#------------------------------------------------------------------------------ #$Date: 2019-11-10 07:54:14 +0200 (Sun, 10 Nov 2019) $ #$Revision: 225918 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/58/4515801.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4515801 loop_ _publ_author_name 'Messinis, Antonis M.' 'Batsanov, Andrei S.' 'Wright, William R. H.' 'Howard, Judith A. K.' 'Hanton, Martin J.' 'Dyer, Philip W.' _publ_section_title ; Bis(Imido) Tungsten Complexes: Efficient Precatalysts for the Homogeneous Dimerization of Ethylene ; _journal_issue 12 _journal_name_full 'ACS Catalysis' _journal_page_first 11249 _journal_paper_doi 10.1021/acscatal.8b02202 _journal_volume 8 _journal_year 2018 _chemical_absolute_configuration ad _chemical_formula_moiety 'C34 H44 Cl2 N4 W' _chemical_formula_sum 'C34 H44 Cl2 N4 W' _chemical_formula_weight 763.48 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens difmap _atom_sites_solution_primary direct _audit_creation_date 2017-10-24 _audit_creation_method ; Olex2 1.2-beta (compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 9.8622(9) _cell_length_b 17.5716(13) _cell_length_c 19.3465(16) _cell_measurement_reflns_used 9950 _cell_measurement_temperature 120 _cell_measurement_theta_max 29.94 _cell_measurement_theta_min 2.32 _cell_volume 3352.6(5) _computing_cell_refinement 'SAINT v7.46A (Bruker, 2008)' _computing_data_collection 'SMART v5.625 (Bruker, 2001)' _computing_data_reduction 'SAINT v7.46A (Bruker, 2008)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL 2016/6 (Sheldrick, 2015)' _computing_structure_solution 'SHELXS (Sheldrick, 2008)' _diffrn_ambient_temperature 120 _diffrn_detector 'CCD area detector' _diffrn_detector_area_resol_mean 5.6 _diffrn_detector_type 'Bruker SMART CCD 6000 area detector' _diffrn_measured_fraction_theta_full 0.987 _diffrn_measured_fraction_theta_max 0.987 _diffrn_measurement_device 'three-circle diffractometer' _diffrn_measurement_device_type 'Bruker SMART CCD 6000 area detector' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0530 _diffrn_reflns_av_unetI/netI 0.0592 _diffrn_reflns_Laue_measured_fraction_full 0.987 _diffrn_reflns_Laue_measured_fraction_max 0.987 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_number 39577 _diffrn_reflns_point_group_measured_fraction_full 0.973 _diffrn_reflns_point_group_measured_fraction_max 0.973 _diffrn_reflns_theta_full 29.992 _diffrn_reflns_theta_max 29.992 _diffrn_reflns_theta_min 1.566 _diffrn_source 'sealed X-ray tube' _diffrn_source_current 35.0 _diffrn_source_power 1.75 _diffrn_source_target Mo _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 3.633 _exptl_absorpt_correction_T_max 0.9174 _exptl_absorpt_correction_T_min 0.5257 _exptl_absorpt_correction_type integration _exptl_absorpt_process_details ; SADABS-2009/1 (Bruker,2010) was used for absorption correction. wR2(int) was 0.0858 before and 0.0709 after correction. The Ratio of minimum to maximum transmission is 0.5730. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour red _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 1.513 _exptl_crystal_description plate _exptl_crystal_F_000 1536 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.09 _exptl_crystal_size_min 0.01 _refine_diff_density_max 1.248 _refine_diff_density_min -1.114 _refine_diff_density_rms 0.123 _refine_ls_abs_structure_details ; Flack x determined using 3402 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons and Flack, 2004). By classical hole-in-one fit to all intensities, x=-0.004(8). Hooft parameter y = -0.007(5). ; _refine_ls_abs_structure_Flack 0.007(5) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.998 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 394 _refine_ls_number_reflns 9510 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 0.999 _refine_ls_R_factor_all 0.0409 _refine_ls_R_factor_gt 0.0297 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0190P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0559 _refine_ls_wR_factor_ref 0.0595 _reflns_Friedel_coverage 0.778 _reflns_Friedel_fraction_full 0.955 _reflns_Friedel_fraction_max 0.955 _reflns_number_gt 8357 _reflns_number_total 9510 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file W-bisimido.cif _cod_data_source_block 5_11srv263 _cod_database_code 4515801 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.965 _shelx_estimated_absorpt_t_min 0.530 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2. Restrained distances C22A-C20 \\sim C22B-C20 with sigma of 0.01 C21B-C20 \\sim C21A-C20 with sigma of 0.01 3. Others Uiso(H18A)=Uiso(H18B)=Uiso(H18C)=FVAR(1) Uiso(H19A)=Uiso(H19B)=Uiso(H19C)=FVAR(2) Uiso(H21A)=Uiso(H21B)=Uiso(H21C)=Uiso(H21D)=Uiso(H21E)=Uiso(H21F)=FVAR(3) Uiso(H34A)=Uiso(H34B)=Uiso(H34C)=FVAR(4) Uiso(H30A)=Uiso(H30B)=Uiso(H30C)=FVAR(5) Uiso(H31A)=Uiso(H31B)=Uiso(H31C)=FVAR(6) Fixed Sof: H20(0.67) H20A(0.33) C21A(0.67) H21A(0.67) H21B(0.67) H21C(0.67) C22A(0.67) H22A(0.67) H22B(0.67) H22C(0.67) C21B(0.33) H21D(0.33) H21E(0.33) H21F(0.33) C22B(0.33) H22D(0.33) H22E(0.33) H22F(0.33) 4.a Riding coordinates: C1(H1), C2(H2), C3(H3), C4(H4), C5(H5), C6(H6), C7(H7), C8(H8), C9(H9), C10(H10), C13(H13), C14(H14), C15(H15), C17(H17), C20(H20), C20(H20A), C25(H25), C26(H26), C27(H27), C29(H29), C32(H32) 4.b Rotating group: C18(H18A,H18B,H18C), C19(H19A,H19B,H19C), C21A(H21A,H21B,H21C), C22A(H22A, H22B,H22C), C21B(H21D,H21E,H21F), C22B(H22D,H22E,H22F), C30(H30A,H30B,H30C), C31(H31A,H31B,H31C), C33(H33A,H33B,H33C), C34(H34A,H34B,H34C) ; _shelx_res_file ; TITL 11srv263 in P2(1)2(1)2(1) 11srv263.res created by SHELXL-2016/6 at 17:34:53 on 24-Oct-2017 REM reset to P212121 #19 CELL 0.71073 9.8622 17.5716 19.3465 90 90 90 ZERR 4 0.0009 0.0013 0.0016 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N Cl W UNIT 136 176 16 8 4 SADI 0.01 C22A C20 C22B C20 SADI 0.01 C21B C20 C21A C20 L.S. 7 PLAN 6 SIZE 0.01 0.09 0.2 TEMP -153 BOND fmap 2 acta 60 OMIT -4 7 22 REM REM REM WGHT 0.019000 FVAR 0.22524 0.04798 0.04398 0.04986 0.07093 0.04517 0.04791 W 5 0.700040 0.602058 0.326029 11.00000 0.01458 0.01133 = 0.01459 -0.00005 -0.00019 -0.00072 CL1 4 0.903761 0.531026 0.309319 11.00000 0.01667 0.01813 = 0.02508 -0.00049 0.00134 0.00239 CL2 4 0.564443 0.708915 0.359382 11.00000 0.02404 0.01421 = 0.02858 0.00166 0.00538 0.00451 N1 3 0.596043 0.530537 0.362945 11.00000 0.01305 0.01303 = 0.01882 -0.00268 0.00262 0.00373 N2 3 0.653011 0.606762 0.238424 11.00000 0.01345 0.01341 = 0.02545 0.00069 0.00371 0.00141 N3 3 0.850093 0.706703 0.305629 11.00000 0.01720 0.01312 = 0.02041 -0.00034 0.00403 -0.00270 N4 3 0.792020 0.617840 0.437796 11.00000 0.02199 0.01433 = 0.01772 -0.00025 -0.00089 -0.00297 C1 1 0.806024 0.763516 0.264714 11.00000 0.02758 0.01721 = 0.02698 0.00565 0.00323 0.00279 AFIX 3 H1 2 0.721434 0.757886 0.241794 11.00000 -1.20000 AFIX 0 C2 1 0.879283 0.829826 0.254761 11.00000 0.04478 0.01689 = 0.03740 0.00741 0.01607 -0.00249 AFIX 3 H2 2 0.846163 0.868466 0.224851 11.00000 -1.20000 AFIX 0 C3 1 1.001577 0.839026 0.289019 11.00000 0.04164 0.02345 = 0.04115 -0.00197 0.01283 -0.01298 AFIX 3 H3 2 1.051947 0.884846 0.284619 11.00000 -1.20000 AFIX 0 C4 1 1.048298 0.780471 0.329457 11.00000 0.02700 0.03449 = 0.03843 -0.00610 0.00046 -0.01208 AFIX 3 H4 2 1.133098 0.784522 0.352477 11.00000 -1.20000 AFIX 0 C5 1 0.970349 0.715482 0.336252 11.00000 0.02285 0.02609 = 0.02697 0.00019 0.00067 -0.00479 AFIX 3 H5 2 1.004039 0.675132 0.364062 11.00000 -1.20000 AFIX 0 C6 1 0.801949 0.684811 0.471604 11.00000 0.03340 0.01537 = 0.02662 -0.00078 -0.00062 -0.00286 AFIX 3 H6 2 0.771179 0.729691 0.449154 11.00000 -1.20000 AFIX 0 C7 1 0.854279 0.690777 0.536712 11.00000 0.04395 0.01910 = 0.02820 -0.00971 -0.00743 -0.00527 AFIX 3 H7 2 0.858919 0.738947 0.558882 11.00000 -1.20000 AFIX 0 C8 1 0.900550 0.626283 0.570169 11.00000 0.04265 0.03191 = 0.02215 -0.00112 -0.01111 -0.00340 AFIX 3 H8 2 0.939740 0.629633 0.614919 11.00000 -1.20000 AFIX 0 C9 1 0.888703 0.557533 0.537532 11.00000 0.03681 0.02107 = 0.02506 0.00330 -0.00419 -0.00001 AFIX 3 H9 2 0.917283 0.512093 0.559792 11.00000 -1.20000 AFIX 0 C10 1 0.834817 0.555202 0.471949 11.00000 0.03049 0.01354 = 0.02175 0.00090 0.00210 -0.00307 AFIX 3 H10 2 0.827347 0.507232 0.449620 11.00000 -1.20000 AFIX 0 C11 1 0.510055 0.473874 0.386793 11.00000 0.01952 0.01401 = 0.01385 0.00183 -0.00039 -0.00044 C12 1 0.535345 0.396352 0.368851 11.00000 0.02406 0.01528 = 0.01602 -0.00181 0.00115 -0.00222 C13 1 0.449923 0.341032 0.395432 11.00000 0.03630 0.01260 = 0.03309 0.00078 0.00894 -0.00049 AFIX 3 H13 2 0.466073 0.289172 0.384242 11.00000 -1.20000 AFIX 0 C14 1 0.342057 0.359200 0.437720 11.00000 0.03095 0.02094 = 0.03818 0.00210 0.01564 -0.00755 AFIX 3 H14 2 0.286707 0.320070 0.456500 11.00000 -1.20000 AFIX 0 C15 1 0.314771 0.434913 0.452677 11.00000 0.02704 0.02458 = 0.03437 0.00185 0.01717 -0.00184 AFIX 3 H15 2 0.237961 0.447373 0.480067 11.00000 -1.20000 AFIX 0 C16 1 0.397610 0.492549 0.428326 11.00000 0.02495 0.01698 = 0.01849 -0.00059 0.00074 0.00021 C17 1 0.652163 0.374784 0.321650 11.00000 0.02292 0.01356 = 0.02189 0.00015 0.00089 -0.00127 AFIX 3 H17 2 0.686673 0.422214 0.299150 11.00000 -1.20000 AFIX 0 C18 1 0.604273 0.320122 0.264505 11.00000 0.03273 0.02433 = 0.02959 -0.00440 0.00143 0.00207 AFIX 7 H18A 2 0.576235 0.271761 0.285285 11.00000 21.00000 H18B 2 0.678683 0.311033 0.231964 11.00000 21.00000 H18C 2 0.527382 0.342791 0.239885 11.00000 21.00000 AFIX 0 C19 1 0.767110 0.339610 0.362350 11.00000 0.03398 0.03252 = 0.02857 -0.00345 0.00315 0.00322 AFIX 7 H19A 2 0.801109 0.376540 0.396130 11.00000 31.00000 H19B 2 0.840450 0.325280 0.330760 11.00000 31.00000 H19C 2 0.734230 0.294220 0.386560 11.00000 31.00000 AFIX 0 C20 1 0.366008 0.575345 0.446741 11.00000 0.02459 0.01813 = 0.02990 0.00312 0.00669 0.00112 PART 1 AFIX 3 H20 2 0.401388 0.607055 0.407791 10.67000 -1.20000 AFIX 3 PART 0 PART 2 H20A 2 0.444178 0.607545 0.431621 10.33000 -1.20000 AFIX 0 PART 0 PART 1 C21A 1 0.215925 0.591876 0.451780 10.67000 0.02078 0.02389 = 0.05254 0.00266 -0.00037 0.00557 AFIX 7 H21A 2 0.169015 0.569237 0.412129 10.67000 41.00000 