#------------------------------------------------------------------------------ #$Date: 2019-11-10 07:54:14 +0200 (Sun, 10 Nov 2019) $ #$Revision: 225918 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/58/4515807.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4515807 loop_ _publ_author_name 'Messinis, Antonis M.' 'Batsanov, Andrei S.' 'Wright, William R. H.' 'Howard, Judith A. K.' 'Hanton, Martin J.' 'Dyer, Philip W.' _publ_section_title ; Bis(Imido) Tungsten Complexes: Efficient Precatalysts for the Homogeneous Dimerization of Ethylene ; _journal_issue 12 _journal_name_full 'ACS Catalysis' _journal_page_first 11249 _journal_paper_doi 10.1021/acscatal.8b02202 _journal_volume 8 _journal_year 2018 _chemical_formula_moiety 'C19 H34 Cl2 N2 O2 W' _chemical_formula_sum 'C19 H34 Cl2 N2 O2 W' _chemical_formula_weight 577.23 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary heavy _atom_sites_solution_secondary difmap _audit_creation_date 2017-11-08 _audit_creation_method ; Olex2 1.2-beta (compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381) ; _cell_angle_alpha 90 _cell_angle_beta 109.016(8) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 13.4052(6) _cell_length_b 9.8029(6) _cell_length_c 18.7197(9) _cell_measurement_reflns_used 9822 _cell_measurement_temperature 120(2) _cell_measurement_theta_max 34.03 _cell_measurement_theta_min 2.38 _cell_volume 2325.7(2) _computing_cell_refinement 'SAINT v7.46A (Bruker, 2008)' _computing_data_collection 'SMART v5.625 (Bruker, 2001)' _computing_data_reduction 'SAINT v7.46A (Bruker, 2008)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'SHELXS (Sheldrick, 2008)' _diffrn_ambient_temperature 120 _diffrn_detector_area_resol_mean 5.6 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 1.000 _diffrn_measurement_device_type 'Bruker SMART 6000 CCD area detector' _diffrn_measurement_method '\w scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0345 _diffrn_reflns_av_unetI/netI 0.0229 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 1.000 _diffrn_reflns_limit_h_max 18 _diffrn_reflns_limit_h_min -18 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 42406 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 1.000 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 29.997 _diffrn_reflns_theta_min 2.302 _diffrn_source 'fine-focus sealed tube' _diffrn_source_current 35.0 _diffrn_source_power 0.3 _diffrn_source_target Mo _diffrn_source_voltage 50.0 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 5.211 _exptl_absorpt_correction_T_max 0.4370 _exptl_absorpt_correction_T_min 0.2945 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2008/1 (Bruker,2008) was used for absorption correction. wR2(int) was 0.1048 before and 0.0515 after correction. The Ratio of minimum to maximum transmission is 0.6739. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour amber _exptl_crystal_density_diffrn 1.649 _exptl_crystal_density_method 'not measured' _exptl_crystal_description irregular _exptl_crystal_F_000 1144 _exptl_crystal_size_max 0.33 _exptl_crystal_size_mid 0.2 _exptl_crystal_size_min 0.15 _refine_diff_density_max 3.532 _refine_diff_density_min -1.106 _refine_diff_density_rms 0.121 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.092 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 251 _refine_ls_number_reflns 6782 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.092 _refine_ls_R_factor_all 0.0301 _refine_ls_R_factor_gt 0.0250 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0187P)^2^+5.5994P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0550 _refine_ls_wR_factor_ref 0.0574 _reflns_Friedel_coverage 0.000 _reflns_number_gt 5929 _reflns_number_total 6782 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file W-bisimido.cif _cod_data_source_block 11_11srv152 _cod_depositor_comments ; The following automatic conversions were performed: data item '_diffrn_source_target' value 'MO' was changed to 'Mo' in accordance with the /home/data/users/saulius/crontab/automatic-downloads/current/ACS/lib/dictionaries/cif_core.dic dictionary named 'cif_core.dic' version 2.4.2 last updated on 2011-04-26. Automatic conversion script Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas ; _cod_database_code 4515807 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.509 _shelx_estimated_absorpt_t_min 0.278 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2. Others Uiso(H1A)=Uiso(H1B)=Uiso(H1C)=FVAR(1) Uiso(H4A)=Uiso(H4B)=Uiso(H4C)=FVAR(2) Uiso(H6A)=Uiso(H6B)=Uiso(H6C)=FVAR(3) Uiso(H7A)=Uiso(H7B)=Uiso(H7C)=FVAR(4) Uiso(H16A)=Uiso(H16B)=Uiso(H16C)=FVAR(5) Uiso(H15A)=Uiso(H15B)=Uiso(H15C)=FVAR(6) Uiso(H18A)=Uiso(H18B)=Uiso(H18C)=FVAR(7) Uiso(H19A)=Uiso(H19B)=Uiso(H19C)=FVAR(8) 3.a Riding coordinates: C2(H2A,H2B), C3(H3A,H3B), C5(H5), C10(H10), C11(H11), C12(H12), C14(H14), C17(H17) 3.b Rotating group: C1(H1A,H1B,H1C), C4(H4A,H4B,H4C), C6(H6A,H6B,H6C), C7(H7A,H7B,H7C), C15(H15A, H15B,H15C), C16(H16A,H16B,H16C), C18(H18A,H18B,H18C), C19(H19A,H19B,H19C) ; _shelx_res_file ; TITL 11srv152 in P21/n #14 11srv152.res created by SHELXL-2016/6 at 16:26:35 on 08-Nov-2017 REM reset to P21/n #14 CELL 0.71073 13.4052 9.8029 18.7197 90 109.016 90 ZERR 4 0.0006 0.0006 0.0009 0 0.008 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl N O W UNIT 76 136 8 8 8 4 L.S. 7 PLAN 6 SIZE 0.15 0.2 0.33 TEMP -153 BOND fmap 2 acta OMIT -3 60 OMIT -1 0 1 OMIT 1 0 1 REM REM REM WGHT 0.018700 5.599400 FVAR 0.25521 0.04123 0.03250 0.04892 0.04171 0.03157 0.03239 FVAR 0.03434 0.04970 W1 6 0.035884 0.452038 0.224769 11.00000 0.01411 0.01479 = 0.01551 0.00104 0.00425 -0.00024 CL1 3 0.043130 0.248157 0.156275 11.00000 0.02254 0.01861 = 0.03195 -0.00660 0.00338 0.00182 CL2 3 0.098862 0.657313 0.293339 11.00000 0.02490 0.02080 = 0.02350 -0.00609 0.00532 -0.00211 O1 5 0.206872 0.386558 0.288549 11.00000 0.01731 0.02539 = 0.01945 0.00251 0.00197 0.00114 O2 5 0.152099 0.527307 0.158271 11.00000 0.01741 0.02711 = 0.01927 0.00167 0.00814 0.00160 N1 4 -0.014203 0.380129 0.290907 11.00000 0.02248 0.02131 = 0.02185 0.00306 0.00857 -0.00051 N2 4 -0.073920 0.521508 0.154875 11.00000 0.01603 0.01621 = 0.01699 0.00000 0.00393 0.00086 C1 1 0.237177 0.362192 0.368519 11.00000 0.03019 0.04812 = 0.02051 0.00877 0.00027 0.00405 AFIX 7 H1A 2 0.243438 0.449462 0.395159 11.00000 21.00000 H1B 2 0.305206 0.314731 0.385459 11.00000 21.00000 H1C 2 0.183536 0.305793 0.379439 11.00000 21.00000 AFIX 0 C2 1 0.288125 0.457588 0.269068 11.00000 0.01538 0.03316 = 0.02910 -0.00092 0.00437 -0.00039 AFIX 3 H2A 2 0.356125 0.408658 0.289448 11.00000 -1.20000 H2B 2 0.296995 0.550908 0.290438 11.00000 -1.20000 AFIX 0 C3 1 0.254715 0.463478 0.184557 11.00000 0.01607 0.03849 = 0.02975 0.00485 0.00972 0.00459 AFIX 3 H3A 2 0.306085 0.517228 0.168347 11.00000 -1.20000 H3B 2 0.251035 0.370328 