#------------------------------------------------------------------------------ #$Date: 2019-11-26 03:52:07 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242549 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/26/4132602.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132602 loop_ _publ_author_name 'Collet, Guillaume' 'Lathion, Timoth\'ee' 'Besnard, C\'eline' 'Piguet, Claude' 'Petoud, St\'ephane' _publ_section_title ; On-Demand Degradation of Metal-Organic Framework Based on Photocleavable Dianthracene-Based Ligand. ; _journal_issue 34 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 10820 _journal_page_last 10828 _journal_paper_doi 10.1021/jacs.8b05047 _journal_volume 140 _journal_year 2018 _chemical_formula_moiety '2(C15 H10 O2), 2(C4 H9 N O)' _chemical_formula_sum 'C38 H38 N2 O6' _chemical_formula_weight 618.70 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2017-07-04 _audit_creation_method ; Olex2 1.2 (compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5337) ; _audit_update_record ; 2018-04-09 deposited with the CCDC. 2018-05-09 downloaded from the CCDC. ; _cell_angle_alpha 66.913(5) _cell_angle_beta 74.315(5) _cell_angle_gamma 74.609(4) _cell_formula_units_Z 2 _cell_length_a 9.2901(5) _cell_length_b 13.6758(7) _cell_length_c 14.4243(8) _cell_measurement_reflns_used 5207 _cell_measurement_temperature 180.00(10) _cell_measurement_theta_max 73.5480 _cell_measurement_theta_min 3.3690 _cell_volume 1596.55(16) _computing_cell_refinement 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 180.00(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.4679 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.966 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w 46.00 148.00 1.00 2.00 -- 110.40 -30.00 150.00 102 2 \w 54.00 103.00 1.00 2.00 -- 110.40 -94.00 -30.00 49 3 \w 83.00 113.00 1.00 2.00 -- 110.40-111.00 -90.00 30 4 \w 37.00 143.00 1.00 2.00 -- 110.40 -30.00 30.00 106 5 \w 80.00 171.00 1.00 2.00 -- 110.40 45.00-150.00 91 6 \w 93.00 124.00 1.00 2.00 -- 110.40 178.00-150.00 31 7 \w 121.00 150.00 1.00 2.00 -- 110.40 178.00-120.00 29 8 \w 60.00 87.00 1.00 2.00 -- 110.40 178.00-120.00 27 9 \w 128.00 169.00 1.00 2.00 -- 110.40 111.00 60.00 41 10 \w 132.00 158.00 1.00 2.00 -- 110.40 111.00 120.00 26 11 \w 101.00 169.00 1.00 2.00 -- 110.40 111.00 150.00 68 12 \w 29.00 80.00 1.00 2.00 -- 110.40 -30.00 -90.00 51 13 \w 1.00 61.00 1.00 1.00 -- 39.06 -99.00 0.00 60 14 \w 38.00 92.00 1.00 1.00 -- 39.06-125.00 120.00 54 15 \w 36.00 111.00 1.00 2.00 -- 110.40-111.00 90.00 75 16 \w 30.00 131.00 1.00 2.00 -- 110.40 -77.00 150.00 101 17 \w -101.00 -8.00 1.00 1.00 -- -39.06 -57.00 120.00 93 18 \w -112.00 -86.00 1.00 1.00 -- -39.06 -99.00 150.00 26 19 \w -118.00 -75.00 1.00 1.00 -- -39.06-125.00 -60.00 43 20 \w -121.00 -12.00 1.00 1.00 -- -39.06 -77.00-120.00 109 21 \w -117.00 -82.00 1.00 1.00 -- -39.06 -99.00-150.00 35 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0861106000 _diffrn_orient_matrix_UB_12 0.0274467000 _diffrn_orient_matrix_UB_13 0.0615362000 _diffrn_orient_matrix_UB_21 -0.1354949000 _diffrn_orient_matrix_UB_22 0.0890086000 _diffrn_orient_matrix_UB_23 0.0163692000 _diffrn_orient_matrix_UB_31 -0.0699053000 _diffrn_orient_matrix_UB_32 -0.0825927000 _diffrn_orient_matrix_UB_33 0.0995784000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0259 _diffrn_reflns_av_unetI/netI 0.0372 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.966 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 17 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 10783 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.966 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 73.784 _diffrn_reflns_theta_min 3.391 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.703 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.802 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.287 _exptl_crystal_description plate _exptl_crystal_F_000 656 _exptl_crystal_size_max 0.174 _exptl_crystal_size_mid 0.162 _exptl_crystal_size_min 0.02 _refine_diff_density_max 0.516 _refine_diff_density_min -0.291 _refine_diff_density_rms 0.051 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.017 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 428 _refine_ls_number_reflns 6235 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.017 _refine_ls_R_factor_all 0.0548 _refine_ls_R_factor_gt 0.0418 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0560P)^2^+0.3704P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1030 _refine_ls_wR_factor_ref 0.1132 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4970 _reflns_number_total 6235 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b05047_si_001.cif _cod_data_source_block ligand_dma _cod_database_code 4132602 _shelx_shelxl_version_number 2017/1 _chemical_oxdiff_formula 'C38 H38 N2 O6' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 99.86 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 67.29 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2. Restrained distances O1-H1 0.85 with sigma of 0.02 O18-H18 0.85 with sigma of 0.02 3.a Ternary CH refined with riding coordinates: C11(H11), C28(H28) 3.b Aromatic/amide H refined with riding coordinates: C6(H6), C9(H9), C33(H33), C13(H13), C8(H8), C7(H7), C26(H26), C30(H30), C16(H16), C32(H32), C23(H23), C31(H31), C14(H14), C25(H25), C15(H15), C24(H24) 3.c Idealised Me refined as rotating group: C40(H40A,H40B,H40C), C36(H36A,H36B,H36C), C37(H37A,H37B,H37C), C43(H43A,H43B, H43C), C46(H46A,H46B,H46C), C45(H45A,H45B,H45C) ; _shelx_res_file ; TITL ligand_dma_a.res in P-1 ligand_dma.res created by SHELXL-2017/1 at 15:33:20 on 04-Jul-2017 REM Old TITL ligand_DMA in P-1 REM SHELXT solution in P-1 REM R1 0.133, Rweak 0.005, Alpha 0.034, Orientation as input REM Formula found by SHELXT: C43 N44 O6 CELL 1.54184 9.2901 13.6758 14.4243 66.913 74.315 74.609 ZERR 2 0.0005 0.0007 0.0008 0.005 0.005 0.004 LATT 1 SFAC C H N O UNIT 76 76 4 12 DFIX 0.85 O1 H1 DFIX 0.85 O18 H18 L.S. 4 PLAN 7 TEMP -93 BOND $H LIST 6 fmap 2 acta OMIT 0 -3 1 REM REM REM WGHT 0.056000 0.370400 FVAR 6.70305 O1 4 0.293259 0.226262 1.007814 11.00000 0.02458 0.02135 = 0.04000 -0.01087 -0.00203 0.00188 H1 2 0.385421 0.186381 0.998114 11.00000 -1.50000 O18 4 0.629241 0.258228 0.494050 11.00000 0.03623 0.02404 = 0.03661 -0.01120 -0.01072 -0.00862 O42 4 0.551396 0.104829 0.998610 11.00000 0.03162 0.03359 = 0.04207 -0.02143 -0.01161 0.00685 O39 4 0.724551 0.372484 0.562398 11.00000 0.03473 0.04084 = 0.05539 -0.03171 -0.00330 -0.00814 O19 4 0.760280 0.109935 0.591433 11.00000 0.03818 0.03399 = 0.04969 -0.01464 -0.02347 -0.00579 O2 4 0.402369 0.365389 0.900123 11.00000 0.02144 0.02991 = 0.05176 -0.00986 0.00831 -0.00132 N35 3 0.681368 0.496112 0.637236 11.00000 0.03734 0.03608 = 0.04110 -0.02223 -0.00141 -0.01125 C12 1 -0.134566 0.415405 0.994404 11.00000 0.01881 0.01922 = 0.02052 -0.00373 -0.00308 -0.00402 C17 1 0.014954 0.377471 0.953959 11.00000 0.01795 0.01842 = 0.02119 -0.00406 -0.00356 -0.00365 C5 1 0.098568 0.373903 1.104636 11.00000 0.01931 0.01673 = 0.02124 -0.00398 -0.00265 -0.00424 C22 1 0.405224 0.124637 0.547081 11.00000 0.02051 0.01963 = 0.01936 -0.00453 -0.00302 -0.00309 C10 1 -0.052072 0.411599 1.143348 11.00000 0.01919 0.01768 = 0.02349 -0.00549 -0.00321 -0.00373 C27 1 0.304848 0.096978 0.508416 11.00000 0.02084 0.01846 = 0.01935 -0.00306 -0.00407 -0.00263 C3 1 0.294104 0.330150 0.960120 11.00000 0.01868 0.02340 = 0.02439 -0.00848 -0.00588 -0.00060 C11 1 -0.159001 0.474015 1.068624 11.00000 0.01589 0.02047 = 0.02126 -0.00561 -0.00099 -0.00267 AFIX 13 H11 2 -0.265171 0.471912 1.108519 11.00000 -1.20000 AFIX 0 C34 1 0.602910 0.117937 0.394312 11.00000 0.02119 0.01741 = 0.02064 -0.00598 -0.00370 -0.00238 C28 1 0.371604 0.037585 0.433204 11.00000 0.02036 0.02198 = 0.02079 -0.00636 -0.00646 -0.00389 AFIX 13 H28 2 0.291063 0.047068 0.394790 11.00000 -1.20000 AFIX 0 C4 1 0.141763 0.400923 0.987702 11.00000 0.01560 0.01951 = 0.02171 -0.00650 -0.00184 -0.00173 C29 1 0.499944 0.090697 0.357029 11.00000 0.02211 0.01775 = 0.02112 -0.00573 -0.00406 -0.00180 C20 1 0.666694 0.152101 0.536986 11.00000 0.02216 0.02635 = 0.02305 -0.01140 -0.00101 -0.00693 C6 1 0.199646 0.318597 1.171660 11.00000 0.02160 0.02188 = 0.02707 -0.00534 -0.00571 -0.00270 AFIX 43 H6 2 0.302972 0.294790 1.145774 11.00000 -1.20000 AFIX 0 C9 1 -0.100082 0.390645 1.248256 11.00000 0.02409 0.02342 = 0.02367 -0.00719 -0.00066 -0.00620 AFIX 43 H9 2 -0.202627 0.415881 1.274445 11.00000 -1.20000 AFIX 0 C33 1 0.725470 0.163027 0.326496 11.00000 0.02550 0.02370 = 0.02631 -0.00836 -0.00178 -0.00720 AFIX 43 H33 2 0.797672 0.179127 0.351640 11.00000 -1.20000 AFIX 0 C13 1 -0.255652 0.397323 0.967872 11.00000 0.01850 0.02538 = 0.02742 -0.00645 -0.00366 -0.00397 AFIX 43 H13 2 -0.356854 0.423188 0.995887 11.00000 -1.20000 AFIX 0 C21 1 0.575390 0.090422 0.510782 11.00000 0.01909 0.02002 = 0.02034 -0.00700 -0.00363 -0.00397 N44 3 0.764926 0.018310 0.928163 11.00000 0.03241 0.03814 = 0.06423 -0.02356 -0.00101 -0.00298 C8 1 0.000930 0.333058 1.314997 11.00000 0.03411 0.02719 = 0.02137 -0.00529 -0.00473 -0.00860 AFIX 43 H8 2 -0.032535 0.317930 1.386734 11.00000 -1.20000 AFIX 0 C7 1 0.150499 0.297929 1.276251 11.00000 0.03187 0.02409 = 0.02674 -0.00359 -0.01266 -0.00387 AFIX 43 H7 2 0.220222 0.259326 1.321578 11.00000 -1.20000 AFIX 0 C26 1 0.148638 0.125149 0.538732 11.00000 0.02128 0.02805 = 0.02602 -0.00616 -0.00425 -0.00363 AFIX 43 H26 2 0.080867 0.105692 0.512743 11.00000 -1.20000 AFIX 0 C30 1 0.518863 0.112294 0.252139 11.00000 0.03215 0.02249 = 0.02270 -0.00692 -0.00792 -0.00368 AFIX 43 H30 2 0.449028 0.094207 0.226664 11.00000 -1.20000 AFIX 0 C16 1 0.040011 0.323974 0.884815 11.00000 0.02279 0.02838 = 0.02746 -0.01161 -0.00238 -0.00280 AFIX 43 H16 2 0.140989 0.299897 0.854983 11.00000 -1.20000 AFIX 0 C32 1 0.742696 0.184660 0.221799 11.00000 0.03289 0.02764 = 0.02521 -0.00709 0.00454 -0.01009 AFIX 43 H32 2 0.825875 0.216431 0.175624 11.00000 -1.20000 AFIX 0 C23 1 0.346359 0.177988 0.617728 11.00000 0.02793 0.03137 = 0.02582 -0.01345 -0.00304 -0.00478 AFIX 43 H23 2 0.413422 0.194683 0.646519 11.00000 -1.20000 AFIX 0 C31 1 0.639225 0.160099 0.184696 11.00000 0.04093 0.02848 = 0.01834 -0.00635 -0.00206 -0.00724 AFIX 43 H31 2 0.650571 0.175952 0.113093 11.00000 -1.20000 AFIX 0 C38 1 0.633114 0.429823 0.610057 11.00000 0.03488 0.02701 = 0.03122 -0.01055 -0.00702 -0.00666 C14 1 -0.230123 0.341738 0.900718 11.00000 0.02486 0.03495 = 0.03327 -0.01218 -0.00821 -0.00846 AFIX 43 H14 2 -0.313265 0.328664 0.883474 11.00000 -1.20000 AFIX 0 C25 1 0.091112 0.181396 0.606575 11.00000 0.02231 0.03838 = 0.03407 -0.01291 0.00171 -0.00117 AFIX 43 H25 2 -0.015543 0.202210 0.625564 11.00000 -1.20000 AFIX 0 C15 1 -0.082248 0.305586 0.859172 11.00000 0.03047 0.03590 = 0.03346 -0.01821 -0.00677 -0.00518 AFIX 43 H15 2 -0.064009 0.267960 0.812832 11.00000 -1.20000 AFIX 0 C24 1 0.190300 0.206958 0.646389 11.00000 0.03198 0.04041 = 0.03411 -0.02093 0.00250 -0.00255 AFIX 43 H24 2 0.151387 0.244565 0.693630 11.00000 -1.20000 AFIX 0 C41 1 0.635040 0.085882 0.920088 11.00000 0.03773 0.02861 = 0.04934 -0.01480 -0.00830 -0.00528 C40 1 0.465842 0.426679 0.637021 11.00000 0.03358 0.03865 = 0.04536 -0.01955 -0.00625 -0.00740 AFIX 137 H40A 2 0.446169 0.376997 0.609934 11.00000 -1.50000 H40B 2 0.408989 0.499254 0.606910 11.00000 -1.50000 H40C 2 0.433411 0.401738 0.711781 11.00000 -1.50000 AFIX 0 C36 1 0.581623 0.566315 0.692474 11.00000 0.04804 0.04222 = 0.04620 -0.02778 -0.00480 -0.00652 AFIX 137 H36A 2 0.553948 0.638623 0.643321 11.00000 -1.50000 H36B 2 0.634728 0.571045 0.740339 11.00000 -1.50000 H36C 2 0.489430 0.536266 0.730734 11.00000 -1.50000 AFIX 0 C37 1 0.841313 0.506632 0.606771 11.00000 0.04218 0.05697 = 0.06324 -0.03429 0.00317 -0.02300 AFIX 137 H37A 2 0.899808 0.450925 0.577623 11.00000 -1.50000 H37B 2 0.880006 0.497775 0.666945 11.00000 -1.50000 H37C 2 0.851461 0.578257 0.555299 11.00000 -1.50000 AFIX 0 C43 1 0.588045 0.138789 0.817836 11.00000 0.06416 0.04873 = 0.03899 -0.01639 -0.00952 0.00695 AFIX 137 H43A 2 0.561759 0.084968 0.799163 11.00000 -1.50000 H43B 2 0.672068 0.169944 0.766058 11.00000 -1.50000 H43C 2 0.499488 0.196152 0.821229 11.00000 -1.50000 AFIX 0 C46 1 0.805636 -0.032538 1.030820 11.00000 0.04321 0.04253 = 0.08284 -0.02235 -0.03298 0.00904 AFIX 137 H46A 2 0.833648 0.021193 1.048689 11.00000 -1.50000 H46B 2 0.891833 -0.092159 1.030524 11.00000 -1.50000 H46C 2 0.718478 -0.060436 1.081464 11.00000 -1.50000 AFIX 0 C45 1 0.867543 -0.013021 0.843914 11.00000 0.04047 0.05163 = 0.07365 -0.02689 0.01587 -0.00375 AFIX 137 H45A 2 0.822201 0.021679 0.782200 11.00000 -1.50000 H45B 2 0.884444 -0.091691 0.862667 11.00000 -1.50000 H45C 2 0.964821 0.009934 0.830360 11.00000 -1.50000 AFIX 0 H18 2 0.669796 0.288635 0.522206 11.00000 0.07507 HKLF 4 REM ligand_dma_a.res in P-1 REM R1 = 0.0418 for 4970 Fo > 4sig(Fo) and 0.0548 for all 6235 data REM 428 parameters refined using 2 restraints END WGHT 0.0560 0.3704 REM Highest difference peak 0.516, deepest hole -0.291, 1-sigma level 0.051 Q1 1 0.6737 0.0411 0.9875 11.00000 0.05 0.52 Q2 1 0.7202 0.0716 0.8685 11.00000 0.05 0.31 Q3 1 -0.1023 0.4463 1.1081 11.00000 0.05 0.22 Q4 1 0.5984 0.0998 0.4511 11.00000 0.05 0.21 Q5 1 0.8022 -0.0769 0.8408 11.00000 0.05 0.18 Q6 1 0.4734 0.6023 0.6617 11.00000 0.05 0.18 Q7 1 0.1240 0.3894 1.0485 11.00000 0.05 0.18 ; _shelx_res_checksum 67479 _shelx_hkl_file ; 0 0 1 3397.38 112.659 21 0 0 1 3176.71 119.689 19 0 0 2 436904. 