#------------------------------------------------------------------------------ #$Date: 2019-11-10 07:51:07 +0200 (Sun, 10 Nov 2019) $ #$Revision: 225914 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/57/4515798.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4515798 loop_ _publ_author_name 'He, Jian' 'Chen, Caiyou' 'Fu, Gregory C.' 'Peters, Jonas C.' _publ_section_title ; Visible-Light-Induced, Copper-Catalyzed Three-Component Coupling of Alkyl Halides, Olefins, and Trifluoromethylthiolate to Generate Trifluoromethyl Thioethers. ; _journal_issue 12 _journal_name_full 'ACS catalysis' _journal_page_first 11741 _journal_page_last 11748 _journal_paper_doi 10.1021/acscatal.8b04094 _journal_volume 8 _journal_year 2018 _chemical_formula_moiety 'C90 H64 Cu2 F6 P4 S2' _chemical_formula_sum 'C90 H64 Cu2 F6 P4 S2' _chemical_formula_weight 1574.49 _chemical_name_systematic (BINAP)CuSCF3 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_date 2017-12-11 _audit_creation_method ; Olex2 1.2 (compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381) ; _cell_angle_alpha 101.643(4) _cell_angle_beta 97.123(4) _cell_angle_gamma 109.481(4) _cell_formula_units_Z 1 _cell_length_a 11.1442(12) _cell_length_b 12.9041(13) _cell_length_c 13.9829(14) _cell_measurement_reflns_used 9021 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 42.66 _cell_measurement_theta_min 2.57 _cell_volume 1816.4(3) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0486 _diffrn_reflns_av_unetI/netI 0.0336 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 21 _diffrn_reflns_limit_h_min -21 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 200649 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 42.105 _diffrn_reflns_theta_min 2.097 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.795 _exptl_absorpt_correction_T_max 0.7487 _exptl_absorpt_correction_T_min 0.7082 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0662 before and 0.0526 after correction. The Ratio of minimum to maximum transmission is 0.9459. The \l/2 correction factor is Not present.' _exptl_crystal_colour 'clear yellow' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.439 _exptl_crystal_description block _exptl_crystal_F_000 808 _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.18 _exptl_crystal_size_min 0.14 _refine_diff_density_max 2.447 _refine_diff_density_min -0.734 _refine_diff_density_rms 0.128 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.055 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 469 _refine_ls_number_reflns 25546 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.055 _refine_ls_R_factor_all 0.0618 _refine_ls_R_factor_gt 0.0405 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0551P)^2^+0.8397P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1041 _refine_ls_wR_factor_ref 0.1151 _reflns_Friedel_coverage 0.000 _reflns_number_gt 19850 _reflns_number_total 25546 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs8b04094_si_002.cif _cod_data_source_block p17316_cut_p53a_a _cod_database_code 4515798 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.897 _shelx_estimated_absorpt_t_min 0.851 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2.a Aromatic/amide H refined with riding coordinates: C43(H43), C12(H12), C9(H9), C16(H16), C11(H11), C35(H35), C23(H23), C28(H28), C44(H44), C45(H45), C6(H6), C39(H39), C22(H22), C42(H42), C21(H21), C15(H15), C13(H13), C29(H29), C4(H4), C33(H33), C10(H10), C19(H19), C38(H38), C5(H5), C25(H25), C7(H7), C3(H3), C18(H18), C24(H24), C32(H32), C17(H17), C34(H34) ; _shelx_res_file ; p17316_cut_p53a_a.res created by SHELXL-2014/7 TITL p17316_cut_p53A_a.res in P-1 REM Old TITL p17316_cut_p53A in P-1 REM SHELXT solution in P-1 REM R1 0.102, Rweak 0.006, Alpha 0.074, Orientation as input REM Formula found by SHELXT: C47 F3 S3 Cu CELL 0.71073 11.1442 12.9041 13.9829 101.643 97.123 109.481 ZERR 1 0.0012 0.0013 0.0014 0.004 0.004 0.004 LATT 1 SFAC C H Cu F P S UNIT 90 64 2 6 4 2 L.S. 10 PLAN 20 SIZE 0.14 0.18 0.21 TEMP -173(2) BOND $H LIST 6 fmap 2 ABIN ACTA REM REM REM WGHT 0.055100 0.839700 FVAR 0.53751 CU1 3 0.526929 0.586487 0.123781 11.00000 0.00895 0.01104 = 0.01129 -0.00111 0.00118 0.00350 S1 6 0.447761 0.390861 0.045981 11.00000 0.01433 0.01008 = 0.01127 0.00159 0.00202 0.00474 P1 5 0.736223 0.688507 0.210805 11.00000 0.00771 0.01288 = 0.00940 -0.00087 0.00092 0.00408 P2 5 0.422707 0.668638 0.230077 11.00000 0.00736 0.00892 = 0.00971 0.00110 0.00170 0.00308 F2 4 0.480644 0.207532 0.074462 11.00000 0.04960 0.01292 = 0.02143 0.00717 0.01239 0.01463 F1 4 0.502469 0.332984 0.209414 11.00000 0.03959 0.02354 = 0.01304 0.00683 0.00619 0.01488 F3 4 0.655234 0.357204 0.126251 11.00000 0.02209 0.03733 = 0.03968 0.02089 0.00621 0.01763 C43 1 0.641319 1.145383 0.434779 11.00000 0.02598 0.01305 = 0.01988 -0.00057 -0.00053 0.01034 AFIX 43 H43 2 0.613329 1.177288 0.491089 11.00000 -1.20000 AFIX 0 C12 1 0.984591 0.719241 0.468570 11.00000 0.01940 0.02167 = 0.01689 0.00036 -0.00488 0.00887 AFIX 43 H12 2 1.067499 0.770146 0.506876 11.00000 -1.20000 AFIX 0 C9 1 0.740678 0.570653 0.356553 11.00000 0.01641 0.01630 = 0.01390 0.00128 0.00336 0.00530 AFIX 43 H9 2 0.657366 0.519932 0.318832 11.00000 -1.20000 AFIX 0 C16 1 0.358637 0.970276 0.278248 11.00000 0.01730 0.01200 = 0.02394 0.00251 0.00162 0.00745 AFIX 43 H16 2 0.335455 1.016587 0.328869 11.00000 -1.20000 AFIX 0 C11 1 0.917680 0.622105 0.497181 11.00000 0.02920 0.02418 = 0.01542 0.00460 0.00039 0.01476 AFIX 43 H11 2 0.955181 0.606305 0.554689 11.00000 -1.20000 AFIX 0 C35 1 0.741786 0.782739 0.650357 11.00000 0.01685 0.01579 = 0.01110 0.00462 0.00124 0.00544 AFIX 43 H35 2 0.709709 0.737541 0.694159 11.00000 -1.20000 AFIX 0 C23 1 0.021904 0.417194 0.245859 11.00000 0.01193 0.02455 = 0.02455 0.01190 0.00396 0.00065 AFIX 43 H23 2 -0.059829 0.363858 0.248167 11.00000 -1.20000 AFIX 0 C40 1 0.726723 1.053519 0.269471 11.00000 0.01454 0.01194 = 0.01960 0.00687 0.00251 0.00236 C28 1 0.474949 0.643445 0.424986 11.00000 0.01033 0.01106 = 0.01230 0.00336 0.00204 0.00253 AFIX 43 H28 2 0.394407 0.580645 0.403264 11.00000 -1.20000 AFIX 0 C44 1 0.676791 1.207839 0.363960 11.00000 0.02862 0.01059 = 0.02793 0.00313 -0.00261 0.00727 AFIX 43 H44 2 0.671724 1.281070 0.372306 11.00000 -1.20000 AFIX 0 C14 1 0.400494 0.798935 0.215865 11.00000 0.00950 0.01098 = 0.01218 0.00313 0.00217 0.00402 C45 1 0.718414 1.162819 0.283409 11.00000 0.02296 0.01239 = 0.02834 0.00931 0.00170 0.00345 AFIX 43 H45 2 0.742152 1.205267 0.236017 11.00000 -1.20000 AFIX 0 C20 1 0.263033 0.574028 0.239578 11.00000 0.00831 0.01146 = 0.01215 0.00267 0.00169 0.00291 C6 1 1.074688 0.775655 0.101173 11.00000 0.00992 0.03690 = 0.02270 -0.00348 0.00408 0.00351 AFIX 43 H6 2 1.156345 0.836744 0.115373 11.00000 -1.20000 AFIX 0 C36 1 0.691132 0.876047 0.322568 11.00000 0.00912 0.00942 = 0.00933 0.00172 0.00189 0.00247 C39 1 0.766998 1.005309 0.185299 11.00000 0.01973 0.02079 = 0.02088 0.01264 0.00815 0.00613 AFIX 43 H39 2 0.789778 1.046943 0.137207 11.00000 -1.20000 AFIX 0 C27 1 0.519135 0.711994 0.359041 11.00000 0.00911 0.00893 = 0.00932 0.00170 0.00208 0.00358 C22 1 0.124122 0.381268 0.229698 11.00000 0.01414 0.01662 = 0.03321 0.01247 0.00119 0.00150 AFIX 43 H22 2 0.112129 0.303307 0.221315 11.00000 -1.20000 AFIX 0 C42 1 0.646910 1.038735 0.423002 11.00000 0.01788 0.01117 = 0.01473 0.00090 0.00186 0.00639 AFIX 43 H42 2 0.622316 0.997727 0.471206 11.00000 -1.20000 AFIX 0 C21 1 0.243712 0.458961 0.225768 11.00000 0.01147 0.01279 = 0.02489 0.00701 0.00225 0.00384 AFIX 43 H21 2 0.312601 0.433619 0.213627 11.00000 -1.20000 AFIX 0 C15 1 0.367856 0.868754 0.290189 11.00000 0.01628 0.01259 = 0.01447 0.00221 0.00236 0.00723 AFIX 43 H15 2 0.351811 0.846427 0.349533 11.00000 -1.20000 AFIX 0 C13 1 0.929926 0.741620 0.383907 11.00000 0.01503 0.01393 = 0.01626 0.00072 -0.00294 0.00496 AFIX 43 H13 2 0.975916 0.807829 0.364484 11.00000 -1.20000 AFIX 0 C29 1 0.546111 0.666094 0.519170 11.00000 0.01251 0.01265 = 0.01252 0.00480 0.00270 0.00373 AFIX 43 H29 2 0.514578 0.618728 0.561535 11.00000 -1.20000 AFIX 0 C4 1 0.928805 0.591258 0.002964 11.00000 0.01627 0.02796 = 0.01332 -0.00112 0.00207 0.01269 AFIX 43 H4 2 0.910173 0.525751 -0.050279 11.00000 -1.20000 AFIX 0 C41 1 0.689019 0.988961 0.339623 11.00000 0.01139 0.00944 = 0.01293 0.00255 0.00143 0.00285 C33 1 0.908015 0.939195 0.617568 11.00000 0.01394 0.01261 = 0.01178 -0.00034 -0.00033 0.00289 AFIX 43 H33 2 0.990737 0.999332 0.639217 11.00000 -1.20000 AFIX 0 C26 1 0.638090 0.803473 0.390417 11.00000 0.00944 0.00881 = 0.00909 0.00144 0.00245 0.00352 C10 1 0.795953 0.548364 0.441416 11.00000 0.02702 0.01930 = 0.01713 0.00621 0.00496 0.00858 AFIX 43 H10 2 0.750122 0.482386 0.461213 11.00000 -1.20000 AFIX 0 C19 1 0.422657 0.832301 0.128921 11.00000 0.01489 0.01961 = 0.01665 0.00882 0.00624 0.00781 AFIX 43 H19 2 0.443279 0.785060 0.077296 11.00000 -1.20000 AFIX 0 C38 1 0.773687 0.899476 0.172009 11.00000 0.01609 0.02143 = 0.01420 0.00776 0.00693 0.00695 AFIX 43 H38 2 0.801755 0.869027 0.115121 11.00000 -1.20000 AFIX 0 C30 1 0.666023 0.759322 0.553818 11.00000 0.01207 0.01141 = 0.00991 0.00228 0.00161 0.00458 C5 1 1.047808 0.680378 0.023477 11.00000 0.01380 0.03822 = 0.01856 -0.00004 0.00520 0.01133 AFIX 43 H5 2 1.110737 0.676126 -0.015629 11.00000 -1.20000 AFIX 0 C25 1 0.160018 0.609430 0.255750 11.00000 0.01140 0.01548 = 0.02329 0.00255 0.00627 0.00520 AFIX 43 H25 2 0.171789 0.687432 0.264905 11.00000 -1.20000 AFIX 0 C7 1 0.982857 0.782487 0.158579 11.00000 0.00995 0.02800 = 0.01777 -0.00477 0.00246 0.00306 AFIX 43 H7 2 1.002154 0.848222 0.211739 11.00000 -1.20000 AFIX 0 C3 1 0.836350 0.597400 0.060184 11.00000 0.01260 0.01973 = 0.01177 -0.00071 0.00097 0.00814 AFIX 43 H3 2 0.755010 0.535890 0.045748 11.00000 -1.20000 AFIX 0 C18 1 0.414669 0.935089 0.117321 11.00000 0.01857 0.02345 = 0.02735 0.01661 0.00938 0.00922 AFIX 43 H18 2 0.430694 0.957753 0.058109 11.00000 -1.20000 AFIX 0 C37 1 0.739230 0.834404 0.242125 11.00000 0.00902 0.01291 = 0.01000 0.00201 0.00212 0.00342 C24 1 0.039746 0.530663 0.258526 11.00000 0.01098 0.02455 = 0.02641 0.00513 0.00755 0.00565 AFIX 43 H24 2 -0.030069 0.555252 0.269173 11.00000 -1.20000 AFIX 0 C32 1 0.835342 0.920441 0.524575 11.00000 0.01153 0.01126 = 0.01117 0.00081 0.00137 0.00255 AFIX 43 H32 2 0.867400 0.969051 0.483275 11.00000 -1.20000 AFIX 0 C17 1 0.383461 1.004030 0.191877 11.00000 0.01652 0.01522 = 0.03357 0.01187 0.00494 0.00638 AFIX 43 H17 2 0.379011 1.074191 0.184074 11.00000 -1.20000 AFIX 0 C8 1 0.807478 0.667277 0.326951 11.00000 0.01228 0.01234 = 0.01145 -0.00040 0.00053 0.00609 C34 1 0.860933 0.869976 0.681198 11.00000 0.01771 0.01587 = 0.01140 0.00181 -0.00151 0.00483 AFIX 43 H34 2 0.911782 0.883780 0.745480 11.00000 -1.20000 AFIX 0 C31 1 0.712721 0.829189 0.489323 11.00000 0.01015 0.00924 = 0.00964 0.00091 0.00193 0.00371 C2 1 0.862226 0.693109 0.138487 11.00000 0.00877 0.01984 = 0.01175 -0.00090 0.00170 0.00589 C1 1 0.524530 0.321342 0.114885 11.00000 0.02310 0.01406 = 0.01499 0.00609 0.00542 0.00887 HKLF 4 REM p17316_cut_p53A_a.res in P-1 REM R1 = 0.0405 for 19850 Fo > 4sig(Fo) and 0.0618 for all 25546 data REM 469 parameters refined