0.163407 11.00000 -1.20000 AFIX 0 C4 1 0.111889 0.527613 0.076903 11.00000 0.02987 0.03455 = 0.01685 0.00199 0.00994 0.00531 AFIX 7 H4A 2 0.103048 0.433443 0.058333 11.00000 31.00000 H4B 2 0.161689 0.575223 0.057173 11.00000 31.00000 H4C 2 0.043579 0.574423 0.059853 11.00000 31.00000 AFIX 0 C5 1 -0.092484 0.347441 0.326101 11.00000 0.02314 0.02806 = 0.02314 0.00702 0.01041 0.00179 AFIX 3 H5 2 -0.160734 0.391051 0.296151 11.00000 -1.20000 AFIX 0 C6 1 -0.108626 0.194189 0.325600 11.00000 0.04915 0.03383 = 0.04327 0.00612 0.02197 -0.01107 AFIX 7 H6A 2 -0.131956 0.161009 0.273370 11.00000 41.00000 H6B 2 -0.162296 0.172759 0.349050 11.00000 41.00000 H6C 2 -0.042006 0.149819 0.354060 11.00000 41.00000 AFIX 0 C7 1 -0.057600 0.407035 0.405889 11.00000 0.03405 0.04623 = 0.03100 0.00333 0.01604 0.00187 AFIX 7 H7A 2 0.008000 0.362924 0.436509 11.00000 51.00000 H7B 2 -0.112630 0.391065 0.428848 11.00000 51.00000 H7C 2 -0.045779 0.505335 0.403469 11.00000 51.00000 AFIX 0 C8 1 -0.165681 0.560738 0.098739 11.00000 0.01415 0.01985 = 0.01473 0.00044 0.00609 0.00373 C9 1 -0.169890 0.692885 0.067208 11.00000 0.02008 0.02147 = 0.01768 0.00220 0.00922 0.00508 C10 1 -0.257384 0.727676 0.005802 11.00000 0.02377 0.02711 = 0.02142 0.00584 0.00893 0.00920 AFIX 3 H10 2 -0.260874 0.815076 -0.016798 11.00000 -1.20000 AFIX 0 C11 1 -0.340498 0.635074 -0.023075 11.00000 0.01970 0.03762 = 0.01948 0.00352 0.00418 0.00798 AFIX 3 H11 2 -0.399198 0.658954 -0.065755 11.00000 -1.20000 AFIX 0 C12 1 -0.336835 0.508630 0.010767 11.00000 0.01824 0.03167 = 0.02048 -0.00249 0.00459 0.00112 AFIX 3 H12 2 -0.394465 0.447660 -0.008463 11.00000 -1.20000 AFIX 0 C13 1 -0.250806 0.468408 0.072302 11.00000 0.01596 0.02288 = 0.01613 -0.00308 0.00596 0.00142 C14 1 -0.083008 0.795348 0.103174 11.00000 0.02266 0.01702 = 0.02416 0.00324 0.01056 0.00128 AFIX 3 H14 2 -0.016268 0.742918 0.126364 11.00000 -1.20000 AFIX 0 C15 1 -0.108342 0.870209 0.167238 11.00000 0.02923 0.02596 = 0.02747 -0.00215 0.01338 0.00167 AFIX 7 H15A 2 -0.176602 0.916439 0.146879 11.00000 71.00000 H15B 2 -0.053172 0.937710 0.189908 11.00000 71.00000 H15C 2 -0.111432 0.804269 0.205799 11.00000 71.00000 AFIX 0 C16 1 -0.063222 0.896556 0.047033 11.00000 0.03808 0.02268 = 0.03140 0.00545 0.01765 -0.00121 AFIX 7 H16A 2 -0.048391 0.846406 0.006343 11.00000 61.00000 H16B 2 -0.002693 0.954397 0.073133 11.00000 61.00000 H16C 2 -0.125902 0.953655 0.025662 11.00000 61.00000 AFIX 0 C17 1 -0.250035 0.330450 0.108744 11.00000 0.01925 0.02216 = 0.02043 -0.00147 0.00573 -0.00346 AFIX 3 H17 2 -0.184415 0.324590 0.153564 11.00000 -1.20000 AFIX 0 C18 1 -0.246529 0.214898 0.054607 11.00000 0.03668 0.02475 = 0.03174 -0.00509 0.01146 -0.00043 AFIX 7 H18A 2 -0.309877 0.218591 0.009866 11.00000 81.00000 H18B 2 -0.243742 0.126958 0.080076 11.00000 81.00000 H18C 2 -0.183707 0.225175 0.039209 11.00000 81.00000 AFIX 0 C19 1 -0.344259 0.312352 0.136836 11.00000 0.03126 0.03703 = 0.03946 0.00482 0.01912 -0.00363 AFIX 7 H19A 2 -0.344758 0.386112 0.172046 11.00000 91.00000 H19B 2 -0.338680 0.224352 0.162685 11.00000 91.00000 H19C 2 -0.409759 0.314994 0.093766 11.00000 91.00000 AFIX 0 HKLF 4 REM 11srv152 in P21/n #14 REM R1 = 0.0250 for 5929 Fo > 4sig(Fo) and 0.0301 for all 6782 data REM 251 parameters refined using 0 restraints END WGHT 0.0184 5.6139 REM Highest difference peak 3.532, deepest hole -1.106, 1-sigma level 0.121 Q1 1 0.0382 0.6428 0.2263 11.00000 0.05 3.53 Q2 1 -0.1095 0.4539 0.3279 11.00000 0.05 3.49 Q3 1 -0.3256 0.1566 0.2452 11.00000 0.05 0.98 Q4 1 -0.1174 0.2512 0.3950 11.00000 0.05 0.96 Q5 1 -0.0276 0.6589 0.1583 11.00000 0.05 0.95 Q6 1 0.0258 0.2491 0.2930 11.00000 0.05 0.94 ; _shelx_res_checksum 77793 _shelx_hkl_file ; -1 0 0 -3.2063 0.2167 1 -1 0 0 -3.4489 0.3057 5 1 0 0 -0.6427 0.5156 5 1 0 0 -1.1143 0.6175 4 -1 0 0 -2.7905 0.4177 2 -1 0 0 -3.3377 0.3112 3 1 0 0 -1.4415 0.4583 3 1 0 0 -1.1987 0.3519 1 -1 0 0 -3.3779 0.2341 4 1 0 0 -1.5609 0.6077 2 2 0 0 2215.16 82.04 2 -2 0 0 2361.24 83.34 5 -2 0 0 2282.66 81.98 2 2 0 0 2389.37 93.29 4 2 0 0 2332.60 84.13 1 -2 0 0 2369.12 83.77 3 2 0 0 2272.99 83.57 3 2 0 0 2351.85 83.15 5 -2 0 0 2350.19 85.61 1 3 0 0 1.36251 0.76666 1 3 0 0 -0.5564 1.2652 4 -3 0 0 1.22809 1.02941 3 3 0 0 0.05765 1.48822 2 -3 0 0 5.22100 1.47894 5 -3 0 0 -0.3948 0.6384 1 4 0 0 1234.48 51.54 4 4 0 0 1277.71 45.07 1 -4 0 0 1256.93 46.05 5 -4 0 0 1227.76 46.13 3 -4 0 0 1238.82 45.02 1 4 0 0 1196.06 45.99 2 -5 0 0 0.54306 1.03721 1 -5 0 0 -1.3122 1.6716 5 5 0 0 -2.3091 1.9531 4 -5 0 0 -0.4027 1.6420 3 5 0 0 0.58420 2.15311 2 -6 0 0 54.6963 3.4889 1 -6 0 0 57.7135 5.1504 5 -6 0 0 62.7919 5.0321 3 6 0 0 61.5176 5.7004 2 -7 0 0 0.72205 2.07366 5 -7 0 0 -1.8552 2.1584 3 7 0 0 -1.2542 2.5679 2 -7 0 0 -1.7218 1.1782 1 -8 0 0 76.8609 4.5980 1 -8 0 0 85.3621 7.1528 5 8 0 0 65.9137 6.9359 2 -8 0 0 84.9752 6.7575 3 -9 0 0 2.29145 2.82635 5 -9 0 0 0.69805 2.68049 3 9 0 0 -0.0113 3.0123 2 10 0 0 1219.71 44.81 1 -10 0 0 1155.26 48.32 5 10 0 0 1274.47 49.05 2 -10 0 0 1154.97 48.47 3 11 0 0 0.70092 2.01172 1 -11 0 0 2.69830 3.63271 5 11 0 0 -1.3114 3.4873 2 -11 0 0 -2.8870 2.9343 3 12 0 0 544.046 26.684 2 -12 0 0 526.225 26.419 3 -12 0 0 564.156 26.892 5 -13 0 0 -0.4751 4.0531 3 13 0 0 4.27435 4.55234 2 -13 0 0 0.18765 4.11956 5 14 0 0 1592.93 63.26 2 -14 0 0 1515.28 64.07 5 -14 0 0 1570.38 64.90 3 -15 0 0 2.06775 4.65660 3 -15 0 0 -2.0461 4.5845 5 15 0 0 -3.4302 5.2980 2 -16 0 0 739.088 36.424 5 -16 0 0 732.226 36.820 3 16 0 0 737.855 35.600 2 17 0 0 -1.2352 6.7597 2 -17 0 0 0.10820 5.94370 5 17 0 0 0.97921 5.39683 3 18 0 0 146.325 15.457 3 18 0 0 132.458 14.527 2 -18 0 0 132.474 14.394 5 -19 0 0 1.35013 7.57957 5 19 0 0 2.84780 7.79992 3 0 -1 0 -1.5322 0.4198 3 0 -1 0 -1.3116 0.5322 5 0 -1 0 -1.8502 0.5220 2 0 -1 0 -2.1378 0.4844 1 0 1 0 -1.6542 0.5268 2 0 1 0 -2.1731 0.4967 1 0 1 0 -0.3504 0.4390 3 0 1 0 -3.0659 0.3023 5 1 -1 0 7874.59 284.96 5 -1 -1 0 7836.59 285.11 1 -1 -1 0 7703.10 285.52 5 1 -1 0 7858.73 282.29 5 1 -1 0 7630.78 282.35 3 1 -1 0 7757.43 286.79 1 1 -1 0 7111.39 272.48 2 -1 -1 0 7593.06 275.04 2 -1 1 0 7448.39 277.48 2 1 1 0 7835.38 284.18 1 1 1 0 7559.65 277.53 2 1 1 0 7576.83 286.67 5 -1 1 0 7453.27 283.87 3 -1 1 0 7737.82 288.50 1 -2 -1 0 115.336 4.511 1 -2 -1 0 109.799 5.208 3 -2 -1 0 102.432 5.166 5 2 -1 0 108.218 5.038 1 2 -1 0 106.512 5.013 3 2 -1 0 110.720 5.118 5 -2 1 0 110.475 5.039 1 -2 1 0 110.427 5.066 3 2 1 0 112.379 4.432 1 -2 1 0 113.393 5.290 2 -2 1 0 111.042 5.182 5 2 1 0 109.982 5.255 2 -3 -1 0 2633.79 96.27 1 -3 -1 0 2540.88 93.16 5 -3 -1 0 2571.55 93.86 3 -3 1 0 2559.70 93.34 5 -3 1 0 2648.95 91.71 2 -3 1 0 2625.23 93.72 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534.710 23.913 5 4 -7 0 538.697 22.468 5 4 7 0 518.380 22.555 3 4 7 0 541.916 23.984 2 -4 7 0 499.256 21.166 3 -4 7 0 531.000 23.737 2 -5 -7 0 221.526 11.411 1 5 -7 0 212.046 12.901 