#------------------------------------------------------------------------------ #$Date: 2019-11-26 03:52:18 +0200 (Tue, 26 Nov 2019) $ #$Revision: 242550 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/13/26/4132603.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4132603 loop_ _publ_author_name 'Collet, Guillaume' 'Lathion, Timoth\'ee' 'Besnard, C\'eline' 'Piguet, Claude' 'Petoud, St\'ephane' _publ_section_title ; On-Demand Degradation of Metal-Organic Framework Based on Photocleavable Dianthracene-Based Ligand. ; _journal_issue 34 _journal_name_full 'Journal of the American Chemical Society' _journal_page_first 10820 _journal_page_last 10828 _journal_paper_doi 10.1021/jacs.8b05047 _journal_volume 140 _journal_year 2018 _chemical_formula_moiety 'C30 H20 O4, 2(C4 H9 N O)' _chemical_formula_sum 'C38 H38 N2 O6' _chemical_formula_weight 618.70 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _atom_sites_solution_primary dual _audit_creation_date 2017-09-25 _audit_creation_method ; Olex2 1.2 (compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381) ; _audit_update_record ; 2018-04-09 deposited with the CCDC. 2018-05-09 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 96.716(2) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 10.6198(3) _cell_length_b 12.0108(3) _cell_length_c 12.5761(3) _cell_measurement_reflns_used 3011 _cell_measurement_temperature 180.01(10) _cell_measurement_theta_max 73.5940 _cell_measurement_theta_min 5.0850 _cell_volume 1593.10(7) _computing_cell_refinement 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro 1.171.38.46 (Rigaku OD, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 180.01(10) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 10.4679 _diffrn_detector_type Atlas _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.969 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -26.00 30.00 1.00 3.10 -- -37.69 57.00 90.00 56 2 \w 25.00 71.00 1.00 3.10 -- 37.69 38.00 -90.00 46 3 \w 105.00 143.00 1.00 15.00 -- 110.40 111.00 -60.00 38 4 \w 109.00 134.00 1.00 15.00 -- 110.40 61.00-150.00 25 5 \w 110.00 175.00 1.00 15.00 -- 110.40 99.00-159.00 65 6 \w 72.00 115.00 1.00 3.10 -- 37.69 178.00-120.00 43 7 \w 100.00 158.00 1.00 15.00 -- 110.40 111.00 90.00 58 8 \w 100.00 178.00 1.00 15.00 -- 110.40 111.00 150.00 78 9 \w 107.00 139.00 1.00 15.00 -- 110.40 -45.00 90.00 32 10 \w 72.00 138.00 1.00 15.00 -- 110.40 -77.00 150.00 66 11 \w 56.00 106.00 1.00 15.00 -- 110.40 -94.00 120.00 50 12 \w 36.00 89.00 1.00 15.00 -- 110.40 -45.00 90.00 53 13 \w -73.00 34.00 1.00 3.10 -- -37.69 77.00 -30.00 107 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, Atlas' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0762622000 _diffrn_orient_matrix_UB_12 0.1015684000 _diffrn_orient_matrix_UB_13 -0.0461458000 _diffrn_orient_matrix_UB_21 -0.1241862000 _diffrn_orient_matrix_UB_22 -0.0662886000 _diffrn_orient_matrix_UB_23 0.0015041000 _diffrn_orient_matrix_UB_31 -0.0107628000 _diffrn_orient_matrix_UB_32 0.0417816000 _diffrn_orient_matrix_UB_33 0.1143014000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0226 _diffrn_reflns_av_unetI/netI 0.0339 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.969 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 15 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_number 5834 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.969 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 73.563 _diffrn_reflns_theta_min 4.192 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.704 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.885 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.46 (Rigaku Oxford Diffraction, 2015) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.290 _exptl_crystal_description prism _exptl_crystal_F_000 656 _exptl_crystal_size_max 0.114 _exptl_crystal_size_mid 0.06 _exptl_crystal_size_min 0.039 _refine_diff_density_max 0.273 _refine_diff_density_min -0.246 _refine_diff_density_rms 0.045 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 214 _refine_ls_number_reflns 3122 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.043 _refine_ls_R_factor_all 0.0507 _refine_ls_R_factor_gt 0.0404 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0538P)^2^+0.2851P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1004 _refine_ls_wR_factor_ref 0.1082 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2581 _reflns_number_total 3122 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ja8b05047_si_002.cif _cod_data_source_block batch3_2b _cod_database_code 4132603 _shelx_shelxl_version_number 2017/1 _chemical_oxdiff_formula C38H38N2O6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.973 _shelx_estimated_absorpt_t_min 0.924 _reflns_odcompleteness_completeness 99.90 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 67.29 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups, All O(H) groups 2.a Ternary CH refined with riding coordinates: C5(H5) 2.b Aromatic/amide H refined with riding coordinates: C1(H1), C2(H2), C3(H3), C7(H7), C8(H8), C9(H9), C10(H10), C14(H14) 2.c Idealised Me refined as rotating group: C20(H20A,H20B,H20C), C22(H22A,H22B,H22C), C23(H23A,H23B,H23C) ; _shelx_res_file ; TITL batch3_2b_a.res in P2(1)/c batch3_2b.res created by SHELXL-2017/1 at 09:44:28 on 25-Sep-2017 REM Old TITL batch3_2b in P2(1)/c REM SHELXT solution in P2(1)/c REM R1 0.123, Rweak 0.155, Alpha 0.042, Orientation as input REM Formula found by SHELXT: C19 N O3 CELL 1.54184 10.619773 12.010778 12.576099 90 96.7157 90 ZERR 2 0.000264 0.000324 0.0003 0 0.0023 0 LATT 1 SYMM -X,0.5+Y,0.5-Z SFAC C H N O UNIT 76 76 4 12 L.S. 10 PLAN 20 SIZE 0.039 0.06 0.114 TEMP -93 BOND $H list 4 MORE -1 CONF fmap 2 ACTA OMIT 6 8 3 REM REM REM WGHT 0.053800 0.285100 FVAR 6.85227 O16 4 0.194562 0.490970 0.779973 11.00000 0.04497 0.05382 = 0.02186 -0.01217 -0.01185 0.02060 O17 4 0.293417 0.370836 0.684293 11.00000 0.02760 0.03595 = 0.02235 -0.00166 -0.00648 0.01016 H17 2 0.350270 0.362256 0.747528 11.00000 -1.50000 C1 1 0.371621 0.582400 0.436109 11.00000 0.02362 0.03027 = 0.03740 0.00197 0.00439 -0.00205 AFIX 43 H1 2 0.455005 0.611921 0.448955 11.00000 -1.20000 AFIX 0 C2 1 0.312531 0.573785 0.332030 11.00000 0.03069 0.03339 = 0.03053 0.00388 0.01083 -0.00168 AFIX 43 H2 2 0.355380 0.596563 0.273478 11.00000 -1.20000 AFIX 0 C3 1 0.190146 0.531543 0.314299 11.00000 0.02989 0.03044 = 0.01987 0.00178 0.00435 0.00209 AFIX 43 H3 2 0.149010 0.526280 0.243222 11.00000 -1.20000 AFIX 0 C4 1 0.127043 0.496825 0.399446 11.00000 0.02203 0.01990 = 0.01884 0.00017 0.00120 0.00360 C5 1 -0.005527 0.449734 0.382860 11.00000 0.02118 0.02282 = 0.01465 -0.00072 -0.00069 0.00261 AFIX 13 H5 2 -0.023238 0.427008 0.306070 11.00000 -1.20000 AFIX 0 C6 1 -0.006889 0.345792 0.450187 11.00000 0.01914 0.02215 = 0.01825 -0.00064 0.00111 0.00327 C7 1 -0.061582 0.247178 0.409249 11.00000 0.02294 0.02705 = 0.01993 -0.00362 0.00135 0.00036 AFIX 43 H7 2 -0.099140 0.243963 0.336949 11.00000 -1.20000 AFIX 0 C8 1 -0.061365 0.153270 0.474011 11.00000 0.02719 0.02302 = 0.02861 -0.00390 0.00362 -0.00187 AFIX 43 H8 2 -0.096529 0.085348 0.445465 11.00000 -1.20000 AFIX 0 C9 1 -0.009602 0.159081 0.580510 11.00000 0.03015 0.02354 = 0.02600 0.00386 0.00599 0.00104 AFIX 43 H9 2 -0.012548 0.095939 0.625647 11.00000 -1.20000 AFIX 0 C10 1 0.046583 0.257256 0.621227 11.00000 0.02534 0.02687 = 0.01894 0.00032 0.00266 0.00196 AFIX 43 H10 2 0.082216 0.260635 0.694048 11.00000 -1.20000 AFIX 0 C11 1 0.050957 0.350320 0.556217 11.00000 0.01820 0.02274 = 0.01778 -0.00182 0.00136 0.00251 C12 1 0.112252 0.461426 0.593419 11.00000 0.01993 0.02243 = 0.01473 -0.00017 -0.00107 0.00289 C13 1 0.187754 0.503263 0.504192 11.00000 0.02089 0.02045 = 0.01963 -0.00003 0.00095 0.00411 C14 1 0.309257 0.547982 0.521718 11.00000 0.02326 0.02666 = 0.02565 -0.00068 -0.00194 0.00016 AFIX 43 H14 2 0.349997 0.555078 0.592771 11.00000 -1.20000 AFIX 0 C15 1 0.203638 0.443667 0.696800 11.00000 0.02277 0.02455 = 0.01772 -0.00022 -0.00254 0.00138 O18 4 0.542544 0.842190 0.652453 11.00000 0.02435 0.04493 = 0.02459 -0.00517 -0.00241 -0.00014 N21 3 0.491752 0.852633 0.475217 11.00000 0.02943 0.03382 = 0.02543 -0.00186 -0.00095 0.00025 C19 1 0.574532 0.831656 0.560642 11.00000 0.02291 0.02796 = 0.02913 -0.00723 0.00034 -0.00138 C20 1 0.705769 0.793214 0.545963 11.00000 0.02687 0.06313 = 0.04752 -0.02312 0.00078 0.00776 AFIX 137 H20A 2 0.700767 0.733064 0.492983 11.00000 -1.50000 H20B 2 0.748205 0.765930 0.614394 11.00000 -1.50000 H20C 2 0.754080 0.855531 0.520921 11.00000 -1.50000 AFIX 0 C22 1 0.520246 0.850155 0.364782 11.00000 0.06134 0.04721 = 0.02669 -0.00027 0.00644 0.00020 AFIX 137 H22A 2 0.610925 0.835929 0.363515 11.00000 -1.50000 H22B 2 0.498006 0.921981 0.330664 11.00000 -1.50000 H22C 2 0.470987 0.790889 0.325830 11.00000 -1.50000 AFIX 0 C23 1 0.360630 0.878175 0.490068 11.00000 0.02734 0.04495 = 0.04046 -0.00160 -0.00815 0.00575 AFIX 137 H23A 2 0.311825 0.808907 0.489801 11.00000 -1.50000 H23B 2 0.323639 0.926368 0.431720 11.00000 -1.50000 H23C 2 0.358354 0.916407 0.558659 11.00000 -1.50000 AFIX 0 HKLF 4 REM batch3_2b_a.res in P2(1)/c REM R1 = 0.0404 for 2581 Fo > 4sig(Fo) and 0.0507 for all 3122 data REM 214 parameters refined using 0 restraints END WGHT 0.0538 0.2851 REM Highest difference peak 0.273, deepest hole -0.246, 1-sigma level 0.045 Q1 1 0.3250 0.8344 0.5573 11.00000 0.05 0.27 Q2 1 0.7790 0.8301 0.5866 11.00000 0.05 0.21 Q3 1 0.2955 0.8508 0.4251 11.00000 0.05 0.19 Q4 1 0.0845 0.4033 0.5801 11.00000 0.05 0.18 Q5 1 0.0611 0.5053 0.6025 11.00000 0.05 0.18 Q6 1 0.1585 0.5056 0.3565 11.00000 0.05 0.17 Q7 1 0.5861 0.9100 0.3391 11.00000 0.05 0.16 Q8 1 0.1532 0.4731 0.5513 11.00000 0.05 0.16 Q9 1 0.1594 0.4555 0.6393 11.00000 0.05 0.15 Q10 1 0.4212 0.8477 0.3176 11.00000 0.05 0.14 Q11 1 0.3400 0.9741 0.4823 11.00000 0.05 0.14 Q12 1 0.3431 0.5466 0.4786 11.00000 0.05 0.14 Q13 1 -0.0071 0.3961 0.4176 11.00000 0.05 0.14 Q14 1 0.3713 0.5416 0.2612 11.00000 0.05 0.13 Q15 1 0.0047 0.3511 0.5045 11.00000 0.05 0.13 Q16 1 0.0699 0.4833 0.3904 11.00000 0.05 0.13 Q17 1 0.1627 0.5009 0.4522 11.00000 0.05 0.12 Q18 1 -0.0186 0.2961 0.4238 11.00000 0.05 0.12 Q19 1 0.3166 0.3661 0.5922 11.00000 0.05 0.12 Q20 1 0.4666 0.5929 0.3009 11.00000 0.05 0.12 ; _shelx_res_checksum 4330 _shelx_hkl_file ; 0 0 1 24.6990 29.3552 13 0 0 2 648992. 