using 0 restraints END WGHT 0.0551 0.8397 REM Highest difference peak 2.447, deepest hole -0.734, 1-sigma level 0.128 Q1 1 0.5361 0.5585 0.1628 11.00000 0.05 2.45 Q2 1 0.4651 0.3667 0.0791 11.00000 0.05 0.95 Q3 1 0.3757 0.9818 0.2374 11.00000 0.05 0.85 Q4 1 0.4248 0.8250 0.1778 11.00000 0.05 0.80 Q5 1 0.6584 1.1743 0.4009 11.00000 0.05 0.79 Q6 1 0.7640 0.5479 0.3920 11.00000 0.05 0.78 Q7 1 0.3743 0.8434 0.2499 11.00000 0.05 0.74 Q8 1 0.0362 0.4797 0.2523 11.00000 0.05 0.74 Q9 1 0.9568 0.7349 0.4283 11.00000 0.05 0.73 Q10 1 0.4023 0.9754 0.1551 11.00000 0.05 0.73 Q11 1 0.7058 1.1923 0.3281 11.00000 0.05 0.72 Q12 1 0.5083 0.6535 0.4714 11.00000 0.05 0.72 Q13 1 0.1014 0.5733 0.2658 11.00000 0.05 0.70 Q14 1 0.7045 1.0176 0.3016 11.00000 0.05 0.69 Q15 1 1.0592 0.7274 0.0645 11.00000 0.05 0.68 Q16 1 0.5020 0.6803 0.3877 11.00000 0.05 0.68 Q17 1 0.2128 0.5916 0.2515 11.00000 0.05 0.67 Q18 1 0.4081 0.8759 0.1199 11.00000 0.05 0.65 Q19 1 0.3739 0.9214 0.2826 11.00000 0.05 0.65 Q20 1 0.6588 1.0993 0.4413 11.00000 0.05 0.64 ; _shelx_res_checksum 38638 _shelx_hkl_file ; -2 0 0 1029.60 27.30 -2 0 0 954.80 26.50 -2 0 0 982.80 26.80 -2 0 0 952.80 26.70 -2 0 0 985.20 26.70 -2 0 0 935.31 26.70 -2 0 0 1019.50 26.80 -2 0 0 998.90 26.90 -2 0 0 987.70 26.90 -2 0 0 1037.80 29.70 2 0 0 997.10 26.80 2 0 0 921.31 26.70 2 0 0 1001.40 26.70 2 0 0 1049.40 29.70 2 0 0 948.61 26.70 2 0 0 964.50 26.80 2 0 0 1015.40 26.90 2 0 0 976.80 26.90 2 0 0 1008.40 26.90 -3 0 0 187.78 5.60 -3 0 0 186.08 6.00 -3 0 0 185.18 6.60 -3 0 0 186.38 5.80 -3 0 0 198.28 9.50 -3 0 0 189.78 5.60 -3 0 0 190.38 5.60 -3 0 0 195.48 6.00 -3 0 0 196.38 5.90 -3 0 0 190.98 5.90 3 0 0 192.58 5.90 3 0 0 194.78 9.30 3 0 0 213.88 6.10 3 0 0 195.38 5.80 3 0 0 196.78 6.10 3 0 0 188.68 6.10 3 0 0 181.18 5.80 3 0 0 191.48 6.00 3 0 0 184.78 6.00 3 0 0 193.48 5.30 3 0 0 188.18 5.60 3 0 0 181.48 6.20 -4 0 0 1287.47 35.80 -4 0 0 1365.36 35.50 -4 0 0 1250.87 35.40 -4 0 0 1225.98 35.40 -4 0 0 1232.78 35.10 -4 0 0 1283.17 35.60 -4 0 0 1262.97 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3.90 -14 7 0 12.80 3.50 13 -7 0 71.29 5.40 13 -7 0 78.19 6.90 13 -7 0 69.19 7.50 13 -7 0 57.79 18.80 13 -7 0 38.70 18.50 13 -7 0 73.09 6.90 -13 7 0 62.09 6.20 -13 7 0 72.89 4.50 -13 7 0 67.99 8.50 -13 7 0 74.19 6.10 -13 7 0 55.79 5.60 12 -7 0 9.30 2.90 12 -7 0 16.70 3.80 12 -7 0 15.50 4.10 12 -7 0 16.40 3.80 12 -7 0 -3.90 13.30 12 -7 0 6.70 14.40 -12 7 0 14.40 2.10 -12 7 0 17.10 3.60 -12 7 0 12.40 1.40 -12 7 0 16.90 5.00 -12 7 0 9.80 2.90 -12 7 0 11.50 1.60 -12 7 0 14.10 3.00 -12 7 0 11.80 3.10 11 -7 0 15.10 3.40 11 -7 0 19.30 19.60 11 -7 0 21.50 3.40 11 -7 0 5.10 11.50 11 -7 0 13.00 3.30 11 -7 0 19.30 4.00 -11 7 0 18.40 2.10 -11 7 0 14.30 3.10 -11 7 0 13.00 2.90 -11 7 0 18.40 3.40 -11 7 0 20.20 2.20 -11 7 0 10.00 4.40 10 -7 0 195.58 8.10 10 -7 0 154.58 9.60 10 -7 0 190.78 8.50 10 -7 0 174.28 8.70 10 -7 0 147.69 18.30 -10 7 0 183.78 6.30 -10 7 0 185.08 6.30 -10 7 0 165.08 10.20 -10 7 0 175.68 7.50 -10 7 0 177.68 7.90 -10 7 0 165.18 18.70 -10 7 0 173.28 9.20 9 -7 0 67.09 5.40 9 -7 0 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298.07 10.20 -6 7 0 296.27 9.80 -6 7 0 303.37 9.80 5 -7 0 644.74 18.00 5 -7 0 624.34 17.60 5 -7 0 620.34 19.50 5 -7 0 596.94 26.10 5 -7 0 602.84 19.00 5 -7 0 609.24 19.00 5 -7 0 642.34 19.10 5 -7 0 643.94 19.20 5 -7 0 629.14 18.70 5 -7 0 654.13 18.80 -5 7 0 637.04 18.30 -5 7 0 649.04 19.00 -5 7 0 618.84 18.60 -5 7 0 618.94 18.10 -5 7 0 614.84 18.60 -5 7 0 624.24 18.60 -5 7 0 632.44 17.20 -5 7 0 611.64 26.70 -5 7 0 606.84 18.20 4 -7 0 1108.59 30.70 4 -7 0 1138.79 32.20 4 -7 0 1136.39 31.90 4 -7 0 1072.29 31.70 4 -7 0 1125.99 32.80 4 -7 0 1165.28 31.90 4 -7 0 1130.89 39.70 4 -7 0 1088.39 32.20 -4 7 0 1100.29 30.80 -4 7 0 1172.38 31.00 -4 7 0 1099.49 29.90 -4 7 0 1092.69 39.80 -4 7 0 1097.09 31.00 -4 7 0 1058.69 31.30 -4 7 0 1121.79 31.40 -4 7 0 1094.59 31.60 -4 7 0 1105.69 31.70 3 -7 0 2343.27 63.09 3 -7 0 2256.27 70.99 3 -7 0 2319.07 63.29 3 -7 0 2234.98 63.49 3 -7 0 2329.17 63.39 3 -7 0 2088.19 63.99 3 -7 0 2276.17 63.69 -3 7 0 2455.05 72.39 -3 7 0 2384.46 61.49 -3 7 0 2267.37 62.29 -3 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705.43 20.60 -13 8 0 690.43 23.10 12 -8 0 505.25 18.10 12 -8 0 531.15 17.70 12 -8 0 502.65 18.60 12 -8 0 478.65 34.60 12 -8 0 507.95 18.50 12 -8 0 486.95 32.60 -12 8 0 475.65 17.30 -12 8 0 484.15 17.20 -12 8 0 528.25 19.60 -12 8 0 519.45 17.50 -12 8 0 493.85 15.10 -12 8 0 490.85 16.90 11 -8 0 7.10 3.20 11 -8 0 5.90 3.30 11 -8 0 9.70 3.00 11 -8 0 6.60 2.80 -11 8 0 8.70 2.80 -11 8 0 7.60 2.60 -11 8 0 10.80 1.80 -11 8 0 8.60 3.00 -11 8 0 11.20 2.20 -11 8 0 5.30 1.60 -11 8 0 9.80 4.30 10 -8 0 81.99 14.30 10 -8 0 82.49 5.90 10 -8 0 90.39 6.70 10 -8 0 89.89 6.60 10 -8 0 75.49 7.30 -10 8 0 83.69 5.10 -10 8 0 80.29 5.60 -10 8 0 88.19 6.60 -10 8 0 83.29 4.20 -10 8 0 83.99 14.60 -10 8 0 77.39 3.60 9 -8 0 459.95 26.80 9 -8 0 481.35 17.80 9 -8 0 509.95 17.50 9 -8 0 535.75 17.00 9 -8 0 490.65 17.90 -9 8 0 460.35 27.30 -9 8 0 516.35 15.40 -9 8 0 511.35 16.20 -9 8 0 500.55 14.60 -9 8 0 484.95 16.60 -9 8 0 525.65 16.50 -9 8 0 532.95 17.70 8 -8 0 310.07 11.10 8 -8 0 298.67 11.60 8 -8 0 344.17 21.30 8 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23.80 -11 11 0 174.48 6.60 -11 11 0 184.88 9.00 -11 11 0 171.48 8.40 -11 11 0 181.38 8.60 10 -11 0 401.86 15.40 10 -11 0 405.76 15.70 10 -11 0 403.86 14.80 10 -11 0 379.46 15.80 -10 11 0 383.86 15.40 -10 11 0 415.46 31.10 -10 11 0 390.66 14.00 -10 11 0 414.96 14.40 -10 11 0 397.16 14.30 -10 11 0 384.06 11.40 -10 11 0 396.36 12.00 9 -11 0 23.90 4.00 9 -11 0 24.00 4.50 9 -11 0 27.60 12.40 9 -11 0 27.80 4.50 9 -11 0 26.70 1.60 9 -11 0 27.70 3.90 -9 11 0 37.60 4.10 -9 11 0 36.60 13.00 -9 11 0 28.30 4.50 -9 11 0 35.50 3.90 -9 11 0 27.90 2.10 -9 11 0 29.30 4.10 -9 11 0 25.40 1.90 8 -11 0 1.70 2.40 8 -11 0 -8.40 9.30 8 -11 0 -3.20 2.40 8 -11 0 1.00 2.90 8 -11 0 1.60 2.20 8 -11 0 0.90 2.70 8 -11 0 3.20 1.20 -8 11 0 1.50 1.30 -8 11 0 2.90 1.90 -8 11 0 4.90 2.20 -8 11 0 13.10 11.00 -8 11 0 2.70 1.10 -8 11 0 0.40 2.10 -8 11 0 1.60 3.00 -8 11 0 2.30 0.80 7 -11 0 104.09 6.50 7 -11 0 110.39 5.10 7 -11 0 97.39 15.10 7 -11 0 107.89 4.60 7 -11 0 102.49 6.50 7 -11 0 111.39 6.60 7 -11 0 104.49 7.20 -7 11 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8.60 3.50 -12 13 0 4.50 5.30 11 -13 0 20.10 4.70 11 -13 0 16.50 4.80 11 -13 0 17.20 4.60 11 -13 0 10.80 18.20 11 -13 0 22.90 5.30 -11 13 0 8.90 5.10 -11 13 0 19.80 3.90 -11 13 0 11.00 3.50 -11 13 0 25.10 19.60 -11 13 0 13.40 3.60 10 -13 0 485.55 17.90 10 -13 0 506.65 36.30 10 -13 0 487.35 18.90 10 -13 0 505.55 19.80 10 -13 0 519.15 19.00 -10 13 0 500.95 17.10 -10 13 0 485.95 18.80 -10 13 0 516.65 38.90 -10 13 0 521.25 17.90 -10 13 0 549.95 17.40 9 -13 0 38.80 3.10 9 -13 0 37.60 5.60 9 -13 0 39.40 5.70 9 -13 0 14.60 14.60 9 -13 0 36.10 6.00 9 -13 0 33.30 4.70 -9 13 0 41.60 5.70 -9 13 0 38.50 17.10 -9 13 0 34.60 4.50 -9 13 0 39.80 2.60 8 -13 0 184.18 9.60 8 -13 0 174.38 6.80 8 -13 0 154.38 9.80 8 -13 0 168.58 8.30 8 -13 0 175.18 9.20 8 -13 0 174.48 9.50 -8 13 0 170.78 9.10 -8 13 0 169.48 8.30 -8 13 0 171.08 7.70 -8 13 0 156.68 8.20 -8 13 0 176.88 7.60 -8 13 0 162.08 22.50 7 -13 0 521.45 18.60 7 -13 0 522.15 19.70 7 -13 0 559.84 16.70 7 -13 0 507.25 19.20 7 -13 0 486.05 18.80 7 -13 0 500.35 33.00 7 -13 0 560.54 18.10 7 -13 0 534.65 18.70 -7 13 0 588.34 17.20 -7 13 0 522.95 18.10 -7 13 0 509.85 17.90 -7 13 0 542.15 18.60 -7 13 0 497.55 34.00 -7 13 0 544.65 16.90 6 -13 0 298.27 13.00 6 -13 0 305.97 13.40 6 -13 0 298.57 13.40 6 -13 0 306.37 11.10 6 -13 0 320.77 26.10 6 -13 0 309.97 12.40 6 -13 0 293.57 12.80 -6 13 0 332.37 11.00 -6 13 0 300.57 11.90 -6 13 0 311.17 10.50 -6 13 0 303.97 11.90 -6 13 0 304.37 28.40 -6 13 0 289.77 12.30 -6 13 0 310.37 10.80 5 -13 0 11.30 3.60 5 -13 0 13.40 12.20 5 -13 0 14.40 3.00 5 -13 0 17.60 4.00 5 -13 0 21.10 4.30 5 -13 0 18.50 4.50 5 -13 0 16.00 3.30 -5 13 0 16.60 2.60 -5 13 0 17.00 2.70 -5 13 0 15.10 2.50 -5 13 0 20.60 3.70 -5 13 0 15.40 3.70 -5 13 0 13.50 3.30 -5 13 0 41.50 13.70 4 -13 0 9.10 3.50 4 -13 0 9.90 3.40 4 -13 0 -1.60 11.80 4 -13 0 14.40 3.80 4 -13 0 10.20 2.90 4 -13 0 6.20 3.60 -4 13 0 8.20 2.70 -4 13 0 9.90 2.10 -4 13 0 -0.20 12.50 -4 13 0 4.50 3.10 -4 13 0 6.70 2.20 -4 13 0 6.10 1.90 3 -13 0 23.30 3.60 3 -13 0 16.80 3.90 3 -13 0 17.30 4.60 3 -13 0 13.40 3.60 3 -13 0 21.40 12.40 3 -13 0 16.90 4.10 -3 13 0 24.40 4.20 -3 13 0 22.70 3.00 -3 13 0 20.80 4.00 -3 13 0 18.60 3.50 -3 13 0 19.50 2.60 -3 13 0 22.90 13.60 -3 13 0 21.70 3.10 2 -13 0 457.75 16.80 2 -13 0 475.65 13.40 2 -13 0 460.75 17.50 2 -13 0 454.55 16.60 2 -13 0 451.45 15.60 2 -13 0 468.55 18.30 -2 13 0 488.15 14.90 -2 13 0 471.65 14.80 -2 13 0 461.05 15.90 -2 13 0 470.15 15.10 -2 13 0 447.66 16.90 -2 13 0 456.55 16.90 -2 13 0 397.66 36.70 1 -13 0 300.17 14.20 1 -13 0 318.37 12.70 1 -13 0 306.07 11.60 1 -13 0 308.17 9.80 1 -13 0 293.27 13.50 1 -13 0 301.57 30.10 1 -13 0 315.57 12.80 -1 13 0 317.07 13.40 -1 13 0 312.77 11.10 -1 13 0 318.37 12.10 -1 13 0 330.97 11.10 -1 13 0 312.57 12.40 -1 13 0 307.87 13.00 0 -13 0 13.70 2.10 0 -13 0 17.80 4.40 0 -13 0 8.50 4.40 0 -13 0 16.50 3.60 0 -13 0 15.60 3.10 0 -13 0 11.30 3.50 0 -13 0 -15.50 15.20 0 13 0 14.20 2.80 0 13 0 13.40 3.80 0 13 0 14.90 4.60 0 13 0 15.90 2.70 0 13 0 18.70 3.30 0 13 0 15.80 3.40 0 13 0 19.00 3.60 -1 -13 0 30.20 4.40 -1 -13 0 31.90 5.90 -1 -13 0 29.50 3.50 -1 -13 0 33.70 4.60 -1 -13 0 30.00 5.00 1 13 0 39.90 5.80 1 13 0 32.70 5.90 1 13 0 33.30 4.50 1 13 0 39.50 5.00 1 13 0 33.70 4.70 -2 -13 0 26.50 4.30 -2 -13 0 29.30 6.00 -2 -13 0 35.40 5.60 -2 -13 0 30.70 4.40 2 13 0 -10.80 18.40 2 13 0 29.80 4.40 2 13 0 26.60 4.60 2 13 0 37.90 5.00 2 13 0 26.70 4.40 -3 -13 0 17.80 19.60 -3 -13 0 8.90 3.40 -3 -13 0 6.50 2.80 -3 -13 0 13.80 5.00 -3 -13 0 0.10 3.70 -3 -13 0 6.00 3.20 3 13 0 23.80 22.70 3 13 0 5.40 3.50 3 13 0 6.20 3.30 3 13 0 7.70 3.40 3 13 0 8.20 4.30 -4 -13 0 -3.60 2.70 -4 -13 0 2.20 4.00 -4 -13 0 -1.80 4.20 -4 -13 0 -0.80 3.20 4 13 0 -2.60 3.50 4 13 0 1.60 3.50 4 13 0 5.50 3.50 4 13 0 4.80 4.30 -5 -13 0 0.30 4.30 -5 -13 0 0.10 3.50 -5 -13 0 3.30 5.20 -5 -13 0 0.20 3.10 5 13 0 0.00 4.00 5 13 0 0.90 3.40 5 13 0 2.30 3.90 -6 -13 0 10.10 4.10 -6 -13 0 3.30 5.20 -6 -13 0 2.50 4.80 6 13 0 6.20 4.30 6 13 0 10.40 5.30 6 13 0 -0.10 3.90 -7 -13 0 3.80 5.60 -7 -13 0 -5.20 5.00 -7 -13 0 5.90 4.50 -7 -13 0 -2.80 5.80 7 13 0 -0.80 4.40 7 13 0 3.00 5.50 7 13 0 1.00 4.10 -8 -13 0 27.70 8.50 -8 -13 0 26.80 6.80 -8 -13 0 13.10 6.90 -8 -13 0 21.90 5.60 8 13 0 24.00 6.90 8 13 0 25.10 5.40 -9 -13 0 23.30 8.20 -9 -13 0 23.40 7.80 -9 -13 0 19.40 6.80 9 13 0 10.10 8.40 9 13 0 18.70 10.00 9 13 0 13.40 6.40 -10 -13 0 -0.40 6.70 -10 -13 0 11.20 6.50 -10 -13 0 15.50 8.70 10 13 0 17.70 6.20 10 13 0 8.50 6.60 -11 -13 0 -4.50 7.10 -11 -13 0 4.20 7.60 11 13 0 10.10 7.40 11 13 0 -3.50 6.30 -12 -13 0 -0.50 8.00 -12 -13 0 18.30 9.00 12 13 0 9.20 7.90 12 13 0 11.10 8.20 20 -14 0 4.10 8.70 20 -14 0 11.10 8.70 20 -14 0 0.40 10.10 -20 14 0 -6.60 7.10 19 -14 0 12.30 7.50 19 -14 0 16.90 7.80 19 -14 0 10.00 9.10 -19 14 0 14.00 8.10 -19 14 0 13.70 6.60 18 -14 0 76.29 10.10 18 -14 0 65.89 10.20 18 -14 0 96.69 11.50 -18 14 0 90.19 9.90 -18 14 0 75.19 9.40 17 -14 0 2.30 6.20 