -25 10.40 4.40 6 -1 -25 17.60 4.20 6 -1 -25 12.50 4.20 -6 1 25 20.20 4.20 -6 1 25 6.80 3.60 5 -1 -25 34.90 6.20 5 -1 -25 40.00 6.00 5 -1 -25 44.50 5.70 5 -1 -25 40.00 6.20 5 -1 -25 31.50 5.40 -5 1 25 38.70 5.10 -5 1 25 37.80 5.00 4 -1 -25 -1.00 3.70 4 -1 -25 7.20 3.40 4 -1 -25 2.50 3.70 4 -1 -25 -2.00 2.80 4 -1 -25 2.40 3.20 -4 1 25 5.90 3.30 3 -1 -25 36.90 5.40 3 -1 -25 42.70 6.90 3 -1 -25 44.90 5.90 3 -1 -25 40.60 6.10 3 -1 -25 38.60 5.80 -3 1 25 32.40 4.80 2 -1 -25 4.40 4.10 2 -1 -25 5.80 4.20 2 -1 -25 6.40 3.90 2 -1 -25 2.60 3.00 2 -1 -25 3.20 4.00 -2 1 25 6.70 3.40 1 -1 -25 -1.60 3.40 1 -1 -25 0.50 3.90 1 -1 -25 -0.90 3.70 1 -1 -25 1.40 3.50 1 -1 -25 0.30 3.60 -1 1 25 2.60 3.00 0 -1 -25 4.40 3.90 0 -1 -25 1.30 3.40 0 -1 -25 0.10 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2 25 10.80 5.10 3 -2 -25 61.89 7.90 3 -2 -25 87.89 8.50 3 -2 -25 74.49 7.70 3 -2 -25 57.29 7.20 3 -2 -25 76.39 6.90 -3 2 25 70.29 6.60 2 -2 -25 2.00 3.40 2 -2 -25 4.20 3.20 2 -2 -25 7.70 4.10 2 -2 -25 5.30 4.30 2 -2 -25 3.40 3.90 -2 2 25 0.90 3.10 1 -2 -25 20.00 4.80 1 -2 -25 18.90 5.60 1 -2 -25 16.90 5.20 1 -2 -25 15.80 5.00 1 -2 -25 14.80 4.30 -1 2 25 14.40 4.00 0 -2 -25 -2.20 3.40 0 -2 -25 -3.90 3.10 0 -2 -25 -5.30 3.60 0 -2 -25 3.10 4.20 0 -2 -25 0.00 3.40 0 2 25 1.70 3.10 9 -3 -25 8.70 4.80 9 -3 -25 14.10 4.50 9 -3 -25 11.80 4.70 -9 3 25 8.50 3.80 -9 3 25 14.80 5.60 -9 3 25 10.20 4.20 8 -3 -25 33.30 5.90 8 -3 -25 8.70 4.70 8 -3 -25 25.20 4.90 -8 3 25 33.10 6.80 -8 3 25 19.60 4.50 -8 3 25 23.70 4.80 7 -3 -25 27.90 6.10 7 -3 -25 41.20 5.80 7 -3 -25 31.50 5.90 -7 3 25 32.20 5.20 -7 3 25 31.10 6.40 -7 3 25 31.90 5.20 6 -3 -25 4.10 3.80 6 -3 -25 2.20 4.30 6 -3 -25 2.80 3.50 -6 3 25 -4.00 2.80 -6 3 25 -4.30 3.60 -6 3 25 -2.70 2.90 5 -3 -25 10.80 4.80 5 -3 -25 9.30 3.60 5 -3 -25 9.70 4.10 5 -3 -25 23.50 5.40 -5 3 25 7.10 3.80 -5 3 25 10.60 3.90 -5 3 25 24.10 6.10 4 -3 -25 3.50 4.30 4 -3 -25 -1.70 2.80 4 -3 -25 -3.60 3.50 4 -3 -25 1.30 3.40 -4 3 25 1.70 3.30 -4 3 25 -2.50 3.70 -4 3 25 -2.70 3.10 3 -3 -25 5.70 3.20 3 -3 -25 2.70 3.50 3 -3 -25 3.60 4.70 3 -3 -25 5.60 4.20 -3 3 25 0.30 4.30 -3 3 25 10.10 4.20 -3 3 25 5.40 3.50 2 -3 -25 6.00 3.30 2 -3 -25 -2.30 4.10 2 -3 -25 -3.30 3.70 2 -3 -25 -3.20 3.60 -2 3 25 -1.40 3.20 -2 3 25 0.90 4.60 1 -3 -25 -1.60 3.40 1 -3 -25 4.80 4.60 1 -3 -25 0.50 3.10 1 -3 -25 0.60 4.00 -1 3 25 1.30 3.40 9 -4 -25 13.90 4.30 9 -4 -25 4.50 4.80 9 -4 -25 12.10 4.60 -9 4 25 19.50 4.80 -9 4 25 9.80 5.20 -9 4 25 7.20 3.70 8 -4 -25 4.30 4.00 8 -4 -25 -2.60 3.70 8 -4 -25 3.30 4.50 -8 4 25 1.60 4.40 -8 4 25 1.60 3.40 -8 4 25 -0.30 3.40 7 -4 -25 13.30 4.40 7 -4 -25 14.00 4.90 7 -4 -25 2.90 4.30 -7 4 25 17.90 4.60 -7 4 25 12.40 5.30 -7 4 25 13.60 4.20 6 -4 -25 44.20 6.50 6 -4 -25 33.20 6.00 6 -4 -25 38.80 6.80 -6 4 25 48.90 7.80 -6 4 25 32.20 5.50 -6 4 25 46.40 6.20 5 -4 -25 28.00 6.50 5 -4 -25 24.60 5.30 5 -4 -25 11.50 4.70 -5 4 25 11.30 4.10 -5 4 25 23.60 6.00 -5 4 25 21.40 4.70 4 -4 -25 57.39 7.30 4 -4 -25 61.79 7.50 4 -4 -25 52.79 7.90 -4 4 25 52.59 6.30 -4 4 25 47.00 6.30 -4 4 25 50.99 7.90 3 -4 -25 42.50 6.50 3 -4 -25 48.00 7.00 3 -4 -25 48.60 8.30 -3 4 25 46.20 6.10 -3 4 25 49.90 6.40 -3 4 25 40.70 7.40 2 -4 -25 -2.00 3.80 2 -4 -25 3.50 4.70 2 -4 -25 5.60 4.40 -2 4 25 -2.30 3.40 -2 4 25 -1.80 4.20 -2 4 25 -5.00 3.30 8 -5 -25 53.29 7.00 8 -5 -25 51.89 7.10 8 -5 -25 75.19 9.30 -8 5 25 50.09 6.60 -8 5 25 52.59 6.40 -8 5 25 45.30 7.60 7 -5 -25 39.40 7.00 7 -5 -25 58.29 7.30 7 -5 -25 34.90 6.00 -7 5 25 41.10 6.30 -7 5 25 35.80 5.50 -7 5 25 30.20 6.70 6 -5 -25 14.80 5.50 6 -5 -25 23.30 5.10 6 -5 -25 12.90 4.80 -6 5 25 6.90 5.30 -6 5 25 2.50 3.60 -6 5 25 12.40 4.20 5 -5 -25 7.30 4.20 5 -5 -25 3.10 4.20 5 -5 -25 5.80 4.70 -5 5 25 2.00 3.80 -5 5 25 2.70 4.50 -5 5 25 0.30 4.00 4 -5 -25 -4.40 3.70 4 -5 -25 0.40 4.60 4 -5 -25 3.70 3.90 -4 5 25 2.70 4.00 -4 5 25 -1.00 4.50 -4 5 25 0.00 3.40 4 5 -26 7.10 3.70 4 5 -26 8.40 4.30 4 5 -26 6.70 4.40 4 5 -26 11.60 3.90 3 5 -26 -0.20 3.80 3 5 -26 -0.70 3.00 3 5 -26 -5.60 2.60 3 5 -26 -0.60 3.60 2 5 -26 2.30 3.80 2 5 -26 -6.50 3.50 2 5 -26 -2.50 2.80 2 5 -26 0.80 3.30 1 5 -26 18.80 4.50 1 5 -26 14.10 4.20 1 5 -26 11.70 4.30 1 5 -26 14.60 4.30 6 4 -26 2.50 3.90 6 4 -26 12.60 4.30 6 4 -26 8.60 4.50 6 4 -26 6.00 3.80 6 4 -26 2.10 3.50 5 4 -26 16.30 5.10 5 4 -26 21.20 5.00 5 4 -26 12.50 4.00 5 4 -26 10.50 4.00 5 4 -26 25.20 5.30 4 4 -26 19.00 5.10 4 4 -26 24.40 5.30 4 4 -26 7.90 4.00 4 4 -26 13.20 4.10 4 4 -26 20.50 4.80 3 4 -26 11.10 4.30 3 4 -26 8.70 3.90 3 4 -26 10.30 3.90 3 4 -26 10.30 4.50 3 4 -26 7.00 3.60 2 4 -26 -3.40 3.20 2 4 -26 1.30 3.20 2 4 -26 -3.00 3.00 2 4 -26 -2.10 3.10 2 4 -26 -1.60 2.90 1 4 -26 -2.00 2.90 1 4 -26 0.40 3.40 1 4 -26 4.00 3.70 1 4 -26 2.50 3.50 1 4 -26 -2.60 3.20 0 4 -26 -2.60 3.00 0 4 -26 0.60 3.40 0 4 -26 1.70 3.70 0 4 -26 1.20 3.30 0 4 -26 -2.30 3.10 7 3 -26 0.10 3.50 7 3 -26 3.10 3.90 7 3 -26 -3.70 2.90 7 3 -26 -1.70 3.10 7 3 -26 -2.20 3.40 6 3 -26 2.50 3.50 6 3 -26 3.90 3.50 6 3 -26 1.10 3.30 6 3 -26 -0.90 3.60 6 3 -26 -2.00 3.10 5 3 -26 -2.40 2.80 5 3 -26 4.50 3.80 5 3 -26 -0.80 3.10 5 3 -26 -0.90 3.50 5 3 -26 -1.90 2.80 4 3 -26 -5.00 3.10 4 3 -26 1.20 3.10 4 3 -26 1.50 3.50 4 3 -26 -1.30 2.90 4 3 -26 -8.40 2.80 3 3 -26 29.10 5.60 3 3 -26 25.50 5.00 3 3 -26 24.70 5.00 3 3 -26 25.80 5.00 3 3 -26 30.00 5.70 2 3 -26 2.20 3.60 2 3 -26 3.90 3.30 2 3 -26 5.70 4.00 2 3 -26 