Crystallography Open Database

Information card for entry 4305297

Preview

Coordinates	4305297.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H34 F6 N4 O2 P Ru
Calculated formula	C32 H34 F6 N4 O2 P Ru
Title of publication	General Synthesis of (Salen)ruthenium(III) Complexes via N...N Coupling of (Salen)ruthenium(VI) Nitrides
Authors of publication	Wai-Lun Man; Hoi-Ki Kwong; William W. Y. Lam; Jing Xiang; Tsz-Wing Wong; Wing-Hong Lam; Wing-Tak Wong; Shie-Ming Peng; Tai-Chu Lau
Journal of publication	Inorganic Chemistry
Year of publication	2008
Journal volume	47
Pages of publication	5936 - 5944
a	21.166 ± 0.003 Å
b	21.166 ± 0.003 Å
c	14.369 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	6437.3 ± 1.9 Å³
Cell temperature	300 ± 2 K
Ambient diffraction temperature	300 ± 2 K
Number of distinct elements	7
Space group number	86
Hermann-Mauguin space group symbol	P 42/n :2
Hall space group symbol	-P 4bc
Residual factor for all reflections	0.1298
Residual factor for significantly intense reflections	0.0762
Weighted residual factors for significantly intense reflections	0.2047
Weighted residual factors for all reflections included in the refinement	0.2439
Goodness-of-fit parameter for all reflections included in the refinement	1.043
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179090 (current)	2016-03-23	cif/4/30/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/30/52.	4305297.cif
120081	2014-07-12	Adding DOIs to range 4/30 structures.	4305297.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4305297.cif
1167	2010-05-13	cif/ Adding data from the rest of 2009 RSC journals, Inorg-Chem-2008 and Chem-Comm-2010_18-19.	4305297.cif