H21B 2 0.201395 0.647036 0.451842 10.67000 41.00000 H21C 2 0.180034 0.570044 0.494660 10.67000 41.00000 AFIX 0 C22A 1 0.442241 0.599996 0.510684 10.67000 0.03790 0.01577 = 0.04833 -0.00491 -0.01057 0.00829 AFIX 7 H22A 2 0.397613 0.579114 0.551794 10.67000 -1.50000 H22B 2 0.442886 0.655676 0.513396 10.67000 -1.50000 H22C 2 0.535672 0.581168 0.508363 10.67000 -1.50000 AFIX 0 PART 0 PART 2 C21B 1 0.241472 0.603423 0.411250 10.33000 0.03726 AFIX 7 H21D 2 0.255423 0.602440 0.361109 10.33000 41.00000 H21E 2 0.222546 0.655688 0.426080 10.33000 41.00000 H21F 2 0.164587 0.570671 0.423280 10.33000 41.00000 AFIX 0 C22B 1 0.352659 0.582132 0.526073 10.33000 0.04198 AFIX 7 H22D 2 0.261781 0.565830 0.540273 10.33000 -1.50000 H22E 2 0.366945 0.635182 0.539973 10.33000 -1.50000 H22F 2 0.420722 0.549734 0.548393 10.33000 -1.50000 AFIX 0 PART 0 C23 1 0.603836 0.616839 0.171718 11.00000 0.02301 0.01342 = 0.01984 -0.00387 -0.00153 0.00010 C24 1 0.695252 0.632585 0.117118 11.00000 0.02485 0.01123 = 0.01651 -0.00351 -0.00032 0.00104 C25 1 0.643934 0.647066 0.052048 11.00000 0.03948 0.01431 = 0.02141 0.00112 -0.00130 0.00019 AFIX 3 H25 2 0.704074 0.657836 0.014958 11.00000 -1.20000 AFIX 0 C26 1 0.503216 0.645945 0.040272 11.00000 0.04426 0.01873 = 0.02098 0.00205 -0.01560 0.00490 AFIX 3 H26 2 0.468656 0.657226 -0.004398 11.00000 -1.20000 AFIX 0 C27 1 0.415395 0.628613 0.093286 11.00000 0.02647 0.02156 = 0.03198 -0.00005 -0.01464 0.00182 AFIX 3 H27 2 0.320745 0.627153 0.084276 11.00000 -1.20000 AFIX 0 C28 1 0.461671 0.613154 0.159554 11.00000 0.02243 0.01072 = 0.02679 -0.00088 -0.00352 -0.00129 C29 1 0.847724 0.628130 0.128724 11.00000 0.02360 0.02250 = 0.01845 0.00002 0.00207 -0.00134 AFIX 3 H29 2 0.863954 0.632500 0.179584 11.00000 -1.20000 AFIX 0 C30 1 0.925621 0.693810 0.093284 11.00000 0.03055 0.05244 = 0.04112 0.01487 0.00436 -0.00947 AFIX 7 H30A 2 0.917983 0.688699 0.042994 11.00000 61.00000 H30B 2 1.021381 0.691731 0.106684 11.00000 61.00000 H30C 2 0.886840 0.742640 0.107733 11.00000 61.00000 AFIX 0 C31 1 0.898768 0.550384 0.106086 11.00000 0.03620 0.03515 = 0.07226 -0.02124 -0.01222 0.01342 AFIX 7 H31A 2 0.845310 0.510664 0.128927 11.00000 71.00000 H31B 2 0.994399 0.544875 0.118904 11.00000 71.00000 H31C 2 0.889364 0.545463 0.055846 11.00000 71.00000 AFIX 0 C32 1 0.367988 0.587919 0.217357 11.00000 0.02020 0.03547 = 0.03193 -0.00298 -0.00687 -0.00321 AFIX 3 H32 2 0.404848 0.608919 0.261567 11.00000 -1.20000 AFIX 0 C33 1 0.370906 0.501572 0.222918 11.00000 0.05334 0.02912 = 0.04751 0.01251 -0.00284 -0.01248 AFIX 7 H33A 2 0.328236 0.479302 0.181878 11.00000 -1.50000 H33B 2 0.321236 0.485612 0.264328 11.00000 -1.50000 H33C 2 0.465106 0.484172 0.226088 11.00000 -1.50000 AFIX 0 C34 1 0.223159 0.616174 0.210014 11.00000 0.02677 0.04821 = 0.08083 0.00786 0.00550 -0.00445 AFIX 7 H34A 2 0.223478 0.671424 0.202978 11.00000 51.00000 H34B 2 0.172237 0.604009 0.252082 11.00000 51.00000 H34C 2 0.180301 0.591347 0.170281 11.00000 51.00000 AFIX 0 HKLF 4 REM 11srv263 in P2(1)2(1)2(1) REM R1 = 0.0297 for 8357 Fo > 4sig(Fo) and 0.0409 for all 9510 data REM 394 parameters refined using 2 restraints END WGHT 0.0194 0.0000 REM Highest difference peak 1.248, deepest hole -1.114, 1-sigma level 0.123 Q1 1 0.7150 0.6048 0.2756 11.00000 0.05 1.25 Q2 1 0.7119 0.6063 0.3748 11.00000 0.05 1.01 Q3 1 0.7993 0.6017 0.3232 11.00000 0.05 1.00 Q4 1 0.3001 0.6971 0.1729 11.00000 0.05 0.73 Q5 1 0.8995 0.5999 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526.086 34.4945 3 1 -2 -4 520.304 34.7778 1 1 2 4 529.755 37.2043 2 -1 -2 4 522.544 36.5813 1 2 -2 4 115.080 11.4145 3 -2 2 4 108.559 10.7624 1 2 2 -4 112.628 11.8840 1 -2 2 4 95.9929 12.5152 2 -2 -2 -4 98.8002 13.0761 2 2 2 -4 106.470 10.5285 2 2 2 -4 107.463 10.2301 3 -2 2 4 104.406 10.5305 3 2 -2 4 90.3960 10.9518 1 -2 -2 4 169.223 14.5860 1 2 2 4 184.027 16.6966 2 3 2 -4 417.563 27.7086 3 -3 2 4 387.350 30.3639 2 3 -2 4 397.591 29.7754 1 3 -2 4 425.855 29.4515 3 3 -2 4 405.424 30.5444 2 -3 -2 -4 389.391 26.9806 1 3 2 -4 370.859 29.7895 1 3 2 -4 413.378 29.3121 2 -3 2 4 392.823 29.5038 1 3 -2 -4 477.112 31.0393 2 -3 2 -4 467.400 30.3178 2 3 -2 -4 467.338 29.8845 1 -3 -2 4 462.665 30.0054 1 3 2 4 477.813 31.2821 2 -3 2 -4 453.490 28.8704 3 3 2 4 446.456 29.0994 3 -3 -2 4 499.862 28.2607 3 -3 2 -4 474.784 28.8683 1 3 2 4 482.417 27.3614 1 -3 -2 4 487.439 29.6108 2 3 2 4 490.846 31.6712 2 -4 -2 -4 2306.32 133.871 4 -4 2 4 2368.62 133.354 2 4 2 -4 2309.66 128.620 3 4 -2 4 2195.26 133.252 1 4 -2 4 2226.92 129.501 3 4 2 -4 2272.38 132.381 2 -4 -2 -4 2244.81 131.668 1 4 2 4 2257.51 129.554 3 4 -2 -4 2336.05 133.743 1 4 2 4 2375.41 133.405 2 -4 2 -4 2268.55 132.947 1 -4 2 -4 2324.02 134.201 4 -4 -2 4 2270.60 132.373 2 -4 2 -4 2249.56 129.122 3 -4 2 -4 2286.55 132.823 2 4 2 4 2255.15 131.859 1 5 -2 4 202.641 18.1665 3 5 2 -4 217.443 19.4689 1 -5 2 4 254.391 22.1851 2 5 2 -4 204.350 16.1915 3 -5 -2 -4 169.521 16.1968 1 5 -2 4 172.276 18.2521 1 -5 2 -4 204.029 17.2427 3 5 2 4 173.334 16.1409 1 -5 -2 4 216.291 20.2735 2 5 -2 -4 173.834 19.0015 1 -5 2 -4 222.048 21.2493 2 -6 -2 -4 1651.29 97.5753 2 6 2 -4 1695.21 92.3589 3 6 -2 4 1619.32 97.1335 1 -6 2 4 1736.68 97.9189 2 6 2 -4 1622.91 97.6429 1 -6 2 -4 1534.05 92.6579 3 -6 -2 4 1578.16 96.6828 2 -6 2 -4 1615.20 97.2508 2 6 -2 -4 1534.89 97.3870 1 6 2 4 1575.95 95.6907 1 7 2 -4 471.530 34.5604 1 7 2 -4 499.339 29.7389 3 7 -2 4 516.321 34.2586 1 -7 2 4 474.756 35.9495 2 -7 -2 -4 491.335 35.5121 2 -7 2 -4 389.286 34.7702 2 7 -2 -4 399.655 33.7730 1 -7 -2 4 438.151 34.7721 2 7 2 4 392.163 31.2307 1 8 2 -4 214.374 18.5712 3 -8 2 4 198.027 24.6942 2 -8 -2 -4 232.955 24.9490 2 8 -2 4 206.023 23.9586 1 8 2 -4 222.977 24.2224 1 8 -2 -4 242.121 24.6155 1 -8 2 -4 288.670 27.2905 2 8 2 4 264.160 22.4425 1 -8 -2 4 265.304 26.1913 2 9 -2 4 211.213 22.9854 1 9 2 -4 162.260 22.2269 1 9 2 -4 171.835 16.4710 3 -9 2 4 167.541 24.0354 2 -9 -2 -4 177.304 23.8039 2 9 -2 -4 166.621 22.0346 1 -9 2 -4 179.215 23.7025 2 -9 -2 4 200.263 24.1621 2 9 2 4 168.852 20.2327 1 10 -2 4 87.1166 19.0315 1 10 2 -4 97.7106 19.1152 1 -10 -2 -4 144.061 23.4533 2 -10 2 4 80.5241 21.4396 2 -10 -2 4 88.7886 21.5660 2 10 -2 -4 60.0471 18.1702 1 10 2 4 85.2176 17.6560 1 -10 2 -4 90.1529 21.4401 2 -11 -2 -4 172.199 26.1948 2 -11 2 4 149.038 26.7576 2 11 -2 4 132.448 22.4785 1 11 2 -4 164.214 24.3053 1 -11 2 -4 177.353 26.7158 2 11 -2 -4 151.125 24.4446 1 -11 -2 4 131.503 25.2422 2 11 2 4 162.466 22.3463 1 -12 2 4 82.4710 24.7764 2 12 -2 4 78.2163 22.3573 1 12 2 -4 78.4959 22.6589 1 12 2 4 130.470 23.1422 1 -12 -2 4 87.1577 25.3247 2 -12 2 -4 124.072 28.1103 2 12 -2 -4 127.714 24.5278 1 13 2 -4 34.9251 20.5280 1 -13 2 4 11.2741 24.5511 2 13 -2 4 15.1954 20.0594 1 -13 -2 4 13.2098 23.2895 2 13 2 4 31.4119 25.6571 2 -13 2 -4 82.5928 26.0994 2 13 -2 -4 42.3660 21.3652 1 0 3 4 580.510 35.7812 3 0 3 -4 611.643 37.9973 1 0 -3 -4 594.128 41.2901 2 0 -3 4 547.213 36.3030 3 0 3 4 676.318 41.3505 2 0 3 4 581.543 35.5695 1 0 3 -4 621.289 36.4490 3 0 -3 -4 592.969 35.5160 1 0 -3 4 581.983 37.9147 1 1 3 -4 337.332 21.9087 3 -1 -3 -4 313.824 24.6681 2 1 -3 4 315.282 22.9079 1 -1 3 4 388.243 24.8653 2 1 -3 4 336.669 20.4438 2 1 -3 4 307.481 21.7285 3 -1 3 4 330.386 21.1253 1 1 3 -4 320.118 24.2043 1 -1 3 4 310.745 20.0560 3 1 -3 -4 272.505 23.8743 2 -1 -3 4 267.128 21.2451 3 1 -3 -4 308.152 20.9355 1 1 3 4 285.013 24.7570 2 -1 -3 4 296.010 23.4601 1 -1 3 -4 274.156 21.7906 3 1 3 4 274.821 21.3086 3 -1 3 -4 267.102 22.1800 1 2 -3 4 111.768 12.8894 1 -2 3 4 108.091 11.0569 3 -2 3 4 123.182 12.3975 1 2 3 -4 137.267 14.6237 1 -2 -3 -4 130.011 14.2752 2 2 -3 4 119.610 12.3743 3 2 3 -4 120.152 13.1767 2 2 -3 4 121.496 13.3795 2 2 3 -4 127.714 14.2348 3 -2 3 4 131.808 14.3060 2 -2 -3 4 160.441 13.2906 2 -2 -3 4 198.149 14.7026 3 -2 3 -4 163.180 15.1950 2 2 3 4 179.817 18.1229 2 -2 -3 4 185.976 17.0078 1 2 -3 -4 171.235 14.4452 1 -2 3 -4 166.465 15.1661 1 2 3 4 175.094 14.8625 3 -2 3 -4 188.113 15.5493 3 2 -3 -4 192.900 18.2322 2 3 -3 4 1844.88 105.892 3 3 3 -4 1912.80 107.735 2 3 3 -4 1863.38 109.969 1 3 3 -4 1944.55 105.802 3 3 -3 4 1932.59 109.471 1 -3 3 4 1914.29 109.183 2 3 -3 4 1916.75 108.462 2 -3 3 4 1876.75 109.264 1 -3 3 -4 1754.41 106.174 3 -3 3 -4 1846.24 109.155 1 3 -3 -4 1771.62 109.073 1 -3 3 -4 1811.52 108.307 2 3 3 4 1891.15 107.268 1 3 3 4 1825.57 109.160 2 -3 -3 4 1881.37 107.879 2 -3 -3 4 1867.55 109.700 1 3 3 4 1848.40 107.272 1 3 3 4 1818.51 106.227 3 4 -3 4 291.503 23.5984 1 4 3 -4 332.670 21.3877 3 -4 3 4 344.438 25.5905 2 4 -3 4 361.133 22.2741 3 -4 -3 -4 340.191 24.8288 4 4 3 -4 306.984 23.0171 2 4 3 4 276.088 20.3734 1 -4 3 -4 287.791 23.9877 2 4 3 4 287.660 20.5457 1 -4 -3 4 280.832 23.2551 1 -4 3 -4 272.947 21.9499 3 -4 -3 4 287.027 23.5001 2 -4 3 -4 256.489 25.1025 4 4 3 4 292.613 25.8544 2 4 -3 -4 287.409 23.4214 1 5 -3 4 3362.93 195.156 1 5 3 -4 3460.16 188.543 3 -5 3 4 3355.90 194.414 2 5 3 -4 3321.62 195.190 1 5 -3 4 3302.52 188.767 3 -5 -3 4 3336.72 193.526 2 5 3 4 3483.62 193.426 1 -5 3 -4 3320.42 188.555 3 5 3 4 3368.13 194.607 2 5 -3 -4 3342.54 195.342 1 -5 3 -4 3256.88 193.882 2 5 3 4 3371.49 193.309 1 6 3 -4 169.040 18.1724 1 -6 3 4 174.642 18.8704 2 6 -3 4 196.110 19.2253 1 6 3 -4 173.835 14.8348 3 -6 3 -4 164.377 17.8711 2 6 -3 -4 133.684 16.3365 1 -6 -3 4 101.742 16.1117 2 -6 3 -4 131.564 14.7673 3 6 3 4 105.040 13.1325 1 7 3 -4 783.273 49.2467 3 -7 3 4 798.784 54.5609 2 7 -3 4 819.969 53.9620 1 7 3 -4 777.181 53.4498 1 -7 -3 4 851.608 53.8291 2 7 3 4 834.739 51.5656 1 7 -3 -4 858.735 54.4760 1 -7 3 -4 795.456 54.1765 2 8 3 -4 177.063 20.3113 1 8 -3 4 116.725 18.2037 1 -8 3 4 161.136 21.9101 2 8 3 -4 164.922 16.2956 3 8 -3 -4 198.409 21.1602 1 8 3 4 160.755 17.7531 1 -8 -3 4 159.954 21.0151 2 -8 3 -4 142.251 21.1698 2 -9 3 4 66.7574 18.4664 2 9 3 -4 31.3115 14.7775 1 9 3 -4 54.9448 11.0277 3 9 -3 4 36.9579 15.6006 1 -9 -3 4 58.4375 18.1699 2 -9 3 -4 76.8678 19.1211 2 9 -3 -4 65.0598 16.3814 1 9 3 4 67.2641 13.9563 1 -10 3 4 -7.0097 18.1995 2 10 -3 4 -1.9663 13.7531 1 10 3 -4 -1.8174 13.7001 1 -10 3 -4 21.4357 18.8937 2 10 -3 -4 29.0957 16.3370 1 10 3 4 15.8610 13.1188 1 -10 -3 