5.50 3.60 2 3 -26 1.50 3.80 1 3 -26 20.50 5.00 1 3 -26 19.20 4.70 1 3 -26 20.80 4.70 1 3 -26 16.70 4.60 1 3 -26 27.00 5.30 0 3 -26 2.40 3.50 0 3 -26 20.80 4.90 0 3 -26 14.40 4.70 0 3 -26 20.40 4.70 0 3 -26 11.10 4.50 7 2 -26 18.00 4.60 7 2 -26 19.10 4.90 7 2 -26 18.90 4.70 7 2 -26 14.20 5.00 7 2 -26 11.20 4.60 6 2 -26 31.00 5.60 6 2 -26 20.90 4.90 6 2 -26 38.70 6.30 6 2 -26 22.40 5.00 6 2 -26 33.10 5.60 5 2 -26 2.40 3.60 5 2 -26 -0.10 3.50 5 2 -26 9.80 4.20 5 2 -26 14.30 4.50 5 2 -26 9.00 4.00 4 2 -26 19.90 5.20 4 2 -26 11.60 4.60 4 2 -26 16.10 4.30 4 2 -26 7.20 4.10 4 2 -26 27.60 5.30 3 2 -26 -1.40 3.20 3 2 -26 1.20 3.60 3 2 -26 2.60 3.90 3 2 -26 0.50 3.60 3 2 -26 -0.40 3.50 2 2 -26 6.40 3.90 2 2 -26 4.60 3.90 2 2 -26 6.80 3.80 2 2 -26 12.70 4.20 2 2 -26 6.80 4.20 1 2 -26 5.50 3.90 1 2 -26 11.80 4.70 1 2 -26 11.60 4.20 1 2 -26 13.40 4.60 1 2 -26 6.30 3.90 0 2 -26 1.50 3.70 0 2 -26 2.10 3.90 0 2 -26 -1.40 3.40 0 2 -26 4.10 3.50 0 2 -26 -1.70 3.50 8 1 -26 17.60 4.80 8 1 -26 11.00 4.50 8 1 -26 16.40 4.80 8 1 -26 13.00 4.10 8 1 -26 13.20 5.00 7 1 -26 25.80 5.30 7 1 -26 31.70 5.40 7 1 -26 39.80 6.10 7 1 -26 37.90 6.70 7 1 -26 25.70 5.20 6 1 -26 19.60 5.50 6 1 -26 23.20 4.90 6 1 -26 13.90 4.70 6 1 -26 16.80 4.50 6 1 -26 21.50 4.70 5 1 -26 6.00 3.80 5 1 -26 -1.10 3.00 5 1 -26 1.10 3.80 5 1 -26 1.70 3.40 5 1 -26 1.30 3.20 4 1 -26 13.20 4.00 4 1 -26 7.70 4.10 4 1 -26 11.30 4.60 4 1 -26 10.30 4.20 4 1 -26 7.40 3.90 3 1 -26 2.70 3.90 3 1 -26 -3.20 2.80 3 1 -26 1.70 3.20 3 1 -26 2.60 3.50 3 1 -26 -1.70 3.10 2 1 -26 38.60 5.90 2 1 -26 32.70 5.70 2 1 -26 38.20 5.70 2 1 -26 33.30 5.70 2 1 -26 27.50 5.80 1 1 -26 13.00 5.00 1 1 -26 14.70 4.70 1 1 -26 11.20 4.50 1 1 -26 12.70 4.30 1 1 -26 12.90 4.70 0 1 -26 12.50 4.60 0 1 -26 9.30 4.50 0 1 -26 12.90 4.70 0 1 -26 5.80 3.90 0 1 -26 10.90 5.10 8 0 -26 2.90 4.10 8 0 -26 -2.60 3.30 8 0 -26 4.70 3.90 8 0 -26 -1.90 3.00 8 0 -26 2.50 3.70 -8 0 26 5.20 3.40 7 0 -26 -2.10 3.80 7 0 -26 2.70 3.50 7 0 -26 4.80 3.80 7 0 -26 -6.10 3.10 7 0 -26 1.40 3.30 -7 0 26 1.00 2.80 6 0 -26 -1.70 3.10 6 0 -26 -1.50 3.40 6 0 -26 -2.80 3.30 6 0 -26 -1.10 3.40 6 0 -26 3.10 3.60 -6 0 26 0.00 2.90 5 0 -26 -1.90 3.30 5 0 -26 -0.20 3.70 5 0 -26 -3.20 3.20 5 0 -26 3.50 4.10 5 0 -26 -0.40 3.50 -5 0 26 -0.50 2.70 4 0 -26 -1.80 3.30 4 0 -26 -0.40 3.70 4 0 -26 3.40 3.80 4 0 -26 7.60 3.70 4 0 -26 -1.10 3.80 -4 0 26 1.10 2.90 3 0 -26 -1.30 3.40 3 0 -26 6.50 4.10 3 0 -26 0.20 3.30 3 0 -26 3.80 3.50 3 0 -26 1.00 3.70 -3 0 26 2.00 2.80 2 0 -26 -4.50 3.10 2 0 -26 1.10 3.80 2 0 -26 4.50 3.60 2 0 -26 4.10 3.60 2 0 -26 1.90 4.00 -2 0 26 2.90 2.80 1 0 -26 17.80 5.20 1 0 -26 15.40 5.30 1 0 -26 12.80 4.40 1 0 -26 23.30 5.00 1 0 -26 21.90 4.60 8 -1 -26 87.59 8.70 8 -1 -26 62.99 6.80 8 -1 -26 39.40 7.20 8 -1 -26 57.39 7.40 8 -1 -26 63.09 6.80 -8 1 26 61.59 6.50 7 -1 -26 4.60 3.60 7 -1 -26 7.80 4.20 7 -1 -26 -1.30 3.80 7 -1 -26 3.30 3.30 7 -1 -26 6.10 4.10 -7 1 26 6.00 3.60 -7 1 26 -0.50 3.20 6 -1 -26 0.40 3.80 6 -1 -26 12.60 4.30 6 -1 -26 16.50 4.50 6 -1 -26 7.80 3.60 6 -1 -26 6.10 3.70 -6 1 26 8.70 3.60 -6 1 26 7.00 3.80 5 -1 -26 -0.70 3.50 5 -1 -26 -0.60 3.20 5 -1 -26 1.40 3.80 5 -1 -26 4.20 3.90 5 -1 -26 -2.10 3.30 -5 1 26 0.30 2.90 4 -1 -26 2.30 4.10 4 -1 -26 4.20 3.60 4 -1 -26 2.40 3.90 4 -1 -26 4.80 3.60 4 -1 -26 0.00 3.70 -4 1 26 7.00 3.30 3 -1 -26 16.20 5.20 3 -1 -26 9.10 4.50 3 -1 -26 16.30 4.60 3 -1 -26 10.60 4.00 3 -1 -26 10.40 4.60 -3 1 26 12.00 3.60 2 -1 -26 7.00 4.20 2 -1 -26 5.00 4.50 2 -1 -26 7.60 4.30 2 -1 -26 2.10 3.50 2 -1 -26 -0.70 3.10 -2 1 26 4.40 3.40 1 -1 -26 1.10 4.30 1 -1 -26 2.40 3.30 1 -1 -26 1.30 4.00 1 -1 -26 6.00 4.10 1 -1 -26 2.10 3.60 -1 1 26 4.70 3.10 8 -2 -26 6.70 3.60 8 -2 -26 9.70 4.60 8 -2 -26 6.50 4.80 -8 2 26 10.20 3.90 -8 2 26 9.40 3.90 7 -2 -26 -2.70 3.60 7 -2 -26 4.90 4.40 7 -2 -26 4.00 3.50 7 -2 -26 -1.50 3.60 -7 2 26 -4.10 3.10 -7 2 26 1.90 3.40 6 -2 -26 4.30 3.40 6 -2 -26 8.50 4.50 6 -2 -26 6.30 4.40 6 -2 -26 5.80 4.20 6 -2 -26 5.00 4.10 -6 2 26 7.50 4.00 -6 2 26 17.30 4.30 5 -2 -26 1.50 3.90 5 -2 -26 1.30 4.30 5 -2 -26 1.20 3.70 5 -2 -26 4.30 4.20 5 -2 -26 5.00 3.40 -5 2 26 8.30 3.70 -5 2 26 4.60 3.80 4 -2 -26 19.70 4.40 4 -2 -26 18.60 5.10 4 -2 -26 15.90 5.10 4 -2 -26 21.60 5.00 4 -2 -26 18.20 4.80 -4 2 26 20.40 4.30 3 -2 -26 -1.00 3.30 3 -2 -26 2.50 3.70 3 -2 -26 -0.10 3.90 3 -2 -26 -1.10 3.10 3 -2 -26 0.90 3.70 -3 2 26 4.70 3.40 2 -2 -26 -0.60 3.80 2 -2 -26 -1.20 3.20 2 -2 -26 -1.80 3.90 2 -2 -26 2.40 3.70 2 -2 -26 1.00 3.30 -2 2 26 2.80 3.40 7 -3 -26 19.60 5.20 7 -3 -26 18.40 5.60 7 -3 -26 7.20 4.30 -7 3 26 8.90 4.10 -7 3 26 11.30 4.30 -7 3 26 9.80 5.00 6 -3 -26 4.40 4.10 6 -3 -26 -3.00 3.90 6 -3 -26 6.30 3.80 -6 3 26 1.10 4.60 -6 3 26 -0.40 3.20 -6 3 26 -0.10 3.10 5 -3 -26 -3.10 4.20 5 -3 -26 -7.80 3.30 5 -3 -26 2.80 3.60 -5 3 26 -2.60 3.00 -5 3 26 -7.40 3.40 -5 3 26 -0.10 4.90 4 -3 -26 -1.80 4.10 4 -3 -26 1.20 3.70 4 -3 -26 -3.10 3.70 -4 3 26 -0.40 3.20 -4 3 26 -0.50 3.30 3 -3 -26 2.70 3.70 3 -3 -26 1.30 3.70 3 -3 -26 6.70 4.70 3 -3 -26 3.60 3.40 -3 3 26 3.50 3.40 5 2 -27 13.70 4.20 5 2 -27 8.50 4.00 5 2 -27 16.10 4.60 4 2 -27 25.00 5.30 4 2 -27 28.40 5.40 4 2 -27 21.90 5.30 4 2 -27 12.70 5.00 4 2 -27 26.70 5.10 3 2 -27 -1.00 3.70 3 2 -27 3.80 3.90 3 2 -27 -7.00 3.10 3 2 -27 0.40 4.10 3 2 -27 2.40 3.60 5 1 -27 2.00 3.20 5 1 -27 2.00 3.30 5 1 -27 0.40 3.50 5 1 -27 -1.20 3.30 5 1 -27 3.40 3.70 4 1 -27 