1811.24 21 0 0 2 457337. 1964.46 19 0 0 3 57248.1 866.746 14 0 0 4 18502.9 567.896 13 0 0 4 16942.0 562.994 14 0 0 5 36264.3 907.052 13 0 0 5 33649.9 895.746 14 0 0 6 21930.3 805.056 14 0 0 6 24978.5 855.081 13 0 0 7-32.2647 150.879 14 0 0 7 128.403 170.915 13 0 0 8 45104.9 1414.69 14 0 0 8 50658.3 1453.73 13 0 0 9-1.71955 132.370 14 0 0 9 496.472 212.683 13 0 0 10 7339.56 641.901 13 0 0 10 7288.62 523.426 2 0 0 10 7099.82 494.778 3 0 0 10 7782.93 487.651 10 0 0 10 6474.38 481.215 11 0 0 11 4830.12 469.119 2 0 0 11 5195.00 417.884 10 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6792.44 504.492 9 1 -7 8 6291.38 506.863 2 1 -7 8 6427.10 494.626 3 1 -7 9 2910.12 342.956 9 1 -7 9 2449.89 311.583 3 1 -7 9 2673.03 345.783 2 1 -7 10 618.053 217.601 2 1 -7 10 640.135 204.907 3 1 -7 11 235.185 127.569 3 1 -7 11 239.693 141.829 2 -1 6 16-12.9048 88.1228 11 -1 6 16 23.8393 85.4089 15 -1 6 15 3334.59 299.733 11 -1 6 15 3167.69 322.097 15 -1 6 14 698.649 212.539 15 -1 6 14 815.865 219.005 11 -1 6 13 2514.44 344.160 15 -1 6 13 2176.44 287.711 11 -1 6 12 13375.6 671.539 11 -1 6 11 8775.77 544.038 11 -1 6 11 8036.58 533.681 5 -1 6 10 1753.77 271.177 5 -1 6 10 1551.22 354.778 19 -1 6 10 1830.27 241.533 11 -1 6 9-384.616 239.657 20 -1 6 9 530.913 245.906 19 -1 6 8 32421.2 1335.53 19 -1 6 8 33338.8 1268.44 20 -1 6 7 4283.96 458.977 20 -1 6 7 4686.79 499.405 19 -1 6 6 7266.81 572.461 19 -1 6 6 6160.97 494.258 20 -1 6 5 1435.26 271.847 20 -1 6 4 82260.2 1585.79 20 1 -6 -4 80552.6 1366.18 18 -1 6 3 52315.2 1262.93 20 1 -6 -3 51184.1 1133.30 18 -1 6 2 15031.0 696.970 20 -1 6 1 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10966.9 664.412 19 -1 5 6 9363.93 573.736 20 -1 5 5 278841. 2793.41 20 1 -5 -5 275796. 2151.37 18 1 -5 -4 67003.3 1118.53 18 -1 5 4 67512.5 1302.90 20 -1 5 3 30322.5 869.390 20 1 -5 -3 29790.5 776.964 18 -1 5 2 17493.6 661.888 20 1 -5 -2 17640.6 624.513 18 1 -5 -1 31811.1 876.283 18 -1 5 1 32705.1 909.370 20 1 -5 0 103277. 1058.34 13 -1 5 0 105661. 1681.12 20 -1 5 -1 29391.8 936.050 20 1 -5 1 31887.0 699.247 13 -1 5 -2 471.983 215.873 20 1 -5 2 602.869 135.265 13 1 -5 3 615.419 159.390 13 1 -5 4 16073.9 734.448 13 1 -5 5-47.0824 117.383 13 1 -5 6 45141.0 1456.35 13 1 -5 7 7655.03 698.817 13 1 -5 7 8387.27 523.543 9 1 -5 8 10593.9 551.774 10 1 -5 8 10739.7 594.968 9 1 -5 8 11056.9 641.792 3 1 -5 9 9980.62 595.295 9 1 -5 9 9784.87 610.876 3 1 -5 10 5432.12 458.395 3 1 -5 10 5076.86 482.112 2 1 -5 10 5317.27 435.298 9 1 -5 11 356.355 176.725 3 1 -5 11 491.014 191.320 2 1 -5 12 1458.71 244.504 2 1 -5 13 355.315 142.022 2 -1 4 16 538.516 116.353 15 -1 4 16 647.047 161.321 11 -1 4 15 127.685 107.068 15 -1 4 15 81.7816 145.054 11 -1 4 14 885.585 238.351 11 -1 4 14 1153.69 239.752 15 -1 4 13 6575.65 463.064 2 -1 4 13 6662.61 512.924 11 -1 4 13 6323.77 535.607 15 -1 4 12 99.0508 109.205 11 -1 4 12-39.1377 126.272 2 -1 4 12 44.3007 163.235 15 -1 4 11 305.171 169.930 2 -1 4 11 366.000 167.684 11 -1 4 10 6178.93 669.873 14 -1 4 9 18965.8 1060.56 19 -1 4 8 17898.4 906.799 20 -1 4 8 18082.7 957.247 19 -1 4 7 21766.0 896.939 20 -1 4 7 22302.9 991.264 19 -1 4 6 14555.6 745.743 19 -1 4 6 13754.0 651.641 20 -1 4 5 2016.38 258.955 20 -1 4 5 2011.39 299.605 19 -1 4 4 451.702 159.750 20 1 -4 -3 5205.38 303.181 18 -1 4 3 5119.47 336.535 20 -1 4 2 33055.8 796.081 20 1 -4 -2 33251.5 763.505 18 1 -4 -1 57267.6 1037.23 18 -1 4 1 56280.3 1041.10 20 -1 4 0 158921. 1787.25 20 1 -4 0 153202. 1789.10 18 -1 4 -1 12091.2 546.071 20 1 -4 1 11992.3 415.463 13 1 -4 1 12962.9 569.060 18 1 -4 2 11218.5 458.634 13 1 -4 3 26102.6 784.526 13 1 -4 4 15368.4 681.496 13 1 -4 5 39664.5 1202.68 13 1 -4 6 235.260 166.115 13 1 -4 7 5022.70 525.770 13 1 -4 8 3824.29 518.598 13 1 -4 8 3914.50 378.111 9 1 -4 8 4156.99 394.720 3 1 -4 8 4299.02 366.098 10 1 -4 9 33240.7 1095.84 3 1 -4 9 31883.1 1010.91 9 1 -4 9 32009.6 995.698 10 1 -4 10 482.330 178.660 3 1 -4 10 582.786 145.369 10 1 -4 10 688.481 221.734 9 1 -4 10 628.206 222.215 2 1 -4 11 5973.84 503.590 2 1 -4 11 6508.97 475.494 3 1 -4 12 316.671 187.491 3 1 -4 12-11.1911 178.148 2 1 -4 13 2186.80 288.414 2 1 -4 14 1168.95 164.878 2 -1 3 16 2590.84 245.530 11 -1 3 15 4472.02 360.739 15 -1 3 15 4629.50 374.287 11 -1 3 14 130.375 175.827 11 -1 3 14 381.237 169.465 2 -1 3 14 350.020 198.520 15 -1 3 13 2529.69 350.383 15 -1 3 13 2303.11 330.762 11 -1 3 13 2221.07 308.908 2 -1 3 12 583.728 195.522 2 -1 3 12 489.049 217.940 15 -1 3 12 643.509 222.316 11 -1 3 11 12254.9 726.136 15 -1 3 11 11403.5 633.314 2 -1 3 11 12642.0 687.874 11 -1 3 10-130.148 95.0852 14 -1 3 9 8252.93 727.308 14 -1 3 8 1902.06 343.800 19 -1 3 7 2714.84 381.109 19 -1 3 7 2754.51 336.931 20 -1 3 6 67725.8 1548.94 19 -1 3 6 65302.6 1379.38 20 -1 3 5 31260.9 858.842 20 -1 3 5 31972.7 974.050 19 -1 3 4 8139.04 405.111 20 -1 3 4 9021.91 477.966 19 -1 3 3 172894. 1618.02 20 -1 3 2 88123.3 1113.89 20 -1 3 1 64096.9 947.056 20 1 -3 -1 61830.0 950.878 18 -1 3 0 36711.8 747.817 20 1 -3 0 36679.2 778.313 18 1 -3 1 47086.8 929.360 18 1 -3 2 4335.27 278.728 13 1 -3 3 42809.9 937.065 13 1 -3 4 4921.13 379.902 13 1 -3 5 56738.3 1338.65 13 1 -3 6 26181.5 1001.48 13 1 -3 7 7111.50 589.665 13 1 -3 8 129.577 187.179 13 1 -3 9 11097.8 589.372 10 1 -3 9 11217.4 634.067 3 1 -3 9 11878.7 879.367 13 1 -3 9 10989.5 584.379 9 1 -3 10 100.985 195.182 2 1 -3 10-153.925 146.740 10 1 -3 10-88.7775 110.834 9 1 -3 11 1840.79 286.264 10 1 -3 11 2273.50 350.991 2 1 -3 11 1721.44 284.511 3 1 -3 12 4996.59 464.867 2 1 -3 12 5930.35 452.370 3 1 -3 13 175.725 179.875 2 1 -3 14 3781.74 351.287 2 -1 2 15 1090.02 202.615 15 -1 2 15 812.370 196.391 11 -1 2 14 2201.04 320.713 11 -1 2 14 2376.56 311.344 15 -1 2 14 2757.73 322.971 2 -1 2 13 2011.72 305.502 15 -1 2 13 2002.11 312.410 11 -1 2 13 2000.10 306.376 2 -1 2 12 141.728 183.739 15 -1 2 12 228.881 187.986 2 -1 2 12 63.0146 162.041 11 -1 2 11 1026.99 267.270 11 -1 2 11 1057.07 281.516 15 -1 2 11 962.192 212.086 10 -1 2 11 532.721 187.551 2 -1 2 10 9355.38 578.898 11 -1 2 10 8449.93 575.553 15 -1 2 10 7471.40 740.364 14 -1 2 9 451.327 232.964 14 -1 2 8 406.876 203.810 14 -1 2 7 53983.1 1302.61 13 -1 2 7 49246.5 1423.72 19 -1 2 6 56448.3 1206.48 13 -1 2 6 55703.5 1382.84 19 -1 2 5 16713.1 620.842 20 -1 2 5 17515.5 609.394 13 -1 2 5 18091.8 720.948 19 1 -2 -4 48484.5 742.915 17 -1 2 4 46088.2 1011.96 19 -1 2 4 45430.4 892.577 20 -1 2 3 3622.08 294.800 19 1 -2 -3 3957.23 226.622 17 -1 2 3 3699.27 237.995 20 -1 2 2 3589.62 208.631 20 1 -2 -2 3661.53 224.842 17 -1 2 1 318842. 1704.31 20 1 -2 -1 309367. 1865.40 17 -1 2 0 40341.8 651.179 20 1 -2 0 43971.4 711.037 17 1 -2 1 263220. 1888.54 18 1 -2 2 643086. 3134.29 18 1 -2 3 103986. 1343.70 13 1 -2 4 59386.2 1165.17 13 1 -2 4 57941.2 1092.23 14 1 -2 5 31392.0 945.824 13 1 -2 5 28376.0 846.175 14 1 -2 6 13451.6 650.774 14 1 -2 6 15336.8 735.394 13 1 -2 7 60684.1 1596.48 13 1 -2 7 55801.0 1425.97 14 1 -2 8 14805.3 878.107 13 1 -2 9 547.264 144.588 10 1 -2 9 479.185 206.517 13 1 -2 10 3505.18 355.945 9 1 -2 10 3267.31 348.993 11 1 -2 10 3522.79 376.209 3 1 -2 10 2878.08 364.752 2 1 -2 10 3806.26 369.212 10 1 -2 11 1273.50 247.715 10 1 -2 11 796.995 224.712 11 1 -2 11 967.705 230.898 3 1 -2 11 854.898 228.774 2 1 -2 12 174.338 176.767 3 1 -2 12 44.7732 124.006 11 1 -2 12-2.61385 177.428 2 1 -2 12 139.427 160.307 10 1 -2 13 386.222 142.027 11 1 -2 13 474.085 216.641 2 1 -2 14 402.439 198.584 2 1 -2 15 1771.10 212.969 2 -1 1 15 18.4055 116.897 2 -1 1 15 96.9706 115.474 11 -1 1 14 2596.04 306.031 15 -1 1 14 3189.37 348.628 2 -1 1 14 2995.62 357.655 11 -1 1 13 512.487 219.387 11 -1 1 13 648.135 228.232 2 -1 1 13 552.609 194.249 15 -1 1 12 16471.6 801.314 2 -1 1 12 15097.2 781.916 11 -1 1 12 14696.7 765.908 15 -1 1 11 699.380 222.364 2 -1 1 11 954.152 231.636 15 -1 1 11 814.634 230.244 11 -1 1 10 353.071 122.157 10 -1 1 10 586.928 217.415 11 -1 1 10 473.150 141.968 7 -1 1 10-74.2190 97.9956 14 -1 1 10 105.313 160.833 15 -1 1 10 600.048 165.658 2 -1 1 9 4465.28 525.704 14 -1 1 8 3115.59 429.590 14 -1 1 8 4053.62 445.613 13 -1 1 7 1615.36 274.355 13 -1 1 7 1440.51 305.180 14 -1 1 6 9186.53 578.118 19 -1 1 6 10405.9 556.504 13 -1 1 5 428.187 187.164 19 -1 1 5 524.873 170.717 13 1 -1 -5 459.737 76.5780 17 1 -1 -4 26432.1 471.468 17 -1 1 4 26064.3 687.151 13 -1 1 4 25976.1 768.633 19 -1 1 4 24602.2 661.932 20 -1 1 3 104408. 1187.33 13 -1 1 3 102213. 1117.33 20 -1 1 3 104432. 1333.96 19 1 -1 -3 104014. 955.373 17 -1 1 2 44912.0 756.778 19 1 -1 -2 46053.4 619.201 17 -1 1 1 47226.1 489.008 20 1 -1 -1 46952.6 618.611 17 1 -1 0 369646. 1191.77 21 1 -1 0 356597. 1670.43 17 1 -1 1 20124.3 398.745 21 1 -1 1 20013.4 396.449 17 1 -1 2 182803. 1402.37 18 1 -1 2 188689. 1476.89 21 1 -1 3 87338.6 1018.72 14 1 -1 3 88731.2 1146.39 13 1 -1 4 54335.8 1028.73 13 1 -1 4 50231.7 908.858 14 1 -1 5 15675.7 581.150 14 1 -1 5 16737.1 648.098 13 1 -1 6 200.359 142.145 13 1 -1 6 75.2315 121.850 14 1 -1 7 4729.99 444.315 13 1 -1 7 4018.56 366.804 14 1 -1 8 3562.75 438.290 13 1 -1 8 3076.81 351.165 14 1 -1 9 1601.64 348.234 13 1 -1 10 5091.90 437.055 3 1 -1 10 4257.70 374.481 10 1 -1 10 4280.34 424.162 2 1 -1 10 4452.01 365.626 9 1 -1 10 4717.73 416.379 11 1 -1 10 4722.77 532.121 13 1 -1 11 17307.8 771.348 11 1 -1 11 17139.3 847.131 2 1 -1 11 19379.8 808.074 10 1 -1 11 18483.5 816.666 3 1 -1 12 5297.48 443.193 10 1 -1 12 4693.88 463.320 2 1 -1 12 4708.72 419.265 11 1 -1 13 124.140 139.538 11 1 -1 13 279.743 206.716 2 1 -1 13 133.455 160.145 10 1 -1 14 1773.63 287.655 2 1 -1 14 1616.38 236.486 11 1 -1 15 6265.28 389.025 2 -1 0 15 5466.21 342.685 2 -1 0 14 366.515 174.610 2 -1 0 14 515.579 184.929 11 -1 0 13 941.222 212.573 15 -1 0 13 315.102 202.474 11 -1 0 13 761.773 236.973 2 -1 0 12 771.783 248.663 2 -1 0 12 845.572 269.001 11 -1 0 12 285.183 162.612 15 -1 0 11 15520.5 789.957 15 -1 0 11 15407.7 788.039 11 -1 0 11 14392.0 767.667 2 -1 0 10 5263.07 442.935 3 -1 0 10 5200.55 467.337 2 -1 0 10 5545.93 458.606 11 -1 0 10 5674.25 463.609 15 -1 0 10 5506.19 436.896 10 -1 0 10 5342.04 412.066 7 -1 0 10 4449.12 552.878 14 -1 0 9 7117.03 636.834 13 -1 0 9 6990.72 638.186 14 -1 0 8 5082.75 552.114 14 -1 0 8 5235.83 485.521 13 -1 0 7 20631.7 897.711 13 -1 0 7 19228.3 923.858 14 -1 0 6 32056.9 1087.43 14 -1 0 6 33063.2 1016.29 13 -1 0 5 5908.12 442.950 14 -1 0 5 5822.86 407.284 13 -1 0 4 98108.7 1394.10 13 -1 0 4 93955.8 1498.76 14 1 0 -4 95446.3 845.709 17 1 0 -3 40602.7 558.157 17 -1 0 3 40960.9 856.101 19 1 0 -2 19978.7 388.914 17 -1 0 2 19298.9 504.272 19 1 0 -1 388023. 1614.32 17 -1 0 1 375112. 1748.80 19 1 0 0 70006.6 662.854 17 -1 0 0 70402.8 536.291 19 1 0 1 160731. 956.330 17 1 0 2 24500.9 328.808 14 1 0 2 24602.7 486.075 21 1 0 2 24187.6 352.797 17 1 0 3 86602.2 614.440 17 1 0 3 85401.4 857.142 14 1 0 3 93401.7 1107.70 21 1 0 3 90801.0 855.866 18 1 0 4 1307.56 197.124 21 1 0 4 1463.73 161.343 14 1 0 4 1495.15 200.181 13 1 0 5 14164.8 510.352 14 1 0 5 14776.2 575.668 13 1 0 5 13759.9 575.599 21 1 0 6 4107.13 364.218 13 1 0 6 3894.48 307.599 14 1 0 7 58773.6 1310.48 14 1 0 7 60279.0 1416.37 13 1 0 8 31880.6 1148.28 13 1 0 8 30368.2 1034.65 14 1 0 9 12227.6 783.268 13 1 0 10 3636.77 482.928 13 1 0 10 3688.95 345.141 10 1 0 11 7024.56 522.304 11 1 0 11 6923.80 502.009 3 1 0 11 6311.35 515.105 2 1 0 11 6160.59 453.842 10 1 0 12 10404.7 652.582 2 1 0 12 10231.6 599.785 10 1 0 12 10042.1 628.209 11 1 0 13 352.298 178.579 11 1 0 13 273.669 190.825 10 1 0 13 112.003 175.046 2 1 0 14 3180.99 335.029 11 1 0 14 2965.54 328.435 2 1 0 15-34.9416 139.345 2 1 0 15-118.893 119.389 11 1 0 16 397.134 108.316 2 -1 -1 15 506.836 151.180 2 -1 -1 14 0.83582 176.896 2 -1 -1 13-220.528 202.105 2 -1 -1 13 167.118 170.823 11 -1 -1 12 1404.12 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2 -1 -3 13 1421.42 250.879 2 -1 -3 12 377.482 232.269 2 -1 -3 11 320.726 184.659 2 -1 -3 11 36.5682 135.238 11 -1 -3 11 387.765 209.303 3 -1 -3 10 4134.03 431.785 3 -1 -3 10 3921.05 396.722 15 -1 -3 10 4138.92 406.657 11 -1 -3 10 3783.03 422.024 2 -1 -3 9 5119.32 438.005 15 -1 -3 9 5268.86 463.765 3 -1 -3 9 5147.63 439.929 11 -1 -3 9 5425.25 471.293 2 -1 -3 9 5207.89 425.473 7 -1 -3 8 3800.52 510.436 13 -1 -3 8 3753.61 363.366 3 -1 -3 8 4015.89 347.973 10 -1 -3 8 2755.60 423.406 14 -1 -3 7 7993.44 661.002 13 -1 -3 7 9085.87 706.708 14 -1 -3 6 6832.52 553.681 13 -1 -3 6 5859.84 552.293 14 -1 -3 5 13546.6 692.385 13 -1 -3 5 13730.0 748.689 14 -1 -3 4 33449.4 1075.15 14 -1 -3 4 34475.4 983.179 13 -1 -3 3 189149. 2030.01 13 -1 -3 3 211218. 2424.06 14 -1 -3 2 20370.8 600.433 13 -1 -3 2 20973.6 695.733 14 -1 -3 1 430272. 2289.81 13 1 3 0 621071. 2821.68 20 1 3 1 9855.45 362.568 20 1 3 2 233982. 