4 9.77735 17.5799 2 11 3 -4 26.8847 18.3415 1 11 -3 4 19.8751 17.8119 1 -11 3 4 39.0470 21.0297 2 11 3 4 28.1940 15.4258 1 -11 -3 4 32.7614 20.8772 2 11 -3 -4 24.6836 17.8297 1 -11 3 -4 30.0872 20.7645 2 -12 3 4 61.2376 23.5619 2 12 -3 4 81.4478 21.5615 1 12 3 -4 49.3757 20.8606 1 12 3 4 71.1093 24.7019 2 12 -3 -4 64.5414 21.6370 1 -12 3 -4 92.8110 25.3839 2 12 3 4 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850.051 48.3580 3 2 -4 4 839.172 48.4829 2 2 4 -4 932.853 51.8384 1 -2 4 4 861.833 49.3290 1 -2 -4 4 741.624 50.7497 1 2 -4 -4 764.707 49.1108 1 -2 4 -4 743.358 47.9359 3 2 4 4 776.210 50.6113 2 -2 4 -4 718.375 49.7137 1 2 -4 -4 788.021 50.5327 2 -2 -4 4 748.830 47.4939 2 -2 -4 4 804.531 48.4304 3 -2 4 -4 762.812 48.3940 2 3 -4 4 1359.61 81.7742 3 3 4 -4 1377.38 83.0318 2 3 -4 4 1314.95 84.9104 1 3 4 -4 1448.11 82.2215 3 -3 4 4 1363.74 85.0004 2 -3 -4 -4 1408.86 84.4769 4 -3 4 -4 1448.43 83.7988 2 -3 -4 4 1457.54 83.2391 2 -3 4 -4 1450.20 82.5047 3 3 4 4 1479.58 82.4712 1 3 -4 -4 1442.99 84.8067 1 -3 -4 4 1471.34 85.7374 1 3 4 4 1428.50 85.1308 2 -3 4 -4 1387.32 84.8853 1 3 4 4 1514.95 82.8205 1 4 4 -4 649.865 41.5829 2 4 -4 4 627.446 43.2089 1 -4 4 4 698.581 43.7256 2 4 -4 4 650.948 40.6355 3 -4 -4 -4 722.442 43.6457 4 4 4 -4 676.400 40.8073 3 4 -4 -4 669.906 42.9630 1 4 4 4 670.439 40.1403 1 -4 -4 4 655.956 42.9493 1 4 4 4 698.621 44.4134 2 -4 -4 4 650.302 41.7096 2 -4 4 -4 624.379 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7 802.796 55.7165 1 -7 -10 7 776.024 55.8869 1 7 10 7 795.628 56.2876 2 7 -10 -7 760.345 54.7421 1 -7 10 -7 759.735 52.0574 3 -7 10 -7 818.513 53.7082 2 8 -10 7 -15.295 15.4786 1 8 10 -7 12.3013 13.1424 3 -8 10 7 25.1105 18.6608 2 -8 10 -7 8.11343 16.5267 2 8 10 7 28.3729 20.0427 2 -8 10 -7 4.93327 13.8098 3 8 -10 -7 -16.292 13.9332 1 -8 -10 7 0.88549 13.6072 1 9 10 -7 56.8605 15.5684 3 9 10 -7 50.8385 19.0918 1 -9 10 7 51.3636 21.3102 2 9 -10 7 33.5117 19.4867 1 9 10 7 28.9758 21.7298 2 -9 10 -7 24.3506 18.7255 2 9 -10 -7 30.6507 17.8115 1 10 10 -7 57.1621 18.8411 1 10 -10 7 42.2089 20.0141 1 10 10 -7 59.4260 16.7963 3 -10 10 7 60.3900 24.1669 2 10 10 7 66.3586 24.3935 2 -10 10 -7 71.0800 21.9122 2 10 -10 -7 51.8851 20.3498 1 -11 10 7 66.7760 25.2924 2 11 -10 7 68.2560 23.6418 1 11 10 -7 37.6035 20.2340 1 11 -10 -7 68.3743 23.1472 1 11 10 7 79.9589 25.9374 2 -11 10 -7 92.2304 24.2174 2 12 10 -7 -23.293 17.3788 1 12 -10 7 -17.483 19.0873 1 -12 10 -7 2.10783 24.4122 2 0 -11 -7 93.7185 12.0533 1 0 -11 7 59.1692 13.9878 1 0 11 7 90.1899 18.7354 2 0 11 -7 86.8319 14.5203 3 -1 11 7 857.296 59.2855 2 -1 -11 -7 898.703 54.8007 1 1 11 -7 860.662 56.6118 3 1 -11 7 812.649 58.0506 1 1 -11 -7 928.719 56.3162 1 1 11 7 867.711 60.3691 2 1 11 7 930.360 54.7290 1 -1 -11 7 867.040 58.9715 1 -1 11 -7 903.726 56.5406 3 -2 11 7 259.185 28.0811 2 2 11 -7 253.739 25.1423 3 -2 -11 -7 281.669 22.0142 1 2 -11 -7 292.122 24.6650 1 -2 11 -7 291.352 24.6985 3 -2 -11 7 287.796 27.0304 1 2 11 7 306.832 32.4770 2 2 11 7 292.723 21.3991 1 3 -11 7 102.729 16.9533 1 -3 -11 -7 118.746 13.4278 4 3 11 -7 139.737 17.0381 3 3 -11 7 84.2461 12.1243 2 -3 -11 -7 126.210 12.0355 1 -3 11 7 125.125 18.6253 2 -3 -11 7 101.037 17.8495 1 3 -11 -7 96.3689 15.7189 1 3 11 7 90.5868 21.6506 2 -3 11 -7 106.527 12.5727 2 3 11 7 93.3614 10.5924 1 -3 11 -7 90.4545 14.7220 3 -4 -11 -7 549.429 38.7500 4 4 -11 7 618.047 43.7749 1 4 11 -7 617.388 42.0012 3 -4 11 7 629.752 44.3128 2 -4 11 -7 552.616 40.0664 3 4 -11 -7 600.634 42.2025 1 4 11 7 596.187 46.5517 2 -4 11 -7 580.197 39.3193 2 -4 -11 7 583.991 43.8886 1 -4 11 -7 563.609 40.8632 4 4 11 7 579.337 36.6117 1 -5 11 7 119.313 13.0478 3 5 11 -7 143.270 18.8638 3 5 -11 7 144.238 20.7507 1 5 11 -7 130.483 15.1202 2 -5 11 7 127.138 21.1038 2 -5 11 -7 154.959 18.0226 2 5 11 7 142.238 23.0544 2 5 11 7 141.304 12.8279 1 -5 -11 7 168.852 21.8404 1 -5 11 -7 145.739 18.4726 3 5 -11 -7 176.411 20.6079 1 -6 11 7 693.934 48.5765 2 6 11 -7 649.806 43.2296 2 6 11 -7 659.649 45.3420 3 6 -11 7 681.602 48.1402 1 6 -11 -7 650.458 47.3576 1 6 11 7 666.090 49.7195 2 -6 11 -7 615.817 44.8027 3 -6 -11 7 529.983 47.5292 1 -6 11 -7 628.173 44.9732 2 7 -11 7 31.2033 15.9563 1 7 11 -7 61.1605 15.3737 3 -7 11 7 47.9185 18.5182 2 7 11 -7 44.7358 13.9008 2 -7 11 -7 74.7598 17.1891 2 7 11 7 31.4820 20.5213 2 -7 11 -7 17.4245 14.0750 3 -7 -11 7 22.3767 13.9978 1 7 -11 -7 29.4403 15.8769 1 8 11 -7 138.355 20.8498 2 8 11 -7 183.728 22.1748 3 -8 11 7 184.918 26.7842 2 8 -11 7 162.416 25.0681 1 -8 11 -7 160.263 22.0668 3 -8 -11 7 190.145 24.5822 1 8 11 7 191.655 28.3222 2 8 -11 -7 188.248 25.5388 1 -8 11 -7 177.185 23.7584 2 9 11 -7 313.745 34.1124 1 9 11 -7 285.912 30.8535 2 9 11 -7 398.474 32.1018 3 9 -11 7 392.911 35.9426 1 -9 11 7 340.653 36.9675 2 9 -11 -7 313.515 34.3382 1 9 11 7 366.261 38.2087 2 -9 11 -7 313.300 33.7075 2 10 -11 7 26.2364 18.6935 1 10 11 -7 16.3470 14.9206 3 10 11 -7 -2.0322 16.4345 1 -10 11 7 4.90917 20.4038 2 10 11 7 4.80827 23.3270 2 10 -11 -7 -6.4190 17.8465 1 -10 11 -7 -5.1971 19.1998 2 11 11 -7 295.058 33.3102 1 -11 11 7 310.652 37.2069 2 11 -11 7 218.599 32.4726 1 11 11 7 278.581 37.1878 2 11 -11 -7 323.037 36.9129 1 -11 11 -7 328.870 35.7138 2 0 -12 7 2009.56 121.515 1 0 12 7 2027.94 121.026 2 0 12 -7 1953.26 117.133 3 0 -12 -7 1965.12 117.837 1 -1 12 7 45.2557 16.8580 2 1 12 -7 65.2955 13.9840 3 1 -12 7 51.7266 14.1617 1 -1 -12 -7 58.7798 11.1674 1 -1 12 -7 77.7574 14.3999 3 1 12 7 68.0838 19.0812 2 1 -12 -7 75.9633 13.2323 1 -1 -12 7 70.8643 15.6160 1 -2 -12 -7 763.700 54.5652 1 -2 12 7 798.197 58.4332 2 2 -12 7 814.369 58.6101 1 2 12 -7 755.604 56.3572 3 2 12 7 916.183 61.0593 2 2 -12 -7 939.792 57.2388 1 -2 12 -7 917.442 56.6281 3 2 12 7 1003.43 54.6005 1 -2 -12 7 1003.01 60.8837 1 3 -12 7 113.457 16.8740 1 -3 -12 -7 90.4039 10.9710 1 -3 -12 -7 95.2481 11.8254 4 -3 12 7 95.1748 17.9212 2 3 12 -7 111.662 16.4332 3 -3 12 -7 94.8722 14.7315 3 -3 -12 7 72.2484 16.5483 1 -3 12 -7 63.3709 11.6295 2 -3 12 -7 91.8070 14.5123 4 3 12 7 72.1541 10.5397 1 3 -12 -7 116.245 16.4417 1 3 12 7 118.363 21.8481 2 4 -12 7 122.674 18.7164 1 -4 12 7 132.064 20.4839 2 -4 -12 -7 108.329 11.9476 1 4 12 -7 90.2971 16.6935 3 -4 -12 7 99.9935 18.5851 1 4 -12 -7 113.373 17.7231 1 4 12 7 105.450 23.0046 2 -4 12 -7 102.031 14.5762 2 -4 12 -7 92.0592 15.5601 3 -4 12 -7 104.629 16.2839 4 5 12 -7 14.2212 12.8745 3 -5 12 7 51.6962 9.49790 3 5 -12 7 39.5044 15.7910 1 -5 12 7 -3.3186 15.2906 2 -5 12 -7 19.7252 12.3358 3 5 12 7 30.1740 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729.311 58.1187 2 10 -12 -7 717.444 57.3627 1 -10 12 -7 687.231 55.1145 2 10 12 7 774.993 59.5368 2 11 -12 7 9.17891 20.4134 1 11 12 -7 2.64749 17.7997 1 -11 12 -7 12.8854 22.3056 2 11 12 7 11.6693 25.0398 2 0 -13 -7 0.12407 9.17501 1 0 -13 7 -13.526 10.6826 1 0 13 -7 -1.4889 10.9019 3 0 13 7 2.50291 15.3652 2 1 -13 7 900.129 65.4550 1 -1 13 7 970.323 66.3885 2 -1 -13 -7 944.155 62.6421 1 1 13 -7 990.191 64.4334 3 -1 13 -7 1051.36 64.4181 3 1 13 7 1052.04 68.3351 2 1 -13 -7 1109.77 64.1992 1 -1 -13 7 1016.80 66.8471 1 2 13 -7 154.595 19.9322 3 -2 -13 -7 158.919 17.2164 1 2 -13 7 153.739 20.9900 1 -2 13 7 159.064 21.9266 2 -2 13 -7 209.182 21.4447 3 2 -13 -7 204.513 20.5062 1 2 13 7 156.044 24.0038 2 -2 -13 7 203.616 23.0712 1 -3 -13 -7 210.378 19.6528 1 -3 13 7 223.289 25.2929 2 3 13 -7 221.896 24.3468 3 3 -13 7 224.385 25.0822 1 -3 13 -7 271.631 24.6027 3 -3 13 -7 241.814 20.5014 2 3 -13 -7 273.454 25.2644 1 -3 13 -7 218.855 22.3620 4 -3 -13 7 236.232 26.3478 1 3 13 7 267.485 28.8802 2 4 13 -7 299.463 27.1324 3 -4 -13 -7 271.251 20.8159 1 -4 13 7 309.079 30.5766 2 4 -13 7 293.326 28.1550 1 -4 13 7 318.539 23.7788 3 4 -13 -7 278.909 27.5271 1 -4 13 -7 221.078 23.4962 2 -4 13 -7 236.113 25.1498 3 4 13 7 304.557 32.6737 2 -4 -13 7 258.875 28.5441 1 -5 13 7 12.7345 9.02695 3 5 13 -7 9.69919 13.5409 3 -5 13 7 4.11710 15.8292 2 5 -13 7 -0.0850 12.7709 1 5 -13 -7 7.81731 12.9967 1 -5 13 -7 7.90389 12.2626 3 -5 -13 7 -7.7939 12.9859 1 -5 13 -7 4.97871 12.0524 2 5 13 7 -12.619 18.5898 2 -6 13 7 162.801 23.7204 2 6 -13 7 172.587 24.4335 1 6 13 -7 160.994 21.4399 3 -6 13 -7 141.405 19.7554 2 -6 -13 7 143.967 22.8179 1 6 13 7 133.559 25.2538 2 6 -13 -7 136.767 21.6073 1 -6 13 -7 124.567 19.2333 3 7 13 -7 117.893 20.2419 3 -7 13 7 132.858 23.3680 2 7 -13 7 99.1434 21.3974 1 -7 -13 7 113.856 21.7119 1 -7 13 -7 114.410 20.1770 2 7 -13 -7 127.029 22.0636 1 -7 13 -7 111.744 18.6318 3 7 13 7 152.054 26.1905 2 8 -13 7 10.2660 16.9544 1 -8 13 7 40.7844 20.5802 2 8 13 -7 25.9119 15.9086 3 -8 13 -7 31.6619 17.4866 2 8 -13 -7 -0.5659 16.5480 1 -8 -13 7 15.4179 15.5929 1 8 13 7 20.9748 22.2346 2 9 13 -7 458.556 38.7690 3 -9 13 7 491.935 44.5088 2 9 -13 7 469.519 41.9046 1 9 -13 -7 381.833 40.3872 1 9 13 7 407.535 44.3649 2 -9 13 -7 425.742 39.4297 2 10 -13 7 2.55020 18.0080 1 10 13 -7 19.0132 17.1607 3 -10 13 7 42.7456 23.5801 2 10 13 -7 31.8802 18.3815 1 10 13 7 12.8666 24.6759 2 -10 13 -7 5.54037 20.6401 2 10 -13 -7 4.75170 18.4183 1 11 13 -7 316.025 35.8559 1 -11 13 -7 318.147 37.0585 2 11 13 7 340.256 41.0024 2 0 -14 -7 686.163 44.0965 1 0 -14 7 560.399 46.4157 1 0 14 -7 712.861 46.0975 3 0 14 7 581.160 47.1413 2 1 14 -7 43.7973 14.6627 3 -1 -14 -7 42.5168 11.7958 1 -1 14 7 26.9772 15.6473 2 1 -14 7 50.2874 14.4585 1 -1 14 -7 54.1823 14.5700 3 1 -14 -7 83.6044 14.4559 1 -1 -14 7 88.0701 17.0769 1 1 14 7 85.2513 19.7580 2 -2 -14 -7 120.495 15.5779 1 2 -14 7 109.609 18.6823 1 2 14 -7 107.042 17.9931 3 -2 14 7 146.885 20.7054 2 2 -14 -7 123.837 17.6181 1 -2 14 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6 14 7 21.3048 21.3518 2 7 -14 7 364.453 36.3536 1 -7 14 7 361.467 37.3955 2 7 14 -7 413.821 34.8335 3 7 -14 -7 386.502 35.8343 1 -7 14 -7 378.518 33.2374 3 -7 14 -7 376.987 33.5639 2 7 14 7 381.548 39.1038 2 -7 -14 7 351.535 36.6076 1 8 -14 7 80.4830 21.9913 1 8 14 -7 47.4113 18.6526 3 -8 14 7 91.8606 23.1120 2 -8 -14 7 47.0292 18.7679 1 8 -14 -7 80.5563 20.8474 1 -8 14 -7 39.7954 18.5684 2 -9 14 7 15.1034 21.8469 2 9 14 -7 33.4102 17.4209 3 9 -14 7 48.3057 20.4732 1 9 -14 -7 -11.987 17.1064 1 -9 -14 7 18.4259 16.6999 1 -9 