2157.31 1 0 0 2 642867. 3318.65 13 0 0 3-16.3558 112.534 6 0 0 3 39.8409 118.648 13 0 0 4 2462.64 325.509 13 0 0 4 2364.57 332.961 6 0 0 5 319.152 229.984 6 0 0 6 23205.1 1310.76 6 0 0 7-57.0122 196.449 6 0 0 8 22116.8 1599.02 6 0 0 9 220.768 285.471 6 0 0 10 7560.36 492.097 11 0 0 10 10518.4 1270.83 6 0 0 11 32.4736 146.871 11 0 0 12-46.4680 183.504 11 0 0 13-38.2270 161.852 11 0 0 14 1097.63 190.311 11 0 0 14 982.540 185.889 10 0 0 15 25.0545 73.9059 10 0 0 15 137.695 109.941 11 0 1 0 60.4093 43.0958 13 0 1 1 198929. 1575.65 13 0 -1 -1 202734. 1156.41 2 0 1 2 33940.9 807.927 13 0 -1 -2 29884.6 592.895 2 0 1 3 66616.3 1360.61 13 0 1 3 65885.1 1504.47 6 0 -1 3 63059.9 836.022 1 0 1 4 69331.9 1792.47 6 0 -1 4 69442.1 934.943 1 0 1 4 72823.1 1645.81 13 0 -1 5 2107.13 393.074 6 0 1 5 1454.33 302.102 13 0 1 5 1505.71 342.995 6 0 -1 6 602.389 310.591 6 0 1 6 623.671 304.697 6 0 1 6 488.463 188.924 13 0 -1 7 9347.44 935.754 6 0 -1 -7 9232.58 721.816 2 0 1 7 9719.24 983.564 6 0 1 8 3657.71 657.961 6 0 -1 8 3190.49 624.656 6 0 -1 9 379.571 287.277 6 0 1 10 165.811 139.758 11 0 -1 10 138.859 102.503 11 0 -1 11 56802.4 1364.87 11 0 1 11 57305.3 1373.53 11 0 1 12 4861.29 404.655 11 0 -1 12 4692.61 390.893 11 0 -1 13 18082.5 735.021 11 0 1 13 18033.9 800.285 10 0 1 13 18815.6 747.663 11 0 1 14 2170.53 247.150 10 0 -1 14 2082.43 252.608 10 0 1 14 2400.10 262.097 11 0 -1 14 2050.23 238.842 11 0 -1 15 388.314 125.763 11 0 -1 15 141.254 97.4373 10 0 2 0 125813. 1538.77 13 0 2 1 242083. 2257.66 13 0 2 2 113584. 1714.41 13 0 2 3 9177.42 580.034 13 0 -2 -3 9643.03 409.329 2 0 -2 -4 45597.1 1020.92 2 0 2 4 46066.0 1397.81 13 0 -2 -5 646.687 163.702 2 0 2 5 501.254 236.895 13 0 -2 -6 3481.48 369.977 2 0 -2 6 3338.59 530.549 6 0 2 6 3280.41 504.403 13 0 -2 7 66898.0 2498.77 6 0 2 7 63247.7 2315.49 13 0 2 8 2197.97 484.131 13 0 -2 8 1903.88 450.267 6 0 -2 9 26925.1 1940.92 6 0 -2 10 52656.1 1263.84 11 0 -2 10 51812.3 1201.83 12 0 2 10 52788.8 1276.97 11 0 2 11 17158.7 746.753 11 0 -2 11 17406.6 751.727 11 0 -2 11 16350.3 697.382 12 0 2 12 1788.30 291.213 10 0 -2 12 1873.07 245.725 11 0 2 12 1832.49 270.572 11 0 2 13 74.7484 125.941 10 0 -2 13 93.8106 136.970 11 0 2 14 668.763 174.672 11 0 2 14 396.894 131.315 10 0 -2 15 3399.67 247.407 10 0 -2 15 3260.76 227.034 11 0 3 0 1.87494 107.634 13 0 3 1 999999. 5599.88 13 0 3 2 152738. 2295.50 13 0 3 3 20884.9 950.224 13 0 3 4 775.097 236.470 13 0 3 5 4510.44 536.118 13 0 3 6 55380.0 2041.89 13 0 -3 7 96497.7 3080.08 6 0 3 7 92786.3 2889.43 13 0 -3 8-196.427 223.070 6 0 3 8 103.147 189.062 13 0 3 9 5505.56 841.405 13 0 -3 9 6842.15 435.381 3 0 -3 9 6695.31 974.722 6 0 -3 9 6316.36 418.592 12 0 3 9 6386.98 427.018 11 0 3 10 50731.1 1391.26 10 0 3 10 52884.8 1277.65 11 0 -3 10 50919.1 1229.52 3 0 -3 10 51358.2 1235.73 11 0 -3 10 50863.9 1218.75 12 0 -3 11 19928.2 791.145 11 0 3 11 20270.8 807.936 11 0 -3 11 20283.4 782.005 12 0 3 11 21690.5 915.805 10 0 3 12 726.271 170.037 10 0 3 12 533.918 170.860 11 0 -3 12 729.060 171.655 12 0 -3 12 693.406 166.487 11 0 3 13 1117.54 219.587 11 0 -3 13 650.274 153.105 12 0 -3 13 549.100 133.562 11 0 3 13 780.764 188.286 10 0 -3 14 846.972 157.670 11 0 -3 15 603.945 107.461 11 0 -3 15 112.819 75.8250 10 0 4 0 36739.5 1220.80 13 0 4 1 27589.8 1079.72 13 0 4 -1 26833.0 1043.24 13 0 4 2 76728.8 1883.61 13 0 4 3 16335.2 935.236 13 0 4 4 13856.6 934.933 13 0 4 5 158.158 207.752 13 0 4 6 55679.4 2171.93 13 0 4 7 441.259 295.958 13 0 -4 8 33055.3 2066.97 6 0 4 8 31052.0 1925.77 13 0 -4 9 36419.1 2343.96 6 0 -4 9 36571.2 1027.47 12 0 -4 9 35003.5 992.736 3 0 -4 9 36429.8 992.149 11 0 4 9 35240.1 1003.58 11 0 4 9 35715.3 2212.99 13 0 -4 10 62941.3 1380.62 3 0 -4 10 62755.5 1390.45 12 0 4 10 66369.5 1512.18 10 0 -4 10 64643.7 1371.37 11 0 4 10 64172.7 1392.44 11 0 4 11 714.038 182.183 10 0 4 11 387.092 162.085 11 0 -4 11 510.466 169.163 11 0 -4 11 515.651 156.504 12 0 4 12 647.727 190.627 11 0 -4 12 422.035 163.292 12 0 -4 12 125.248 118.411 11 0 -4 13 264.898 103.852 11 0 -4 13 233.827 119.723 12 0 -4 14 326.271 101.903 11 0 5 0 17.9955 188.295 13 0 5 1 363.208 235.860 13 0 5 -1 458.170 222.023 13 0 5 -2 102.056 174.543 13 0 5 2 159.784 205.121 13 0 5 3 39237.1 1585.29 13 0 5 4 27636.8 1445.88 13 0 5 5 8269.46 841.376 13 0 5 6 10.4223 193.111 13 0 5 7 41828.2 2157.36 13 0 -5 8 4816.16 362.868 3 0 -5 8 4547.09 361.141 12 0 -5 8 4917.46 825.892 6 0 5 8 3702.51 738.387 13 0 -5 9 24722.3 806.050 11 0 -5 9 26207.5 894.628 12 0 -5 9 25617.3 865.261 3 0 5 10 8069.21 493.942 11 0 -5 10 7056.31 470.029 3 0 -5 10 7212.04 448.638 11 0 -5 10 6982.11 487.483 12 0 -5 11 12244.9 608.377 3 0 -5 11 12724.3 582.512 11 0 -5 11 11850.7 617.199 12 0 5 11 11810.7 576.649 11 0 -5 12 1773.46 212.867 11 0 -5 12 2038.21 261.842 12 0 -5 13 313.801 129.906 12 0 -5 13 266.904 116.929 11 0 -5 14 1508.08 152.394 12 0 6 0 188343. 3537.42 13 0 6 -1 7845.97 739.219 13 0 6 1 7662.77 749.345 13 0 6 -2 47068.6 1795.55 13 0 6 2 47230.7 1849.91 13 0 6 3 1191.67 355.939 13 0 6 -3 1332.13 371.310 13 0 6 4 35789.9 1802.14 13 0 6 -4 36675.6 1715.45 13 0 6 5 6126.03 780.110 13 0 6 6 196.215 226.698 13 0 6 7-82.0201 158.242 13 0 -6 8 67.8396 103.593 3 0 6 8 76.3803 117.063 7 0 -6 8-6.41469 102.376 12 0 6 8-21.2559 182.653 13 0 -6 9 4763.89 396.395 3 0 -6 9 4562.78 394.191 12 0 -6 10 3833.10 353.806 3 0 -6 10 4127.08 372.987 12 0 -6 11 79.3742 140.626 12 0 -6 11-24.2189 130.333 3 0 -6 12 16.7337 106.887 12 0 -6 13 233.497 117.244 12 0 7 0-28.7147 188.692 13 0 7 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3954.40 660.154 13 0 -8 5 4296.76 337.432 12 0 -8 6 69.9386 116.776 12 0 8 6 279.052 124.257 7 0 8 7 2045.55 267.911 7 0 -8 7 2502.11 314.219 12 0 -8 7 1847.86 256.641 3 0 8 8 12247.1 653.298 7 0 -8 8 12649.1 627.917 12 0 -8 8 12117.0 604.460 3 0 -8 9 5988.91 423.607 3 0 -8 9 6160.36 450.944 12 0 -8 10 7792.95 489.890 12 0 -8 10 7555.15 453.627 3 0 -8 11 415.405 130.814 3 0 -8 11 30.1493 121.315 12 0 -8 12 808.575 155.599 12 0 -8 13 240.399 83.0488 12 0 9 0 374.294 252.245 13 0 9 1 1970.00 487.655 13 0 9 -1 2041.18 514.686 13 0 9 2 2075.54 267.409 7 0 9 -2 2228.70 523.569 13 0 9 2 1317.33 445.295 13 0 9 -3 507.119 263.910 13 0 9 3 841.866 349.276 13 0 9 3 489.624 169.437 7 0 9 -4-110.674 151.001 13 0 9 4 441.217 174.540 7 0 -9 5 3203.59 291.410 12 0 9 5 3462.75 355.395 7 0 9 6 93.1677 135.250 7 0 -9 6 213.753 127.055 12 0 9 7 8245.71 531.711 7 0 -9 7 7476.18 477.084 3 0 -9 7 8117.62 497.876 12 0 -9 8 54.6499 109.891 3 0 -9 8 85.3546 143.798 12 0 9 8 89.7086 118.152 7 0 -9 9 29.8232 111.686 3 0 -9 9 90.3141 108.143 12 0 -9 10 85.6310 115.466 12 0 -9 10 59.6488 103.878 3 0 -9 11 2097.70 226.998 12 0 -9 11 1878.52 192.429 3 0 -9 12 1968.02 185.560 12 0 10 0 125732. 1992.95 7 0 10 1 2751.87 323.034 7 0 10 -1 2860.06 319.727 7 0 10 -2 10646.5 589.267 7 0 10 2 10379.3 595.694 7 0 10 3 1550.94 263.413 7 0 10 4 9649.95 581.109 7 0 10 5 727.758 209.532 7 0 -10 6 441.518 154.963 12 0 10 6 324.634 156.340 7 0 -10 7 1619.68 222.118 12 0 10 7 1754.88 266.452 7 0 -10 7 1464.14 233.335 3 0 10 8 1971.05 265.830 7 0 -10 8 1949.59 245.007 12 0 -10 8 1625.70 228.681 3 0 -10 9 5533.91 366.945 12 0 -10 9 5059.64 341.176 3 0 -10 10 849.892 154.047 12 0 -10 10 700.564 130.243 3 0 -10 11 1843.77 182.802 12 0 11 0 163.067 146.199 7 0 11 1 191.024 137.079 7 0 11 -1 145.008 125.542 7 0 11 2 98.4751 142.217 7 0 11 -2 17.6030 133.686 7 0 11 3 12719.5 666.010 7 0 11 -3 13315.0 643.398 7 0 11 4 125.015 147.687 7 0 11 -4 16.3119 118.239 7 0 11 5 166.778 147.313 7 0 11 -5 166.159 127.215 7 0 11 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283.532 3 2 -3 10 2263.54 306.839 12 2 -3 11 675.540 157.953 11 2 -3 11 1058.48 224.149 12 2 3 11 1016.53 239.199 10 2 3 11 1323.32 285.575 11 2 3 12-132.148 159.728 10 2 -3 12 69.4679 122.854 12 2 -3 12-3.40236 117.662 11 2 3 13 2507.45 273.239 10 2 -3 13 2304.31 245.571 11 2 3 14 15315.5 510.822 10 2 -3 14 15926.8 615.443 10 -2 -4 14 7369.93 368.000 11 -2 4 13 447.571 141.344 11 -2 -4 13 291.314 111.117 12 -2 -4 13 164.114 112.793 11 -2 4 12 4849.21 364.415 11 -2 -4 12 4575.57 360.073 12 -2 -4 12 4400.80 370.072 11 -2 -4 11 5554.59 416.992 12 -2 4 11 4823.84 376.783 11 -2 -4 11 5571.31 431.986 11 -2 -4 10 5135.14 403.678 12 -2 -4 10 4905.30 373.282 3 -2 -4 10 4802.98 404.371 11 -2 4 10 4710.31 370.410 8 -2 -4 9 542.866 149.490 12 -2 -4 9 1004.92 174.178 3 -2 4 9 562.368 151.293 8 -2 -4 8 1606.07 512.974 6 -2 4 7 250.304 206.275 13 -2 -4 7 76.4997 171.219 6 -2 4 6 43470.8 1800.62 13 -2 -4 6 43986.7 1616.98 1 -2 4 5 67572.7 2099.20 13 2 4 -4 118614. 2059.47 13 -2 4 4 112169. 2519.11 13 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299.237 10 2 4 14 3547.85 229.458 10 -2 -5 14 56.4999 84.9554 11 -2 -5 13 1467.16 197.340 12 -2 -5 13 1806.45 207.475 11 -2 -5 12 317.159 133.301 12 -2 -5 12 344.344 129.316 11 -2 -5 11 23.2334 124.025 12 -2 -5 11 75.4915 123.845 11 -2 -5 10 2072.54 279.131 12 -2 -5 10 2064.45 267.726 11 -2 -5 10 1780.29 240.732 3 -2 5 10 1973.11 256.866 8 -2 -5 9 596.002 154.975 3 -2 5 9 573.967 150.692 8 -2 -5 9 806.747 186.167 12 -2 -5 8 16711.8 1563.79 6 -2 5 8 16056.8 642.727 8 -2 5 7 10103.4 1012.05 13 -2 5 6 364.890 231.981 13 -2 5 5 899.328 296.712 13 -2 5 4 1661.49 365.793 13 2 5 -4 1792.43 289.376 13 2 5 -3 99558.2 2102.59 13 -2 5 3 99721.5 2541.52 13 -2 5 2 4098.34 530.033 13 2 5 -2 4765.81 467.884 13 2 5 -1 3448.49 401.401 13 -2 5 1 3325.77 480.640 13 -2 5 0 133895. 