1.30 3.90 4 1 -27 5.80 3.70 4 1 -27 -2.00 3.50 4 1 -27 0.60 3.10 4 1 -27 3.70 3.80 3 1 -27 49.99 7.40 3 1 -27 38.90 6.00 3 1 -27 53.69 7.10 3 1 -27 43.20 6.40 3 1 -27 47.10 6.40 5 0 -27 14.60 4.70 5 0 -27 7.80 4.30 5 0 -27 7.40 4.20 5 0 -27 11.40 4.50 5 0 -27 16.50 5.40 4 0 -27 18.90 4.60 4 0 -27 10.00 5.00 4 0 -27 17.80 4.60 4 0 -27 11.90 4.70 4 0 -27 16.20 5.00 5 -1 -27 0.90 4.20 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 91381 _shelx_shelxl_version_number 2014/7 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Co1 Co 0.56899(2) 0.66995(2) 0.24669(2) 0.02568(6) Uani 1 1 d . . . . K1 K 0.45867(4) 0.39044(3) 0.16115(2) 0.04698(11) Uani 1 1 d . . . . Si1 Si 0.50685(4) 0.71166(4) 0.14270(2) 0.02983(10) Uani 1 1 d . . . . N1 N 0.32894(10) 0.49106(10) 0.21611(6) 0.0255(2) Uani 1 1 d . . . . O1 O 0.59963(13) 0.25112(12) 0.19382(7) 0.0500(3) Uani 1 1 d . . . . C8 C 0.25340(13) 0.61439(12) 0.31865(7) 0.0254(3) Uani 1 1 d . . . . C23 C 0.15657(12) 0.30423(12) 0.11817(7) 0.0237(3) Uani 1 1 d . . . . C3 C 0.12153(12) 0.38471(12) 0.15700(7) 0.0237(3) Uani 1 1 d . . . . C7 C 0.17320(13) 0.53509(12) 0.25310(7) 0.0243(3) Uani 1 1 d . . . . C2 C 0.20944(12) 0.47398(11) 0.20921(7) 0.0222(3) Uani 1 1 d . . . . C34 C 0.15325(13) 0.30740(12) 0.04951(7) 0.0259(3) Uani 1 1 d . . . . C29 C 0.21906(13) 0.14541(13) 0.04855(8) 0.0299(3) Uani 1 1 d . . . . C33 C 0.18653(14) 0.22913(13) 0.01685(8) 0.0297(3) Uani 1 1 d . . . . H33 H 0.1869 0.2333 -0.0290 0.036 Uiso 1 1 calc R . . . C4 C 0.00096(13) 0.36601(13) 0.14499(8) 0.0299(3) Uani 1 1 d . . . . H4 H -0.0579 0.3070 0.1094 0.036 Uiso 1 1 calc R . . . C6 C 0.05142(14) 0.51400(14) 0.23852(8) 0.0312(3) Uani 1 1 d . . . . H6 H 0.0264 0.5570 0.2666 0.037 Uiso 1 1 calc R . . . C24 C 0.18934(13) 0.21991(12) 0.15144(7) 0.0277(3) Uani 1 1 d . . . . C28 C 0.21935(14) 0.14219(13) 0.11569(8) 0.0308(3) Uani 1 1 d . . . . H28 H 0.2407 0.0852 0.1382 0.037 Uiso 1 1 calc R . . . C1 C 0.42545(13) 0.57810(12) 0.23253(7) 0.0251(3) Uani 1 1 d . . . . C5 C -0.03413(13) 0.43259(15) 0.18448(8) 0.0339(3) Uani 1 1 d . . . . H5 H -0.1161 0.4224 0.1745 0.041 Uiso 1 1 calc R . . . C19 C 0.27533(14) 0.56606(13) 0.37835(8) 0.0301(3) Uani 1 1 d . . . . C25 C 0.18590(16) 0.20727(14) 0.22403(8) 0.0365(4) Uani 1 1 d . . . . H25 H 0.1849 0.2806 0.2450 0.044 Uiso 1 1 calc R . . . C9 C 0.28977(13) 0.73475(13) 0.32286(7) 0.0281(3) Uani 1 1 d . . . . C35 C 0.10890(14) 0.38916(13) 0.00875(8) 0.0303(3) Uani 1 1 d . . . . H35 H 0.1102 0.4517 0.0416 0.036 Uiso 1 1 calc R . . . C18 C 0.32901(15) 0.63916(14) 0.44097(8) 0.0345(3) Uani 1 1 d . . . . H18 H 0.3434 0.6065 0.4813 0.041 Uiso 1 1 calc R . . . C14 C 0.36198(15) 0.75814(14) 0.44606(8) 0.0335(3) Uani 1 1 d . . . . C40 C 0.75315(13) 0.75945(14) 0.26081(9) 0.0339(3) Uani 1 1 d . . . . C13 C 0.34299(14) 0.80401(14) 0.38667(8) 0.0326(3) Uani 1 1 d . . . . H13 H 0.3670 0.8856 0.3894 0.039 Uiso 1 1 calc R . . . C10 C 0.26994(15) 0.79022(14) 0.25922(8) 0.0344(3) Uani 1 1 d . . . . H10 H 0.2469 0.7292 0.2192 0.041 Uiso 1 1 calc R . . . C39 C 0.72935(13) 0.64254(14) 0.27133(9) 0.0334(3) Uani 1 1 d . . . . C38 C 0.67743(14) 0.62476(15) 0.32548(8) 0.0349(3) Uani 1 1 d . . . . C42 C 0.67102(14) 0.73071(16) 0.34920(8) 0.0367(4) Uani 1 1 d . . . . C41 C 0.71774(14) 0.81394(14) 0.30977(9) 0.0368(4) Uani 1 1 d . . . . C30 C 0.24808(16) 0.05939(15) 0.00823(9) 0.0393(4) Uani 1 1 d . . . . H30 H 0.3067 0.1051 -0.0149 0.047 Uiso 1 1 calc R . . . C20 C 0.23831(19) 0.43547(15) 0.37584(9) 0.0431(4) Uani 1 1 d . . . . H20 H 0.2322 0.4021 0.3292 0.052 Uiso 1 1 calc R . . . C15A C 0.412(2) 0.836(2) 0.5141(13) 0.0420(16) Uani 0.578(4) 1 d . P A 1 H15A H 0.4266 0.9165 0.5043 0.050 Uiso 0.578(4) 1 calc R P A 1 C48 C 0.54388(18) 0.63163(18) 0.07513(9) 0.0455(4) Uani 1 1 d . . . . H48A H 0.6270 0.6379 0.0922 0.068 Uiso 1 1 calc GR . . . H48B H 0.5338 0.6663 0.0336 0.068 Uiso 1 1 calc GR . . . H48C H 0.4897 0.5498 0.0651 0.068 Uiso 1 1 calc GR . . . C36 C 0.18732(18) 0.44672(16) -0.03569(9) 0.0430(4) Uani 1 1 d . . . . H36A H 0.2717 0.4802 -0.0082 0.064 Uiso 1 1 calc GR . . . H36B H 0.1636 0.5081 -0.0543 0.064 Uiso 1 1 calc GR . . . H36C H 0.1769 0.3887 -0.0731 0.064 Uiso 1 1 calc GR . . . C50 C 0.34172(15) 0.68032(16) 0.10376(9) 0.0394(4) Uani 1 1 d . . . . H50A H 0.2943 0.5992 0.1046 0.059 Uiso 1 1 calc GR . . . H50B H 0.3275 0.6946 0.0566 0.059 Uiso 1 1 calc GR . . . H50C H 0.3179 0.7309 0.1299 0.059 Uiso 1 1 calc GR . . . C12 C 0.38413(18) 0.88839(16) 0.25749(10) 0.0445(4) Uani 1 1 d . . . . H12A H 0.4075 0.9513 0.2950 0.067 Uiso 1 1 calc GR . . . H12B H 0.3696 0.9173 0.2141 0.067 Uiso 1 1 calc GR . . . H12C H 0.4487 0.8596 0.2622 0.067 Uiso 1 1 calc GR . . . C3AA C 0.1663(2) 0.8310(2) 0.25131(11) 0.0542(5) Uani 1 1 d . . . . H3AA H 0.0936 0.7657 0.2510 0.081 Uiso 1 1 calc GR . . . H3AB H 0.1523 0.8614 0.2084 0.081 Uiso 1 1 calc GR . . . H3AC H 0.1865 0.8921 0.2894 0.081 Uiso 1 1 calc GR . . . C49 C 0.57313(17) 0.87023(16) 0.13231(10) 0.0437(4) Uani 1 1 d . . . . H49A H 0.5578 0.9180 0.1653 0.066 Uiso 1 1 calc GR . . . H49B H 0.5358 0.8795 0.0861 0.066 Uiso 1 1 calc GR . . . H49C H 0.6598 0.8947 0.1402 0.066 Uiso 1 1 calc GR . . . C45 C 0.82639(16) 0.81883(19) 0.21599(11) 0.0512(5) Uani 1 1 d . . . . H45A H 0.7931 0.7729 0.1703 0.077 Uiso 1 1 calc GR . . . H45B H 0.9096 0.8263 0.2351 0.077 Uiso 1 1 calc GR . . . H45C H 0.8242 0.8960 0.2133 0.077 Uiso 1 1 calc GR . . . C44 C 0.76515(19) 0.5604(2) 0.23450(13) 0.0503(5) Uani 1 1 d . . . . C31 C 0.3056(2) -0.01185(19) 0.05146(12) 0.0577(5) Uani 1 1 d . . . . H31A H 0.3754 0.0401 0.0882 0.087 Uiso 1 1 calc GR . . . H31B H 0.3312 -0.0573 0.0230 0.087 Uiso 1 1 calc GR . . . H31C H 0.2472 -0.0642 0.0710 0.087 Uiso 1 1 calc GR . . . C37 C -0.02072(17) 0.32525(18) -0.03635(10) 0.0475(4) Uani 1 1 d . . . . H37A H -0.0249 0.2615 -0.0679 0.071 Uiso 1 1 calc GR . . . H37B H -0.0475 0.3792 -0.0622 0.071 Uiso 1 1 calc GR . . . H37C H -0.0727 0.2942 -0.0078 0.071 Uiso 1 1 calc GR . . . C26 C 0.2941(2) 0.1898(2) 0.26834(10) 0.0579(5) Uani 1 1 d . . . . H26A H 0.2984 0.1190 0.2487 0.087 Uiso 1 1 calc GR . . . H26B H 0.2862 0.1827 0.3142 0.087 Uiso 1 1 calc GR . . . H26C H 0.3673 0.2563 0.2707 0.087 Uiso 1 1 calc GR . . . C53 C 0.63639(19) 0.20767(18) 0.14236(11) 0.0521(5) Uani 1 1 d . . . . H53A H 0.5968 0.1221 0.1322 0.063 Uiso 1 1 calc R . . . H53B H 0.7243 0.2292 0.1576 0.063 Uiso 1 1 calc R . . . C46 C 0.73761(19) 0.94029(17) 0.32117(12) 0.0574(5) Uani 1 1 d . . . . H46A H 0.7395 0.9714 0.2787 0.086 Uiso 1 1 calc GR . . . H46B H 0.8141 0.9829 0.3562 0.086 Uiso 1 1 calc GR . . . H46C H 0.6722 0.9488 0.3360 0.086 Uiso 1 1 calc GR . . . C32 C 0.1359(2) -0.01982(19) -0.04709(11) 0.0608(6) Uani 1 1 d . . . . H32A H 0.0760 -0.0656 -0.0262 0.091 Uiso 1 1 calc GR . . . H32B H 0.1564 -0.0719 -0.0744 0.091 Uiso 1 1 calc GR . . . H32C H 0.1031 0.0270 -0.0764 0.091 Uiso 1 1 calc GR . . . C43 C 0.63917(19) 0.51415(19) 0.35469(11) 0.0553(5) Uani 1 1 d . . . . H43A H 0.5636 0.5017 0.3649 0.083 Uiso 1 1 calc GR . . . H43B H 0.7012 0.5199 0.3966 0.083 Uiso 1 1 calc GR . . . H43C H 0.6279 0.4490 0.3216 0.083 Uiso 1 1 calc GR . . . C47 C 0.6265(2) 0.7511(2) 0.40825(10) 0.0593(6) Uani 1 1 d . . . . H47A H 0.5952 0.8124 0.4017 0.089 Uiso 1 1 calc GR . . . H47B H 0.6929 0.7746 0.4505 0.089 Uiso 1 1 calc GR . . . H47C H 0.5626 0.6796 0.4110 0.089 Uiso 1 1 calc GR . . . C22 C 0.3296(2) 0.4032(2) 0.42612(13) 0.0639(6) Uani 1 1 d . . . . H22A H 0.4093 0.4429 0.4206 0.096 Uiso 1 1 calc GR . . . H22B H 0.3075 0.3192 0.4176 0.096 Uiso 1 1 calc GR . . . H22C H 0.3310 0.4266 0.4726 0.096 Uiso 1 1 calc GR . . . C27 C 0.0701(2) 0.1089(2) 0.22384(11) 0.0616(6) Uani 1 1 d . . . . H27A H 0.0010 0.1246 0.1983 0.092 Uiso 1 1 calc GR . . . H27B H 0.0679 0.1030 0.2707 0.092 Uiso 1 1 calc GR . . . H27C H 0.0673 0.0358 0.2023 0.092 Uiso 1 1 calc GR . . . C54 C 0.6020(3) 0.2587(3) 0.08027(15) 0.0718(7) Uani 1 1 d . . . . C57 C 1.0290(3) 0.7989(3) 0.41418(14) 0.0811(8) Uani 1 1 d . . . . H57A H 1.1100 0.8042 0.4141 0.097 Uiso 1 1 calc R . . . H57B H 0.9779 0.7794 0.3663 0.097 Uiso 1 1 calc R . . . C52 C 0.6266(2) 0.2042(2) 0.25539(12) 0.0645(6) Uani 1 1 d . . . . H52A H 0.5950 0.1188 0.2441 0.077 Uiso 1 1 calc R . . . H52B H 0.5846 0.2239 0.2860 0.077 Uiso 1 1 calc R . . . C51 C 0.7592(3) 0.2481(3) 0.29273(14) 0.0826(8) Uani 1 1 d . . . . H51A H 0.8006 0.2229 0.2644 0.124 Uiso 1 1 calc GR . . . H51B H 0.7709 0.2170 0.3355 0.124 Uiso 1 1 calc GR . . . H51C H 0.7921 0.3329 0.3025 0.124 Uiso 1 1 calc GR . . . C56 C 0.9784(3) 0.7034(3) 0.45135(16) 0.0878(9) Uani 1 1 d . . . . H56A H 1.0263 0.7245 0.4999 0.105 Uiso 1 1 calc R . . . H56B H 0.8952 0.6941 0.4488 0.105 Uiso 1 1 calc R . . . C58 C 1.0381(3) 0.9132(3) 0.44340(17) 0.0965(10) Uani 1 1 d . . . . H58A H 1.0843 0.9296 0.4921 0.116 Uiso 1 1 calc R . . . H58B H 0.9563 0.9086 0.4408 0.116 Uiso 1 1 calc R . . . C21 C 0.1171(3) 0.3798(2) 0.3864(2) 0.0986(11) Uani 1 1 d . . . . H21A H 0.1215 0.4060 0.4330 0.148 Uiso 1 1 calc GR . . . H21B H 0.0921 0.2954 0.3789 0.148 Uiso 1 1 calc GR . . . H21C H 0.0587 0.4015 0.3542 0.148 Uiso 1 1 calc GR . . . C16A C 0.5348(6) 0.8360(7) 0.5538(4) 0.085(3) Uani 0.578(4) 1 d . P A 1 H16A H 0.5259 0.7571 0.5616 0.127 Uiso 0.578(4) 1 calc GR P A 1 H16B H 0.5652 0.8873 0.5976 0.127 Uiso 0.578(4) 1 calc GR P A 1 H16C H 0.5915 0.8635 0.5273 0.127 Uiso 0.578(4) 1 calc GR P A 1 C55 C 0.9778(4) 0.5939(4) 0.4238(2) 0.1143(12) Uani 1 1 d . . . . H55A H 0.9299 0.5721 0.3759 0.172 Uiso 1 1 calc GR . . . H55B H 0.9430 0.5338 0.4494 0.172 Uiso 1 1 calc GR . . . H55C H 1.0603 0.6019 0.4276 0.172 Uiso 1 1 calc GR . . . C59 C 1.0960(4) 1.0135(4) 0.4102(2) 0.1256(14) Uani 1 1 d . . . . H59A H 1.0543 0.9967 0.3613 0.188 Uiso 1 1 calc GR . . . H59B H 1.1804 1.0255 0.4174 0.188 Uiso 1 1 calc GR . . . H59C H 1.0910 1.0836 0.4304 0.188 Uiso 1 1 calc GR . . . C17A C 0.3233(4) 0.8103(5) 0.5560(2) 0.0718(11) Uani 0.578(4) 1 d . P A 1 H17A H 0.2510 0.8216 0.5310 0.108 Uiso 0.578(4) 1 calc GR P A 1 H17B H 0.3606 0.8628 0.5996 0.108 Uiso 0.578(4) 1 calc GR P A 1 H17C H 0.3016 0.7300 0.5642 0.108 Uiso 0.578(4) 1 calc GR P A 1 H44A H 0.722(2) 0.482(2) 0.2409(11) 0.059(7) Uiso 1 1 d . . . . H44B H 0.745(2) 0.559(2) 0.1838(15) 0.082(8) Uiso 1 1 d . . . . H44C H 0.845(3) 0.578(2) 0.2502(14) 0.083(8) Uiso 1 1 d . . . . H54A H 0.520(3) 0.237(3) 0.0639(16) 0.093(10) Uiso 1 1 d . . . . H54B H 0.641(3) 0.340(3) 0.0886(14) 0.087(9) Uiso 1 1 d . . . . H54C H 0.628(3) 0.238(3) 0.0486(18) 0.101(11) Uiso 1 1 d . . . . C16B C 0.4846(8) 0.7910(10) 0.5693(6) 0.085(3) Uani 0.422(4) 1 d . P A 2 H16D H 0.4235 0.7256 0.5800 0.127 Uiso 0.422(4) 1 calc GR P A 2 H16E H 0.5287 0.8502 0.6100 0.127 Uiso 0.422(4) 1 calc GR