14 -7 7.26891 19.9104 2 9 14 7 3.63350 24.0372 2 10 14 -7 99.6325 22.2374 3 -10 14 7 137.751 28.6669 2 10 14 -7 115.645 24.1929 1 10 -14 7 128.617 26.4626 1 -10 14 -7 84.1902 24.5795 2 10 -14 -7 83.8953 25.1500 1 10 14 7 117.000 29.0106 2 0 15 -7 25.7962 13.6237 3 0 -15 -7 39.9075 12.0355 1 0 -15 7 42.7789 15.2852 1 0 15 7 27.3767 17.3501 2 1 -15 7 43.3152 15.1264 1 -1 15 7 22.0257 16.1532 2 -1 -15 -7 47.9661 12.4274 1 1 15 -7 38.0641 14.0614 3 1 -15 -7 23.4737 11.8306 1 1 15 7 30.6145 17.6000 2 -1 15 -7 43.4025 14.5925 3 -1 -15 7 23.5789 14.5286 1 -2 -15 -7 142.854 17.6034 1 -2 15 7 177.286 22.7945 2 2 15 -7 180.229 21.2201 3 2 -15 7 168.645 21.7361 1 -2 15 -7 123.189 18.9509 3 2 -15 -7 152.190 19.5822 1 -2 15 -7 131.099 15.5668 4 -2 -15 7 130.758 21.5561 1 2 15 7 130.366 23.3425 2 3 15 -7 78.3879 16.9778 3 -3 15 7 65.6789 13.9608 3 3 -15 7 83.5126 17.9214 1 -3 15 7 105.176 19.1194 2 -3 -15 -7 64.2389 11.6989 1 3 15 7 80.0138 21.7642 2 3 -15 -7 79.7260 16.5264 1 -3 15 -7 75.5034 15.5016 3 -3 -15 7 79.3813 18.6781 1 -4 15 7 1095.58 67.6492 3 4 15 -7 1092.72 71.4408 3 -4 15 7 1079.44 72.8260 2 4 -15 7 1101.64 73.6402 1 4 -15 -7 1105.52 72.5714 1 -4 15 -7 1065.70 69.7546 3 -4 -15 7 1126.89 74.8747 1 4 15 7 1086.20 75.6055 2 5 15 -7 99.6084 18.4967 3 -5 15 7 -4.1686 16.7960 2 5 -15 7 -9.4542 13.8549 1 5 -15 -7 29.0263 15.7067 1 -5 15 -7 24.3089 13.0595 3 -5 15 -7 21.3862 13.1431 2 -5 -15 7 21.9345 14.9925 1 5 15 7 -1.8611 20.8335 2 6 -15 7 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299.987 29.5942 4 7 -1 9 291.986 26.4105 1 7 -1 9 258.700 29.0601 2 -7 1 9 293.119 29.2553 2 7 1 -9 256.424 21.4641 3 -7 -1 9 266.621 27.4420 2 7 1 9 323.965 25.2726 1 -7 1 -9 335.602 26.2195 3 7 -1 -9 313.132 27.8933 1 -7 1 -9 298.978 29.5396 4 7 1 9 297.421 30.3485 2 8 1 -9 252.407 26.4021 1 8 -1 9 192.921 23.0793 1 8 -1 9 215.678 25.8643 2 -8 1 9 205.379 25.6700 2 8 1 9 244.051 24.0857 1 8 1 9 269.477 27.8896 2 -8 -1 9 252.266 26.7665 2 8 -1 -9 242.159 25.7374 1 9 1 -9 13.6626 15.6665 1 -9 1 9 38.4317 18.2629 2 9 -1 9 19.0774 18.4367 2 9 -1 9 35.2927 13.8905 1 9 -1 -9 34.2204 15.9861 1 9 1 9 49.0802 19.5285 2 -9 -1 9 -4.1180 17.7630 2 9 1 9 -7.6228 12.2879 1 10 -1 9 158.389 26.8337 2 -10 1 9 203.681 27.1754 2 10 1 -9 173.429 25.0249 1 10 -1 9 168.078 22.4266 1 10 1 9 127.355 26.1062 2 -10 -1 9 160.820 26.2262 2 10 -1 -9 190.414 24.9368 1 -11 1 9 59.9086 24.0094 2 11 1 -9 89.2941 21.8706 1 11 -1 9 78.0573 24.5932 2 11 1 9 78.5076 24.3458 2 -11 -1 9 63.1567 22.8111 2 11 -1 -9 72.0135 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-5 2 9 67.3797 15.2423 2 5 -2 9 59.0265 11.7926 1 -5 2 9 48.4732 8.12621 3 5 2 -9 68.1636 14.5920 1 5 2 9 70.8533 15.6443 2 -5 -2 9 65.6171 13.6819 2 5 -2 -9 54.9914 12.6518 1 5 -2 -9 57.4662 8.61877 3 -5 2 -9 57.0618 13.3261 3 5 2 9 59.6785 9.15875 1 -6 -2 -9 83.5023 17.9399 4 6 2 -9 83.8396 15.9530 1 -6 2 9 88.4700 17.6434 2 -6 -2 -9 60.6429 9.60222 1 6 2 -9 102.177 11.9269 3 6 -2 9 66.4849 13.9629 1 6 -2 9 84.9523 17.5084 2 -6 2 -9 126.607 16.8543 3 -6 2 -9 118.665 18.6498 4 6 2 9 123.426 12.5523 1 6 -2 -9 141.916 17.2345 1 -6 -2 9 124.180 17.1060 2 6 2 9 110.643 18.6662 2 7 -2 9 509.634 38.2782 1 -7 -2 -9 504.965 40.6076 4 7 2 -9 494.049 33.8672 3 7 2 -9 475.141 39.4926 1 -7 2 9 518.519 40.9235 2 7 -2 9 531.749 40.7315 2 -7 2 -9 599.829 42.1288 4 7 -2 -9 507.275 39.4221 1 7 2 9 485.101 40.6368 2 -7 2 -9 593.958 38.2310 3 7 2 9 533.043 36.3652 1 -7 -2 9 597.423 40.0315 2 -8 2 9 66.6500 18.7003 2 8 -2 9 55.9038 18.7387 2 8 2 -9 48.8784 9.82297 3 8 -2 9 43.1931 14.3007 1 8 2 -9 62.1434 16.5683 1 8 -2 -9 64.3731 15.9905 1 -8 -2 9 59.7282 17.7305 2 8 2 9 55.9053 18.9080 2 8 2 9 44.1113 12.9620 1 9 -2 9 659.106 49.5281 1 9 2 -9 577.208 49.9129 1 9 -2 9 666.428 51.1394 2 -9 2 9 672.007 51.0608 2 -9 -2 9 798.925 51.0435 2 9 2 9 742.529 52.4890 2 9 2 9 696.796 47.6591 1 9 -2 -9 680.540 50.4048 1 10 -2 9 146.350 26.5669 2 10 2 -9 173.680 25.5586 1 -10 2 9 192.799 27.0100 2 10 -2 9 159.130 23.6684 1 -10 -2 9 163.354 25.5828 2 10 2 9 192.914 27.2911 2 10 -2 -9 126.817 23.2623 1 -11 2 9 503.120 42.1552 2 11 2 -9 480.712 40.4138 1 11 -2 9 398.939 40.9820 2 11 -2 9 362.742 36.2954 1 11 -2 -9 375.486 38.7274 1 -11 -2 9 387.806 39.2831 2 11 2 9 374.010 41.3472 2 12 2 -9 27.9636 20.6515 1 12 -2 9 42.1574 25.1076 2 -12 2 9 58.9332 25.7036 2 12 -2 -9 47.1143 21.7113 1 -12 -2 9 67.9153 24.6629 2 0 3 -9 2211.44 123.610 3 0 3 -9 2088.61 124.668 2 0 -3 -9 2214.58 123.014 3 0 -3 -9 2154.93 124.292 1 0 -3 9 2046.33 126.618 1 0 -3 9 2119.92 124.530 2 0 -3 -9 2185.38 124.660 1 0 3 9 2182.75 127.098 2 -1 -3 -9 245.688 14.3421 1 1 -3 9 209.284 19.5907 2 -1 -3 -9 222.411 15.1572 1 1 3 -9 246.440 21.0050 2 -1 -3 -9 246.999 19.4899 3 1 -3 9 220.683 19.0081 1 1 3 -9 222.828 19.3053 3 -1 3 9 236.434 25.2784 2 -1 -3 9 157.038 17.6645 2 1 -3 -9 157.963 16.6056 1 1 3 9 173.652 21.1789 2 1 -3 -9 160.239 17.8829 3 -1 3 -9 165.763 17.7147 2 1 -3 -9 154.802 16.2350 1 -1 3 -9 177.718 19.9022 3 -1 -3 9 154.338 18.7899 1 2 -3 9 1842.29 103.779 2 2 -3 9 1768.92 103.450 2 -2 -3 -9 1805.16 102.627 3 -2 3 9 1657.76 105.140 2 2 3 -9 1754.70 101.983 3 2 3 -9 1716.26 103.279 2 -2 3 9 1686.98 101.267 3 2 -3 9 1724.17 104.668 1 -2 -3 9 1737.41 105.531 1 -2 -3 9 1877.59 103.073 2 2 -3 -9 1802.97 104.197 1 -2 3 -9 1775.70 103.061 3 2 -3 -9 1800.03 101.117 3 2 3 9 1787.93 106.024 2 3 -3 9 136.776 15.8407 1 3 -3 9 166.701 17.0686 2 3 3 -9 164.868 16.0575 2 -3 3 9 153.900 16.3096 3 3 3 -9 176.643 17.2309 3 -3 -3 -9 160.710 16.7555 3 -3 3 9 158.561 18.3664 2 -3 3 -9 176.118 19.0852 3 3 -3 -9 193.427 15.4339 3 -3 -3 9 202.227 19.4964 1 -3 -3 9 175.041 16.9373 2 3 3 9 176.073 19.2905 2 3 -3 -9 160.379 17.6333 1 4 3 -9 108.159 12.4775 3 -4 3 9 87.4351 15.3126 2 4 -3 9 81.6547 13.2381 1 4 -3 9 99.8110 14.9056 2 -4 3 9 114.154 10.8568 3 -4 3 -9 76.1193 13.8842 3 4 -3 -9 106.609 14.0928 1 4 3 9 72.2304 16.2957 2 -4 -3 9 81.5146 14.6229 1 -4 -3 9 97.8246 12.8921 2 4 -3 -9 101.633 10.5635 3 -5 -3 -9 295.598 20.0475 1 -5 3 9 358.986 28.3082 2 5 -3 9 369.130 26.1366 1 5 -3 9 361.484 28.0210 2 5 3 9 269.284 20.4471 1 -5 3 -9 323.032 26.4980 3 -5 -3 9 261.909 25.9122 1 5 3 9 299.650 28.7012 2 -5 -3 9 265.849 24.9230 2 5 -3 -9 254.426 24.9512 1 6 -3 9 128.885 18.7872 2 6 3 -9 115.102 12.5955 3 6 3 -9 119.489 17.7568 1 6 -3 9 107.969 15.5381 1 -6 -3 -9 99.3544 17.9549 4 -6 3 9 112.001 18.2262 2 -6 3 -9 93.0431 16.1377 3 6 -3 -9 84.5991 15.2529 1 -6 3 -9 81.8898 17.9961 4 6 3 9 102.229 18.8588 2 6 3 9 93.5434 11.4930 1 -6 -3 9 92.1434 15.8489 2 7 3 -9 143.266 14.9227 3 7 3 -9 100.567 18.4279 1 7 -3 9 153.280 20.5794 2 -7 3 9 130.326 20.7015 2 -7 -3 -9 95.5709 20.0426 4 7 -3 9 120.165 18.2240 1 7 3 9 125.559 14.3342 1 -7 -3 9 131.638 18.8823 2 7 -3 -9 116.030 18.4672 1 -7 3 -9 128.465 21.3621 4 -7 3 -9 118.875 17.2053 3 7 3 9 119.626 20.9131 2 8 -3 9 418.583 37.5200 1 8 3 -9 390.580 31.8176 3 8 3 -9 438.210 38.5665 1 8 -3 9 453.168 39.2718 2 -8 3 9 410.436 39.3783 2 8 3 9 581.482 41.5652 2 -8 -3 9 569.595 39.3374 2 8 3 9 552.430 35.4088 1 -8 3 -9 556.081 36.5878 3 8 -3 -9 544.077 39.1054 1 9 -3 9 192.099 26.4893 2 9 -3 9 237.662 25.9862 1 -9 3 9 208.873 27.2902 2 9 3 -9 175.176 24.6830 1 9 3 9 190.564 27.3823 2 -9 -3 9 227.180 26.3437 2 9 -3 -9 228.264 26.0162 1 10 -3 9 613.581 50.2355 2 10 3 -9 580.774 48.4785 1 10 -3 9 604.647 47.4447 1 -10 3 9 589.931 49.6512 2 -10 -3 9 676.956 49.0553 2 10 3 9 726.498 51.9139 2 10 -3 -9 610.873 48.9303 1 11 3 -9 154.453 25.1832 1 11 -3 9 139.663 26.7184 2 -11 3 9 122.954 26.8054 2 11 -3 9 110.915 22.1053 1 11 -3 -9 125.811 24.1751 1 11 3 9 128.990 27.6755 2 -11 -3 9 123.313 24.5427 2 12 3 -9 301.160 34.9506 1 12 -3 9 277.288 36.1634 2 -12 3 9 339.555 37.3413 2 -12 -3 9 245.871 33.5505 2 12 3 9 243.828 35.7297 2 12 -3 -9 259.161 33.6602 1 0 4 -9 289.005 23.7452 3 0 4 9 293.950 27.7418 2 0 -4 -9 303.794 19.8352 1 0 -4 -9 303.759 20.0046 1 0 4 -9 274.317 20.9872 2 0 -4 9 265.518 23.8482 1 0 -4 -9 258.362 22.0383 3 0 -4 9 280.879 21.9651 2 -1 -4 -9 637.666 38.4094 1 1 -4 9 658.160 42.1103 1 1 4 -9 710.293 41.3550 3 -1 -4 -9 715.867 41.3095 3 -1 4 9 700.989 46.2199 2 -1 -4 -9 708.561 37.8777 1 1 4 -9 681.349 40.4441 2 1 -4 9 665.042 40.5470 2 -1 4 -9 617.228 41.4854 3 -1 -4 9 581.018 39.0409 2 1 -4 -9 571.624 39.4892 1 1 -4 -9 602.847 39.7364 3 -1 -4 9 505.214 41.7865 1 1 4 9 597.975 44.8660 2 1 -4 -9 604.091 39.7891 1 2 -4 9 338.896 29.3392 2 2 4 -9 375.865 29.5343 3 -2 4 9 426.278 33.6571 2 2 4 -9 345.543 29.1295 2 2 -4 9 397.332 29.2800 2 -2 4 9 363.897 28.4835 3 2 -4 9 387.754 30.5221 1 -2 -4 9 488.188 32.1293 1 2 -4 -9 496.771 29.7496 1 2 4 9 516.048 35.4975 2 -2 4 -9 488.903 31.8747 3 -2 -4 9 485.487 28.2772 2 2 -4 -9 487.251 28.6806 3 3 -4 9 449.074 31.8870 1 3 -4 9 447.913 31.5487 2 -3 4 9 440.723 28.9912 3 3 4 -9 450.300 30.4910 2 3 4 -9 452.701 30.3192 3 -3 4 9 474.505 34.2757 2 3 -4 -9 428.840 30.9426 1 -3 -4 9 445.597 29.3961 2 -3 4 -9 370.597 31.6214 3 3 4 9 424.000 34.9614 2 3 -4 -9 446.709 28.2419 3 -3 -4 9 418.343 32.6867 1 -4 4 9 847.005 53.4930 2 4 -4 9 776.888 51.8573 1 4 4 -9 873.695 49.8307 3 4 -4 9 862.267 51.9135 2 -4 4 9 813.196 48.3032 3 -4 -4 9 724.001 52.6863 1 4 -4 -9 777.173 51.6171 1 -4 -4 9 770.051 49.8822 2 -4 4 -9 755.553 51.1124 3 4 4 9 826.508 53.8416 2 5 -4 9 -0.6648 10.1222 1 5 -4 9 8.95720 12.4104 2 5 4 -9 8.51226 8.46524 3 -5 4 9 20.6032 13.6102 2 -5 -4 9 16.4158 10.6295 2 -5 -4 9 17.0477 11.3314 1 5 4 9 2.32023 13.6935 2 5 -4 -9 -1.7250 9.98142 1 -5 4 -9 12.1592 11.2407 3 6 4 -9 942.390 52.6321 3 -6 -4 -9 841.974 56.6514 4 -6 4 9 956.576 58.1040 2 6 -4 9 933.455 56.9253 2 6 -4 9 854.704 55.9215 1 6 4 9 777.932 51.2294 1 -6 4 -9 832.599 57.2222 4 6 4 9 827.306 57.8064 2 6 4 9 829.733 51.2030 1 6 -4 -9 815.527 56.1176 1 -6 4 -9 876.712 55.5802 3 -6 -4 9 764.987 54.3603 2 -7 4 9 352.322 31.1891 2 7 -4 9 297.853 27.8871 1 7 4 -9 299.953 29.1412 1 7 4 -9 262.877 23.2618 3 -7 -4 -9 277.407 30.0333 4 7 -4 -9 296.730 27.7607 1 -7 -4 9 309.875 28.1886 2 -7 4 -9 328.025 27.6661 3 7 4 9 306.152 23.4093 1 7 4 9 342.398 31.9086 2 -7 4 -9 307.665 30.9038 4 8 4 -9 235.192 27.0597 1 8 4 -9 238.922 