1750.33 20 1 3 3-9.75460 121.039 20 1 3 4 22639.3 653.747 20 1 3 4 23472.0 491.523 13 1 3 5 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10 14 248.168 137.258 15 -2 10 13 5.54590 126.076 5 -2 10 12 5157.13 412.708 5 -2 10 11 508.176 217.391 5 -2 10 10 5177.68 459.515 5 -2 10 9 440.284 212.464 5 -2 10 8 13316.6 728.340 5 2 -10 -7 251.602 144.109 1 -2 10 7-198.086 175.880 5 -2 10 6 10757.2 628.291 5 2 -10 -6 10721.3 642.856 1 2 -10 -5 1462.43 265.454 1 -2 10 5 1164.91 241.130 5 2 -10 -4 37483.5 1186.98 1 2 -10 -3 505.090 199.911 16 2 -10 -3 473.358 197.830 1 2 -10 -2 10964.6 645.185 1 2 -10 -2 10641.4 588.966 16 2 -10 -1-111.989 197.991 1 2 -10 -1-52.0382 140.728 16 2 -10 0 507.799 176.855 1 2 -10 0 372.755 196.671 16 2 -10 1 3826.33 404.856 1 2 -10 1 3759.15 403.150 16 2 -10 2-6.80774 170.448 16 2 -10 2-23.4614 162.418 9 2 -10 2 14.6233 148.915 1 2 -10 3-496.701 156.498 1 2 -10 3-191.404 156.946 9 2 -10 3-155.263 168.763 16 2 -10 4 4122.97 394.733 9 2 -10 4 4052.31 402.604 16 2 -10 5 2034.80 268.835 9 2 -10 5 1916.27 281.059 16 2 -10 6 899.258 210.321 16 2 -10 6 666.854 174.358 9 2 -10 7 109.397 153.254 9 -2 9 15-54.7944 114.299 15 -2 9 14 606.742 146.917 5 -2 9 14 562.128 194.126 15 -2 9 13 890.011 231.719 15 -2 9 13 756.027 184.456 5 -2 9 12 2449.68 326.689 5 -2 9 11 10098.3 619.740 5 -2 9 10 93.0221 143.344 5 -2 9 9 18499.0 857.135 5 -2 9 8 13354.7 728.355 5 -2 9 7 7006.82 528.251 5 2 -9 -7 6321.98 465.065 1 -2 9 6 53834.8 1370.89 5 2 -9 -6 51900.4 1316.98 1 2 -9 -5 326.981 166.066 1 -2 9 5 727.840 201.376 5 -2 9 4 1171.92 226.138 5 -2 9 4 1575.78 292.611 20 2 -9 -4 1588.06 275.983 1 -2 9 3-756.257 272.344 20 2 -9 -3 196.084 153.891 1 2 -9 -2 11973.8 665.449 1 -2 9 2 10979.8 822.876 20 2 -9 -2 10991.1 579.240 16 2 -9 -1 15776.6 772.716 1 2 -9 -1 15501.5 690.416 16 -2 9 1 15205.6 930.805 20 2 -9 0 3634.84 367.262 16 2 -9 0 3719.31 420.397 1 -2 9 0 3696.23 562.904 20 2 -9 1 8267.25 579.773 1 -2 9 -1 6846.30 683.392 20 2 -9 1 7524.99 515.794 16 2 -9 2 2388.59 305.141 1 2 -9 2 1914.21 296.442 16 2 -9 3 671.024 222.734 16 2 -9 3 252.421 162.303 1 2 -9 3 594.635 173.208 9 2 -9 4 269.722 213.969 16 2 -9 4 501.577 199.923 9 2 -9 5 448.793 216.088 16 2 -9 5 263.515 172.278 9 2 -9 6 5409.04 440.140 9 2 -9 6 5331.90 419.530 16 2 -9 7 332.254 175.949 2 2 -9 7 509.013 190.567 9 2 -9 7 694.504 176.681 3 2 -9 7 505.101 166.022 16 2 -9 8 108.813 136.500 9 2 -9 8 99.6372 118.550 2 2 -9 9-29.9402 89.2372 2 -2 8 15 99.4613 117.781 15 -2 8 14 12422.8 608.080 15 -2 8 13 460.132 208.151 15 -2 8 13 264.886 147.685 5 -2 8 12 158.386 169.400 5 -2 8 11 2356.86 330.053 5 -2 8 10 845.168 236.106 5 -2 8 9 23641.3 960.585 5 -2 8 8 13237.6 707.854 5 -2 8 7 40941.2 1198.26 5 -2 8 7 42387.4 1683.72 19 -2 8 6 285.572 285.842 19 -2 8 5 7872.40 622.846 20 -2 8 4 31958.6 1212.84 20 -2 8 3 1671.42 347.938 20 -2 8 2 33541.3 1278.78 20 -2 8 1 60160.0 1745.77 20 -2 8 0 434.692 188.508 20 -2 8 -1 715.014 261.271 20 2 -8 2 12760.8 675.707 1 2 -8 2 11197.9 594.722 16 -2 8 -2 10444.2 817.028 20 2 -8 3 11478.7 633.859 1 2 -8 3 11698.7 627.151 16 -2 8 -3 12890.2 942.788 20 2 -8 4 10115.8 611.278 16 2 -8 4 9107.28 571.797 9 2 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497.130 20 2 -7 5 10053.5 593.047 9 2 -7 5 10052.0 579.889 16 2 -7 6 219.020 148.287 16 2 -7 6-59.4701 164.367 9 2 -7 7 8432.43 552.511 9 2 -7 7 8173.98 499.371 16 2 -7 8 297.499 193.542 3 2 -7 8-58.4121 176.492 9 2 -7 9 198.894 185.296 2 2 -7 9 112.802 154.535 9 2 -7 9-11.2626 137.310 3 2 -7 10 176.161 147.181 2 2 -7 10 212.086 159.367 9 2 -7 11 8000.54 419.560 2 -2 6 16 124.808 80.4358 15 -2 6 15 191.996 118.018 11 -2 6 15 372.158 156.497 15 -2 6 14 1322.31 264.850 15 -2 6 14 887.641 203.004 11 -2 6 13 2302.62 275.109 11 -2 6 13 1726.55 291.397 15 -2 6 12 11442.5 622.010 5 -2 6 12 11004.1 572.275 11 -2 6 11 2989.68 367.336 5 -2 6 10 1743.11 288.482 5 -2 6 9-161.837 132.626 5 -2 6 9 401.780 209.050 19 -2 6 8 1528.13 340.374 19 -2 6 7 2962.21 438.750 19 -2 6 6 7044.83 627.106 19 -2 6 6 7029.94 519.234 20 -2 6 5 4994.62 430.561 20 2 -6 -4 241.736 125.101 18 -2 6 4 94.4750 130.232 20 2 -6 -3 4886.39 413.189 18 -2 6 3 4344.87 401.385 20 2 -6 -2 8586.69 564.760 18 -2 6 2 9177.67 562.298 20 2 -6 -1 31440.9 1057.62 18 -2 6 1 30161.6 1004.01 20 2 -6 0 113023. 2062.28 18 -2 6 0 112132. 2009.90 20 -2 6 -1 3112.30 377.240 20 -2 6 -2 1494.91 307.223 20 -2 6 -3 2671.47 392.017 20 -2 6 -4 9.00874 76.7246 20 -2 6 -5 2572.34 431.685 20 2 -6 5 2402.19 286.196 9 -2 6 -6 1651.10 400.943 20 2 -6 6 1574.87 265.149 16 2 -6 6 1405.04 228.423 9 2 -6 7 8875.48 566.654 9 2 -6 7 9174.59 519.888 16 2 -6 8 10484.3 608.619 3 2 -6 8 9898.73 601.369 9 2 -6 9 2089.99 304.609 9 2 -6 9 1693.02 278.231 3 2 -6 10 990.357 233.003 3 2 -6 10 1223.84 241.380 9 2 -6 10 986.183 239.281 2 2 -6 11 5267.99 419.325 2 2 -6 11 6300.81 368.090 3 2 -6 12 497.961 155.525 2 -2 5 15 1929.36 249.082 15 -2 5 15 1534.85 199.151 11 -2 5 14 174.648 172.281 15 -2 5 14 587.483 181.878 11 -2 5 13 1369.58 282.501 15 -2 5 13 1492.24 253.187 11 -2 5 12 43.1686 189.109 15 -2 5 12 161.572 144.160 11 -2 5 11 8751.56 557.959 11 -2 5 11 7323.51 519.323 5 -2 5 10 2491.44 325.263 5 -2 5 10 2239.17 307.254 11 -2 5 9 61469.5 1444.21 5 -2 5 9 67160.3 2156.90 19 -2 5 8 8068.24 691.674 19 -2 5 7 17572.9 979.979 19 -2 5 6 19672.9 820.909 20 -2 5 6 18619.5 946.523 19 2 -5 -5 22927.8 766.114 18 -2 5 5 24098.6 994.362 19 -2 5 5 22838.6 821.347 20 -2 5 4 22063.1 773.260 20 2 -5 -4 22672.2 776.207 18 -2 5 3-0.84377 128.069 20 2 -5 -3 1.77610 136.951 18 2 -5 -2 4655.43 384.700 18 -2 5 2 4119.72 342.849 20 -2 5 1 56598.1 1224.80 20 2 -5 -1 56883.2 1294.46 18 2 -5 0 57114.5 1344.01 18 -2 5 0 55609.3 1264.16 20 2 -5 1 1308.34 181.920 13 2 -5 1 1623.86 293.361 18 -2 5 -1 1280.92 261.400 20 -2 5 -2 2243.38 311.172 20 2 -5 2 1724.54 219.374 13 2 -5 3 35353.1 1011.62 13 -2 5 -3 36638.8 1223.25 20 2 -5 4 24150.4 912.872 13 2 -5 5 19280.5 892.189 13 2 -5 6 940.181 253.956 13 2 -5 7 3554.20 471.068 13 2 -5 7 4178.86 398.362 9 2 -5 8 27525.7 958.368 3 2 -5 8 28091.1 965.796 9 2 -5 9 10092.1 591.058 3 2 -5 9 9974.84 593.455 9 2 -5 10 1742.38 275.597 3 2 -5 10 1195.41 240.570 9 2 -5 11 6899.53 516.724 2 2 -5 11 7533.94 480.051 9 2 -5 11 8065.80 465.921 3 2 -5 12 905.060 204.123 2 2 -5 13 1279.51 191.478 2 -2 4 15-17.3408 117.486 11 -2 4 15 182.275 132.666 15 -2 4 14 242.360 174.498 11 -2 4 14-274.228 170.803 15 -2 4 13 645.958 231.631 15 -2 4 13 83.3489 131.472 11 -2 4 12 1295.41 292.758 15 -2 4 12 1478.62 270.997 11 -2 4 11 832.993 258.114 15 -2 4 11 940.623 234.529 11 -2 4 10 213.324 106.030 11 -2 4 10 437.325 162.876 2 -2 4 9 9612.02 796.532 19 -2 4 8 2071.84 400.998 19 -2 4 7 34843.3 1343.22 19 -2 4 6 44447.0 1411.34 19 -2 4 6 42270.9 1140.34 20 -2 4 5 17296.5 675.342 20 -2 4 5 17689.9 828.476 19 -2 4 4 19059.0 804.763 19 -2 4 4 18791.9 651.389 20 -2 4 3 94187.5 1362.01 20 -2 4 2 16061.1 568.907 20 2 -4 -1 39422.6 992.182 18 -2 4 1 38114.3 890.939 20 -2 4 0 23179.9 720.813 20 2 -4 0 24620.1 812.379 18 -2 4 -1 848.685 203.835 20 2 -4 1 792.116 209.655 18 2 -4 2 8733.79 441.047 13 2 -4 2 9350.42 555.227 18 2 -4 3 10333.7 530.819 13 2 -4 4 77586.6 1568.58 13 2 -4 5 2579.95 335.564 13 2 -4 6 20431.3 967.295 13 2 -4 7 118.382 106.823 13 2 -4 8 11112.4 607.828 3 2 -4 8 11040.8 828.152 13 2 -4 8 11941.1 622.840 9 2 -4 8 10911.9 555.688 10 2 -4 9 12311.9 635.635 9 2 -4 9 11932.6 599.082 10 2 -4 9 11626.1 625.266 3 2 -4 10 8564.36 513.530 10 2 -4 10 8414.05 531.023 9 2 -4 10 9285.94 559.995 3 2 -4 11 252.066 145.411 3 2 -4 11 400.888 169.457 10 2 -4 11 298.576 180.764 9 2 -4 11 41.2201 173.280 2 2 -4 12 2934.33 360.020 2 2 -4 13 323.909 149.033 2 2 -4 14 913.643 156.700 2 -2 3 15 7483.34 412.823 15 -2 3 14 3956.59 383.684 15 -2 3 14 4099.22 378.240 11 -2 3 13 768.304 211.613 11 -2 3 13 778.795 231.175 15 -2 3 12 2759.60 333.591 2 -2 3 12 2551.01 342.917 11 -2 3 12 2991.38 393.637 15 -2 3 11 709.961 230.916 15 -2 3 11 1020.00 242.513 2 -2 3 11 1138.90 263.145 11 -2 3 10 4597.10 459.396 15 -2 3 10 5010.06 422.669 2 -2 3 10 3962.74 575.668 14 -2 3 10 5004.04 431.294 11 -2 3 9 5128.80 599.401 14 -2 3 8 1435.02 306.779 19 -2 3 7 945.761 282.454 19 -2 3 6 2872.54 306.468 20 -2 3 6 2892.02 394.681 19 -2 3 5 515.484 227.074 19 -2 3 5 133.488 142.524 20 2 -3 -5 388.439 125.620 17 -2 3 4 68.5482 174.750 19 2 -3 -4 58.0202 124.575 17 -2 3 4 243.623 121.463 20 2 -3 -3 10611.3 481.932 17 -2 3 3 9441.94 392.675 20 2 -3 -2 71572.6 1211.80 17 -2 3 2 68672.7 1011.59 20 2 -3 -1 2152.06 239.505 17 -2 3 1 1772.31 186.623 20 -2 3 0 4790.96 295.149 20 2 -3 0 5362.56 347.288 17 2 -3 1 17760.9 613.617 17 2 -3 1 16471.3 635.800 18 2 -3 2 26095.3 816.555 18 2 -3 3 27018.7 858.110 18 2 -3 3 25291.7 777.930 13 2 -3 4 82755.2 1512.17 13 2 -3 5 46976.6 1263.32 13 2 -3 6 12988.6 728.528 13 2 -3 7 4660.41 472.879 13 2 -3 8 19859.1 1074.20 13 2 -3 9 8868.56 516.961 10 2 -3 9 9054.20 540.106 9 2 -3 9 9418.65 558.101 3 2 -3 10 32368.1 1026.33 3 2 -3 10 31870.0 988.201 9 2 -3 10 30732.5 983.658 10 2 -3 11 993.448 230.896 10 2 -3 11 1109.68 215.492 3 2 -3 11 935.906 220.484 9 2 -3 11 960.785 243.007 2 2 -3 12 890.454 267.666 2 2 -3 12 992.144 232.081 10 2 -3 13 7328.83 500.861 2 2 -3 14 759.715 192.730 2 -2 2 15 938.306 173.190 15 -2 2 14 908.711 222.468 15 -2 2 14 732.400 196.319 11 -2 2 13 8013.86 565.704 15 -2 2 13 7945.36 535.652 11 -2 2 13 7929.06 519.840 2 -2 2 12 2101.92 343.082 15 -2 2 12 1714.63 310.025 11 -2 2 12 1810.76 297.183 2 -2 2 11 6546.54 559.624 15 -2 2 11 6661.66 514.898 11 -2 2 11 7390.80 540.924 2 -2 2 10 16824.2 840.514 15 -2 2 10 14379.1 1053.50 14 -2 2 10 16478.1 775.630 11 -2 2 10 16045.2 755.741 2 -2 2 9 78.6386 211.167 14 -2 2 8 3030.51 446.954 14 -2 2 7 8487.36 650.019 19 -2 2 6 16238.4 841.500 19 -2 2 5 734.660 256.908 19 2 -2 -5 542.238 132.212 17 -2 2 4 2418.21 299.626 19 -2 2 4 2297.49 211.034 20 2 -2 -4 2316.07 222.811 17 -2 2 3 11752.3 393.942 20 2 -2 -3 12906.0 475.836 17 -2 2 3 13158.1 571.912 19 -2 2 2 18165.1 431.933 20 2 -2 -2 18603.8 568.640 17 2 -2 -1 223.358 124.792 17 -2 2 1 278.030 90.2007 20 -2 2 0 194725. 1466.62 20 2 -2 0 213944. 1863.61 17 2 -2 1 65365.6 1039.62 17 2 -2 2 34434.9 846.014 18 2 -2 2 33067.5 751.906 17 2 -2 3 12591.1 535.302 18 2 -2 4 36779.4 956.537 13 2 -2 4 38222.3 947.562 18 2 -2 5 11983.4 609.515 13 2 -2 6 54777.9 1402.52 13 2 -2 7 15020.7 816.606 13 2 -2 8 5242.33 536.412 13 2 -2 9 8098.43 699.231 13 2 -2 9 6789.72 456.965 10 2 -2 10 19673.7 762.914 9 2 -2 10 20306.0 805.364 10 2 -2 10 20196.2 805.245 3 2 -2 11 91.3572 126.995 9 2 -2 11-52.0617 149.893 10 2 -2 11 391.344 174.864 3 2 -2 12 2441.98 321.283 10 2 -2 12 2117.56 334.450 2 2 -2 13-137.963 177.574 2 2 -2 13 41.7671 153.634 10 2 -2 14 3919.92 347.490 2 2 -2 15 2182.50 222.165 2 -2 1 15 534.273 120.809 15 -2 1 14 1897.23 266.734 15 -2 1 14 1600.07 260.742 11 -2 1 13 6845.75 496.689 2 -2 1 13 5868.23 477.643 15 -2 1 13 5889.95 465.564 11 -2 1 12 1917.81 331.383 15 -2 1 12 2192.36 325.605 2 -2 1 12 2251.58 345.067 11 -2 1 11 8950.32 510.660 7 -2 1 11 7845.39 611.805 15 -2 1 11 8056.15 574.817 11 -2 1 11 8510.75 586.150 2 -2 1 10 865.655 258.437 15 -2 1 10 921.101 239.372 6 -2 1 10 640.553 232.966 2 -2 1 10 1054.62 253.960 11 -2 1 10 723.025 206.778 7 -2 1 9 2139.81 438.061 14 -2 1 8 9455.82 763.842 14 -2 1 7-27.4034 135.800 14 -2 1 6 40173.2 1293.61 19 2 -1 -5 5528.54 297.147 17 -2 1 5 4902.85 432.117 19 -2 1 4 15681.6 676.971 19 2 -1 -4 16708.2 513.725 17 -2 1 3 151136. 1827.97 19 2 -1 -3 147356. 1488.44 17 -2 1 2 69325.5 1105.31 19 -2 1 2 66623.2 688.329 20 2 -1 -2 69120.5 1010.04 17 -2 1 1 12305.4 249.034 20 -2 1 1 11972.4 412.927 19 2 -1 -1 12303.9 427.803 17 2 -1 0 46089.9 550.944 21 2 -1 0 45312.1 793.412 17 2 -1 1 99189.8 1147.12 17 2 -1 1 91982.3 982.643 21 2 -1 2 2288.13 210.133 21 2 -1 2 2472.99 206.204 17 2 -1 3 20725.8 523.522 17 2 -1 3 20158.3 600.789 21 2 -1 3 20755.4 606.454 18 2 -1 4 50234.5 968.922 18 2 -1 4 49234.3 809.885 17 2 -1 5 105785. 1662.65 13 2 -1 6 162.527 156.640 13 2 -1 7 1708.17 308.835 13 2 -1 8 290.138 173.144 13 2 -1 9 5550.06 566.764 13 2 -1 10 6263.20 448.243 3 2 -1 10 6735.61 663.424 13 2 -1 10 6040.52 424.705 9 2 -1 10 6251.54 451.285 10 2 -1 11 21761.6 855.633 10 2 -1 11 20494.2 755.437 9 2 -1 11 20102.3 803.391 11 2 -1 11 21519.3 843.465 3 2 -1 12 8577.84 606.502 2 2 -1 12 9316.27 565.950 11 2 -1 12 9097.55 569.048 10 2 -1 13 535.195 186.605 10 2 -1 13 899.003 192.686 11 2 -1 13 683.865 188.932 2 2 -1 14 865.274 235.805 2 2 -1 15 636.644 176.438 2 -2 0 14 763.733 197.096 2 -2 0 14 500.684 183.861 15 -2 0 13 958.022 246.377 2 -2 0 13 649.352 202.555 15 -2 0 13 468.600 232.644 11 -2 0 12-200.607 191.698 15 -2 0 12 26.2287 177.910 2 -2 0 12 180.580 230.592 11 -2 0 11 891.579 274.754 15 -2 0 11 1121.87 275.053 2 -2 0 11 913.493 258.928 11 -2 0 11 1350.54 240.212 7 -2 0 10 2346.23 293.280 7 -2 0 10 2462.48 342.113 11 -2 0 10 2128.63 320.111 15 -2 0 10 1915.07 322.674 2 -2 0 9 3361.26 345.495 3 -2 0 9 2245.37 430.278 14 -2 0 9 3532.30 374.540 2 -2 0 9 2639.47 333.689 11 -2 0 9 3232.19 391.361 15 -2 0 9 3588.88 330.636 7 -2 0 9 2939.42 325.456 6 -2 0 8 15375.4 985.182 14 -2 0 7 3191.83 425.535 14 -2 0 6 151.018 216.901 14 2 0 -5 88390.3 1134.84 17 -2 0 5 91353.4 1845.26 14 -2 0 4 17106.1 715.024 19 2 0 -4 17632.1 509.614 17 -2 0 3 5218.91 369.663 19 2 0 -3 5265.13 287.153 17 2 0 -2 25650.5 600.810 17 -2 0 2 25340.3 676.697 19 -2 0 1 909.253 154.135 19 2 0 -1 426.027 134.546 17 2 0 0 99111.1 1127.44 17 -2 0 0 99293.6 926.822 19 2 0 1 3560.52 230.019 17 2 0 2 277178. 1777.36 17 2 0 2 273537. 