17 -14 0 5.30 6.40 17 -14 0 12.50 7.20 -17 14 0 12.00 9.60 -17 14 0 -7.00 6.80 -17 14 0 8.00 5.40 16 -14 0 7.70 5.90 16 -14 0 15.80 7.20 16 -14 0 7.70 6.60 -16 14 0 4.90 6.00 -16 14 0 -10.70 8.70 15 -14 0 -5.80 6.20 15 -14 0 1.30 5.30 15 -14 0 4.30 5.30 15 -14 0 4.70 5.80 -15 14 0 -2.10 4.30 -15 14 0 -9.70 7.60 -15 14 0 -1.10 4.40 14 -14 0 73.29 8.80 14 -14 0 63.29 8.10 14 -14 0 65.59 9.30 14 -14 0 66.59 9.50 -14 14 0 71.39 9.60 -14 14 0 58.89 7.40 -14 14 0 65.09 7.60 -14 14 0 60.79 7.10 13 -14 0 15.40 5.80 13 -14 0 8.30 5.70 13 -14 0 16.50 5.30 13 -14 0 14.00 5.30 -13 14 0 13.00 4.10 -13 14 0 11.40 6.40 -13 14 0 16.00 4.40 -13 14 0 10.50 4.10 12 -14 0 137.69 10.30 12 -14 0 130.49 10.20 12 -14 0 142.29 11.00 12 -14 0 140.49 9.50 -12 14 0 152.38 8.50 -12 14 0 137.49 8.70 -12 14 0 171.48 11.70 -12 14 0 143.59 8.60 11 -14 0 179.28 10.10 11 -14 0 183.38 11.90 11 -14 0 169.08 26.00 11 -14 0 185.68 11.00 -11 14 0 178.38 8.90 -11 14 0 185.68 9.70 -11 14 0 189.58 9.40 -11 14 0 188.38 11.50 -11 14 0 157.88 28.20 -11 14 0 185.08 9.50 10 -14 0 451.55 17.00 10 -14 0 422.96 17.70 10 -14 0 450.65 18.80 10 -14 0 457.65 35.90 10 -14 0 446.86 17.80 -10 14 0 387.36 37.80 -10 14 0 444.86 15.60 -10 14 0 439.86 15.70 -10 14 0 472.75 17.90 -10 14 0 457.45 16.60 9 -14 0 137.79 5.80 9 -14 0 129.69 8.10 9 -14 0 143.39 10.00 9 -14 0 127.29 22.10 9 -14 0 133.29 9.00 9 -14 0 148.79 9.30 -9 14 0 114.19 23.60 -9 14 0 139.49 8.20 -9 14 0 134.89 7.20 -9 14 0 142.19 9.30 -9 14 0 134.89 7.40 8 -14 0 898.51 29.70 8 -14 0 816.82 45.20 8 -14 0 915.61 28.30 8 -14 0 904.61 30.50 8 -14 0 900.01 29.10 8 -14 0 905.61 29.70 8 -14 0 957.60 26.50 -8 14 0 876.41 28.30 -8 14 0 934.91 27.50 -8 14 0 858.81 48.70 -8 14 0 901.91 28.40 -8 14 0 892.51 28.90 7 -14 0 651.43 23.70 7 -14 0 681.73 22.80 7 -14 0 679.83 21.90 7 -14 0 643.64 23.20 7 -14 0 682.03 23.10 7 -14 0 711.23 21.00 7 -14 0 645.64 23.70 -7 14 0 628.14 21.90 -7 14 0 673.63 22.60 -7 14 0 713.23 42.60 -7 14 0 692.33 21.00 -7 14 0 663.33 20.30 -7 14 0 665.13 22.20 -7 14 0 708.13 20.90 6 -14 0 207.98 8.60 6 -14 0 179.08 10.60 6 -14 0 175.28 10.10 6 -14 0 183.68 9.50 6 -14 0 234.48 27.80 6 -14 0 179.58 10.10 6 -14 0 192.38 10.80 -6 14 0 182.78 8.90 -6 14 0 187.08 7.60 -6 14 0 201.18 8.10 -6 14 0 187.38 9.80 -6 14 0 192.48 9.30 -6 14 0 186.78 7.80 -6 14 0 173.08 24.50 5 -14 0 60.39 16.00 5 -14 0 55.09 5.80 5 -14 0 56.19 6.60 5 -14 0 49.70 5.20 5 -14 0 46.40 6.60 5 -14 0 48.80 6.40 5 -14 0 50.29 6.30 -5 14 0 46.80 4.10 -5 14 0 29.00 16.60 -5 14 0 51.19 4.30 -5 14 0 51.49 5.60 -5 14 0 46.00 5.20 -5 14 0 49.80 4.00 -5 14 0 53.79 6.00 4 -14 0 5.60 2.90 4 -14 0 -0.80 3.10 4 -14 0 2.50 3.60 4 -14 0 6.30 3.40 4 -14 0 -12.00 12.50 4 -14 0 3.70 3.60 -4 14 0 1.10 2.10 -4 14 0 -10.60 15.80 -4 14 0 5.30 3.00 -4 14 0 0.40 3.70 -4 14 0 3.40 2.10 -4 14 0 5.80 2.00 3 -14 0 45.40 5.80 3 -14 0 44.70 5.90 3 -14 0 40.20 4.90 3 -14 0 44.00 7.00 3 -14 0 30.60 15.20 3 -14 0 35.50 5.10 -3 14 0 45.20 3.90 -3 14 0 42.70 5.20 -3 14 0 34.50 4.90 -3 14 0 35.00 17.60 -3 14 0 32.00 5.20 -3 14 0 52.19 4.10 2 -14 0 7.00 14.40 2 -14 0 10.30 3.70 2 -14 0 3.20 4.00 2 -14 0 5.50 1.50 2 -14 0 6.50 4.20 2 -14 0 8.50 2.80 2 -14 0 5.70 3.50 -2 14 0 5.00 2.20 -2 14 0 8.60 3.20 -2 14 0 7.70 3.20 -2 14 0 4.30 2.20 -2 14 0 7.00 17.10 -2 14 0 9.90 3.00 -2 14 0 3.70 3.80 1 -14 0 108.39 6.70 1 -14 0 109.09 7.70 1 -14 0 100.29 7.40 1 -14 0 78.79 19.50 1 -14 0 105.39 4.70 1 -14 0 102.29 8.70 1 -14 0 95.79 8.20 -1 14 0 113.39 7.80 -1 14 0 123.19 6.00 -1 14 0 112.79 6.30 -1 14 0 114.29 8.50 -1 14 0 112.29 7.10 -1 14 0 85.09 22.40 -1 14 0 113.79 6.20 0 -14 0 20.80 2.60 0 -14 0 21.40 5.20 0 -14 0 24.90 17.90 0 -14 0 17.10 3.90 0 -14 0 15.00 4.20 0 -14 0 14.70 3.20 0 -14 0 18.20 4.50 0 14 0 24.10 3.30 0 14 0 13.60 19.30 0 14 0 19.70 4.10 0 14 0 11.30 4.90 0 14 0 20.90 3.70 0 14 0 19.60 4.00 0 14 0 22.20 3.30 0 14 0 14.90 4.10 -1 -14 0 29.80 6.40 -1 -14 0 27.10 3.10 -1 -14 0 28.20 4.80 -1 -14 0 21.00 5.20 -1 -14 0 27.50 4.70 -1 -14 0 13.40 18.20 1 14 0 31.00 6.20 1 14 0 23.10 4.10 1 14 0 29.60 4.30 1 14 0 19.40 4.50 1 14 0 30.20 4.80 1 14 0 25.50 3.80 1 14 0 3.60 21.60 -2 -14 0 18.30 22.90 -2 -14 0 28.50 6.60 -2 -14 0 22.00 4.70 -2 -14 0 31.10 6.70 -2 -14 0 21.20 3.30 -2 -14 0 22.50 4.30 2 14 0 23.60 4.50 2 14 0 24.80 4.90 2 14 0 27.40 5.20 2 14 0 13.10 24.10 2 14 0 24.00 6.40 2 14 0 26.40 4.40 -3 -14 0 89.59 7.70 -3 -14 0 86.99 6.30 -3 -14 0 96.09 9.40 -3 -14 0 100.89 9.10 -3 -14 0 84.59 7.10 3 14 0 102.69 7.50 3 14 0 94.89 9.10 3 14 0 100.29 7.50 3 14 0 99.09 8.10 -4 -14 0 -1.50 4.90 -4 -14 0 -1.70 3.80 -4 -14 0 -2.90 3.30 -4 -14 0 -3.80 3.00 -4 -14 0 1.70 4.60 4 14 0 -1.80 3.40 4 14 0 0.70 3.90 4 14 0 -5.10 4.10 4 14 0 0.50 3.90 -5 -14 0 -2.40 5.40 -5 -14 0 -2.00 3.60 -5 -14 0 3.30 4.00 -5 -14 0 7.70 5.50 5 14 0 -8.10 4.00 5 14 0 3.30 4.90 5 14 0 -1.20 3.80 5 14 0 -4.30 4.30 -6 -14 0 24.10 6.80 -6 -14 0 27.60 6.50 -6 -14 0 11.60 5.40 -6 -14 0 24.00 5.10 6 14 0 17.60 4.80 6 14 0 25.50 5.80 6 14 0 23.40 5.70 6 14 0 27.10 6.70 -7 -14 0 38.90 6.20 -7 -14 0 35.20 8.50 -7 -14 0 41.10 7.90 7 14 0 39.00 8.40 7 14 0 51.09 7.60 7 14 0 32.60 7.40 7 14 0 27.10 5.60 -8 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0 3.30 4.60 14 -15 0 24.00 6.80 14 -15 0 23.80 6.00 14 -15 0 22.10 6.10 14 -15 0 32.20 6.90 -14 15 0 30.60 8.10 -14 15 0 18.90 5.00 -14 15 0 20.30 4.90 -14 15 0 15.30 5.20 13 -15 0 337.07 16.30 13 -15 0 377.36 17.50 13 -15 0 337.47 15.70 13 -15 0 335.27 17.30 -13 15 0 340.57 14.10 -13 15 0 333.17 14.60 -13 15 0 384.06 17.70 -13 15 0 354.66 14.90 12 -15 0 146.09 11.00 12 -15 0 134.39 11.50 12 -15 0 141.69 10.50 12 -15 0 150.78 10.10 -12 15 0 140.79 9.20 -12 15 0 153.08 8.70 -12 15 0 176.88 12.40 -12 15 0 151.98 9.30 11 -15 0 68.39 7.60 11 -15 0 83.09 9.00 11 -15 0 69.29 8.30 11 -15 0 78.09 8.60 -11 15 0 67.99 6.80 -11 15 0 72.89 7.20 -11 15 0 69.29 9.00 -11 15 0 75.69 6.40 -11 15 0 57.19 6.60 10 -15 0 23.80 5.80 10 -15 0 22.40 5.30 10 -15 0 48.40 22.70 10 -15 0 31.90 5.10 -10 15 0 27.90 6.00 -10 15 0 32.50 4.30 -10 15 0 25.90 4.30 -10 15 0 9.70 23.70 -10 15 0 27.80 4.90 9 -15 0 113.59 5.80 9 -15 0 124.49 8.90 9 -15 0 104.39 9.50 9 -15 0 119.69 9.50 9 -15 0 116.69 8.00 9 -15 0 141.69 23.90 -9 15 0 170.18 27.90 -9 15 0 116.79 9.30 -9 15 0 120.29 7.90 -9 15 0 102.19 7.80 -9 15 0 108.39 7.00 -9 15 0 110.89 6.80 8 -15 0 85.59 20.70 8 -15 0 97.89 7.30 8 -15 0 91.59 8.30 8 -15 0 91.09 8.00 8 -15 0 104.09 6.00 8 -15 0 89.89 8.40 8 -15 0 94.39 8.00 -8 15 0 91.09 6.00 -8 15 0 81.39 23.10 -8 15 0 97.09 8.40 -8 15 0 108.09 7.20 -8 15 0 114.69 6.60 -8 15 0 102.99 7.40 7 -15 0 168.38 10.60 7 -15 0 172.58 10.10 7 -15 0 189.18 27.50 7 -15 0 159.48 10.40 7 -15 0 157.38 9.40 7 -15 0 163.78 8.70 7 -15 0 151.88 10.20 7 -15 0 161.18 9.00 -7 15 0 162.28 7.10 -7 15 0 160.58 9.10 -7 15 0 243.08 32.80 -7 15 0 166.08 7.90 -7 15 0 168.58 8.20 -7 15 0 170.68 9.60 -7 15 0 155.78 8.60 6 -15 0 9.40 3.40 6 -15 0 14.70 4.60 6 -15 0 7.50 4.20 6 -15 0 10.70 3.60 6 -15 0 9.30 4.20 6 -15 0 2.00 17.10 6 -15 0 8.80 4.10 -6 15 0 19.20 18.60 -6 15 0 13.50 4.60 -6 15 0 10.50 2.70 -6 15 0 14.40 3.70 -6 15 0 12.80 4.10 -6 15 0 12.70 2.60 -6 15 0 12.10 3.10 5 -15 0 78.69 7.20 5 -15 0 78.99 6.80 5 -15 0 81.59 6.40 5 -15 0 69.29 7.40 5 -15 0 71.99 8.10 5 -15 0 77.59 8.00 -5 15 0 74.59 5.00 -5 15 0 76.49 5.50 -5 15 0 70.39 20.70 -5 15 0 77.19 4.90 -5 15 0 75.59 7.20 -5 15 0 69.49 6.20 -5 15 0 74.99 6.00 4 -15 0 207.08 9.90 4 -15 0 197.18 11.20 4 -15 0 205.38 10.80 4 -15 0 195.18 12.00 4 -15 0 212.48 10.10 4 -15 0 199.08 11.30 -4 15 0 207.98 8.70 -4 15 0 193.38 27.50 -4 15 0 201.78 9.90 -4 15 0 205.88 10.80 -4 15 0 213.48 8.40 -4 15 0 222.48 8.50 3 -15 0 22.10 5.00 3 -15 0 21.00 3.90 3 -15 0 17.60 4.70 3 -15 0 17.30 4.60 3 -15 0 13.00 5.30 -3 15 0 17.50 3.80 -3 15 0 20.60 3.00 -3 15 0 16.20 3.30 -3 15 0 21.60 5.30 -3 15 0 9.50 3.70 -3 15 0 18.60 3.00 -3 15 0 -4.00 20.20 2 -15 0 265.07 12.40 2 -15 0 266.97 11.30 2 -15 0 269.17 13.60 2 -15 0 266.47 12.50 2 -15 0 256.27 14.20 -2 15 0 267.47 10.20 -2 15 0 273.17 11.70 -2 15 0 285.37 10.80 -2 15 0 230.48 31.40 -2 15 0 262.77 12.70 -2 15 0 277.27 12.90 1 -15 0 242.08 13.70 1 -15 0 227.88 10.40 1 -15 0 191.48 27.40 1 -15 0 230.88 11.50 1 -15 0 240.88 8.20 1 -15 0 249.38 11.80 -1 15 0 253.27 10.20 -1 15 0 234.08 32.10 -1 15 0 246.28 9.80 -1 15 0 235.68 9.70 -1 15 0 241.88 12.70 -1 15 0 243.78 11.10 0 -15 0 280.37 12.60 0 -15 0 262.97 13.80 0 -15 0 265.07 9.30 0 -15 0 203.68 33.20 0 -15 0 274.77 12.30 0 -15 0 261.27 11.10 0 -15 0 248.78 14.40 0 15 0 248.88 12.10 0 15 0 267.27 10.70 0 15 0 277.27 10.70 0 15 0 256.47 12.90 0 15 0 249.48 35.00 0 15 0 266.47 11.90 0 15 0 274.77 13.80 0 15 0 265.07 11.00 -1 -15 0 11.10 3.50 -1 -15 0 8.20 4.40 -1 -15 0 8.60 5.50 -1 -15 0 12.10 4.20 -1 -15 0 11.60 3.00 -1 -15 0 14.30 5.40 1 15 0 11.90 5.50 1 15 0 10.80 3.70 1 15 0 18.80 4.80 1 15 0 7.90 4.20 1 15 0 12.60 3.40 1 15 0 9.60 3.30 1 15 0 6.10 3.90 -2 -15 0 195.08 12.50 -2 -15 0 170.78 12.50 -2 -15 0 167.78 9.10 -2 -15 0 180.48 10.20 -2 -15 0 169.88 8.30 -2 -15 0 187.18 10.00 2 15 0 179.98 12.50 2 15 0 179.68 9.50 2 15 0 179.08 8.90 2 15 0 182.58 9.80 2 15 0 180.18 11.40 2 15 0 170.28 10.00 -3 -15 0 109.69 8.20 -3 -15 0 114.59 10.40 -3 -15 0 91.59 8.50 -3 -15 0 110.39 7.30 -3 -15 0 97.19 10.50 3 15 0 104.49 8.50 3 15 0 119.19 10.20 3 15 0 114.59 8.40 3 15 0 111.89 8.20 3 15 0 109.79 11.40 -4 -15 0 5.30 4.60 -4 -15 0 -1.10 3.70 -4 -15 0 6.70 5.30 -4 -15 0 9.90 5.10 -4 -15 0 7.20 6.00 4 15 0 2.50 4.20 4 15 0 12.40 5.10 4 15 0 8.50 4.70 4 15 0 5.90 5.00 -5 -15 0 18.60 6.30 -5 -15 0 20.30 9.80 -5 -15 0 20.50 7.60 -5 -15 0 20.00 4.90 5 15 0 22.60 5.70 5 15 0 17.20 5.50 5 15 0 4.60 5.50 5 15 0 19.30 5.30 -6 -15 0 8.40 7.20 -6 -15 0 1.50 6.00 -6 -15 0 6.70 5.00 -6 -15 0 5.90 6.70 6 15 0 7.70 5.90 6 15 0 -1.20 4.50 6 15 0 -2.00 5.20 6 15 0 -7.60 5.80 -7 -15 0 49.50 9.80 -7 -15 0 50.69 6.80 -7 -15 0 33.10 9.10 -7 -15 0 45.90 8.60 7 15 0 68.99 9.70 7 15 0 77.29 9.10 7 15 0 45.40 7.70 -8 -15 0 33.70 9.80 -8 -15 0 25.30 8.10 -8 -15 0 39.50 7.30 8 15 0 37.00 7.70 8 15 0 23.50 6.30 8 15 0 25.20 7.50 -9 -15 0 3.10 7.50 -9 -15 0 7.60 7.40 -9 -15 0 11.70 9.60 9 15 0 7.80 7.10 9 15 0 6.30 8.10 9 15 0 11.50 6.60 -10 -15 0 27.40 9.20 -10 -15 0 14.60 8.50 10 15 0 1.80 7.90 10 15 0 10.30 8.50 10 15 0 13.20 9.10 19 -16 0 14.20 8.20 19 -16 0 26.20 10.30 19 -16 0 5.90 8.20 -19 16 0 1.20 11.20 -19 16 0 -4.70 6.60 18 -16 0 59.29 11.10 18 -16 0 48.50 9.60 18 -16 0 45.20 9.60 -18 16 0 37.00 8.90 -18 16 0 54.99 8.00 17 -16 0 108.09 13.70 17 -16 0 118.99 12.80 17 -16 0 142.99 12.50 -17 16 0 110.49 14.50 -17 16 0 125.09 10.90 -17 16 0 132.69 12.30 16 -16 0 178.38 13.80 16 -16 0 169.08 13.90 16 -16 0 174.68 13.10 -16 16 0 174.58 17.80 -16 16 0 175.98 14.10 -16 16 0 145.39 11.20 15 -16 0 42.40 10.70 15 -16 0 66.69 10.00 15 -16 0 48.10 8.30 -15 16 0 32.20 10.40 -15 16 0 66.49 8.40 -15 16 0 51.59 7.00 14 -16 0 58.89 8.10 14 -16 0 61.89 9.40 14 -16 0 73.49 9.40 14 -16 0 47.40 8.00 -14 16 0 59.59 7.90 -14 16 0 67.69 7.70 -14 16 0 63.09 8.70 -14 16 0 72.19 10.70 13 -16 0 144.89 11.60 13 -16 0 113.39 10.90 13 -16 0 95.29 10.40 13 -16 0 126.89 10.10 -13 16 0 139.59 13.20 -13 16 0 111.89 8.90 -13 16 0 107.89 8.30 -13 16 0 111.79 9.20 12 -16 0 65.99 8.20 12 -16 0 66.59 9.30 12 -16 0 63.09 9.00 12 -16 0 71.09 8.60 -12 16 0 76.29 6.90 -12 16 0 72.49 7.50 -12 16 0 74.19 9.50 -12 16 0 75.09 8.00 11 -16 0 15.80 5.80 11 -16 0 17.50 5.80 11 -16 0 23.00 5.80 11 -16 0 29.00 5.70 -11 16 0 25.00 5.20 -11 16 0 28.50 5.00 -11 16 0 21.50 6.90 -11 16 0 31.40 4.60 -11 16 0 26.60 4.90 10 -16 0 3.30 4.90 10 -16 0 2.30 4.60 10 -16 0 1.50 4.10 10 -16 0 0.60 5.10 -10 16 0 -5.70 5.50 -10 16 0 -3.40 3.10 -10 16 0 -4.00 3.30 -10 16 0 1.80 3.70 9 -16 0 18.40 5.40 9 -16 0 12.90 3.10 9 -16 0 13.70 4.30 9 -16 0 6.00 4.70 9 -16 0 14.40 27.40 -9 16 0 18.50 4.10 -9 16 0 13.70 4.20 -9 16 0 15.10 4.40 -9 16 0 20.10 3.70 -9 16 0 25.70 6.10 8 -16 0 42.60 21.20 8 -16 0 2.60 4.70 8 -16 0 2.60 3.10 8 -16 0 2.50 4.20 8 -16 0 -5.20 4.10 8 -16 0 3.50 3.70 8 -16 0 4.30 3.50 -8 16 0 3.20 3.50 -8 16 0 1.50 3.20 -8 16 0 4.30 4.80 -8 16 0 5.40 24.80 -8 16 0 4.60 3.00 -8 16 0 2.50 3.70 7 -16 0 34.70 5.60 7 -16 0 -10.00 20.90 7 -16 0 33.80 6.10 7 -16 0 32.70 5.90 7 -16 0 37.20 6.20 7 -16 0 42.90 5.50 7 -16 0 45.60 5.90 -7 16 0 30.80 5.00 -7 16 0 31.40 5.10 -7 16 0 37.60 4.60 -7 16 0 36.70 4.40 -7 16 0 22.10 24.40 -7 16 0 31.10 5.90 6 -16 0 135.49 10.20 6 -16 0 141.19 8.30 6 -16 0 139.29 10.50 6 -16 0 132.39 8.90 6 -16 0 156.48 25.30 6 -16 0 114.49 9.50 6 -16 0 141.99 10.40 -6 16 0 136.29 7.20 -6 16 0 137.89 8.60 -6 16 0 141.39 6.80 -6 16 0 132.79 8.70 -6 16 0 125.89 7.80 -6 16 0 144.59 28.10 -6 16 0 143.39 9.50 5 -16 0 7.10 4.20 5 -16 0 10.30 4.10 5 -16 0 15.40 4.10 5 -16 0 8.40 4.50 5 -16 0 9.90 5.00 5 -16 0 22.00 20.10 -5 16 0 -4.40 22.60 -5 16 0 8.20 3.90 -5 16 0 11.10 3.40 -5 16 0 16.80 4.10 -5 16 0 19.50 5.20 -5 16 0 14.40 2.90 4 -16 0 85.19 22.80 4 -16 0 74.29 7.40 4 -16 0 74.39 7.60 4 -16 0 74.19 9.10 4 -16 0 89.19 7.40 4 -16 0 74.39 8.20 4 -16 0 77.79 9.80 -4 16 0 82.49 7.10 -4 16 0 86.59 6.00 -4 16 0 87.29 8.20 -4 16 0 32.40 25.40 -4 16 0 86.49 6.30 -4 16 0 80.99 5.50 3 -16 0 3.80 20.10 3 -16 0 26.10 5.80 3 -16 0 38.00 5.90 3 -16 0 27.80 6.70 3 -16 0 28.70 4.50 3 -16 0 20.90 4.80 3 -16 0 32.60 5.80 -3 16 0 40.60 4.80 -3 16 0 27.00 5.20 -3 16 0 30.50 5.10 -3 16 0 26.30 3.60 -3 16 0 26.90 4.10 -3 16 0 29.20 26.00 -3 16 0 45.20 6.70 2 -16 0 46.60 6.90 2 -16 0 57.09 7.20 2 -16 0 58.49 7.50 2 -16 0 61.59 7.70 2 -16 0 -14.70 24.10 2 -16 0 51.09 6.40 2 -16 0 59.49 8.20 -2 16 0 55.69 7.70 -2 16 0 57.79 5.40 -2 16 0 60.79 5.70 -2 16 0 40.50 6.40 -2 16 0 45.00 27.90 -2 16 0 43.50 5.10 -2 16 0 52.29 6.30 1 -16 0 85.69 8.20 1 -16 0 75.29 6.90 1 -16 0 74.29 9.40 1 -16 0 64.59 9.30 1 -16 0 85.29 8.00 -1 16 0 66.49 8.30 -1 16 0 67.79 9.00 -1 16 0 66.59 5.80 -1 16 0 72.09 6.00 -1 16 0 74.09 31.00 -1 16 0 72.19 7.20 -1 16 0 74.49 9.30 0 -16 0 23.00 5.10 0 -16 0 16.80 5.60 0 -16 0 20.40 4.80 0 -16 0 22.90 4.20 0 -16 0 29.90 6.80 0 16 0 15.80 3.70 0 16 0 27.60 5.90 0 16 0 18.40 6.50 0 16 0 26.90 4.10 0 16 0 16.80 4.70 0 16 0 22.60 4.40 -1 -16 0 37.80 6.90 -1 -16 0 34.40 7.80 -1 -16 0 53.69 6.70 -1 -16 0 41.00 6.10 -1 -16 0 35.70 5.90 1 16 0 32.80 5.40 1 16 0 36.10 8.50 1 16 0 36.20 5.30 1 16 0 22.60 5.40 1 16 0 48.00 5.80 1 16 0 42.40 6.00 1 16 0 31.90 5.80 -2 -16 0 212.38 11.20 -2 -16 0 205.08 13.70 -2 -16 0 188.48 9.60 -2 -16 0 188.78 13.90 -2 -16 0 187.88 12.30 -2 -16 0 201.08 11.40 2 16 0 208.28 12.80 2 16 0 192.78 10.10 2 16 0 176.18 9.50 2 16 0 185.88 13.20 2 16 0 189.18 10.20 2 16 0 198.68 11.40 2 16 0 205.18 10.90 -3 -16 0 73.99 9.60 -3 -16 0 88.89 8.90 -3 -16 0 72.19 6.90 -3 -16 0 85.29 11.10 -3 -16 0 69.89 10.60 3 16 0 76.29 7.90 3 16 0 78.29 11.00 3 16 0 77.19 8.30 3 16 0 67.99 8.70 3 16 0 71.49 7.30 3 16 0 64.19 8.40 -4 -16 0 38.80 6.10 -4 -16 0 25.90 7.40 -4 -16 0 30.20 5.00 -4 -16 0 37.60 7.70 -4 -16 0 31.00 7.50 4 16 0 33.60 7.60 4 16 0 22.30 5.80 4 16 0 27.70 8.40 4 16 0 33.80 6.20 4 16 0 32.00 6.60 -5 -16 0 2.90 7.30 -5 -16 0 3.70 4.70 -5 -16 0 2.10 6.00 5 16 0 9.00 6.20 5 16 0 -4.20 5.10 5 16 0 -1.40 6.80 5 16 0 3.80 5.60 5 16 0 9.90 5.30 -6 -16 0 32.30 7.90 -6 -16 0 31.20 9.50 -6 -16 0 37.70 6.20 -6 -16 0 39.10 9.60 6 16 0 38.00 7.30 6 16 0 56.09 7.60 6 16 0 46.90 7.70 -7 -16 0 -10.10 6.70 -7 -16 0 8.00 8.80 -7 -16 0 7.20 7.80 7 16 0 19.40 6.70 7 16 0 8.00 6.50 7 16 0 17.00 7.20 -8 -16 0 -2.80 9.50 -8 -16 0 -12.30 7.40 8 16 0 5.60 7.70 8 16 0 10.20 7.20 8 16 0 -2.40 7.70 -9 -16 0 0.70 8.70 9 16 0 13.40 8.90 9 16 0 2.00 8.10 9 16 0 -3.20 7.90 19 -17 0 9.40 8.50 19 -17 0 3.60 10.40 -19 17 0 16.20 7.60 18 -17 0 108.59 15.20 18 -17 0 64.19 10.50 18 -17 0 85.99 11.60 -18 17 0 101.29 13.50 -18 17 0 82.79 9.60 17 -17 0 78.69 11.90 17 -17 0 67.59 9.50 17 -17 0 101.79 13.60 -17 17 0 65.79 8.60 -17 17 0 74.99 9.70 16 -17 0 73.99 11.10 16 -17 0 86.29 11.20 16 -17 0 115.19 11.50 -16 17 0 89.39 11.20 -16 17 0 72.49 9.90 15 -17 0 108.69 12.60 15 -17 0 81.79 11.00 15 -17 0 87.69 10.60 -15 17 0 108.19 9.80 -15 17 0 122.29 13.50 -15 17 0 78.49 11.10 -15 17 0 105.59 9.70 14 -17 0 121.39 13.20 14 -17 0 142.59 12.40 14 -17 0 161.48 11.80 14 -17 0 129.39 15.10 -14 17 0 117.49 17.10 -14 17 0 152.58 10.40 -14 17 0 141.29 9.80 -14 17 0 122.99 10.60 13 -17 0 71.99 9.40 13 -17 0 54.89 8.40 13 -17 0 61.59 9.70 13 -17 0 71.09 8.90 -13 17 0 61.69 7.90 -13 17 0 72.09 10.70 -13 17 0 65.39 7.90 -13 17 0 64.99 8.40 12 -17 0 14.10 6.10 12 -17 0 15.40 6.10 12 -17 0 17.00 6.70 12 -17 0 20.70 5.60 -12 17 0 26.50 8.10 -12 17 0 11.80 4.50 -12 17 0 15.40 5.10 -12 17 0 14.10 4.50 11 -17 0 18.80 5.30 11 -17 0 32.40 6.50 11 -17 0 28.90 7.20 11 -17 0 35.90 7.60 -11 17 0 29.30 4.80 -11 17 0 16.20 4.60 -11 17 0 28.40 5.40 -11 17 0 25.60 7.60 -11 17 0 21.70 5.20 10 -17 0 23.10 5.60 10 -17 0 14.70 5.80 10 -17 0 27.30 6.30 10 -17 0 18.60 5.20 -10 17 0 22.30 4.20 -10 17 0 32.50 7.20 -10 17 0 22.00 4.70 -10 17 0 14.70 4.50 -10 17 0 26.30 5.30 9 -17 0 36.20 4.40 9 -17 0 41.20 6.20 9 -17 0 41.10 7.00 9 -17 0 38.60 5.70 9 -17 0 39.30 7.30 -9 17 0 32.10 5.60 -9 17 0 34.70 5.80 -9 17 0 43.10 7.70 -9 17 0 37.20 4.70 -9 17 0 36.30 5.20 8 -17 0 80.19 9.10 8 -17 0 91.49 6.90 8 -17 0 84.99 9.10 8 -17 0 78.59 8.20 8 -17 0 100.79 8.00 8 -17 0 77.09 9.40 -8 17 0 90.19 8.00 -8 17 0 85.19 6.40 -8 17 0 76.79 9.60 -8 17 0 86.59 7.10 -8 17 0 76.69 7.70 7 -17 0 51.69 6.40 7 -17 0 38.90 6.70 7 -17 0 45.50 7.40 7 -17 0 42.80 7.00 7 -17 0 21.70 29.10 7 -17 0 49.00 7.70 7 -17 0 49.90 6.70 -7 17 0 51.49 5.40 -7 17 0 40.10 6.00 -7 17 0 44.60 6.20 -7 17 0 41.30 44.90 -7 17 0 45.10 6.90 -7 17 0 38.20 4.80 6 -17 0 5.10 5.50 6 -17 0 6.40 4.00 6 -17 0 5.50 4.70 6 -17 0 2.10 4.50 6 -17 0 -6.10 4.50 6 -17 0 25.50 24.00 6 -17 0 -0.90 4.20 -6 17 0 43.70 31.10 -6 17 0 5.00 4.10 -6 17 0 1.40 3.60 -6 17 0 -3.00 3.20 -6 17 0 -8.40 4.80 -6 17 0 0.60 2.90 5 -17 0 125.39 29.60 5 -17 0 187.28 12.70 5 -17 0 194.48 13.10 5 -17 0 190.78 10.60 5 -17 0 200.48 11.70 5 -17 0 213.38 10.90 5 -17 0 213.08 12.50 -5 17 0 197.78 10.50 -5 17 0 184.68 10.90 -5 17 0 162.08 34.40 -5 17 0 194.88 8.80 -5 17 0 216.88 9.50 -5 17 0 199.08 12.00 4 -17 0 225.28 12.90 4 -17 0 244.08 11.80 4 -17 0 224.08 13.10 4 -17 0 250.87 14.70 4 -17 0 257.07 14.20 4 -17 0 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7.10 1 -12 7 95.89 5.30 1 -12 7 100.19 6.80 1 -12 7 89.39 6.30 -2 12 -7 14.60 1.50 -2 12 -7 14.20 3.10 -2 12 -7 19.90 10.10 -2 12 -7 14.40 4.10 -2 12 -7 11.30 2.90 -2 12 -7 12.60 3.10 -2 12 -7 18.60 2.40 2 -12 7 12.40 3.70 2 -12 7 14.80 3.60 2 -12 7 15.10 3.80 2 -12 7 10.70 3.10 2 -12 7 13.60 2.20 -3 12 -7 122.69 6.60 -3 12 -7 124.09 8.20 -3 12 -7 121.39 6.70 -3 12 -7 146.49 17.80 -3 12 -7 131.69 4.70 -3 12 -7 136.79 7.20 3 -12 7 118.49 7.50 3 -12 7 125.69 7.40 3 -12 7 116.79 7.80 3 -12 7 120.69 7.40 -4 12 -7 18.50 9.90 -4 12 -7 22.70 2.40 -4 12 -7 20.60 3.20 -4 12 -7 20.40 3.80 -4 12 -7 17.80 4.40 -4 12 -7 18.00 3.30 4 -12 7 25.20 4.40 4 -12 7 19.50 3.90 4 -12 7 17.30 3.70 4 -12 7 21.80 3.80 4 -12 7 14.40 3.60 -5 12 -7 163.28 7.80 -5 12 -7 154.18 7.70 -5 12 -7 161.68 6.30 -5 12 -7 152.58 9.10 -5 12 -7 168.98 17.60 -5 12 -7 158.08 8.20 5 -12 7 165.18 8.60 5 -12 7 168.68 8.20 5 -12 7 172.38 8.60 5 -12 7 161.88 8.50 5 -12 7 153.18 8.60 -6 12 -7 5.10 2.80 -6 12 -7 2.50 2.70 -6 12 -7 0.80 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170.58 12.70 8 11 -10 289.87 12.70 8 11 -10 292.37 16.30 8 11 -10 270.17 12.20 8 11 -10 282.57 11.00 8 11 -10 283.87 12.80 8 11 -10 280.37 13.40 -8 -11 10 270.07 15.20 -8 -11 10 304.47 14.60 -8 -11 10 312.17 14.90 7 11 -10 227.98 11.50 7 11 -10 229.98 9.40 7 11 -10 232.08 11.10 7 11 -10 219.98 10.40 7 11 -10 217.08 15.40 7 11 -10 237.28 11.00 -7 -11 10 226.68 12.40 -7 -11 10 246.28 12.90 -7 -11 10 234.08 13.60 6 11 -10 270.17 45.10 6 11 -10 268.47 11.00 6 11 -10 263.97 12.20 6 11 -10 273.17 14.40 6 11 -10 278.37 11.70 6 11 -10 282.37 11.80 6 11 -10 277.67 10.30 -6 -11 10 216.08 39.50 -6 -11 10 264.97 12.40 -6 -11 10 270.77 13.90 -6 -11 10 246.58 13.40 5 11 -10 523.15 40.80 5 11 -10 537.05 18.40 5 11 -10 526.35 18.70 5 11 -10 536.15 20.90 5 11 -10 540.45 18.30 5 11 -10 533.05 17.60 5 11 -10 498.05 17.50 -5 -11 10 534.95 20.80 -5 -11 10 536.15 39.00 -5 -11 10 516.75 19.10 -5 -11 10 528.95 19.90 4 11 -10 333.47 13.00 4 11 -10 347.37 12.40 4 11 -10 336.67 12.90 4 11 -10 341.47 30.70 4 11 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5 -14 -0.60 5.80 -8 5 -14 6.30 3.80 8 -5 14 -2.20 3.50 8 -5 14 -0.40 3.90 8 -5 14 2.90 4.10 8 -5 14 -0.40 3.30 -9 5 -14 1.80 4.80 -9 5 -14 2.60 3.20 -9 5 -14 0.50 3.30 -9 5 -14 2.10 3.90 -9 5 -14 3.40 7.00 9 -5 14 4.60 3.90 9 -5 14 -1.30 3.90 9 -5 14 0.80 4.00 9 -5 14 -7.60 4.20 -10 5 -14 147.79 10.70 -10 5 -14 139.69 9.50 -10 5 -14 147.59 9.40 -10 5 -14 156.18 14.00 -10 5 -14 146.99 8.20 10 -5 14 139.89 11.60 10 -5 14 161.28 9.50 10 -5 14 159.08 10.70 -11 5 -14 181.78 12.40 -11 5 -14 194.08 11.40 -11 5 -14 191.48 16.50 -11 5 -14 191.68 10.70 11 -5 14 188.58 13.50 11 -5 14 185.98 12.00 11 -5 14 173.98 10.60 -12 5 -14 139.49 10.30 -12 5 -14 149.79 10.80 -12 5 -14 131.09 15.60 12 -5 14 145.19 11.70 12 -5 14 146.29 14.30 12 -5 14 141.79 10.70 -13 5 -14 4.20 9.80 -13 5 -14 12.50 5.70 -13 5 -14 17.10 6.40 13 -5 14 14.50 6.80 -14 5 -14 9.70 6.10 -14 5 -14 4.10 6.10 14 -5 14 -0.40 7.50 -15 5 -14 49.50 8.10 -15 5 -14 52.09 8.80 15 -5 14 42.30 9.20 15 -5 14 30.00 9.50 17 4 -14 156.18 15.10 17 4 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12.80 4.00 9 4 -14 10.50 4.30 -9 -4 14 6.00 4.80 -9 -4 14 6.30 4.30 -9 -4 14 16.40 2.70 -9 -4 14 15.90 4.00 8 4 -14 3.60 2.90 8 4 -14 2.90 3.60 8 4 -14 5.30 3.60 8 4 -14 3.40 3.10 -8 -4 14 0.40 3.60 -8 -4 14 1.00 3.70 -8 -4 14 2.40 3.20 -8 -4 14 0.60 3.20 7 4 -14 69.19 6.00 7 4 -14 72.99 16.70 7 4 -14 64.89 5.20 7 4 -14 65.39 6.10 7 4 -14 62.39 6.00 7 4 -14 83.39 17.10 -7 -4 14 66.69 5.90 -7 -4 14 76.19 7.20 -7 -4 14 62.79 6.80 6 4 -14 1.10 3.10 6 4 -14 5.30 2.60 6 4 -14 1.80 11.60 6 4 -14 6.30 11.60 6 4 -14 2.80 2.80 6 4 -14 4.30 3.10 -6 -4 14 4.90 3.40 -6 -4 14 2.90 3.30 -6 -4 14 3.70 3.40 5 4 -14 3.30 3.00 5 4 -14 7.20 3.20 5 4 -14 8.90 10.10 5 4 -14 -0.50 2.80 5 4 -14 0.10 10.70 5 4 -14 4.60 2.30 -5 -4 14 0.30 2.80 -5 -4 14 6.00 2.60 -5 -4 14 2.40 2.90 4 4 -14 2.80 2.00 4 4 -14 8.20 8.00 4 4 -14 -1.90 2.40 4 4 -14 -5.30 8.10 4 4 -14 -4.90 2.60 4 4 -14 -1.30 2.50 -4 -4 14 3.20 2.30 -4 -4 14 -0.20 2.40 -4 -4 14 -1.70 