P A 2 H16F H 0.5405 0.7642 0.5544 0.127 Uiso 0.422(4) 1 calc GR P A 2 C15B C 0.427(3) 0.840(3) 0.5155(18) 0.0420(16) Uani 0.422(4) 1 d . P A 2 H15B H 0.4928 0.9075 0.5077 0.050 Uiso 0.422(4) 1 calc R P A 2 C17B C 0.3433(6) 0.8869(7) 0.5342(3) 0.0718(11) Uani 0.422(4) 1 d . P A 2 H17D H 0.3180 0.9301 0.4991 0.108 Uiso 0.422(4) 1 calc GR P A 2 H17E H 0.3838 0.9388 0.5780 0.108 Uiso 0.422(4) 1 calc GR P A 2 H17F H 0.2727 0.8229 0.5378 0.108 Uiso 0.422(4) 1 calc GR P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Co1 0.01996(10) 0.02581(10) 0.03057(11) 0.00213(8) 0.00733(8) 0.00843(8) K1 0.0443(2) 0.0369(2) 0.0672(3) 0.00055(18) 0.0246(2) 0.01957(17) Si1 0.0287(2) 0.0313(2) 0.0314(2) 0.00424(17) 0.01046(17) 0.01262(17) N1 0.0224(6) 0.0249(6) 0.0294(6) 0.0013(5) 0.0075(5) 0.0099(5) O1 0.0581(8) 0.0448(7) 0.0550(8) 0.0125(6) 0.0200(7) 0.0260(7) C8 0.0259(7) 0.0274(7) 0.0253(7) 0.0009(5) 0.0086(5) 0.0129(6) C23 0.0213(6) 0.0210(6) 0.0257(7) 0.0002(5) 0.0046(5) 0.0065(5) C3 0.0253(7) 0.0232(6) 0.0235(6) 0.0045(5) 0.0073(5) 0.0100(5) C7 0.0268(7) 0.0235(6) 0.0246(7) 0.0048(5) 0.0084(5) 0.0114(5) C2 0.0221(6) 0.0220(6) 0.0236(6) 0.0053(5) 0.0068(5) 0.0093(5) C34 0.0244(7) 0.0250(7) 0.0261(7) 0.0015(5) 0.0064(5) 0.0083(6) C29 0.0266(7) 0.0246(7) 0.0357(8) -0.0027(6) 0.0071(6) 0.0090(6) C33 0.0319(8) 0.0301(7) 0.0275(7) 0.0013(6) 0.0096(6) 0.0123(6) C4 0.0236(7) 0.0307(7) 0.0296(7) 0.0002(6) 0.0034(6) 0.0077(6) C6 0.0298(7) 0.0366(8) 0.0321(8) 0.0013(6) 0.0113(6) 0.0176(6) C24 0.0288(7) 0.0236(7) 0.0269(7) 0.0011(5) 0.0041(6) 0.0088(6) C28 0.0338(8) 0.0235(7) 0.0332(8) 0.0024(6) 0.0048(6) 0.0126(6) C1 0.0276(7) 0.0265(7) 0.0250(7) 0.0033(5) 0.0086(5) 0.0142(6) C5 0.0222(7) 0.0429(9) 0.0370(8) 0.0029(7) 0.0073(6) 0.0144(7) C19 0.0352(8) 0.0300(7) 0.0279(7) 0.0030(6) 0.0096(6) 0.0158(6) C25 0.0532(10) 0.0292(8) 0.0269(7) 0.0054(6) 0.0075(7) 0.0185(7) C9 0.0292(7) 0.0284(7) 0.0296(7) 0.0026(6) 0.0101(6) 0.0136(6) C35 0.0353(8) 0.0316(8) 0.0268(7) 0.0054(6) 0.0080(6) 0.0168(6) C18 0.0421(9) 0.0386(9) 0.0249(7) 0.0046(6) 0.0080(6) 0.0192(7) C14 0.0352(8) 0.0355(8) 0.0290(7) -0.0038(6) 0.0065(6) 0.0158(7) C40 0.0219(7) 0.0329(8) 0.0432(9) 0.0040(7) 0.0077(6) 0.0076(6) C13 0.0370(8) 0.0271(7) 0.0339(8) -0.0001(6) 0.0100(6) 0.0133(6) C10 0.0444(9) 0.0288(8) 0.0322(8) 0.0053(6) 0.0117(7) 0.0163(7) C39 0.0221(7) 0.0344(8) 0.0431(9) 0.0024(7) 0.0068(6) 0.0126(6) C38 0.0258(7) 0.0382(8) 0.0386(8) 0.0088(7) 0.0052(6) 0.0124(6) C42 0.0264(7) 0.0474(10) 0.0327(8) -0.0018(7) 0.0031(6) 0.0153(7) C41 0.0260(7) 0.0314(8) 0.0454(9) -0.0045(7) 0.0022(7) 0.0096(6) C30 0.0428(9) 0.0319(8) 0.0465(10) -0.0024(7) 0.0161(8) 0.0172(7) C20 0.0686(12) 0.0320(8) 0.0285(8) 0.0061(7) 0.0099(8) 0.0220(8) C15A 0.050(5) 0.0401(19) 0.0303(12) -0.0061(11) 0.003(3) 0.019(3) C48 0.0509(11) 0.0559(11) 0.0382(9) 0.0027(8) 0.0156(8) 0.0293(9) C36 0.0549(11) 0.0454(10) 0.0370(9) 0.0172(8) 0.0183(8) 0.0240(9) C50 0.0350(9) 0.0499(10) 0.0330(8) 0.0072(7) 0.0081(7) 0.0173(8) C12 0.0546(11) 0.0357(9) 0.0451(10) 0.0101(7) 0.0206(8) 0.0148(8) C3AA 0.0563(12) 0.0595(12) 0.0580(12) 0.0234(10) 0.0148(10) 0.0347(10) C49 0.0470(10) 0.0402(9) 0.0464(10) 0.0133(8) 0.0173(8) 0.0160(8) C45 0.0302(9) 0.0580(12) 0.0634(12) 0.0192(10) 0.0183(8) 0.0102(8) C44 0.0385(10) 0.0509(12) 0.0658(14) -0.0035(10) 0.0121(9) 0.0261(9) C31 0.0644(13) 0.0496(11) 0.0694(14) -0.0019(10) 0.0143(11) 0.0390(11) C37 0.0408(10) 0.0530(11) 0.0442(10) 0.0078(8) 0.0001(8) 0.0214(9) C26 0.0627(13) 0.0672(14) 0.0367(10) 0.0149(9) 0.0001(9) 0.0260(11) C53 0.0512(11) 0.0431(10) 0.0590(12) 0.0007(9) 0.0158(9) 0.0160(9) C46 0.0488(11) 0.0349(10) 0.0736(14) -0.0096(9) -0.0005(10) 0.0145(9) C32 0.0682(14) 0.0456(11) 0.0574(12) -0.0204(9) 0.0018(10) 0.0247(10) C43 0.0477(11) 0.0552(12) 0.0626(13) 0.0274(10) 0.0131(10) 0.0192(10) C47 0.0513(12) 0.0910(17) 0.0376(10) -0.0048(10) 0.0099(9) 0.0339(12) C22 0.0804(16) 0.0501(12) 0.0717(15) 0.0213(11) 0.0167(12) 0.0396(12) C27 0.0617(13) 0.0746(15) 0.0456(11) 0.0241(11) 0.0228(10) 0.0160(11) C54 0.087(2) 0.0656(17) 0.0579(15) 0.0097(12) 0.0229(15) 0.0230(16) C57 0.0685(17) 0.122(3) 0.0614(15) 0.0269(16) 0.0205(13) 0.0434(17) C52 0.0818(17) 0.0600(13) 0.0647(14) 0.0280(11) 0.0320(13) 0.0326(12) C51 0.094(2) 0.0781(18) 0.0713(17) 0.0274(14) 0.0055(15) 0.0394(16) C56 0.0670(17) 0.123(3) 0.0733(18) 0.0181(18) 0.0147(14) 0.0395(18) C58 0.092(2) 0.120(3) 0.083(2) 0.018(2) 0.0261(18) 0.048(2) C21 0.0645(16) 0.0492(14) 0.169(3) 0.0496(18) 0.0231(19) 0.0107(12) C16A 0.070(4) 0.104(6) 0.062(4) -0.045(4) -0.028(3) 0.053(4) C55 0.121(3) 0.135(3) 0.113(3) 0.026(2) 0.033(2) 0.080(3) C59 0.148(4) 0.139(3) 0.102(3) 0.053(3) 0.055(3) 0.053(3) C17A 0.072(2) 0.088(3) 0.047(2) -0.0225(19) 0.0208(16) 0.022(2) C16B 0.070(4) 0.104(6) 0.062(4) -0.045(4) -0.028(3) 0.053(4) C15B 0.050(5) 0.0401(19) 0.0303(12) -0.0061(11) 0.003(3) 0.019(3) C17B 0.072(2) 0.088(3) 0.047(2) -0.0225(19) 0.0208(16) 0.022(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' K K 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle Si1 Co1 K1 83.717(15) C1 Co1 K1 57.51(5) C1 Co1 Si1 85.99(5) C1 Co1 C40 170.46(6) C1 Co1 C39 131.37(6) C1 Co1 C38 108.62(7) C1 Co1 C42 116.04(7) C1 Co1 C41 147.50(7) C40 Co1 K1 113.37(5) C40 Co1 Si1 96.09(5) C40 Co1 C42 66.18(7) C40 Co1 C41 39.63(6) C39 Co1 K1 81.80(4) C39 Co1 Si1 117.18(5) C39 Co1 C40 