Crystallography Open Database

Information card for entry 4316842

Preview

Coordinates	4316842.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H82 In6 N18 Ni3 O2 S18 Sb4
Calculated formula	C24 H78 In6 N18 Ni2.996 O2 S18 Sb4
Title of publication	Two Novel Thioindate-Thioantimonate Compounds [Ni(dien)2]2In2Sb4S11 and [Ni(dien)2]3(In3Sb2S9)2.2H2O with Transition Metal Complexes
Authors of publication	Jian Zhou; Xian-Hong Yin; Feng Zhang
Journal of publication	Inorganic Chemistry
Year of publication	2010
Journal volume	49
Pages of publication	9671 - 9676
a	25.508 ± 0.005 Å
b	13.194 ± 0.003 Å
c	21.653 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	7287 ± 3 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	8
Space group number	60
Hermann-Mauguin space group symbol	P b c n
Hall space group symbol	-P 2n 2ab
Residual factor for all reflections	0.0931
Residual factor for significantly intense reflections	0.0611
Weighted residual factors for significantly intense reflections	0.1386
Weighted residual factors for all reflections included in the refinement	0.1541
Goodness-of-fit parameter for all reflections included in the refinement	1.054
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4316842.cif
91935	2013-12-29	cod/ (saulius@koala.ibt.lt) Adding DOIs that could be assigned unambiguously to the rest of COD CIFs.	4316842.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4316842.cif
10351	2011-02-11	../uploads/cif-deposit/cod/cif Adding structures of 4316842 via cif-deposit CGI script.	4316842.cif