2862.82 13 2 5 0 130692. 2528.89 13 2 5 1 4174.37 489.301 13 -2 5 -1 4538.09 577.511 13 2 5 2 8783.96 752.831 13 2 5 3 1239.52 344.729 13 2 5 4 14389.9 1104.44 13 2 5 5 4382.96 648.032 13 2 5 6 3604.78 632.506 13 2 5 7 2722.18 604.383 13 2 -5 8 7712.15 499.037 12 2 -5 8 7739.45 482.001 3 2 5 8 6970.56 996.264 13 2 5 8 8201.14 547.367 10 2 -5 9 1409.02 238.842 3 2 -5 9 1164.20 217.854 12 2 5 10 1191.99 250.968 10 2 -5 10 1068.74 236.995 12 2 -5 10 812.250 196.255 3 2 -5 11 13071.1 626.010 3 2 -5 11 12799.5 649.243 12 2 5 11 12555.8 638.033 10 2 5 12 3772.82 332.456 10 2 -5 12 3753.59 340.470 12 2 -5 13 1583.18 200.498 12 2 5 13 1916.96 207.855 10 2 -5 14-131.483 94.8216 10 -2 -6 13 2013.38 210.843 12 -2 -6 13 1870.62 181.350 11 -2 -6 12 1610.38 222.277 12 -2 -6 12 1650.38 212.467 11 -2 -6 11 7274.79 471.481 12 -2 -6 11 7832.63 452.987 11 -2 -6 10 19032.7 710.660 3 -2 6 10 19426.6 715.672 8 -2 -6 10 19453.1 785.803 12 -2 -6 10 19512.9 745.007 11 -2 6 9 69.2459 83.2883 8 -2 -6 9 80.5277 123.766 3 -2 -6 9 82.3041 128.200 12 -2 6 8 327.439 117.652 8 -2 -6 8 678.726 159.489 3 -2 6 7-433.410 278.341 13 -2 6 7 191.458 126.268 7 -2 6 6 9865.06 1015.72 13 -2 6 5 1014.62 364.539 13 -2 6 4 1670.20 400.232 13 2 6 -3 102.530 164.224 13 -2 6 3 19.2910 176.227 13 -2 6 2 129.577 190.003 13 2 6 -2 3.79057 142.517 13 2 6 -1 51118.3 1739.50 13 -2 6 1 48762.4 1931.83 13 2 6 0 45517.9 1673.72 13 -2 6 0 44453.5 1853.42 13 2 6 1 9375.77 806.966 13 -2 6 -1 9454.66 868.256 13 -2 6 -2 136804. 3375.76 13 2 6 2 130076. 3131.43 13 2 6 3 3367.16 562.005 13 2 6 4 7848.85 858.380 13 2 6 5 1410.86 412.290 13 2 6 6 457.123 274.787 13 2 6 7 42.0572 191.065 10 2 6 7 365.520 299.734 13 2 -6 7 221.146 111.920 3 2 -6 7 13.9744 129.965 12 2 -6 8 77605.0 1560.11 12 2 6 8 73662.1 1580.65 10 2 -6 8 73371.0 1485.10 3 2 -6 9 4044.68 369.673 3 2 6 9 4124.09 407.603 10 2 -6 9 4616.13 410.592 12 2 -6 10 32963.9 1044.53 12 2 -6 10 31716.9 979.623 3 2 6 10 31941.1 1018.71 10 2 -6 11 4853.98 381.910 3 2 -6 11 4442.58 389.392 12 2 6 11 4086.10 357.241 10 2 -6 12 775.156 177.453 12 2 6 12 634.484 154.438 10 -2 -7 13 3584.24 255.294 12 -2 -7 12 160.030 109.902 12 -2 -7 11 2150.08 255.395 12 -2 -7 10 13642.5 652.172 12 -2 -7 10 12931.4 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12802.6 613.766 7 2 -7 7 13492.5 646.671 12 2 7 8 2016.94 290.401 10 2 7 8 2413.63 280.084 7 2 -7 8 2220.50 288.426 3 2 -7 8 2417.47 308.786 12 2 -7 9 5839.53 432.535 3 2 -7 9 6181.48 460.370 12 2 -7 10 2594.85 307.575 12 2 7 10 3040.08 312.230 10 2 -7 10 2786.97 298.494 3 2 7 11 652.308 171.847 10 2 -7 11 592.730 160.524 3 2 -7 11 700.131 179.854 12 2 -7 12 1557.70 209.215 12 -2 -8 13 148.550 80.1128 12 -2 -8 12 577.195 133.743 12 -2 -8 11 4339.47 348.475 12 -2 -8 10 1083.07 199.666 12 -2 -8 10 1098.41 172.273 3 -2 -8 9 1147.71 219.651 12 -2 -8 9 1402.94 194.591 3 -2 -8 8 2143.23 282.570 12 -2 -8 8 2031.35 235.223 3 -2 -8 7 295.122 140.019 3 -2 8 7 107.742 143.647 7 -2 -8 6 1220.62 195.050 3 -2 8 6 1600.30 253.430 7 -2 8 5 3090.42 329.485 7 -2 8 5 3931.97 716.134 13 -2 8 4 655.010 281.601 13 -2 8 3 4747.17 752.562 13 -2 8 2 977.498 373.051 13 2 8 -2 221.357 189.573 13 -2 8 1 22673.9 1592.83 13 2 8 -1 20776.0 1388.35 13 2 8 0 113.630 176.041 13 -2 8 0 2.43651 186.768 13 2 8 1 1073.93 382.583 13 -2 8 -1-173.006 272.423 13 2 8 2 30262.9 1838.80 13 -2 8 -2 31117.1 1935.88 13 2 8 3 2509.52 562.066 13 -2 8 -3 2047.81 540.981 13 2 8 4 9339.36 549.086 10 2 8 4 8699.97 520.323 7 -2 8 -4 8760.30 1099.25 13 2 8 4 9479.67 1092.81 13 2 -8 5 2480.46 262.411 12 2 8 5 2510.81 295.778 7 2 8 6 2127.50 300.189 10 2 -8 6 1897.36 246.030 12 2 8 6 1993.41 268.784 7 2 8 7 5291.91 442.060 10 2 8 7 5541.05 420.651 7 2 -8 7 4822.20 400.534 12 2 -8 7 5645.10 432.774 3 2 8 8 5917.28 423.167 7 2 -8 8 5935.81 434.570 3 2 -8 8 6139.40 461.347 12 2 8 8 6017.31 451.383 10 2 -8 9 3656.30 341.397 3 2 -8 9 3545.51 348.229 12 2 8 9 3875.71 355.440 10 2 -8 10 9006.40 483.566 3 2 -8 10 9074.17 516.525 12 2 8 10 9004.22 480.609 10 2 -8 11 4482.04 345.015 12 2 -8 11 5014.43 330.348 3 2 -8 12 1643.32 182.471 12 -2 -9 12 23.5379 75.4004 12 -2 -9 11 367.809 119.661 12 -2 -9 10 866.079 183.870 12 -2 -9 9 4547.39 323.638 3 -2 -9 9 5038.63 387.542 12 -2 -9 8 3344.48 293.893 3 -2 -9 8 3004.57 316.368 12 -2 -9 7 453.255 143.316 12 -2 9 7 407.061 184.390 7 -2 -9 7 350.032 126.722 3 -2 -9 6 530.437 121.140 12 -2 -9 6 590.807 164.984 3 -2 9 6 548.207 178.648 7 -2 9 5 7199.86 494.789 7 -2 9 4 539.458 177.725 7 -2 9 3 8455.08 518.180 7 -2 9 3 7615.69 1006.49 13 -2 9 2 3749.06 349.192 7 -2 9 2 3057.96 663.943 13 2 9 -1 2062.11 459.412 13 -2 9 1 2198.46 538.183 13 -2 9 1 2144.83 260.499 7 -2 9 0 1650.65 486.850 13 2 9 0 2584.31 545.019 13 -2 9 0 2013.09 250.875 7 2 9 1 12896.8 632.729 7 2 9 1 11729.3 1167.38 13 -2 9 -1 13137.2 1302.92 13 -2 9 -1 13600.8 605.620 7 2 9 2 2221.51 295.987 10 2 9 2 1643.08 460.858 13 2 9 2 2438.95 294.538 7 2 9 3 95.8424 141.270 10 2 9 3 94.7416 113.028 7 2 9 4 4450.85 395.231 7 2 9 4 4181.88 389.502 10 2 9 5 374.451 178.529 10 2 9 5 558.034 168.803 7 2 9 6 5996.62 481.807 10 2 -9 6 5713.74 411.724 12 2 9 6 6096.62 449.997 7 2 -9 7 4379.81 366.172 12 2 -9 7 4113.56 370.452 3 2 9 7 4208.44 383.518 10 2 9 7 4094.39 360.965 7 2 -9 8 3527.68 332.870 3 2 -9 8 3281.29 324.488 12 2 9 8 3902.13 351.390 10 2 -9 9 10513.7 523.617 3 2 -9 9 10494.6 540.816 12 2 -9 10 4990.85 332.408 3 2 -9 10 4540.21 342.488 12 2 -9 11-111.884 96.0894 12 2 -9 11 122.850 85.4593 3 -2 -10 11 125.639 83.0758 12 -2 -10 10 2997.49 253.728 12 -2 -10 9 1190.98 187.101 12 -2 -10 8 124.257 115.267 12 -2 -10 7 4132.04 320.712 3 -2 -10 7 4179.53 341.506 12 -2 10 7 4273.71 381.663 7 -2 10 6 7109.69 498.208 7 -2 -10 6 6794.18 421.325 3 -2 -10 6 7017.42 443.377 12 -2 -10 5 13321.3 598.371 12 -2 10 5 12935.1 659.853 7 -2 10 4 152.610 127.054 7 -2 10 3 41.8900 130.545 7 -2 10 2 86536.1 1647.22 7 2 10 -1 2736.02 320.113 7 -2 10 1 2150.77 267.979 7 -2 10 0 88355.5 1626.89 7 2 10 0 93182.7 1755.11 7 -2 10 -1 13780.9 627.782 7 2 10 1 14350.6 697.911 7 2 10 2 1510.02 252.384 7 -2 10 -2 1860.01 254.184 7 2 10 3 3686.81 374.673 7 2 10 4 5159.34 431.547 10 2 10 4 4964.62 425.208 7 2 10 5 11914.4 618.511 7 2 10 5 11237.0 606.497 10 2 10 6 674.948 193.971 10 2 -10 6 843.434 192.800 3 2 10 6 647.829 163.754 7 2 10 7 1238.31 208.724 7 2 -10 7 1565.47 246.797 3 2 -10 7 1296.71 209.039 12 2 -10 8 16550.8 641.210 12 2 -10 8 17825.8 667.042 3 2 -10 9 4896.10 330.613 3 2 -10 9 4386.64 317.435 12 2 -10 10 2961.11 234.099 12 2 -10 10 2940.14 226.020 3 -2 -11 10 251.019 79.8627 12 -2 -11 9 1680.48 181.086 12 -2 -11 8 464.505 128.157 12 -2 -11 7 5622.13 353.582 12 -2 11 7 5314.40 395.527 7 -2 11 6 6858.86 459.269 7 -2 -11 6 6970.11 405.530 12 -2 11 5 16708.3 721.371 7 -2 11 4 20.9060 139.080 7 -2 11 3 8011.78 506.146 7 2 11 -2 860.894 217.960 7 -2 11 2 948.806 205.117 7 -2 11 1 275.164 159.144 7 2 11 -1 56.3597 120.539 7 2 11 0 632.740 193.363 7 -2 11 0 535.635 165.133 7 -2 11 -1 158.017 122.210 7 2 11 1-22.8602 137.117 7 -2 11 -2 5499.31 390.038 7 2 11 2 5848.51 457.970 7 2 11 3 697.121 198.612 7 2 11 4 270.277 155.274 7 2 11 5 8354.04 508.167 7 2 -11 6-71.4350 120.163 3 2 11 6-53.4332 103.433 7 2 -11 7 11154.7 509.212 3 2 11 7 10820.2 503.033 7 2 -11 8 4337.75 297.057 3 2 -11 8 4181.04 272.034 12 2 -11 9 2279.72 179.326 12 2 -11 9 2115.50 191.127 3 2 12 -8 131.991 80.0314 7 2 12 -7-49.4769 85.0881 7 2 12 -6 2143.99 237.581 7 -2 12 6 2527.07 253.766 7 -2 12 5 2917.78 298.004 7 2 12 -5 2794.60 277.643 7 -2 12 4 351.402 147.716 7 2 12 -4 400.242 132.451 7 -2 12 3 118.222 114.354 7 2 12 -3-25.7621 127.504 7 -2 12 2 8709.90 499.809 7 2 12 -2 8285.95 509.497 7 -2 12 1 9509.30 516.691 7 2 12 -1 9741.88 561.856 7 2 12 0 22258.0 844.668 7 -2 12 0 22090.5 766.996 7 2 12 1 1599.34 253.242 7 -2 12 -1 1661.30 218.810 7 -2 12 -2 95.2821 101.174 7 2 12 2-115.328 144.189 7 2 12 3 916.402 188.311 7 2 12 4 35.3546 118.270 7 2 -12 5 2979.86 275.120 3 2 12 5 3492.75 304.171 7 2 -12 6 3098.42 265.398 3 2 12 6 3167.34 261.586 7 2 -12 7 168.291 87.6233 3 2 -12 8 23176.7 548.058 3 2 13 -7 86.3666 57.0315 7 2 13 -6 339.892 96.1701 7 -2 13 5 637.295 137.556 7 2 13 -5 582.970 133.313 7 2 13 -4 2360.47 239.024 7 -2 13 4 2301.90 226.681 7 2 13 -3 2126.71 242.941 7 -2 13 3 1706.86 207.079 7 2 13 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1 -6 620.219 338.449 2 -4 -1 -7 1390.44 419.689 2 -4 1 -7 2.55605 143.935 2 -4 -1 -8 2811.73 603.105 2 -4 1 -8 2661.32 594.818 2 4 -1 8 2326.44 300.296 12 4 1 8 2524.68 318.096 11 4 -1 8 3134.08 336.585 11 4 1 9-56.4091 207.072 10 4 -1 9 273.028 127.709 12 4 1 9 461.470 218.701 11 4 -1 9 98.2841 135.552 11 4 1 10-258.124 242.076 10 4 -1 10 1146.56 290.111 11 4 1 11 867.105 238.507 10 4 -1 11 685.279 207.832 10 4 1 12 891.270 227.191 10 4 -1 12 791.540 192.896 10 4 1 13 14134.1 589.735 10 4 -1 13 14353.7 604.844 10 4 1 14 1494.02 159.154 10 4 -1 14 1852.98 174.334 10 -4 -2 15 1274.71 140.088 11 -4 2 14 305.585 103.394 11 -4 -2 14 408.101 132.603 11 -4 -2 13 56.3982 117.465 11 -4 2 13 54.0792 111.058 11 -4 2 12 2452.62 272.701 11 -4 -2 12 2520.66 306.622 11 -4 2 11 606.552 163.538 11 -4 2 10 3263.80 325.470 5 -4 -2 10 3456.93 338.305 5 -4 2 10 3027.44 308.810 8 -4 2 10 3240.87 319.752 11 -4 -2 9 2468.77 673.260 6 -4 2 9 3007.47 296.947 5 -4 -2 9 2945.20 