1 -5 -7 0 261.943 13.936 5 5 -7 0 245.021 12.089 5 -5 7 0 253.207 13.512 2 -5 7 0 200.481 10.702 3 5 7 0 223.147 13.357 2 5 7 0 242.452 12.579 3 -6 -7 0 830.865 32.885 1 6 -7 0 848.722 33.576 5 -6 -7 0 911.129 36.083 5 6 -7 0 842.345 35.533 1 -6 7 0 820.867 34.982 2 6 7 0 812.337 34.624 3 6 7 0 815.251 34.970 2 -6 7 0 795.136 32.919 3 7 -7 0 24.4048 4.4875 5 -7 -7 0 23.8480 3.5374 1 -7 -7 0 35.6034 5.7673 5 7 -7 0 29.1591 4.9942 1 7 7 0 31.3167 5.2520 2 -7 7 0 31.7722 4.3373 3 -7 7 0 27.2773 5.1359 2 7 7 0 26.3122 4.7764 3 8 -7 0 1141.96 43.32 5 -8 -7 0 1098.54 45.45 5 8 -7 0 1071.10 44.96 1 8 7 0 1026.39 44.53 3 -8 7 0 1067.94 43.05 3 -8 7 0 1065.38 44.84 2 8 7 0 1097.26 44.63 2 9 -7 0 249.621 14.753 1 9 -7 0 210.790 12.972 5 -9 -7 0 265.310 15.948 5 9 7 0 217.898 14.232 2 -9 7 0 267.712 15.996 2 9 7 0 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2 -2 229.361 13.978 2 12 -2 -2 886.423 37.331 2 -12 -2 2 860.346 37.701 5 12 2 -2 869.974 35.728 2 -12 2 2 808.061 34.069 1 -12 2 2 868.341 37.997 5 -12 2 2 819.227 36.790 3 12 2 -2 772.996 36.580 3 -11 -2 2 95.3239 9.0174 5 11 -2 -2 90.5553 8.8265 2 -11 2 2 93.9699 9.1678 5 11 2 -2 96.8422 8.2432 2 -11 2 2 73.9037 6.4841 1 11 2 -2 82.9513 8.0888 3 -11 2 2 81.9069 8.0656 3 10 -2 -2 898.430 37.550 2 -10 -2 2 892.016 37.812 5 -10 -2 2 834.147 33.016 1 -10 2 2 903.230 38.308 5 10 2 -2 845.400 37.400 3 -10 2 2 926.122 37.388 3 10 2 -2 923.574 36.299 2 -10 2 2 923.531 35.603 1 9 -2 -2 566.135 24.829 2 -9 -2 2 549.904 25.440 4 -9 -2 2 495.251 20.770 1 -9 -2 2 555.968 24.929 5 -9 2 2 526.565 25.129 5 9 2 -2 564.749 24.787 3 -9 2 2 536.908 24.115 3 -9 2 2 548.917 22.937 1 9 2 -2 584.200 23.763 2 -8 -2 2 216.535 11.845 5 -8 -2 2 187.122 8.654 1 -8 -2 2 203.034 11.128 4 -8 2 2 201.704 11.073 3 8 2 -2 202.937 11.408 3 -8 2 2 186.628 11.376 2 8 2 -2 181.647 10.405 2 -8 2 2 212.816 12.274 5 -8 2 2 193.405 10.219 1 -7 -2 2 780.021 33.224 4 -7 -2 2 781.296 31.557 5 -7 -2 2 747.034 28.924 1 -7 2 2 768.220 30.830 2 -7 2 2 753.474 31.790 5 7 2 -2 790.988 30.144 2 7 2 -2 773.585 31.550 3 -7 2 2 761.361 30.848 3 -7 2 2 763.099 30.321 1 -6 -2 2 34.9044 3.0582 1 -6 -2 2 31.5854 3.5352 4 -6 -2 2 38.7481 4.1551 5 -6 2 2 39.8412 4.4886 5 -6 2 2 35.0256 3.5149 1 6 2 -2 28.1561 3.8604 3 -6 2 2 36.2474 3.6966 3 6 2 -2 36.3835 3.8046 2 -6 2 2 41.5882 4.1235 2 -5 -2 2 824.993 32.898 5 -5 -2 2 865.488 31.801 1 5 2 -2 840.681 33.165 3 -5 2 2 835.959 33.044 5 -5 2 2 862.761 32.551 1 -5 2 2 873.427 31.954 2 5 2 -2 809.181 31.509 2 -5 2 2 834.701 32.354 3 -4 -2 2 1931.03 70.03 1 -4 -2 2 1886.09 70.50 5 -4 2 2 1916.63 70.54 5 -4 2 2 1926.85 70.26 3 4 2 -2 1934.30 68.56 2 -4 2 2 1948.90 70.72 1 -4 2 2 1936.90 68.67 2 4 2 -2 1956.79 71.14 3 -3 -2 2 548.347 21.817 5 -3 -2 2 570.426 21.329 1 -3 2 2 565.607 21.057 2 3 2 -2 573.250 22.134 3 -3 2 2 550.801 21.165 3 -3 2 2 532.218 21.790 1 3 2 -2 577.095 21.021 2 2 -2 -2 445.604 16.923 5 2 -2 -2 427.852 15.982 3 -2 -2 2 425.555 16.693 5 -2 -2 2 406.371 16.527 1 -2 2 2 455.763 16.177 3 2 2 -2 416.805 16.850 3 -2 2 2 426.104 16.236 2 -2 2 2 423.143 16.961 1 2 2 -2 427.485 16.179 2 -1 -2 2 108.579 4.943 5 1 -2 -2 102.006 5.180 5 -1 -2 2 103.168 5.211 1 -1 2 2 103.050 5.072 2 1 2 -2 111.425 5.083 2 -1 2 2 107.469 5.368 1 1 2 -2 110.278 5.253 3 0 -2 -2 2627.89 96.44 5 0 -2 -2 2701.00 98.92 3 0 -2 2 2716.63 96.32 5 0 -2 2 2638.16 97.22 1 0 2 -2 2751.47 96.11 5 0 2 -2 2762.92 97.09 3 0 2 2 2710.28 94.68 2 0 2 2 2721.63 98.48 3 0 2 -2 2734.04 94.60 2 0 2 2 2632.95 97.04 1 -1 -2 -2 18.9969 1.7056 3 -1 -2 -2 19.9444 2.0896 5 1 -2 2 18.9458 1.3741 5 1 -2 2 13.9341 1.9819 1 -1 -2 -2 19.0963 1.7903 1 -1 2 -2 16.3183 1.7540 3 -1 2 -2 19.1401 1.4797 5 -1 2 -2 20.8532 2.1800 2 1 2 2 11.8461 1.9245 2 1 2 2 19.5390 1.6958 3 1 2 2 21.9313 1.9186 1 -2 -2 -2 1094.54 40.54 5 2 -2 2 1155.06 39.73 5 2 -2 2 1055.47 39.56 5 -2 -2 -2 1102.71 39.90 1 2 -2 2 1132.73 40.79 1 -2 -2 -2 1080.54 40.42 3 -2 2 -2 1054.78 40.42 3 2 2 2 1099.04 39.84 1 2 2 2 1082.30 40.17 2 -2 2 -2 1088.04 40.13 2 -3 -2 -2 38.5299 3.4246 5 -3 -2 -2 36.4576 3.3775 3 3 -2 2 39.0688 3.3441 1 -3 -2 -2 38.0317 2.2367 1 3 2 2 39.2668 2.0984 1 -3 2 -2 41.0898 3.3988 3 -3 2 -2 32.9014 3.5156 2 3 2 2 37.7930 3.6996 2 -3 2 -2 39.6738 2.8995 5 -4 -2 -2 1874.79 69.70 3 4 -2 2 1988.98 69.43 1 -4 -2 -2 1883.11 69.31 5 -4 2 -2 1876.50 68.92 2 -4 2 -2 1869.33 69.55 3 -4 2 -2 1887.97 68.79 5 4 2 2 1853.29 68.76 2 -5 -2 -2 1942.41 74.84 5 -5 -2 -2 2073.28 84.39 4 -5 -2 -2 2124.45 75.72 3 5 -2 2 2091.60 74.83 1 -5 2 -2 2008.64 74.73 5 5 2 2 2033.80 74.61 2 -5 2 -2 2031.49 75.39 3 -5 2 -2 2006.82 74.82 2 -6 -2 -2 102.110 6.777 5 6 -2 2 103.027 6.061 1 -6 -2 -2 96.4013 7.8219 4 -6 -2 -2 89.8102 6.6404 3 -6 2 -2 94.5126 6.7402 3 -6 2 -2 109.539 8.242 2 6 2 2 93.4109 7.5456 2 -6 2 -2 93.3699 6.7690 5 -7 -2 -2 1050.66 41.92 3 -7 -2 -2 1027.39 41.32 5 7 -2 2 1041.33 40.25 1 -7 -2 -2 1069.71 46.55 4 -7 2 -2 1024.08 41.57 3 -7 2 -2 1052.74 41.42 5 7 2 2 1095.22 42.19 2 8 -2 2 -0.0434 1.9342 1 -8 -2 -2 0.24900 2.79148 4 -8 -2 -2 1.56779 2.40761 3 -8 -2 -2 1.46662 2.35004 5 8 -2 2 1.97064 2.87729 2 -8 2 -2 -0.2613 2.4139 3 8 2 2 2.10293 2.97861 2 -8 2 -2 0.29668 2.49627 5 9 -2 2 366.535 16.329 1 -9 -2 -2 368.364 18.268 5 -9 -2 -2 345.417 18.444 3 -9 -2 -2 343.694 19.943 4 9 -2 2 383.059 20.166 2 9 2 2 362.720 18.973 2 -9 2 -2 363.792 18.375 5 -9 2 -2 365.411 18.179 3 -10 -2 -2 197.479 12.473 5 10 -2 2 177.433 13.153 2 -10 -2 -2 180.613 12.950 4 10 -2 2 185.713 10.250 1 -10 -2 -2 166.499 11.877 3 -10 2 -2 195.586 12.336 3 -10 2 -2 166.509 11.791 5 10 2 2 181.939 12.958 2 11 -2 2 160.308 9.817 1 -11 -2 -2 190.236 12.756 5 -11 -2 -2 191.433 12.812 3 11 -2 2 156.744 13.030 2 -11 2 -2 153.648 11.808 3 -11 2 -2 180.451 12.577 5 11 2 2 170.613 12.650 2 -12 -2 -2 260.595 16.579 5 12 -2 2 253.364 17.297 2 -12 -2 -2 284.339 17.317 3 12 -2 2 269.290 13.757 1 12 2 2 270.947 17.291 2 -12 2 -2 262.249 16.545 3 -12 2 -2 268.882 16.412 5 13 -2 2 21.2538 6.5095 2 -13 -2 -2 12.6800 5.5280 5 -13 -2 -2 14.3698 5.6813 3 13 2 2 9.28758 5.32061 2 -13 2 -2 10.9693 5.1566 3 -13 2 -2 14.7629 5.4551 5 -14 -2 -2 249.871 17.136 5 14 -2 2 234.976 17.446 2 -14 -2 -2 241.685 17.010 3 -14 2 -2 215.558 15.668 5 14 2 2 245.228 17.159 2 -14 2 -2 236.066 16.740 3 15 -2 2 0.62084 5.95453 2 -15 -2 -2 -1.3607 5.1808 5 -15 -2 -2 2.15187 4.95323 3 -15 2 -2 1.22956 5.03812 3 -15 2 -2 -2.7839 5.4372 5 15 2 2 0.10192 5.46039 2 -16 -2 -2 215.724 17.479 5 16 -2 2 253.373 18.468 2 -16 -2 -2 191.281 16.513 3 16 2 2 218.934 17.275 2 -16 2 -2 167.056 15.862 5 -16 2 -2 249.674 18.183 3 17 -2 2 0.09965 7.00257 2 -17 -2 -2 -1.1459 6.6059 5 17 2 2 -4.8836 5.9936 3 17 2 2 2.12546 6.86004 2 -17 2 -2 12.2867 8.2825 3 -18 -2 -2 196.781 18.103 5 18 -2 2 199.101 17.879 2 18 2 2 187.295 18.113 3 18 2 2 180.548 17.022 2 -18 2 -2 190.775 18.060 3 -19 -2 -2 43.8421 11.0973 5 19 -2 2 36.1177 10.8022 2 19 2 2 52.7280 11.9552 3 19 2 2 40.8360 11.4447 2 -20 -3 2 166.485 18.884 5 20 -3 -2 159.987 17.853 3 -19 -3 2 -3.2203 7.5501 5 19 -3 -2 8.76480 8.12164 3 19 3 -2 0.39987 7.24567 3 18 -3 -2 326.257 22.150 3 -18 -3 2 260.855 21.081 5 -18 3 2 224.153 19.663 5 18 3 -2 317.365 21.720 3 17 -3 -2 1.80689 6.24957 3 17 -3 -2 11.0918 7.2849 2 -17 -3 2 3.57092 5.74798 5 17 3 -2 17.0209 6.7383 3 17 3 -2 7.77886 6.22505 2 -17 3 2 5.82058 7.22810 5 -16 -3 2 103.703 12.278 5 16 -3 -2 94.3089 11.5617 2 16 3 -2 89.1827 10.4658 2 16 3 -2 106.740 11.686 3 -16 3 2 94.7638 11.6273 5 -15 -3 2 104.344 11.936 5 15 -3 -2 98.6620 11.2447 2 15 3 -2 102.332 10.156 2 -15 3 2 106.774 11.425 3 -15 3 2 104.128 11.969 5 15 3 -2 96.9435 11.1191 3 -14 -3 2 65.7366 9.0465 5 14 -3 -2 41.0172 7.9506 2 14 -3 -2 39.4021 6.0684 1 -14 3 2 46.7369 8.0558 5 -14 3 2 36.0687 6.9542 3 14 3 -2 38.7044 6.9608 2 14 3 -2 49.5441 7.8973 3 -13 -3 2 469.437 24.516 5 13 -3 -2 405.834 23.437 2 13 -3 -2 444.906 21.327 1 -13 3 2 470.344 24.891 5 13 3 -2 460.759 23.996 3 -13 3 2 453.657 23.631 3 13 3 -2 436.064 22.125 2 -12 -3 2 82.9943 8.9545 5 12 -3 -2 58.4381 7.9784 2 12 3 -2 55.1099 6.9438 2 -12 3 2 54.9390 8.1041 5 -12 3 2 91.4260 8.6644 3 12 3 -2 65.6793 7.7560 3 -12 3 2 66.2359 6.6268 1 -11 -3 2 667.469 31.741 4 11 -3 -2 675.387 31.011 2 -11 -3 2 665.521 31.013 5 -11 3 2 695.703 30.430 3 -11 3 2 669.209 31.546 5 -11 3 2 727.187 29.299 1 11 3 -2 637.547 30.652 3 11 3 -2 685.839 29.421 2 -10 -3 2 455.354 22.595 4 -10 -3 2 464.960 22.520 5 -10 3 2 432.295 22.241 2 10 3 -2 481.917 22.546 3 -10 3 2 472.209 23.089 5 -10 3 2 426.731 21.322 3 -10 3 2 458.446 20.705 1 10 3 -2 460.728 21.048 2 -9 -3 2 1044.68 40.71 1 -9 -3 2 1130.62 47.81 4 -9 -3 2 1063.04 44.80 5 -9 3 2 1108.91 43.55 1 9 3 -2 1127.69 45.09 3 -9 3 2 1147.65 44.40 3 -9 3 2 1103.48 44.29 2 9 3 -2 1132.90 43.22 2 -9 3 2 1134.67 45.63 5 -8 -3 2 1346.04 55.13 4 -8 -3 2 1318.62 51.33 5 -8 -3 2 1282.74 47.98 1 -8 3 2 1339.18 51.67 5 -8 3 2 1290.24 50.13 1 8 3 -2 1284.22 49.23 2 -8 3 2 1295.47 50.46 3 -8 3 2 1315.24 50.20 2 8 3 -2 1259.77 51.24 3 -7 -3 2 2.05007 1.64689 1 -7 -3 2 4.63995 2.37229 5 -7 3 2 6.00476 2.77721 5 7 3 -2 3.61799 2.27962 2 -7 3 2 2.36447 2.33392 2 -7 3 2 0.71423 1.95393 1 -7 3 2 0.13216 1.78130 3 7 3 -2 3.19702 2.51373 3 -6 -3 2 1241.53 45.71 1 -6 -3 2 1222.02 47.35 5 -6 3 2 1184.23 45.89 2 -6 3 2 1254.90 46.62 3 6 3 -2 1244.15 45.83 2 -6 3 2 1212.54 46.93 1 -6 3 2 1214.47 47.29 5 6 3 -2 1265.76 47.83 3 -5 -3 2 266.651 10.888 1 -5 -3 2 226.399 11.822 5 5 3 -2 252.798 11.539 2 -5 3 2 252.074 11.230 3 -5 3 2 240.819 11.893 5 -5 3 2 255.249 11.883 1 -5 3 2 252.963 11.643 2 5 3 -2 239.381 12.135 3 -4 -3 2 1125.23 41.48 1 4 -3 -2 1122.59 42.24 5 -4 -3 2 1120.74 42.38 5 4 3 -2 1137.81 42.73 3 4 3 -2 1120.19 41.09 2 -4 3 2 1081.70 41.12 2 -4 3 2 1103.72 41.42 3 -4 3 2 1139.71 42.55 1 -3 -3 2 647.109 24.684 1 3 -3 -2 644.562 25.115 5 -3 -3 2 628.826 25.085 5 3 3 -2 663.328 24.586 2 -3 3 2 643.512 24.572 2 -3 3 2 643.687 24.132 3 -3 3 2 648.484 25.471 1 3 3 -2 641.998 25.303 3 -2 -3 2 475.436 18.183 1 -2 -3 2 450.764 18.143 5 2 -3 -2 460.035 16.991 3 2 -3 -2 454.155 18.218 5 -2 3 2 477.088 17.139 3 -2 3 2 461.491 18.600 1 2 3 -2 457.927 18.226 3 2 3 -2 441.779 17.800 2 -2 3 2 448.141 17.862 2 -1 -3 2 75.4648 4.5175 5 -1 -3 2 83.2081 4.9416 1 1 -3 -2 81.7397 4.8392 5 -1 3 2 86.7983 4.9289 2 1 3 -2 84.0882 4.6838 3 1 3 -2 88.6984 4.8246 2 -1 3 2 89.8139 5.1051 1 0 -3 2 305.960 12.528 1 0 -3 2 295.372 11.506 5 0 -3 -2 271.056 12.090 5 0 3 2 283.258 10.853 3 0 3 -2 300.442 12.176 2 0 3 -2 300.207 11.862 3 0 3 2 274.035 12.017 1 0 3 2 284.250 12.170 2 0 3 2 283.407 10.947 3 -1 -3 -2 1849.77 66.55 5 -1 -3 -2 1875.36 66.15 3 1 -3 2 1807.92 65.43 5 1 -3 2 1823.40 67.06 1 1 3 2 1836.85 66.39 1 1 3 2 1762.11 65.78 3 -1 3 -2 1840.28 65.36 2 -1 3 -2 1819.40 65.37 5 1 3 2 1834.48 65.45 2 -1 3 -2 1815.54 66.27 3 -2 -3 -2 248.907 11.181 5 2 -3 2 246.888 11.303 1 -2 -3 -2 247.211 10.533 3 2 -3 2 240.607 9.753 5 2 3 2 254.502 11.398 2 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215.989 12.387 2 -7 3 -2 191.271 12.335 2 -8 -3 -2 699.715 29.931 5 -8 -3 -2 693.999 30.148 3 -8 -3 -2 728.870 33.560 4 8 -3 2 695.483 28.698 1 -8 3 -2 647.042 29.328 5 8 3 2 721.932 30.524 2 -8 3 -2 698.898 31.138 2 -8 3 -2 699.420 29.752 3 9 -3 2 48.7572 5.3276 1 -9 -3 -2 57.9761 7.1489 4 -9 -3 -2 47.6796 6.2148 3 -9 -3 -2 57.0811 6.5783 5 -9 3 -2 51.8659 6.3370 5 9 3 2 54.3821 6.9632 2 -9 3 -2 68.7417 6.7700 3 10 -3 2 339.307 17.082 1 10 -3 2 371.179 20.412 2 -10 -3 -2 350.704 18.995 5 -10 -3 -2 376.827 19.662 3 -10 3 -2 378.531 19.159 3 10 3 2 368.746 19.565 2 -10 3 -2 357.027 19.046 5 -11 -3 -2 178.896 13.136 5 11 -3 2 204.748 14.929 2 11 -3 2 198.462 11.543 1 -11 -3 -2 217.087 13.972 3 11 3 2 195.902 13.797 2 -11 3 -2 188.723 12.943 3 -11 3 -2 165.292 12.751 5 -12 -3 -2 112.344 11.792 4 12 -3 2 144.750 10.071 1 -12 -3 -2 169.991 12.907 3 12 -3 2 167.959 13.957 2 -12 -3 -2 174.859 13.051 5 12 3 2 189.215 13.568 2 -12 3 -2 168.072 12.353 3 -12 3 -2 138.608 11.922 5 -13 -3 -2 184.550 13.857 3 13 -3 2 135.662 13.718 2 -13 -3 -2 193.185 14.337 5 -13 3 -2 135.438 12.604 5 -13 3 -2 165.967 12.952 3 13 3 2 179.683 14.004 2 14 -3 2 3.33071 6.40493 2 -14 -3 -2 13.5921 6.2565 3 -14 -3 -2 14.8430 6.0758 5 14 3 2 20.6771 6.5709 2 -14 3 -2 8.04048 5.43030 5 -14 3 -2 19.6231 6.2384 3 15 -3 2 220.264 17.703 2 -15 -3 -2 199.188 16.552 5 -15 3 -2 237.949 17.138 3 15 3 2 212.291 16.595 2 -16 -3 -2 17.6553 7.5367 5 16 -3 2 -2.5086 6.3169 2 -16 3 -2 6.09006 6.31635 3 16 3 2 4.16218 6.37094 2 16 3 2 11.5441 6.2247 3 -17 -3 -2 134.771 15.539 5 17 -3 2 112.034 14.227 2 17 3 2 162.642 16.023 3 -17 3 -2 126.412 14.390 3 17 3 2 144.096 14.794 2 -18 -3 -2 41.3799 10.7238 5 18 -3 2 33.8302 10.8318 2 -18 3 -2 30.4882 9.4236 3 18 3 2 27.3442 9.7806 3 18 3 2 36.1929 9.8789 2 -19 -3 -2 84.1989 14.1529 5 19 -3 2 100.962 14.755 2 -19 3 -2 95.2700 14.4525 3 19 3 2 80.6599 12.8125 2 20 -4 -2 1.20532 8.76954 3 19 -4 -2 362.926 25.607 3 -19 -4 2 352.619 26.009 5 19 4 -2 379.197 25.440 3 18 -4 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45.73 5 -8 2 4 1191.04 44.28 1 8 2 -4 1130.13 45.09 3 -7 -2 4 776.157 31.280 1 7 -2 -4 806.701 32.072 3 -7 -2 4 824.718 33.563 4 -7 -2 4 769.027 32.720 5 7 2 -4 817.232 32.962 3 -7 2 4 823.024 33.393 5 7 2 -4 804.220 30.450 2 -7 2 4 808.830 32.041 1 -7 2 4 800.781 31.151 2 -6 -2 4 37.7071 3.7438 1 -6 -2 4 37.4159 2.9516 4 6 -2 -4 31.5831 3.4586 3 -6 -2 4 35.5827 4.3361 5 6 2 -4 29.4926 3.0395 2 -6 2 4 35.2525 3.4412 2 6 2 -4 23.6919 3.5275 3 -6 2 4 37.0509 4.4015 5 -6 2 4 30.4958 3.6597 1 -5 -2 4 191.928 9.469 1 -5 -2 4 182.812 9.926 5 5 -2 -4 195.295 9.333 3 -5 2 4 203.619 9.972 1 -5 2 4 197.946 10.266 5 5 2 -4 196.395 8.553 2 5 2 -4 188.478 10.133 3 -5 2 4 198.336 8.843 2 -4 -2 