1837.40 21 2 0 3 1243.56 193.358 21 2 0 3 1243.94 139.986 17 2 0 4 1972.89 241.486 21 2 0 4 1788.55 147.706 17 2 0 4 1920.47 190.828 18 2 0 5 3202.24 306.096 13 2 0 5 3069.40 299.856 21 2 0 5 3496.69 183.087 17 2 0 6 20690.8 795.398 21 2 0 6 19308.3 554.984 14 2 0 6 19370.8 755.526 13 2 0 7 26012.7 954.856 13 2 0 8 8118.32 602.458 13 2 0 9 3794.23 437.570 13 2 0 10 458.610 217.960 13 2 0 11 3233.01 390.174 2 2 0 11 3160.03 352.742 3 2 0 11 3068.17 343.767 11 2 0 11 2890.62 297.444 12 2 0 11 3666.13 380.208 10 2 0 12 2601.26 319.991 10 2 0 12 1729.39 301.880 11 2 0 12 2644.41 364.070 2 2 0 13 397.027 174.845 11 2 0 13 635.983 187.342 10 2 0 14 400.214 196.620 2 2 0 14 127.599 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4966.03 227.622 14 2 2 1 5183.50 209.375 20 2 2 1 5095.27 291.207 17 2 2 2 1642.36 188.372 17 2 2 2 1718.21 152.978 20 2 2 3 1274.29 151.860 17 2 2 3 1170.88 64.8192 19 2 2 3 1491.30 172.936 20 2 2 4 62650.0 1076.88 20 2 2 4 60366.1 838.698 17 2 2 5 59589.4 700.561 14 2 2 5 58185.0 1131.97 21 2 2 5 58191.1 596.965 18 2 2 6 72.8909 43.4475 14 2 2 6 33.5066 146.862 21 2 2 6-0.75411 134.033 13 2 2 7 101620. 1707.30 13 2 2 7 100985. 1776.17 21 2 2 8 1651.54 273.325 13 2 2 8 1591.77 289.385 21 2 2 9 352.595 171.044 13 2 2 10 5743.55 533.299 13 2 2 11 2259.95 287.260 12 2 2 11 2090.28 381.555 13 2 2 11 2453.84 305.810 11 2 2 11 2708.68 337.956 2 2 2 12 262.298 154.218 12 2 2 12-24.8758 143.184 11 2 2 12 126.175 154.466 10 2 2 12 251.388 157.076 2 2 2 13 3450.45 332.139 12 2 2 13 3273.78 378.432 11 2 2 13 3065.75 368.175 2 2 2 13 2792.03 331.295 10 2 2 14 9837.26 593.725 11 2 2 14 10619.8 595.600 2 2 2 14 11167.3 591.281 10 2 2 15 6108.10 426.314 10 2 2 15 5648.96 433.174 11 2 2 15 4761.75 367.992 2 2 2 16 254.883 137.080 11 -2 -3 13 306.454 145.208 2 -2 -3 12 135.106 128.726 15 -2 -3 12 85.5145 174.477 2 -2 -3 11 4542.85 428.841 3 -2 -3 11 4403.98 407.029 15 -2 -3 11 4458.69 441.299 2 -2 -3 10 2078.18 298.125 7 -2 -3 10 1834.01 296.686 15 -2 -3 10 1290.44 259.941 3 -2 -3 10 1545.05 279.792 11 -2 -3 10 1405.86 287.244 2 -2 -3 9 14594.7 759.241 15 -2 -3 9 14867.3 755.119 3 -2 -3 9 14380.6 729.584 11 -2 -3 9 13415.3 743.379 2 -2 -3 9 14437.5 691.471 7 -2 -3 8 1209.44 244.487 7 -2 -3 8 696.837 223.827 15 -2 -3 8 249.469 176.621 14 -2 -3 8 987.056 232.525 11 -2 -3 8 829.161 212.321 3 -2 -3 8 776.988 210.769 2 -2 -3 7 4066.74 518.733 14 -2 -3 6 1331.10 298.084 14 -2 -3 5 39610.6 1365.69 14 -2 -3 4-81.3200 180.737 14 2 3 -4 199.417 130.241 17 2 3 -3 12464.9 529.561 17 -2 -3 3 12144.3 645.901 14 2 3 -2 3654.57 293.443 17 -2 -3 2 3268.49 336.396 14 -2 -3 1 418.897 146.261 14 2 3 -1 486.503 119.622 20 -2 -3 0 6211.93 356.357 14 2 3 0 6537.49 293.845 20 -2 -3 -1 571644. 2767.04 14 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4 6 71266.8 1135.02 13 2 4 6 72324.3 1489.95 20 2 4 6 71546.5 1129.16 19 2 4 7 884.223 175.639 13 2 4 7 951.333 234.827 20 2 4 7 1244.13 239.480 21 2 4 7 1163.07 195.149 19 2 4 8 37651.9 1034.34 13 2 4 8 36951.2 1003.93 19 2 4 8 36719.3 1109.66 21 2 4 8 37261.7 1285.01 20 2 4 9 603.442 189.057 13 2 4 9 570.740 204.541 21 2 4 10-15.5897 135.771 13 2 4 10-275.807 153.507 21 2 4 11 7145.16 587.355 13 2 4 11 7121.65 462.420 12 2 4 11 6984.30 489.837 11 2 4 12 994.274 198.451 12 2 4 12 771.096 210.010 11 2 4 13 12928.6 646.854 12 2 4 13 14031.4 721.975 11 2 4 13 13151.3 635.311 10 2 4 14 4275.41 411.631 11 2 4 14 3961.87 363.018 10 2 4 15 1339.21 246.158 10 2 4 15 1473.89 258.414 11 2 4 16 8394.35 475.141 11 2 4 17 3569.43 270.172 11 -2 -5 12 49.5259 116.111 2 -2 -5 11-84.0412 116.899 15 -2 -5 11 254.957 181.558 3 -2 -5 11 32.7484 146.313 2 -2 -5 10 866.349 244.585 2 -2 -5 10 931.631 226.880 15 -2 -5 10 674.429 215.501 3 -2 -5 9 13463.9 716.759 3 -2 -5 9 12302.2 666.562 15 -2 -5 9 13163.1 729.376 2 -2 -5 9 13830.4 680.727 7 -2 -5 8 54334.4 1413.47 15 -2 -5 8 55576.3 1348.28 7 -2 -5 8 56023.6 1454.28 3 -2 -5 8 54651.6 1448.08 2 -2 -5 7 8608.87 566.728 15 -2 -5 7 8290.67 518.659 7 -2 -5 7 7934.23 563.579 3 -2 -5 7 7486.14 551.281 2 -2 -5 6 62.5731 186.997 14 2 5 -6-136.139 101.116 20 -2 -5 5 5497.68 580.042 14 2 5 -5 6215.64 572.991 20 -2 -5 4 1315.09 280.587 14 2 5 -4 1226.08 240.365 20 -2 -5 3 15117.2 815.821 14 2 5 -3 15504.7 738.843 20 2 5 -2 32599.6 979.594 20 -2 -5 2 33356.6 1118.66 14 2 5 -1 18907.5 709.293 20 2 5 0 1090.91 204.705 20 2 5 1-14.4931 102.923 20 2 5 2 225383. 2234.72 20 2 5 3 24200.0 745.124 20 2 5 4 170612. 2009.02 20 2 5 5 60785.9 848.872 13 2 5 5 63051.6 1318.90 20 2 5 6 17544.0 533.431 13 2 5 6 16992.1 752.479 20 2 5 6 16985.3 602.522 19 2 5 7 787.433 164.188 13 2 5 7 445.171 144.973 19 2 5 8 269.098 109.705 13 2 5 8-211.727 143.873 19 2 5 8 235.463 183.993 20 2 5 8 118.766 144.434 21 2 5 9 2081.62 323.631 21 2 5 9 1295.40 190.705 13 2 5 9 1363.24 355.557 20 2 5 10 3733.86 422.409 21 2 5 11 1336.57 240.987 11 2 5 11 1489.85 225.847 12 2 5 12 999.271 213.675 12 2 5 12 938.025 222.160 11 2 5 13 798.880 228.731 11 2 5 13 1010.89 216.538 10 2 5 14 771.526 226.546 11 2 5 14 921.023 225.397 10 2 5 15 320.954 190.424 11 2 5 15 122.268 135.354 10 2 5 16 2141.97 279.775 11 2 5 17 2044.62 233.718 11 -2 -6 12 2254.42 182.719 2 -2 -6 11 265.080 184.399 3 -2 -6 11 208.190 129.771 2 -2 -6 10 7057.47 438.365 15 -2 -6 10 6466.82 463.653 3 -2 -6 10 6373.56 455.710 2 -2 -6 9 1454.02 246.802 15 -2 -6 9 1236.55 267.773 3 -2 -6 9 949.910 232.575 2 -2 -6 8 4823.09 465.547 3 -2 -6 8 4489.39 435.178 2 -2 -6 8 4813.93 435.252 15 -2 -6 8 5288.50 436.704 7 -2 -6 7 16876.9 739.709 7 -2 -6 7 15926.5 764.670 15 -2 -6 7 18238.9 831.853 2 -2 -6 7 16686.3 817.601 3 -2 -6 6 3236.52 378.740 15 2 6 -6 2653.70 388.369 20 -2 -6 6 2517.85 314.797 2 -2 -6 6 3267.58 324.602 7 2 6 -5 1736.14 293.996 20 2 6 -4 15830.8 878.417 20 2 6 -3 169.957 162.318 20 2 6 -2 49779.9 1345.13 20 2 6 -1 6316.04 474.560 20 2 6 0 5677.65 434.421 20 2 6 1 80894.8 1510.45 20 2 6 2 31531.1 947.691 20 2 6 3 32263.9 955.379 20 2 6 4 10586.5 566.471 20 2 6 5 22843.1 845.469 20 2 6 6 164.840 191.864 20 2 6 7 13392.3 750.522 20 2 6 7 14128.1 633.444 19 2 6 8 399.211 156.822 21 2 6 8 10.7540 86.1792 19 2 6 8 244.749 197.689 20 2 6 9-368.999 255.449 20 2 6 9 1.23490 144.710 21 2 6 10 34401.6 1490.84 20 2 6 11 1299.70 231.172 12 2 6 11 1183.44 253.883 11 2 6 12-303.274 169.614 11 2 6 13 3.59687 179.224 11 2 6 14 19849.1 845.262 11 2 6 15 2859.03 349.850 11 2 6 16 130.429 178.062 11 2 6 17 549.641 156.380 11 -2 -7 11 604.508 131.154 2 -2 -7 10 233.634 170.317 3 -2 -7 10 295.693 144.936 2 -2 -7 9 195.820 124.017 15 -2 -7 9 186.299 173.421 3 -2 -7 9 36.1703 129.963 2 -2 -7 8 2497.13 339.151 2 -2 -7 8 2835.51 358.530 3 -2 -7 8 2475.87 313.339 15 -2 -7 7 5404.21 456.389 15 -2 -7 7 5346.81 492.769 3 -2 -7 7 5343.79 478.849 2 -2 -7 7 4824.34 410.949 7 -2 -7 6 812.762 250.814 15 -2 -7 6 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7 14352.8 779.912 21 4 4 8 184.021 143.639 13 4 4 8 310.636 191.085 21 4 4 9 3304.62 410.525 13 4 4 9 2955.51 417.665 21 4 4 10 11093.6 726.665 13 4 4 10 11368.1 802.538 21 4 4 11 78820.4 2052.09 13 4 4 11 79025.2 1543.04 12 4 4 11 78679.5 1575.17 11 4 4 11 82607.8 2237.56 21 4 4 12 264.133 186.470 12 4 4 12 286.858 187.551 11 4 4 13 20787.5 826.606 12 4 4 13 21373.7 863.639 11 4 4 14 131.106 179.648 12 4 4 14-116.560 169.664 11 4 4 15 4480.71 367.247 12 4 4 15 3939.96 354.155 11 4 4 15 4170.22 358.196 10 4 4 16 4646.94 334.103 11 4 4 16 5360.30 351.971 10 4 4 17 6180.91 298.051 11 4 4 17 7568.07 335.815 10 -4 -5 11-6.19926 114.765 15 -4 -5 10 224.737 159.732 15 -4 -5 9 6428.72 492.377 15 -4 -5 9 6021.72 428.639 3 -4 -5 9 5819.47 430.877 2 -4 -5 9 6543.61 465.128 7 -4 -5 8-95.0142 156.185 7 -4 -5 8-309.457 191.061 15 -4 -5 8 1.07109 172.316 3 -4 -5 8-231.918 177.944 2 -4 -5 7 8738.24 614.360 15 -4 -5 7 8037.19 540.750 3 -4 -5 7 8837.94 577.512 2 -4 -5 7 8847.78 574.322 7 -4 -5 6 847.946 251.336 7 -4 -5 6 659.788 227.754 6 -4 -5 6 1042.70 243.421 15 -4 -5 6 868.339 223.650 3 -4 -5 6 1108.45 197.923 2 -4 -5 5 842.152 206.699 6 -4 -5 5 1102.60 251.596 15 -4 -5 5 1059.68 195.686 3 -4 -5 4 257.924 166.761 14 4 5 -3 3608.87 405.786 17 -4 -5 3 4016.34 475.086 14 -4 -5 2 5147.84 534.823 14 4 5 -2 5353.95 495.843 17 -4 -5 1 2650.90 349.639 14 4 5 -1 2916.07 366.575 17 -4 -5 0 420.641 162.975 14 4 5 0 36.4350 158.728 17 4 5 1 12495.1 705.303 17 4 5 2 3493.98 278.751 20 4 5 2 3852.53 404.559 17 4 5 3 145.130 147.013 20 4 5 3 365.591 227.220 17 4 5 4 6248.84 413.413 20 4 5 4 5817.55 462.679 17 4 5 5 11516.4 627.910 17 4 5 5 12777.7 626.773 20 4 5 6 19319.2 829.003 20 4 5 6 19746.4 815.576 17 4 5 7 9606.59 640.803 20 4 5 7 9080.87 540.896 17 4 5 8 27170.2 1113.84 21 4 5 8 26418.7 936.500 13 4 5 8 27228.1 1164.81 20 4 5 9 13587.7 733.089 13 4 5 9 14575.1 854.074 21 4 5 10 8644.61 658.302 13 4 5 10 8880.34 704.171 21 4 5 11 46293.0 1183.92 12 -4 -5 -11 43877.3 1171.15 4 4 5 11 45977.2 1214.77 11 4 5 11 47381.7 1672.64 21 4 5 12 94810.4 1736.71 12 4 5 12 92440.7 1764.89 11 4 5 13 20054.1 815.576 12 4 5 13 19425.2 843.790 11 4 5 14 5439.82 436.840 12 4 5 14 4552.61 420.433 11 4 5 15 5571.92 414.469 12 4 5 15 5592.92 422.017 11 4 5 15 5948.87 413.942 10 4 5 16 1954.72 260.708 11 4 5 16 1896.44 239.836 10 4 5 17 360.079 122.793 11 4 5 17 286.902 118.972 10 -4 -6 10 1892.80 230.892 15 -4 -6 9 1114.29 237.490 15 -4 -6 9 1164.01 221.942 3 -4 -6 9 1082.44 202.419 2 -4 -6 9 1264.63 248.009 7 -4 -6 8 250.284 183.923 15 -4 -6 8-90.1867 160.908 3 -4 -6 8 272.532 131.897 2 -4 -6 8-41.4645 167.021 7 -4 -6 7 9062.04 617.004 15 -4 -6 7 8291.34 551.942 3 -4 -6 7 9272.18 561.125 2 -4 -6 7 9633.00 576.451 7 -4 -6 6 651.062 226.423 7 -4 -6 6 401.374 227.050 15 -4 -6 6 259.003 158.165 3 -4 -6 5 19611.4 873.808 15 -4 -6 5 18296.0 787.148 3 -4 -6 5 19167.9 788.433 7 -4 -6 4 17136.7 731.549 6 -4 -6 4 18493.1 826.340 15 -4 -6 4 17877.4 701.614 16 -4 -6 4 17633.9 1092.75 14 -4 -6 3 1436.67 291.317 14 4 6 -3 1373.28 312.242 17 -4 -6 2 404.372 176.872 14 4 6 -2 383.889 168.466 17 -4 -6 1 119.882 174.049 14 4 6 -1 245.763 188.962 17 4 6 0 5052.00 498.003 17 4 6 1 39955.2 1031.23 20 4 6 1 40110.9 1325.33 17 4 6 2 26263.5 822.013 20 4 6 2 26096.7 1051.16 17 4 6 3 25959.0 837.693 20 4 6 3 24884.5 1011.44 17 4 6 4 26738.8 894.365 20 4 6 4 25241.2 1011.01 17 4 6 5 1442.04 255.605 20 4 6 5 1562.30 289.935 17 4 6 6 951.533 228.852 20 4 6 6 940.381 222.860 17 4 6 7 46.0624 143.458 17 4 6 7 328.034 160.638 20 4 6 8 3116.21 435.452 20 4 6 9 10948.4 752.826 21 4 6 9 10224.6 776.890 20 4 6 10 18837.4 1039.66 21 4 6 11 26135.2 897.716 12 -4 -6 -11 25077.4 913.539 4 4 6 11 25761.3 1230.21 21 4 6 12 74790.2 1554.52 12 4 6 12 72819.7 1582.28 11 4 6 13 40.8921 155.402 12 4 6 13 76.8844 188.655 11 4 6 14 6191.67 463.371 12 4 6 14 6187.88 479.828 11 4 6 15 26077.3 890.832 11 4 6 15 26208.1 793.417 10 4 6 16 1498.11 226.579 11 4 6 16 1453.86 210.440 10 4 6 17 4666.67 303.656 11 4 6 17 4519.93 251.697 10 -4 -7 9 87.1367 147.273 15 -4 -7 9 344.223 155.398 3 -4 -7 8 1529.30 257.562 15 -4 -7 8 1646.74 241.694 3 -4 -7 8 2310.88 299.385 7 -4 -7 7 3847.66 410.026 15 -4 -7 7 3805.24 364.517 3 -4 -7 7 3803.32 369.836 7 -4 -7 6 5266.90 476.870 15 -4 -7 6 5644.21 468.522 3 -4 -7 6 5991.32 454.709 7 -4 -7 5 123.489 149.352 7 -4 -7 5-32.9998 115.257 16 -4 -7 5-40.4621 190.926 15 -4 -7 4 7901.71 560.324 15 -4 -7 4 7620.33 486.852 16 -4 -7 4 7921.31 510.067 7 -4 -7 3 160.730 116.544 16 -4 -7 3 74.6304 166.727 15 4 7 -2 28700.5 1260.36 17 4 7 -1 240.014 135.578 17 4 7 0 8411.88 673.523 17 4 7 1 13440.8 685.538 20 4 7 1 11638.9 775.572 17 4 7 2 19435.2 802.311 20 4 7 2 17161.9 914.853 17 4 7 3 954.560 224.532 20 4 7 3 1080.31 290.573 17 4 7 4 25877.1 941.027 20 4 7 4 23395.5 1054.83 17 4 7 5 15263.6 758.749 20 4 7 5 14407.6 820.335 17 4 7 6-52.5034 110.869 20 4 7 6-11.7517 110.072 17 4 7 7 1698.36 297.064 17 4 7 7 1643.38 311.585 20 4 7 8-107.865 200.508 20 4 7 9 7314.09 638.681 21 4 7 9 6431.99 636.364 20 4 7 10 24.5475 111.999 12 4 7 10 184.494 203.416 20 4 7 10 526.232 259.438 21 -4 -7 -10 84.3733 142.999 4 4 7 11 20288.6 1117.64 21 4 7 11 21242.8 810.285 12 -4 -7 -11 19303.8 835.339 4 4 7 12 98772.1 1780.19 12 4 7 12 100354. 