2.80 3 4 -14 4.40 2.80 3 4 -14 2.30 2.50 3 4 -14 2.20 2.50 3 4 -14 2.50 2.80 3 4 -14 -6.20 7.10 3 4 -14 -2.00 6.50 3 4 -14 7.40 2.30 -3 -4 14 7.20 3.00 -3 -4 14 2.40 2.60 -3 -4 14 4.10 2.30 -3 -4 14 1.80 2.30 2 4 -14 70.99 5.50 2 4 -14 66.69 5.50 2 4 -14 63.19 3.70 2 4 -14 58.89 8.30 2 4 -14 65.19 5.00 2 4 -14 51.79 7.80 2 4 -14 66.99 5.90 2 4 -14 65.39 4.50 -2 -4 14 59.39 5.80 -2 -4 14 67.59 5.20 -2 -4 14 71.69 4.50 -2 -4 14 68.69 4.90 1 4 -14 58.49 5.10 1 4 -14 55.29 5.40 1 4 -14 52.09 6.90 1 4 -14 49.20 5.40 1 4 -14 57.59 3.80 1 4 -14 41.40 4.40 1 4 -14 55.29 4.30 -1 -4 14 52.39 4.50 -1 -4 14 47.40 5.40 -1 -4 14 55.99 4.10 -1 -4 14 57.69 5.10 -1 -4 14 49.60 2.20 0 4 -14 262.47 10.50 0 4 -14 261.27 9.50 0 4 -14 271.27 10.00 0 4 -14 259.57 11.20 0 4 -14 266.47 11.10 0 4 -14 262.47 10.50 0 -4 14 277.77 10.00 0 -4 14 257.87 8.20 0 -4 14 256.77 10.60 0 -4 14 247.18 10.80 0 -4 14 263.17 8.20 0 -4 14 268.37 9.50 0 -4 14 256.27 8.20 -1 4 -14 77.39 5.50 -1 4 -14 92.89 6.40 -1 4 -14 82.39 5.80 -1 4 -14 83.89 5.60 -1 4 -14 90.19 6.50 -1 4 -14 83.09 6.70 -1 4 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9.30 -3 5 -21 85.29 9.70 3 -5 21 45.90 7.00 3 -5 21 48.80 7.40 3 -5 21 80.19 11.20 3 -5 21 78.29 11.00 -4 5 -21 71.89 10.70 -4 5 -21 71.09 11.40 -4 5 -21 67.79 9.70 -4 5 -21 83.39 9.80 4 -5 21 50.59 8.40 4 -5 21 47.30 7.20 -5 5 -21 81.99 11.60 -5 5 -21 85.69 9.60 -5 5 -21 134.59 16.00 -5 5 -21 87.19 10.70 5 -5 21 79.49 13.80 -6 5 -21 -6.60 5.30 -6 5 -21 0.30 5.80 -6 5 -21 10.50 10.40 -7 5 -21 13.30 6.20 -7 5 -21 -0.30 11.00 -7 5 -21 -10.00 5.90 -8 5 -21 62.19 8.40 -8 5 -21 92.49 11.40 -8 5 -21 67.39 13.70 -9 5 -21 44.80 8.50 -9 5 -21 61.69 9.00 -9 5 -21 20.50 13.50 13 4 -21 7.40 7.60 13 4 -21 -15.40 8.80 -13 -4 21 -14.80 9.70 -13 -4 21 -7.70 8.60 12 4 -21 51.69 9.40 12 4 -21 56.59 9.80 -12 -4 21 63.09 11.30 -12 -4 21 50.09 10.20 11 4 -21 171.48 14.10 11 4 -21 147.99 12.50 -11 -4 21 144.79 14.20 -11 -4 21 158.38 15.70 10 4 -21 118.09 11.20 10 4 -21 88.79 11.80 -10 -4 21 86.09 13.40 -10 -4 21 88.89 12.00 -10 -4 21 98.29 12.90 9 4 -21 14.60 6.70 9 4 -21 14.00 6.80 -9 -4 21 9.10 7.80 -9 -4 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22 -4.70 9.60 -6 -13 22 9.50 10.50 5 13 -22 20.90 8.00 5 13 -22 20.50 10.30 5 13 -22 9.40 8.30 -5 -13 22 8.70 10.10 -5 -13 22 -16.70 9.20 4 13 -22 24.00 7.90 4 13 -22 34.10 10.40 4 13 -22 5.20 8.20 -4 -13 22 34.40 10.80 -4 -13 22 24.70 9.60 3 13 -22 -3.00 9.50 3 13 -22 17.70 7.50 3 13 -22 1.40 7.10 -3 -13 22 5.30 9.00 2 13 -22 17.50 7.30 2 13 -22 18.50 9.40 2 13 -22 37.50 8.60 -2 -13 22 36.20 10.30 1 13 -22 5.60 9.60 1 13 -22 8.40 7.30 -1 -13 22 1.90 8.00 -1 -13 22 16.80 9.10 0 13 -22 19.40 10.40 0 13 -22 24.70 7.50 0 13 -22 11.60 7.40 0 -13 22 4.40 7.60 0 -13 22 0.10 8.80 -1 13 -22 29.40 8.90 -1 13 -22 30.60 11.00 -1 13 -22 33.10 8.30 1 -13 22 47.10 10.50 1 -13 22 17.70 8.30 1 -13 22 41.20 10.00 -2 13 -22 44.80 8.40 -2 13 -22 42.10 12.30 -2 13 -22 31.30 8.70 2 -13 22 31.10 9.80 2 -13 22 38.90 8.80 2 -13 22 51.49 10.20 -3 13 -22 18.50 10.70 -3 13 -22 10.00 8.60 -3 13 -22 13.30 8.30 3 -13 22 9.50 8.40 3 -13 22 10.20 8.60 -4 13 -22 36.50 9.00 -4 13 -22 50.39 12.30 -4 13 -22 27.30 8.30 4 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22 83.39 10.50 -3 -12 22 119.29 14.50 2 12 -22 55.89 8.70 2 12 -22 66.19 11.10 2 12 -22 78.69 11.30 -2 -12 22 62.19 10.80 -2 -12 22 39.50 10.90 1 12 -22 -5.00 6.80 1 12 -22 -3.00 8.80 1 12 -22 10.80 7.30 -1 -12 22 -10.20 8.00 0 12 -22 11.10 9.40 0 12 -22 7.50 7.90 0 12 -22 2.80 7.10 0 -12 22 16.20 7.50 0 -12 22 2.00 8.00 -1 12 -22 -13.60 8.70 -1 12 -22 -3.60 6.90 -1 12 -22 -13.50 6.50 1 -12 22 -11.00 7.40 1 -12 22 -7.20 8.10 1 -12 22 3.90 7.20 -2 12 -22 3.50 6.90 -2 12 -22 11.60 9.70 -2 12 -22 -6.70 7.00 2 -12 22 11.90 8.60 2 -12 22 -9.70 11.30 2 -12 22 -7.10 8.30 2 -12 22 19.90 8.40 -3 12 -22 23.80 8.00 -3 12 -22 -2.60 7.10 -3 12 -22 17.10 10.90 3 -12 22 21.10 9.00 3 -12 22 1.40 7.80 3 -12 22 13.30 8.40 -4 12 -22 2.50 8.00 -4 12 -22 -13.30 9.80 -4 12 -22 -0.30 7.60 4 -12 22 0.00 8.70 4 -12 22 14.50 8.80 -5 12 -22 37.70 9.30 -5 12 -22 34.90 8.90 -5 12 -22 45.00 12.30 -5 12 -22 34.00 8.30 5 -12 22 27.10 9.00 5 -12 22 30.80 8.70 5 -12 22 38.00 10.00 -6 12 -22 -9.20 11.10 -6 12 -22 2.00 8.90 -6 12 -22 12.60 8.20 -7 12 -22 27.60 12.40 -7 12 -22 40.90 10.70 -7 12 -22 37.50 8.80 -8 12 -22 8.70 9.30 -8 12 -22 4.60 11.80 9 11 -22 19.80 9.30 -9 -11 22 26.20 11.50 -9 -11 22 12.00 10.50 8 11 -22 16.80 8.40 8 11 -22 26.40 8.70 -8 -11 22 14.20 9.70 -8 -11 22 17.80 10.50 7 11 -22 28.60 8.60 7 11 -22 26.00 10.30 7 11 -22 42.40 8.00 -7 -11 22 43.70 9.70 -7 -11 22 42.20 10.80 6 11 -22 64.69 10.90 6 11 -22 42.80 8.20 6 11 -22 54.59 9.00 -6 -11 22 47.40 9.70 -6 -11 22 70.99 12.30 5 11 -22 54.89 8.80 5 11 -22 72.59 11.10 5 11 -22 50.99 8.40 -5 -11 22 45.50 10.60 -5 -11 22 48.60 9.50 4 11 -22 116.69 14.30 4 11 -22 82.19 11.00 4 11 -22 81.89 12.20 4 11 -22 97.39 11.40 -4 -11 22 69.49 9.70 -4 -11 22 67.99 11.20 3 11 -22 60.79 10.30 3 11 -22 79.89 9.10 3 11 -22 80.39 11.10 3 11 -22 67.89 11.30 -3 -11 22 96.39 13.60 -3 -11 22 54.99 8.80 2 11 -22 -4.30 6.00 2 11 -22 -7.30 6.20 2 11 -22 18.20 9.30 -2 -11 22 -7.30 8.20 -2 -11 22 5.40 9.80 1 11 -22 1.00 6.70 1 11 -22 -10.20 8.50 1 11 -22 3.00 6.70 1 11 -22 0.00 6.40 -1 -11 22 9.70 8.60 -1 -11 22 2.90 7.10 0 11 -22 23.10 10.20 0 11 -22 5.90 6.60 0 11 -22 15.30 6.50 0 -11 22 11.00 8.80 0 -11 22 23.10 8.80 -1 11 -22 2.90 6.60 -1 11 -22 18.00 9.50 -1 11 -22 -1.90 6.30 1 -11 22 -0.90 8.10 1 -11 22 15.70 9.30 1 -11 22 11.30 8.90 1 -11 22 1.20 8.80 -2 11 -22 3.40 9.50 -2 11 -22 13.90 7.40 -2 11 -22 -5.30 7.00 2 -11 22 -4.90 8.20 2 -11 22 -0.50 7.90 2 -11 22 -2.20 8.80 2 -11 22 4.70 7.40 2 -11 22 9.00 9.00 -3 11 -22 54.39 11.80 -3 11 -22 41.00 8.50 -3 11 -22 48.70 8.90 3 -11 22 16.90 8.00 3 -11 22 35.70 9.20 3 -11 22 35.20 11.50 -4 11 -22 27.00 8.00 -4 11 -22 24.40 10.70 -4 11 -22 11.00 7.60 4 -11 22 23.20 8.80 4 -11 22 14.40 8.40 -5 11 -22 97.79 12.90 -5 11 -22 102.49 12.40 -5 11 -22 134.29 12.60 -5 11 -22 92.69 15.10 5 -11 22 117.99 14.10 5 -11 22 87.79 12.10 -6 11 -22 88.29 14.60 -6 11 -22 119.49 13.50 -6 11 -22 103.49 13.40 -7 11 -22 9.30 8.50 -7 11 -22 -8.00 9.20 -8 11 -22 30.40 13.00 -8 11 -22 19.10 9.00 -9 11 -22 4.20 9.30 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8.60 9.10 0 10 -22 6.40 6.60 0 10 -22 3.20 6.40 0 -10 22 16.90 8.40 0 -10 22 8.20 7.90 0 -10 22 13.60 6.80 -1 10 -22 10.60 7.20 -1 10 -22 8.10 6.50 -1 10 -22 19.70 9.30 1 -10 22 16.60 8.50 1 -10 22 -9.30 11.50 1 -10 22 3.80 8.10 -2 10 -22 116.29 12.20 -2 10 -22 121.99 12.30 -2 10 -22 138.99 16.00 -2 10 -22 122.19 11.60 2 -10 22 109.39 16.60 2 -10 22 114.09 11.70 2 -10 22 133.49 15.10 -3 10 -22 66.69 9.70 -3 10 -22 63.59 8.80 -3 10 -22 77.69 12.50 3 -10 22 71.49 15.10 3 -10 22 46.80 10.80 3 -10 22 53.19 8.70 -4 10 -22 53.29 8.80 -4 10 -22 15.20 10.70 -4 10 -22 35.40 8.30 4 -10 22 23.30 13.40 4 -10 22 36.60 8.40 -5 10 -22 107.29 12.50 -5 10 -22 114.69 16.60 -5 10 -22 113.69 12.50 -5 10 -22 103.89 12.30 -6 10 -22 34.20 11.70 -6 10 -22 21.00 8.10 -6 10 -22 32.90 9.70 -7 10 -22 38.80 8.90 -7 10 -22 23.90 12.20 -8 10 -22 25.70 9.60 -8 10 -22 8.00 13.30 -9 10 -22 18.40 13.70 10 9 -22 8.50 7.80 -10 -9 22 25.00 10.30 -10 -9 22 12.20 11.20 9 9 -22 -15.70 11.70 9 9 -22 4.20 7.60 9 9 -22 -3.10 9.00 -9 -9 22 10.90 10.00 -9 -9 22 5.30 9.10 8 9 -22 20.70 7.30 8 9 -22 -5.10 7.30 8 9 -22 1.20 8.40 -8 -9 22 -5.10 8.50 7 9 -22 4.70 7.00 7 9 -22 6.70 6.80 7 9 -22 4.30 7.50 -7 -9 22 16.50 8.80 -7 -9 22 9.60 8.60 6 9 -22 8.30 6.40 6 9 -22 -0.80 7.50 6 9 -22 -5.70 6.50 -6 -9 22 -3.80 8.40 -6 -9 22 -4.20 7.60 5 9 -22 47.90 11.80 5 9 -22 65.59 8.80 5 9 -22 90.29 11.90 -5 -9 22 66.49 11.10 -5 -9 22 50.19 9.20 4 9 -22 114.69 11.10 4 9 -22 114.19 11.70 4 9 -22 100.09 10.90 4 9 -22 85.89 11.30 -4 -9 22 97.09 12.90 -4 -9 22 94.09 13.00 3 9 -22 21.40 6.20 3 9 -22 18.30 6.80 3 9 -22 13.40 8.70 3 9 -22 12.10 6.50 -3 -9 22 10.70 7.20 -3 -9 22 14.60 8.30 -3 -9 22 -10.70 8.20 2 9 -22 16.60 6.90 2 9 -22 19.30 9.00 2 9 -22 34.20 6.70 2 9 -22 24.30 7.50 -2 -9 22 21.90 8.30 -2 -9 22 34.70 7.60 1 9 -22 85.69 10.10 1 9 -22 110.89 14.50 1 9 -22 82.59 10.40 1 9 -22 81.09 9.70 -1 -9 22 92.69 14.50 -1 -9 22 76.29 10.50 -1 -9 22 64.89 8.80 0 9 -22 148.89 11.70 0 9 -22 124.99 14.70 0 9 -22 139.09 12.50 0 9 -22 113.29 10.90 0 -9 22 135.19 11.90 -1 9 -22 116.79 12.20 -1 9 -22 139.89 15.10 -1 9 -22 120.99 11.10 -1 9 -22 134.29 11.70 1 -9 22 128.69 18.70 1 -9 22 132.59 14.60 1 -9 22 102.89 11.70 1 -9 22 118.09 14.10 -2 9 -22 94.29 12.90 -2 9 -22 94.29 11.60 -2 9 -22 83.79 11.50 -2 9 -22 84.39 10.90 2 -9 22 126.39 13.40 -3 9 -22 1.60 7.20 -3 9 -22 10.90 10.20 -3 9 -22 6.80 6.90 -3 9 -22 16.00 9.60 3 -9 22 6.10 6.90 3 -9 22 7.90 7.40 3 -9 22 8.50 8.30 -4 9 -22 32.60 7.90 -4 9 -22 35.00 7.90 -4 9 -22 39.10 8.40 -4 9 -22 38.60 11.40 4 -9 22 43.80 8.80 4 -9 22 46.50 8.30 -5 9 -22 29.50 8.50 -5 9 -22 38.10 9.00 -5 9 -22 34.60 11.50 -5 9 -22 15.00 7.60 -6 9 -22 17.40 8.70 -6 9 -22 48.60 11.90 -7 9 -22 27.70 12.50 -8 9 -22 40.20 14.40 -9 9 -22 22.50 14.30 11 8 -22 34.70 10.00 11 8 -22 53.19 11.40 -11 -8 22 29.30 11.10 -11 -8 22 32.40 10.90 10 8 -22 -17.80 7.70 10 8 -22 -0.80 8.60 -10 -8 22 -7.30 8.50 -10 -8 22 -10.80 9.70 9 8 -22 4.60 8.40 9 8 -22 9.90 7.30 -9 -8 22 -12.50 8.40 -9 -8 22 7.30 9.70 8 8 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194.58 15.50 0 -8 22 127.89 13.40 0 -8 22 159.18 13.70 0 -8 22 149.09 12.30 -1 8 -22 25.90 7.10 -1 8 -22 30.00 8.00 -1 8 -22 41.40 10.30 -1 8 -22 19.10 6.70 1 -8 22 33.70 7.40 1 -8 22 45.30 8.90 1 -8 22 46.20 8.60 -2 8 -22 4.20 6.10 -2 8 -22 26.80 7.10 -2 8 -22 11.50 9.90 -2 8 -22 10.10 6.60 2 -8 22 15.20 7.90 2 -8 22 9.90 7.60 2 -8 22 2.00 7.80 -3 8 -22 31.40 7.90 -3 8 -22 23.20 9.80 -3 8 -22 25.30 8.10 -3 8 -22 32.70 7.80 3 -8 22 32.70 8.30 3 -8 22 28.20 7.70 3 -8 22 19.20 7.10 -4 8 -22 40.20 8.70 -4 8 -22 44.80 8.50 -4 8 -22 40.60 11.10 -4 8 -22 35.90 7.90 4 -8 22 18.90 10.30 -5 8 -22 9.20 7.70 -5 8 -22 22.90 10.90 -5 8 -22 15.10 8.10 -6 8 -22 3.40 10.60 -7 8 -22 5.00 11.80 -8 8 -22 12.50 12.70 -9 8 -22 2.10 13.20 11 7 -22 1.70 7.70 11 7 -22 9.50 9.30 -11 -7 22 19.40 10.90 -11 -7 22 18.10 10.20 10 7 -22 0.40 7.40 10 7 -22 -7.10 8.00 -10 -7 22 -0.10 8.60 -10 -7 22 17.30 9.70 9 7 -22 0.50 7.60 9 7 -22 -11.50 6.60 -9 -7 22 12.80 8.60 -9 -7 22 -2.00 9.10 8 7 -22 -2.30 7.30 -8 -7 22 7.40 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7.60 -3 -6 23 17.90 8.50 2 6 -23 2.50 6.10 2 6 -23 -12.00 6.10 -2 -6 23 0.50 7.50 -2 -6 23 3.30 7.70 -2 -6 23 4.80 8.90 1 6 -23 2.80 6.80 1 6 -23 2.60 5.90 -1 -6 23 2.20 7.60 -1 -6 23 -5.50 7.90 0 6 -23 9.90 6.80 0 6 -23 10.40 6.80 0 -6 23 16.80 10.20 0 -6 23 7.00 8.20 0 -6 23 24.70 8.50 -1 6 -23 15.50 7.00 -1 6 -23 5.20 6.60 1 -6 23 11.50 10.00 1 -6 23 -10.30 8.30 1 -6 23 -9.40 7.70 -2 6 -23 0.90 6.80 -2 6 -23 -2.10 10.50 -2 6 -23 -0.70 6.30 2 -6 23 15.30 9.80 -3 6 -23 0.40 10.50 -3 6 -23 20.40 7.90 -3 6 -23 23.50 7.40 -4 6 -23 8.10 8.00 -4 6 -23 -6.10 7.20 -4 6 -23 14.60 11.80 -5 6 -23 2.10 8.10 -5 6 -23 -9.30 11.40 -6 6 -23 15.30 12.40 -7 6 -23 118.89 16.90 11 5 -23 23.90 9.00 11 5 -23 4.30 9.40 -11 -5 23 4.70 9.70 -11 -5 23 -14.40 10.70 10 5 -23 -4.90 