39.79(6) C39 Co1 C42 66.67(6) C39 Co1 C41 66.59(6) C38 Co1 K1 89.18(5) C38 Co1 Si1 156.87(5) C38 Co1 C40 66.64(6) C38 Co1 C39 39.78(6) C38 Co1 C42 39.90(7) C38 Co1 C41 66.36(7) C42 Co1 K1 127.21(5) C42 Co1 Si1 148.00(5) C42 Co1 C41 38.95(7) C41 Co1 K1 148.38(4) C41 Co1 Si1 110.70(5) Co1 K1 Si1 34.799(8) Co1 K1 C44 55.81(3) Co1 K1 C54 128.32(6) Co1 K1 H44A 65.8(5) Si1 K1 H44A 86.4(5) N1 K1 Co1 54.45(3) N1 K1 Si1 61.58(3) N1 K1 O1 141.33(4) N1 K1 C23 52.95(3) N1 K1 C24 64.60(4) N1 K1 C28 89.13(4) N1 K1 C1 25.25(4) N1 K1 C44 107.95(4) N1 K1 C54 175.36(6) N1 K1 H44A 113.0(4) O1 K1 Co1 119.07(3) O1 K1 Si1 138.92(3) O1 K1 C23 128.09(4) O1 K1 C24 104.68(4) O1 K1 C28 86.50(4) O1 K1 C1 136.71(4) O1 K1 C44 67.90(5) O1 K1 C54 42.23(5) O1 K1 H44A 54.9(5) C23 K1 Co1 104.90(2) C23 K1 Si1 92.98(3) C23 K1 C44 160.59(4) C23 K1 C54 123.05(6) C23 K1 H44A 163.1(4) C24 K1 Co1 118.89(3) C24 K1 Si1 116.13(3) C24 K1 C23 24.52(3) C24 K1 C28 24.58(4) C24 K1 C44 158.73(5) C24 K1 C54 112.78(6) C24 K1 H44A 146.9(5) C28 K1 Co1 143.47(3) C28 K1 Si1 133.77(3) C28 K1 C23 42.33(3) C28 K1 C44 154.04(5) C28 K1 C54 88.21(6) C28 K1 H44A 139.7(5) C1 K1 Co1 29.21(3) C1 K1 Si1 43.91(3) C1 K1 C23 76.77(4) C1 K1 C24 89.81(4) C1 K1 C28 114.36(4) C1 K1 C44 83.83(4) C1 K1 C54 157.26(7) C1 K1 H44A 91.3(4) C44 K1 Si1 72.19(4) C44 K1 H44A 14.8(5) C54 K1 Si1 118.12(5) C54 K1 C44 75.87(7) C54 K1 H44A 71.4(4) Co1 Si1 K1 61.484(13) C48 Si1 Co1 112.45(6) C48 Si1 K1 65.23(6) C50 Si1 Co1 119.25(6) C50 Si1 K1 94.80(6) C50 Si1 C48 103.21(8) C50 Si1 C49 99.53(8) C49 Si1 Co1 116.32(6) C49 Si1 K1 163.87(6) C49 Si1 C48 103.99(9) C2 N1 K1 138.95(9) C1 N1 K1 83.31(8) C1 N1 C2 134.25(12) C53 O1 K1 119.27(11) C53 O1 C52 112.07(16) C52 O1 K1 128.09(13) C19 C8 C7 118.86(13) C9 C8 C7 120.67(13) C9 C8 C19 119.67(13) C3 C23 K1 110.88(8) C34 C23 K1 89.35(8) C34 C23 C3 122.27(12) C34 C23 C24 119.39(13) C24 C23 K1 71.33(8) C24 C23 C3 118.29(12) C2 C3 C23 120.44(12) C4 C3 C23 119.70(12) C4 C3 C2 119.69(13) C2 C7 C8 125.59(12) C6 C7 C8 115.95(12) C6 C7 C2 118.23(13) N1 C2 C3 116.36(12) N1 C2 C7 123.98(12) C7 C2 C3 119.55(12) C23 C34 C35 122.25(13) C33 C34 C23 118.79(13) C33 C34 C35 118.89(13) C33 C29 C30 119.49(14) C28 C29 C33 117.49(13) C28 C29 C30 122.98(14) C34 C33 H33 118.6 C29 C33 C34 122.79(14) C29 C33 H33 118.6 C3 C4 H4 119.7 C5 C4 C3 120.66(14) C5 C4 H4 119.7 C7 C6 H6 118.9 C5 C6 C7 122.14(14) C5 C6 H6 118.9 C23 C24 K1 84.15(8) C23 C24 C25 121.48(13) C28 C24 K1 81.97(9) C28 C24 C23 119.24(13) C28 C24 C25 119.19(13) C25 C24 K1 106.79(10) K1 C28 H28 108.1 C29 C28 K1 89.15(9) C29 C28 C24 122.26(14) C29 C28 H28 118.9 C24 C28 K1 73.45(8) C24 C28 H28 118.9 Co1 C1 K1 93.28(6) N1 C1 Co1 164.62(12) N1 C1 K1 71.44(8) C4 C5 H5 120.4 C6 C5 C4 119.30(14) C6 C5 H5 120.4 C8 C19 C20 121.26(13) C18 C19 C8 119.03(14) C18 C19 C20 119.69(14) C24 C25 H25 107.4 C24 C25 C27 110.23(14) C26 C25 C24 113.79(16) C26 C25 H25 107.4 C26 C25 C27 110.31(16) C27 C25 H25 107.4 C8 C9 C10 121.11(13) C13 C9 C8 119.03(14) C13 C9 C10 119.85(13) C34 C35 H35 108.0 C34 C35 C36 113.04(13) C34 C35 C37 110.72(13) C36 C35 H35 108.0 C36 C35 C37 109.02(14) C37 C35 H35 108.0 C19 C18 H18 119.0 C14 C18 C19 121.91(15) C14 C18 H18 119.0 C18 C14 C15A 121.7(11) C18 C14 C15B 121.8(14) C13 C14 C18 118.05(14) C13 C14 C15A 120.2(11) C13 C14 C15B 120.0(15) C39 C40 Co1 69.77(9) C39 C40 C41 108.12(15) C39 C40 C45 124.17(16) C41 C40 Co1 71.07(9) C41 C40 C45 126.53(16) C45 C40 Co1 134.43(13) C9 C13 H13 118.9 C14 C13 C9 122.25(14) C14 C13 H13 118.9 C9 C10 H10 107.3 C9 C10 C12 111.94(14) C9 C10 C3AA 111.45(14) C12 C10 H10 107.3 C12 C10 C3AA 111.25(15) C3AA C10 H10 107.3 C40 C39 Co1 70.44(9) C40 C39 C44 124.16(17) C38 C39 Co1 69.51(9) C38 C39 C40 107.52(14) C38 C39 C44 128.10(17) C44 C39 Co1 129.56(13) C39 C38 Co1 70.71(9) C39 C38 C42 108.28(15) C39 C38 C43 126.04(17) C42 C38 Co1 71.07(9) C42 C38 C43 125.65(17) C43 C38 Co1 125.46(12) C38 C42 Co1 69.03(9) C38 C42 C47 125.62(18) C41 C42 Co1 71.34(9) C41 C42 C38 108.35(14) C41 C42 C47 125.99(17) C47 C42 Co1 127.25(12) C40 C41 Co1 69.30(9) C40 C41 C46 125.91(18) C42 C41 Co1 69.71(9) C42 C41 C40 107.72(14) C42 C41 C46 126.15(17) C46 C41 Co1 130.61(13) C29 C30 H30 107.3 C31 C30 C29 114.31(15) C31 C30 H30 107.3 C32 C30 C29 110.09(15) C32 C30 H30 107.3 C32 C30 C31 110.36(16) C19 C20 H20 107.3 C22 C20 C19 113.04(16) C22 C20 H20 107.3 C21 C20 C19 111.84(17) C21 C20 H20 107.3 C21 C20 C22 109.75(19) C14 C15A H15A 106.5 C14 C15A C16A 111.1(14) C14 C15A C17A 113.1(16) C16A C15A H15A 106.5 C17A C15A H15A 106.5 C17A C15A C16A 112.7(17) Si1 C48 H48A 109.5 Si1 C48 H48B 109.5 Si1 C48 H48C 109.5 H48A C48 H48B 109.5 H48A C48 H48C 109.5 H48B C48 H48C 109.5 C35 C36 H36A 109.5 C35 C36 H36B 109.5 C35 C36 H36C 109.5 H36A C36 H36B 109.5 H36A C36 H36C 109.5 H36B C36 H36C 109.5 Si1 C50 H50A 109.5 Si1 C50 H50B 109.5 Si1 C50 H50C 109.5 H50A C50 H50B 109.5 H50A C50 H50C 109.5 H50B C50 H50C 109.5 C10 C12 H12A 109.5 C10 C12 H12B 109.5 C10 C12 H12C 109.5 H12A C12 H12B 109.5 H12A C12 H12C 109.5 H12B C12 H12C 109.5 C10 C3AA H3AA 109.5 C10 C3AA H3AB 109.5 C10 C3AA H3AC 109.5 H3AA C3AA H3AB 109.5 H3AA C3AA H3AC 109.5 H3AB C3AA H3AC 109.5 Si1 C49 H49A 109.5 Si1 C49 H49B 109.5 Si1 C49 H49C 109.5 H49A C49 H49B 109.5 H49A C49 H49C 109.5 H49B C49 H49C 109.5 C40 C45 H45A 109.5 C40 C45 H45B 109.5 C40 C45 H45C 109.5 H45A C45 H45B 109.5 H45A C45 H45C 109.5 H45B C45 