21.9339 3 8 -4 9 252.200 26.8870 1 -8 4 9 274.984 30.4980 2 -8 4 -9 271.727 25.7708 3 8 4 9 336.276 32.1414 2 -8 -4 9 274.282 27.6533 2 8 4 9 253.202 23.2921 1 8 -4 -9 283.345 27.6222 1 9 -4 9 278.392 28.5511 1 9 4 -9 259.318 28.3976 1 -9 4 9 273.036 29.5288 2 9 4 9 217.766 28.7416 2 -9 -4 9 225.457 27.0248 2 9 -4 -9 247.763 28.5561 1 -10 4 9 66.1608 21.8336 2 10 4 -9 41.4971 18.6623 1 10 -4 9 39.8722 17.9847 1 10 -4 -9 66.5747 18.6439 1 10 4 9 74.1527 22.5981 2 -10 -4 9 70.9402 20.3439 2 11 -4 9 107.283 25.1951 2 11 4 -9 152.277 25.6015 1 11 -4 9 140.567 23.7019 1 -11 4 9 152.335 27.9187 2 -11 -4 9 137.418 25.4620 2 11 4 9 101.569 26.4126 2 11 -4 -9 117.222 24.5967 1 12 -4 9 81.0904 27.5141 2 -12 4 9 80.8517 26.2170 2 12 4 -9 98.2939 24.1197 1 -12 -4 9 76.1898 24.5472 2 12 4 9 63.6853 26.3694 2 12 -4 -9 96.4635 24.9411 1 0 -5 9 48.4645 11.4289 1 0 5 9 38.5826 14.3709 2 0 5 -9 44.5895 10.4936 3 0 -5 -9 62.6237 7.50155 1 0 -5 -9 38.9923 6.61735 1 1 -5 9 234.278 20.9816 1 1 -5 9 238.208 18.8566 2 1 5 -9 238.403 20.6727 3 1 -5 9 221.234 17.6497 2 -1 5 9 229.385 23.8394 2 -1 -5 9 200.480 21.6015 1 1 -5 -9 193.902 17.3594 1 1 -5 -9 219.848 17.5308 1 -1 5 -9 201.185 20.7430 3 1 5 9 221.351 23.4082 2 2 -5 9 790.221 53.2626 1 2 5 -9 880.874 51.8255 3 -2 5 9 839.669 54.9885 2 2 5 -9 828.314 50.7084 2 -2 5 9 802.060 50.2262 3 2 -5 9 883.605 51.3085 2 2 -5 9 886.805 51.1044 2 2 5 9 880.128 56.8989 2 -2 -5 9 775.611 49.5961 2 -2 -5 9 831.387 54.4884 1 -2 5 -9 814.555 52.5124 3 2 -5 -9 831.041 51.7439 1 3 -5 9 1360.04 83.3579 2 3 5 -9 1363.31 82.1857 3 -3 5 9 1243.61 80.5660 3 -3 5 9 1386.19 85.8263 2 3 5 -9 1419.15 82.5021 2 3 -5 9 1324.61 85.1741 1 -3 -5 9 1407.25 81.8882 2 3 -5 -9 1465.12 84.4735 1 3 5 9 1508.81 87.1696 2 -3 5 -9 1519.29 84.0930 3 -3 -5 9 1441.71 86.2820 1 4 5 -9 48.9442 10.8058 3 -4 5 9 38.6298 8.25828 3 4 -5 9 66.2891 13.1002 2 -4 5 9 82.4175 15.6914 2 4 -5 9 59.5380 11.8629 1 -4 5 -9 33.3849 11.9102 3 -4 -5 9 31.6680 9.71851 2 4 -5 -9 9.35678 9.49458 1 4 5 9 19.6913 14.4299 2 -4 -5 9 18.8139 11.4991 1 5 -5 9 1217.95 81.3895 1 5 5 -9 1311.52 78.1392 3 -5 5 9 1325.68 82.5355 2 5 -5 9 1237.70 80.4398 2 5 -5 -9 1322.80 81.5388 1 -5 5 -9 1319.59 79.6567 3 5 5 9 1396.03 83.4205 2 -5 -5 9 1381.01 83.5293 1 -5 -5 9 1357.23 79.2279 2 6 -5 9 102.108 16.9137 1 -6 -5 -9 128.296 18.0938 4 6 5 -9 121.529 14.2038 3 -6 5 9 126.584 19.3933 2 6 5 9 96.6243 19.7654 2 -6 5 -9 91.3128 16.8643 3 6 -5 -9 89.1295 16.2175 1 -6 -5 9 107.232 15.9233 2 -6 -5 9 72.0023 16.2324 1 -6 5 -9 97.2016 18.4736 4 -7 5 9 472.983 35.6333 2 -7 -5 -9 461.495 34.6392 4 7 5 -9 455.264 34.8894 1 7 5 -9 449.138 28.9284 3 7 -5 9 450.488 33.9374 1 7 5 9 335.353 34.3244 2 7 -5 -9 344.260 32.1110 1 7 5 9 345.214 26.9885 1 -7 5 -9 374.862 31.8377 3 -7 -5 9 313.749 31.2881 2 -7 5 -9 361.161 34.3989 4 -7 5 -9 348.966 32.8685 2 8 5 -9 143.802 16.9007 3 -8 5 9 149.902 24.4088 2 8 -5 9 183.464 23.1048 1 8 5 -9 144.626 22.7883 1 -8 5 -9 184.921 24.2115 2 -8 5 -9 193.391 21.2353 3 -8 -5 9 174.736 21.6734 2 8 5 9 189.761 25.2800 2 8 -5 -9 195.061 23.0591 1 9 5 -9 43.3498 17.6187 1 9 -5 9 56.6851 17.7423 1 -9 5 9 51.1818 20.7884 2 -9 -5 9 33.1065 17.1308 2 9 -5 -9 66.3378 17.8846 1 -9 5 -9 43.6161 19.5095 2 -9 5 -9 54.4102 14.7720 3 9 5 9 70.5880 21.7147 2 10 -5 9 -3.8205 15.0465 1 10 5 -9 1.91230 16.6618 1 -10 5 9 1.08107 20.5834 2 10 -5 -9 8.05527 16.1236 1 10 5 9 23.7725 21.1792 2 -10 -5 9 4.58323 17.4390 2 11 5 -9 81.8725 22.8949 1 -11 5 9 59.7101 24.6167 2 11 -5 9 65.0273 20.9820 1 11 5 9 66.3764 25.0397 2 11 -5 -9 46.1885 20.1803 1 -11 -5 9 79.1434 22.0984 2 12 -5 9 -3.3011 18.3593 1 12 5 -9 12.0122 19.5653 1 12 -5 9 28.8162 23.1309 2 -12 5 9 69.1499 25.6630 2 -12 -5 9 -3.9814 21.0478 2 12 5 9 8.55766 24.9091 2 12 -5 -9 16.3462 20.0587 1 0 6 9 38.3713 14.5119 2 0 -6 -9 47.7764 6.70700 1 0 6 -9 40.5535 10.4940 3 0 -6 -9 38.2993 7.00842 1 0 -6 9 26.2265 10.8711 1 -1 6 9 521.870 35.1254 1 1 -6 9 555.107 38.8847 1 1 6 -9 557.426 36.9120 3 -1 6 9 521.121 41.7173 2 -1 6 -9 558.648 37.1526 3 -1 -6 9 539.079 39.0880 1 1 -6 -9 555.053 35.3276 1 1 6 9 594.554 41.6960 2 -2 6 9 472.361 35.8469 2 2 -6 9 470.565 29.8651 2 2 -6 9 438.388 29.9836 2 2 -6 9 464.565 33.5380 1 2 6 -9 467.350 31.5451 3 2 6 9 432.341 37.3035 2 -2 6 -9 411.214 32.1525 3 -2 -6 9 457.122 34.2942 1 2 -6 -9 425.083 30.4108 1 -3 6 9 573.037 37.4759 3 3 -6 9 652.428 39.8478 2 3 -6 9 641.999 42.2465 1 3 6 -9 619.701 38.1607 2 3 -6 9 602.588 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7 -9 469.663 33.6730 3 8 7 -9 463.025 39.3734 1 8 7 9 463.774 40.8495 2 -8 -7 9 427.313 35.6900 2 8 -7 -9 446.911 37.5771 1 -8 7 -9 460.334 36.4746 3 -8 7 -9 441.711 37.7912 2 9 7 -9 59.6541 14.1373 3 9 -7 9 96.8201 20.2031 1 9 7 -9 64.9451 19.8079 1 9 7 9 75.7379 23.1595 2 -9 -7 9 79.3148 18.8490 2 -9 7 -9 47.3651 19.9278 2 9 -7 -9 52.0552 18.2894 1 -9 7 -9 50.1796 16.2585 3 10 7 -9 443.200 40.1334 1 -10 7 9 429.874 41.8626 2 10 -7 9 467.955 40.5214 1 10 -7 -9 402.029 38.8091 1 10 7 9 411.203 42.6074 2 -10 -7 9 377.001 37.8110 2 -10 7 -9 526.317 41.6858 2 11 7 -9 78.6156 21.8040 1 11 -7 9 55.9451 22.5607 1 -11 7 9 51.6380 24.4251 2 -11 7 -9 118.047 25.0704 2 11 7 9 74.3571 25.5991 2 -11 -7 9 92.2835 22.5314 2 11 -7 -9 101.481 22.6808 1 12 7 -9 260.390 33.3066 1 12 -7 9 199.716 30.4357 1 -12 -7 9 254.205 32.1027 2 0 -8 -9 133.285 13.8552 1 0 -8 9 132.018 17.1099 1 0 8 9 162.948 21.1265 2 0 8 -9 131.054 16.0193 3 0 8 9 122.899 12.9055 1 1 -8 9 1347.69 80.7674 1 -1 -8 -9 1382.14 75.7230 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14 -9 126.666 18.5982 3 3 14 9 141.430 24.4886 2 -3 14 -9 122.691 17.1554 4 3 -14 -9 121.938 18.4807 1 -3 -14 9 127.137 21.6139 1 4 14 -9 648.421 48.3247 3 -4 14 9 691.972 51.6580 2 4 -14 9 689.263 51.1800 1 4 -14 -9 688.908 49.0375 1 -4 -14 9 721.360 52.0743 1 -4 14 -9 629.655 46.6524 4 4 14 9 721.275 54.5714 2 -4 14 -9 650.396 47.4943 3 5 14 -9 242.041 25.8081 3 -5 14 9 208.187 27.7371 2 5 -14 9 251.436 27.5933 1 5 -14 -9 225.586 25.8880 1 -5 -14 9 190.859 26.1812 1 -5 14 -9 228.747 24.7796 3 5 14 9 201.109 32.6882 2 6 -14 9 342.530 35.3510 1 -6 14 9 402.184 38.2751 2 6 14 -9 394.218 34.5839 3 6 -14 -9 379.722 35.0954 1 -6 -14 9 410.037 37.2804 1 -6 14 -9 347.103 33.6900 3 6 14 9 357.931 40.7178 2 7 -14 9 69.1108 20.2622 1 7 14 -9 69.0194 18.7310 3 -7 14 9 101.220 22.9546 2 7 14 9 102.330 26.6575 2 -7 14 -9 87.0845 19.1117 3 -7 -14 9 57.0064 20.6224 1 7 -14 -9 67.2013 20.0312 1 8 -14 9 80.2965 22.8269 1 8 14 -9 85.4133 20.6168 3 -8 14 9 65.7167 23.1434 2 8 14 9 79.8123 26.5889 2 -8 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31.8552 26.8799 2 -12 -4 11 99.3132 25.8181 2 0 5 -11 12.5663 10.3516 3 0 -5 -11 24.1185 6.46887 1 0 5 -11 12.1645 8.01140 2 0 5 11 21.2677 14.5844 2 0 -5 -11 25.7822 6.64361 1 0 -5 11 28.3675 11.1757 1 0 -5 11 17.8094 9.12306 2 -1 -5 -11 320.309 20.2393 1 -1 5 11 294.801 30.4386 2 -1 -5 -11 297.352 20.8935 1 1 -5 11 340.498 26.4581 1 1 5 -11 346.248 26.0433 3 1 5 -11 295.727 23.0285 2 1 -5 11 302.854 22.8367 2 1 -5 11 277.541 24.5969 2 -1 -5 11 320.600 22.5917 2 -1 5 -11 286.223 26.0818 3 1 5 11 317.867 30.3741 2 1 -5 -11 334.975 22.8308 1 -1 -5 11 344.149 27.4794 1 1 -5 -11 295.147 23.0564 1 -2 5 11 118.176 19.8603 2 2 5 -11 99.5856 14.3473 3 2 -5 11 106.758 12.7965 2 2 5 -11 108.065 14.0126 2 2 -5 11 85.4867 14.9592 1 2 -5 11 100.739 13.7203 2 -2 -5 11 116.006 11.9019 2 -2 -5 11 115.579 15.8727 1 -2 5 -11 140.061 16.7655 3 2 5 11 125.258 21.3762 2 2 -5 -11 148.940 14.1575 1 -3 5 11 868.897 58.4908 2 3 -5 11 855.267 55.2486 2 3 5 -11 816.594 54.4942 2 3 -5 11 840.020 56.6904 1 3 5 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23.8420 2 11 5 11 50.7815 25.0839 2 11 -5 -11 18.5159 19.3141 1 -11 -5 11 60.0839 22.1764 2 12 -5 11 48.7857 27.2698 2 -12 -5 11 14.8075 23.2048 2 0 6 -11 363.983 29.2102 3 0 6 11 343.672 32.7404 2 0 -6 -11 408.788 25.4258 1 0 -6 -11 380.983 25.5054 1 0 -6 11 350.930 30.1453 1 1 -6 11 655.295 45.5496 1 1 -6 11 634.359 41.3802 2 1 6 -11 674.469 44.3451 3 -1 6 11 660.847 48.6756 2 1 -6 11 661.108 42.3990 2 1 -6 -11 724.950 42.6720 1 -1 -6 11 695.467 46.5007 1 1 6 11 698.388 48.7626 2 -1 6 -11 677.339 44.9161 3 1 -6 -11 640.451 42.2999 1 2 6 -11 550.288 37.4416 3 2 -6 11 526.168 35.8710 2 2 -6 11 481.484 35.2720 2 -2 6 11 595.396 43.3253 2 2 -6 11 465.449 37.8963 1 2 6 11 626.982 44.6478 2 2 -6 -11 587.361 36.5340 1 -2 6 -11 577.736 39.0668 3 -2 -6 11 530.866 39.4993 1 3 6 -11 230.823 21.2209 3 -3 6 11 221.070 23.6665 2 3 -6 11 198.537 21.3291 1 3 6 -11 208.134 20.3635 2 3 -6 11 213.748 20.8445 2 -3 -6 11 184.192 17.3807 2 -3 6 -11 211.535 21.3540 3 3 -6 -11 211.037 20.1692 1 3 6 11 232.937 26.0689 2 -3 -6 11 194.232 22.2398 1 4 -6 11 523.110 37.2017 2 4 -6 11 492.710 38.0182 1 -4 6 11 541.987 40.4344 2 -4 6 11 411.891 33.5323 3 4 6 -11 466.156 35.4567 3 -4 6 -11 545.603 38.4862 3 4 -6 -11 572.128 37.4367 1 -4 -6 11 547.268 34.3988 2 4 6 11 567.698 42.5594 2 -4 -6 11 540.165 38.8050 1 5 -6 11 237.504 25.6325 2 -5 6 11 249.548 26.1466 2 5 -6 11 217.908 23.7566 1 5 6 -11 195.420 21.4576 3 -5 -6 11 227.395 25.1605 1 -5 6 -11 234.913 24.6315 3 -5 -6 11 240.415 21.4160 2 5 6 11 284.553 27.6617 2 5 -6 -11 230.263 23.1452 1 6 6 -11 285.577 24.8858 3 -6 -6 -11 277.292 28.9748 4 6 -6 11 321.535 29.5521 2 6 -6 11 301.617 28.2813 1 -6 6 11 344.260 31.7555 2 6 6 11 279.019 30.4353 2 -6 6 -11 291.274 30.2503 4 -6 -6 11 286.593 28.9497 1 -6 -6 11 306.759 26.2309 2 -6 6 -11 289.787 28.4653 3 6 -6 -11 276.490 27.5140 1 7 -6 11 255.399 27.5685 1 -7 6 11 282.066 30.5681 2 7 6 -11 254.362 23.6397 3 7 -6 11 281.264 29.7700 2 -7 -6 -11 271.587 28.0495 4 7 6 11 291.209 30.5033 2 -7 6 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76.1122 3 0 7 11 1210.41 79.3497 2 0 -7 -11 1228.38 73.6915 1 0 -7 11 1157.16 78.1548 1 0 -7 -11 1290.50 73.8208 1 1 -7 11 737.567 47.6025 1 -1 7 11 732.683 50.6321 2 1 7 -11 686.935 45.4335 3 1 -7 -11 673.529 43.1915 1 -1 7 -11 623.089 45.4376 3 1 7 11 683.797 49.4098 2 -1 -7 11 669.278 47.9934 1 2 -7 11 515.484 38.3622 1 2 7 -11 570.149 37.2965 3 -2 7 11 501.280 41.1934 2 2 -7 11 499.605 33.9082 