7.50 10 5 -23 1.50 8.50 -10 -5 23 -6.80 9.00 -10 -5 23 -8.40 9.00 9 5 -23 17.30 8.00 9 5 -23 25.80 8.80 -9 -5 23 47.10 11.10 -9 -5 23 12.90 9.20 8 5 -23 122.09 13.10 8 5 -23 106.09 11.80 -8 -5 23 122.19 13.30 -8 -5 23 103.79 14.20 7 5 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-0.0079 0 5 17 3.8730 -0.0127 0 5 18 3.4555 -0.0129 0 5 19 2.7249 -0.0070 0 5 20 1.9510 0.0016 0 5 21 1.2797 0.0070 0 5 22 0.7651 0.0058 0 5 23 0.4289 -0.0010 0 6 0 3.3184 0.0023 0 6 1 2.7708 -0.0083 0 6 2 1.2681 -0.0136 0 6 3 -0.8822 -0.0069 0 6 4 -3.2120 0.0053 0 6 5 -5.2475 0.0113 0 6 6 -6.6044 0.0071 0 6 7 -7.0385 -0.0001 0 6 8 -6.4949 -0.0016 0 6 9 -5.1307 0.0027 0 6 10 -3.2464 0.0063 0 6 11 -1.1569 0.0048 0 6 12 0.8789 0.0009 0 6 13 2.6232 -0.0008 0 6 14 3.8212 -0.0005 0 6 15 4.2746 -0.0019 0 6 16 3.9812 -0.0061 0 6 17 3.1713 -0.0090 0 6 18 2.1769 -0.0053 0 6 19 1.2602 0.0057 0 6 20 0.5548 0.0184 0 6 21 0.1136 0.0254 0 6 22 -0.0605 0.0232 0 7 0 1.9323 0.0034 0 7 1 -0.1689 0.0049 0 7 2 -2.5850 0.0104 0 7 3 -4.8985 0.0132 0 7 4 -6.6655 0.0080 0 7 5 -7.4829 -0.0022 0 7 6 -7.1396 -0.0084 0 7 7 -5.7450 -0.0056 0 7 8 -3.6881 0.0020 0 7 9 -1.4329 0.0062 0 7 10 0.6743 0.0035 0 7 11 2.4325 -0.0017 0 7 12 3.6880 -0.0032 0 7 13 4.2843 0.0003 0 7 14 4.1422 0.0041 0 7 15 3.3689 0.0038 0 7 16 2.2470 0.0004 0 7 17 1.1007 -0.0002 0 7 18 0.1661 0.0072 0 7 19 -0.4393 0.0215 0 7 20 -0.6859 0.0358 0 7 21 -0.6214 0.0417 0 8 0 -2.0661 0.0078 0 8 1 -4.3325 0.0065 0 8 2 -6.1830 -0.0007 0 8 3 -7.2303 -0.0100 0 8 4 -7.1918 -0.0152 0 8 5 -6.0372 -0.0129 0 8 6 -4.0504 -0.0057 0 8 7 -1.7120 0.0005 0 8 8 0.5162 0.0019 0 8 9 2.3272 -0.0007 0 8 10 3.5564 -0.0036 0 8 11 4.1136 -0.0035 0 8 12 3.9782 0.0002 0 8 13 3.2493 0.0048 0 8 14 2.1564 0.0061 0 8 15 0.9857 0.0021 0 8 16 -0.0165 -0.0042 0 8 17 -0.6946 -0.0058 0 8 18 -0.9878 0.0021 0 8 19 -0.9303 0.0166 0 8 20 -0.6465 0.0286 0 8 21 -0.3077 0.0299 0 9 0 -5.8267 -0.0031 0 9 1 -6.8633 -0.0116 0 9 2 -6.8836 -0.0147 0 9 3 -5.8593 -0.0092 0 9 4 -4.0409 -0.0005 0 9 5 -1.8588 0.0032 0 9 6 0.2663 0.0007 0 9 7 2.0475 -0.0025 0 9 8 3.3102 -0.0015 0 9 9 3.9249 0.0023 0 9 10 3.8239 0.0046 0 9 11 3.0921 0.0042 0 9 12 1.9910 0.0031 0 9 13 0.8483 0.0019 0 9 14 -0.0870 -0.0020 0 9 15 -0.6938 -0.0099 0 9 16 -0.9382 -0.0173 0 9 17 -0.8480 -0.0173 0 9 18 -0.5354 -0.0082 0 9 19 -0.1850 0.0037 0 9 20 0.0462 0.0101 0 10 0 -6.7222 -0.0049 0 10 1 -5.6657 -0.0008 0 10 2 -3.8206 0.0099 0 10 3 -1.6594 0.0156 0 10 4 0.3379 0.0090 0 10 5 1.8969 -0.0036 0 10 6 2.9639 -0.0088 0 10 7 3.5411 -0.0015 0 10 8 3.5687 0.0099 0 10 9 3.0050 0.0136 0 10 10 1.9876 0.0080 0 10 11 0.8440 0.0007 0 10 12 -0.0902 -0.0022 0 10 13 -0.6470 -0.0025 0 10 14 -0.8287 -0.0048 0 10 15 -0.7052 -0.0090 0 10 16 -0.3731 -0.0102 0 10 17 0.0071 -0.0061 0 10 18 0.2392 -0.0003 0 10 19 0.2293 0.0028 0 11 0 -3.7231 0.0060 0 11 1 -1.5443 0.0138 0 11 2 0.5140 0.0125 0 11 3 2.0521 -0.0003 0 11 4 2.9390 -0.0138 0 11 5 3.2713 -0.0147 0 11 6 3.1810 -0.0024 0 11 7 2.7136 0.0103 0 11 8 1.9050 0.0120 0 11 9 0.9205 0.0045 0 11 10 0.0417 -0.0021 0 11 11 -0.5054 -0.0015 0 11 12 -0.6758 0.0028 0 11 13 -0.5584 0.0056 0 11 14 -0.2605 0.0067 0 11 15 0.1108 0.0089 0 11 16 0.3986 0.0119 0 11 17 0.4388 0.0114 0 11 18 0.2120 0.0062 0 12 0 0.4069 0.0012 0 12 1 1.9830 -0.0038 0 12 2 2.9374 -0.0125 0 12 3 3.2405 -0.0157 0 12 4 3.0181 -0.0087 0 12 5 2.4387 0.0026 0 12 6 1.6450 0.0072 0 12 7 0.7826 0.0025 0 12 8 0.0390 -0.0033 0 12 9 -0.4126 -0.0019 0 12 10 -0.5202 0.0050 0 12 11 -0.3728 0.0094 0 12 12 -0.1020 0.0081 0 12 13 0.2075 0.0063 0 12 14 0.4904 0.0093 0 12 15 0.6350 0.0143 0 12 16 0.5322 0.0137 0 12 17 0.2150 0.0054 0 13 0 2.5645 -0.0121 0 13 1 2.9428 -0.0131 0 13 2 2.8141 -0.0053 0 13 3 2.2892 0.0066 0 13 4 1.5141 0.0116 0 13 5 0.6673 0.0045 0 13 6 -0.0483 -0.0069 0 13 7 -0.4579 -0.0093 0 13 8 -0.5014 0.0004 0 13 9 -0.2709 0.0113 0 13 10 0.0577 0.0114 0 13 11 0.3495 0.0013 0 13 12 0.5624 -0.0073 0 13 13 0.6863 -0.0063 0 13 14 0.6759 0.0006 0 13 15 0.4894 0.0041 0 13 16 0.1875 0.0008 0 14 0 2.2545 -0.0063 0 14 1 1.8416 0.0032 0 14 2 1.2497 0.0125 0 14 3 0.5983 0.0113 0 14 4 0.0264 -0.0009 0 14 5 -0.3188 -0.0121 0 14 6 -0.3489 -0.0106 0 14 7 -0.1007 0.0014 0 14 8 0.2736 0.0102 0 14 9 0.5998 0.0064 0 14 10 0.7794 -0.0051 0 14 11 0.8069 -0.0125 0 14 12 0.7135 -0.0112 0 14 13 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0.0048 1 3 15 0.3048 0.0048 1 3 16 1.8574 0.0032 1 3 17 3.1205 0.0026 1 3 18 3.7582 0.0049 1 3 19 3.6446 0.0083 1 3 20 2.9593 0.0096 1 3 21 2.0363 0.0092 1 3 22 1.1714 0.0112 1 3 23 0.5470 0.0157 1 4 0 -1.3541 0.0252 1 4 1 -0.1462 0.0216 1 4 2 0.5086 0.0038 1 4 3 0.2234 -0.0138 1 4 4 -0.8144 -0.0179 1 4 5 -2.1846 -0.0089 1 4 6 -3.6034 0.0016 1 4 7 -4.9177 0.0049 1 4 8 -5.8756 0.0022 1 4 9 -6.1065 -0.0006 1 4 10 -5.3997 -0.0012 1 4 11 -3.9183 -0.0011 1 4 12 -2.0647 -0.0013 1 4 13 -0.1753 -0.0011 1 4 14 1.5852 -0.0009 1 4 15 3.0739 -0.0022 1 4 16 4.0537 -0.0048 1 4 17 4.3083 -0.0065 1 4 18 3.8422 -0.0053 1 4 19 2.9113 -0.0035 1 4 20 1.8673 -0.0042 1 4 21 0.9954 -0.0080 1 4 22 0.4527 -0.0123 1 4 23 0.2530 -0.0151 1 5 0 3.2656 0.0001 1 5 1 2.4409 -0.0171 1 5 2 0.6502 -0.0240 1 5 3 -1.6252 -0.0141 1 5 4 -3.8857 0.0029 1 5 5 -5.7773 0.0117 1 5 6 -7.0343 0.0079 1 5 7 -7.3980 0.0003 1 5 8 -6.7103 -0.0018 1 5 9 -5.0903 0.0016 1 5 10 -2.9372 0.0042 1 5 11 -0.7071 0.0029 1 5 12 1.3031 0.0006 1 5 13 2.9515 -0.0001 1 5 14 4.1068 -0.0003 1 5 15 4.6057 -0.0023 1 5 16 4.3738 -0.0051 1 5 17 3.5418 -0.0060 1 5 18 2.4049 -0.0053 1 5 19 1.2822 -0.0065 1 5 20 0.4193 -0.0114 1 5 21 -0.0438 -0.0168 1 5 22 -0.1073 -0.0177 1 6 0 1.8960 -0.0108 1 6 1 -0.6340 -0.0039 1 6 2 -3.3330 0.0098 1 6 3 -5.7397 0.0190 1 6 4 -7.4758 0.0154 1 6 5 -8.2061 0.0031 1 6 6 -7.7179 -0.0056 1 6 7 -6.0871 -0.0036 1 6 8 -3.7256 0.0044 1 6 9 -1.1955 0.0086 1 6 10 1.0636 0.0061 1 6 11 2.8438 0.0017 1 6 12 4.0665 0.0006 1 6 13 4.6519 0.0023 1 6 14 4.5362 0.0034 1 6 15 3.7856 0.0025 1 6 16 2.6355 0.0016 1 6 17 1.3950 0.0016 1 6 18 0.3272 0.0012 1 6 19 -0.3939 -0.0005 1 6 20 -0.6838 -0.0018 1 6 21 -0.5778 0.0003 1 6 22 -0.2591 0.0053 1 7 0 -2.4913 0.0141 1 7 1 -5.0212 0.0175 1 7 2 -7.0335 0.0115 1 7 3 -8.1463 -0.0012 1 7 4 -8.0624 -0.0116 1 7 5 -6.7231 -0.0124 1 7 6 -4.4298 -0.0048 1 7 7 -1.7555 0.0031 1 7 8 0.7243 0.0046 1 7 9 2.6567 0.0003 1 7 10 3.9235 -0.0042 1 7 11 4.5094 -0.0046 1 7 12 4.4184 -0.0016 1 7 13 3.7164 0.0017 1 7 14 2.5968 0.0030 1 7 15 1.3505 0.0022 1 7 16 0.2557 0.0004 1 7 17 -0.5080 -0.0014 1 7 18 -0.8725 -0.0014 1 7 19 -0.8634 0.0013 1 7 20 -0.5930 0.0058 1 7 21 -0.2394 0.0093 1 8 0 -6.2886 0.0020 1 8 1 -7.5240 -0.0090 1 8 2 -7.6941 -0.0153 1 8 3 -6.6899 -0.0121 1 8 4 -4.7029 -0.0033 1 8 5 -2.2015 0.0028 1 8 6 0.2601 0.0022 1 8 7 2.2627 -0.0023 1 8 8 3.6037 -0.0053 1 8 9 4.2311 -0.0048 1 8 10 4.1638 -0.0027 1 8 11 3.4936 -0.0010 1 8 12 2.4212 0.0003 1 8 13 1.2308 0.0011 1 8 14 0.1985 0.0000 1 8 15 -0.4906 -0.0039 1 8 16 -0.7719 -0.0087 1 8 17 -0.6960 -0.0104 1 8 18 -0.4101 -0.0074 1 8 19 -0.1026 -0.0024 1 8 20 0.0901 0.0000 1 9 0 -7.2140 -0.0120 1 9 1 -6.3014 -0.0052 1 9 2 -4.4845 0.0087 1 9 3 -2.1828 0.0169 1 9 4 0.0865 0.0113 1 9 5 1.9313 -0.0022 1 9 6 3.1835 -0.0102 1 9 7 3.8171 -0.0063 1 9 8 3.8343 0.0034 1 9 9 3.2699 0.0087 1 9 10 2.2779 0.0069 1 9 11 1.1444 0.0032 1 9 12 0.1729 0.0021 1 9 13 -0.4435 0.0022 1 9 14 -0.6516 -0.0002 1 9 15 -0.5025 -0.0044 1 9 16 -0.1365 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2 -18 16 -0.0768 0.0105 2 -18 17 0.8230 0.0078 2 -18 18 1.5686 0.0096 2 -18 19 1.7671 0.0164 2 -18 20 1.3201 0.0214 2 -18 21 0.5557 0.0177 2 -17 0 0.2129 -0.0134 2 -17 1 0.5755 0.0007 2 -17 2 0.8706 0.0131 2 -17 3 0.9815 0.0197 2 -17 4 0.8099 0.0209 2 -17 5 0.3378 0.0182 2 -17 6 -0.3557 0.0128 2 -17 7 -1.1351 0.0074 2 -17 8 -1.8465 0.0053 2 -17 9 -2.3302 0.0065 2 -17 10 -2.4579 0.0074 2 -17 11 -2.2070 0.0056 2 -17 12 -1.6807 0.0030 2 -17 13 -1.0044 0.0035 2 -17 14 -0.1994 0.0078 2 -17 15 0.7812 0.0123 2 -17 16 1.8502 0.0138 2 -17 17 2.6690 0.0128 2 -17 18 2.8329 0.0111 2 -17 19 2.2303 0.0083 2 -17 20 1.1986 0.0024 2 -17 21 0.2802 -0.0065 2 -17 22 -0.1889 -0.0139 2 -16 0 1.4861 0.0227 2 -16 1 1.5529 0.0239 2 -16 2 1.2732 0.0169 2 -16 3 0.5811 0.0084 2 -16 4 -0.4430 0.0014 2 -16 5 -1.5729 -0.0043 2 -16 6 -2.5397 -0.0074 2 -16 7 -3.1423 -0.0056 2 -16 8 -3.2869 -0.0001 2 -16 9 -2.9690 0.0035 2 -16 10 -2.2579 0.0014 2 -16 11 -1.2866 -0.0036 2 -16 12 -0.2104 -0.0049 2 -16 13 0.8533 -0.0001 2 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0.0063 2 1 18 1.7644 0.0116 2 1 19 2.6417 0.0144 2 1 20 3.0333 0.0103 2 1 21 2.8414 0.0046 2 1 22 2.1506 0.0131 2 1 23 1.2233 0.0447 2 1 24 0.4202 0.0838 2 2 0 -8.7289 -0.0257 2 2 1 -8.7779 -0.0046 2 2 2 -6.9282 0.0129 2 2 3 -4.6513 0.0162 2 2 4 -2.9738 0.0086 2 2 5 -2.0530 0.0009 2 2 6 -1.6368 -0.0011 2 2 7 -1.6581 0.0006 2 2 8 -2.2318 0.0018 2 2 9 -3.2193 0.0016 2 2 10 -4.0754 0.0009 2 2 11 -4.2346 0.0001 2 2 12 -3.5535 -0.0007 2 2 13 -2.3042 -0.0008 2 2 14 -0.8259 0.0009 2 2 15 0.6912 0.0045 2 2 16 2.1145 0.0092 2 2 17 3.2305 0.0140 2 2 18 3.8013 0.0167 2 2 19 3.7246 0.0166 2 2 20 3.0927 0.0176 2 2 21 2.1321 0.0289 2 2 22 1.1345 0.0540 2 2 23 0.3908 0.0800 2 3 0 -3.3198 0.0340 2 3 1 -1.7007 0.0301 2 3 2 -0.7530 0.0112 2 3 3 -0.8725 -0.0076 2 3 4 -1.7158 -0.0135 2 3 5 -2.7629 -0.0079 2 3 6 -3.7970 -0.0013 2 3 7 -4.8079 -0.0002 2 3 8 -5.6113 -0.0027 2 3 9 -5.7891 -0.0045 2 3 10 -5.0448 -0.0055 2 3 11 -3.5004 -0.0075 2 3 12 -1.5758 -0.0097 2 3 13 0.3483 -0.0097 2 3 14 2.0719 -0.0067 2 3 15 3.4518 -0.0025 2 3 16 4.2950 0.0012 2 3 17 4.4451 0.0034 2 3 18 3.9256 0.0034 2 3 19 2.9470 0.0016 2 3 20 1.8047 0.0018 2 3 21 0.7949 0.0088 2 3 22 0.1586 0.0208 2 3 23 -0.0171 0.0269 2 4 0 2.3629 0.0061 2 4 1 1.5153 -0.0187 2 4 2 -0.3621 -0.0292 2 4 3 -2.6161 -0.0195 2 4 4 -4.6654 -0.0019 2 4 5 -6.2395 0.0066 2 4 6 -7.2179 0.0024 2 4 7 -7.4041 -0.0051 2 4 8 -6.5928 -0.0071 2 4 9 -4.8349 -0.0046 2 4 10 -2.5242 -0.0036 2 4 11 -0.1703 -0.0055 2 4 12 1.8751 -0.0071 2 4 13 3.4576 -0.0059 2 4 14 4.4793 -0.0032 2 4 15 4.8342 -0.0008 2 4 16 4.4955 0.0009 2 4 17 3.5988 0.0008 2 4 18 2.3994 -0.0044 2 4 19 1.1776 -0.0151 2 4 20 0.1953 -0.0247 2 4 21 -0.3379 -0.0247 2 4 22 -0.3665 -0.0135 2 5 0 1.2804 -0.0278 2 5 1 -1.5534 -0.0188 2 5 2 -4.3906 0.0018 2 5 3 -6.7057 0.0176 2 5 4 -8.2019 0.0165 2 5 5 -8.6735 0.0030 2 5 6 -7.9691 -0.0074 2 5 7 -6.1419 -0.0063 2 5 8 -3.5691 0.0013 2 5 9 -0.8278 0.0056 2 5 10 1.5840 0.0041 2 5 11 3.4097 0.0017 2 5 12 4.5678 0.0020 2 5 13 5.0211 0.0039 2 5 14 4.7688 0.0054 2 5 15 3.9249 0.0069 2 5 16 2.7277 0.0078 2 5 17 1.4447 0.0039 2 5 18 0.2977 -0.0080 2 5 19 -0.5299 -0.0228 2 5 20 -0.8928 -0.0289 2 5 21 -0.7731 -0.0190 2 5 22 -0.3641 0.0013 2 6 0 -3.4010 0.0110 2 6 1 -6.1013 0.0226 2 6 2 -8.0849 0.0213 2 6 3 -9.0283 0.0073 2 6 4 -8.7131 -0.0079 2 6 5 -7.1203 -0.0123 2 6 6 -4.5598 -0.0052 2 6 7 -1.6216 0.0039 2 6 8 1.0797 0.0061 2 6 9 3.1531 0.0020 2 6 10 4.4675 -0.0020 2 6 11 5.0201 -0.0021 2 6 12 4.8413 -0.0003 2 6 13 4.0318 0.0013 2 6 14 2.8186 0.0029 2 6 15 1.5045 0.0048 2 6 16 0.3468 0.0043 2 6 17 -0.5045 -0.0022 2 6 18 -0.9760 -0.0122 2 6 19 -1.0440 -0.0179 2 6 20 -0.7743 -0.0132 2 6 21 -0.3528 -0.0004 2 7 0 -7.1546 0.0123 2 7 1 -8.4195 -0.0007 2 7 2 -8.5197 -0.0123 2 7 3 -7.3564 -0.0143 2 7 4 -5.1217 -0.0067 2 7 5 -2.3131 0.0027 2 7 6 0.4443 0.0057 2 7 7 2.6571 0.0013 2 7 8 4.0973 -0.0051 2 7 9 4.7427 -0.0084 2 7 10 4.6545 -0.0081 2 7 11 3.9411 -0.0067 2 7 12 2.7983 -0.0053 2 7 13 1.5115 -0.0032 2 7 14 0.3701 -0.0008 2 7 15 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-0.6151 -0.1133 18 -16 7 -0.3790 -0.1167 18 -16 8 -0.1639 -0.0755 18 -15 0 -0.6831 -0.0776 18 -15 1 -0.7312 -0.0756 18 -15 2 -0.7032 -0.0630 18 -15 3 -0.6603 -0.0586 18 -15 4 -0.5607 -0.0707 18 -15 5 -0.3663 -0.0863 18 -15 6 -0.1459 -0.0805 18 -15 7 -0.0241 -0.0410 18 -15 8 -0.0431 0.0140 18 -15 9 -0.1222 0.0475 18 -14 0 -0.5266 0.0131 18 -14 1 -0.4138 0.0133 18 -14 2 -0.2944 0.0070 18 -14 3 -0.1382 -0.0036 18 -14 4 0.0583 -0.0128 18 -14 5 0.1840 -0.0114 18 -14 6 0.1161 0.0038 18 -14 7 -0.1100 0.0220 18 -14 8 -0.3032 0.0227 18 -14 9 -0.3125 -0.0037 18 -13 0 0.0376 0.0477 18 -13 1 0.1179 0.0268 18 -13 2 0.2213 0.0163 18 -13 3 0.3636 0.0138 18 -13 4 0.4090 0.0107 18 -13 5 0.2134 0.0021 18 -13 6 -0.1627 -0.0121 18 -13 7 -0.4625 -0.0303 18 -13 8 -0.4842 -0.0488 18 -13 9 -0.2813 -0.0601 18 -13 10 -0.0777 -0.0562 18 -12 0 0.3030 -0.0249 18 -12 1 0.2791 -0.0193 18 -12 2 0.3599 -0.0051 18 -12 3 0.4102 -0.0004 18 -12 4 0.2455 -0.0130 18 -12 5 -0.1187 -0.0347 18 -12 6 -0.4420 -0.0494 18 -12 7 -0.5032 -0.0454 18 -12 8 -0.3188 -0.0231 18 -12 9 -0.0859 0.0052 18 -12 10 0.0498 0.0242 18 -11 0 0.0032 -0.0174 18 -11 1 0.0689 0.0052 18 -11 2 0.1973 0.0130 18 -11 3 0.1713 0.0048 18 -11 4 -0.0548 -0.0097 18 -11 5 -0.2991 -0.0153 18 -11 6 -0.3612 -0.0017 18 -11 7 -0.2268 0.0278 18 -11 8 -0.0290 0.0556 18 -11 9 0.1383 0.0624 18 -11 10 0.2877 0.0430 18 -10 0 -0.3146 0.0321 18 -10 1 -0.1118 0.0237 18 -10 2 -0.0246 0.0150 18 -10 3 -0.1210 0.0108 18 -10 4 -0.2510 0.0113 18 -10 5 -0.2440 0.0176 18 -10 6 -0.1002 0.0291 18 -10 7 0.0610 0.0379 18 -10 8 0.1870 0.0327 18 -10 9 0.3338 0.0117 18 -10 10 0.5167 -0.0125 18 -9 0 -0.3423 -0.0132 18 -9 1 -0.2403 -0.0164 18 -9 2 -0.3024 -0.0052 18 -9 3 -0.3701 0.0043 18 -9 4 -0.2779 0.0049 18 -9 5 -0.0610 0.0006 18 -9 6 0.1071 -0.0042 18 -9 7 0.1500 -0.0106 18 -9 8 0.1696 -0.0175 18 -9 9 0.2707 -0.0181 18 -9 10 0.3827 -0.0072 18 -8 0 -0.3183 -0.0329 18 -8 1 -0.3873 -0.0091 18 -8 2 -0.4477 0.0045 18 -8 3 -0.3268 0.0032 18 -8 4 -0.0644 -0.0034 18 -8 5 0.1219 -0.0078 18 -8 6 0.0960 -0.0097 18 -8 7 -0.0437 -0.0074 18 -8 8 -0.1046 0.0056 18 -8 9 -0.0389 0.0292 18 -8 10 0.0202 0.0488 18 -7 0 -0.2652 0.0161 18 -7 1 -0.2809 0.0139 18 -7 2 -0.1766 0.0041 18 -7 3 0.0369 0.0007 18 -7 4 0.1848 0.0038 18 -7 5 0.1271 0.0043 18 -7 6 -0.0797 0.0028 18 -7 7 -0.2477 0.0126 18 -7 8 -0.2574 0.0382 18 -7 9 -0.1546 0.0611 18 -7 10 -0.0652 0.0556 18 -6 0 0.0174 -0.0049 18 -6 1 0.1482 -0.0200 18 -6 2 0.2671 -0.0153 18 -6 3 0.3061 -0.0027 18 -6 4 0.2240 -0.0021 18 -6 5 0.0660 -0.0119 18 -6 6 -0.0722 -0.0090 18 -6 7 -0.1198 0.0195 18 -6 8 -0.0655 0.0537 18 -6 9 0.0528 0.0585 18 -5 0 0.4155 -0.0304 18 -5 1 0.5084 -0.0118 18 -5 2 0.4403 0.0057 18 -5 3 0.3088 0.0013 18 -5 4 0.2188 -0.0178 18 -5 5 0.1827 -0.0205 18 -5 6 0.1496 0.0115 18 -5 7 0.1139 0.0572 18 -5 8 0.1373 0.0745 18 -5 9 0.2425 0.0448 18 -4 0 0.6523 0.0290 18 -4 1 0.5785 0.0373 18 -4 2 0.4022 0.0195 18 -4 3 0.3125 -0.0104 18 -4 4 0.3204 -0.0206 18 -4 5 0.2982 0.0066 18 -4 6 0.1934 0.0520 18 -4 7 0.1135 0.0750 18 -4 8 0.1654 0.0530 18 -3 0 0.6771 0.0353 18 -3 1 0.5343 0.0117 18 -3 2 0.4133 -0.0164 18 -3 3 0.3732 -0.0286 18 -3 4 0.3076 -0.0137 18 -3 5 0.1625 0.0172 18 -3 6 0.0510 0.0377 18 -3 7 0.0968 0.0295 18 -3 8 0.2373 -0.0019 18 -2 0 0.5686 -0.0089 18 -2 1 0.4830 -0.0101 18 -2 2 0.4035 -0.0109 18 -2 3 0.2754 -0.0091 18 -2 4 0.0926 -0.0031 18 -2 5 -0.0130 0.0037 18 -2 6 0.0712 0.0049 18 -2 7 0.2574 -0.0016 18 -1 0 0.3681 0.0300 18 -1 1 0.3605 0.0420 18 -1 2 0.2477 0.0332 18 -1 3 0.0385 0.0147 18 -1 4 -0.1002 0.0006 18 -1 5 -0.0219 -0.0029 18 -1 6 0.1960 0.0009 18 0 0 0.2094 0.0438 18 0 1 0.2380 0.0324 18 0 2 0.0666 0.0113 18 0 3 -0.1495 -0.0065 18 0 4 -0.1828 -0.0144 18 0 5 -0.0094 -0.0134 18 1 0 0.2654 -0.0413 18 1 1 0.2223 -0.0338 18 1 2 -0.0362 -0.0244 18 1 3 -0.2345 -0.0198 18 1 4 -0.1976 -0.0209 18 2 0 0.4145 -0.0486 18 2 1 0.2176 -0.0095 18 2 2 -0.0698 0.0104 18 2 3 -0.1810 0.0083 18 3 0 0.3922 0.0168 18 3 1 0.1621 0.0323 19 -17 0 -0.0388 -0.0589 19 -17 1 -0.2481 -0.0832 19 -16 0 -0.3381 -0.0978 19 -16 1 -0.4613 -0.0939 19 -16 2 -0.4467 -0.0739 19 -16 3 -0.3432 -0.0631 19 -16 4 -0.1853 -0.0754 19 -15 0 -0.2540 0.0017 19 -15 1 -0.1667 0.0133 19 -15 2 0.0184 0.0180 19 -15 3 0.2358 0.0086 19 -15 4 0.3908 -0.0105 19 -15 5 0.3819 -0.0228 19 -15 6 0.1968 -0.0144 19 -14 0 0.3413 0.0941 19 -14 1 0.5025 0.0822 19 -14 2 0.6690 0.0708 19 -14 3 0.7433 0.0543 19 -14 4 0.6059 0.0311 19 -14 5 0.2540 0.0080 19 -14 6 -0.1304 -0.0081 19 -13 0 0.8215 0.0385 19 -13 1 0.8347 0.0366 19 -13 2 0.8033 0.0345 19 -13 3 0.6161 0.0155 19 -13 4 0.2456 -0.0194 19 -13 5 -0.1499 -0.0529 19 -13 6 -0.3476 -0.0666 19 -13 7 -0.2862 -0.0560 19 -12 0 0.6316 -0.0052 19 -12 1 0.5359 0.0094 19 -12 2 0.4025 0.0036 19 -12 3 0.1599 -0.0220 19 -12 4 -0.1084 -0.0486 19 -12 5 -0.2400 -0.0531 19 -12 6 -0.1886 -0.0265 19 -12 7 -0.0798 0.0182 19 -11 0 0.0622 0.0241 19 -11 1 0.0468 0.0170 19 -11 2 -0.0224 0.0019 19 -11 3 -0.1282 -0.0105 19 -11 4 -0.1576 -0.0093 19 -11 5 -0.0773 0.0106 19 -11 6 0.0075 0.0415 19 -11 7 -0.0013 0.0643 19 -11 8 -0.0521 0.0617 19 -10 0 -0.2835 -0.0030 19 -10 1 -0.2214 -0.0088 19 -10 2 -0.2307 -0.0041 19 -10 3 -0.1980 0.0030 19 -10 4 -0.0668 0.0099 19 -10 5 0.0623 0.0173 19 -10 6 0.0681 0.0216 19 -10 7 -0.0137 0.0158 19 -10 8 -0.0288 -0.0001 19 -9 0 -0.2451 -0.0319 19 -9 1 -0.2337 -0.0113 19 -9 2 -0.2202 0.0016 19 -9 3 -0.0894 0.0030 19 -9 4 0.0854 0.0003 19 -9 5 0.1366 -0.0018 19 -9 6 0.0283 -0.0041 19 -9 7 -0.0939 -0.0053 19 -9 8 -0.0936 0.0004 19 -8 0 -0.0308 0.0132 19 -8 1 -0.0652 0.0149 19 -8 2 -0.0073 0.0087 19 -8 3 0.1323 0.0058 19 -8 4 0.1945 0.0062 19 -8 5 0.0854 0.0040 19 -8 6 -0.1017 0.0026 19 -8 7 -0.2031 0.0133 19 -8 8 -0.1721 0.0373 19 -7 0 0.1522 0.0093 19 -7 1 0.1568 -0.0077 19 -7 2 0.2063 -0.0068 19 -7 3 0.2203 -0.0008 19 -7 4 0.1301 -0.0064 19 -7 5 -0.0219 -0.0179 19 -7 6 -0.1281 -0.0122 19 -7 7 -0.1312 0.0197 19 -6 0 0.2668 -0.0343 19 -6 1 0.2880 -0.0223 19 -6 2 0.2431 -0.0105 19 -6 3 0.1597 -0.0206 19 -6 4 0.0870 -0.0420 19 -6 5 0.0482 -0.0404 19 -6 6 0.0321 0.0000 19 -6 7 0.0299 0.0530 19 -5 0 0.4070 0.0068 19 -5 1 0.3671 0.0154 19 -5 2 0.2703 -0.0053 19 -5 3 0.2238 -0.0372 19 -5 4 0.2174 -0.0414 19 -5 5 0.1718 -0.0004 19 -5 6 0.0736 0.0589 19 -4 0 0.5928 0.0393 19 -4 1 0.5082 0.0070 19 -4 2 0.4302 -0.0313 19 -4 3 0.3709 -0.0430 19 -4 4 0.2497 -0.0131 19 -4 5 0.0667 0.0369 19 -4 6 -0.0593 0.0671 19 -3 0 0.6804 -0.0091 19 -3 1 0.6044 -0.0332 19 -3 2 0.4823 -0.0428 19 -3 3 0.2725 -0.0291 19 -3 4 0.0254 0.0001 19 -3 5 -0.1048 0.0237 19 -2 0 0.5280 -0.0102 19 -2 1 0.4405 -0.0067 19 -2 2 0.2117 -0.0066 19 -2 3 -0.0694 -0.0034 19 -2 4 -0.2040 0.0043 19 -1 0 0.2073 0.0208 19 -1 1 0.0812 0.0160 19 -1 2 -0.1718 0.0041 19 -1 3 -0.3348 -0.0022 19 0 0 -0.0175 -0.0257 19 0 1 -0.1630 -0.0245 19 0 2 -0.3441 -0.0226 19 1 0 -0.0202 -0.0514 20 -14 0 0.7078 0.0915 20 -14 1 0.7545 0.0891 20 -14 2 0.6907 0.0771 20 -13 0 0.7753 0.0182 20 -13 1 0.6292 0.0210 20 -13 2 0.3590 0.0003 20 -13 3 0.0112 -0.0385 20 -12 0 0.3614 0.0092 20 -12 1 0.1560 -0.0028 20 -12 2 -0.0742 -0.0256 20 -12 3 -0.2113 -0.0432 20 -12 4 -0.1603 -0.0393 20 -11 0 -0.1310 -0.0064 20 -11 1 -0.2146 -0.0155 20 -11 2 -0.2393 -0.0170 20 -11 3 -0.1210 -0.0119 20 -11 4 0.0860 0.0002 20 -10 0 -0.2547 -0.0300 20 -10 1 -0.2042 -0.0148 20 -10 2 -0.0724 -0.0064 20 -10 3 0.1488 -0.0058 20 -10 4 0.3119 -0.0061 20 -9 0 0.0416 0.0129 20 -9 1 0.1142 0.0145 20 -9 2 0.2555 0.0072 20 -9 3 0.3904 0.0022 20 -9 4 0.3727 0.0017 20 -8 0 0.3403 0.0327 20 -8 1 0.3445 0.0117 20 -8 2 0.3622 0.0063 20 -8 3 0.3064 0.0063 20 -8 4 0.1461 -0.0018 20 -7 0 0.2973 -0.0180 20 -7 1 0.2136 -0.0173 20 -7 2 0.1007 -0.0128 20 -7 3 -0.0221 -0.0265 20 -7 4 -0.0906 -0.0496 20 -6 0 0.1002 -0.0189 20 -6 1 -0.0204 -0.0109 20 -6 2 -0.1157 -0.0289 20 -6 3 -0.1124 -0.0579 20 -5 0 0.1114 0.0172 20 -5 1 0.0451 -0.0099 20 -5 2 0.0475 -0.0447 20 -5 3 0.0920 -0.0529 20 -4 0 0.3300 -0.0105 20 -4 1 0.3189 -0.0436 20 -4 2 0.2651 -0.0555 20 -3 0 0.4394 -0.0353 20 -3 1 0.3465 -0.0423 0 0 0 0.0 0.0 ; _shelx_fab_checksum 14262 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn Cu1 Cu 0.52693(2) 0.58649(2) 0.12378(2) 0.01118(3) Uani 1 1 d . S1 S 0.44776(2) 0.39086(2) 0.04598(2) 0.01207(4) Uani 1 1 d . P1 P 0.73622(2) 0.68851(2) 0.21081(2) 0.01058(4) Uani 1 1 d . P2 P 0.42271(2) 0.66864(2) 0.23008(2) 0.00885(4) Uani 1 1 d . F2 F 0.48064(10) 0.20753(6) 0.07446(6) 0.02628(16) Uani 1 1 d . F1 F 0.50247(9) 0.33298(7) 0.20941(5) 0.02414(15) Uani 1 1 d . F3 F 0.65523(8) 0.35720(8) 0.12625(7) 0.02961(17) Uani 1 1 d . C43 C 0.64132(12) 1.14538(9) 0.43478(9) 0.02005(19) Uani 1 1 d . H43 H 0.6133 1.1773 0.4911 0.024 Uiso 1 1 calc R C12 C 0.98459(12) 0.71924(10) 0.46857(8) 0.02051(19) Uani 1 1 d . H12 H 1.0675 0.7701 0.5069 0.025 Uiso 1 1 calc R C9 C 0.74068(10) 0.57065(9) 0.35655(8) 0.01612(15) Uani 1 1 d . H9 H 0.6574 0.5199 0.3188 0.019 Uiso 1 1 calc R C16 C 0.35864(11) 0.97028(9) 0.27825(9) 0.01779(17) Uani 1 1 d . H16 H 0.3355 1.0166 0.3289 0.021 Uiso 1 1 calc R C11 C 0.91768(13) 0.62210(11) 0.49718(9) 0.0221(2) Uani 1 1 d . H11 H 0.9552 0.6063 0.5547 0.027 Uiso 1 1 calc R C35 C 0.74179(10) 0.78274(9) 0.65036(7) 0.01472(15) Uani 1 1 d . H35 H 0.7097 0.7375 0.6942 0.018 Uiso 1 1 calc R C23 C 0.02190(10) 0.41719(11) 0.24586(9) 0.02109(19) Uani 1 1 d . H23 H -0.0598 0.3639 0.2482 0.025 Uiso 1 1 calc R C40 C 0.72672(10) 1.05352(8) 0.26947(8) 0.01569(15) Uani 1 1 d . C28 C 0.47495(9) 0.64345(8) 0.42499(7) 0.01158(13) Uani 1 1 d . H28 H 0.3944 0.5806 0.4033 0.014 Uiso 1 1 calc R C44 C 0.67679(13) 1.20784(9) 0.36396(10) 0.0235(2) Uani 1 1 d . H44 H 0.6717 1.2811 0.3723 0.028 Uiso 1 1 calc R C14 C 0.40049(8) 0.79894(7) 0.21586(7) 0.01081(12) Uani 1 1 d . C45 C 0.71841(12) 1.16282(9) 0.28341(10) 0.0218(2) Uani 1 1 d . H45 H 0.7422 1.2053 0.2360 0.026 Uiso 1 1 calc R C20 C 0.26303(8) 0.57403(8) 0.23958(7) 0.01094(12) Uani 1 1 d . C6 C 1.07469(11) 0.77565(13) 0.10117(10) 0.0262(2) Uani 1 1 d . H6 H 1.1563 0.8367 0.1154 0.031 Uiso 1 1 calc R C36 C 0.69113(8) 0.87605(7) 0.32257(6) 0.00966(12) Uani 1 1 d . C39 C 0.76700(11) 1.00531(10) 0.18530(9) 0.01934(18) Uani 1 1 d . H39 H 0.7898 1.0469 0.1372 0.023 Uiso 1 1 calc R C27 C 0.51913(8) 0.71199(7) 0.35904(6) 0.00914(12) Uani 1 1 d . C22 C 0.12412(11) 0.38127(10) 0.22970(10) 0.0219(2) Uani 1 1 d . H22 H 0.1121 0.3033 0.2213 0.026 Uiso 1 1 calc R C42 C 0.64691(10) 1.03873(8) 0.42300(8) 0.01484(15) Uani 1 1 d . H42 H 0.6223 0.9977 0.4712 0.018 Uiso 1 1 calc R C21 C 0.24371(10) 0.45896(8) 0.22577(9) 0.01637(16) Uani 1 1 d . H21 H 0.3126 0.4336 0.2136 0.020 Uiso 1 1 calc R C15 C 0.36786(10) 0.86875(8) 0.29019(7) 0.01422(14) Uani 1 1 d . H15 H 0.3518 0.8464 0.3495 0.017 Uiso 1 1 calc R C13 C 0.92993(10) 0.74162(9) 0.38391(8) 0.01625(16) Uani 1 1 d . H13 H 0.9759 0.8078 0.3645 0.020 Uiso 1 1 calc R C29 C 0.54611(9) 0.66609(8) 0.51917(7) 0.01255(13) Uani 1 