H45C 109.5 K1 C44 H44A 53.1(14) K1 C44 H44B 71.5(16) K1 C44 H44C 158.4(18) C39 C44 K1 88.02(10) C39 C44 H44A 109.1(14) C39 C44 H44B 113.9(16) C39 C44 H44C 111.2(18) H44A C44 H44B 106(2) H44A C44 H44C 109(2) H44B C44 H44C 107(2) C30 C31 H31A 109.5 C30 C31 H31B 109.5 C30 C31 H31C 109.5 H31A C31 H31B 109.5 H31A C31 H31C 109.5 H31B C31 H31C 109.5 C35 C37 H37A 109.5 C35 C37 H37B 109.5 C35 C37 H37C 109.5 H37A C37 H37B 109.5 H37A C37 H37C 109.5 H37B C37 H37C 109.5 C25 C26 H26A 109.5 C25 C26 H26B 109.5 C25 C26 H26C 109.5 H26A C26 H26B 109.5 H26A C26 H26C 109.5 H26B C26 H26C 109.5 O1 C53 H53A 110.1 O1 C53 H53B 110.1 O1 C53 C54 108.1(2) H53A C53 H53B 108.4 C54 C53 H53A 110.1 C54 C53 H53B 110.1 C41 C46 H46A 109.5 C41 C46 H46B 109.5 C41 C46 H46C 109.5 H46A C46 H46B 109.5 H46A C46 H46C 109.5 H46B C46 H46C 109.5 C30 C32 H32A 109.5 C30 C32 H32B 109.5 C30 C32 H32C 109.5 H32A C32 H32B 109.5 H32A C32 H32C 109.5 H32B C32 H32C 109.5 C38 C43 H43A 109.5 C38 C43 H43B 109.5 C38 C43 H43C 109.5 H43A C43 H43B 109.5 H43A C43 H43C 109.5 H43B C43 H43C 109.5 C42 C47 H47A 109.5 C42 C47 H47B 109.5 C42 C47 H47C 109.5 H47A C47 H47B 109.5 H47A C47 H47C 109.5 H47B C47 H47C 109.5 C20 C22 H22A 109.5 C20 C22 H22B 109.5 C20 C22 H22C 109.5 H22A C22 H22B 109.5 H22A C22 H22C 109.5 H22B C22 H22C 109.5 C25 C27 H27A 109.5 C25 C27 H27B 109.5 C25 C27 H27C 109.5 H27A C27 H27B 109.5 H27A C27 H27C 109.5 H27B C27 H27C 109.5 K1 C54 H54A 60(2) K1 C54 H54B 67.8(18) K1 C54 H54C 160(2) C53 C54 K1 90.05(16) C53 C54 H54A 111(2) C53 C54 H54B 111.2(18) C53 C54 H54C 110(2) H54A C54 H54B 111(3) H54A C54 H54C 109(3) H54B C54 H54C 103(3) H57A C57 H57B 107.7 C56 C57 H57A 108.8 C56 C57 H57B 108.8 C58 C57 H57A 108.8 C58 C57 H57B 108.8 C58 C57 C56 114.0(3) O1 C52 H52A 108.8 O1 C52 H52B 108.8 O1 C52 C51 113.7(2) H52A C52 H52B 107.7 C51 C52 H52A 108.8 C51 C52 H52B 108.8 C52 C51 H51A 109.5 C52 C51 H51B 109.5 C52 C51 H51C 109.5 H51A C51 H51B 109.5 H51A C51 H51C 109.5 H51B C51 H51C 109.5 C57 C56 H56A 109.1 C57 C56 H56B 109.1 H56A C56 H56B 107.8 C55 C56 C57 112.4(3) C55 C56 H56A 109.1 C55 C56 H56B 109.1 C57 C58 H58A 108.3 C57 C58 H58B 108.3 C57 C58 C59 115.8(3) H58A C58 H58B 107.4 C59 C58 H58A 108.3 C59 C58 H58B 108.3 C20 C21 H21A 109.5 C20 C21 H21B 109.5 C20 C21 H21C 109.5 H21A C21 H21B 109.5 H21A C21 H21C 109.5 H21B C21 H21C 109.5 C15A C16A H16A 109.5 C15A C16A H16B 109.5 C15A C16A H16C 109.5 H16A C16A H16B 109.5 H16A C16A H16C 109.5 H16B C16A H16C 109.5 C56 C55 H55A 109.5 C56 C55 H55B 109.5 C56 C55 H55C 109.5 H55A C55 H55B 109.5 H55A C55 H55C 109.5 H55B C55 H55C 109.5 C58 C59 H59A 109.5 C58 C59 H59B 109.5 C58 C59 H59C 109.5 H59A C59 H59B 109.5 H59A C59 H59C 109.5 H59B C59 H59C 109.5 C15A C17A H17A 109.5 C15A C17A H17B 109.5 C15A C17A H17C 109.5 H17A C17A H17B 109.5 H17A C17A H17C 109.5 H17B C17A H17C 109.5 H16D C16B H16E 109.5 H16D C16B H16F 109.5 H16E C16B H16F 109.5 C15B C16B H16D 109.5 C15B C16B H16E 109.5 C15B C16B H16F 109.5 C14 C15B H15B 106.2 C16B C15B C14 115(2) C16B C15B H15B 106.2 C16B C15B C17B 114(2) C17B C15B C14 109.0(19) C17B C15B H15B 106.2 C15B C17B H17D 109.5 C15B C17B H17E 109.5 C15B C17B H17F 109.5 H17D C17B H17E 109.5 H17D C17B H17F 109.5 H17E C17B H17F 109.5 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Co1 K1 3.4509(4) Co1 Si1 2.2414(5) Co1 C1 1.6867(15) Co1 C40 2.1004(15) Co1 C39 2.0916(15) Co1 C38 2.0757(16) Co1 C42 2.1026(16) Co1 C41 2.1240(16) K1 Si1 3.9037(6) K1 N1 2.7829(12) K1 O1 2.8822(14) K1 C23 3.3854(14) K1 C24 3.2240(15) K1 C28 3.3304(16) K1 C1 2.9156(14) K1 C44 3.512(2) K1 C54 3.472(4) K1 H44A 3.03(2) Si1 C48 1.9161(18) Si1 C50 1.8949(17) Si1 C49 1.9069(18) N1 C2 1.3977(17) N1 C1 1.2524(19) O1 C53 1.414(2) O1 C52 1.439(3) C8 C7 1.5056(19) C8 C19 1.407(2) C8 C9 1.401(2) C23 C3 1.5021(19) C23 C34 1.408(2) C23 C24 1.412(2) C3 C2 1.4149(19) C3 C4 1.391(2) C7 C2 1.4115(19) C7 C6 1.394(2) C34 C33 1.397(2) C34 C35 1.523(2) C29 C33 1.390(2) C29 C28 1.386(2) C29 C30 1.523(2) C33 H33 0.9500 C4 H4 0.9500 C4 C5 1.386(2) C6 H6 0.9500 C6 C5 1.383(2) C24 C28 1.399(2) C24 C25 1.523(2) C28 H28 0.9500 C5 H5 0.9500 C19 C18 1.394(2) C19 C20 1.526(2) C25 H25 1.0000 C25 C26 1.519(3) C25 C27 1.527(3) C9 C13 1.393(2) C9 C10 1.522(2) C35 H35 1.0000 C35 C36 1.531(2) C35 C37 1.532(2) C18 H18 0.9500 C18 C14 1.387(2) C14 C13 1.381(2) C14 C15A 1.51(3) C14 C15B 1.55(4) C40 C39 1.426(2) C40 C41 1.432(2) C40 C45 1.505(2) C13 H13 0.9500 C10 H10 1.0000 C10 C12 1.525(2) C10 C3AA 1.529(2) C39 C38 1.418(2) C39 C44 1.501(2) C38 C42 1.426(2) C38 C43 1.508(3) C42 C41 1.409(3) C42 C47 1.507(2) C41 C46 1.507(2) C30 H30 1.0000 C30 C31 1.523(3) C30 C32 1.521(3) C20 H20 1.0000 C20 C22 1.518(3) C20 C21 1.502(3) C15A H15A 1.0000 C15A C16A 1.55(2) C15A C17A 1.53(2) C48 H48A 0.9800 C48 H48B 0.9800 C48 H48C 0.9800 C36 H36A 0.9800 C36 H36B 0.9800 C36 H36C 0.9800 C50 H50A 0.9800 C50 H50B 0.9800 C50 H50C 0.9800 C12 H12A 0.9800 C12 H12B 0.9800 C12 H12C 0.9800 C3AA H3AA 0.9800 C3AA H3AB 0.9800 C3AA H3AC 0.9800 C49 H49A 0.9800 C49 H49B 0.9800 C49 H49C 0.9800 C45 H45A 0.9800 C45 H45B 0.9800 C45 H45C 0.9800 C44 H44A 0.97(2) C44 H44B 1.01(3) C44 H44C 0.90(3) C31 H31A 0.9800 C31 H31B 0.9800 C31 H31C 0.9800 C37 H37A 0.9800 C37 H37B 0.9800 C37 H37C 0.9800 C26 H26A 0.9800 C26 H26B 0.9800 C26 H26C 0.9800 C53 H53A 0.9900 C53 H53B 0.9900 C53 C54 1.494(4) C46 H46A 0.9800 C46 H46B 0.9800 C46 H46C 0.9800 C32 H32A 0.9800 C32 H32B 