288.262 5 -4 2 9 2555.75 281.926 8 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277.226 2 -4 -2 -7 1549.52 450.137 2 -4 2 -7 1422.32 451.913 2 4 -2 8 3016.76 287.546 3 4 2 8 3414.95 392.727 10 4 -2 8 3527.55 368.968 12 4 2 8 3874.39 390.055 11 4 -2 8 3704.87 335.931 11 4 -2 9 10719.3 626.304 12 4 -2 9 10292.2 560.801 11 4 2 9 11450.1 718.741 10 4 -2 10 3907.18 370.840 11 4 2 10 3813.16 423.586 10 4 2 11-48.8482 177.105 10 4 2 12 1199.14 238.829 10 4 -2 12 302.045 163.282 10 4 2 13 2779.83 271.146 10 4 -2 13 2732.97 273.801 10 4 2 14 38.3316 72.8241 10 4 -2 14 14.3329 70.6859 10 -4 -3 15 3681.97 208.221 11 -4 -3 14 115.974 94.2462 11 -4 -3 13 10250.4 516.804 11 -4 3 12 4984.51 353.720 11 -4 -3 12 4164.47 372.491 11 -4 -3 11 2945.16 295.156 12 -4 3 10 3863.82 343.349 5 -4 -3 10 3743.40 339.798 5 -4 3 10 3918.84 355.955 8 -4 3 9 5540.11 393.609 5 -4 -3 9 6216.36 411.875 5 -4 3 9 5865.49 421.246 8 -4 -3 8 11634.1 1284.40 6 -4 -3 7 29510.0 1612.25 1 -4 -3 7 28844.9 1835.83 6 -4 -3 6 34114.5 1826.07 6 -4 -3 6 33453.8 1647.67 1 -4 -3 5 1670.85 375.886 1 -4 -3 5 1813.46 418.836 6 -4 -3 4 6790.54 687.537 1 -4 3 4 6919.38 546.030 13 -4 -3 3 7101.95 685.265 1 -4 3 3 6362.88 539.016 13 -4 3 2 2819.73 381.016 13 -4 3 1 9135.95 701.800 13 4 3 -1 10020.4 497.500 13 -4 3 1 10183.3 617.317 2 4 3 0 47938.7 1293.79 13 -4 3 0 49725.3 1505.45 2 -4 3 -1 7921.14 664.535 2 4 3 1 8157.77 622.867 13 4 3 2 20259.6 1068.67 13 4 3 3 31384.1 1475.05 13 -4 -3 -3 29247.5 1504.59 2 4 3 4 22278.8 1382.22 13 -4 -3 -4 20595.6 1322.49 2 4 3 5 10622.4 1039.76 13 -4 -3 -5 10259.0 989.653 2 -4 -3 -6 983.114 341.430 2 -4 3 -7 8484.18 1064.79 2 -4 -3 -7 8055.06 949.234 2 4 -3 7 8169.89 518.719 12 4 3 7 8497.42 575.050 10 4 3 8 1473.51 276.395 10 4 -3 8 1640.48 224.999 3 4 -3 8 1712.49 271.652 12 4 -3 9 4322.96 365.566 3 4 -3 9 4308.14 412.013 12 4 3 9 4368.58 439.879 10 4 3 10 124.095 170.365 10 4 -3 10 10.7102 140.061 12 4 -3 10 191.030 160.164 11 4 3 11 474.987 193.597 10 4 3 12 7055.42 462.609 10 4 -3 12 6123.22 453.878 10 4 3 13 3346.44 273.122 10 4 -3 13 3374.02 286.606 10 -4 -4 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12 4 4 10 4036.83 414.641 10 4 4 11 496.732 208.630 10 4 4 12 971.247 184.835 10 4 -4 13 350.738 117.213 10 4 4 13 338.281 115.998 10 -4 -5 14 1875.90 162.099 11 -4 -5 13 389.830 105.637 12 -4 -5 13 466.387 116.965 11 -4 -5 12 373.355 125.191 12 -4 -5 12 531.921 152.477 11 -4 5 11 5006.06 383.543 8 -4 -5 11 5393.44 398.043 12 -4 5 10 6708.70 458.186 8 -4 5 9 3861.03 355.355 8 -4 5 8 2138.45 256.386 8 -4 -5 7-589.782 311.351 6 -4 5 7 112.048 99.7837 8 -4 -5 6-261.262 213.872 1 -4 -5 5 1660.26 440.374 1 -4 5 4 1500.88 321.852 13 -4 5 3 10525.3 880.502 13 -4 5 2 55368.9 2000.56 13 -4 5 1 26544.9 1402.73 13 -4 5 0 178.427 179.955 13 4 5 0 221.578 184.965 13 4 5 1 1450.89 324.248 13 4 5 2 8816.54 799.989 13 4 5 3 1306.57 337.732 13 4 5 4 46056.4 2130.37 13 4 5 5 1574.95 488.963 13 4 5 6 1140.65 211.193 10 4 5 6 1256.08 441.219 13 4 -5 6 853.724 170.905 3 4 -5 6 1073.12 207.231 12 4 5 7 509.298 216.187 10 4 -5 7 257.724 121.132 3 4 -5 7 405.718 175.586 12 4 -5 8 24807.1 848.677 3 4 5 8 26868.3 1015.88 10 4 -5 8 25332.5 956.050 12 4 -5 9 5048.49 398.185 3 4 5 9 3984.74 412.978 10 4 -5 9 4900.36 439.799 12 4 -5 10 5606.49 398.210 3 4 -5 10 5096.82 441.678 12 4 5 10 5804.10 468.068 10 4 5 11 3002.71 322.701 10 4 5 12 2793.19 272.400 10 4 5 13 95.8259 80.2942 10 4 -5 13 248.877 88.8523 10 -4 -6 13 4498.63 268.429 12 -4 -6 13 4906.31 282.504 11 -4 -6 12 4038.89 305.233 12 -4 -6 12 3954.01 303.998 11 -4 6 11 1695.59 220.524 8 -4 -6 11 2015.03 252.091 12 -4 -6 11 1875.57 240.260 11 -4 6 10 27510.8 877.993 8 -4 -6 10 23474.5 854.374 12 -4 6 9 956.484 200.870 8 -4 6 8 143.952 123.348 8 -4 6 7 8135.37 488.821 8 -4 6 6 47358.6 1120.66 8 -4 6 6 45860.0 1165.93 7 -4 -6 6 48570.9 2287.13 1 -4 6 5 26787.9 1592.27 13 -4 -6 5 23686.6 1576.16 1 -4 6 4 161.766 177.420 13 -4 6 3-713.898 273.536 13 -4 6 2 56246.2 2224.51 13 -4 6 1 14654.9 1145.51 13 4 6 0 36371.8 1527.68 13 -4 6 0 37362.0 1872.97 13 4 6 1 51360.5 1936.78 13 -4 6 -1 51995.1 2296.33 13 4 6 2 698.638 270.019 13 -4 6 -2 175.922 205.529 13 4 6 3 1674.67 418.945 13 4 6 4 25083.4 1657.94 13 4 6 5 2390.28 311.742 10 4 6 5 1887.11 507.885 13 4 -6 5 2508.08 289.939 12 4 -6 6 24724.5 823.531 3 4 -6 6 24556.6 890.103 12 4 6 6 25463.0 964.697 10 4 6 7 701.172 231.938 10 4 -6 7 1082.83 200.074 3 4 -6 7 994.751 217.141 12 4 -6 8 22411.8 809.054 3 4 -6 8 21833.0 889.069 12 4 6 8 22981.3 931.446 10 4 -6 9 8536.62 498.304 3 4 -6 9 8443.44 561.629 12 4 6 9 8296.48 554.577 10 4 -6 10 4329.64 340.748 3 4 -6 10 4231.28 385.894 12 4 6 10 4212.73 379.759 10 4 6 11-103.797 136.888 10 4 6 12 5353.59 321.962 10 4 -6 12 4703.47 300.207 10 -4 -7 13 114.083 72.6202 12 -4 -7 12 10205.3 454.784 12 -4 -7 12 9850.27 404.602 11 -4 -7 11 6700.55 421.107 12 -4 -7 11 6825.57 390.778 11 -4 7 10 4982.34 367.853 8 -4 -7 10 5297.69 408.050 12 -4 7 9 57398.7 1259.48 8 -4 7 8-73.4811 142.882 8 -4 7 7 1371.17 214.789 8 -4 7 6 18807.6 720.755 8 -4 7 6 18618.6 778.549 7 -4 7 5 351.091 133.752 8 -4 7 5 576.550 140.667 7 -4 7 4 1204.91 390.386 13 -4 7 3 3515.22 625.840 13 -4 7 2 4693.46 713.243 13 -4 7 1 67.4948 212.340 13 -4 7 0 23197.8 1593.75 13 4 7 1 5895.42 720.118 13 -4 7 -1 6142.58 843.530 13 4 7 2 3646.79 623.026 13 -4 7 -2 3260.03 655.297 13 -4 7 -3 11318.7 1257.30 13 4 7 3 11133.5 1118.42 13 4 7 4-213.767 157.877 10 -4 7 -4 262.861 273.111 13 4 7 4-101.449 154.716 13 4 -7 5 16884.6 732.487 12 4 7 5 18546.9 823.630 10 4 7 6 182.174 164.146 10 4 -7 6 515.741 166.722 3 4 -7 6 94.3189 134.144 12 4 -7 7 8300.92 503.930 3 4 -7 7 8128.53 539.458 12 4 7 7 8982.04 598.604 10 4 7 8 95.1619 164.348 10 4 -7 8 156.641 115.701 3 4 -7 8-32.6970 127.075 12 4 7 9 365.550 186.323 10 4 -7 9 425.167 150.309 3 4 -7 9 324.767 175.752 12 4 7 10 109.186 138.677 10 4 -7 10 258.132 118.328 3 4 -7 10 39.2103 115.441 12 4 7 11 988.656 176.776 10 4 7 12 1169.82 141.500 10 -4 -8 12 491.842 112.319 12 -4 -8 11 527.158 142.237 12 -4 8 10 6580.28 381.516 8 -4 -8 10 6172.23 414.354 12 -4 8 9 4501.66 338.807 8 -4 -8 9 4493.91 380.433 12 -4 8 8 12230.9 571.298 8 -4 8 7 5306.68 389.580 8 -4 8 6 1322.66 206.868 8 -4 8 6 1233.01 236.457 7 -4 8 5 12678.4 592.802 8 -4 8 5 13157.2 636.307 7 -4 8 4 8271.64 484.505 8 -4 8 4 7232.31 462.584 7 -4 8 4 6781.11 902.869 13 -4 8 3 3579.26 319.142 8 -4 8 3 3490.49 665.971 13 -4 8 2 20228.8 739.445 8 -4 8 2 21918.9 1650.94 13 -4 8 1 42778.3 2310.75 13 -4 8 1 40455.4 1045.25 8 -4 8 0 522.318 314.372 13 -4 8 0 411.917 154.978 8 -4 8 -1 15588.3 1452.77 13 4 8 1 13222.5 610.573 7 4 8 1 14060.7 704.557 10 -4 8 -2 25889.4 1868.18 13 4 8 2 23733.8 1626.49 13 4 8 2 24817.2 831.048 7 4 8 2 26625.0 978.931 10 4 8 3 29027.1 1894.97 13 4 8 3 30883.5 1075.71 10 4 8 4 17583.9 825.702 10 4 8 5 1280.48 292.101 10 4 -8 5 881.953 202.261 12 4 8 6 2323.79 336.674 10 4 -8 6 2426.03 288.441 3 4 -8 6 2297.35 303.452 12 4 8 7 160.642 165.499 10 4 -8 7-67.7110 110.093 3 4 -8 7 8.20574 133.933 12 4 8 8 238.898 189.795 10 4 -8 8-40.5902 114.024 3 4 -8 8 166.719 147.728 12 4 -8 9 12487.2 547.722 3 4 -8 9 12100.0 589.176 12 4 8 9 12108.8 602.184 10 4 -8 10 1537.60 188.400 3 4 8 10 2084.17 264.776 10 4 8 11 3256.98 238.528 10 -4 -9 12 161.931 62.3080 12 -4 -9 11 548.427 125.428 12 -4 -9 10 147.215 112.302 12 -4 9 9 558.055 127.941 8 -4 -9 9 494.079 165.159 12 -4 9 8 8386.16 443.841 8 -4 -9 8 8175.89 491.876 12 -4 9 7 15260.7 620.201 8 -4 9 6-12.5474 107.688 8 -4 9 6-39.7876 125.706 7 -4 9 5 1270.50 201.097 8 -4 9 5 1181.35 219.724 7 -4 9 4 2818.94 290.133 8 -4 9 4 2425.09 293.977 7 -4 9 3 1278.65 198.596 8 -4 9 3 1150.18 207.737 7 -4 9 2 12889.1 603.674 8 -4 9 1 3406.88 326.045 8 -4 9 0 2230.53 266.489 8 4 9 0 2070.75 266.589 7 4 9 1 3563.01 338.611 7 -4 9 -1 3676.47 340.197 8 4 9 2 936.616 251.475 10 4 9 2 771.217 206.677 7 4 9 3-41.2123 196.644 10 4 9 3 66.0492 131.912 7 4 9 4 1043.22 251.522 10 4 9 4 1102.62 201.570 7 4 9 5 7913.97 569.202 10 4 -9 6 6412.33 438.412 12 4 -9 6 5880.85 420.160 3 4 9 6 6300.91 495.276 10 4 9 7 485.230 185.818 10 4 -9 7 320.733 146.486 3 4 -9 7 182.462 120.204 12 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506.308 3 5 4 9 10565.3 637.280 10 5 4 10 2796.23 346.959 10 5 4 11-47.2012 155.020 10 5 -4 11-120.749 153.303 10 5 -4 12 1575.85 196.513 10 5 4 12 1957.52 237.916 10 5 4 13-93.1116 85.1127 10 -5 -5 13-73.4428 83.9599 11 -5 -5 12 4403.26 308.569 12 -5 -5 12 4387.02 337.970 11 -5 5 11 4748.48 364.886 8 -5 -5 11 4320.04 349.203 12 -5 5 10 598.722 169.699 8 -5 5 9 3176.28 332.218 8 -5 5 8 6171.62 441.678 8 -5 5 7 12411.4 604.403 8 -5 -5 7 13064.8 1246.26 1 -5 -5 6 32320.3 1978.26 6 -5 5 6 36439.7 991.231 8 -5 -5 6 31931.0 1910.06 1 -5 -5 5 16047.4 1281.55 6 -5 -5 5 15383.3 1301.07 1 -5 -5 4 8931.65 970.070 1 -5 5 3 5293.81 662.406 13 -5 5 2 3928.73 567.983 13 -5 5 1 4696.93 647.567 13 -5 5 0 10397.0 954.822 13 -5 5 -1 253.555 188.366 2 -5 5 -2 7724.54 826.742 2 5 5 2 7189.00 792.520 13 5 5 3 161.878 183.193 13 -5 5 -3 135.471 192.488 2 -5 5 -4 4818.52 742.280 2 5 5 4 5523.64 779.062 13 5 5 5 22506.2 1701.15 13 5 -5 5 21259.3 820.360 12 5 5 5 20769.4 845.526 10 5 -5 6 50830.9 1132.31 3 5 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2099.12 269.811 8 -7 3 8 7639.61 474.733 5 -7 -3 8 7462.96 473.550 5 -7 3 8 7173.99 464.025 8 -7 3 7 36493.6 1000.18 5 -7 -3 7 33201.0 969.969 5 -7 3 7 33601.3 988.001 8 -7 3 6 595.149 180.371 8 -7 3 6 427.175 135.080 5 -7 -3 6 591.326 180.970 5 -7 -3 6 660.804 338.764 1 -7 -3 5 31952.6 2021.03 1 -7 3 5 30224.3 889.108 5 -7 -3 5 28690.7 878.686 5 -7 3 5 28862.0 881.094 8 -7 -3 4 12973.5 1257.25 1 -7 -3 3 15261.9 1331.16 1 -7 -3 2 1495.06 