2 2 -7 11 510.644 34.2734 2 -2 7 -11 489.642 37.4186 3 2 7 11 566.638 43.5849 2 -2 -7 11 518.515 39.0662 1 2 -7 -11 519.891 35.3193 1 3 7 -11 189.995 19.1715 3 3 -7 11 173.347 17.4526 2 3 -7 11 165.547 19.7425 1 -3 7 11 166.935 22.0613 2 -3 7 -11 196.472 20.6399 3 3 7 11 201.885 25.5700 2 3 -7 -11 171.627 17.9926 1 -3 -7 11 161.090 20.0023 1 -4 7 11 273.659 27.2720 2 4 7 -11 171.923 17.5522 2 4 7 -11 194.364 20.7763 3 4 -7 11 223.862 22.5684 2 4 -7 11 194.736 21.9135 1 4 -7 -11 192.294 20.0704 1 -4 -7 11 208.510 22.6155 1 -4 7 -11 179.643 21.1292 3 -4 -7 11 171.645 18.1986 2 4 7 11 209.119 25.6498 2 -5 7 11 -1.6294 15.0193 2 5 -7 11 -1.4899 12.0920 1 5 7 -11 4.27581 10.4152 3 -5 -7 11 4.88053 10.3810 2 -5 7 -11 15.1768 13.0551 3 -5 -7 11 8.25939 12.1750 1 5 7 11 39.9719 19.0533 2 5 -7 -11 19.4206 11.5841 1 6 7 -11 162.525 18.8789 3 6 -7 11 200.301 22.8798 2 6 -7 11 160.213 22.7881 1 -6 -7 -11 163.780 22.7076 4 6 7 11 223.684 27.0866 2 -6 -7 11 188.014 20.8074 2 6 -7 -11 161.077 21.4922 1 -6 7 -11 173.775 21.8942 3 -6 7 -11 210.004 24.4441 4 -6 -7 11 245.250 26.0775 1 -7 7 11 86.8065 20.5519 2 7 -7 11 49.4120 16.3482 1 7 7 -11 58.0207 13.8344 3 7 -7 11 66.8751 18.8675 2 -7 -7 -11 37.1037 17.5772 4 7 -7 -11 74.0617 17.0913 1 7 7 11 69.6143 21.1943 2 -7 -7 11 51.9726 14.5055 2 -7 -7 11 70.1084 17.6824 1 -7 7 -11 61.3697 16.8531 3 -7 7 -11 44.4258 19.1625 4 8 -7 11 379.442 34.4301 1 8 7 -11 385.956 30.3076 3 -8 7 11 388.142 37.1969 2 8 -7 11 359.616 35.6858 2 8 7 -11 339.805 36.3453 1 8 -7 -11 401.094 34.7570 1 -8 -7 11 369.755 32.7268 2 -8 7 -11 367.933 36.3504 4 -8 7 -11 389.140 35.3658 3 8 7 11 384.819 38.6559 2 9 7 -11 304.351 32.4377 1 9 -7 11 269.597 30.6197 2 9 -7 11 292.688 30.3866 1 -9 7 11 275.539 32.6236 2 -9 7 -11 270.272 28.9840 3 -9 -7 11 231.767 26.9611 2 9 -7 -11 230.417 29.4224 1 9 7 11 244.740 33.0493 2 10 -7 11 234.555 29.3557 2 10 -7 11 208.326 27.8096 1 -10 7 11 163.918 29.5906 2 10 7 -11 179.488 28.9132 1 -10 -7 11 157.588 25.3867 2 10 -7 -11 163.946 27.2161 1 10 7 11 215.571 32.0963 2 11 -7 11 155.719 28.9115 2 11 7 -11 101.512 26.2170 1 -11 7 11 100.901 27.3235 2 11 -7 11 98.7649 24.1526 1 11 7 11 155.946 29.3965 2 11 -7 -11 102.117 25.0558 1 0 -8 11 818.754 52.8609 1 0 -8 -11 766.319 46.9064 1 0 8 -11 792.173 50.3145 3 0 8 11 717.508 53.6924 2 0 -8 -11 728.187 46.6429 1 1 8 -11 659.971 45.4303 3 -1 8 11 691.502 50.2067 2 1 -8 11 648.549 46.8134 1 1 -8 -11 662.607 42.9461 1 -1 -8 11 701.865 48.0784 1 -1 8 -11 692.896 45.6083 3 1 8 11 680.382 49.7945 2 2 -8 11 272.063 25.3128 1 -2 8 11 265.705 27.3563 2 2 8 -11 212.094 22.7540 3 2 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35.4433 1 11 -8 11 316.467 36.4665 2 -11 8 11 307.759 37.7268 2 11 8 -11 290.098 36.1172 1 11 8 11 243.991 38.5323 2 11 -8 -11 271.308 34.5091 1 0 9 -11 73.2397 14.7598 3 0 -9 -11 137.626 14.0696 1 0 9 11 107.708 20.2502 2 0 -9 11 120.644 17.6493 1 -1 -9 -11 94.6333 10.3737 1 -1 -9 -11 97.6673 10.4909 1 1 9 -11 110.650 16.0134 3 1 -9 11 90.4472 16.6521 1 -1 -9 11 130.624 18.9269 1 -1 9 -11 133.896 16.6536 3 1 9 11 154.320 21.6627 2 1 -9 -11 134.225 13.9454 1 2 -9 11 265.540 26.9825 1 -2 9 11 300.797 31.8951 2 2 9 -11 300.975 25.9006 3 -2 9 -11 278.707 26.4442 3 -2 -9 11 254.068 27.1272 1 2 -9 -11 298.853 23.8968 1 2 9 11 328.847 33.5021 2 3 9 -11 632.484 43.8743 3 3 -9 11 660.666 41.7903 2 3 -9 11 686.286 46.6885 1 -3 9 11 660.493 47.8278 2 -3 -9 11 628.026 46.7226 1 -3 9 -11 631.018 45.0310 3 3 9 11 582.074 51.1688 2 3 -9 -11 628.689 43.5509 1 4 9 -11 327.270 27.6107 3 4 -9 11 301.388 27.3921 2 4 -9 11 325.581 29.9030 1 -4 9 11 338.909 32.2253 2 -4 9 -11 303.044 28.9958 3 4 -9 -11 341.024 27.8931 1 4 9 11 308.523 33.7290 2 -4 -9 11 325.457 30.0940 1 5 9 -11 687.334 45.3492 3 5 -9 11 619.040 47.1279 1 5 -9 11 636.282 45.6672 2 -5 9 11 576.102 48.0877 2 -5 -9 11 661.790 41.8555 2 -5 -9 11 757.419 49.2267 1 5 -9 -11 611.704 46.0069 1 5 9 11 657.799 51.3599 2 -5 9 -11 660.788 46.7003 3 6 -9 11 93.9259 18.5634 2 -6 -9 -11 84.7160 17.8574 4 -6 9 11 128.261 22.5238 2 6 9 -11 102.439 16.7418 3 6 -9 11 112.248 19.5185 1 -6 -9 11 132.542 20.8882 1 6 9 11 124.948 25.5023 2 -6 -9 11 122.268 15.4287 2 6 -9 -11 138.369 19.4908 1 -6 9 -11 142.423 20.4254 3 -6 9 -11 103.804 21.1641 4 7 9 -11 176.800 22.0196 3 -7 -9 -11 182.695 24.0491 4 7 -9 11 309.040 28.3194 2 7 -9 11 206.996 26.1820 1 -7 9 11 171.530 26.2870 2 -7 -9 11 194.744 26.4096 1 -7 9 -11 226.459 24.9417 3 -7 9 -11 189.669 25.9448 4 7 -9 -11 191.905 24.4058 1 -7 -9 11 232.834 23.4347 2 7 9 11 204.375 29.6692 2 -8 9 11 86.5919 23.1506 2 8 -9 11 92.8425 21.1359 1 8 9 -11 110.450 17.3595 3 8 9 11 111.875 25.8579 2 -8 9 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31.4114 1 5 -7 -12 359.697 30.3653 1 6 7 -12 457.512 37.3505 3 6 -7 12 462.179 41.1601 2 -6 -7 -12 480.225 40.8949 4 6 -7 12 538.235 41.3656 1 -6 7 12 544.281 43.7693 2 -6 -7 12 585.896 43.0473 1 -6 7 -12 574.514 42.6774 4 -6 -7 12 539.400 37.7236 2 6 7 12 622.216 46.4809 2 -6 7 -12 601.618 41.5847 3 6 -7 -12 542.314 40.8472 1 7 -7 12 282.716 28.8402 1 -7 7 12 247.873 29.2757 2 7 -7 12 273.904 29.8880 2 7 7 -12 230.479 23.8355 3 -7 -7 -12 296.697 29.4676 4 7 7 12 251.958 31.2300 2 -7 7 -12 274.632 29.6177 4 -7 -7 12 232.719 28.6273 1 -7 7 -12 262.235 26.8740 3 7 -7 -12 232.864 26.1965 1 -7 -7 12 221.767 25.2130 2 8 -7 12 173.889 25.1647 2 8 7 -12 116.157 25.2934 1 8 7 -12 157.648 18.7397 3 -8 -7 -12 164.912 23.9843 4 -8 7 12 176.138 26.1360 2 8 -7 12 145.832 23.0226 1 8 7 12 130.970 26.4768 2 -8 -7 12 113.086 19.8751 2 -8 7 -12 154.758 25.9560 4 8 -7 -12 123.152 22.3011 1 -8 7 -12 118.269 22.2256 3 -9 7 12 -13.854 20.4048 2 9 -7 12 10.4490 16.7754 1 9 7 -12 23.5351 19.4580 1 9 -7 12 13.3133 20.1917 2 9 -7 -12 45.4329 19.0795 1 -9 7 -12 39.6629 18.5310 3 9 7 12 31.8684 22.0992 2 -9 -7 12 49.0154 17.5071 2 -10 7 12 10.9946 21.4078 2 10 -7 12 26.0257 17.9135 1 10 7 -12 12.5848 19.1049 1 10 -7 12 -8.3033 21.8164 2 10 7 12 10.9670 24.3992 2 10 -7 -12 6.99105 18.0454 1 -11 7 12 20.7873 23.9429 2 11 7 -12 46.8942 23.7799 1 11 -7 12 34.8785 24.8088 2 11 7 12 38.7639 27.5766 2 11 -7 -12 55.4858 22.2215 1 0 -8 -12 402.982 29.1866 1 0 8 12 427.111 37.9605 2 0 -8 12 448.034 35.4920 1 0 -8 -12 477.891 29.6269 1 -1 8 12 155.919 23.5646 2 1 8 -12 164.331 18.8864 3 1 -8 12 192.102 20.8143 1 -1 8 -12 151.719 19.2585 3 1 8 12 133.781 22.5634 2 -1 -8 12 173.787 21.3960 1 1 -8 -12 155.397 15.9250 1 2 -8 12 314.776 29.8234 1 -2 8 12 327.746 34.6879 2 2 8 -12 326.567 28.0705 3 -2 8 -12 281.131 28.1341 3 -2 -8 12 336.701 30.5238 1 2 8 12 346.958 34.2759 2 2 -8 -12 334.281 25.4319 1 3 -8 12 537.532 35.1803 2 3 8 -12 546.068 37.0348 3 3 -8 12 529.833 39.1648 1 -3 8 12 618.355 42.7215 2 3 8 12 467.805 45.3081 2 -3 -8 12 440.988 38.1525 1 -3 8 -12 478.454 38.3281 3 3 -8 -12 432.816 35.5084 1 4 8 -12 256.824 25.2871 3 -4 8 12 225.788 27.6393 2 4 -8 12 263.159 26.9781 1 4 -8 12 305.493 25.8447 2 -4 -8 12 303.462 28.3035 1 4 8 12 327.811 33.0540 2 -4 8 -12 278.354 28.0167 3 4 -8 -12 293.736 25.8617 1 5 8 -12 827.233 57.9177 3 5 -8 12 868.168 61.7203 1 5 -8 12 901.294 59.6471 2 -5 8 12 1067.83 64.3122 2 -5 8 -12 913.124 60.6393 3 5 -8 -12 930.760 60.7348 1 -5 -8 12 912.389 62.2842 1 5 8 12 958.032 65.1951 2 -5 -8 12 863.812 56.0389 2 6 -8 12 97.8808 19.9215 1 6 8 -12 105.788 16.4327 3 -6 8 12 101.280 21.8228 2 6 -8 12 111.739 20.0139 2 -6 -8 -12 122.803 20.4433 4 -6 -8 12 101.970 19.5245 1 -6 8 -12 132.667 20.2572 3 6 -8 -12 150.274 20.2757 1 -6 8 -12 121.343 22.0539 4 6 8 12 92.6304 24.0275 2 -6 -8 12 99.2452 15.0893 2 7 8 -12 276.599 27.1387 3 7 -8 12 390.320 32.9646 2 -7 8 12 367.760 35.5324 2 -7 -8 -12 278.976 31.5718 4 7 -8 12 283.761 30.5176 1 -7 8 -12 337.796 32.9887 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40.3639 18.0169 3 1 -19 12 320.154 35.4569 1 -1 19 12 299.291 36.6099 2 1 19 -12 306.442 33.1132 3 -1 -19 12 375.942 37.7567 1 -1 19 -12 293.922 33.4728 3 1 19 12 313.602 38.3214 2 -2 19 12 217.796 30.8355 2 2 -19 12 189.441 28.3365 1 2 19 -12 156.439 24.9794 3 -2 -19 12 177.742 29.2658 1 -2 19 -12 139.918 24.7266 3 2 19 12 150.359 28.8304 2 -3 19 12 168.240 28.7804 2 3 19 -12 207.083 27.5942 3 3 -19 12 155.012 29.0253 1 -3 19 -12 119.218 23.8361 3 3 19 12 157.044 29.7011 2 -3 -19 12 246.881 32.1725 1 -4 19 12 66.5261 24.9067 2 4 -19 12 80.5451 22.3378 1 4 19 -12 58.5601 21.9337 3 -4 19 -12 18.0937 18.5269 3 -4 -19 12 47.2025 21.1047 1 4 19 12 23.7500 23.1209 2 5 -19 12 23.0454 19.3057 1 5 19 -12 5.88353 18.6776 3 -5 19 12 45.2779 23.5473 2 -5 -19 12 32.6536 19.8434 1 -5 19 -12 44.9827 19.6864 3 5 19 12 27.8420 24.2073 2 -6 19 -12 49.7142 23.2675 3 6 19 12 94.7293 29.7746 2 6 -19 -12 57.3380 21.0284 1 0 -20 12 264.387 34.6075 1 0 20 -12 240.820 30.3335 3 0 20 12 300.608 36.1287 2 1 -20 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47.0392 2 4 -7 14 552.628 43.4502 1 4 7 -14 544.899 41.2473 3 4 -7 14 564.379 41.8848 2 -4 7 -14 668.802 44.9319 3 -4 -7 14 578.785 43.7840 1 -4 -7 14 580.023 37.9760 2 4 -7 -14 607.401 42.4946 1 5 -7 14 270.128 27.6463 1 5 -7 14 249.115 25.5285 2 5 7 -14 221.824 24.7091 3 -5 7 14 242.096 29.6445 2 -5 7 -14 270.525 27.6249 3 5 7 14 314.522 33.2199 2 -5 -7 14 203.780 21.7812 2 -5 -7 14 241.450 26.6752 1 5 -7 -14 243.421 25.7526 1 6 -7 14 531.240 41.8073 1 6 7 -14 474.714 38.4018 3 6 -7 14 489.054 40.9400 2 -6 7 14 520.608 44.5063 2 -6 7 -14 517.584 41.2440 3 6 7 14 548.143 46.9031 2 -6 -7 14 518.320 37.5915 2 -6 -7 14 538.659 42.0504 1 6 -7 -14 539.295 40.7453 1 7 -7 14 93.1996 21.5751 2 -7 -7 -14 83.5787 21.1564 4 7 -7 14 44.4127 17.6197 1 -7 7 14 105.904 23.5592 2 7 7 -14 83.3443 16.5786 3 7 7 14 80.6580 25.5668 2 -7 7 -14 60.0980 19.2772 3 -7 7 -14 115.230 23.3230 4 -7 -7 14 54.5435 18.6406 1 7 -7 -14 67.9450 17.8558 1 -8 -7 -14 273.481 32.1539 4 8 -7 14 249.616 29.4062 1 8 7 -14 298.158 27.6784 3 8 7 -14 293.962 33.9809 1 -8 7 14 328.715 35.3873 2 8 -7 14 287.277 32.1603 2 8 -7 -14 267.964 30.2269 1 8 7 14 272.769 35.6812 2 -8 7 -14 278.779 33.0140 4 -8 7 -14 321.886 32.8388 3 -9 7 14 22.9878 23.0384 2 9 7 -14 35.6075 21.8314 1 9 -7 14 -3.7248 16.2514 1 9 -7 14 