4 273.117 12.807 5 -4 -2 4 285.851 12.471 1 4 -2 -4 298.988 12.142 3 4 2 -4 290.655 12.918 3 4 2 -4 290.935 11.375 2 -4 2 4 282.191 12.951 5 -4 2 4 278.939 12.794 1 -4 2 4 276.059 11.502 2 -3 -2 4 355.923 14.322 1 3 -2 -4 329.461 14.451 5 -3 -2 4 342.779 14.318 5 3 -2 -4 329.621 13.402 3 3 2 -4 333.662 14.400 3 -3 2 4 342.019 13.253 2 3 2 -4 339.625 13.084 2 -3 2 4 352.787 14.717 1 2 -2 -4 2080.86 72.82 3 2 -2 -4 2004.68 73.19 5 -2 -2 4 1996.81 72.82 5 -2 -2 4 2001.25 73.57 1 -2 2 4 2060.46 73.99 1 2 2 -4 2000.18 73.62 3 -2 2 4 1956.94 70.99 2 2 2 -4 2075.43 71.04 2 -2 2 4 1986.42 72.61 3 -1 -2 4 1995.05 73.46 1 1 -2 -4 2010.99 72.90 5 -1 -2 4 2025.97 72.38 5 1 -2 -4 2002.91 72.57 3 1 2 -4 2055.17 71.16 2 -1 2 4 2013.07 71.21 2 1 2 -4 1888.45 71.97 5 -1 2 4 2070.74 72.55 3 1 2 -4 2067.26 73.51 3 -1 2 4 2028.93 73.61 1 0 -2 4 2604.89 92.87 5 0 -2 -4 2567.66 92.65 5 0 -2 -4 2569.71 92.63 3 0 -2 4 2519.78 93.39 1 0 2 -4 2583.98 90.90 2 0 2 -4 2635.09 93.39 3 0 2 4 2609.33 91.01 2 0 2 -4 2520.89 92.30 5 0 2 4 2668.13 93.43 1 0 2 4 2510.42 92.41 3 1 -2 4 185.016 8.812 1 -1 -2 -4 202.736 8.900 5 -1 -2 -4 192.424 8.323 3 -1 2 -4 192.902 8.864 3 1 2 4 193.646 9.184 2 1 2 4 193.072 8.493 1 -1 2 -4 176.460 8.944 2 -2 -2 -4 2065.19 75.50 3 2 -2 4 2040.31 75.67 1 -2 -2 -4 2105.61 75.28 5 2 2 4 2019.28 74.50 2 2 2 4 2082.19 74.99 1 -2 2 -4 2114.37 74.75 2 -2 2 -4 2082.08 75.77 3 3 -2 4 50.6284 4.0018 1 -3 -2 -4 52.8695 4.2611 5 -3 -2 -4 57.4512 4.3216 3 3 -2 4 41.6607 2.6805 5 -3 -2 -4 48.9572 3.3125 1 -3 2 -4 46.5918 3.1198 5 -3 2 -4 43.5644 4.0461 3 3 2 4 55.7942 5.0385 2 -3 2 -4 50.5816 4.8069 2 3 2 4 49.5413 2.9610 1 -4 -2 -4 1425.43 54.11 5 -4 -2 -4 1471.27 54.72 3 -4 -2 -4 1527.84 52.62 1 4 -2 4 1435.87 54.05 1 -4 2 -4 1363.06 53.08 5 4 2 4 1498.27 52.66 1 -4 2 -4 1465.02 54.92 2 4 2 4 1394.33 54.54 2 -4 2 -4 1477.72 54.70 3 -5 -2 -4 501.730 21.661 5 -5 -2 -4 538.683 22.227 3 5 -2 4 500.451 21.084 1 -5 -2 -4 547.241 25.750 4 -5 2 -4 543.168 22.199 3 -5 2 -4 547.017 23.747 2 5 2 4 501.672 22.922 2 -5 2 -4 488.996 20.989 5 -6 -2 -4 734.201 29.960 3 6 -2 4 719.965 28.546 1 -6 -2 -4 743.196 34.123 4 -6 -2 -4 691.858 29.235 5 -6 2 -4 725.606 29.863 3 6 2 4 706.330 30.856 2 -6 2 -4 727.513 28.984 5 7 -2 4 504.317 20.518 1 7 -2 4 445.976 23.231 2 -7 -2 -4 497.232 25.252 4 -7 -2 -4 468.060 21.971 3 -7 -2 -4 480.069 21.464 5 7 2 4 490.985 23.482 2 -7 2 -4 473.983 21.243 5 -7 2 -4 514.987 22.195 3 8 -2 4 49.6303 7.2588 2 -8 -2 -4 55.7451 7.3917 4 -8 -2 -4 55.7722 5.9111 5 -8 -2 -4 53.8339 6.0947 3 8 -2 4 49.5616 4.7992 1 -8 2 -4 59.6748 6.1131 3 -8 2 -4 38.5240 5.2330 5 8 2 4 55.2226 7.3415 2 -9 -2 -4 461.475 21.877 5 -9 -2 -4 430.425 21.878 3 -9 -2 -4 453.560 25.074 4 9 -2 4 432.433 23.530 2 9 -2 4 450.938 19.724 1 -9 2 -4 467.859 22.041 3 9 2 4 473.681 23.751 2 -9 2 -4 451.426 21.361 5 10 -2 4 13.0240 5.0498 2 -10 -2 -4 14.8998 5.2198 4 10 -2 4 10.3270 2.9570 1 -10 -2 -4 11.7437 4.4839 3 -10 -2 -4 7.59138 3.90905 5 10 2 4 16.2189 5.0968 2 -10 2 -4 13.9203 4.1910 3 -10 2 -4 10.7892 4.1532 5 -11 -2 -4 197.114 13.169 5 -11 -2 -4 197.599 13.264 3 11 -2 4 157.215 9.902 1 11 -2 4 174.432 14.112 2 -11 -2 -4 163.789 13.941 4 -11 2 -4 179.466 12.691 3 11 2 4 187.350 14.339 2 -11 2 -4 170.858 12.312 5 -12 -2 -4 281.447 16.746 5 -12 -2 -4 242.121 16.215 3 12 -2 4 243.287 17.334 2 12 2 4 260.049 17.736 2 -12 2 -4 272.700 16.642 3 -12 2 -4 213.286 15.211 5 -13 -2 -4 127.456 11.942 3 13 -2 4 125.692 13.206 2 -13 -2 -4 131.280 12.142 5 -13 2 -4 152.778 12.355 3 13 2 4 166.402 13.727 2 -13 2 -4 123.033 11.478 5 -14 -2 -4 271.465 18.309 5 -14 -2 -4 296.293 19.337 3 14 -2 4 287.350 19.976 2 -14 2 -4 220.495 16.718 5 14 2 4 289.772 19.663 2 -14 2 -4 274.512 18.256 3 -15 -2 -4 121.261 13.003 3 -15 -2 -4 84.1137 11.3525 5 15 -2 4 95.3670 12.4676 2 -15 2 -4 99.0763 11.8472 3 15 2 4 77.2808 11.4132 2 16 -2 4 266.992 20.682 2 -16 -2 -4 304.686 21.542 3 -16 -2 -4 294.140 21.344 5 -16 2 -4 299.687 20.868 3 16 2 4 294.252 20.865 2 -17 -2 -4 11.3280 7.8329 3 -17 -2 -4 -1.1939 6.4879 5 17 -2 4 -3.9379 7.1971 2 -17 2 -4 -6.4933 6.1482 3 17 2 4 5.20366 7.82417 2 -18 -2 -4 174.267 17.983 5 18 -2 4 147.975 16.662 2 18 2 4 188.135 17.876 2 -18 2 -4 175.461 17.963 3 19 -2 4 53.2403 12.9342 2 19 2 4 31.4480 10.7406 2 20 -3 -4 226.761 20.656 3 -20 -3 4 246.514 21.644 5 20 3 -4 266.820 21.469 3 19 -3 -4 13.0498 8.0186 3 -19 -3 4 12.4581 9.1699 5 19 3 -4 9.71604 6.76140 3 -19 3 4 8.57025 7.86712 5 -18 -3 4 331.024 23.013 5 18 -3 -4 334.901 22.185 3 18 3 -4 326.429 22.427 3 -18 3 4 277.467 21.780 5 -17 -3 4 -4.6877 4.8985 5 17 -3 -4 1.98495 6.05501 3 17 3 -4 5.41495 5.43361 3 -17 3 4 -1.5261 6.5990 5 16 -3 -4 240.425 17.527 3 16 -3 -4 258.696 17.773 2 -16 -3 4 256.931 18.480 5 16 3 -4 249.766 18.052 3 -16 3 4 263.573 18.797 5 16 3 -4 217.159 15.231 2 15 -3 -4 77.7245 10.0147 2 15 -3 -4 91.3085 10.4327 3 -15 -3 4 104.403 11.228 5 -15 3 4 84.6000 10.9167 5 15 3 -4 86.3162 8.8394 2 15 3 -4 85.0127 9.9205 3 14 -3 -4 283.867 18.014 2 -14 -3 4 288.883 19.173 5 14 -3 -4 316.046 18.581 3 14 3 -4 337.590 19.121 3 -14 3 4 317.564 19.980 5 14 3 -4 265.311 16.152 2 -14 3 4 300.862 16.518 1 -13 -3 4 563.485 27.499 5 13 -3 -4 510.492 25.670 3 13 -3 -4 500.958 25.515 2 13 3 -4 519.852 23.784 2 13 3 -4 509.797 26.042 3 -13 3 4 551.570 27.777 5 -13 3 4 487.969 23.912 1 12 -3 -4 14.6154 4.9405 2 -12 -3 4 9.69821 4.85781 5 -12 3 4 7.91436 3.86274 1 12 3 -4 11.5878 4.0204 2 -12 3 4 9.15771 5.10386 5 12 3 -4 18.6954 4.7081 3 -11 -3 4 506.422 22.852 1 -11 -3 4 546.418 27.304 5 11 3 -4 654.716 25.461 2 11 3 -4 595.919 27.426 3 -11 3 4 611.088 28.608 5 -11 3 4 602.951 26.781 3 -11 3 4 588.148 25.939 1 -10 -3 4 104.569 8.808 5 -10 -3 4 70.2553 5.6354 1 -10 -3 4 82.7624 6.5900 4 -10 3 4 102.254 8.692 2 -10 3 4 106.713 8.346 3 -10 3 4 91.3651 8.9926 5 10 3 -4 92.2252 7.2396 2 -10 3 4 107.693 7.866 1 10 3 -4 122.421 9.236 3 -9 -3 4 712.598 31.054 4 -9 -3 4 698.097 31.014 5 -9 -3 4 670.983 28.016 1 -9 3 4 728.770 30.103 3 -9 3 4 673.321 29.670 1 -9 3 4 756.030 30.006 2 9 3 -4 695.202 30.749 3 9 3 -4 759.690 28.822 2 -9 3 4 722.219 31.722 5 -8 -3 4 946.401 40.032 4 -8 -3 4 922.744 36.765 1 -8 -3 4 956.038 38.959 5 8 3 -4 958.419 36.350 2 -8 3 4 924.795 39.134 5 -8 3 4 978.796 38.204 1 8 3 -4 944.807 38.925 3 -8 3 4 1009.68 38.07 3 -8 3 4 908.670 36.931 2 -7 -3 4 135.207 7.930 1 -7 -3 4 143.214 9.315 5 -7 3 4 119.364 8.383 1 7 3 -4 146.961 7.908 2 -7 3 4 158.629 9.763 5 -7 3 4 157.770 8.468 3 -7 3 4 140.547 8.264 2 7 3 -4 146.817 9.386 3 6 -3 -4 1685.70 59.91 3 -6 -3 4 1616.80 60.76 5 -6 -3 4 1637.52 59.86 1 6 3 -4 1563.57 61.06 3 -6 3 4 1604.21 58.38 2 6 3 -4 1621.58 58.08 2 -6 3 4 1549.43 60.56 1 -6 3 4 1558.28 60.70 5 5 -3 -4 2.52308 1.51988 3 5 -3 -4 3.87981 2.16145 5 -5 -3 4 2.82604 1.80262 1 -5 -3 4 1.25845 1.79741 5 -5 3 4 1.42362 1.47088 2 5 3 -4 1.96972 1.45666 2 -5 