424.621 1 -7 -3 1 3919.75 682.862 1 -7 -3 0 6923.81 826.538 1 -7 3 -1 3090.55 564.826 2 -7 -3 -1 3065.16 523.111 1 -7 3 -2 10583.0 1099.80 2 7 3 3 481.175 249.598 9 -7 3 -3-181.763 224.596 2 7 3 4 1176.15 246.248 10 7 3 4 813.750 320.634 9 7 3 5 63833.8 2105.73 9 7 3 5 59129.9 1403.67 10 7 3 6 4398.23 585.855 9 7 3 6 4007.50 392.090 10 7 3 7 1582.66 263.067 10 7 3 7 1365.28 354.524 9 7 3 8 251.863 160.038 10 7 3 9 534.537 197.901 10 7 3 10 1975.00 241.927 10 7 -3 10 2881.93 335.292 9 7 -3 11 19205.6 717.314 9 7 3 11 17846.9 558.715 10 -7 -4 13 172.614 80.6986 11 -7 -4 12-1.83608 97.3023 11 -7 4 11 148.156 97.9753 8 -7 -4 11 174.843 91.5302 12 -7 4 10 20.8158 93.4159 5 -7 -4 10-49.9238 110.881 5 -7 4 10 245.856 139.608 8 -7 4 9 491.678 151.218 5 -7 -4 9 641.632 162.925 5 -7 4 9 847.460 204.764 8 -7 4 8 14457.8 623.537 5 -7 -4 8 13271.7 608.381 5 -7 4 8 12624.4 630.228 8 -7 4 7 4026.31 334.113 5 -7 -4 7 3648.46 320.942 5 -7 4 7 3593.18 342.201 8 -7 4 6 13251.7 585.038 5 -7 -4 6 12485.5 577.916 5 -7 4 6 12650.1 613.843 8 -7 -4 5 922.212 479.458 1 -7 4 5 706.629 164.491 8 -7 4 5 829.872 157.833 5 -7 -4 5 700.860 158.475 5 -7 -4 4 8999.72 490.831 5 -7 4 4 8379.60 496.830 8 -7 -4 4 8471.57 1051.84 1 -7 -4 3-208.553 235.930 1 -7 -4 2 34985.3 2016.64 1 -7 -4 1 164.220 273.153 1 -7 -4 0 2318.89 510.306 1 -7 -4 -1 37707.7 1953.97 1 7 4 2 28074.3 1533.75 9 7 4 2 22200.1 834.377 10 7 4 3 4651.86 634.577 9 -7 4 -3 4516.46 793.433 2 7 4 3 3820.71 374.518 10 7 4 4 1212.97 229.484 10 7 4 4 2070.94 447.149 9 7 4 5 131.282 173.309 10 7 4 5 62.6065 301.722 9 7 4 6 26449.4 1439.14 9 7 4 6 21071.6 871.116 10 7 4 7 243.615 180.527 10 7 4 8 6185.14 459.750 10 7 4 9 1461.79 231.150 10 7 -4 10 3177.39 336.709 9 7 4 10 2437.46 250.142 10 7 -4 11 11372.7 517.913 9 7 4 11 10932.9 422.055 10 -7 -5 13 402.763 80.1658 11 -7 -5 12 322.549 100.862 11 -7 5 11 179.876 107.267 8 -7 -5 11 215.912 101.785 12 -7 5 10 161.108 116.703 8 -7 5 9 7372.06 469.897 8 -7 5 8 2128.11 275.557 8 -7 5 7 5054.98 402.662 8 -7 5 6 5302.94 415.075 8 -7 5 5 6496.48 452.644 8 -7 5 4 2296.21 286.410 8 -7 -5 3 1394.79 533.572 1 -7 5 3 745.493 190.184 8 -7 -5 2 988.488 379.372 1 -7 5 2 1753.81 250.210 8 -7 5 1 431.365 150.777 8 -7 -5 1-776.661 353.145 1 -7 5 0 15085.9 664.146 8 -7 -5 0 16098.3 1357.04 1 7 5 0 15724.7 718.496 10 -7 -5 -1 7909.07 946.925 1 7 5 1 8128.67 533.811 10 7 5 2 87.9598 160.722 10 7 5 3 1376.60 268.156 10 7 5 4 45129.0 1272.63 10 7 5 5 5428.07 462.448 10 7 5 6 1496.55 278.373 10 7 5 7 1690.08 281.639 10 7 5 8 3657.28 362.132 10 7 5 9-23.7968 135.348 10 7 5 10-43.7064 111.447 10 7 -5 10 215.249 158.180 9 7 -5 11 2360.40 228.301 9 7 5 11 2517.82 194.222 10 -7 -6 12 704.544 99.7203 12 -7 -6 12 810.073 121.771 11 -7 6 11 1287.64 167.612 8 -7 -6 11 1238.19 161.995 12 -7 6 10-9.34583 95.9006 8 -7 6 9 81.4764 110.913 8 -7 6 8 3507.84 335.692 8 -7 6 7 5063.39 400.520 8 -7 6 6 14929.5 687.090 8 -7 6 5 19803.7 792.738 8 -7 6 4 4151.77 377.951 8 -7 6 3 3143.06 328.290 8 -7 6 2 224.755 154.568 8 -7 6 1 0.65933 129.275 8 -7 6 0 10419.1 578.010 8 7 6 0 10810.7 623.510 10 7 6 1 43890.9 1258.37 10 7 6 2 9426.57 601.897 10 7 6 3 644.480 202.607 10 7 6 4 27646.0 1028.92 10 7 6 5 2941.65 374.428 10 7 6 6 19434.1 840.385 10 7 6 7 285.191 203.728 10 7 6 8 17134.1 713.387 10 7 6 9 45.0384 132.091 10 7 6 10 697.741 146.315 10 7 -6 10 635.086 151.296 9 -7 -7 11 3802.56 247.580 12 -7 -7 11 3978.45 254.311 11 -7 7 10 4842.32 318.671 8 -7 7 9 46.6560 109.732 8 -7 7 8 125.012 135.304 8 -7 7 7 472.406 174.411 8 -7 7 6 2185.10 270.646 8 -7 7 5 5839.77 438.583 8 -7 7 4 1394.08 268.979 8 -7 7 3 727.389 194.031 8 -7 7 2 413.881 162.573 8 -7 7 1 27590.2 935.877 8 -7 7 0 10351.4 576.925 8 7 7 1 2278.79 320.395 10 -7 7 -1 1797.34 267.035 8 7 7 2 28024.1 1038.38 10 7 7 3 212.287 177.772 10 7 7 4 509.278 216.081 10 7 7 5 10209.6 638.844 10 7 7 6 1089.97 246.664 10 7 7 7 1544.24 256.610 10 7 7 8 938.575 250.152 10 7 7 9 426.035 137.652 10 7 -7 9 981.931 181.495 9 7 7 10 663.905 113.474 10 -7 -8 11 8.33761 53.8926 12 -7 8 10 151.695 69.9005 8 -7 -8 10 267.959 111.452 12 -7 8 9 2137.96 213.997 8 -7 8 8 8602.87 451.771 8 -7 8 7 673.372 167.443 8 -7 8 6 3131.18 309.320 8 -7 8 5 3791.03 349.861 8 -7 8 4 388.285 170.881 8 -7 8 3 14493.4 675.404 8 -7 8 2 700.610 174.732 8 -7 8 1 536.504 181.304 8 -7 8 0 11165.6 600.905 8 -7 8 -1 3327.10 342.706 8 -7 8 -2 28919.1 940.831 8 7 8 2 29722.0 1057.28 10 7 8 3 4494.48 442.834 10 7 8 4 2135.62 310.677 10 7 8 5 829.191 235.995 10 7 8 6 5603.89 428.932 10 7 -8 7 4343.02 349.355 9 7 8 7 3178.98 312.189 10 7 -8 8 8016.75 415.916 9 7 8 8 7663.07 411.327 10 7 8 9 735.016 125.737 10 -7 -9 10-46.8916 63.0211 12 -7 9 9 1586.70 160.890 8 -7 -9 9 1597.99 178.893 12 -7 9 8 7160.91 368.835 8 -7 9 7 19272.3 647.689 8 -7 9 6 342.240 135.244 8 -7 9 5 242.097 118.863 8 -7 9 4 3534.89 330.759 8 -7 9 3 4543.05 378.804 8 -7 9 2 6144.04 434.973 8 -7 9 1 405.803 144.925 8 -7 9 0 117.439 119.094 8 -7 9 -1 162.775 130.601 8 -7 9 -2 3388.14 325.216 8 -7 9 -3 2751.90 295.990 8 -7 9 -4 826.342 180.279 8 7 9 4 889.164 226.406 10 7 9 5 474.627 183.133 10 -7 9 -5 557.532 148.408 8 7 9 6 1803.51 241.083 10 -7 9 -6 1979.00 216.224 8 -7 9 -7 2309.03 204.799 8 7 9 7 1985.67 226.223 10 -7 9 -8 1128.59 127.247 8 -7 -10 9 181.302 64.1650 12 -7 10 8 503.800 95.1100 8 -7 -10 8 292.291 85.2600 12 -7 10 7 1412.58 162.724 8 -7 10 6 403.774 111.275 8 -7 10 5 572.139 132.086 8 -7 10 4 971.293 168.055 8 7 10 -4 783.512 164.184 7 -7 10 3 1877.10 227.292 8 7 10 -3 1688.75 201.611 7 -7 10 2-113.720 114.327 8 -7 10 1 2406.52 261.241 8 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1201.80 5 -8 -1 5 47217.4 1191.72 5 -8 1 4 5456.27 841.589 1 -8 1 4 5619.02 409.447 5 -8 -1 4 5376.70 413.768 5 -8 -1 4 4174.34 745.487 1 -8 1 3 505.890 273.479 1 -8 1 3 328.169 120.086 5 -8 -1 3 195.263 107.883 5 -8 -1 3 231.274 123.349 4 -8 1 3 242.035 115.747 4 -8 1 2 94.8942 177.524 1 -8 -1 2 160.755 190.970 1 -8 -1 2 308.694 129.417 4 -8 1 2 420.495 115.074 4 -8 -1 1 1074.38 349.678 1 -8 1 1 369.007 294.767 1 -8 -1 1 718.410 167.878 4 -8 1 1 1063.59 191.482 4 8 1 0 6311.15 739.403 9 -8 -1 0 5650.82 759.388 1 -8 -1 0 5371.29 391.477 4 -8 1 0 5546.96 395.411 4 -8 1 -1 8.19326 114.163 2 8 1 1-275.454 317.510 9 8 -1 1-38.3075 249.648 9 -8 -1 -1 8.49063 113.281 4 8 1 2 17548.4 1152.75 9 8 -1 2 18672.8 1057.98 9 -8 1 -2 15632.3 1429.27 2 8 1 3 8204.86 801.682 9 8 -1 3 8233.55 699.727 9 8 1 4 42327.8 1701.43 9 8 -1 4 41938.0 1521.43 9 8 1 5 58897.4 1975.30 9 8 -1 5 59182.6 1783.91 9 8 1 6 1588.18 397.546 9 8 -1 6 1233.28 358.348 9 8 1 7 21312.5 1163.49 9 8 -1 7 20996.7 1058.33 9 8 1 8 138.054 132.706 10 8 1 8 84.6621 222.450 9 8 -1 8 286.859 219.749 9 8 1 9 1843.46 223.780 10 8 1 9 2006.37 345.746 9 8 -1 9 1978.38 330.642 9 8 1 10 712.182 130.661 10 8 1 10 857.291 232.021 9 8 -1 10 712.482 238.079 9 -8 -2 13 422.528 85.8040 11 -8 -2 12 2002.69 204.264 11 -8 2 11 5.77561 100.226 5 -8 -2 11 122.636 106.074 5 -8 2 10-110.946 97.0082 8 -8 2 10-31.7624 107.447 5 -8 -2 10-12.9442 116.033 5 -8 2 9 27.9034 94.4111 8 -8 2 9 295.533 129.103 5 -8 -2 9 250.314 150.483 5 -8 2 8 1994.21 251.964 8 -8 2 8 1628.89 256.470 5 -8 -2 8 1800.53 248.011 5 -8 2 7 31794.1 970.840 5 -8 -2 7 31989.6 977.004 5 -8 2 7 31522.7 924.973 8 -8 2 6 23384.1 830.254 5 -8 -2 6 22702.2 824.338 5 -8 2 6 21736.9 760.066 8 -8 2 5 48.2189 88.3611 8 -8 2 5-20.2408 114.270 5 -8 -2 5 5.82778 123.500 5 -8 -2 4 35275.4 2181.64 1 -8 2 4 35864.3 1023.73 5 -8 -2 4 34805.7 1016.71 5 -8 2 3 10.0090 120.896 5 -8 -2 3-16.7830 135.569 5 -8 2 3 87.7493 111.371 4 -8 -2 3 132.867 188.228 1 -8 -2 2 2962.91 303.261 4 -8 2 2 3205.00 298.575 4 -8 -2 1 35172.9 2008.78 1 -8 -2 1 34680.9 975.591 4 -8 2 1 36000.3 989.884 4 -8 2 0 1192.62 210.898 4 8 2 0 1297.64 397.013 9 8 -2 0 1118.72 305.645 9 -8 -2 0 572.470 278.099 1 -8 -2 0 1227.82 212.289 4 8 2 1 50007.0 2091.55 9 8 -2 1 45057.2 1600.01 9 8 2 2 23660.8 1436.81 9 8 -2 2 22768.2 1102.82 9 -8 -2 -2 19623.1 740.513 4 8 2 3 72403.1 2429.88 9 8 -2 3 67947.5 1857.29 9 8 2 4 55754.6 2100.71 9 8 -2 4 59187.2 1732.08 9 8 -2 5 3630.77 488.493 9 8 2 5 2675.86 472.800 9 8 2 6 52367.1 1930.36 9 8 -2 6 55195.7 1653.42 9 8 2 6 49374.5 1210.47 10 8 2 7 13768.1 969.614 9 8 -2 7 15061.3 855.192 9 8 2 7 13176.7 621.568 10 8 2 8-23.2326 125.534 10 8 2 8-286.067 269.381 9 8 -2 8 323.310 209.947 9 8 -2 9 6840.58 545.374 9 8 2 9 6524.85 381.552 10 8 2 10 522.879 127.526 10 8 -2 10 249.620 170.053 9 -8 -3 13 1920.12 149.634 11 -8 -3 12 3524.44 261.615 11 -8 3 11 726.861 139.778 5 -8 -3 11 576.107 131.676 5 -8 3 10 9185.53 469.206 5 -8 -3 10 8305.56 453.573 5 -8 3 9 29427.1 880.787 5 -8 -3 9 27016.3 848.469 5 -8 3 9 27128.1 840.024 8 -8 3 8 2681.71 286.213 5 -8 -3 8 2537.58 279.506 5 -8 3 8 2724.95 297.789 8 -8 3 7 8009.11 477.991 5 -8 -3 7 6628.34 445.742 5 -8 3 7 6709.03 449.695 8 -8 3 6 725.271 182.845 8 -8 3 6 1011.72 190.773 5 -8 -3 6 760.443 185.144 5 -8 3 5 56296.5 1256.02 5 -8 -3 5 52587.0 1234.62 5 -8 3 5 53673.3 1224.62 8 -8 3 4 974.233 181.360 8 -8 3 4 955.216 191.391 5 -8 -3 4 872.889 178.415 5 -8 -3 3 20031.8 1625.49 1 -8 3 3 19626.3 747.705 5 -8 -3 3 19635.3 767.046 5 -8 3 3 18434.7 709.130 8 -8 3 3 20244.1 728.353 4 -8 3 2 4122.32 336.217 8 -8 -3 2 4043.38 740.045 1 -8 3 2 4565.12 353.408 4 -8 3 1 7217.48 446.809 8 -8 -3 1 7032.24 447.195 4 -8 3 1 7379.60 446.445 4 -8 -3 1 7292.24 921.716 1 -8 3 0 2064.70 251.320 8 -8 -3 0 2149.01 252.604 4 8 -3 1 6278.23 585.296 9 -8 3 -1 5271.99 386.391 8 -8 -3 -1 5094.42 379.329 4 8 3 2 2701.28 519.798 9 8 -3 2 2644.96 379.632 9 -8 -3 -2 2395.36 266.364 4 8 3 3 502.935 321.027 9 8 -3 3 1312.46 314.292 9 -8 -3 -3 920.000 182.900 4 8 3 4 28993.8 1611.96 9 8 -3 4 27771.9 1161.99 