0.76545 20.7485 2 -9 7 -14 2.59233 20.4153 4 9 7 14 15.9627 25.4912 2 9 -7 -14 5.55823 17.0416 1 -9 7 -14 30.1157 19.5954 3 10 -7 14 -9.2861 23.1213 2 10 7 -14 -24.145 20.0952 1 -10 7 14 11.6649 23.3270 2 10 7 14 -17.465 24.4067 2 10 -7 -14 -1.0146 17.5658 1 11 -7 14 46.0247 25.7018 2 0 8 14 75.3981 19.5690 2 0 -8 14 53.2843 15.6332 1 0 8 -14 66.8270 15.5435 3 0 -8 -14 65.1063 10.0925 1 -1 8 14 106.837 22.1274 2 1 -8 14 116.198 19.5542 1 1 8 -14 107.266 17.6164 3 1 -8 -14 106.823 13.7806 1 -1 8 -14 115.966 18.4207 3 1 8 14 147.211 22.0952 2 -1 -8 14 129.871 19.7181 1 -2 8 14 105.644 23.0992 2 2 -8 14 51.6056 13.1581 2 2 -8 14 58.2804 16.2183 1 2 8 -14 69.2542 15.3068 3 -2 8 -14 66.5829 16.6618 3 -2 -8 14 70.4295 17.0118 1 2 8 14 53.6374 20.6391 2 2 -8 -14 112.194 14.0655 1 3 8 -14 479.455 37.3102 3 -3 8 14 541.346 44.6852 2 3 -8 14 483.810 39.2440 1 3 -8 14 446.389 35.5247 2 3 8 14 544.617 45.6876 2 -3 -8 14 459.085 38.6465 1 3 -8 -14 525.236 36.5514 1 -3 8 -14 522.863 39.5958 3 4 8 -14 271.725 26.8852 3 -4 8 14 272.854 30.3232 2 4 -8 14 244.421 26.2331 2 4 -8 14 286.651 28.6598 1 4 8 14 272.674 33.8840 2 -4 -8 14 275.564 28.3231 1 4 -8 -14 301.965 26.3232 1 -4 8 -14 241.157 27.1353 3 5 8 -14 693.248 46.3173 3 5 -8 14 701.968 47.1843 2 -5 8 14 632.140 51.0411 2 5 -8 14 590.884 48.0826 1 -5 -8 14 578.883 48.1828 1 -5 8 -14 629.914 47.8987 3 5 8 14 727.452 54.7490 2 5 -8 -14 672.814 47.3098 1 6 -8 14 131.207 20.8688 2 6 8 -14 130.939 19.2051 3 6 -8 14 104.033 20.8632 1 -6 8 14 132.698 24.7057 2 6 -8 -14 120.601 20.3801 1 6 8 14 155.197 28.0688 2 -6 8 -14 97.1112 20.6428 3 -6 -8 14 134.545 21.4817 1 7 -8 14 295.235 32.0124 1 7 -8 14 343.414 33.8460 2 7 8 -14 299.418 29.3263 3 -7 -8 -14 283.403 32.4614 4 -7 8 14 346.146 35.6824 2 7 8 14 335.336 37.5851 2 -7 8 -14 312.782 33.7151 4 -7 8 -14 318.257 32.2407 3 -7 -8 14 287.328 32.7270 1 7 -8 -14 336.068 32.1338 1 8 8 -14 93.6387 17.6621 3 8 -8 14 76.0771 20.1279 1 -8 -8 -14 72.1158 21.6834 4 8 -8 14 118.934 23.1643 2 -8 8 14 76.0050 23.7411 2 8 8 -14 79.6567 22.9039 1 8 8 14 38.3664 25.4110 2 8 -8 -14 60.2744 19.7672 1 -8 8 -14 105.617 21.3480 3 -8 8 -14 29.4556 21.9596 4 9 -8 14 160.432 26.3004 2 -9 8 14 115.625 26.5803 2 9 -8 14 99.9431 22.8954 1 9 8 -14 91.6899 26.5193 1 9 -8 -14 133.996 25.0840 1 9 8 14 101.614 29.4019 2 -9 8 -14 73.6638 23.4872 3 -10 8 14 0.07717 24.6410 2 10 -8 14 22.4507 18.1159 1 10 -8 14 59.4948 26.0754 2 10 8 -14 34.8835 22.6600 1 10 8 14 20.8545 27.0975 2 10 -8 -14 44.1879 21.1795 1 11 -8 14 12.9289 27.1171 2 0 -9 -14 5.96989 8.01715 1 0 9 14 39.6154 18.5958 2 0 -9 14 0.39184 14.0442 1 0 9 -14 44.0627 14.5484 3 1 -9 14 643.422 48.7330 1 1 9 -14 661.308 47.1379 3 -1 9 14 630.964 51.2984 2 -1 -9 14 683.926 49.6193 1 1 9 14 669.387 50.6107 2 -1 9 -14 674.570 47.9980 3 1 -9 -14 710.658 44.1582 1 -2 9 14 159.238 27.3697 2 2 -9 14 196.114 23.5098 1 2 9 -14 192.310 22.1528 3 -2 -9 14 207.110 24.7691 1 -2 9 -14 180.605 22.7942 3 2 -9 -14 193.741 19.7750 1 2 9 14 201.730 27.3378 2 -3 9 14 381.840 36.2051 2 3 9 -14 274.138 28.1094 3 3 -9 14 295.982 25.8676 2 3 -9 14 333.087 31.4667 1 3 -9 -14 277.410 26.3036 1 -3 9 -14 276.735 29.8314 3 -3 -9 14 306.478 29.9533 1 3 9 14 348.047 36.1875 2 4 -9 14 219.911 23.8882 2 4 -9 14 255.801 27.3680 1 4 9 -14 211.293 23.3451 3 -4 9 14 191.083 27.8772 2 -4 9 -14 230.708 25.6294 3 4 9 14 224.708 32.7468 2 4 -9 -14 208.516 22.9788 1 -4 -9 14 194.617 25.3193 1 5 -9 14 54.2185 16.7190 2 -5 9 14 49.8103 21.4774 2 5 -9 14 72.1972 17.8576 1 5 9 -14 50.4996 15.6131 3 -5 -9 14 98.9072 19.2242 1 5 -9 -14 36.7368 15.2767 1 5 9 14 69.3037 25.6650 2 -5 9 -14 37.3461 17.0765 3 -6 -9 -14 49.0496 18.8870 4 6 9 -14 63.0544 16.2814 3 6 -9 14 57.1110 18.3573 1 -6 9 14 64.5597 21.7903 2 6 -9 14 71.4776 18.2831 2 6 9 14 58.0199 25.4307 2 -6 -9 14 49.6355 17.0862 1 -6 9 -14 80.0739 19.0770 3 6 -9 -14 89.8648 18.7017 1 -7 9 14 144.424 27.2321 2 7 -9 14 154.613 24.3609 2 7 -9 14 144.701 24.0675 1 7 9 -14 143.075 20.9000 3 -7 -9 -14 175.355 24.7214 4 -7 -9 14 115.187 23.3771 1 -7 9 -14 184.861 26.2475 4 7 9 14 141.971 29.3365 2 -7 9 -14 167.846 23.7916 3 7 -9 -14 153.581 23.0887 1 -8 -9 -14 81.4432 22.2335 4 8 -9 14 96.9826 21.4292 1 8 9 -14 109.551 19.7145 3 8 -9 14 49.0873 21.4423 2 -8 9 14 81.1744 24.3598 2 8 9 14 76.5472 27.8433 2 -8 9 -14 105.088 21.5064 3 -8 9 -14 72.2384 24.0414 4 8 -9 -14 64.8293 20.5351 1 -9 9 14 248.419 32.6155 2 9 9 -14 210.296 31.8120 1 9 -9 14 183.557 27.7144 1 9 -9 14 179.900 29.5251 2 9 -9 -14 124.671 26.3886 1 -9 9 -14 169.969 27.8259 3 9 9 14 172.153 33.5222 2 10 -9 14 19.0105 20.2590 1 10 -9 14 107.250 28.1698 2 10 9 -14 83.0317 27.3201 1 10 -9 -14 42.0316 21.5970 1 0 10 -14 447.412 36.3079 3 0 -10 14 479.044 38.5170 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20.6509 3 -1 4 25 69.1486 24.8464 2 -1 4 -25 52.5486 20.4683 3 1 -4 -25 59.3427 20.6410 3 1 4 25 33.5261 24.1411 2 -1 -4 25 61.8112 18.7477 1 -2 4 25 82.3182 24.8730 2 2 4 -25 71.6024 22.0576 3 2 -4 -25 68.4775 20.8846 3 -2 -4 25 100.220 21.3854 1 -2 4 -25 74.9429 22.5311 3 2 4 25 70.9822 25.8003 2 -3 4 25 117.147 26.1064 2 3 4 -25 146.581 24.9259 3 3 4 25 113.639 29.1617 2 3 -4 -25 100.530 22.6413 3 4 4 -25 143.960 26.6628 1 4 4 -25 93.8089 22.9399 3 -4 4 25 104.134 28.1062 2 4 4 25 174.528 32.0653 2 5 4 -25 187.927 30.2183 1 -5 4 25 178.883 33.4898 2 0 5 25 -3.6248 22.8986 2 0 5 -25 -10.564 17.6684 3 1 5 -25 4.38293 18.2085 3 -1 5 25 15.6336 22.7663 2 -1 5 -25 9.92280 18.6372 3 1 5 25 56.2873 24.3793 2 -1 -5 25 5.71194 15.4762 1 -2 5 25 70.5253 24.0627 2 2 5 -25 51.2927 20.9514 3 -2 -5 25 29.8205 17.8787 1 -2 5 -25 31.1352 21.3864 3 3 5 -25 121.862 25.0048 3 -3 5 25 148.261 28.7878 2 3 5 25 125.274 29.8790 2 -3 -5 25 116.347 23.5932 1 4 5 -25 168.879 27.4182 3 -4 5 25 193.933 32.9357 2 4 5 25 222.747 34.8995 2 0 -6 25 168.921 26.6244 1 0 6 -25 198.722 29.5361 3 0 6 25 211.134 31.8229 2 1 6 -25 90.5894 23.7305 3 -1 6 25 85.4588 25.6885 2 -1 6 -25 95.3129 24.2046 3 -1 -6 25 91.4789 20.4058 1 1 6 25 138.483 28.8929 2 2 6 -25 120.385 24.9206 3 -2 6 25 122.109 26.7412 2 -2 -6 25 118.906 22.8055 1 2 6 25 109.621 29.2418 2 -3 6 25 116.831 27.2879 2 3 6 -25 135.847 25.4629 3 -3 -6 25 108.394 23.1011 1 3 6 25 105.500 31.3109 2 4 6 -25 51.2044 21.6039 3 -4 6 25 49.9387 25.7132 2 -4 -6 25 60.2979 20.9393 1 0 -7 25 96.1938 22.7219 1 0 7 -25 145.415 27.1508 3 0 7 25 133.527 29.8846 2 -1 7 25 312.372 36.6903 2 1 7 -25 213.527 30.8986 3 -1 -7 25 285.214 31.4299 1 -2 7 25 110.722 28.1634 2 2 7 -25 71.1987 22.9370 3 2 7 25 146.735 30.0968 2 -2 -7 25 81.3046 21.6190 1 -3 7 25 44.6213 25.1035 2 3 7 -25 23.4244 21.6795 3 -3 -7 25 40.1112 20.0635 1 0 8 25 333.613 38.2258 2 0 -8 25 182.172 28.6315 1 -1 8 25 110.964 29.4872 2 -1 -8 25 116.439 24.1367 1 1 8 25 117.617 29.9537 2 -2 -8 25 150.037 25.4113 1 -3 -8 25 15.7450 19.0496 1 0 -9 25 41.8595 21.5287 1 1 -9 25 59.8266 22.3110 1 -1 -9 25 66.4504 22.3504 1 -2 -9 25 69.3566 22.6255 1 0 0 -26 370.363 38.9121 3 1 0 -26 52.5199 20.8781 3 -1 0 -26 28.4582 20.6064 3 2 0 -26 198.205 28.6186 3 3 0 -26 25.7056 20.7328 3 0 -1 -26 -22.056 18.9173 3 0 1 -26 31.8403 19.3261 3 -1 -1 -26 244.370 31.3947 3 1 1 -26 218.218 29.9192 3 -1 1 -26 182.693 29.0078 3 1 -1 -26 189.344 28.5019 3 2 1 -26 61.9252 21.8988 3 2 -1 -26 83.2435 23.4019 3 3 1 -26 107.626 23.2467 3 3 -1 -26 67.9682 22.4845 3 3 1 26 127.840 29.5850 2 4 1 26 68.3029 29.3443 2 0 2 26 3.08465 22.8544 2 0 2 -26 2.08497 18.4814 3 0 -2 -26 8.99637 19.0236 3 1 2 -26 18.2153 19.7075 3 -1 2 26 60.5723 23.9131 2 -1 -2 -26 26.8073 20.5990 3 1 2 26 49.6097 25.3805 2 -1 2 -26 56.6142 21.5234 3 1 -2 -26 44.4263 21.3120 3 2 2 -26 55.0069 21.3047 3 2 -2 -26 43.8838 21.1167 3 2 2 26 45.0358 25.4630 2 3 2 -26 219.841 29.2616 3 3 2 26 183.600 33.2572 2 3 -2 -26 263.463 31.0486 3 0 -3 -26 9.99558 18.7860 3 0 3 26 -13.467 22.3410 2 0 3 -26 6.63325 19.8058 3 -1 -3 -26 31.6532 20.9665 3 1 3 -26 51.0023 21.5931 3 -1 3 26 28.3845 22.8298 2 1 3 26 1.20620 22.9634 2 -1 3 -26 47.5261 21.7652 3 1 -3 -26 21.3014 19.8982 3 2 3 -26 84.7239 23.4043 3 -2 3 26 116.812 27.2789 2 2 3 26 78.5845 28.1815 2 2 -3 -26 95.6052 22.6156 3 -3 3 26 -29.318 21.9592 2 3 3 -26 24.8095 20.3752 3 3 3 26 54.2654 27.6847 2 0 -4 -26 381.142 39.7594 3 0 4 26 400.795 43.0132 2 0 4 -26 439.717 41.4183 3 -1 4 26 55.8371 24.4240 2 1 4 -26 35.5804 19.9495 3 1 -4 -26 4.25164 18.6895 3 1 4 26 31.0818 24.5052 2 2 4 -26 192.034 27.3313 3 -2 4 26 165.838 29.9384 2 2 4 26 151.031 30.8473 2 2 -4 -26 122.713 24.9972 3 -3 4 26 54.4681 26.1952 2 3 4 -26 54.7108 24.3744 1 3 4 -26 47.5021 21.4506 3 3 4 26 51.9271 28.7958 2 0 5 26 -8.9640 23.8226 2 -1 5 26 384.234 39.8954 2 1 5 -26 294.973 34.9546 3 1 5 26 318.528 39.7368 2 2 5 -26 11.8821 19.4903 3 -2 5 26 7.17482 22.4654 2 -2 -5 26 37.4081 19.6212 1 2 5 26 -7.5428 24.5873 2 0 6 26 234.079 34.2062 2 -1 6 26 37.2108 24.2333 2 1 6 26 -0.6790 24.0913 2 -2 6 26 82.7378 26.1080 2 -2 -6 26 75.2848 21.9049 1 -1 -7 26 -7.9638 17.5855 1 1 0 -27 73.2331 23.5293 3 1 -1 -27 69.8257 23.2866 3 1 -2 -27 14.0267 18.9830 3 0 3 27 4.23059 25.3768 2 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 3212 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group W W 0.70004(2) 0.60206(2) 0.32603(2) 0.01350(5) Uani 1 1 d . . . . Cl1 Cl 0.90376(13) 0.53103(7) 0.30932(7) 0.0200(3) Uani 1 1 d . . . . Cl2 Cl 0.56444(14) 0.70891(7) 0.35938(7) 0.0223(3) Uani 1 1 d . . . . N1 N 0.5960(4) 0.5305(2) 0.3629(2) 0.0150(9) Uani 1 1 d . . . . N2 N 0.6530(4) 0.6068(3) 0.2384(2) 0.0174(9) Uani 1 1 d . . . . N3 N 0.8501(4) 0.7067(2) 0.3056(2) 0.0169(9) Uani 1 1 d . . . . N4 N 0.7920(5) 0.6178(2) 0.4378(2) 0.0180(9) Uani 1 1 d . . . . C1 C 0.8060(7) 0.7635(3) 0.2647(3) 0.0239(11) Uani 1 1 d . . . . H1 H 0.721434 0.757886 0.241794 0.029 Uiso 1 1 d R . . . C2 C 0.8793(7) 0.8298(3) 0.2548(3) 0.0330(16) Uani 1 1 d . . . . H2 H 0.846163 0.868466 0.224851 0.040 Uiso 1 1 d R . . . C3 C 1.0016(7) 0.8390(4) 0.2890(3) 0.0354(16) Uani 1 1 d . . . . H3 H 1.051947 0.884846 0.284619 0.042 Uiso 1 1 d R . . . C4 C 1.0483(6) 0.7805(3) 0.3295(4) 0.0333(14) Uani 1 1 d . . . . H4 H 1.133098 0.784522 0.352477 0.040 Uiso 1 