3 4 3.43140 1.85894 1 5 3 -4 3.30838 1.89322 3 -4 -3 4 2837.74 101.49 1 4 -3 -4 2799.12 101.47 5 4 -3 -4 2858.30 100.76 3 -4 -3 4 2701.92 101.16 5 4 3 -4 2807.24 102.11 3 4 3 -4 2782.06 98.30 2 -4 3 4 2763.87 98.48 2 -4 3 4 2789.41 102.14 1 -3 -3 4 446.838 18.521 5 3 -3 -4 483.269 17.365 3 -3 -3 4 447.460 18.552 1 3 -3 -4 436.857 17.232 3 3 -3 -4 483.255 19.030 5 -3 3 4 452.723 17.851 2 -3 3 4 435.762 18.947 1 3 3 -4 457.827 17.719 2 3 3 -4 463.299 18.919 3 2 -3 -4 1896.55 69.83 3 2 -3 -4 1967.04 70.61 5 2 -3 -4 1959.82 70.06 3 -2 -3 4 1900.09 70.90 1 -2 -3 4 1921.40 69.96 5 -2 3 4 1909.11 68.71 2 2 3 -4 1931.51 68.63 2 -2 3 4 2003.27 71.30 1 2 3 -4 1907.74 70.96 3 1 -3 -4 74.0436 3.2563 3 -1 -3 4 70.1213 4.0709 5 -1 -3 4 69.2193 4.8582 1 1 -3 -4 65.7001 4.6410 5 1 3 -4 69.9324 4.5884 2 -1 3 4 84.5036 4.9866 2 -1 3 4 74.7021 3.3559 3 -1 3 4 70.5679 4.8824 1 1 3 -4 83.8996 5.0616 3 0 -3 -4 321.558 12.140 3 0 -3 4 301.244 11.965 5 0 -3 -4 313.455 13.451 5 0 -3 4 310.060 13.569 1 0 3 4 304.207 11.986 3 0 3 -4 321.291 12.009 5 0 3 4 305.838 13.363 2 0 3 4 314.162 13.265 1 0 3 -4 299.506 13.231 2 0 3 -4 328.868 13.455 3 1 -3 4 1046.58 37.87 5 -1 -3 -4 1056.75 38.68 3 -1 -3 -4 1017.68 39.40 5 1 -3 4 1044.68 39.84 1 1 3 4 1040.49 39.03 1 1 3 4 1063.62 39.19 2 -1 3 -4 1056.29 37.78 5 -1 3 -4 1035.02 39.36 3 -1 3 -4 1058.55 39.05 2 -2 -3 -4 1.35384 1.34966 3 2 -3 4 3.49018 1.77517 1 -2 -3 -4 0.52856 1.68167 5 -2 3 -4 3.74300 1.92662 2 -2 3 -4 2.18951 1.52662 3 2 3 4 1.40911 1.17638 1 2 3 4 -0.2733 1.6195 2 -3 -3 -4 1870.78 67.97 3 3 -3 4 1847.20 65.93 5 3 -3 4 1814.90 68.23 1 -3 -3 -4 1830.59 67.96 5 3 -3 4 1920.16 66.04 5 -3 3 -4 1832.80 67.55 2 -3 3 -4 1781.51 67.96 3 3 3 4 1835.12 67.48 2 3 3 4 1827.99 66.67 1 -4 -3 -4 608.032 24.257 3 4 -3 4 598.662 24.196 1 -4 -3 -4 602.514 24.420 5 -4 -3 -4 566.307 22.339 1 -4 3 -4 588.075 22.271 5 4 3 4 608.145 25.019 2 -4 3 -4 597.165 24.206 3 -4 3 -4 602.522 25.075 2 4 3 4 556.906 21.943 1 -5 -3 -4 1057.46 41.36 5 -5 -3 -4 1089.04 41.68 3 5 -3 4 1070.93 41.14 1 -5 3 -4 1044.28 42.06 2 -5 3 -4 1053.22 41.38 3 5 3 4 1063.18 42.01 2 -5 3 -4 1053.66 39.66 5 -6 -3 -4 1346.31 53.06 3 6 -3 4 1412.32 52.41 1 -6 -3 -4 1406.07 60.27 4 -6 -3 -4 1350.57 52.73 5 -6 3 -4 1389.72 52.96 3 -6 3 -4 1402.88 53.87 2 -6 3 -4 1339.59 51.37 5 6 3 4 1325.65 53.18 2 -7 -3 -4 129.263 10.620 4 -7 -3 -4 128.784 8.856 3 -7 -3 -4 127.824 8.793 5 7 -3 4 123.318 8.045 1 -7 3 -4 118.033 10.238 2 -7 3 -4 117.490 8.426 3 7 3 4 127.085 9.951 2 -7 3 -4 112.837 7.872 5 -8 -3 -4 819.124 36.202 5 8 -3 4 950.555 35.690 1 -8 -3 -4 888.307 37.188 3 -8 -3 -4 915.518 42.190 4 -8 3 -4 820.804 35.559 5 -8 3 -4 902.775 36.748 3 8 3 4 863.703 37.691 2 -9 -3 -4 13.7192 5.2516 4 -9 -3 -4 15.7245 4.5125 3 -9 -3 -4 11.7231 4.1061 5 9 -3 4 17.5597 4.9899 2 9 -3 4 8.32212 3.15467 1 -9 3 -4 11.1636 4.0542 3 9 3 4 10.2926 4.3362 2 -9 3 -4 10.7629 4.0007 5 -10 -3 -4 850.730 36.744 3 -10 -3 -4 820.391 40.870 4 -10 -3 -4 848.842 36.388 5 10 -3 4 805.778 37.883 2 10 -3 4 826.319 34.002 1 -10 3 -4 806.721 35.890 3 10 3 4 838.720 37.370 2 -10 3 -4 797.879 35.235 5 -11 -3 -4 98.9793 9.7660 5 11 -3 4 88.9505 7.9699 1 11 -3 4 110.482 11.271 2 -11 -3 -4 101.280 9.819 3 -11 -3 -4 98.8151 11.2441 4 -11 3 -4 106.935 9.898 3 -11 3 -4 97.6022 9.3888 5 11 3 4 109.412 11.047 2 12 -3 4 277.068 18.320 2 -12 -3 -4 276.271 16.883 5 12 -3 4 220.061 13.148 1 -12 -3 -4 226.730 16.141 3 -12 -3 -4 260.753 18.353 4 -12 3 -4 252.962 15.935 3 -12 3 -4 189.210 14.661 5 12 3 4 262.098 17.466 2 -13 -3 -4 101.811 11.202 3 13 -3 4 93.6598 11.7651 2 -13 -3 -4 96.8111 10.7623 5 -13 3 -4 91.5042 10.2178 3 13 3 4 105.147 11.752 2 -14 -3 -4 70.6960 10.3097 3 -14 -3 -4 80.4359 10.4650 5 14 -3 4 73.6712 11.1081 2 14 3 4 64.7619 9.6247 2 -14 3 -4 60.5981 9.3400 3 -15 -3 -4 166.821 15.547 5 15 -3 4 143.004 15.354 2 -15 -3 -4 179.598 15.507 3 -15 3 -4 184.220 15.591 3 15 3 4 161.776 15.480 2 -16 -3 -4 0.19833 7.01632 5 16 -3 4 4.50066 6.69960 2 -16 -3 -4 -2.6377 6.5726 3 16 3 4 -4.3982 6.5470 2 -16 3 -4 4.06959 6.48081 3 -17 -3 -4 112.362 14.855 5 17 -3 4 118.107 15.130 2 -17 3 -4 124.340 14.356 3 17 3 4 132.891 15.140 2 18 -3 4 29.2722 10.5427 2 -18 -3 -4 14.9052 10.2615 5 18 3 4 43.9430 10.9440 3 -18 3 -4 27.0674 9.8621 3 18 3 4 41.6033 10.9720 2 20 -4 -4 7.16062 9.50403 3 19 -4 -4 320.834 23.058 3 -19 -4 4 337.021 24.430 5 19 4 -4 278.278 22.111 3 18 -4 -4 25.0127 8.2704 3 -18 -4 4 22.1589 7.9180 5 18 4 -4 25.7294 8.5685 3 -18 4 4 15.0614 8.4412 5 17 -4 -4 457.246 27.188 3 -17 -4 4 503.010 29.396 5 17 4 -4 497.201 27.931 3 -17 4 4 482.762 29.000 5 16 -4 -4 0.82774 5.30010 3 16 -4 -4 2.08101 5.97597 2 -16 -4 4 -4.7910 5.3493 5 16 4 -4 -0.5070 4.8829 2 -16 4 4 4.44890 6.67190 5 16 4 -4 0.68337 5.47355 3 15 -4 -4 266.059 18.532 2 -15 -4 4 289.540 19.480 5 15 -4 -4 283.133 18.355 3 -15 4 4 286.874 19.891 5 15 4 -4 298.491 19.204 3 15 4 -4 271.076 16.421 2 14 -4 -4 32.8681 7.3503 2 14 -4 -4 28.2907 6.3024 3 -14 -4 4 45.5859 8.0556 5 14 4 -4 42.6747 7.7480 3 -14 4 4 23.9074 7.0475 5 14 4 -4 26.9020 5.5414 2 -14 4 4 27.7386 5.5054 1 -13 -4 4 195.956 14.795 5 13 -4 -4 182.586 13.319 3 13 -4 -4 213.011 14.545 2 13 4 -4 218.738 12.946 2 13 4 -4 185.221 13.792 3 -13 4 4 174.975 12.194 1 -13 4 4 198.319 15.297 5 -12 -4 4 98.7371 9.7828 5 -12 4 4 93.0127 9.5481 2 12 4 -4 81.2829 7.8906 2 -12 4 4 108.153 9.215 1 -12 4 4 109.842 10.964 5 12 4 -4 85.0544 9.2798 3 -11 -4 4 2.15860 2.89600 4 -11 -4 4 6.44765 4.24782 5 11 4 -4 10.8665 4.3832 3 -11 4 4 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7 5 1852.55 69.83 3 2 -7 5 180.443 11.291 1 2 -7 5 160.547 8.208 5 -2 -7 -5 177.314 11.034 5 2 7 5 146.264 8.070 3 -2 7 -5 160.846 10.887 2 2 7 5 188.317 10.065 1 -2 7 -5 156.727 9.484 3 2 7 5 160.679 10.832 2 3 -7 5 1585.08 58.75 5 -3 -7 -5 1672.30 62.78 5 -3 -7 -5 1630.14 60.94 1 3 -7 5 1599.96 63.18 1 -3 7 -5 1594.27 61.17 3 3 7 5 1501.61 60.13 3 3 7 5 1715.21 62.66 2 -3 7 -5 1618.91 62.09 2 -4 -7 -5 2.80135 3.05002 5 -4 -7 -5 2.44280 2.30832 1 4 -7 5 3.30736 3.29523 1 4 -7 5 3.14472 1.76329 5 -4 7 -5 1.90949 3.42439 2 4 7 5 3.76172 3.56930 2 4 7 5 1.26390 2.48872 3 -4 7 -5 2.65170 2.45197 3 5 -7 5 1053.03 42.99 1 -5 -7 -5 1018.37 42.63 5 -5 -7 -5 964.139 39.308 1 5 7 5 1078.36 43.24 2 5 7 5 1028.57 41.23 3 -5 7 -5 1045.97 43.06 2 -5 7 -5 1019.79 41.23 3 -6 -7 -5 357.201 19.109 5 6 -7 5 372.573 19.231 1 6 7 5 373.290 19.844 2 6 7 5 362.553 18.059 3 -6 7 -5 336.059 17.608 3 -6 7 -5 355.579 19.778 2 -7 -7 -5 178.195 12.493 5 7 -7 5 159.864 11.741 1 7 7 5 161.620 12.445 2 7 7 5 161.423 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6.28923 3.98247 2 -6 5 -6 12.4857 4.2979 2 7 -5 6 8.94622 3.83977 1 -7 -5 -6 8.36324 4.08130 3 -7 -5 -6 13.0653 4.2734 5 -7 5 -6 4.92751 4.18444 2 -7 5 -6 6.81497 3.48990 3 7 5 6 8.60330 4.25491 2 -8 -5 -6 650.412 29.633 5 -8 -5 -6 661.160 