1854.89 11 4 7 13 9729.95 580.841 12 4 7 13 10596.1 629.588 11 4 7 14 6341.35 483.858 11 4 7 15 1555.66 265.595 11 4 7 15 1078.66 192.151 10 4 7 16 243.754 132.986 10 4 7 16 324.920 153.558 11 4 7 17 7236.70 378.594 11 -4 -8 8 878.726 196.108 15 -4 -8 8 924.018 190.467 3 -4 -8 7 1841.77 273.195 15 -4 -8 7 1990.51 282.963 3 -4 -8 7 1819.09 252.473 7 -4 -8 6 96.6716 174.527 15 -4 -8 6-416.188 199.146 3 -4 -8 6 97.8817 152.486 7 -4 -8 5 1316.30 241.182 7 -4 -8 5 1557.07 235.557 16 -4 -8 5 1279.02 289.620 15 -4 -8 4 5711.98 494.177 15 -4 -8 4 6417.23 466.448 16 -4 -8 4 6007.73 431.179 7 -4 -8 3 34627.7 1126.48 15 -4 -8 3 31616.2 995.208 16 -4 -8 3 32482.7 966.962 7 -4 -8 2 10071.5 613.343 15 4 8 -2 9112.01 748.744 17 -4 -8 2 9542.20 558.303 16 -4 -8 1 13558.6 681.474 15 4 8 -1 12719.0 871.377 17 -4 -8 1 13015.1 620.771 16 4 8 0 28812.5 1309.75 17 4 8 1 4285.69 525.547 17 4 8 2 49828.0 1405.02 20 4 8 3 449.759 187.654 20 4 8 4 63043.6 1586.57 20 4 8 5 7991.00 598.409 20 4 8 6 8645.17 641.563 20 4 8 6 7427.85 641.141 17 4 8 7 55242.8 1687.18 20 4 8 7 54302.7 1649.23 17 4 8 8 1092.04 248.697 20 4 8 9-272.160 138.342 20 -4 -8 -9-17.3859 93.9772 4 4 8 10 596.455 241.753 20 4 8 10-187.836 142.312 12 4 8 10 225.693 121.247 5 -4 -8 -10-17.1897 135.079 4 4 8 10 481.570 219.286 21 4 8 11 29713.6 938.518 5 4 8 11 29915.2 960.232 12 -4 -8 -11 29554.2 1032.98 4 4 8 12 4512.54 398.142 5 4 8 13 1449.33 268.843 11 4 8 14 92.6612 169.053 11 4 8 15 11366.5 601.665 11 4 8 16-53.6435 122.959 11 4 8 17 2861.82 249.047 11 -4 -9 8 4894.54 304.102 3 -4 -9 7 342.990 158.987 3 -4 -9 6 1234.82 253.800 15 -4 -9 6 1396.78 261.988 3 -4 -9 6 1630.18 234.635 7 -4 -9 5 374.397 199.340 15 -4 -9 5 457.525 196.657 3 -4 -9 5 254.309 149.782 7 -4 -9 5 624.012 180.658 16 -4 -9 4 2117.86 272.779 7 -4 -9 4 2870.01 368.308 15 -4 -9 4 2886.63 333.781 16 -4 -9 3 17712.0 817.034 15 -4 -9 3 16460.7 737.354 16 -4 -9 2 491.877 177.753 16 -4 -9 2 123.882 187.662 15 -4 -9 1 19216.8 826.458 15 4 9 -1 17876.2 1093.68 17 -4 -9 1 18801.0 779.567 16 -4 -9 0 15997.6 731.990 15 4 9 0 17305.6 1059.65 17 -4 -9 0 17118.4 725.165 16 -4 -9 -1 890.375 207.811 16 4 9 1 336.601 183.266 17 4 9 2 48019.5 1513.26 20 4 9 3 34584.7 1260.28 20 4 9 4 9696.84 704.177 20 4 9 5 1012.96 244.925 20 4 9 6 294.068 174.713 20 4 9 7 36.9861 109.995 20 4 9 7-138.843 238.751 17 4 9 8 15919.5 696.476 5 -4 -9 -8 16319.6 738.775 4 4 9 8 16083.1 995.659 20 -4 -9 -9-30.7419 161.424 4 4 9 9-132.622 115.971 5 4 9 10 24751.0 891.709 5 -4 -9 -10 24506.7 945.741 4 4 9 11 3533.86 351.451 5 -4 -9 -11 2855.56 370.626 4 4 9 12 4003.40 365.429 5 4 9 13 3464.51 330.838 5 4 9 13 3031.25 375.260 11 4 9 14 628.043 215.530 11 4 9 15 2149.29 291.620 11 4 9 16-16.1498 137.193 11 4 9 17 3960.34 281.915 11 -4 -10 7 21.7649 101.381 3 -4 -10 6 492.616 165.040 3 -4 -10 5 44.4824 155.985 16 -4 -10 5 23.3520 165.443 3 -4 -10 4 2.78576 138.412 16 -4 -10 3 18197.9 770.826 16 -4 -10 2 1403.66 258.912 16 -4 -10 1 11816.2 645.048 16 -4 -10 0 1643.39 279.448 16 4 10 1 7576.05 774.721 17 -4 -10 -1 10004.1 588.941 16 -4 -10 -2 390.815 179.191 16 4 10 3 3843.10 471.111 20 -4 -10 -3 3071.05 303.841 16 -4 -10 -4 2590.01 308.188 16 4 10 4 2899.07 394.952 20 4 10 5-112.045 132.733 20 4 10 6 3114.94 340.605 5 4 10 6 2496.86 371.017 20 4 10 7 47648.8 1220.46 5 -4 -10 -7 46246.5 1213.95 4 4 10 7 51539.6 1779.75 20 4 10 7 47978.7 1754.20 17 4 10 8 3417.85 471.784 20 4 10 8 2210.55 281.950 5 -4 -10 -8 2929.38 355.322 4 4 10 9 21292.7 845.089 5 -4 -10 -9 20288.8 857.094 4 4 10 10 6212.80 467.741 5 4 10 11-219.099 157.709 5 4 10 12 15010.2 691.301 5 4 10 13 119.745 117.736 5 4 10 13 28.9482 171.772 11 4 10 14-154.334 148.062 5 4 10 14 117.346 180.274 11 4 10 15-5.20744 158.571 11 4 10 16 435.012 166.513 11 4 10 17 315.545 110.573 11 -4 -11 6 1857.02 199.661 3 -4 -11 5 558.860 146.059 16 -4 -11 5 711.120 179.183 3 -4 -11 4 408.316 164.322 16 -4 -11 3 1962.98 286.312 16 -4 -11 2 18266.1 764.881 16 -4 -11 1 9174.59 562.609 16 -4 -11 0-223.914 196.665 16 -4 -11 -1 108.389 142.058 16 -4 -11 -2 35124.9 1065.62 16 -4 -11 -3 12851.2 641.649 16 4 11 4 7899.12 494.703 5 -4 -11 -4 8730.07 513.001 16 4 11 5 37285.8 1071.62 5 -4 -11 -5 37991.9 1024.42 16 4 11 6 3674.75 355.396 5 4 11 7 8214.27 536.633 5 4 11 8 2035.53 293.691 5 4 11 9 10036.7 606.688 5 4 11 10 19168.3 814.644 5 4 11 11 6335.63 480.697 5 4 11 12 22049.9 841.645 5 4 11 13 560.007 177.213 5 4 11 13 693.790 200.298 11 4 11 14 1873.31 251.257 5 4 11 14 1855.44 267.286 11 4 11 15 655.914 187.436 11 4 11 16 530.626 152.373 11 4 11 17-6.82933 73.5845 11 -4 -12 5 1046.41 155.764 3 -4 -12 4 918.351 175.629 16 -4 -12 4 802.045 189.218 3 -4 -12 3 3311.40 307.036 16 -4 -12 2 4976.94 402.961 16 -4 -12 1 161.158 175.681 16 -4 -12 0 781.407 259.308 16 -4 -12 -1 5891.54 466.499 16 -4 -12 -2 1286.29 273.470 16 -4 -12 -3 38480.5 1101.37 1 -4 -12 -3 38076.0 1088.47 16 4 12 4 17535.4 707.240 5 -4 -12 -4 18272.1 750.634 16 4 12 5 17910.9 745.466 5 -4 -12 -5 17245.3 712.555 16 4 12 6 22442.1 846.932 5 4 12 7 5118.58 428.453 5 4 12 8 7182.55 511.426 5 4 12 9 11693.2 637.707 5 4 12 10 211.914 151.714 5 4 12 11 2035.28 294.724 5 4 12 12 10437.5 575.902 5 4 12 12 9502.21 533.818 11 4 12 13 92.5574 150.011 5 4 12 13-97.9815 158.996 11 4 12 14 390.681 177.183 5 4 12 14 216.591 155.779 11 4 12 15 133.949 105.178 5 4 12 15 58.5968 113.295 11 4 12 16 286.845 110.042 11 -4 -13 4 2.17724 72.0970 3 -4 -13 3 1252.64 182.393 16 -4 -13 3 1311.92 194.765 3 -4 -13 2 35.1556 146.465 16 -4 -13 1-18.0283 160.936 16 -4 -13 0 2642.93 319.234 16 -4 -13 -1 296.247 191.349 16 -4 -13 -2 2387.44 300.173 16 -4 -13 -3 2187.30 294.444 1 -4 -13 -3 2499.91 300.609 16 -4 -13 -4 3160.17 345.902 1 -4 -13 -4 3094.27 329.233 16 4 13 5 20924.7 767.988 5 -4 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16721.3 453.830 16 -4 -16 -5 12062.9 443.352 1 -4 -16 -6 1742.74 211.188 1 -4 -16 -7 671.815 158.434 1 4 16 8 235.607 100.089 5 -4 -16 -8-170.431 120.568 1 4 16 9 3481.19 245.054 5 -4 -16 -9 4246.43 302.107 1 -4 -16 -10 110.617 113.330 1 4 16 10 28.5834 93.8188 5 4 16 11 3836.38 244.061 5 -4 -16 -11 3915.55 261.178 1 4 16 12 1955.25 169.959 5 5 -12 -5 1007.74 164.837 1 5 -12 -4 714.596 152.492 1 5 -12 -3 3261.35 287.175 1 5 -12 -2 346.450 137.196 1 5 -12 -2 128.758 88.4071 9 5 -12 -1-131.794 98.5963 9 5 -12 -1-26.3083 128.694 1 5 -12 0 6945.47 376.965 1 5 -12 0 6653.36 289.610 9 5 -12 1 141.365 77.7228 1 -5 11 9 2864.69 227.077 4 -5 11 8 33.6616 85.9686 4 -5 11 7 1998.18 222.776 4 -5 11 6 1959.88 220.524 4 5 -11 -5 1361.30 224.451 1 5 -11 -4 663.476 203.381 1 5 -11 -3 4359.48 373.099 1 5 -11 -2-0.95179 159.307 1 5 -11 -1 21429.5 797.800 1 5 -11 0 14949.5 663.144 1 5 -11 1 1182.72 224.852 1 5 -11 1 1100.36 178.165 9 5 -11 2 213.092 149.563 1 5 -11 2 412.072 137.827 9 5 -11 3-141.719 101.070 1 5 -11 3 74.1374 109.105 9 5 -11 4-31.9250 75.5853 9 -5 10 10 2556.37 243.040 4 -5 10 9 5618.60 382.173 4 -5 10 8 317.611 155.610 4 -5 10 7 2106.26 273.360 4 -5 10 6 366.057 171.208 4 5 -10 -5 11048.1 577.417 1 -5 10 5 10768.9 566.149 4 5 -10 -4 4630.29 408.860 1 5 -10 -3 10027.3 597.905 1 5 -10 -2 5280.46 454.507 1 5 -10 -1 11491.7 658.152 1 5 -10 0 7667.07 546.232 1 5 -10 1 564.697 209.156 1 5 -10 2 2111.27 299.684 1 5 -10 3 326.491 203.983 1 5 -10 3 387.425 160.547 9 5 -10 4 1084.54 203.036 1 5 -10 4 1097.12 190.180 9 5 -10 5 155.097 104.118 9 5 -10 6 28.5114 77.8771 9 -5 9 11 87.4346 94.3875 4 -5 9 10 246.821 153.322 4 -5 9 9 1970.24 281.970 4 -5 9 8 963.028 221.571 5 -5 9 7 256.088 192.020 5 -5 9 6 541.962 186.138 5 -5 9 5-11.4844 162.921 4 -5 9 5 144.602 154.516 5 5 -9 -5 81.5033 136.206 1 -5 9 4-27.9741 121.343 4 -5 9 4 330.354 148.170 5 5 -9 -4 105.104 193.614 1 5 -9 -3 338.452 171.719 1 5 -9 -2-134.034 190.400 1 5 -9 -1 64.6261 152.678 1 5 -9 0 7231.74 577.400 1 5 -9 1 10373.6 656.571 1 5 -9 2 9173.11 617.192 1 5 -9 3 3124.97 363.404 1 5 -9 4 1674.99 271.979 1 5 -9 4 1551.83 256.429 9 5 -9 5 2678.15 269.770 1 5 -9 5 2677.59 288.857 9 5 -9 6 2057.06 239.896 9 5 -9 7 638.860 144.194 9 -5 8 12 5415.11 280.113 4 -5 8 11-155.088 140.278 4 -5 8 11-91.0300 127.071 15 -5 8 10 9503.39 467.465 15 -5 8 10 9314.46 520.855 4 -5 8 9 4725.29 423.250 5 -5 8 8 4462.87 422.010 5 -5 8 7-41.8813 138.741 5 -5 8 6 269.175 205.498 5 -5 8 5 17095.7 804.977 5 -5 8 4 457.373 218.871 5 5 -8 -4 681.469 191.740 1 -5 8 3 292.625 173.800 4 -5 8 3 587.631 210.750 5 5 -8 -3 586.203 190.572 1 5 -8 -2 9867.36 653.811 1 5 -8 -1 2430.36 360.962 1 5 -8 0 131.562 243.483 1 5 -8 1 12339.9 747.518 1 5 -8 2 5503.32 516.123 1 5 -8 3 1272.92 284.008 1 5 -8 4 501.649 200.235 1 5 -8 5 123.745 173.000 9 5 -8 5 369.024 188.964 1 5 -8 6 10.3118 127.426 1 5 -8 6-4.42221 150.212 9 5 -8 7 4263.81 334.743 9 5 -8 8-11.2618 122.544 9 5 -8 9-41.5228 76.8007 9 -5 7 12 648.763 140.716 4 -5 7 12 655.580 139.687 15 -5 7 11 6435.91 396.783 15 -5 7 11 5840.11 389.678 4 -5 7 10 1760.95 251.424 15 -5 7 10 1517.88 256.559 4 -5 7 9 2472.19 297.168 15 -5 7 9 2017.59 298.773 5 -5 7 8 240.342 153.061 5 -5 7 7 8023.92 591.155 5 -5 7 6 6863.44 534.296 5 -5 7 5 8362.64 593.667 5 -5 7 4 8612.51 595.395 5 5 -7 -4 7561.06 544.039 1 -5 7 3-142.262 133.374 5 5 -7 -3 174.244 179.139 1 5 -7 -2 8463.32 594.718 1 -5 7 2 9253.94 603.634 4 5 -7 -1 10341.4 667.481 1 5 -7 0 6406.10 524.263 1 5 -7 1 15224.1 820.891 1 5 -7 2 4070.24 438.473 1 5 -7 3 570.619 227.380 1 5 -7 4 1401.44 270.239 1 5 -7 5 10502.1 642.611 1 5 -7 6-86.3727 126.456 1 5 -7 6 108.878 143.673 9 5 -7 7 1815.67 279.337 9 5 -7 8 1281.50 177.017 12 5 -7 8 1353.97 235.374 9 5 -7 9 969.144 177.350 9 5 -7 10-82.8479 88.1218 9 5 -7 10-103.483 91.6334 2 -5 6 12 1870.25 217.643 15 -5 6 12 1741.24 190.067 4 -5 6 11 2743.90 313.729 15 -5 6 11 2368.44 277.870 4 -5 6 10 2092.95 290.441 15 -5 6 10 2284.50 305.541 4 -5 6 9 1008.92 205.141 15 -5 6 9 372.413 210.320 5 -5 6 8 2630.25 354.608 15 -5 6 8 2382.47 361.553 5 -5 6 7 48.1815 201.518 5 -5 6 6 12609.5 728.485 5 -5 6 5 987.616 261.382 5 -5 6 4 40976.0 1255.09 5 -5 6 3 11286.5 652.027 5 5 -6 -3 9541.18 616.296 1 5 -6 -3 10884.1 799.621 18 -5 6 2 10297.8 607.826 5 5 -6 -2 11667.5 670.068 1 5 -6 -2 9909.39 801.157 18 5 -6 -1 23512.5 971.227 1 5 -6 -1 20664.1 1132.10 18 -5 6 1 21913.8 877.845 4 5 -6 0-330.407 172.924 18 5 -6 0 261.436 136.351 1 5 -6 1-447.717 232.107 18 5 -6 1 195.967 208.757 1 5 -6 2 38456.9 1266.45 1 5 -6 3 2855.98 371.361 1 5 -6 4 2799.36 385.533 1 5 -6 5 4291.95 430.087 1 5 -6 6-35.0765 181.881 1 5 -6 7 12092.6 628.333 9 5 -6 8 1799.32 241.274 12 5 -6 8 1504.30 258.647 9 5 -6 9 380.006 151.537 12 5 -6 9 1075.27 208.510 9 5 -6 10 4787.11 319.100 9 5 -6 11 4647.94 309.948 2 -5 5 13 329.156 118.810 15 -5 5 12 713.169 198.659 15 -5 5 11 467.324 162.825 4 -5 5 11 507.167 190.931 15 -5 5 10 4815.29 423.839 15 -5 5 10 5293.57 444.931 4 -5 5 9 248.818 165.066 15 -5 5 8 15547.7 771.848 15 -5 5 8 14668.8 783.687 5 -5 5 7 10645.4 636.165 15 -5 5 7 9650.98 648.102 5 -5 5 6 16790.1 846.156 5 -5 5 5 1143.67 302.266 5 -5 5 5 1218.16 337.878 19 -5 5 4 1988.65 314.104 5 -5 5 4 2078.36 364.667 19 5 -5 -4 1970.04 323.607 18 -5 5 3 13766.2 704.055 5 -5 5 3 11898.9 852.868 19 5 -5 -3 12219.0 826.136 18 5 -5 -2 5184.38 558.015 18 5 -5 -1 3374.71 475.112 18 5 -5 0 1679.63 344.209 18 5 -5 1-7.41701 151.054 1 5 -5 1 233.447 192.634 18 5 -5 2 3640.27 404.035 1 5 -5 2 3442.95 498.029 18 5 -5 3 12152.7 699.347 1 5 -5 3 10820.2 872.880 18 5 -5 4 6282.65 527.921 1 5 -5 5 5898.14 500.574 1 5 -5 6 4784.39 442.304 1 5 -5 7 16284.3 776.437 1 5 -5 7 17299.5 756.197 9 5 -5 8 1835.68 252.814 9 5 -5 9 2774.72 296.387 12 5 -5 9 3383.31 329.174 9 5 -5 10 184.592 114.154 12 5 -5 10 216.227 155.042 9 5 -5 11 2756.26 241.663 9 5 -5 12 2612.90 233.373 2 -5 4 13 4002.38 286.061 15 -5 4 12 1569.13 238.751 15 -5 4 11 6133.08 474.794 15 -5 4 10 14731.6 751.434 15 -5 4 10 13776.5 677.033 4 -5 4 9 1072.08 222.921 6 -5 4 9 1572.97 293.345 15 -5 4 8 864.538 194.049 6 -5 4 8 1000.16 252.587 15 -5 4 8 750.250 250.686 5 -5 4 7 21105.6 899.372 15 -5 4 7 21022.7 940.770 5 -5 4 6 890.492 280.487 5 -5 4 5 550.489 240.405 5 -5 4 5 1531.88 350.559 19 -5 4 4 37604.1 1165.62 5 -5 4 4 34917.6 1473.37 19 5 -4 -4 34159.6 1339.63 17 -5 4 3-514.260 226.434 19 5 -4 -3 137.210 164.889 17 -5 4 2 620.845 228.353 19 5 -4 -2 804.278 248.417 17 5 -4 -1 6694.30 602.370 17 5 -4 0 8117.92 675.100 18 5 -4 0 8723.25 689.755 17 5 -4 1 668.768 244.144 18 5 -4 1 78.5582 178.732 17 5 -4 2 15710.1 952.761 18 5 -4 3 387.520 234.762 18 5 -4 4 7907.82 556.352 1 5 -4 4 8313.33 735.855 18 5 -4 5 7266.04 526.016 1 5 -4 5 6679.90 659.433 13 5 -4 6-72.7791 155.183 1 5 -4 7 228.304 152.360 1 5 -4 8 15345.7 698.981 9 5 -4 9 1243.54 235.926 9 5 -4 9 1014.73 216.683 12 5 -4 10 330.129 160.635 12 5 -4 10 443.985 172.399 9 5 -4 11 2476.31 242.854 12 5 -4 11 2520.70 252.948 9 5 -4 12 1436.93 230.223 2 5 -4 13-78.8665 111.381 2 -5 3 13 5193.21 321.900 15 -5 3 12 809.648 209.236 15 -5 3 11 381.390 227.782 15 -5 3 10 2084.78 255.798 6 -5 3 10 2009.71 324.139 15 -5 3 9 1351.80 243.569 6 -5 3 9 1578.73 317.507 15 -5 3 9 1566.79 269.788 4 -5 3 8 13507.7 666.533 6 -5 3 8 11967.0 714.832 15 -5 3 7 28867.8 1070.42 15 -5 3 7 27919.5 1068.10 5 -5 3 6 1904.37 289.118 15 -5 3 6 1534.17 276.583 5 -5 3 6 1829.22 431.133 19 -5 3 5 1048.05 265.095 5 5 -3 -5 1567.27 293.412 17 5 -3 -4 2677.32 375.396 17 -5 3 4 2370.29 468.156 19 -5 3 3 24483.7 1109.77 19 5 -3 -3 26019.1 1115.13 17 -5 3 2 5496.58 503.890 19 5 -3 -2 6028.14 561.393 17 5 -3 -1 13678.5 802.963 17 5 -3 0 1989.75 353.365 17 5 -3 1 534.458 184.646 17 5 -3 2 40185.4 1424.86 18 5 -3 2 42953.0 1403.19 17 5 -3 3 13892.4 852.824 18 5 -3 3 15144.7 837.521 17 5 -3 4 18228.6 986.858 18 5 -3 5 10853.7 796.295 18 5 -3 6 3099.57 362.843 1 5 -3 6 2469.17 375.897 13 5 -3 7 3642.88 383.628 1 5 -3 8 1912.80 257.676 9 5 -3 9 3802.43 386.467 12 5 -3 9 3479.18 334.496 9 5 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5062.38 429.655 1 5 -2 7 6435.55 624.064 13 5 -2 8 9567.63 535.830 9 5 -2 9-55.1593 97.2633 9 5 -2 9 137.955 177.863 12 5 -2 10 4577.75 414.024 12 5 -2 11 2001.49 273.711 12 5 -2 11 2088.79 263.346 10 5 -2 12 2972.66 293.231 12 5 -2 12 2258.70 264.933 10 5 -2 13 1698.54 255.711 2 5 -2 13 1584.25 208.631 12 5 -2 13 1666.93 202.332 10 5 -2 14 57.2380 123.608 2 -5 1 13 759.581 153.078 15 -5 1 12 2058.13 273.624 15 -5 1 11 5417.49 458.848 15 -5 1 10 2027.37 286.484 6 -5 1 10 1795.40 305.395 15 -5 1 9 3257.39 348.533 6 -5 1 9 3302.07 385.555 15 -5 1 8 9571.70 596.383 6 -5 1 8 8768.59 641.544 15 -5 1 7 25225.0 929.439 6 -5 1 7 23378.2 991.847 15 -5 1 6 1101.64 266.621 15 -5 1 6 1674.97 311.822 4 -5 1 6 1778.15 374.424 14 -5 1 5 1178.03 309.460 14 -5 1 4 3940.53 491.841 19 -5 1 4 4424.46 511.944 14 5 -1 -4 5165.93 482.667 17 5 -1 -3 601.309 229.719 17 -5 1 3 86.5802 226.044 19 -5 1 2 10058.7 632.825 19 5 -1 -2 10644.9 673.050 17 5 -1 -1 8742.98 608.180 17 5 -1 0 4904.30 463.064 17 5 -1 1 9064.86 595.117 17 5 -1 2 23695.2 953.737 17 5 -1 3 18365.9 725.447 21 5 -1 3 17224.8 812.884 17 5 -1 4 1666.20 271.858 21 5 -1 4 1356.25 245.389 17 5 -1 5 10839.8 677.571 21 5 -1 5 10952.7 703.178 18 5 -1 5 10657.2 645.419 17 5 -1 6 4365.00 443.825 18 5 -1 7 8690.89 670.347 13 5 -1 8 1255.85 279.363 1 5 -1 8 1469.22 314.455 13 5 -1 9 2281.40 305.149 12 5 -1 10 1364.29 270.653 12 5 -1 11 67.8310 143.482 12 5 -1 12 4125.26 356.013 12 5 -1 12 4214.15 362.064 10 5 -1 13 998.573 229.143 2 5 -1 13 974.635 185.880 12 5 -1 13 1233.65 217.741 10 5 -1 14 603.455 144.478 12 5 -1 14 488.875 141.803 10 5 -1 14 191.588 153.038 2 -5 0 13 1727.57 177.453 15 -5 0 12 132.275 150.675 15 -5 0 11 434.024 208.224 15 -5 0 11 241.383 128.003 7 -5 0 10 879.449 227.598 6 -5 0 10 783.533 235.506 15 -5 0 10 495.932 147.786 7 -5 0 9 8568.68 553.325 6 -5 0 9 7796.17 599.384 15 -5 0 9 8714.54 497.675 7 -5 0 8 20775.2 858.429 6 -5 0 8 19401.0 921.468 15 -5 0 8 19144.0 732.592 7 -5 0 7 1688.93 287.466 6 -5 0 7 1155.20 239.459 15 -5 0 6 435.771 199.113 6 -5 0 6-64.4197 135.944 15 -5 0 6-152.489 311.378 14 -5 0 5 885.631 240.336 14 -5 0 4 4581.54 548.669 14 5 0 -4 5214.34 478.792 17 -5 0 3 56.2581 148.534 14 5 0 -3 29.2215 113.997 17 -5 0 2 3839.93 445.238 14 5 0 -2 3601.63 388.848 17 -5 0 1 9210.67 589.429 14 5 0 -1 9006.41 593.200 17 5 0 0 890.853 232.165 17 5 0 1 4071.02 408.858 17 5 0 2 1450.91 222.821 21 5 0 2 1069.84 243.868 17 5 0 3 30745.4 936.697 21 5 0 3 31144.6 1046.51 17 5 0 4 6035.16 460.433 21 5 0 4 6192.51 478.418 17 5 0 5 26522.0 1007.95 21 5 0 5 26451.5 952.712 17 5 0 6 8264.90 605.008 21 5 0 6 7884.60 578.342 18 5 0 7 23409.0 1086.12 21 5 0 8 39171.9 1490.82 13 5 0 9 187.792 167.018 12 5 0 10 8540.65 532.452 12 5 0 11 2353.76 306.113 12 5 0 12 38.7803 125.424 12 5 0 13 3087.62 303.693 12 5 0 13 2941.21 338.397 2 5 0 13 3791.68 346.187 10 5 0 14 1474.33 200.816 12 5 0 14 1361.52 211.397 10 5 0 14 1046.35 210.637 2 5 0 15 389.799 101.725 12 5 0 15 295.656 120.251 2 5 0 15 369.673 123.397 10 -5 -1 12 6669.87 388.212 15 -5 -1 11 8700.70 526.692 15 -5 -1 11 7728.04 392.473 7 -5 -1 10 11896.7 679.246 15 -5 -1 10 11549.1 540.910 7 -5 -1 9 3687.98 380.294 6 -5 -1 9 3122.28 390.404 15 -5 -1 9 2886.10 320.564 7 -5 -1 8 17570.1 798.193 6 -5 -1 8 18459.1 900.054 15 -5 -1 8 17824.3 738.710 7 -5 -1 7 7515.63 534.040 6 -5 -1 7 6829.24 574.179 15 -5 -1 6 20.1935 134.388 6 -5 -1 6 97.9931 209.107 14 -5 -1 5 815.941 251.119 14 -5 -1 4 9351.02 763.832 14 5 1 -4 9302.95 628.793 17 -5 -1 3 8057.03 664.078 14 5 1 -3 8107.15 600.485 17 -5 -1 2 16096.2 851.923 14 5 1 -2 15287.5 786.798 17 -5 -1 1 257.362 107.217 14 5 1 -1 22.5077 138.540 17 -5 -1 0 37354.4 1067.10 14 5 1 0 37707.7 1182.90 17 5 1 1 2240.73 325.636 17 5 1 2 56059.8 1394.33 17 5 1 3 359.355 171.190 21 5 1 3 139.109 185.621 17 5 1 4 38986.4 1129.86 21 5 1 4 39558.4 1148.18 17 5 1 5 115038. 1945.00 17 5 1 5 115435. 2077.93 21 5 1 6 23692.9 1010.94 21 5 1 6 24219.4 913.056 18 5 1 6 23705.2 876.670 17 5 1 7 16413.7 896.554 21 5 1 8 24029.4 1121.04 13 5 1 8 23213.6 1119.26 21 5 1 9 3897.36 496.373 13 5 1 9 2999.85 330.934 12 5 1 10 331.532 180.965 12 5 1 11 3115.98 359.379 12 5 1 12 11417.5 618.700 12 5 1 13 46.5109 133.956 2 5 1 13 100.173 155.273 12 5 1 14 6167.37 405.238 12 5 1 14 5921.64 416.747 2 5 1 14 5802.88 409.748 10 5 1 15 114.292 112.321 12 5 1 15 121.902 140.246 10 5 1 16 1427.12 164.629 10 -5 -2 12 1045.13 165.078 15 -5 -2 11 164.592 132.967 15 -5 -2 10 1732.46 307.826 15 -5 -2 10 1522.90 245.073 7 -5 -2 9 1894.80 280.985 7 -5 -2 9 1917.94 302.232 6 -5 -2 9 1975.55 325.543 15 -5 -2 8 482.852 175.578 7 -5 -2 8 418.072 208.734 6 -5 -2 8 635.016 225.070 15 -5 -2 7 14129.7 725.346 6 -5 -2 7 12398.9 738.598 15 -5 -2 6 5416.12 462.708 6 -5 -2 6 5633.47 502.752 15 -5 -2 5 50717.3 1289.45 6 -5 -2 5 51202.4 1359.44 15 -5 -2 5 47682.2 1833.87 14 -5 -2 4 26542.3 1291.44 14 5 2 -4 26487.5 1042.58 17 -5 -2 3 20066.4 1042.31 14 5 2 -3 20956.6 934.827 17 -5 -2 2 97566.7 2100.52 14 5 2 -2 97488.4 1968.09 17 -5 -2 1 13166.5 711.005 14 5 2 -1 13517.6 740.965 17 -5 -2 0 21937.4 821.926 14 5 2 0 20196.8 884.515 17 5 2 1 22164.2 914.997 17 5 2 2 2993.82 347.088 17 5 2 3 39298.7 1176.32 17 5 2 4 2229.74 310.313 17 5 2 5 1329.06 240.128 17 5 2 5 1057.01 231.021 21 5 2 6 656.098 187.796 21 5 2 6 1047.29 222.465 17 5 2 7 65711.1 1745.27 21 5 2 8 7360.54 638.248 21 5 2 9 9129.11 712.434 13 5 2 9 9661.92 550.306 12 5 2 9 8483.54 709.890 21 5 2 10 10037.4 573.202 12 5 2 10 10430.9 848.760 21 5 2 11 28989.0 976.693 12 5 2 12 2081.25 298.893 12 5 2 13 801.213 218.269 12 5 2 14 1958.88 276.220 12 5 2 14 1672.18 253.081 10 5 2 15 4155.54 320.952 12 5 2 15 4141.11 332.762 10 5 2 16 1810.13 197.985 10 -5 -3 12 385.754 105.783 15 -5 -3 11-179.098 172.575 15 -5 -3 10 8120.86 518.097 15 -5 -3 10 8587.51 462.196 7 -5 -3 9 982.257 238.881 7 -5 -3 9 926.398 255.777 15 -5 -3 8 175.740 166.403 7 -5 -3 8-101.117 195.756 6 -5 -3 8-1.33688 192.437 15 -5 -3 7 3652.79 421.200 6 -5 -3 7 3661.83 439.049 15 -5 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19314.4 842.371 4 6 -5 1 171.238 169.357 1 6 -5 2 22027.8 977.757 1 6 -5 3 1596.37 283.469 1 6 -5 4-297.774 219.888 1 6 -5 5 23468.6 989.597 1 6 -5 6 1533.82 283.814 1 6 -5 7 16961.3 776.312 1 6 -5 7 15323.5 684.605 9 6 -5 8 1874.11 287.999 1 6 -5 8 1764.69 256.901 9 6 -5 9 2854.29 284.042 12 6 -5 9 3296.95 300.734 9 6 -5 10-201.070 118.657 12 6 -5 10 242.773 124.570 9 -6 4 11 924.650 174.088 15 -6 4 10 4639.40 366.538 15 -6 4 10 4085.63 319.681 4 -6 4 9 5484.52 373.519 6 -6 4 9 5600.79 437.935 4 -6 4 8 6165.42 427.073 6 -6 4 8 6718.61 474.242 15 -6 4 8 6621.55 507.658 4 -6 4 7 3857.62 438.148 4 -6 4 6 425.942 253.836 4 -6 4 5 20445.8 948.177 4 -6 4 4 18157.7 898.157 4 -6 4 3 1063.47 289.126 4 6 -4 -2 11763.9 666.413 1 -6 4 2 12317.0 715.439 4 6 -4 -1 17250.5 818.316 1 -6 4 1 17638.3 836.671 4 6 -4 -1 18410.3 1079.52 17 6 -4 0 31623.9 1110.20 1 -6 4 0 30076.9 1044.16 4 6 -4 0 29118.1 1367.17 18 6 -4 0 30356.9 1368.61 17 6 -4 1 22509.0 952.773 1 -6 4 -1 22252.7 883.763 4 6 -4 1 23221.8 1220.59 18 6 -4 2 2408.31 341.216 1 6 -4 2 2841.52 450.708 18 6 -4 3 9730.31 646.805 1 6 -4 4 2521.09 379.282 1 6 -4 5 3440.35 397.654 1 6 -4 6 1163.66 254.883 1 6 -4 7 9067.64 618.104 1 6 -4 8 152.255 140.659 1 6 -4 8 85.5511 171.413 9 6 -4 9 11477.7 581.343 12 6 -4 9 10926.2 530.020 9 6 -4 10 1600.90 235.680 12 6 -4 10 1687.13 214.881 9 6 -4 11 750.483 152.636 12 6 -4 12 64.5058 109.562 2 -6 3 11 872.842 173.107 15 -6 3 10 42.5583 104.266 6 -6 3 10 129.839 175.147 15 -6 3 9 2751.71 289.924 6 -6 3 9 2716.45 328.952 15 -6 3 9 2407.72 285.079 4 -6 3 8 330.212 159.574 6 -6 3 8 464.595 196.536 4 -6 3 8 745.400 206.755 15 -6 3 7 20891.0 823.586 6 -6 3 7 21697.2 883.740 15 -6 3 7 20141.6 917.232 4 -6 3 6 15933.6 835.878 4 -6 3 5 4512.18 470.806 4 -6 3 4 51907.9 1462.17 4 -6 3 3 1246.56 233.162 4 6 -3 -3 839.874 216.558 17 -6 3 2-99.8598 165.875 4 6 -3 -2-238.156 211.594 17 -6 3 1 318.647 138.450 4 6 -3 -1 397.579 189.266 17 -6 3 0 908.429 186.146 4 6 -3 0 1392.38 377.004 17 6 -3 1 967.313 220.787 1 6 -3 1 1679.25 375.399 17 6 -3 2 161.712 107.505 1 6 -3 2 740.806 255.693 18 6 -3 2 646.929 236.252 17 6 -3 3 16915.4 828.522 1 6 -3 3 17047.3 1046.51 18 6 -3 3 18285.9 1017.00 17 6 -3 4 65884.7 1619.29 1 6 -3 4 64076.8 1987.43 18 6 -3 5 14459.2 783.685 1 6 -3 6 2339.63 365.591 1 6 -3 7 9596.11 627.511 1 6 -3 8 6661.92 508.963 1 6 -3 8 7661.54 487.383 9 6 -3 9 1574.81 265.291 12 6 -3 9 1682.24 245.464 9 6 -3 10 3116.26 325.003 12 6 -3 10 3510.64 308.800 9 6 -3 11 3319.80 302.021 12 6 -3 12 1309.95 175.164 12 6 -3 13 1263.96 165.003 2 -6 2 12 338.068 105.309 15 -6 2 11 134.039 142.408 15 -6 2 10 1607.29 223.402 6 -6 2 10 1139.61 240.024 15 -6 2 9-169.190 153.564 6 -6 2 9 80.8587 205.257 15 -6 2 8 22.6878 138.282 6 -6 2 8-67.6722 151.220 4 -6 2 8-52.2015 185.654 15 -6 2 7 414.386 196.390 6 -6 2 7 813.220 230.010 4 -6 2 7 496.200 203.629 15 -6 2 6 721.139 222.897 4 -6 2 5 14528.7 765.838 4 -6 2 4 64.5146 183.224 4 6 -2 -4 644.523 224.514 17 -6 2 3 38739.7 1218.95 4 6 -2 -3 37990.3 1437.35 17 -6 2 2 461.663 173.248 4 6 -2 -2 1297.96 300.459 17 6 -2 -1 1325.88 270.422 17 6 -2 0 154.547 155.648 17 6 -2 1 1255.39 281.012 17 6 -2 2 465.716 164.343 17 6 -2 3 2715.82 419.614 18 6 -2 3 3189.86 401.564 17 6 -2 4 5621.44 478.006 1 6 -2 4 6168.14 630.538 18 6 -2 4 6396.84 593.409 17 6 -2 5-240.123 185.410 1 6 -2 5 516.732 280.177 18 6 -2 6 7957.79 577.864 1 6 -2 6 9979.49 765.036 18 6 -2 7 306.008 198.290 1 6 -2 8 22178.9 921.402 1 6 -2 8 22827.7 795.197 9 6 -2 9 7016.77 509.361 1 6 -2 9 7014.49 504.032 12 6 -2 10 638.729 222.184 12 6 -2 11 1159.86 223.385 12 6 -2 11 1007.31 205.030 10 6 -2 12 146.889 128.174 12 6 -2 12 127.011 91.0210 10 6 -2 13 1439.75 209.589 2 6 -2 13 1735.22 186.287 12 -6 1 12 999.425 150.202 15 -6 1 11 665.159 183.416 15 -6 1 10 1687.39 235.507 6 -6 1 10 1594.24 270.252 15 -6 1 9 16630.3 699.334 6 -6 1 9 17364.6 785.732 15 -6 1 8 7967.94 531.902 6 -6 1 8 8424.92 584.819 15 -6 1 7 926.084 228.360 6 -6 1 7 710.571 229.871 4 -6 1 7 559.288 208.592 15 -6 1 6 5217.02 472.790 15 -6 1 6 5011.68 459.806 4 -6 1 5 252.198 177.106 4 -6 1 4-112.248 138.679 4 6 -1 -4 322.456 174.824 17 -6 1 3 918.878 241.604 4 6 -1 -3 1434.45 305.901 17 6 -1 -2 24062.9 1105.80 17 6 -1 -1-105.612 84.1221 17 6 -1 0 8203.15 637.307 17 6 -1 1 4289.99 490.246 17 6 -1 2 11595.3 755.537 17 6 -1 3 3861.12 474.274 17 6 -1 4 2615.54 375.940 17 6 -1 5 20616.4 1042.01 18 6 -1 5 21448.6 1015.90 17 6 -1 6 968.181 223.418 1 6 -1 6 1572.82 301.828 18 6 -1 7 3481.77 399.901 1 6 -1 8 7487.86 554.550 1 6 -1 9 18882.8 824.879 1 6 -1 9 18889.8 811.220 12 6 -1 10 23940.6 891.888 12 6 -1 11 4337.55 391.062 12 6 -1 12 63.3894 138.253 12 6 -1 12 135.789 127.143 10 6 -1 13 38.6569 172.060 2 6 -1 13 99.1537 122.801 12 6 -1 13 218.296 116.506 10 6 -1 14 1861.51 177.657 12 6 -1 14 1741.86 193.580 2 6 -1 14 1585.98 160.311 10 -6 0 11 350.804 164.855 15 -6 0 10 6041.89 444.615 15 -6 0 9 6882.33 471.630 6 -6 0 9 7548.19 543.978 15 -6 0 9 7335.09 415.389 7 -6 0 8 292.215 148.955 7 -6 0 8 450.701 190.198 6 -6 0 8 204.942 124.533 15 -6 0 7 1389.75 273.313 6 -6 0 7 1261.58 265.810 15 -6 0 6 16557.5 777.675 6 -6 0 6 16093.6 800.918 15 -6 0 5 10514.9 627.048 15 -6 0 5 10009.3 601.624 4 -6 0 4 3662.91 496.149 14 -6 0 4 3951.16 384.950 4 6 0 -4 3895.11 432.937 17 -6 0 3 4057.83 490.470 14 -6 0 3 4166.39 417.780 4 6 0 -3 5071.07 501.404 17 6 0 -2 2578.92 374.481 17 6 0 -1 3661.58 448.932 17 6 0 0 1380.13 278.640 17 6 0 1 2376.73 370.489 17 6 0 2 1494.74 289.665 17 6 0 3 24179.1 1053.21 17 6 0 4 957.052 270.128 17 6 0 5 1742.71 287.524 21 6 0 5 2245.09 310.691 17 6 0 6 4124.58 439.349 21 6 0 6 4475.75 473.823 18 6 0 7 5226.57 449.283 1 6 0 8 1981.85 299.874 1 6 0 9 179.927 191.582 12 6 0 9 495.120 194.815 1 6 0 10 5065.37 435.041 12 6 0 11 24147.7 890.038 12 6 0 12 45.2156 139.600 12 6 0 13 723.999 187.125 12 6 0 13 1008.12 203.925 10 6 0 14 310.174 131.142 12 6 0 14 129.249 101.731 10 6 0 14 286.252 135.973 2 6 0 15 560.219 100.855 10 -6 -1 11 26.3910 106.985 15 -6 -1 10 518.737 199.589 15 -6 -1 10 674.785 145.347 7 -6 -1 9 3630.78 357.696 6 -6 -1 9 4296.70 411.707 15 -6 -1 9 3472.85 303.345 7 -6 -1 8 3130.04 366.689 6 -6 -1 8 2536.70 352.135 15 -6 -1 8 2928.72 310.804 7 -6 -1 7-21.0281 191.974 6 -6 -1 7 123.609 140.020 15 -6 -1 6 6387.68 511.351 6 -6 -1 6 6694.29 541.537 15 -6 -1 5 1618.93 310.512 15 -6 -1 4 713.707 207.977 4 -6 -1 4 787.790 234.832 14 -6 -1 3-452.793 263.525 14 6 1 -3 255.788 120.499 17 6 1 -2 3535.33 426.243 17 -6 -1 2 3821.01 472.420 14 6 1 -1 9370.71 669.661 17 6 1 0 738.442 200.637 17 6 1 1 2130.66 377.917 17 6 1 2 310.813 183.703 17 6 1 3 44053.3 1216.65 21 6 1 3 42623.2 1381.88 17 6 1 4 6476.55 509.118 21 6 1 4 6058.13 533.189 17 6 1 5 24272.9 1033.80 21 6 1 5 23635.8 1018.36 17 6 1 6 37062.2 1330.79 21 6 1 7 566.513 176.384 1 6 1 7 360.069 207.403 21 6 1 8 4782.62 442.631 1 6 1 8 4516.27 533.542 21 6 1 9 3942.25 374.762 12 6 1 10-48.5998 147.046 12 6 1 11 7371.44 518.332 12 6 1 12 4694.36 404.373 12 6 1 13 738.201 205.862 12 6 1 14 478.363 176.681 12 6 1 14 296.094 133.215 10 6 1 15 5450.52 300.935 12 6 1 15 5753.17 313.404 10 -6 -2 11-100.209 111.289 15 -6 -2 10 15.8965 156.129 15 -6 -2 10 117.599 108.129 7 -6 -2 9-74.3204 127.566 7 -6 -2 9 67.3763 188.919 15 -6 -2 8-142.142 160.232 7 -6 -2 8 91.4743 169.685 6 -6 -2 8-137.739 161.121 15 -6 -2 7 8081.88 560.532 6 -6 -2 7 6966.44 549.770 15 -6 -2 6 341.814 168.811 6 -6 -2 6 214.935 181.652 15 -6 -2 5 7504.20 534.840 6 -6 -2 5 7174.11 537.096 15 -6 -2 4 4174.25 409.452 15 -6 -2 4 2946.22 502.573 14 -6 -2 3 5818.94 628.785 14 6 2 -3 5340.67 527.318 17 -6 -2 2-249.256 165.238 14 6 2 -2-253.479 156.862 17 6 2 -1 326.583 127.140 17 6 2 0 1462.89 277.611 17 6 2 1 57.6140 133.939 17 6 2 2 9445.80 666.602 17 6 2 3 16033.7 853.293 17 6 2 4 2965.61 355.362 21 6 2 4 3543.39 411.427 17 6 2 5 394.797 189.037 21 6 2 5 246.583 184.996 17 6 2 6 14988.6 848.048 21 6 2 6 14670.3 794.604 17 6 2 7 1010.57 297.750 21 6 2 8 1913.14 263.745 12 6 2 8 2619.09 437.895 21 6 2 9 318.505 167.321 12 6 2 9-891.389 275.126 21 6 2 10 1795.22 288.087 12 6 2 11 776.784 214.762 12 6 2 12 1020.25 237.049 12 6 2 13-166.271 156.078 12 6 2 14 1813.16 258.034 12 6 2 14 1552.43 229.665 10 6 2 15 220.235 119.534 12 6 2 15 222.757 128.828 10 6 2 16 3364.36 215.721 10 -6 -3 11 11825.5 410.473 15 -6 -3 10-123.659 151.939 15 -6 -3 10 104.148 113.092 7 -6 -3 9 2347.23 311.164 15 -6 -3 9 2414.60 266.134 7 -6 -3 8 3086.99 353.659 6 -6 -3 8 3410.89 387.600 15 -6 -3 8 3435.48 327.835 7 -6 -3 7 1373.41 251.267 7 -6 -3 7 1580.17 300.580 6 -6 -3 7 1788.91 303.557 15 -6 -3 6 20383.6 869.438 6 -6 -3 6 19728.0 889.094 15 -6 -3 