1 d R . . . C5 C 0.9703(6) 0.7155(3) 0.3363(3) 0.0253(13) Uani 1 1 d . . . . H5 H 1.004039 0.675132 0.364062 0.030 Uiso 1 1 d R . . . C6 C 0.8019(7) 0.6848(3) 0.4716(3) 0.0251(11) Uani 1 1 d . . . . H6 H 0.771179 0.729691 0.449154 0.030 Uiso 1 1 d R . . . C7 C 0.8543(6) 0.6908(3) 0.5367(3) 0.0304(14) Uani 1 1 d . . . . H7 H 0.858919 0.738947 0.558882 0.037 Uiso 1 1 d R . . . C8 C 0.9005(7) 0.6263(3) 0.5702(3) 0.0322(15) Uani 1 1 d . . . . H8 H 0.939740 0.629633 0.614919 0.039 Uiso 1 1 d R . . . C9 C 0.8887(7) 0.5575(3) 0.5375(3) 0.0276(14) Uani 1 1 d . . . . H9 H 0.917283 0.512093 0.559792 0.033 Uiso 1 1 d R . . . C10 C 0.8348(6) 0.5552(3) 0.4719(3) 0.0219(12) Uani 1 1 d . . . . H10 H 0.827347 0.507232 0.449620 0.026 Uiso 1 1 d R . . . C11 C 0.5101(5) 0.4739(3) 0.3868(3) 0.0158(10) Uani 1 1 d . . . . C12 C 0.5353(5) 0.3964(3) 0.3689(2) 0.0185(10) Uani 1 1 d . . . . C13 C 0.4499(6) 0.3410(3) 0.3954(3) 0.0273(14) Uani 1 1 d . . . . H13 H 0.466073 0.289172 0.384242 0.033 Uiso 1 1 d R . . . C14 C 0.3421(6) 0.3592(4) 0.4377(3) 0.0300(15) Uani 1 1 d . . . . H14 H 0.286707 0.320070 0.456500 0.036 Uiso 1 1 d R . . . C15 C 0.3148(7) 0.4349(3) 0.4527(3) 0.0287(14) Uani 1 1 d . . . . H15 H 0.237961 0.447373 0.480067 0.034 Uiso 1 1 d R . . . C16 C 0.3976(6) 0.4925(3) 0.4283(3) 0.0201(11) Uani 1 1 d . . . . C17 C 0.6522(5) 0.3748(3) 0.3217(3) 0.0195(10) Uani 1 1 d . . . . H17 H 0.686673 0.422214 0.299150 0.023 Uiso 1 1 d R . . . C18 C 0.6043(6) 0.3201(3) 0.2645(3) 0.0289(13) Uani 1 1 d . . . . H18A H 0.576235 0.271761 0.285285 0.048(12) Uiso 1 1 d GR . . . H18B H 0.678683 0.311033 0.231964 0.048(12) Uiso 1 1 d GR . . . H18C H 0.527382 0.342791 0.239885 0.048(12) Uiso 1 1 d GR . . . C19 C 0.7671(6) 0.3396(4) 0.3623(3) 0.0317(15) Uani 1 1 d . . . . H19A H 0.801109 0.376540 0.396130 0.044(11) Uiso 1 1 d GR . . . H19B H 0.840450 0.325280 0.330760 0.044(11) Uiso 1 1 d GR . . . H19C H 0.734230 0.294220 0.386560 0.044(11) Uiso 1 1 d GR . . . C20 C 0.3660(6) 0.5753(3) 0.4467(3) 0.0242(13) Uani 1 1 d D . . . H20 H 0.401388 0.607055 0.407791 0.029 Uiso 0.67 1 d R P A 1 H20A H 0.444178 0.607545 0.431621 0.029 Uiso 0.33 1 d R P B 2 C21A C 0.2159(8) 0.5919(5) 0.4518(5) 0.032(2) Uani 0.67 1 d D P C 1 H21A H 0.169015 0.569237 0.412129 0.050(17) Uiso 0.67 1 d GR P C 1 H21B H 0.201395 0.647036 0.451842 0.050(17) Uiso 0.67 1 d GR P C 1 H21C H 0.180034 0.570044 0.494660 0.050(17) Uiso 0.67 1 d GR P C 1 C22A C 0.4422(9) 0.6000(6) 0.5107(5) 0.034(2) Uani 0.67 1 d D P C 1 H22A H 0.397613 0.579114 0.551794 0.051 Uiso 0.67 1 d GR P C 1 H22B H 0.442886 0.655676 0.513396 0.051 Uiso 0.67 1 d GR P C 1 H22C H 0.535672 0.581168 0.508363 0.051 Uiso 0.67 1 d GR P C 1 C21B C 0.2415(16) 0.6034(14) 0.4112(10) 0.037(5) Uiso 0.33 1 d D P C 2 H21D H 0.255423 0.602440 0.361109 0.050(17) Uiso 0.33 1 d GR P C 2 H21E H 0.222546 0.655688 0.426080 0.050(17) Uiso 0.33 1 d GR P C 2 H21F H 0.164587 0.570671 0.423280 0.050(17) Uiso 0.33 1 d GR P C 2 C22B C 0.353(2) 0.5821(13) 0.5261(7) 0.042(5) Uiso 0.33 1 d D P C 2 H22D H 0.261781 0.565830 0.540273 0.063 Uiso 0.33 1 d GR P C 2 H22E H 0.366945 0.635182 0.539973 0.063 Uiso 0.33 1 d GR P C 2 H22F H 0.420722 0.549734 0.548393 0.063 Uiso 0.33 1 d GR P C 2 C23 C 0.6038(5) 0.6168(2) 0.1717(3) 0.0188(10) Uani 1 1 d . . . . C24 C 0.6953(7) 0.6326(3) 0.1171(2) 0.0175(10) Uani 1 1 d . . . . C25 C 0.6439(6) 0.6471(3) 0.0520(3) 0.0251(13) Uani 1 1 d . . . . H25 H 0.704074 0.657836 0.014958 0.030 Uiso 1 1 d R . . . C26 C 0.5032(7) 0.6459(3) 0.0403(3) 0.0280(14) Uani 1 1 d . . . . H26 H 0.468656 0.657226 -0.004398 0.034 Uiso 1 1 d R . . . C27 C 0.4154(6) 0.6286(3) 0.0933(3) 0.0267(13) Uani 1 1 d . . . . H27 H 0.320745 0.627153 0.084276 0.032 Uiso 1 1 d R . . . C28 C 0.4617(5) 0.6132(3) 0.1596(3) 0.0200(12) Uani 1 1 d . . . . C29 C 0.8477(6) 0.6281(3) 0.1287(3) 0.0215(12) Uani 1 1 d . . . . H29 H 0.863954 0.632500 0.179584 0.026 Uiso 1 1 d R . . . C30 C 0.9256(7) 0.6938(4) 0.0933(3) 0.0414(17) Uani 1 1 d . . . . H30A H 0.917983 0.688699 0.042994 0.045(12) Uiso 1 1 d GR . . . H30B H 1.021381 0.691731 0.106684 0.045(12) Uiso 1 1 d GR . . . H30C H 0.886840 0.742640 0.107733 0.045(12) Uiso 1 1 d GR . . . C31 C 0.8988(8) 0.5504(4) 0.1061(4) 0.048(2) Uani 1 1 d . . . . H31A H 0.845310 0.510664 0.128927 0.048(13) Uiso 1 1 d GR . . . H31B H 0.994399 0.544875 0.118904 0.048(13) Uiso 1 1 d GR . . . H31C H 0.889364 0.545463 0.055846 0.048(13) Uiso 1 1 d GR . . . C32 C 0.3680(6) 0.5879(4) 0.2174(3) 0.0292(15) Uani 1 1 d . . . . H32 H 0.404848 0.608919 0.261567 0.035 Uiso 1 1 d R . . . C33 C 0.3709(8) 0.5016(4) 0.2229(4) 0.0433(19) Uani 1 1 d . . . . H33A H 0.328236 0.479302 0.181878 0.065 Uiso 1 1 d GR . . . H33B H 0.321236 0.485612 0.264328 0.065 Uiso 1 1 d GR . . . H33C H 0.465106 0.484172 0.226088 0.065 Uiso 1 1 d GR . . . C34 C 0.2232(7) 0.6162(4) 0.2100(4) 0.052(2) Uani 1 1 d . . . . H34A H 0.223478 0.671424 0.202978 0.071(15) Uiso 1 1 d GR . . . H34B H 0.172237 0.604009 0.252082 0.071(15) Uiso 1 1 d GR . . . H34C H 0.180301 0.591347 0.170281 0.071(15) Uiso 1 1 d GR . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 W 0.01458(8) 0.01133(7) 0.01459(8) -0.00005(9) -0.00019(9) -0.00072(8) Cl1 0.0167(6) 0.0181(6) 0.0251(7) -0.0005(5) 0.0013(5) 0.0024(5) Cl2 0.0240(7) 0.0142(6) 0.0286(7) 0.0017(6) 0.0054(6) 0.0045(5) N1 0.013(2) 0.013(2) 0.019(2) -0.0027(18) 0.0026(17) 0.0037(17) N2 0.0135(19) 0.0134(19) 0.025(2) 0.001(2) 0.0037(16) 0.0014(18) N3 0.017(2) 0.013(2) 0.020(2) -0.0003(18) 0.0040(17) -0.0027(17) N4 0.022(2) 0.014(2) 0.0177(19) -0.0003(16) -0.001(2) -0.0030(19) C1 0.028(3) 0.017(2) 0.027(3) 0.006(2) 0.003(3) 0.003(3) C2 0.045(4) 0.017(3) 0.037(4) 0.007(3) 0.016(3) -0.002(3) C3 0.042(4) 0.023(3) 0.041(4) -0.002(3) 0.013(3) -0.013(3) C4 0.027(3) 0.034(3) 0.038(3) -0.006(3) 0.000(3) -0.012(2) C5 0.023(3) 0.026(3) 0.027(3) 0.000(3) 0.001(2) -0.005(2) C6 0.033(3) 0.015(2) 0.027(3) -0.001(2) -0.001(3) -0.003(3) C7 0.044(4) 0.019(3) 0.028(3) -0.010(3) -0.007(3) -0.005(3) C8 0.043(4) 0.032(3) 0.022(3) -0.001(3) -0.011(3) -0.003(3) C9 0.037(4) 0.021(3) 0.025(3) 0.003(3) -0.004(3) 0.000(3) C10 0.030(3) 0.014(2) 0.022(3) 0.001(2) 0.002(2) -0.003(2) C11 0.020(3) 0.014(2) 0.014(2) 0.002(2) 0.000(2) 0.000(2) C12 0.024(3) 0.015(2) 0.016(2) -0.002(3) 0.0012(19) -0.002(2) C13 0.036(4) 0.013(3) 0.033(3) 0.001(3) 0.009(3) 0.000(2) C14 0.031(4) 0.021(3) 0.038(4) 0.002(3) 0.016(3) -0.008(2) C15 0.027(3) 0.025(3) 0.034(3) 0.002(3) 0.017(3) -0.002(3) C16 0.025(3) 0.017(3) 0.018(3) -0.001(2) 0.001(2) 0.000(2) C17 0.023(2) 0.014(2) 0.022(3) 0.000(2) 0.001(2) -0.0013(18) C18 0.033(3) 0.024(3) 0.030(3) -0.004(3) 0.001(3) 0.002(3) C19 0.034(4) 0.033(3) 0.029(3) -0.003(3) 0.003(3) 0.003(3) C20 0.025(3) 0.018(3) 0.030(3) 0.003(3) 0.007(3) 0.001(2) C21A 0.021(5) 0.024(5) 0.053(6) 0.003(5) 0.000(4) 0.006(4) C22A 0.038(5) 0.016(4) 0.048(6) -0.005(5) -0.011(4) 0.008(5) C23 0.023(2) 0.013(2) 0.020(2) -0.004(2) -0.002(2) 0.0001(18) C24 0.025(3) 0.011(2) 0.017(2) -0.0035(19) 0.000(3) 0.001(2) C25 0.039(4) 0.014(2) 0.021(3) 0.001(2) -0.001(2) 0.000(2) C26 0.044(4) 0.019(3) 0.021(3) 0.002(2) -0.016(3) 0.005(3) C27 0.026(3) 0.022(3) 0.032(3) 0.000(3) -0.015(3) 0.002(2) C28 0.022(3) 0.011(2) 0.027(3) -0.001(2) -0.004(2) -0.001(2) C29 0.024(3) 0.022(3) 0.018(3) 0.000(2) 0.002(2) -0.001(2) C30 0.031(4) 0.052(4) 0.041(4) 0.015(4) 0.004(3) -0.009(3) C31 0.036(4) 0.035(4) 0.072(6) -0.021(4) -0.012(4) 0.013(3) C32 0.020(3) 0.035(4) 0.032(3) -0.003(3) -0.007(2) -0.003(3) C33 0.053(5) 0.029(4) 0.048(4) 0.013(3) -0.003(4) -0.012(3) C34 0.027(4) 0.048(5) 0.081(6) 0.008(4) 0.005(4) -0.004(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0.00 0.00 1.00 0.0060 0.00 0.00 -1.00 0.0060 0.00 -1.00 0.00 0.0450 0.00 1.00 0.00 0.0450 -1.00 1.00 0.00 0.0800 1.00 -1.00 0.00 0.0800 1.00 1.00 0.00 0.0850 -1.00 -1.00 0.00 0.0850 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle Cl1 W Cl2 156.46(5) Cl1 W N3 81.89(11) N1 W Cl1 99.84(13) N1 W Cl2 97.14(13) N1 W N3 165.72(17) N1 W N4 86.36(17) N2 W Cl1 96.66(14) N2 W Cl2 94.33(15) N2 W N1 105.6(2) N2 W N3 88.17(18) N2 W N4 167.98(18) N3 W Cl2 77.71(11) N4 W Cl1 82.07(12) N4 W Cl2 82.86(11) N4 W N3 79.82(14) C11 N1 W 175.5(4) C23 N2 W 173.0(4) C1 N3 W 117.8(4) C5 N3 W 124.4(4) C5 N3 C1 117.5(5) C6 N4 W 125.0(3) C6 N4 C10 116.8(4) C10 N4 W 118.2(3) N3 C1 C2 122.5(6) C1 C2 C3 119.1(6) C4 C3 C2 118.5(6) C3 C4 C5 119.1(6) N3 C5 C4 123.2(6) N4 C6 C7 122.8(5) C6 C7 C8 119.6(6) C9 C8 C7 118.7(6) C8 C9 C10 119.0(6) N4 C10 C9 123.2(5) N1 C11 C12 119.8(5) N1 C11 C16 120.3(5) C16 C11 C12 119.9(5) C11 C12 C17 121.1(5) C13 C12 C11 118.2(5) C13 C12 C17 120.6(5) C14 C13 C12 121.8(5) C13 C14 C15 119.7(6) C16 C15 C14 121.1(6) C11 C16 C20 121.0(5) C15 C16 C11 119.2(5) C15 C16 C20 119.8(5) C12 C17 C18 110.8(4) C19 C17 C12 111.0(5) C19 C17 C18 110.4(4) C16 C20 C22B 108.8(9) C21A C20 C16 113.4(6) C22A C20 C16 111.2(6) C22A C20 C21A 112.3(7) C21B C20 C16 112.0(11) C21B C20 C22B 111.2(12) N2 C23 C24 119.7(5) N2 C23 C28 119.4(5) C24 C23 C28 120.8(5) C23 C24 C29 120.6(5) C25 C24 C23 118.9(6) C25 C24 C29 120.4(5) C24 C25 C26 120.5(6) C27 C26 C25 120.2(5) C26 C27 C28 121.7(6) C23 C28 C32 119.4(5) C27 C28 C23 117.9(5) C27 C28 C32 122.5(5) C24 C29 C30 112.8(5) C31 C29 C24 109.3(5) C31 C29 C30 112.2(5) C28 C32 C33 109.4(5) C28 C32 C34 114.1(6) C34 C32 C33 110.5(6) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance W Cl1 2.3873(13) W Cl2 2.3938(13) W N1 1.772(4) W N2 1.759(4) W N3 2.393(4) W N4 2.361(4) N1 C11 1.387(6) N2 C23 1.390(7) N3 C1 1.346(6) N3 C5 1.335(7) N4 C6 1.350(6) N4 C10 1.351(6) C1 C2 1.384(8) C2 C3 1.386(10) C3 C4 1.372(9) C4 C5 1.383(7) C6 C7 1.365(8) C7 C8 1.383(8) C8 C9 1.368(8) C9 C10 1.376(8) C11 C12 1.428(8) C11 C16 1.408(7) C12 C13 1.385(8) C12 C17 1.518(7) C13 C14 1.379(8) C14 C15 1.388(8) C15 C16 1.384(8) C16 C20 1.530(8) C17 C18 1.539(8) C17 C19 1.512(8) C20 C21A 1.512(9) C20 C22A 1.511(10) C20 C21B 1.491(13) C20 C22B 1.545(14) C23 C24 1.416(8) C23 C28 1.423(7) C24 C25 1.380(7) C24 C29 1.522(9) C25 C26 1.407(9) C26 C27 1.377(9) C27 C28 1.388(7) C28 C32 1.517(8) C29 C30 1.547(8) C29 C31 1.520(8) C32 C33 1.521(9) C32 C34 1.519(8)