9 8 3 5 1649.21 246.653 10 8 3 5 1586.98 441.324 9 8 -3 5 2433.35 393.347 9 8 3 6 640.440 191.822 10 8 3 6 764.345 358.035 9 8 -3 6 1234.62 342.811 9 8 -3 7 4485.31 491.483 9 8 3 7 4132.57 570.067 9 8 3 7 3662.27 343.251 10 8 3 8 108.487 123.902 10 8 3 8-65.8384 219.949 9 8 -3 8 381.234 245.744 9 8 3 9 522.901 143.497 10 8 -3 9 415.555 188.343 9 8 -3 10 5010.72 404.792 9 8 3 10 4973.69 287.473 10 -8 -4 12 334.505 90.1358 11 -8 4 10-43.3885 85.4691 5 -8 -4 10 70.4981 84.6344 5 -8 4 10 12.5095 93.2924 8 -8 4 9 8707.59 453.344 5 -8 -4 9 7943.94 440.988 5 -8 4 9 8525.29 476.461 8 -8 4 8 8356.90 465.016 5 -8 -4 8 8302.88 467.288 5 -8 4 8 8366.01 490.449 8 -8 4 7 4896.19 363.249 5 -8 -4 7 3776.11 330.232 5 -8 4 7 4023.91 346.760 8 -8 4 6 8831.50 481.483 5 -8 -4 6 8436.00 483.297 5 -8 4 6 8487.22 503.511 8 -8 4 5 35333.7 968.374 5 -8 -4 5 33685.1 964.571 5 -8 4 5 33802.6 990.873 8 -8 4 4 9996.12 515.801 5 -8 -4 4 9159.05 513.795 5 -8 4 4 9691.21 536.227 8 -8 4 3 9642.78 510.651 5 -8 -4 3 8062.23 473.638 5 -8 4 3 8312.14 501.634 8 -8 4 2 15423.1 643.138 5 -8 -4 2 14354.8 643.179 5 -8 4 2 14367.0 646.056 8 -8 4 2 14118.0 604.190 4 -8 4 1 399.727 143.339 8 -8 4 1 679.978 170.903 4 -8 4 0 16889.0 693.456 8 -8 -4 0 16497.2 657.069 4 -8 4 0 17932.8 701.718 4 -8 4 -1 1463.03 240.773 8 -8 -4 -1 990.219 188.152 4 8 -4 2 1118.33 284.155 9 8 -4 3 98808.2 2111.10 9 8 4 3 86921.2 1678.44 10 8 4 4 21702.4 1409.43 9 8 -4 4 20233.6 970.156 9 8 4 4 17451.1 760.961 10 8 4 5 44252.7 1934.79 9 8 -4 5 44067.1 1413.26 9 8 -4 6 2457.58 380.831 9 8 4 6 6960.30 509.700 10 8 4 7 1893.72 261.847 10 8 -4 7 2339.36 364.806 9 8 4 8 24.7514 122.690 10 8 -4 8 364.918 212.037 9 8 4 9 958.669 174.315 10 8 -4 9 903.404 203.996 9 8 -4 10 6823.69 434.244 9 8 4 10 6806.26 315.933 10 -8 -5 12 2114.51 176.447 11 -8 -5 11-109.478 82.0765 12 -8 5 10 305.847 120.157 8 -8 5 9 110.044 97.7216 8 -8 -5 8 14506.9 571.918 5 -8 5 8 15360.7 652.680 8 -8 5 7 472.790 149.287 8 -8 5 6 3371.40 330.540 8 -8 5 5 1217.12 217.463 8 -8 5 4 34463.9 1027.70 8 -8 5 3 739.423 187.087 8 -8 5 2 3257.16 332.646 8 -8 5 1 185.106 135.319 8 -8 5 0 1005.92 171.214 4 -8 5 0 819.216 199.990 8 -8 5 -1 7799.35 500.179 8 8 5 1 7035.17 498.173 10 8 5 2 7358.50 506.289 10 8 -5 3 11500.3 715.219 9 8 5 3 9420.18 581.193 10 8 5 4 829.754 246.469 10 8 -5 4 1508.66 308.797 9 8 5 5 1022.30 229.382 10 8 -5 5 1955.62 342.689 9 8 -5 6 3542.47 423.119 9 8 5 6 2989.17 338.195 10 8 -5 7 5019.73 454.812 9 8 5 7 3794.89 352.619 10 8 5 8-37.6524 118.916 10 8 -5 8 223.231 169.579 9 8 5 9 126.366 113.252 10 8 -5 9 251.652 142.888 9 8 -5 10 14829.5 580.455 9 -8 -6 11-1.37464 56.3557 12 -8 6 10 1166.49 164.875 8 -8 6 9 1152.94 181.389 8 -8 6 8 1517.49 223.533 8 -8 6 7-49.1563 118.599 8 -8 6 6 23.1784 120.978 8 -8 6 5 7615.32 493.522 8 -8 6 4 30248.5 963.164 8 -8 6 3-77.9929 133.435 8 -8 6 2 84.2656 133.018 8 -8 6 1 1363.98 232.761 8 -8 6 0-62.6381 125.676 8 -8 6 -1 7246.26 485.661 8 8 6 1 7992.66 526.908 10 8 6 2 186.135 151.438 10 -8 6 -2 411.092 184.579 8 8 6 3 25260.8 941.949 10 8 -6 4 4007.57 419.438 9 8 6 4 3149.85 358.263 10 8 -6 5 8316.86 576.959 9 8 6 5 6557.21 483.260 10 8 -6 6 13754.1 711.786 9 8 6 6 11176.4 586.747 10 8 -6 7 13104.3 657.232 9 8 6 7 11334.8 551.070 10 8 6 8 1185.13 197.855 10 8 -6 8 1035.78 202.385 9 8 -6 9 6170.84 390.906 9 8 6 9 5514.85 297.079 10 -8 7 10 4409.11 265.785 8 -8 -7 10 3991.38 263.042 12 -8 7 9 4354.29 301.313 8 -8 7 8 2934.23 274.771 8 -8 7 7 519.591 156.548 8 -8 7 6 613.082 171.579 8 -8 7 5 506.878 145.177 8 -8 7 4 1094.63 202.800 8 -8 7 3 7234.44 480.741 8 -8 7 2-72.2360 155.557 8 -8 7 1 941.543 200.813 8 -8 7 0 8642.21 518.679 8 -8 7 -1 2654.89 305.082 8 -8 7 -2 1076.49 219.655 8 8 7 2 944.131 215.254 10 -8 7 -3 6294.19 431.323 8 8 7 3 6270.72 480.873 10 8 7 4 4768.28 415.531 10 8 7 5-65.8365 143.576 10 8 -7 5 12.9333 141.463 9 8 7 6 73.4478 145.156 10 8 -7 6 281.400 144.024 9 8 7 7 1369.57 210.254 10 8 -7 7 1172.93 205.299 9 8 7 8 11.9218 92.2277 10 8 -7 8 10.5351 104.841 9 -8 8 10 737.249 99.5768 8 -8 -8 10 566.133 93.9377 12 -8 8 9 1325.25 153.800 8 -8 8 8 1838.77 204.059 8 -8 8 7 10843.8 492.900 8 -8 8 6 10248.0 506.516 8 -8 8 5 8198.33 472.700 8 -8 8 4 596.904 154.883 8 -8 8 3 2317.27 280.568 8 -8 8 2 4002.61 358.255 8 -8 8 1 10518.2 568.865 8 -8 8 0 1472.10 233.606 8 -8 8 -1 5572.93 415.838 8 -8 8 -2 2215.63 277.169 8 -8 8 -3 11516.9 552.014 8 -8 8 -4 2136.14 249.868 8 8 8 4 2607.44 302.935 10 -8 8 -5 4347.21 323.749 8 8 8 5 3995.62 344.686 10 8 8 6-65.4444 123.389 10 -8 8 -6 102.993 85.6655 8 -8 8 -7 2358.75 197.731 8 8 8 7 2421.56 227.185 10 -8 8 -8 327.302 82.6705 8 -8 9 9 443.209 83.6113 8 -8 -9 9 390.649 82.9855 12 -8 9 8 39.3187 66.6283 8 -8 9 7 2675.39 224.239 8 -8 9 6 2565.26 238.935 8 -8 9 5 2710.30 261.342 8 -8 9 4 516.881 147.338 8 -8 9 3 4221.68 333.003 8 -8 9 2 260.525 128.670 8 -8 9 1 321.960 133.150 8 -8 9 0 101.315 121.416 8 -8 9 -1 2312.85 262.620 8 -8 9 -2 217.872 113.850 8 -8 9 -3 101.042 108.343 8 -8 9 -4 688.723 147.902 8 -8 9 -5 2334.37 207.977 8 -8 9 -6 477.626 102.793 8 -8 10 7 79.2729 65.3248 8 -8 10 6-21.2950 71.9222 8 -8 10 5 480.633 110.307 8 -8 10 4 2023.46 206.819 8 -8 10 3 1922.83 210.924 8 -8 10 2 807.432 154.178 8 -8 10 1-15.6730 94.5527 8 -8 10 0 1148.53 178.693 8 -8 10 -1 232.334 105.440 8 -8 10 -2 589.671 129.515 8 -8 10 -3-18.1636 77.4171 8 -8 10 -4-38.7927 65.9963 8 -8 10 -5 295.303 74.7589 8 -8 11 5 2132.00 154.270 8 -8 11 4 880.603 114.749 8 -8 11 3-61.1771 66.0808 8 -8 11 2 110.756 77.9306 8 -8 11 1 147.065 78.0463 8 -8 11 0 1402.19 155.243 8 -8 11 -1 2628.20 195.907 8 -8 11 -2 1163.25 132.703 8 -8 11 -3 352.569 74.1976 8 -9 0 11 68.6428 82.7135 5 -9 0 10 60.4488 99.0368 5 -9 0 9-131.154 138.481 5 -9 0 8 25.9946 129.849 5 -9 0 7-112.980 122.658 5 -9 0 6 7237.18 485.945 5 -9 0 5 9.50080 106.337 5 -9 0 4 21534.0 832.501 5 -9 0 3-21.5489 120.900 5 -9 0 2 6862.05 465.498 4 -9 0 1 206.822 158.191 4 9 0 0-338.845 402.188 9 -9 0 0 38.3951 128.050 4 9 0 1-212.090 346.352 9 -9 0 -1-72.5366 135.908 4 9 0 2 1406.23 340.888 9 -9 0 -2 1877.18 270.072 4 9 0 3-320.861 390.938 9 9 0 4 8829.94 840.323 9 9 0 5 255.819 326.196 9 9 0 6 2040.60 424.245 9 9 0 7-118.341 251.021 9 9 0 8 1733.70 357.889 9 -9 0 -8 2014.47 202.573 4 9 0 9-78.3510 174.121 9 -9 0 -9 74.5039 54.9621 4 -9 1 11 1222.92 167.126 5 -9 -1 11 1305.78 172.908 5 -9 -1 11 1095.54 150.886 11 -9 1 10 579.034 153.969 5 -9 -1 10 459.295 131.420 5 -9 1 9 9933.73 517.872 5 -9 -1 9 9695.17 511.517 5 -9 1 8 27560.2 884.067 5 -9 -1 8 27381.2 887.312 5 -9 1 7 1865.27 258.410 5 -9 -1 7 1947.12 260.369 5 -9 1 6 2130.09 272.766 5 -9 -1 6 2126.20 274.025 5 -9 1 5 17579.6 747.128 5 -9 -1 5 15875.1 715.247 5 -9 1 4 10014.7 569.184 5 -9 -1 4 10660.5 581.927 5 -9 1 3-0.68402 125.404 5 -9 -1 3 34.0537 132.083 5 -9 1 3-92.0192 120.549 4 -9 -1 2 107.079 121.500 4 -9 1 2 299.439 152.711 4 -9 -1 1 194.015 136.692 4 -9 1 1 158.223 147.787 4 9 -1 0 4535.70 693.648 9 -9 -1 0 3576.31 346.777 4 -9 1 0 3766.54 356.302 4 9 1 1 15066.1 1229.69 9 9 -1 1 14263.2 1098.39 9 -9 -1 -1 13087.0 629.705 4 -9 1 -1 12634.8 620.422 4 9 -1 2 22145.7 1311.23 9 -9 -1 -2 19355.9 766.269 4 9 1 3-653.385 487.794 9 9 -1 3-190.875 278.270 9 -9 -1 -3 45.9410 114.448 4 9 -1 4 5394.08 658.040 9 9 1 4 5544.23 735.536 9 -9 -1 -4 4997.30 391.021 4 -9 -1 -5 1635.98 233.950 4 9 1 5 1499.38 427.598 9 9 -1 5 640.751 291.009 9 -9 -1 -6 342.900 135.209 4 9 1 6-1.56220 287.954 9 9 -1 6 265.588 224.280 9 9 1 7 207.198 264.886 9 9 -1 7 79.5121 235.525 9 -9 -1 -7-40.2987 98.2749 4 9 1 8 33.8184 219.048 9 9 -1 8-87.4538 220.689 9 -9 -1 -8-140.455 78.9676 4 9 1 9 2403.67 361.100 9 9 -1 9 1843.53 301.678 9 -9 1 -9 2209.79 183.083 4 -9 -2 12 705.786 99.7295 11 -9 2 11 797.678 133.117 5 -9 -2 11 775.391 141.971 5 -9 2 10 1140.02 172.149 5 -9 -2 10 1271.77 191.785 5 -9 2 9 58.9433 81.6683 8 -9 2 9 263.245 133.359 5 -9 -2 9 255.790 124.807 5 -9 2 8 915.042 169.766 8 -9 2 8 776.815 176.571 5 -9 -2 8 768.906 183.355 5 -9 2 7 1926.54 226.018 8 -9 2 7 1436.95 222.007 5 -9 -2 7 1417.39 227.107 5 -9 2 6 6232.73 431.114 5 -9 -2 6 6468.67 449.447 5 -9 2 5 16399.3 705.611 5 -9 -2 5 15927.4 704.303 5 -9 2 4 47983.5 1201.43 5 -9 -2 4 46521.1 1207.31 5 -9 2 3 38566.7 1083.45 5 -9 -2 3 36599.2 1082.51 5 -9 2 3 37686.7 1044.82 4 -9 2 2 464.128 162.514 5 -9 2 2 449.321 157.082 4 -9 -2 1 3363.38 331.654 4 -9 2 1 3576.46 339.148 4 -9 -2 0 22764.4 823.316 4 -9 2 0 22438.9 830.556 4 -9 2 -1 215.424 143.752 4 9 -2 1-67.5585 358.082 9 -9 -2 -1 277.563 130.537 4 9 2 2 4223.00 713.129 9 9 -2 2 3489.51 543.629 9 -9 -2 -2 2696.13 290.321 4 9 2 3 4342.60 687.880 9 9 -2 3 3467.06 524.032 9 -9 -2 -3 3750.49 340.006 4 9 2 4 1491.99 498.956 9 9 -2 4 1078.05 334.799 9 -9 -2 -4 1129.28 202.797 4 9 -2 5 5807.33 611.769 9 -9 -2 -5 5714.04 379.421 4 9 2 6 3716.70 603.856 9 9 -2 6 3273.51 497.786 9 -9 -2 -6 2896.67 256.743 4 9 2 7 308.759 250.555 9 9 -2 7 270.561 229.016 9 9 2 8 5370.19 558.086 9 9 -2 8 4913.92 492.312 9 9 -2 9 2051.80 309.586 9 -9 -3 12 67.4533 51.7575 11 -9 3 10 3578.37 267.154 5 -9 -3 10 3460.27 266.450 5 -9 3 10 3513.92 251.253 8 -9 3 9 2424.59 244.072 5 -9 -3 9 2096.69 239.185 5 -9 3 9 2532.79 246.226 8 -9 3 8 429.497 128.090 8 -9 3 8 279.137 122.891 5 -9 -3 8 109.556 101.757 5 -9 3 7 2129.28 250.741 8 -9 3 7 1894.51 243.092 5 -9 -3 7 1778.18 241.888 5 -9 3 6 7360.70 455.769 5 -9 -3 6 6985.30 448.258 5 -9 3 6 7111.17 434.392 8 -9 3 5 29643.7 918.089 5 -9 -3 5 29358.0 924.860 5 -9 3 5 30826.3 901.037 8 -9 3 4 6302.91 438.213 5 -9 -3 4 6027.13 437.942 5 -9 3 4 5974.38 404.426 8 -9 3 3 26977.8 892.717 5 -9 -3 3 26270.1 900.037 5 -9 3 3 26355.5 836.885 8 -9 3 3 25985.1 855.703 4 -9 3 2 2406.98 263.250 8 -9 3 2 2154.64 268.734 5 -9 -3 2 