5 1664.63 287.451 6 -6 -3 5 2292.34 313.891 15 -6 -3 4 14136.7 713.804 6 -6 -3 4 14977.7 759.060 15 -6 -3 3 1791.53 275.708 15 -6 -3 3 1579.08 326.323 14 6 3 -3 1174.15 268.319 17 -6 -3 2 41526.3 1520.69 14 6 3 -2 39955.9 1438.05 17 6 3 -1 7686.23 614.512 17 6 3 0 13185.1 816.561 17 6 3 1 8622.88 663.606 17 6 3 2 12840.8 792.529 17 6 3 3 2546.94 382.811 17 6 3 4 5862.34 531.585 17 6 3 5 1643.88 311.223 21 6 3 5 1924.25 323.441 17 6 3 6 11401.7 758.062 21 6 3 6 11263.2 702.360 17 6 3 7 2268.11 341.978 21 6 3 8 5763.49 434.054 12 6 3 8 5738.28 614.422 21 6 3 9 2798.32 407.749 13 6 3 9 3205.10 339.032 12 -6 -3 -9 3471.33 337.967 4 6 3 9 2939.17 435.247 21 6 3 10 9762.83 578.900 12 6 3 11 2635.62 338.187 12 6 3 12 9596.32 576.511 12 6 3 13 284.958 163.288 12 6 3 14 2519.39 310.030 12 6 3 15-54.1322 125.832 12 6 3 15-14.3347 106.911 10 6 3 16 64.4830 110.036 12 6 3 16 285.325 119.276 10 -6 -4 10 3273.91 277.352 15 -6 -4 9 280.126 183.092 15 -6 -4 9 535.656 168.470 7 -6 -4 8 759.386 201.645 7 -6 -4 8 235.731 203.671 15 -6 -4 7 4375.55 422.896 6 -6 -4 7 3795.85 420.669 15 -6 -4 7 4102.15 381.836 7 -6 -4 6 22522.4 897.861 6 -6 -4 6 21393.2 924.546 15 -6 -4 5 5222.60 455.466 6 -6 -4 5 5754.64 497.047 15 -6 -4 4 1285.27 268.509 6 -6 -4 4 1399.07 264.798 15 -6 -4 3 5722.05 450.861 6 -6 -4 3 6109.24 479.433 15 6 4 -3 5370.25 565.272 17 -6 -4 3 6844.03 446.733 16 -6 -4 2 306.455 170.088 14 6 4 -2 90.7733 74.9211 17 6 4 -1 8073.70 672.801 17 6 4 0 21581.5 1068.64 17 6 4 1 29848.5 1238.20 17 6 4 2 1827.35 328.005 17 6 4 3 970.500 231.937 17 6 4 4 566.461 200.205 17 6 4 5 457.013 241.277 17 6 4 6 11.7135 99.0932 21 6 4 6 454.205 207.005 17 6 4 7 3483.63 437.064 21 6 4 8 3345.73 499.722 21 6 4 9 167.341 164.717 13 6 4 9 40.9043 104.423 12 -6 -4 -9-289.443 145.674 4 6 4 10 594.077 182.976 12 -6 -4 -10 838.754 205.171 4 6 4 11 1687.66 268.801 12 -6 -4 -11 1351.42 250.985 4 6 4 12 2426.23 320.932 12 6 4 13 1258.76 232.954 12 6 4 14 731.972 212.513 12 6 4 15-40.8062 134.156 12 6 4 15-130.657 143.599 10 6 4 16 2886.33 232.663 12 6 4 16 2922.58 243.680 10 -6 -5 10 467.838 115.424 15 -6 -5 9 46.4937 161.611 15 -6 -5 9 74.3192 133.579 7 -6 -5 8 255.838 168.134 7 -6 -5 8-43.0669 185.902 15 -6 -5 7-253.947 186.526 7 -6 -5 7 45.5891 182.170 15 -6 -5 6 15017.8 717.516 6 -6 -5 6 15751.0 779.192 15 -6 -5 6 15557.6 715.756 7 -6 -5 5 5728.84 482.233 6 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158.735 12 -6 -6 -10 242.209 159.599 4 6 6 11 196.030 150.583 12 -6 -6 -11 119.079 142.493 4 6 6 12 2989.75 336.905 12 6 6 12 2787.89 335.120 11 -6 -6 -12 3157.22 354.770 4 6 6 13 3288.94 349.799 12 -6 -6 -13 3698.27 365.234 4 6 6 13 3339.67 344.111 11 6 6 14 6469.06 446.006 12 6 6 14 6347.23 432.804 11 6 6 15 187.833 148.585 12 6 6 15 222.576 132.678 11 6 6 16 124.621 107.657 11 6 6 16 176.036 121.398 10 -6 -7 8 334.729 130.948 15 -6 -7 8 459.402 131.277 7 -6 -7 7-75.6560 177.452 15 -6 -7 7 133.168 160.082 7 -6 -7 6 2993.05 361.525 15 -6 -7 6 3252.90 333.435 7 -6 -7 5 623.776 206.455 7 -6 -7 5 154.528 210.321 15 -6 -7 4 22075.3 917.620 15 -6 -7 4 22162.9 796.838 16 -6 -7 3 1394.72 234.527 16 -6 -7 3 1161.56 218.093 6 -6 -7 3 1348.96 293.710 15 -6 -7 2-170.450 135.365 16 -6 -7 2-48.8075 182.623 15 -6 -7 1 13625.7 706.716 15 -6 -7 1 13470.9 663.223 16 -6 -7 0 9418.10 561.267 15 6 7 0 9042.21 772.472 17 -6 -7 0 9107.53 544.469 16 -6 -7 -1 913.081 227.001 16 -6 -7 -1 911.786 223.634 15 6 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110.679 10 -6 -9 6 7485.18 358.536 7 -6 -9 5 133.215 133.886 7 -6 -9 4 1723.47 245.434 7 -6 -9 4 1905.67 251.574 16 -6 -9 4 2513.77 347.273 15 -6 -9 3 554.790 205.991 7 -6 -9 3 822.196 197.421 16 -6 -9 3 409.932 215.043 15 -6 -9 2 249.508 178.479 16 -6 -9 2 9.12884 205.748 15 -6 -9 1 9648.60 601.910 15 -6 -9 1 10087.8 587.997 16 -6 -9 0 1754.45 269.633 16 -6 -9 -1 52.8508 171.506 16 -6 -9 -2 20584.7 815.041 16 -6 -9 -3 15527.1 702.408 16 -6 -9 -4 8144.97 512.658 16 -6 -9 -5 11700.3 606.091 4 6 9 5 13730.1 1009.44 17 -6 -9 -5 12138.0 593.999 16 -6 -9 -6 1479.86 231.287 16 6 9 6 1270.58 394.094 17 -6 -9 -6 1305.64 247.248 4 6 9 7 254.317 238.975 17 -6 -9 -7 918.710 232.495 4 -6 -9 -8 6294.99 493.449 4 -6 -9 -9 20188.5 865.836 4 6 9 10 7546.26 513.485 5 -6 -9 -10 7854.08 565.415 4 6 9 11 478.683 172.849 5 -6 -9 -11 487.869 229.462 4 6 9 12 5594.58 407.212 5 -6 -9 -12 4778.06 444.407 4 6 9 13 178.602 152.251 11 6 9 14 7264.95 477.213 11 6 9 15 10.1813 142.918 11 6 9 16 1559.65 200.778 11 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4 -7 6 1 2156.56 304.135 4 7 -6 -1 1763.97 311.118 1 -7 6 0-87.4350 120.092 4 7 -6 0 167.765 186.097 1 7 -6 1 3860.30 433.726 1 7 -6 2 17.2180 214.147 1 7 -6 3 1204.88 298.881 1 7 -6 4 1534.28 295.166 1 7 -6 5 722.994 224.225 1 7 -6 6 400.572 185.477 1 7 -6 6 389.785 179.649 9 7 -6 7 2038.28 257.228 1 7 -6 7 1866.34 228.598 12 7 -6 7 2012.86 232.533 9 7 -6 8 8696.74 388.009 12 7 -6 8 9026.46 371.909 9 -7 5 9 3306.66 269.490 4 -7 5 8 641.449 180.672 4 -7 5 7 2515.57 261.141 6 -7 5 7 2484.38 321.685 4 -7 5 6 526.057 231.209 4 -7 5 5 83.5657 153.136 4 -7 5 4 194.455 204.320 4 -7 5 3 3382.17 414.675 4 -7 5 2 28.6404 136.065 4 7 -5 -2 265.643 138.129 1 -7 5 1 1140.65 241.359 4 7 -5 -1 1173.80 251.769 1 -7 5 0-4.73646 201.776 4 7 -5 0 126.506 205.734 1 7 -5 1 11104.4 711.258 1 -7 5 -1 11573.5 628.356 4 7 -5 2 4742.21 487.967 1 7 -5 3 14218.7 786.636 1 7 -5 4 1956.94 329.272 1 7 -5 5 928.764 251.832 1 7 -5 6 12496.2 683.102 1 7 -5 7 9938.80 566.732 1 7 -5 7 10027.9 504.158 9 7 -5 8 11096.7 513.739 1 7 -5 8 11486.5 526.267 12 7 -5 8 11147.3 481.018 9 7 -5 9 9147.46 413.695 12 7 -5 9 8488.14 362.404 9 7 -5 10 1399.06 145.923 12 -7 4 9 1417.15 165.527 6 -7 4 9 1458.10 193.095 4 -7 4 8 618.982 156.175 6 -7 4 8 616.568 188.978 4 -7 4 7 279.180 151.760 6 -7 4 7 413.924 181.689 4 -7 4 6 106.111 181.831 4 -7 4 5 3410.03 422.467 4 -7 4 4 14883.1 807.686 4 -7 4 3 15.1632 194.032 4 -7 4 2 29803.1 1115.26 4 7 -4 -1 5773.87 485.960 1 -7 4 1 5340.83 491.745 4 -7 4 0 930.900 242.409 4 7 -4 0 1015.21 255.060 1 -7 4 -1 731.373 223.610 4 7 -4 1 480.159 223.273 1 -7 4 -2-2.21486 117.754 4 7 -4 2-55.2009 230.460 1 7 -4 3 12672.4 758.096 1 7 -4 4 11675.3 734.504 1 7 -4 5 802.656 254.858 1 7 -4 6 21907.6 927.365 1 7 -4 7 352.775 199.410 1 7 -4 7 41.8608 129.743 9 7 -4 8 332.110 156.054 1 7 -4 8-55.1510 141.443 9 7 -4 9 11130.4 524.657 12 7 -4 9 10759.6 453.542 9 7 -4 10-65.3504 110.332 12 7 -4 11 500.540 104.603 12 -7 3 9 965.331 176.172 4 -7 3 9 898.612 159.183 6 -7 3 8 106.342 138.588 6 -7 3 8 223.811 140.254 4 -7 3 7 79.5618 168.092 6 -7 3 7-178.805 152.059 4 -7 3 6 3094.32 375.266 4 -7 3 5 8372.12 609.778 4 -7 3 4 593.849 204.568 4 -7 3 3-61.2235 191.029 4 -7 3 2-48.0631 152.624 4 7 -3 -1 5876.55 481.858 1 -7 3 1 5296.94 490.896 4 -7 3 0-14.2533 154.714 4 7 -3 0 398.519 171.507 1 7 -3 1 7419.91 576.011 1 -7 3 -1 7629.89 557.185 4 -7 3 -2 205.468 185.492 4 7 -3 2 237.273 160.323 1 7 -3 3 28200.6 1110.78 1 -7 3 -3 28433.8 965.601 4 7 -3 4 474.889 218.173 1 7 -3 5 8644.71 614.670 1 7 -3 6 580.120 253.240 1 7 -3 7 3864.24 435.347 1 7 -3 8-13.5838 162.167 1 7 -3 8-148.130 144.212 9 7 -3 9 33731.4 976.197 1 7 -3 9 34860.4 992.899 12 7 -3 10 1283.13 210.363 12 7 -3 11 413.752 121.882 12 7 -3 12 6170.79 278.649 12 7 -3 12 6062.30 317.564 2 -7 2 9 2132.49 236.483 6 -7 2 9 2172.45 241.665 15 -7 2 8 1427.61 199.329 4 -7 2 8 1552.16 243.972 6 -7 2 7 10862.7 572.985 6 -7 2 7 11241.8 615.973 4 -7 2 6 460.801 182.870 4 -7 2 5 20543.0 916.230 4 -7 2 4 19306.0 909.039 4 -7 2 3 36792.5 1239.90 4 -7 2 2 7266.40 584.891 4 -7 2 1 5796.80 492.909 4 -7 2 0 152.784 172.223 4 7 -2 0 238.862 162.825 1 -7 2 -1 1081.31 240.548 4 7 -2 1 1182.29 255.465 1 -7 2 -2 1378.67 263.222 4 7 -2 2 2006.40 328.464 1 -7 2 -3 1026.17 246.963 4 7 -2 3 861.613 222.750 1 7 -2 4 7366.85 590.851 1 -7 2 -4 6415.95 481.101 4 7 -2 5 2358.69 360.528 1 7 -2 6 15079.3 815.879 1 7 -2 7 2429.03 359.149 1 7 -2 8 12679.4 711.850 1 7 -2 9 7011.80 503.857 1 7 -2 9 7394.79 500.831 12 7 -2 10 29388.3 911.134 12 7 -2 11 3786.65 313.783 12 7 -2 12 241.378 107.529 12 -7 1 10 346.631 116.317 15 -7 1 9 94.6831 129.763 6 -7 1 9 123.398 120.790 15 -7 1 8 5974.94 425.230 6 -7 1 8 5950.74 422.791 15 -7 1 7 4699.97 408.183 6 -7 1 7 4952.34 406.427 4 -7 1 6 8655.94 559.624 6 -7 1 6 7672.36 538.990 4 -7 1 5 2849.04 362.704 4 -7 1 4 1380.67 294.502 4 -7 1 3 4331.65 446.968 4 -7 1 2-43.9238 135.427 4 -7 1 2 302.047 169.363 8 -7 1 1 5244.21 469.024 4 -7 1 1 4753.72 405.247 8 -7 1 0 114.571 151.507 4 7 -1 0 852.707 254.305 17 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106.723 16 10 11 6 205.842 104.567 5 -10 -11 -7 270.868 88.7791 16 10 11 7 439.257 137.928 5 10 11 8 80.2417 91.5163 5 -10 -11 -8 56.7610 85.5805 4 10 11 9-5.53214 81.0649 5 -10 -11 -9-14.8337 74.5554 4 10 11 10 424.728 99.9243 5 -10 -11 -10 333.438 98.2750 4 10 12 7 552.701 106.853 5 10 12 8 2438.92 179.306 5 -11 0 -1 50.1977 74.4517 4 -11 0 -2 2728.04 218.866 4 -11 0 -3 2391.97 201.401 4 -11 -1 0 5696.24 279.140 4 -11 -1 -1 45.0015 62.0130 16 -11 -1 -1 78.0911 91.6248 6 -11 -1 -1-36.5129 109.182 4 -11 -1 -2 5823.94 283.804 6 -11 -1 -2 5843.31 319.746 4 -11 -1 -3 3120.40 246.153 4 -11 -1 -4 3.56029 96.6296 4 -11 -1 -5 136.757 101.479 4 -11 -2 0 440.102 106.618 4 -11 -2 -1 6955.39 337.598 4 -11 -2 -1 6015.20 284.382 16 -11 -2 -2 326.258 107.530 6 -11 -2 -2 476.275 142.384 4 -11 -2 -3-18.6378 115.610 4 -11 -2 -4 35.8761 120.683 4 -11 -2 -5 1815.33 197.619 4 -11 -2 -6 670.777 136.665 8 -11 -2 -6 624.507 135.669 4 -11 -2 -7 5635.55 287.909 8 -11 -3 -1 1111.29 149.732 16 -11 -3 -1 1169.37 163.981 4 -11 -3 -2 200.656 110.825 16 -11 -3 -2 221.832 108.043 4 -11 -3 -3 215.274 130.654 4 -11 -3 -4 13993.9 517.713 4 -11 -3 -5 2230.19 230.237 4 -11 -3 -6 5089.61 312.641 4 -11 -3 -6 5134.93 310.032 8 -11 -3 -7 3346.85 235.832 4 -11 -3 -7 3784.23 261.317 8 -11 -3 -8-16.2338 93.5650 8 -11 -4 -1 4389.24 251.382 4 -11 -4 -1 4341.30 250.721 16 -11 -4 -2 2015.52 198.965 4 -11 -4 -2 2069.07 200.056 16 -11 -4 -3 9309.07 418.330 4 -11 -4 -3 9347.96 408.433 16 -11 -4 -4 428.825 132.636 16 -11 -4 -4 351.469 138.788 4 -11 -4 -5 2106.08 235.122 4 -11 -4 -6 110.434 111.786 8 -11 -4 -6 136.877 143.936 4 -11 -4 -7 981.596 152.688 16 -11 -4 -7 1082.95 179.249 8 -11 -4 -7 1038.13 161.973 4 -11 -4 -8 205.837 110.269 4 -11 -4 -8 184.204 101.298 8 -11 -4 -9 1390.82 157.403 8 -11 -5 -1 3591.44 227.886 16 -11 -5 -2 1977.63 186.589 4 -11 -5 -2 2423.75 211.351 16 -11 -5 -3 204.143 110.993 16 -11 -5 -3 111.492 102.580 4 -11 -5 -4 1545.74 200.896 4 -11 -5 -4 1573.05 206.754 16 -11 -5 -5 1504.63 191.690 4 -11 -5 -5 1760.11 202.345 16 -11 -5 -6 4236.13 294.337 4 -11 -5 -6 3934.89 270.078 16 -11 -5 -7 11.4852 103.431 16 -11 -5 -7-7.08109 115.046 8 -11 -5 -7 14.4097 108.107 4 -11 -5 -8 5929.10 323.580 4 -11 -5 -8 6183.97 334.630 8 -11 -5 -8 5260.29 254.622 16 -11 -5 -9 1324.91 167.780 8 -11 -5 -9 1141.16 150.709 4 -11 -6 -1 4959.29 244.644 16 -11 -6 -2 1485.94 165.939 16 -11 -6 -3 565.363 139.789 16 -11 -6 -3 427.236 118.647 4 -11 -6 -4 565.952 134.371 16 -11 -6 -4 168.596 115.008 4 -11 -6 -5 2582.27 233.932 4 -11 -6 -5 2368.41 224.537 16 -11 -6 -6 4457.21 298.614 4 -11 -6 -6 4304.56 272.547 16 -11 -6 -7 11265.0 450.722 4 -11 -6 -7 11090.0 394.488 16 -11 -6 -8 308.660 125.348 4 -11 -6 -8 47.2353 104.497 8 -11 -6 -9 402.128 116.742 4 -11 -6 -9 420.116 111.728 8 -11 -7 -2 144.655 84.7338 16 -11 -7 -3-34.9231 92.5406 16 -11 -7 -4 3908.33 237.918 4 -11 -7 -4 4292.22 272.073 16 -11 -7 -5 481.072 130.783 16 -11 -7 -5 514.347 116.383 4 -11 -7 -6 486.794 133.844 16 -11 -7 -6 661.181 154.015 4 -11 -7 -7 5821.18 323.099 4 -11 -7 -7 6348.18 292.562 16 -11 -7 -8 6677.63 334.985 4 -11 -7 -9 307.005 108.901 4 -11 -8 -3 498.161 108.085 16 -11 -8 -4 3675.02 233.229 16 -11 -8 -5 4713.79 263.214 16 -11 -8 -6 2112.07 186.189 4 -11 -8 -6 2080.18 181.187 16 -11 -8 -7 3736.46 251.031 4 -11 -8 -7 3256.83 203.926 16 -11 -8 -8 8842.03 364.192 4 -11 -8 -9 18.7482 73.2980 4 11 9 7 691.013 102.267 5 0 0 0 0.00 0.00 0 TITL ligand_DMA in P-1 REM P-1 (#2 in standard setting) CELL 1.54184 9.290073 13.675827 14.424352 66.9132 74.3150 74.6090 ZERR 2.00 0.000502 0.000690 0.000775 0.0049 0.0047 0.0045 LATT 1 SFAC C H N O UNIT 76.00 76.00 4.00 12.00 TREF HKLF 4 END ; _shelx_hkl_checksum 96545 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.187 _oxdiff_exptl_absorpt_empirical_full_min 0.898 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn O1 O 0.29326(13) 0.22626(9) 1.00781(9) 0.0306(3) Uani 1 1 d D H1 H 0.3854(19) 0.1864(17) 0.9981(16) 0.046 Uiso 1 1 d DR O18 O 0.62924(14) 0.25823(9) 0.49405(9) 0.0306(3) Uani 1 1 d D O42 O 0.55140(14) 0.10483(10) 0.99861(10) 0.0347(3) Uani 1 1 d . O39 O 0.72455(14) 0.37248(11) 0.56240(11) 0.0396(3) Uani 1 1 d . O19 O 0.76028(14) 0.10994(10) 0.59143(10) 0.0375(3) Uani 1 1 d . O2 O 0.40237(13) 0.36539(10) 0.90012(10) 0.0396(3) Uani 1 1 d . N35 N 0.68137(18) 0.49611(13) 0.63724(12) 0.0356(3) Uani 1 1 d . C12 C -0.13457(16) 0.41541(11) 0.99440(11) 0.0205(3) Uani 1 1 d . C17 C 0.01495(16) 0.37747(11) 0.95396(11) 0.0200(3) Uani 1 1 d . C5 C 0.09857(16) 0.37390(11) 1.10464(11) 0.0200(3) Uani 1 1 d . C22 C 0.40522(16) 0.12464(12) 0.54708(11) 0.0208(3) Uani 1 1 d . C10 C -0.05207(16) 0.41160(11) 1.14335(11) 0.0207(3) Uani 1 1 d . C27 C 0.30485(16) 0.09698(11) 0.50842(11) 0.0208(3) Uani 1 1 d . C3 C 0.29410(16) 0.33015(12) 0.96012(11) 