0.9800 C32 H32C 0.9800 C43 H43A 0.9800 C43 H43B 0.9800 C43 H43C 0.9800 C47 H47A 0.9800 C47 H47B 0.9800 C47 H47C 0.9800 C22 H22A 0.9800 C22 H22B 0.9800 C22 H22C 0.9800 C27 H27A 0.9800 C27 H27B 0.9800 C27 H27C 0.9800 C54 H54A 0.92(3) C54 H54B 0.94(3) C54 H54C 0.87(3) C57 H57A 0.9900 C57 H57B 0.9900 C57 C56 1.492(4) C57 C58 1.476(5) C52 H52A 0.9900 C52 H52B 0.9900 C52 C51 1.512(4) C51 H51A 0.9800 C51 H51B 0.9800 C51 H51C 0.9800 C56 H56A 0.9900 C56 H56B 0.9900 C56 C55 1.453(5) C58 H58A 0.9900 C58 H58B 0.9900 C58 C59 1.505(5) C21 H21A 0.9800 C21 H21B 0.9800 C21 H21C 0.9800 C16A H16A 0.9800 C16A H16B 0.9800 C16A H16C 0.9800 C55 H55A 0.9800 C55 H55B 0.9800 C55 H55C 0.9800 C59 H59A 0.9800 C59 H59B 0.9800 C59 H59C 0.9800 C17A H17A 0.9800 C17A H17B 0.9800 C17A H17C 0.9800 C16B H16D 0.9800 C16B H16E 0.9800 C16B H16F 0.9800 C16B C15B 1.45(4) C15B H15B 1.0000 C15B C17B 1.49(3) C17B H17D 0.9800 C17B H17E 0.9800 C17B H17F 0.9800 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion Co1 C40 C39 C38 -59.88(11) Co1 C40 C39 C44 125.14(17) Co1 C40 C41 C42 59.34(11) Co1 C40 C41 C46 -125.83(17) Co1 C39 C38 C42 -61.47(11) Co1 C39 C38 C43 120.36(17) Co1 C39 C44 K1 -23.72(17) Co1 C38 C42 C41 -60.79(11) Co1 C38 C42 C47 121.52(17) Co1 C42 C41 C40 -59.08(11) Co1 C42 C41 C46 126.11(17) K1 Co1 C1 N1 6.5(4) K1 N1 C2 C3 -5.0(2) K1 N1 C2 C7 171.16(10) K1 N1 C1 Co1 -6.8(5) K1 O1 C53 C54 6.5(2) K1 O1 C52 C51 -118.5(2) K1 C23 C3 C2 -6.71(15) K1 C23 C3 C4 178.08(10) K1 C23 C34 C33 65.92(13) K1 C23 C34 C35 -117.12(13) K1 C23 C24 C28 -77.40(13) K1 C23 C24 C25 106.12(14) K1 C24 C28 C29 -78.12(14) K1 C24 C25 C26 -43.66(16) K1 C24 C25 C27 -168.18(13) Si1 Co1 C1 K1 85.10(3) Si1 Co1 C1 N1 91.6(5) O1 C53 C54 K1 -4.67(17) C8 C7 C2 N1 -9.1(2) C8 C7 C2 C3 167.00(13) C8 C7 C6 C5 -172.16(14) C8 C19 C18 C14 -0.4(2) C8 C19 C20 C22 141.28(17) C8 C19 C20 C21 -94.2(2) C8 C9 C13 C14 0.5(2) C8 C9 C10 C12 -129.88(15) C8 C9 C10 C3AA 104.80(18) C23 C3 C2 N1 7.70(19) C23 C3 C2 C7 -168.66(12) C23 C3 C4 C5 174.08(14) C23 C34 C33 C29 2.2(2) C23 C34 C35 C36 137.29(15) C23 C34 C35 C37 -100.06(17) C23 C24 C28 K1 78.65(12) C23 C24 C28 C29 0.5(2) C23 C24 C25 C26 -137.10(16) C23 C24 C25 C27 98.39(18) C3 C23 C34 C33 -179.60(13) C3 C23 C34 C35 -2.6(2) C3 C23 C24 K1 -104.21(11) C3 C23 C24 C28 178.40(13) C3 C23 C24 C25 1.9(2) C3 C4 C5 C6 -3.5(2) C7 C8 C19 C18 -167.36(14) C7 C8 C19 C20 10.9(2) C7 C8 C9 C13 167.12(13) C7 C8 C9 C10 -11.7(2) C7 C6 C5 C4 2.8(2) C2 N1 C1 Co1 -167.8(4) C2 N1 C1 K1 -161.04(17) C2 C3 C4 C5 -1.2(2) C2 C7 C6 C5 2.6(2) C34 C23 C3 C2 -109.80(16) C34 C23 C3 C4 74.98(18) C34 C23 C24 K1 78.22(12) C34 C23 C24 C28 0.8(2) C34 C23 C24 C25 -175.65(14) C33 C34 C35 C36 -45.76(19) C33 C34 C35 C37 76.89(18) C33 C29 C28 K1 -70.25(13) C33 C29 C28 C24 -0.5(2) C33 C29 C30 C31 168.59(16) C33 C29 C30 C32 -66.5(2) C4 C3 C2 N1 -177.08(13) C4 C3 C2 C7 6.6(2) C6 C7 C2 N1 176.76(13) C6 C7 C2 C3 -7.2(2) C24 C23 C3 C2 72.71(17) C24 C23 C3 C4 -102.51(16) C24 C23 C34 C33 -2.1(2) C24 C23 C34 C35 174.83(13) C28 C29 C33 C34 -0.9(2) C28 C29 C30 C31 -13.7(2) C28 C29 C30 C32 111.14(19) C28 C24 C25 C26 46.4(2) C28 C24 C25 C27 -78.1(2) C1 N1 C2 C3 145.53(16) C1 N1 C2 C7 -38.3(2) C19 C8 C7 C2 -84.06(18) C19 C8 C7 C6 90.23(17) C19 C8 C9 C13 -2.5(2) C19 C8 C9 C10 178.67(14) C19 C18 C14 C13 -1.6(2) C19 C18 C14 C15A 175.5(9) C19 C18 C14 C15B -177.1(14) C25 C24 C28 K1 -104.79(13) C25 C24 C28 C29 177.08(14) C9 C8 C7 C2 106.26(16) C9 C8 C7 C6 -79.45(18) C9 C8 C19 C18 2.4(2) C9 C8 C19 C20 -179.34(15) C35 C34 C33 C29 -174.85(14) C18 C19 C20 C22 -40.5(2) C18 C19 C20 C21 84.0(2) C18 C14 C13 C9 1.6(2) C18 C14 C15A C16A 65.7(19) C18 C14 C15A C17A -62.2(17) C18 C14 C15B C16B 19(3) C18 C14 C15B C17B -110(2) C40 C39 C38 Co1 60.48(11) C40 C39 C38 C42 -0.99(18) C40 C39 C38 C43 -179.16(16) C40 C39 C44 K1 -115.77(15) C13 C9 C10 C12 51.3(2) C13 C9 C10 C3AA -74.1(2) C13 C14 C15A C16A -117.2(15) C13 C14 C15A C17A 114.9(15) C13 C14 C15B C16B -156.2(16) C13 C14 C15B C17B 75(3) C10 C9 C13 C14 179.34(15) C39 Co1 C1 K1 -38.16(9) C39 Co1 C1 N1 -31.7(5) C39 C40 C41 Co1 -60.21(11) C39 C40 C41 C42 -0.88(18) C39 C40 C41 C46 173.95(16) C39 C38 C42 Co1 61.24(11) C39 C38 C42 C41 0.46(18) C39 C38 C42 C47 -177.23(16) C38 Co1 C1 K1 -76.55(6) C38 Co1 C1 N1 -70.1(5) C38 C39 C44 K1 70.33(17) C38 C42 C41 Co1 59.34(11) C38 C42 C41 C40 0.26(18) C38 C42 C41 C46 -174.55(16) C42 Co1 C1 K1 -119.13(6) C42 Co1 C1 N1 -112.7(5) C41 Co1 C1 K1 -151.57(10) C41 Co1 C1 N1 -145.1(4) C41 C40 C39 Co1 61.04(11) C41 C40 C39 C38 1.15(17) C41 C40 C39 C44 -173.82(16) C30 C29 C33 C34 176.92(14) C30 C29 C28 K1 112.02(14) C30 C29 C28 C24 -178.23(15) C20 C19 C18 C14 -178.63(16) C15A C14 C13 C9 -175.6(9) C45 C40 C39 Co1 -130.66(17) C45 C40 C39 C38 169.46(16) C45 C40 C39 C44 -5.5(3) C45 C40 C41 Co1 131.83(17) C45 C40 C41 C42 -168.83(16) C45 C40 C41 C46 6.0(3) C44 C39 C38 Co1 -124.81(18) C44 C39 C38 C42 173.72(17) C44 C39 C38 C43 -4.4(3) C53 O1 C52 C51 70.3(3) C43 C38 C42 Co1 -120.58(17) C43 C38 C42 C41 178.63(16) C43 C38 C42 C47 0.9(3) C47 C42 C41 Co1 -122.98(17) C47 C42 C41 C40 177.94(16) C47 C42 C41 C46 3.1(3) C52 O1 C53 C54 178.6(2) C56 C57 C58 C59 176.3(3) C58 C57 C56 C55 -176.4(3) C15B C14 C13 C9 177.1(13) loop_ _publcif_info_datablock.id _publcif_info_datablock.publ_exptl _publcif_info_datablock.publ_geom _publcif_info_datablock.structure {d85fa9ab-89cd-403d-ac26-cbf861b2cda7} y y y