2001.94 277.656 5 -9 3 2 1985.16 257.099 4 -9 3 1 84.7820 97.2100 8 -9 3 1 28.2683 130.981 4 -9 -3 0 3803.32 342.093 4 -9 3 0 3926.12 352.090 4 9 -3 1 6676.90 698.530 9 -9 -3 -1 5430.69 406.456 4 -9 3 -1 6215.90 446.329 4 9 -3 2 980.412 330.017 9 -9 -3 -2 1156.60 199.225 4 9 -3 3 15821.7 991.202 9 -9 -3 -3 15032.7 618.602 4 9 3 4 3107.17 612.243 9 9 -3 4 2621.29 424.223 9 -9 -3 -4 2673.28 260.402 4 9 3 5 3049.77 556.932 9 9 -3 5 2775.86 441.660 9 9 -3 6-9.82371 203.290 9 9 -3 7 4648.12 495.891 9 9 -3 8-189.325 198.552 9 9 -3 9 2249.07 300.172 9 -9 4 10 91.9389 77.6179 5 -9 -4 10 178.665 81.5252 5 -9 4 10 319.617 94.2596 8 -9 4 9 2864.84 240.899 5 -9 -4 9 2619.29 240.091 5 -9 4 9 2590.16 239.484 8 -9 4 8 58.8568 104.145 8 -9 4 8 24.6077 83.2504 5 -9 -4 8-72.8587 104.225 5 -9 4 7 4531.84 338.184 5 -9 -4 7 4179.87 332.152 5 -9 4 7 5058.62 372.668 8 -9 4 6 6379.82 403.914 5 -9 -4 6 6104.64 398.310 5 -9 4 6 6353.12 412.654 8 -9 4 5-48.3878 122.536 8 -9 4 5-61.0242 106.033 5 -9 -4 5-36.2804 112.658 5 -9 4 4 580.576 174.499 8 -9 4 4 528.905 138.065 5 -9 -4 4 528.804 159.380 5 -9 4 3 5461.14 389.386 5 -9 -4 3 5760.61 409.393 5 -9 4 3 5357.28 396.217 8 -9 4 2 2430.59 267.465 5 -9 -4 2 2444.33 284.730 5 -9 4 2 2188.45 263.106 8 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138.685 8 -10 7 -1 942.217 157.601 8 -10 7 -2-88.7130 82.8421 8 -10 7 -3 2701.55 225.582 8 -10 7 -4 1266.36 146.174 8 -10 7 -4 970.562 113.839 4 -10 7 -5 461.412 81.8288 8 -10 8 7 5578.46 237.663 8 -10 8 6 1250.35 132.431 8 -10 8 5 2266.47 195.401 8 -10 8 4 355.862 97.1183 8 -10 8 3-126.586 90.1169 8 -10 8 2 8326.27 388.892 8 -10 8 1-83.2566 93.3153 8 -10 8 0 6271.56 334.308 8 -10 8 -1 2875.64 224.326 8 -10 8 -2 17.8830 67.7615 8 -10 8 -3 26453.5 577.023 8 -10 8 -4 6047.62 249.743 8 -10 9 5 2361.38 160.166 8 -10 9 4-76.2240 57.5429 8 -10 9 3 565.741 103.596 8 -10 9 2-112.575 67.4068 8 -10 9 1 6084.01 292.043 8 -10 9 0 324.990 87.5452 8 -10 9 -1 91.1655 60.7257 8 -10 9 -2 1337.67 128.881 8 -11 0 10 145.876 62.9003 5 -11 0 9-51.7128 69.6067 5 -11 0 8 368.877 115.106 5 -11 0 7-87.6896 98.1879 5 -11 0 6 15.8407 97.0822 5 -11 0 5-53.3040 113.885 5 -11 0 4 2432.08 269.728 5 -11 0 3 10.0133 128.693 5 -11 0 2 718.038 179.084 5 -11 0 1-12.8363 138.003 5 -11 0 0 2661.31 298.693 5 -11 0 0 2502.52 282.623 4 -11 0 -1-41.1520 123.104 4 -11 0 -2 819.483 173.070 4 -11 0 -3 56.3211 106.275 4 -11 0 -4 6117.61 351.052 4 -11 0 -5-22.2340 83.6097 4 -11 0 -6 2279.36 174.295 4 -11 1 10 5492.90 238.486 5 -11 -1 10 5293.94 237.571 5 -11 1 9 14.7893 69.6834 5 -11 -1 9 156.982 81.7807 5 -11 1 8 6174.21 335.808 5 -11 -1 8 6137.15 337.246 5 -11 1 7 289.217 118.549 5 -11 -1 7 357.848 125.151 5 -11 1 6 48.6242 91.8533 5 -11 -1 6-18.6098 99.5110 5 -11 1 5 1157.87 193.701 5 -11 -1 5 1432.35 205.639 5 -11 1 4 845.767 189.240 5 -11 -1 4 647.730 168.923 5 -11 1 3 663.663 156.708 5 -11 -1 3 656.818 166.312 5 -11 1 2 937.183 191.724 5 -11 -1 2 753.181 184.048 5 -11 1 1 4934.37 386.757 5 -11 -1 1 4869.71 385.846 5 -11 1 1 4822.14 380.275 4 -11 1 0 1508.40 239.235 5 -11 -1 0 1204.58 207.349 5 -11 1 0 1464.01 218.443 4 -11 -1 -1 2980.04 286.044 4 -11 1 -1 2645.05 273.502 4 -11 -1 -2 6459.24 394.508 4 -11 1 -2 6355.60 402.725 4 -11 -1 -3 1320.96 190.819 4 -11 1 -3 1242.69 182.168 4 -11 -1 -4-41.6214 76.3165 4 -11 1 -4 51.2659 97.7031 4 -11 -1 -5 425.858 103.758 4 -11 1 -5 401.950 99.2481 4 -11 -1 -6 2771.89 173.972 4 -11 1 -6 3221.51 210.877 4 -11 2 9-48.4562 61.2416 5 -11 -2 9 4.25475 57.6588 5 -11 2 8 388.574 98.3127 5 -11 -2 8 487.366 113.875 5 -11 2 7 3336.31 259.892 5 -11 -2 7 3298.82 262.169 5 -11 2 6-9.89841 90.9423 5 -11 -2 6 168.887 104.134 5 -11 2 5 1780.80 217.143 5 -11 -2 5 1671.88 219.736 5 -11 2 4 3543.54 306.454 5 -11 -2 4 3687.31 314.448 5 -11 2 3-56.4942 107.236 5 -11 -2 3 27.5053 111.606 5 -11 2 2 3053.86 295.628 5 -11 -2 2 3476.26 325.937 5 -11 2 1 854.191 170.508 5 -11 -2 1 1034.10 201.502 5 -11 2 1 819.643 166.418 4 -11 2 0 4733.69 357.054 5 -11 -2 0 5117.39 388.262 5 -11 2 0 4692.95 351.783 4 -11 2 -1 577.719 154.156 4 -11 2 -2 527.882 153.155 4 -11 -2 -3 10767.8 459.061 4 -11 2 -3 10792.1 486.784 4 11 -2 4 1966.34 402.058 9 -11 -2 -4 1573.94 168.598 4 -11 2 -4 1429.76 181.207 4 11 -2 5 2211.52 379.331 9 -11 2 -5 1876.15 188.412 4 -11 2 -6 130.120 64.3266 4 -11 -3 9 62.5158 46.1723 5 -11 3 8-21.7708 57.6001 5 -11 -3 8 37.7912 62.6987 5 -11 3 7 265.644 96.8933 5 -11 -3 7 151.147 80.7882 5 -11 3 6 51.1708 77.6940 5 -11 -3 6 238.347 106.190 5 -11 3 5 19.4102 83.3489 5 -11 -3 5-115.695 93.4779 5 -11 3 4 754.932 139.363 5 -11 -3 4 732.648 150.555 5 -11 3 3 2601.65 251.622 5 -11 -3 3 2591.63 262.046 5 -11 3 2 3009.68 276.283 5 -11 -3 2 3264.01 292.813 5 -11 3 1 314.915 127.520 5 -11 -3 1 201.729 109.264 5 -11 3 1 567.139 148.654 4 -11 3 0 536.285 132.264 5 -11 -3 0 792.019 179.551 5 -11 3 0 544.839 149.479 4 -11 3 -1 362.800 127.693 5 -11 -3 -1 185.713 123.777 5 -11 3 -1 261.970 111.540 4 -11 3 -2 5276.99 344.323 4 -11 3 -3 158.510 96.1834 4 11 -3 4 161.092 222.313 9 -11 3 -4 200.975 95.0703 4 11 -3 5 87.9779 189.983 9 -11 3 -5-73.9855 80.0075 4 -11 3 -6 2058.18 156.183 4 -11 -4 8 416.492 81.5340 5 -11 4 7 1123.21 128.849 5 -11 -4 7 1234.75 131.166 5 -11 4 6 2312.85 197.252 5 -11 -4 6 2309.65 201.134 5 -11 4 5 12624.8 458.316 5 -11 -4 5 11809.7 465.057 5 -11 4 4 12576.6 475.214 5 -11 -4 4 12874.4 504.467 5 -11 4 3 2472.33 222.015 5 -11 -4 3 2304.61 226.565 5 -11 4 2 3105.33 250.221 5 -11 -4 2 3560.97 286.069 5 -11 4 1 153.655 95.9351 5 -11 -4 1 314.004 95.3041 5 -11 4 0 1121.65 153.320 5 -11 -4 0 1121.18 180.217 5 -11 4 0 1198.62 172.376 4 -11 4 -1 8.65258 73.2711 5 -11 -4 -1 26.6109 100.296 5 -11 4 -1 66.2406 112.515 4 -11 4 -2 894.804 143.841 5 -11 -4 -2 895.070 153.666 5 -11 4 -2 959.271 158.160 4 -11 4 -3 657.474 123.542 5 -11 -4 -3 644.729 131.529 5 -11 4 -3 681.779 130.682 4 -11 4 -4 1005.84 123.411 5 -11 4 -4 1248.08 154.911 4 -11 -4 -5 9122.81 325.954 5 -11 4 -5 12713.6 403.450 4 -11 4 -6 1745.73 136.401 4 -11 5 6 35281.6 648.170 8 -11 5 5 13371.5 433.689 8 -11 5 4 3658.75 242.195 8 -11 5 3 1782.74 182.038 8 -11 5 2 549.908 111.366 8 -11 -5 2 602.126 119.412 5 -11 5 1 99.2997 69.8904 8 -11 -5 1-49.3774 91.8874 5 -11 -5 0 1064.71 146.724 5 -11 5 -1 171.251 96.2366 4 -11 5 -2 2240.82 197.869 4 -11 5 -3 502.188 105.187 4 -11 5 -4 417.417 95.1581 4 -11 5 -5 648.098 92.6141 4 -11 6 6 2311.52 162.657 8 -11 6 5 9636.67 347.463 8 -11 6 4 138.001 76.7790 8 -11 6 3 30.9286 76.3079 8 -11 6 2 641.779 106.451 8 -11 6 1 205.189 87.6730 8 -11 6 0 2849.52 207.996 8 -11 6 -1 1.69893 69.2448 8 -11 6 -2 1938.52 154.412 8 -11 6 -2 1726.87 148.481 4 -11 6 -3 92.7937 62.6811 4 -11 7 5 8670.28 296.292 8 -11 7 4 107.318 60.5852 8 -11 7 3 417.991 91.2741 8 -11 7 2 141.007 75.3703 8 -11 7 1 35.8184 62.8832 8 -11 7 0 938.048 116.400 8 -11 7 -1-3.26473 55.6790 8 -12 0 8 1018.30 113.395 5 -12 0 7-44.0494 67.1188 5 -12 0 6 5252.02 292.752 5 -12 0 5 8.32498 81.2594 5 -12 0 4 7.75574 91.1575 5 -12 0 3-39.1606 96.4560 5 -12 0 2 43.1758 90.6899 5 -12 0 1 69.2217 100.225 5 -12 0 0 19407.6 628.905 5 -12 0 -1-174.964 101.158 5 -12 0 -2 6542.13 352.265 5 -12 0 -3 38.9171 77.2586 5 -12 0 -4 3390.85 225.469 5 -12 1 8 697.536 91.8247 5 -12 -1 8 619.406 89.0939 5 -12 1 7 1315.38 139.482 5 -12 -1 7 1281.92 143.624 5 -12 1 6 469.027 104.717 5 -12 -1 6 559.369 112.154 5 -12 1 5 57.2237 76.6493 5 -12 -1 5 35.7649 76.8907 5 -12 1 4 642.358 129.716 5 -12 -1 4 1012.07 157.187 5 -12 1 3 1202.14 165.935 5 -12 -1 3 1097.54 165.987 5 -12 1 2 1947.35 210.871 5 -12 -1 2 2194.66 224.998 5 -12 1 1 118.234 99.2984 5 -12 -1 1 185.086 105.328 5 -12 1 0 70.2422 86.9328 5 -12 -1 0 216.236 115.937 5 -12 1 -1 10194.6 439.793 5 -12 -1 -1 10906.1 458.899 5 -12 1 -2 1157.86 156.918 5 -12 -1 -2 1269.86 170.014 5 -12 1 -3 450.606 101.439 5 -12 -1 -3 325.988 99.1301 5 -12 1 -3 421.116 99.2622 4 -12 1 -4 143.808 76.3556 5 -12 -1 -4 59.4921 64.3481 5 -12 1 -4 52.3299 60.3106 4 -12 2 7 8599.71 311.558 5 -12 -2 7 8790.29 322.710 5 -12 2 6 257.021 80.0940 5 -12 -2 6 346.348 93.5576 5 -12 2 5 232.312 86.0557 5 -12 -2 5 235.416 95.2019 5 -12 2 4 422.806 107.001 5 -12 -2 4 432.574 120.531 5 -12 2 3 1955.11 197.561 5 -12 -2 3 2051.74 201.117 5 -12 2 2 2918.24 239.969 5 -12 -2 2 3073.22 251.696 5 -12 2 1 6341.53 347.342 5 -12 -2 1 6066.29 347.539 5 -12 2 0 1072.32 154.682 5 -12 -2 0 1024.41 154.966 5 -12 2 -1 14316.0 491.020 5 -12 -2 -1 15213.5 524.591 5 -12 2 -2 3579.72 242.981 5 -12 -2 -2 3731.19 258.889 5 -12 2 -2 3818.14 253.685 4 -12 2 -3 8058.03 328.349 5 -12 -2 -3 8356.64 346.787 5 -12 2 -3 8928.46 354.195 4 -12 2 -4 5187.64 234.365 5 -12 -2 -4 5066.43 250.611 5 -12 2 -4 5865.47 259.002 4 -12 3 6 7366.46 284.447 5 -12 -3 6 7715.05 304.717 5 -12 3 5 62.6238 65.4091 5 -12 -3 5 86.2808 70.0469 5 -12 3 4 841.958 128.610 5 -12 -3 4 917.864 135.038 5 -12 3 3-199.857 80.4166 5 -12 -3 3 30.9840 71.0051 5 -12 3 2 1688.94 170.978 5 -12 -3 2 1957.77 189.677 5 -12 3 1-18.2679 72.2369 5 -12 -3 1 32.3988 75.6028 5 -12 3 0 124.787 83.5304 5 -12 -3 0-44.1864 74.0161 5 -12 3 -1 21.8053 60.9431 5 -12 -3 -1 129.150 73.2065 5 -12 3 -2 3365.33 205.223 5 -12 -3 -2 4050.38 241.100 5 -12 3 -2 3805.47 240.161 4 -12 3 -3 783.173 93.9377 5 -12 -3 -3 951.915 116.329 5 -12 3 -3 946.850 119.301 4 -12 3 -4 32.6087 50.0197 4 -12 -4 5 43.4701 44.7632 5 -12 -4 4 3111.51 192.696 5 -12 4 3 1239.58 125.058 5 -12 -4 3 1323.19 137.938 5 -12 -4 2 1400.79 143.476 5 -12 4 2 979.311 112.542 5 -12 4 1 4538.92 228.234 5 -12 -4 1 4920.02 257.250 5 -12 -4 0 1496.11 144.044 5 -12 -4 -1 2989.35 191.603 5 -13 0 4 66.9689 51.7246 5 -13 0 3-34.5494 59.2457 5 -13 0 2 216.542 66.5726 5 -13 0 1 56.5094 62.5976 5 -13 0 0 222.342 67.0412 5 -13 0 -1 44.1232 44.5807 