0.0224(3) Uani 1 1 d . C11 C -0.15900(16) 0.47401(12) 1.06862(11) 0.0204(3) Uani 1 1 d . H11 H -0.265171 0.471912 1.108519 0.024 Uiso 1 1 calc R C34 C 0.60291(16) 0.11794(11) 0.39431(11) 0.0202(3) Uani 1 1 d . C28 C 0.37160(16) 0.03758(12) 0.43320(11) 0.0208(3) Uani 1 1 d . H28 H 0.291063 0.047068 0.394790 0.025 Uiso 1 1 calc R C4 C 0.14176(15) 0.40092(11) 0.98770(11) 0.0198(3) Uani 1 1 d . C29 C 0.49994(16) 0.09070(11) 0.35703(11) 0.0210(3) Uani 1 1 d . C20 C 0.66669(17) 0.15210(12) 0.53699(11) 0.0231(3) Uani 1 1 d . C6 C 0.19965(17) 0.31860(12) 1.17166(12) 0.0245(3) Uani 1 1 d . H6 H 0.302972 0.294790 1.145774 0.029 Uiso 1 1 calc R C9 C -0.10008(17) 0.39065(12) 1.24826(11) 0.0244(3) Uani 1 1 d . H9 H -0.202627 0.415881 1.274445 0.029 Uiso 1 1 calc R C33 C 0.72547(18) 0.16303(12) 0.32650(12) 0.0253(3) Uani 1 1 d . H33 H 0.797672 0.179127 0.351640 0.030 Uiso 1 1 calc R C13 C -0.25565(17) 0.39732(13) 0.96787(12) 0.0247(3) Uani 1 1 d . H13 H -0.356854 0.423188 0.995887 0.030 Uiso 1 1 calc R C21 C 0.57539(16) 0.09042(11) 0.51078(11) 0.0197(3) Uani 1 1 d . N44 N 0.76493(18) 0.01831(14) 0.92816(14) 0.0454(4) Uani 1 1 d . C8 C 0.00093(19) 0.33306(13) 1.31500(12) 0.0280(3) Uani 1 1 d . H8 H -0.032535 0.317930 1.386734 0.034 Uiso 1 1 calc R C7 C 0.15050(19) 0.29793(13) 1.27625(12) 0.0280(3) Uani 1 1 d . H7 H 0.220222 0.259326 1.321578 0.034 Uiso 1 1 calc R C26 C 0.14864(17) 0.12515(13) 0.53873(12) 0.0263(3) Uani 1 1 d . H26 H 0.080867 0.105692 0.512743 0.032 Uiso 1 1 calc R C30 C 0.51886(18) 0.11229(12) 0.25214(11) 0.0257(3) Uani 1 1 d . H30 H 0.449028 0.094207 0.226664 0.031 Uiso 1 1 calc R C16 C 0.04001(18) 0.32397(13) 0.88481(12) 0.0264(3) Uani 1 1 d . H16 H 0.140989 0.299897 0.854983 0.032 Uiso 1 1 calc R C32 C 0.74270(19) 0.18466(13) 0.22180(12) 0.0304(3) Uani 1 1 d . H32 H 0.825875 0.216431 0.175624 0.036 Uiso 1 1 calc R C23 C 0.34636(18) 0.17799(13) 0.61773(12) 0.0278(3) Uani 1 1 d . H23 H 0.413422 0.194683 0.646519 0.033 Uiso 1 1 calc R C31 C 0.6392(2) 0.16010(13) 0.18470(12) 0.0303(4) Uani 1 1 d . H31 H 0.650571 0.175952 0.113093 0.036 Uiso 1 1 calc R C38 C 0.6331(2) 0.42982(14) 0.61006(13) 0.0305(3) Uani 1 1 d . C14 C -0.23012(18) 0.34174(14) 0.90072(13) 0.0297(3) Uani 1 1 d . H14 H -0.313265 0.328664 0.883474 0.036 Uiso 1 1 calc R C25 C 0.09111(19) 0.18140(15) 0.60658(13) 0.0338(4) Uani 1 1 d . H25 H -0.015543 0.202210 0.625564 0.041 Uiso 1 1 calc R C15 C -0.08225(19) 0.30559(14) 0.85917(13) 0.0313(4) Uani 1 1 d . H15 H -0.064009 0.267960 0.812832 0.038 Uiso 1 1 calc R C24 C 0.1903(2) 0.20696(15) 0.64639(13) 0.0356(4) Uani 1 1 d . H24 H 0.151387 0.244565 0.693630 0.043 Uiso 1 1 calc R C41 C 0.6350(2) 0.08588(15) 0.92009(15) 0.0382(4) Uani 1 1 d . C40 C 0.4658(2) 0.42668(16) 0.63702(15) 0.0376(4) Uani 1 1 d . H40A H 0.446169 0.376997 0.609934 0.056 Uiso 1 1 calc GR H40B H 0.408989 0.499254 0.606910 0.056 Uiso 1 1 calc GR H40C H 0.433411 0.401738 0.711781 0.056 Uiso 1 1 calc GR C36 C 0.5816(2) 0.56631(16) 0.69247(16) 0.0427(4) Uani 1 1 d . H36A H 0.553948 0.638623 0.643321 0.064 Uiso 1 1 calc GR H36B H 0.634728 0.571045 0.740339 0.064 Uiso 1 1 calc GR H36C H 0.489430 0.536266 0.730734 0.064 Uiso 1 1 calc GR C37 C 0.8413(2) 0.50663(19) 0.60677(18) 0.0496(5) Uani 1 1 d . H37A H 0.899808 0.450925 0.577623 0.074 Uiso 1 1 calc GR H37B H 0.880006 0.497775 0.666945 0.074 Uiso 1 1 calc GR H37C H 0.851461 0.578257 0.555299 0.074 Uiso 1 1 calc GR C43 C 0.5880(3) 0.13879(19) 0.81784(16) 0.0538(6) Uani 1 1 d . H43A H 0.561759 0.084968 0.799163 0.081 Uiso 1 1 calc GR H43B H 0.672068 0.169944 0.766058 0.081 Uiso 1 1 calc GR H43C H 0.499488 0.196152 0.821229 0.081 Uiso 1 1 calc GR C46 C 0.8056(3) -0.03254(18) 1.0308(2) 0.0550(6) Uani 1 1 d . H46A H 0.833648 0.021193 1.048689 0.082 Uiso 1 1 calc GR H46B H 0.891833 -0.092159 1.030524 0.082 Uiso 1 1 calc GR H46C H 0.718478 -0.060436 1.081464 0.082 Uiso 1 1 calc GR C45 C 0.8675(3) -0.0130(2) 0.8439(2) 0.0601(6) Uani 1 1 d . H45A H 0.822201 0.021679 0.782200 0.090 Uiso 1 1 calc GR H45B H 0.884444 -0.091691 0.862667 0.090 Uiso 1 1 calc GR H45C H 0.964821 0.009934 0.830360 0.090 Uiso 1 1 calc GR H18 H 0.670(3) 0.289(2) 0.522(2) 0.075(9) Uiso 1 1 d D loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0246(6) 0.0214(5) 0.0400(6) -0.0109(5) -0.0020(5) 0.0019(4) O18 0.0362(6) 0.0240(6) 0.0366(6) -0.0112(5) -0.0107(5) -0.0086(5) O42 0.0316(6) 0.0336(6) 0.0421(7) -0.0214(5) -0.0116(5) 0.0069(5) O39 0.0347(7) 0.0408(7) 0.0554(8) -0.0317(6) -0.0033(6) -0.0081(6) O19 0.0382(7) 0.0340(6) 0.0497(7) -0.0146(6) -0.0235(6) -0.0058(5) O2 0.0214(6) 0.0299(6) 0.0518(8) -0.0099(6) 0.0083(5) -0.0013(5) N35 0.0373(8) 0.0361(8) 0.0411(8) -0.0222(7) -0.0014(6) -0.0113(6) C12 0.0188(7) 0.0192(7) 0.0205(7) -0.0037(5) -0.0031(5) -0.0040(5) C17 0.0179(7) 0.0184(7) 0.0212(7) -0.0041(5) -0.0036(5) -0.0036(5) C5 0.0193(7) 0.0167(6) 0.0212(7) -0.0040(5) -0.0026(5) -0.0042(5) C22 0.0205(7) 0.0196(7) 0.0194(6) -0.0045(6) -0.0030(5) -0.0031(5) C10 0.0192(7) 0.0177(7) 0.0235(7) -0.0055(6) -0.0032(5) -0.0037(5) C27 0.0208(7) 0.0185(7) 0.0194(6) -0.0031(5) -0.0041(5) -0.0026(5) C3 0.0187(7) 0.0234(7) 0.0244(7) -0.0085(6) -0.0059(6) -0.0006(6) C11 0.0159(6) 0.0205(7) 0.0213(7) -0.0056(6) -0.0010(5) -0.0027(5) C34 0.0212(7) 0.0174(7) 0.0206(7) -0.0060(5) -0.0037(5) -0.0024(5) C28 0.0204(7) 0.0220(7) 0.0208(7) -0.0064(6) -0.0065(5) -0.0039(6) C4 0.0156(6) 0.0195(7) 0.0217(7) -0.0065(5) -0.0018(5) -0.0017(5) C29 0.0221(7) 0.0177(7) 0.0211(7) -0.0057(6) -0.0041(6) -0.0018(5) C20 0.0222(7) 0.0263(8) 0.0230(7) -0.0114(6) -0.0010(6) -0.0069(6) C6 0.0216(7) 0.0219(7) 0.0271(7) -0.0053(6) -0.0057(6) -0.0027(6) C9 0.0241(7) 0.0234(7) 0.0237(7) -0.0072(6) -0.0007(6) -0.0062(6) C33 0.0255(7) 0.0237(7) 0.0263(7) -0.0084(6) -0.0018(6) -0.0072(6) C13 0.0185(7) 0.0254(7) 0.0274(7) -0.0065(6) -0.0037(6) -0.0040(6) C21 0.0191(7) 0.0200(7) 0.0203(7) -0.0070(5) -0.0036(5) -0.0040(5) N44 0.0324(8) 0.0381(9) 0.0642(11) -0.0236(8) -0.0010(7) -0.0030(7) C8 0.0341(8) 0.0272(8) 0.0214(7) -0.0053(6) -0.0047(6) -0.0086(7) C7 0.0319(8) 0.0241(8) 0.0267(8) -0.0036(6) -0.0127(6) -0.0039(6) C26 0.0213(7) 0.0281(8) 0.0260(7) -0.0062(6) -0.0042(6) -0.0036(6) C30 0.0321(8) 0.0225(7) 0.0227(7) -0.0069(6) -0.0079(6) -0.0037(6) C16 0.0228(7) 0.0284(8) 0.0275(7) -0.0116(6) -0.0024(6) -0.0028(6) C32 0.0329(8) 0.0276(8) 0.0252(8) -0.0071(6) 0.0045(6) -0.0101(7) C23 0.0279(8) 0.0314(8) 0.0258(7) -0.0135(7) -0.0030(6) -0.0048(6) C31 0.0409(9) 0.0285(8) 0.0183(7) -0.0064(6) -0.0021(6) -0.0072(7) C38 0.0349(9) 0.0270(8) 0.0312(8) -0.0106(7) -0.0070(7) -0.0067(7) C14 0.0249(8) 0.0350(9) 0.0333(8) -0.0122(7) -0.0082(6) -0.0085(7) C25 0.0223(8) 0.0384(9) 0.0341(9) -0.0129(7) 0.0017(6) -0.0012(7) C15 0.0305(8) 0.0359(9) 0.0335(8) -0.0182(7) -0.0068(7) -0.0052(7) C24 0.0320(9) 0.0404(10) 0.0341(9) -0.0209(8) 0.0025(7) -0.0026(7) C41 0.0377(10) 0.0286(9) 0.0493(10) -0.0148(8) -0.0083(8) -0.0053(7) C40 0.0336(9) 0.0387(10) 0.0454(10) -0.0195(8) -0.0063(8) -0.0074(8) C36 0.0480(11) 0.0422(10) 0.0462(10) -0.0278(9) -0.0048(9) -0.0065(9) C37 0.0422(11) 0.0570(13) 0.0632(13) -0.0343(11) 0.0032(10) -0.0230(10) C43 0.0642(14) 0.0487(12) 0.0390(10) -0.0164(9) -0.0095(10) 0.0070(11) C46 0.0432(11) 0.0425(11) 0.0828(16) -0.0224(11) -0.0330(11) 0.0090(9) C45 0.0405(12) 0.0516(13) 0.0737(15) -0.0269(12) 0.0159(11) -0.0038(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 -1 1 0.0521 1 0 0 0.0887 2 1 -1 0.0882 -1 1 -1 0.0588 -1 0 0 0.0623 0 -1 -1 0.0100 0 1 1 0.0100 -1 -1 0 0.0674 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C3 O1 H1 112.0(15) . . C20 O18 H18 107.8(19) . . C38 N35 C36 123.99(16) . . C38 N35 C37 119.96(15) . . C37 N35 C36 115.96(15) . . C17 C12 C11 117.99(13) . . C13 C12 C17 120.28(14) . . C13 C12 C11 121.71(13) . . C12 C17 C4 116.74(12) . . C16 C17 C12 118.92(13) . . C16 C17 C4 124.32(13) . . C10 C5 C4 116.40(12) . . C6 C5 C10 119.24(13) . . C6 C5 C4 124.33(13) . . C27 C22 C21 117.06(13) . . C23 C22 C27 119.02(14) . . C23 C22 C21 123.90(13) . . C5 C10 C11 118.30(13) . . C9 C10 C5 119.92(14) . . C9 C10 C11 121.78(13) . . C22 C27 C28 117.98(13) . . C26 C27 C22 119.99(14) . . C26 C27 C28 122.04(13) . . O1 C3 C4 112.78(12) . . O2 C3 O1 123.18(14) . . O2 C3 C4 124.03(14) . . C12 C11 H11 107.6 . . C12 C11 C4 113.07(11) . 2_567 C10 C11 C12 108.07(12) . . C10 C11 H11 107.6 . . C10 C11 C4 112.67(11) . 2_567 C4 C11 H11 107.6 2_567 . C29 C34 C21 116.54(12) . . C33 C34 C29 119.56(13) . . C33 C34 C21 123.84(13) . . C27 C28 H28 107.8 . . C27 C28 C29 108.16(12) . . C27 C28 C21 112.54(11) . 2_656 C29 C28 H28 107.8 . . C29 C28 C21 112.48(11) . 2_656 C21 C28 H28 107.8 2_656 . C17 C4 C5 107.38(11) . . C17 C4 C3 109.93(12) . . C17 C4 C11 110.74(11) . 2_567 C5 C4 C3 110.03(11) . . C5 C4 C11 110.16(11) . 2_567 C3 C4 C11 108.60(11) . 2_567 C34 C29 C28 118.30(12) . . C30 C29 C34 119.68(13) . . C30 C29 C28 122.02(13) . . O18 C20 C21 112.35(12) . . O19 C20 O18 123.02(14) . . O19 C20 C21 124.62(14) . . C5 C6 H6 119.8 . . C7 C6 C5 120.35(14) . . C7 C6 H6 119.8 . . C10 C9 H9 119.8 . . C8 C9 C10 120.42(14) . . C8 C9 H9 119.8 . . C34 C33 H33 119.9 . . C34 C33 C32 120.15(14) . . C32 C33 H33 119.9 . . C12 C13 H13 119.7 . . C12 C13 C14 120.58(14) . . C14 C13 H13 119.7 . . C22 C21 C34 107.62(11) . . C22 C21 C28 110.49(11) . 2_656 C22 C21 C20 109.70(12) . . C34 C21 C28 110.20(11) . 2_656 C34 C21 C20 110.23(11) . . C20 C21 C28 108.59(11) . 2_656 C41 N44 C46 117.12(18) . . C41 N44 C45 124.6(2) . . C45 N44 C46 118.26(18) . . C9 C8 H8 120.3 . . C7 C8 C9 119.50(14) . . C7 C8 H8 120.3 . . C6 C7 H7 119.7 . . C8 C7 C6 120.53(14) . . C8 C7 H7 119.7 . . C27 C26 H26 119.7 . . C25 C26 C27 120.55(15) . . C25 C26 H26 119.7 . . C29 C30 H30 119.8 . . C31 C30 C29 120.31(14) . . C31 C30 H30 119.8 . . C17 C16 H16 119.8 . . C17 C16 C15 120.35(15) . . C15 C16 H16 119.8 . . C33 C32 H32 119.9 . . C31 C32 C33 120.29(14) . . C31 C32 H32 119.9 . . C22 C23 H23 119.8 . . C24 C23 C22 120.47(15) . . C24 C23 H23 119.8 . . C30 C31 H31 120.0 . . C32 C31 C30 119.95(14) . . C32 C31 H31 120.0 . . O39 C38 N35 120.65(16) . . O39 C38 C40 121.04(15) . . N35 C38 C40 118.31(16) . . C13 C14 H14 120.3 . . C15 C14 C13 119.32(15) . . C15 C14 H14 120.3 . . C26 C25 H25 120.3 . . C24 C25 C26 119.49(15) . . C24 C25 H25 120.3 . . C16 C15 H15 119.7 . . C14 C15 C16 120.51(15) . . C14 C15 H15 119.7 . . C23 C24 H24 119.8 . . C25 C24 C23 120.44(16) . . C25 C24 H24 119.8 . . O42 C41 N44 119.79(19) . . O42 C41 C43 121.05(17) . . N44 C41 C43 119.16(19) . . C38 C40 H40A 109.5 . . C38 C40 H40B 109.5 . . C38 C40 H40C 109.5 . . H40A C40 H40B 109.5 . . H40A C40 H40C 109.5 . . H40B C40 H40C 109.5 . . N35 C36 H36A 109.5 . . N35 C36 H36B 109.5 . . N35 C36 H36C 109.5 . . H36A C36 H36B 109.5 . . H36A C36 H36C 109.5 . . H36B C36 H36C 109.5 . . N35 C37 H37A 109.5 . . N35 C37 H37B 109.5 . . N35 C37 H37C 109.5 . . H37A C37 H37B 109.5 . . H37A C37 H37C 109.5 . . H37B C37 H37C 109.5 . . C41 C43 H43A 109.5 . . C41 C43 H43B 109.5 . . C41 C43 H43C 109.5 . . H43A C43 H43B 109.5 . . H43A C43 H43C 109.5 . . H43B C43 H43C 109.5 . . N44 C46 H46A 109.5 . . N44 C46 H46B 109.5 . . N44 C46 H46C 109.5 . . H46A C46 H46B 109.5 . . H46A C46 H46C 109.5 . . H46B C46 H46C 109.5 . . N44 C45 H45A 109.5 . . N44 C45 H45B 109.5 . . N44 C45 H45C 109.5 . . H45A C45 H45B 109.5 . . H45A C45 H45C 109.5 . . H45B C45 H45C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 O1 H1 0.893(16) . O1 C3 1.3147(19) . O18 C20 1.3246(19) . O18 H18 0.882(17) . O42 C41 1.265(2) . O39 C38 1.250(2) . O19 C20 1.2054(19) . O2 C3 1.2052(19) . N35 C38 1.329(2) . N35 C36 1.464(2) . N35 C37 1.460(2) . C12 C17 1.398(2) . C12 C11 1.512(2) . C12 C13 1.388(2) . C17 C4 1.5364(19) . C17 C16 1.393(2) . C5 C10 1.399(2) . C5 C4 1.5383(19) . C5 C6 1.389(2) . C22 C27 1.399(2) . C22 C21 1.5311(19) . C22 C23 1.393(2) . C10 C11 1.511(2) . C10 C9 1.391(2) . C27 C28 1.510(2) . C27 C26 1.392(2) . C3 C4 1.539(2) . C11 H11 1.0000 . C11 C4 1.6113(19) 2_567 C34 C29 1.403(2) . C34 C33 1.390(2) . C34 C21 1.5338(19) . C28 H28 1.0000 . C28 C29 1.511(2) . C28 C21 1.615(2) 2_656 C29 C30 1.393(2) . C20 C21 1.5418(19) . C6 H6 0.9500 . C6 C7 1.388(2) . C9 H9 0.9500 . C9 C8 1.389(2) . C33 H33 0.9500 . C33 C32 1.392(2) . C13 H13 0.9500 . C13 C14 1.389(2) . N44 C41 1.313(2) . N44 C46 1.475(3) . N44 C45 1.461(3) . C8 H8 0.9500 . C8 C7 1.382(2) . C7 H7 0.9500 . C26 H26 0.9500 . C26 C25 1.387(2) . C30 H30 0.9500 . C30 C31 1.388(2) . C16 H16 0.9500 . C16 C15 1.393(2) . C32 H32 0.9500 . C32 C31 1.383(2) . C23 H23 0.9500 . C23 C24 1.389(2) . C31 H31 0.9500 . C38 C40 1.504(2) . C14 H14 0.9500 . C14 C15 1.385(2) . C25 H25 0.9500 . C25 C24 1.384(3) . C15 H15 0.9500 . C24 H24 0.9500 . C41 C43 1.494(3) . C40 H40A 0.9800 . C40 H40B 0.9800 . C40 H40C 0.9800 . C36 H36A 0.9800 . C36 H36B 0.9800 . C36 H36C 0.9800 . C37 H37A 0.9800 . C37 H37B 0.9800 . C37 H37C 0.9800 . C43 H43A 0.9800 . C43 H43B 0.9800 . C43 H43C 0.9800 . C46 H46A 0.9800 . C46 H46B 0.9800 . C46 H46C 0.9800 . C45 H45A 0.9800 . C45 H45B 0.9800 . C45 H45C 0.9800 . loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -0.0011 -0.9995 0.9978 0.0339 -0.0725 0.1820 0.9983 0.0001 -0.0004 0.0859 -0.1353 -0.0698 1.9976 0.9997 -0.9985 0.1380 -0.1980 -0.3216 -0.9972 0.9995 -0.9974 -0.1198 0.2078 -0.1122 -0.9983 -0.0001 0.0004 -0.0859 0.1353 0.0698 -0.0007 -0.9994 -0.9988 -0.0890 -0.1052 -0.0169 0.0007 0.9994 0.9988 0.0890 0.1052 0.0169 -0.9991 -0.9996 -0.0001 -0.1135 0.0464 0.1524