1 d . H29 H 0.5146 0.6187 0.5615 0.015 Uiso 1 1 calc R C4 C 0.92881(11) 0.59126(11) 0.00296(8) 0.01908(18) Uani 1 1 d . H4 H 0.9102 0.5258 -0.0503 0.023 Uiso 1 1 calc R C41 C 0.68902(9) 0.98896(7) 0.33962(7) 0.01167(13) Uani 1 1 d . C33 C 0.90802(10) 0.93919(8) 0.61757(7) 0.01413(14) Uani 1 1 d . H33 H 0.9907 0.9993 0.6392 0.017 Uiso 1 1 calc R C26 C 0.63809(8) 0.80347(7) 0.39042(6) 0.00916(12) Uani 1 1 d . C10 C 0.79595(13) 0.54836(10) 0.44142(9) 0.02088(19) Uani 1 1 d . H10 H 0.7501 0.4824 0.4612 0.025 Uiso 1 1 calc R C19 C 0.42266(10) 0.83230(9) 0.12892(8) 0.01576(15) Uani 1 1 d . H19 H 0.4433 0.7851 0.0773 0.019 Uiso 1 1 calc R C38 C 0.77369(10) 0.89948(9) 0.17201(8) 0.01640(16) Uani 1 1 d . H38 H 0.8018 0.8690 0.1151 0.020 Uiso 1 1 calc R C30 C 0.66602(9) 0.75932(8) 0.55382(7) 0.01120(13) Uani 1 1 d . C5 C 1.04781(11) 0.68038(12) 0.02348(9) 0.0240(2) Uani 1 1 d . H5 H 1.1107 0.6761 -0.0156 0.029 Uiso 1 1 calc R C25 C 0.16002(10) 0.60943(9) 0.25575(9) 0.01679(16) Uani 1 1 d . H25 H 0.1718 0.6874 0.2649 0.020 Uiso 1 1 calc R C7 C 0.98286(10) 0.78249(11) 0.15858(9) 0.0213(2) Uani 1 1 d . H7 H 1.0022 0.8482 0.2117 0.026 Uiso 1 1 calc R C3 C 0.83635(10) 0.59740(9) 0.06018(7) 0.01501(15) Uani 1 1 d . H3 H 0.7550 0.5359 0.0457 0.018 Uiso 1 1 calc R C18 C 0.41467(11) 0.93509(10) 0.11732(10) 0.02076(19) Uani 1 1 d . H18 H 0.4307 0.9578 0.0581 0.025 Uiso 1 1 calc R C37 C 0.73923(8) 0.83440(8) 0.24213(7) 0.01094(12) Uani 1 1 d . C24 C 0.03975(10) 0.53066(11) 0.25853(9) 0.02077(19) Uani 1 1 d . H24 H -0.0301 0.5553 0.2692 0.025 Uiso 1 1 calc R C32 C 0.83534(9) 0.92044(8) 0.52458(7) 0.01218(13) Uani 1 1 d . H32 H 0.8674 0.9691 0.4833 0.015 Uiso 1 1 calc R C17 C 0.38346(11) 1.00403(9) 0.19188(10) 0.02080(19) Uani 1 1 d . H17 H 0.3790 1.0742 0.1841 0.025 Uiso 1 1 calc R C8 C 0.80748(9) 0.66728(8) 0.32695(7) 0.01233(13) Uani 1 1 d . C34 C 0.86093(10) 0.86998(9) 0.68120(7) 0.01605(16) Uani 1 1 d . H34 H 0.9118 0.8838 0.7455 0.019 Uiso 1 1 calc R C31 C 0.71272(8) 0.82919(7) 0.48932(6) 0.00989(12) Uani 1 1 d . C2 C 0.86223(9) 0.69311(9) 0.13849(7) 0.01410(15) Uani 1 1 d . C1 C 0.52453(11) 0.32134(9) 0.11488(8) 0.01636(16) Uani 1 1 d . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cu1 0.00895(4) 0.01104(5) 0.01129(5) -0.00111(3) 0.00118(3) 0.00350(3) S1 0.01433(9) 0.01008(8) 0.01127(8) 0.00159(6) 0.00202(7) 0.00474(7) P1 0.00771(8) 0.01288(9) 0.00940(8) -0.00087(7) 0.00092(6) 0.00408(7) P2 0.00736(8) 0.00892(8) 0.00971(8) 0.00110(6) 0.00170(6) 0.00308(6) F2 0.0496(5) 0.0129(3) 0.0214(3) 0.0072(2) 0.0124(3) 0.0146(3) F1 0.0396(4) 0.0235(3) 0.0130(3) 0.0068(2) 0.0062(3) 0.0149(3) F3 0.0221(3) 0.0373(4) 0.0397(5) 0.0209(4) 0.0062(3) 0.0176(3) C43 0.0260(5) 0.0130(4) 0.0199(4) -0.0006(3) -0.0005(4) 0.0103(4) C12 0.0194(4) 0.0217(4) 0.0169(4) 0.0004(3) -0.0049(3) 0.0089(4) C9 0.0164(4) 0.0163(4) 0.0139(4) 0.0013(3) 0.0034(3) 0.0053(3) C16 0.0173(4) 0.0120(3) 0.0239(5) 0.0025(3) 0.0016(3) 0.0074(3) C11 0.0292(5) 0.0242(5) 0.0154(4) 0.0046(4) 0.0004(4) 0.0148(4) C35 0.0169(4) 0.0158(4) 0.0111(3) 0.0046(3) 0.0012(3) 0.0054(3) C23 0.0119(4) 0.0246(5) 0.0246(5) 0.0119(4) 0.0040(3) 0.0007(3) C40 0.0145(4) 0.0119(3) 0.0196(4) 0.0069(3) 0.0025(3) 0.0024(3) C28 0.0103(3) 0.0111(3) 0.0123(3) 0.0034(3) 0.0020(2) 0.0025(2) C44 0.0286(5) 0.0106(4) 0.0279(5) 0.0031(3) -0.0026(4) 0.0073(4) C14 0.0095(3) 0.0110(3) 0.0122(3) 0.0031(2) 0.0022(2) 0.0040(2) C45 0.0230(5) 0.0124(4) 0.0283(5) 0.0093(4) 0.0017(4) 0.0034(3) C20 0.0083(3) 0.0115(3) 0.0122(3) 0.0027(2) 0.0017(2) 0.0029(2) C6 0.0099(4) 0.0369(6) 0.0227(5) -0.0035(4) 0.0041(3) 0.0035(4) C36 0.0091(3) 0.0094(3) 0.0093(3) 0.0017(2) 0.0019(2) 0.0025(2) C39 0.0197(4) 0.0208(4) 0.0209(4) 0.0126(4) 0.0082(4) 0.0061(4) C27 0.0091(3) 0.0089(3) 0.0093(3) 0.0017(2) 0.0021(2) 0.0036(2) C22 0.0141(4) 0.0166(4) 0.0332(6) 0.0125(4) 0.0012(4) 0.0015(3) C42 0.0179(4) 0.0112(3) 0.0147(4) 0.0009(3) 0.0019(3) 0.0064(3) C21 0.0115(3) 0.0128(3) 0.0249(5) 0.0070(3) 0.0022(3) 0.0038(3) C15 0.0163(4) 0.0126(3) 0.0145(4) 0.0022(3) 0.0024(3) 0.0072(3) C13 0.0150(4) 0.0139(3) 0.0163(4) 0.0007(3) -0.0029(3) 0.0050(3) C29 0.0125(3) 0.0126(3) 0.0125(3) 0.0048(3) 0.0027(3) 0.0037(3) C4 0.0163(4) 0.0280(5) 0.0133(4) -0.0011(3) 0.0021(3) 0.0127(4) C41 0.0114(3) 0.0094(3) 0.0129(3) 0.0026(2) 0.0014(3) 0.0029(2) C33 0.0139(3) 0.0126(3) 0.0118(3) -0.0003(3) -0.0003(3) 0.0029(3) C26 0.0094(3) 0.0088(3) 0.0091(3) 0.0014(2) 0.0024(2) 0.0035(2) C10 0.0270(5) 0.0193(4) 0.0171(4) 0.0062(3) 0.0050(4) 0.0086(4) C19 0.0149(4) 0.0196(4) 0.0167(4) 0.0088(3) 0.0062(3) 0.0078(3) C38 0.0161(4) 0.0214(4) 0.0142(4) 0.0078(3) 0.0069(3) 0.0070(3) C30 0.0121(3) 0.0114(3) 0.0099(3) 0.0023(2) 0.0016(2) 0.0046(3) C5 0.0138(4) 0.0382(6) 0.0186(4) 0.0000(4) 0.0052(3) 0.0113(4) C25 0.0114(3) 0.0155(4) 0.0233(4) 0.0026(3) 0.0063(3) 0.0052(3) C7 0.0099(3) 0.0280(5) 0.0178(4) -0.0048(4) 0.0025(3) 0.0031(3) C3 0.0126(3) 0.0197(4) 0.0118(3) -0.0007(3) 0.0010(3) 0.0081(3) C18 0.0186(4) 0.0235(5) 0.0273(5) 0.0166(4) 0.0094(4) 0.0092(4) C37 0.0090(3) 0.0129(3) 0.0100(3) 0.0020(2) 0.0021(2) 0.0034(2) C24 0.0110(4) 0.0245(5) 0.0264(5) 0.0051(4) 0.0075(3) 0.0056(3) C32 0.0115(3) 0.0113(3) 0.0112(3) 0.0008(2) 0.0014(2) 0.0025(3) C17 0.0165(4) 0.0152(4) 0.0336(6) 0.0119(4) 0.0049(4) 0.0064(3) C8 0.0123(3) 0.0123(3) 0.0114(3) -0.0004(3) 0.0005(3) 0.0061(3) C34 0.0177(4) 0.0159(4) 0.0114(3) 0.0018(3) -0.0015(3) 0.0048(3) C31 0.0101(3) 0.0092(3) 0.0096(3) 0.0009(2) 0.0019(2) 0.0037(2) C2 0.0088(3) 0.0198(4) 0.0117(3) -0.0009(3) 0.0017(2) 0.0059(3) C1 0.0231(4) 0.0141(4) 0.0150(4) 0.0061(3) 0.0054(3) 0.0089(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_3 S1 Cu1 S1 84.569(11) 2_665 P1 Cu1 S1 123.874(11) . P1 Cu1 S1 100.038(11) 2_665 P1 Cu1 P2 97.947(12) . P2 Cu1 S1 127.760(11) 2_665 P2 Cu1 S1 122.980(11) . Cu1 S1 Cu1 95.429(11) 2_665 C1 S1 Cu1 125.87(4) 2_665 C1 S1 Cu1 110.22(4) . C37 P1 Cu1 102.37(3) . C8 P1 Cu1 124.54(3) . C8 P1 C37 105.85(4) . C2 P1 Cu1 115.45(3) . C2 P1 C37 104.92(5) . C2 P1 C8 101.94(5) . C14 P2 Cu1 119.52(3) . C14 P2 C20 105.20(4) . C14 P2 C27 102.78(4) . C20 P2 Cu1 115.47(3) . C20 P2 C27 103.24(4) . C27 P2 Cu1 108.75(3) . C44 C43 H43 119.7 . C42 C43 H43 119.7 . C42 C43 C44 120.62(11) . C11 C12 H12 120.0 . C13 C12 H12 120.0 . C13 C12 C11 119.93(10) . C10 C9 H9 119.9 . C10 C9 C8 120.13(10) . C8 C9 H9 119.9 . C15 C16 H16 120.1 . C15 C16 C17 119.84(10) . C17 C16 H16 120.1 . C12 C11 H11 120.1 . C10 C11 C12 119.85(10) . C10 C11 H11 120.1 . C30 C35 H35 119.7 . C34 C35 H35 119.7 . C34 C35 C30 120.69(9) . C22 C23 H23 120.1 . C24 C23 H23 120.1 . C24 C23 C22 119.75(10) . C45 C40 C41 119.55(10) . C39 C40 C45 121.35(10) . C39 C40 C41 119.06(9) . C27 C28 H28 119.3 . C29 C28 H28 119.3 . C29 C28 C27 121.43(8) . C43 C44 H44 120.0 . C45 C44 C43 119.91(10) . C45 C44 H44 120.0 . C15 C14 P2 122.80(7) . C19 C14 P2 118.19(7) . C19 C14 C15 118.95(9) . C40 C45 H45 119.5 . C44 C45 C40 120.98(11) . C44 C45 H45 119.5 . C21 C20 P2 116.86(7) . C21 C20 C25 119.04(9) . C25 C20 P2 124.05(7) . C5 C6 H6 119.8 . C5 C6 C7 120.40(11) . C7 C6 H6 119.8 . C41 C36 C26 119.37(8) . C37 C36 C41 119.69(8) . C37 C36 C26 120.92(8) . C40 C39 H39 119.5 . C38 C39 C40 120.97(9) . C38 C39 H39 119.5 . C28 C27 P2 118.37(6) . C26 C27 P2 122.06(6) . C26 C27 C28 119.36(8) . C23 C22 H22 119.8 . C21 C22 C23 120.31(10) . C21 C22 H22 119.8 . C43 C42 H42 119.5 . C43 C42 C41 120.95(10) . C41 C42 H42 119.5 . C20 C21 H21 119.8 . C22 C21 C20 120.32(10) . C22 C21 H21 119.8 . C16 C15 C14 120.80(9) . C16 C15 H15 119.6 . C14 C15 H15 119.6 . C12 C13 H13 119.7 . C12 C13 C8 120.54(10) . C8 C13 H13 119.7 . C28 C29 H29 119.7 . C28 C29 C30 120.60(8) . C30 C29 H29 119.7 . C5 C4 H4 119.9 . C5 C4 C3 120.20(10) . C3 C4 H4 119.9 . C40 C41 C36 119.40(8) . C42 C41 C40 117.99(9) . C42 C41 C36 122.58(8) . C32 C33 H33 119.7 . C32 C33 C34 120.59(9) . C34 C33 H33 119.7 . C27 C26 C36 121.45(8) . C27 C26 C31 119.81(8) . C31 C26 C36 118.74(7) . C9 C10 H10 119.8 . C11 C10 C9 120.38(11) . C11 C10 H10 119.8 . C14 C19 H19 119.9 . C14 C19 C18 120.25(10) . C18 C19 H19 119.9 . C39 C38 H38 119.5 . C39 C38 C37 120.98(9) . C37 C38 H38 119.5 . C35 C30 C31 119.54(8) . C29 C30 C35 121.28(8) . C29 C30 C31 119.17(8) . C6 C5 C4 119.75(10) . C6 C5 H5 120.1 . C4 C5 H5 120.1 . C20 C25 H25 119.9 . C20 C25 C24 120.30(10) . C24 C25 H25 119.9 . C6 C7 H7 119.8 . C6 C7 C2 120.39(10) . C2 C7 H7 119.8 . C4 C3 H3 119.7 . C4 C3 C2 120.55(10) . C2 C3 H3 119.7 . C19 C18 H18 119.9 . C17 C18 C19 120.26(10) . C17 C18 H18 119.9 . C36 C37 P1 122.37(7) . C36 C37 C38 119.62(9) . C38 C37 P1 117.29(7) . C23 C24 C25 120.28(10) . C23 C24 H24 119.9 . C25 C24 H24 119.9 . C33 C32 H32 119.6 . C33 C32 C31 120.84(9) . C31 C32 H32 119.6 . C16 C17 H17 120.1 . C18 C17 C16 119.89(10) . C18 C17 H17 120.1 . C9 C8 P1 118.70(7) . C9 C8 C13 119.16(9) . C13 C8 P1 122.05(8) . C35 C34 C33 120.06(9) . C35 C34 H34 120.0 . C33 C34 H34 120.0 . C30 C31 C26 119.62(8) . C32 C31 C26 122.09(8) . C32 C31 C30 118.25(8) . C7 C2 P1 124.86(8) . C3 C2 P1 116.37(8) . C3 C2 C7 118.71(9) . F2 C1 S1 112.85(8) . F2 C1 F1 104.82(8) . F1 C1 S1 112.25(7) . F3 C1 S1 115.73(7) . F3 C1 F2 105.26(9) . F3 C1 F1 104.99(9) . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Cu1 S1 2.3457(3) . Cu1 S1 2.4882(4) 2_665 Cu1 P1 2.2925(4) . Cu1 P2 2.3012(3) . S1 Cu1 2.4881(4) 2_665 S1 C1 1.7667(11) . P1 C37 1.8327(10) . P1 C8 1.8298(10) . P1 C2 1.8217(10) . P2 C14 1.8243(9) . P2 C20 1.8302(9) . P2 C27 1.8523(9) . F2 C1 1.3538(13) . F1 C1 1.3621(13) . F3 C1 1.3507(14) . C43 H43 0.9500 . C43 C44 1.4118(18) . C43 C42 1.3759(14) . C12 H12 0.9500 . C12 C11 1.3929(18) . C12 C13 1.3901(15) . C9 H9 0.9500 . C9 C10 1.3946(16) . C9 C8 1.3949(15) . C16 H16 0.9500 . C16 C15 1.3887(14) . C16 C17 1.3927(17) . C11 H11 0.9500 . C11 C10 1.3896(18) . C35 H35 0.9500 . C35 C30 1.4174(13) . C35 C34 1.3716(15) . C23 H23 0.9500 . C23 C22 1.3919(18) . C23 C24 1.3810(18) . C40 C45 1.4200(15) . C40 C39 1.4126(16) . C40 C41 1.4253(14) . C28 H28 0.9500 . C28 C27 1.4236(12) . C28 C29 1.3710(13) . C44 H44 0.9500 . C44 C45 1.3662(19) . C14 C15 1.3995(13) . C14 C19 1.3925(13) . C45 H45 0.9500 . C20 C21 1.3961(13) . C20 C25 1.3965(13) . C6 H6 0.9500 . C6 C5 1.3842(18) . C6 C7 1.3909(16) . C36 C41 1.4368(12) . C36 C26 1.5017(12) . C36 C37 1.3925(12) . C39 H39 0.9500 . C39 C38 1.3690(16) . C27 C26 1.3951(12) . C22 H22 0.9500 . C22 C21 1.3905(15) . C42 H42 0.9500 . C42 C41 1.4236(14) . C21 H21 0.9500 . C15 H15 0.9500 . C13 H13 0.9500 . C13 C8 1.4020(14) . C29 H29 0.9500 . C29 C30 1.4141(13) . C4 H4 0.9500 . C4 C5 1.3852(18) . C4 C3 1.3933(14) . C33 H33 0.9500 . C33 C32 1.3734(13) . C33 C34 1.4102(15) . C26 C31 1.4352(12) . C10 H10 0.9500 . C19 H19 0.9500 . C19 C18 1.3984(15) . C38 H38 0.9500 . C38 C37 1.4228(13) . C30 C31 1.4243(13) . C5 H5 0.9500 . C25 H25 0.9500 . C25 C24 1.3969(15) . C7 H7 0.9500 . C7 C2 1.3992(15) . C3 H3 0.9500 . C3 C2 1.3949(14) . C18 H18 0.9500 . C18 C17 1.3861(18) . C24 H24 0.9500 . C32 H32 0.9500 . C32 C31 1.4221(13) . C17 H17 0.9500 . C34 H34 0.9500 . loop_ _smtbx_masks_void_nr _smtbx_masks_void_average_x _smtbx_masks_void_average_y _smtbx_masks_void_average_z _smtbx_masks_void_volume _smtbx_masks_void_count_electrons 1 0.000 0.000 0.000 117.1 23.0