5 -13 -1 4 960.921 106.785 5 -13 1 4 800.607 98.0007 5 -13 1 3 6998.95 275.321 5 -13 -1 3 7597.73 290.745 5 -13 1 2 2277.41 164.013 5 -13 -1 2 2185.32 163.829 5 -13 1 1 142.374 63.8717 5 -13 -1 1 206.803 68.1489 5 -13 1 0 2845.53 174.579 5 -13 -1 0 2800.63 179.308 5 -13 -2 2 3564.40 191.478 5 -13 -2 1 587.546 87.5753 5 0 0 0 0.00 0.00 0 TITL batch3_2b in P2(1)/c REM P2(1)/c (#14 in standard setting) CELL 1.54184 10.619773 12.010778 12.576099 90.0000 96.7157 90.0000 ZERR 2.00 0.000264 0.000324 0.000300 0.0000 0.0023 0.0000 LATT 1 SYMM -x, y+1/2,-z+1/2 SFAC C H N O UNIT 76.00 76.00 4.00 12.00 TREF HKLF 4 END ; _shelx_hkl_checksum 49318 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 2.825 _oxdiff_exptl_absorpt_empirical_full_min 0.807 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn O16 O 0.19456(12) 0.49097(11) 0.77997(9) 0.0415(3) Uani 1 1 d . O17 O 0.29342(10) 0.37084(10) 0.68429(8) 0.0294(2) Uani 1 1 d . H17 H 0.350(2) 0.3623(19) 0.7475(17) 0.044 Uiso 1 1 d R C1 C 0.37162(14) 0.58240(13) 0.43611(13) 0.0304(3) Uani 1 1 d . H1 H 0.455005 0.611921 0.448955 0.036 Uiso 1 1 calc R C2 C 0.31253(15) 0.57379(13) 0.33203(12) 0.0310(3) Uani 1 1 d . H2 H 0.355380 0.596563 0.273478 0.037 Uiso 1 1 calc R C3 C 0.19015(14) 0.53154(13) 0.31430(11) 0.0266(3) Uani 1 1 d . H3 H 0.149010 0.526280 0.243222 0.032 Uiso 1 1 calc R C4 C 0.12704(12) 0.49682(11) 0.39945(10) 0.0204(3) Uani 1 1 d . C5 C -0.00553(12) 0.44973(11) 0.38286(9) 0.0198(3) Uani 1 1 d . H5 H -0.023238 0.427008 0.306070 0.024 Uiso 1 1 calc R C6 C -0.00689(12) 0.34579(11) 0.45019(10) 0.0199(3) Uani 1 1 d . C7 C -0.06158(12) 0.24718(12) 0.40925(11) 0.0234(3) Uani 1 1 d . H7 H -0.099140 0.243963 0.336949 0.028 Uiso 1 1 calc R C8 C -0.06136(14) 0.15327(12) 0.47401(12) 0.0262(3) Uani 1 1 d . H8 H -0.096529 0.085348 0.445465 0.031 Uiso 1 1 calc R C9 C -0.00960(14) 0.15908(12) 0.58051(11) 0.0264(3) Uani 1 1 d . H9 H -0.012548 0.095939 0.625647 0.032 Uiso 1 1 calc R C10 C 0.04658(13) 0.25726(12) 0.62123(11) 0.0237(3) Uani 1 1 d . H10 H 0.082216 0.260635 0.694048 0.028 Uiso 1 1 calc R C11 C 0.05096(12) 0.35032(11) 0.55622(10) 0.0196(3) Uani 1 1 d . C12 C 0.11225(12) 0.46143(11) 0.59342(9) 0.0193(3) Uani 1 1 d . C13 C 0.18775(12) 0.50326(11) 0.50419(10) 0.0204(3) Uani 1 1 d . C14 C 0.30926(13) 0.54798(12) 0.52172(11) 0.0256(3) Uani 1 1 d . H14 H 0.349997 0.555078 0.592771 0.031 Uiso 1 1 calc R C15 C 0.20364(13) 0.44367(12) 0.69680(10) 0.0221(3) Uani 1 1 d . O18 O 0.54254(10) 0.84219(10) 0.65245(8) 0.0317(3) Uani 1 1 d . N21 N 0.49175(12) 0.85263(12) 0.47522(10) 0.0299(3) Uani 1 1 d . C19 C 0.57453(13) 0.83166(13) 0.56064(12) 0.0269(3) Uani 1 1 d . C20 C 0.70577(16) 0.79321(19) 0.54596(15) 0.0461(5) Uani 1 1 d . H20A H 0.700767 0.733064 0.492983 0.069 Uiso 1 1 calc GR H20B H 0.748205 0.765930 0.614394 0.069 Uiso 1 1 calc GR H20C H 0.754080 0.855531 0.520921 0.069 Uiso 1 1 calc GR C22 C 0.5202(2) 0.85016(17) 0.36478(13) 0.0450(4) Uani 1 1 d . H22A H 0.610925 0.835929 0.363515 0.067 Uiso 1 1 calc GR H22B H 0.498006 0.921981 0.330664 0.067 Uiso 1 1 calc GR H22C H 0.470987 0.790889 0.325830 0.067 Uiso 1 1 calc GR C23 C 0.36063(15) 0.87818(16) 0.49007(14) 0.0385(4) Uani 1 1 d . H23A H 0.311825 0.808907 0.489801 0.058 Uiso 1 1 calc GR H23B H 0.323639 0.926368 0.431720 0.058 Uiso 1 1 calc GR H23C H 0.358354 0.916407 0.558659 0.058 Uiso 1 1 calc GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O16 0.0450(7) 0.0538(8) 0.0219(5) -0.0122(5) -0.0119(5) 0.0206(6) O17 0.0276(5) 0.0360(6) 0.0223(5) -0.0017(4) -0.0065(4) 0.0102(4) C1 0.0236(7) 0.0303(8) 0.0374(8) 0.0020(6) 0.0044(6) -0.0021(6) C2 0.0307(7) 0.0334(8) 0.0305(7) 0.0039(6) 0.0108(6) -0.0017(6) C3 0.0299(7) 0.0304(7) 0.0199(6) 0.0018(5) 0.0044(5) 0.0021(6) C4 0.0220(6) 0.0199(6) 0.0188(6) 0.0002(5) 0.0012(5) 0.0036(5) C5 0.0212(6) 0.0228(6) 0.0147(6) -0.0007(5) -0.0007(5) 0.0026(5) C6 0.0191(6) 0.0221(6) 0.0183(6) -0.0006(5) 0.0011(5) 0.0033(5) C7 0.0229(6) 0.0271(7) 0.0199(6) -0.0036(5) 0.0014(5) 0.0004(5) C8 0.0272(7) 0.0230(7) 0.0286(7) -0.0039(5) 0.0036(5) -0.0019(5) C9 0.0302(7) 0.0235(7) 0.0260(7) 0.0039(5) 0.0060(6) 0.0010(6) C10 0.0253(6) 0.0269(7) 0.0189(6) 0.0003(5) 0.0027(5) 0.0020(5) C11 0.0182(6) 0.0227(7) 0.0178(6) -0.0018(5) 0.0014(5) 0.0025(5) C12 0.0199(6) 0.0224(6) 0.0147(6) -0.0002(5) -0.0011(5) 0.0029(5) C13 0.0209(6) 0.0205(6) 0.0196(6) 0.0000(5) 0.0010(5) 0.0041(5) C14 0.0233(6) 0.0267(7) 0.0257(6) -0.0007(5) -0.0019(5) 0.0002(5) C15 0.0228(6) 0.0246(7) 0.0177(6) -0.0002(5) -0.0025(5) 0.0014(5) O18 0.0243(5) 0.0449(7) 0.0246(5) -0.0052(4) -0.0024(4) -0.0001(5) N21 0.0294(6) 0.0338(7) 0.0254(6) -0.0019(5) -0.0009(5) 0.0003(5) C19 0.0229(7) 0.0280(7) 0.0291(7) -0.0072(5) 0.0003(5) -0.0014(6) C20 0.0269(8) 0.0631(12) 0.0475(10) -0.0231(9) 0.0008(7) 0.0078(8) C22 0.0613(12) 0.0472(10) 0.0267(8) -0.0003(7) 0.0064(8) 0.0002(9) C23 0.0273(7) 0.0450(10) 0.0405(9) -0.0016(7) -0.0081(6) 0.0058(7) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 -1 1 0.0301 0 1 -1 0.0301 0 -1 -1 0.0536 0 1 1 0.0536 1 0 0 0.0197 -1 0 0 0.0197 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C15 O17 H17 111.8(13) . . C2 C1 H1 119.9 . . C2 C1 C14 120.27(14) . . C14 C1 H1 119.9 . . C1 C2 H2 120.3 . . C1 C2 C3 119.35(13) . . C3 C2 H2 120.3 . . C2 C3 H3 119.6 . . C2 C3 C4 120.77(13) . . C4 C3 H3 119.6 . . C3 C4 C5 122.09(12) . . C3 C4 C13 119.83(13) . . C13 C4 C5 118.07(12) . . C4 C5 H5 107.6 . . C4 C5 C6 107.60(10) . . C4 C5 C12 113.06(11) . 3_566 C6 C5 H5 107.6 . . C6 C5 C12 113.02(10) . 3_566 C12 C5 H5 107.6 3_566 . C7 C6 C5 121.84(12) . . C7 C6 C11 120.16(12) . . C11 C6 C5 118.00(12) . . C6 C7 H7 119.9 . . C8 C7 C6 120.11(12) . . C8 C7 H7 119.9 . . C7 C8 H8 120.1 . . C9 C8 C7 119.82(13) . . C9 C8 H8 120.1 . . C8 C9 H9 119.9 . . C8 C9 C10 120.11(13) . . C10 C9 H9 119.9 . . C9 C10 H10 119.7 . . C11 C10 C9 120.51(12) . . C11 C10 H10 119.7 . . C6 C11 C12 116.54(12) . . C10 C11 C6 119.17(12) . . C10 C11 C12 124.26(12) . . C11 C12 C5 110.51(10) . 3_566 C11 C12 C13 107.49(10) . . C11 C12 C15 109.84(11) . . C13 C12 C5 110.92(10) . 3_566 C13 C12 C15 109.25(10) . . C15 C12 C5 108.81(10) . 3_566 C4 C13 C12 116.53(12) . . C14 C13 C4 119.15(12) . . C14 C13 C12 124.30(12) . . C1 C14 C13 120.58(13) . . C1 C14 H14 119.7 . . C13 C14 H14 119.7 . . O16 C15 O17 123.36(12) . . O16 C15 C12 124.07(13) . . O17 C15 C12 112.57(11) . . C19 N21 C22 125.11(14) . . C19 N21 C23 119.14(13) . . C22 N21 C23 115.74(14) . . O18 C19 N21 120.17(13) . . O18 C19 C20 120.17(14) . . N21 C19 C20 119.65(14) . . C19 C20 H20A 109.5 . . C19 C20 H20B 109.5 . . C19 C20 H20C 109.5 . . H20A C20 H20B 109.5 . . H20A C20 H20C 109.5 . . H20B C20 H20C 109.5 . . N21 C22 H22A 109.5 . . N21 C22 H22B 109.5 . . N21 C22 H22C 109.5 . . H22A C22 H22B 109.5 . . H22A C22 H22C 109.5 . . H22B C22 H22C 109.5 . . N21 C23 H23A 109.5 . . N21 C23 H23B 109.5 . . N21 C23 H23C 109.5 . . H23A C23 H23B 109.5 . . H23A C23 H23C 109.5 . . H23B C23 H23C 109.5 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 O16 C15 1.2041(18) . O17 H17 0.95(2) . O17 C15 1.3168(18) . C1 H1 0.9500 . C1 C2 1.388(2) . C1 C14 1.391(2) . C2 H2 0.9500 . C2 C3 1.389(2) . C3 H3 0.9500 . C3 C4 1.3919(19) . C4 C5 1.5089(18) . C4 C13 1.3994(18) . C5 H5 1.0000 . C5 C6 1.5095(18) . C5 C12 1.6097(17) 3_566 C6 C7 1.3912(19) . C6 C11 1.4024(18) . C7 H7 0.9500 . C7 C8 1.391(2) . C8 H8 0.9500 . C8 C9 1.389(2) . C9 H9 0.9500 . C9 C10 1.392(2) . C10 H10 0.9500 . C10 C11 1.3888(19) . C11 C12 1.5337(18) . C12 C13 1.5379(17) . C12 C15 1.5436(17) . C13 C14 1.3912(19) . C14 H14 0.9500 . O18 C19 1.2475(18) . N21 C19 1.330(2) . N21 C22 1.456(2) . N21 C23 1.459(2) . C19 C20 1.500(2) . C20 H20A 0.9800 . C20 H20B 0.9800 . C20 H20C 0.9800 . C22 H22A 0.9800 . C22 H22B 0.9800 . C22 H22C 0.9800 . C23 H23A 0.9800 . C23 H23B 0.9800 . C23 H23C 0.9800 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_4 C1 C2 C3 C4 -0.7(2) . . C2 C1 C14 C13 0.8(2) . . C2 C3 C4 C5 -179.52(13) . . C2 C3 C4 C13 -0.7(2) . . C3 C4 C5 C6 133.48(13) . . C3 C4 C5 C12 -100.99(14) . 3_566 C3 C4 C13 C12 -179.02(12) . . C3 C4 C13 C14 2.1(2) . . C4 C5 C6 C7 -133.09(13) . . C4 C5 C6 C11 45.89(15) . . C4 C13 C14 C1 -2.2(2) . . C5 C4 C13 C12 -0.16(18) . . C5 C4 C13 C14 -179.00(12) . . C5 C6 C7 C8 -179.74(12) . . C5 C6 C11 C10 177.42(11) . . C5 C6 C11 C12 -0.78(17) . . C5 C12 C13 C4 -75.78(14) 3_566 . C5 C12 C13 C14 103.00(14) 3_566 . C5 C12 C15 O16 -0.8(2) 3_566 . C5 C12 C15 O17 179.32(11) 3_566 . C6 C7 C8 C9 1.8(2) . . C6 C11 C12 C5 76.59(13) . 3_566 C6 C11 C12 C13 -44.59(15) . . C6 C11 C12 C15 -163.34(11) . . C7 C6 C11 C10 -3.59(19) . . C7 C6 C11 C12 178.21(11) . . C7 C8 C9 C10 -2.6(2) . . C8 C9 C10 C11 0.3(2) . . C9 C10 C11 C6 2.8(2) . . C9 C10 C11 C12 -179.17(12) . . C10 C11 C12 C5 -101.51(14) . 3_566 C10 C11 C12 C13 137.32(13) . . C10 C11 C12 C15 18.56(17) . . C11 C6 C7 C8 1.3(2) . . C11 C12 C13 C4 45.14(15) . . C11 C12 C13 C14 -136.08(13) . . C11 C12 C15 O16 -121.86(16) . . C11 C12 C15 O17 58.23(15) . . C12 C5 C6 C7 101.36(14) 3_566 . C12 C5 C6 C11 -79.66(14) 3_566 . C12 C13 C14 C1 179.05(13) . . C13 C4 C5 C6 -45.35(15) . . C13 C4 C5 C12 80.18(14) . 3_566 C13 C12 C15 O16 120.47(16) . . C13 C12 C15 O17 -59.44(15) . . C14 C1 C2 C3 0.6(2) . . C15 C12 C13 C4 164.28(12) . . C15 C12 C13 C14 -16.95(18) . . C22 N21 C19 O18 175.88(16) . . C22 N21 C19 C20 -5.3(3) . . C23 N21 C19 O18 -5.5(2) . . C23 N21 C19 C20 173.38(16) . . loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -0.0006 -0.9994 1.0002 -0.1476 0.0678 0.0726 0.0006 0.9994 -1.0002 0.1476 -0.0678 -0.0726 0.0004 -1.0000 -0.9981 -0.0555 0.0647 -0.1559 -0.0004 1.0000 0.9981 0.0555 -0.0647 0.1559 0.9993 -0.0003 0.0013 -0.0763 -0.1241 -0.0106 -0.9993 0.0003 -0.0013 0.0763 0.1241 0.0106