34.559 4 -8 -5 -6 648.946 29.604 3 8 -5 6 625.857 28.537 1 -8 5 -6 609.553 30.966 2 8 5 6 647.564 30.896 2 -8 5 -6 633.970 28.996 3 9 -5 6 -0.3894 3.6309 1 -9 -5 -6 1.56142 4.10586 3 -9 -5 -6 4.50075 4.93866 4 -9 -5 -6 -1.6025 3.5762 5 9 5 6 6.11257 5.20982 2 -9 5 -6 3.72691 3.68879 3 -9 5 -6 -1.5697 5.0066 2 -10 -5 -6 1050.16 52.01 4 10 -5 6 1016.24 47.05 2 10 -5 6 1063.07 43.95 1 -10 -5 -6 1062.91 45.44 5 -10 -5 -6 1106.39 46.10 3 -10 5 -6 999.270 44.685 3 10 5 6 1030.27 46.69 2 -11 -5 -6 -0.3846 4.4859 3 11 -5 6 -2.5414 4.4645 2 -11 -5 -6 0.50287 4.60929 5 11 -5 6 -0.9728 4.0978 1 -11 -5 -6 -1.8795 5.3780 4 11 5 6 0.38469 5.25981 2 -11 5 -6 0.40305 4.14856 3 -12 -5 -6 570.570 33.475 4 12 -5 6 518.640 26.218 1 -12 -5 -6 561.774 29.399 3 12 -5 6 536.654 30.820 2 -12 -5 -6 555.734 28.925 5 12 5 6 544.176 29.926 2 -12 5 -6 508.117 27.542 3 -13 -5 -6 10.4638 7.4454 4 -13 -5 -6 13.0477 6.4876 5 13 -5 6 17.6951 8.5623 2 -13 -5 -6 11.2507 6.5012 3 -13 5 -6 29.0681 7.1786 3 13 5 6 6.14867 6.76587 2 14 -5 6 337.665 24.072 2 -14 -5 -6 265.021 23.587 4 -14 -5 -6 324.665 22.383 5 -14 -5 -6 361.369 23.223 3 -14 5 -6 334.530 21.279 3 14 5 6 344.897 23.405 2 -15 -5 -6 22.2552 8.5625 5 15 -5 6 9.12644 8.85941 2 15 5 6 15.7726 7.8781 2 -15 5 -6 17.1336 7.4462 3 16 -5 6 30.4136 10.7955 2 -16 -5 -6 31.7060 10.2771 5 16 5 6 32.0777 10.4850 2 -16 5 -6 38.5914 10.3034 3 16 5 6 33.3861 10.1060 3 -17 -5 -6 -0.8337 9.1226 5 17 -5 6 -0.6327 8.9323 2 -17 5 -6 -3.1009 8.0273 3 17 5 6 5.76648 9.71288 2 17 5 6 -4.1158 8.2973 3 -19 -6 6 125.053 16.497 5 19 6 -6 139.427 15.740 3 18 -6 -6 9.93224 9.51060 5 -18 -6 6 14.1645 8.6626 5 18 6 -6 13.2722 7.8103 3 17 -6 -6 528.919 32.680 5 -17 -6 6 662.079 35.499 5 17 6 -6 658.812 33.975 3 16 -6 -6 3.29910 5.64303 3 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10 -6 -6 13.9050 4.8101 5 -10 -6 6 5.32271 3.63976 1 10 6 -6 15.5365 5.1531 3 -10 6 6 14.1478 4.3173 2 10 6 -6 2.23679 3.32359 2 -10 6 6 10.1807 4.6499 1 -9 -6 6 43.8722 6.6516 5 -9 -6 6 40.0177 5.5057 1 9 -6 -6 25.6631 5.3156 5 9 -6 -6 40.7661 4.9132 3 -9 6 6 28.8020 5.4325 1 9 6 -6 41.0517 5.2879 2 -9 6 6 49.2534 5.8537 2 9 6 -6 44.0255 6.2564 3 -8 -6 6 40.1901 5.0820 1 8 -6 -6 34.9671 5.7941 5 8 -6 -6 30.3296 4.0104 3 -8 -6 6 38.8889 5.9987 5 -8 6 6 44.1520 6.2397 1 8 6 -6 36.0570 4.7084 2 -8 6 6 38.1239 5.1818 2 8 6 -6 45.0826 6.3205 3 -7 -6 6 1458.36 57.59 5 7 -6 -6 1503.04 57.83 5 7 -6 -6 1442.99 54.58 3 -7 -6 6 1457.38 56.60 1 7 6 -6 1485.30 55.26 2 7 6 -6 1489.52 58.21 3 -7 6 6 1492.99 55.71 2 -7 6 6 1407.05 58.06 1 6 -6 -6 7.18887 1.99278 3 6 -6 -6 8.05720 3.36345 5 -6 -6 6 11.7087 3.2249 1 -6 -6 6 10.6536 3.5461 5 6 6 -6 12.6752 3.7377 3 6 6 -6 10.9464 3.0854 2 -6 6 6 9.97505 3.46276 1 -6 6 6 11.5750 3.2937 2 -5 -6 6 1524.65 58.15 5 5 -6 -6 1463.62 58.42 5 -5 -6 6 1540.58 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2 10 329.640 17.654 1 9 -2 -10 182.415 10.944 3 -9 -2 10 182.682 11.770 1 -9 -2 10 183.549 12.199 5 9 2 -10 175.910 11.634 3 -9 2 10 147.835 8.311 2 -9 2 10 187.961 12.531 5 -9 2 10 184.449 11.974 1 -8 -2 10 873.256 35.900 5 8 -2 -10 819.196 34.287 3 -8 -2 10 865.084 35.926 1 8 2 -10 812.946 35.302 3 -8 2 10 859.990 35.907 1 -8 2 10 809.572 30.764 2 -8 2 10 853.937 35.899 5 -7 -2 10 152.094 10.151 5 7 -2 -10 145.742 9.040 3 -7 -2 10 161.186 10.569 1 7 2 -10 154.127 9.999 3 -7 2 10 152.659 10.343 5 -7 2 10 142.168 6.717 2 -7 2 10 144.040 10.284 1 -6 -2 10 2946.64 109.59 1 6 -2 -10 2910.59 107.52 3 6 -2 -10 2913.37 108.46 5 -6 -2 10 2912.78 108.03 5 -6 -2 10 3042.09 102.44 2 -6 2 10 2887.07 102.59 2 6 2 -10 3032.15 102.81 2 -6 2 10 2902.81 109.74 1 6 2 -10 2842.99 108.64 3 5 -2 -10 130.685 8.015 3 5 -2 -10 150.840 9.223 5 -5 -2 10 144.533 9.712 1 -5 -2 10 135.478 8.766 5 5 2 -10 152.189 9.149 3 -5 2 10 131.800 6.472 2 5 2 -10 137.843 6.535 2 -5 2 10 149.863 9.890 1 4 -2 -10 2086.94 77.39 5 -4 -2 10 1980.58 78.41 1 -4 -2 10 2089.26 76.69 5 4 -2 -10 2119.56 76.74 3 -4 2 10 2068.26 79.11 1 4 2 -10 2035.25 77.79 3 4 2 -10 2097.62 73.89 2 -4 2 10 2127.64 73.70 2 -3 -2 10 965.896 40.094 1 3 -2 -10 1037.38 38.59 3 -3 -2 10 1009.00 38.24 5 3 -2 -10 1045.54 39.37 5 -3 2 10 1006.30 40.89 1 -3 2 10 1010.92 37.10 2 3 2 -10 947.156 39.387 3 3 2 -10 981.984 37.401 2 -2 -2 10 503.835 22.602 1 2 -2 -10 524.347 21.830 5 2 -2 -10 539.347 21.325 3 2 2 -10 511.740 22.233 3 -2 2 10 519.071 20.807 2 2 2 -10 501.572 21.223 2 -2 2 10 489.111 23.245 1 -1 -2 10 1012.99 41.43 1 1 -2 -10 1053.75 40.11 3 1 -2 -10 1070.85 40.39 5 1 2 -10 1088.06 41.36 3 -1 2 10 1005.74 42.21 1 -1 2 10 1017.53 39.48 2 1 2 -10 1035.18 38.55 5 1 2 -10 1071.27 40.54 2 0 -2 -10 4.28131 2.16095 5 0 -2 -10 5.24552 2.11371 3 0 -2 10 6.85578 2.86787 1 0 2 -10 8.15390 2.80869 3 0 2 -10 4.47011 1.40090 5 0 2 10 9.19151 2.68717 2 0 2 10 13.7675 3.4887 1 1 -2 10 728.427 31.444 1 -1 -2 -10 769.019 30.759 3 1 -2 10 771.463 32.476 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1 -11 -3 10 117.672 10.562 5 11 -3 -10 106.160 8.872 3 -11 3 10 85.0441 7.3749 2 11 3 -10 121.098 10.070 3 -11 3 10 147.435 11.812 5 -11 3 10 108.380 9.388 1 10 -3 -10 631.995 26.862 3 -10 -3 10 640.662 28.710 5 -10 -3 10 602.617 27.709 1 -10 3 10 634.612 29.305 5 -10 3 10 530.580 23.913 2 10 3 -10 564.608 22.610 2 -10 3 10 643.074 28.396 1 10 3 -10 625.725 28.466 3 -9 -3 10 351.159 18.221 1 -9 -3 10 359.021 18.532 5 9 -3 -10 340.410 16.872 3 9 3 -10 328.206 13.548 2 -9 3 10 351.884 18.396 1 -9 3 10 321.874 14.569 2 9 3 -10 368.728 18.745 3 -8 -3 10 336.952 17.139 1 8 -3 -10 312.337 15.476 3 8 -3 -10 316.630 17.088 5 -8 -3 10 320.951 16.872 5 -8 3 10 293.391 13.325 2 -8 3 10 333.904 17.444 1 8 3 -10 322.628 12.752 2 8 3 -10 313.820 16.878 3 -7 -3 10 327.763 16.619 5 -7 -3 10 339.413 17.211 1 7 -3 -10 333.769 15.350 3 7 -3 -10 327.064 16.916 5 -7 3 10 310.443 13.458 2 -7 3 10 330.156 17.264 1 7 3 -10 324.082 16.755 3 7 3 -10 316.069 12.967 2 6 -3 -10 3.00642 2.58220 5 -6 -3 10 2.61873 2.86220 1 6 -3 -10 3.65367 2.32973 3 -6 -3 10 0.78615 1.42198 4 -6 -3 10 3.05561 2.70074 5 6 3 -10 0.29886 2.28146 3 -6 3 10 1.55533 1.55251 2 -6 3 10 -1.6039 2.6285 1 6 3 -10 0.29576 1.43558 2 -5 -3 10 1683.68 66.35 1 -5 -3 10 1808.30 65.53 5 5 -3 -10 1786.05 66.04 5 5 -3 -10 1701.32 64.19 3 -5 -3 10 1760.72 70.30 4 5 3 -10 1758.71 61.85 2 5 3 -10 1650.08 65.99 3 -5 3 10 1694.25 66.98 1 -5 3 10 1712.22 61.96 2 -4 -3 10 603.443 25.580 1 4 -3 -10 588.368 23.398 3 -4 -3 10 566.922 24.004 5 4 -3 -10 536.730 24.661 5 -4 3 10 603.026 22.832 2 4 3 -10 542.850 24.821 3 -4 3 10 558.352 25.815 1 4 3 -10 624.103 22.811 2 -3 -3 10 479.363 20.103 5 3 -3 -10 491.140 21.369 5 -3 -3 10 486.947 21.910 1 3 -3 -10 479.060 19.876 3 -3 3 10 469.296 22.281 1 -3 3 10 494.248 19.915 2 3 3 -10 499.986 19.978 2 3 3 -10 487.276 21.599 3 -2 -3 10 1850.01 69.72 1 -2 -3 10 1830.48 66.70 5 2 -3 -10 1815.63 67.47 3 2 -3 -10 1872.96 68.72 5 -2 3 10 1841.39 66.60 2 -2 3 10 1777.82 70.08 1 2 3 -10 1824.91 66.81 2 2 3 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15.949 1 -9 -3 -10 283.417 21.357 4 -9 -3 -10 278.580 17.686 3 -9 -3 -10 295.129 17.547 5 9 3 10 296.048 20.172 2 -9 3 -10 296.643 18.017 3 -10 -3 -10 158.787 16.261 4 -10 -3 -10 138.158 12.760 3 10 -3 10 161.016 15.149 2 -10 -3 -10 157.024 12.884 5 10 3 10 171.659 15.878 2 -10 3 -10 162.631 13.157 3 -11 -3 -10 147.259 16.874 4 11 -3 10 166.923 15.938 2 -11 -3 -10 131.397 12.289 3 -11 -3 -10 130.758 12.526 5 11 3 10 153.173 15.263 2 -11 3 -10 151.348 13.355 3 -12 -3 -10 381.400 22.787 3 -12 -3 -10 324.967 21.552 5 12 -3 10 344.644 24.064 2 12 3 10 383.554 25.028 2 -12 3 -10 328.540 21.457 3 -13 -3 -10 31.8375 8.3675 3 -13 -3 -10 11.6032 7.3678 5 13 -3 10 16.5470 8.0051 2 -13 3 -10 21.0232 7.6203 3 13 3 10 28.2902 8.6674 2 14 -3 10 347.638 25.052 2 -14 -3 -10 343.853 23.719 3 -14 -3 -10 358.822 24.373 5 14 3 10 380.547 26.002 2 -14 3 -10 359.421 23.338 3 15 -3 10 26.3497 10.1731 2 -15 -3 -10 10.8548 8.3377 3 -15 3 -10 23.7438 8.2026 3 15 3 10 10.6335 8.4064 2 -16 -3 -10 247.287 21.396 3 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8.20084 5.78919 1 8 11 -10 4.00784 5.36852 3 -8 11 10 11.7018 6.3055 2 8 11 -10 -0.2700 5.2167 2 7 -11 -10 713.172 34.910 5 -7 -11 10 671.336 33.437 1 -7 -11 10 669.372 32.942 5 7 11 -10 785.034 33.926 2 -7 11 10 666.948 35.000 1 7 11 -10 666.470 33.373 3 -7 11 10 693.601 33.800 2 6 -11 -10 3.38149 5.62119 5 -6 -11 10 1.33713 4.90126 1 6 11 -10 5.29829 5.48167 3 6 11 -10 4.82699 5.03810 2 -6 11 10 4.98911 5.62751 1 -6 11 10 0.66939 5.38202 2 -5 -11 10 525.983 26.722 1 5 -11 -10 522.552 27.028 5 -5 11 10 469.753 26.505 1 5 11 -10 433.438 24.544 3 -5 11 10 498.628 26.375 2 5 11 -10 458.695 25.201 2 -4 -11 10 52.6384 8.3114 1 4 -11 -10 56.8761 8.9413 5 4 11 -10 50.5673 8.2681 2 4 11 -10 33.9406 6.9819 3 -4 11 10 47.8943 8.4480 1 -4 11 10 62.1947 9.2550 2 -3 -11 10 225.326 16.547 1 3 -11 -10 203.861 15.940 5 -3 11 10 229.782 16.284 1 3 11 -10 208.540 15.054 3 -3 11 10 249.730 16.788 2 3 11 -10 244.718 16.577 2 2 -11 -10 27.6478 7.0676 5 -2 -11 10 30.7442 7.2643 1 -2 11 10 26.5136 6.6704 1 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401.666 25.104 1 -7 -11 -10 394.807 25.057 5 -7 11 -10 401.818 27.040 2 7 11 10 417.540 26.910 2 -8 -11 -10 2.49182 6.58836 5 8 -11 10 0.33520 6.66189 1 -8 11 -10 4.65470 8.55121 2 8 11 10 5.63551 7.38659 2 -9 -11 -10 270.839 20.618 5 9 -11 10 268.147 20.748 1 -9 11 -10 287.360 23.289 2 9 11 10 242.167 21.608 2 10 -11 10 9.13059 8.16925 1 -13 -12 10 67.7728 13.9893 5 -12 -12 10 12.2657 9.3629 5 12 -12 -10 28.5656 8.8340 1 12 -12 -10 13.7766 9.9392 5 11 -12 -10 38.3292 10.1321 5 11 -12 -10 25.2174 8.7623 1 -11 -12 10 21.8076 9.1625 5 -11 12 10 23.7481 8.5051 2 -10 -12 10 119.115 13.625 5 10 -12 -10 128.885 14.630 5 -10 12 10 147.681 14.448 2 9 -12 -10 1.71282 7.18484 5 -9 12 10 6.57191 6.70829 2 9 12 -10 15.9024 7.2000 2 8 -12 -10 186.807 16.928 5 -8 -12 10 191.636 15.876 1 -8 12 10 177.230 16.207 1 8 12 -10 159.954 14.498 2 -8 12 10 189.928 16.081 2 7 -12 -10 3.98543 6.41279 5 -7 -12 10 15.0550 6.6501 1 -7 12 10 19.2165 7.4496 2 -7 12 10 3.41267 6.63325 1 7 12 -10 7.02767 6.59768 2 -6 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11.7227 2 9 10 11 50.0477 11.1733 2 10 -10 11 0.56096 7.31559 1 -10 -10 -11 -2.6657 6.6654 5 10 10 11 3.59902 8.23000 2 -10 10 -11 -1.7731 9.4598 2 11 -10 11 75.0356 13.1614 1 15 11 -11 -5.5870 9.3789 3 -14 -11 11 229.360 20.866 5 14 -11 -11 230.703 21.384 5 -14 11 11 287.080 22.150 1 14 11 -11 217.306 19.612 3 13 -11 -11 -3.9605 8.2051 5 -13 -11 11 3.32046 8.91907 5 13 11 -11 1.38530 7.68048 3 -13 11 11 2.54739 7.54203 1 -12 -11 11 321.921 22.476 5 12 -11 -11 282.023 21.926 5 -12 11 11 343.068 23.803 1 12 11 -11 298.195 21.890 3 11 -11 -11 0.77870 6.90475 5 -11 -11 11 2.23291 6.77865 5 11 11 -11 -6.2375 5.5443 3 -11 11 11 -2.1133 6.6598 1 10 -11 -11 217.509 17.676 5 -10 -11 11 175.105 16.184 5 10 11 -11 168.497 15.400 3 -10 11 11 188.034 17.247 1 -10 11 11 181.966 14.977 2 -9 -11 11 4.98057 6.71335 5 9 -11 -11 12.9447 7.2008 5 -9 -11 11 6.12664 6.20645 1 -9 11 11 14.8228 6.6682 1 9 11 -11 7.40341 6.14326 3 -9 11 11 7.10027 6.29130 2 -8 -11 11 46.2561 8.7959 1 8 -11 -11 58.9274 9.7234 5 -8 11 11 67.1920 9.5053 2 -8 11 11 62.8830 10.2248 1 8 11 -11 43.4971 8.8463 3 8 11 -11 46.2025 7.9185 2 -7 -11 11 19.1973 6.6307 1 7 -11 -11 15.3073 7.1327 5 -7 11 11 12.5896 7.0192 1 7 11 -11 12.4300 5.8653 2 7 11 -11 8.65722 6.01271 3 -7 11 11 13.0493 6.1077 2 6 -11 -11 -2.7907 5.4153 5 -6 -11 11 1.09521 5.42030 1 -6 11 11 -5.1463 5.1501 2 -6 11 11 2.75873 5.50248 1 6 11 -11 0.98425 4.89197 2 6 11 -11 -1.7534 5.3380 3 -5 -11 11 37.7426 7.6541 1 5 -11 -11 30.0574 7.6063 5 -5 11 11 30.1356 7.7241 1 5 11 -11 20.4450 6.8708 3 5 11 -11 18.7166 6.4352 2 -5 11 11 40.7672 8.2197 2 4 -11 -11 30.7632 7.8276 5 -4 -11 11 32.4333 7.6368 1 -4 11 11 25.0938 6.8265 1 4 11 -11 46.1378 7.9710 2 -4 11 11 48.5423 8.4999 2 4 11 -11 29.2674 7.2171 3 -3 -11 11 14.5459 6.2982 1 3 -11 -11 14.3453 5.7566 5 -3 11 11 6.36410 5.49342 2 -3 11 11 13.3411 6.1139 1 3 11 -11 13.1120 6.0838 2 3 11 -11 4.92864 5.36769 3 2 -11 -11 567.176 30.263 5 -2 -11 11 606.898 31.156 1 2 11 -11 586.867 30.109 2 2 11 -11 562.755 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6 11 11 76.0585 12.1043 2 -7 -11 -11 6.10765 6.79513 5 7 -11 11 8.15921 7.48720 1 7 11 11 0.23582 7.57677 2 -7 11 -11 11.3474 7.7698 2 -8 -11 -11 13.8365 7.5800 5 8 -11 11 4.22545 7.72277 1 8 11 11 12.5819 8.4889 2 -8 11 -11 6.18243 9.11231 2 9 -11 11 14.2844 8.3225 1 13 -12 -11 142.723 17.134 5 -13 -12 11 163.885 17.683 5 -12 -12 11 6.05557 9.42266 5 12 -12 -11 6.33640 8.99000 5 11 -12 -11 164.576 16.906 5 -11 12 11 164.554 17.193 1 10 -12 -11 9.12586 7.82733 5 -10 12 11 8.36843 7.11258 2 -10 12 11 7.13613 7.72048 1 9 -12 -11 160.394 15.920 5 -9 12 11 115.575 14.641 1 -9 12 11 143.023 14.254 2 -8 -12 11 49.8700 9.4289 1 8 -12 -11 71.8574 11.4820 5 -8 12 11 72.0814 10.8486 2 8 12 -11 48.2185 8.9265 2 -8 12 11 77.7050 11.1107 1 7 -12 -11 21.8818 8.3833 5 -7 -12 11 24.0981 7.6900 1 7 12 -11 20.6613 7.2229 2 -7 12 11 26.3318 8.4453 1 -7 12 11 22.3214 7.8358 2 6 -12 -11 168.351 15.325 5 -6 -12 11 158.208 14.494 1 -6 12 11 158.786 15.178 1 -6 12 11 118.820 13.650 2 6 12 -11 143.751 13.762 2 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165.894 15.051 5 3 -12 11 153.146 15.415 1 -3 12 -11 160.763 16.289 2 3 12 11 160.151 15.809 2 -4 -12 -11 4.19177 7.12309 5 4 -12 11 16.7753 7.9522 1 4 12 11 10.6274 6.8215 2 -4 12 -11 0.38298 7.53055 2 -5 -12 -11 138.660 14.932 5 5 -12 11 140.029 15.119 1 5 12 11 148.491 16.048 2 -5 12 -11 138.445 16.372 2 6 -12 11 61.2303 11.3049 1 -6 -12 -11 48.3385 10.0612 5 6 12 11 62.6601 11.5769 2 -6 12 -11 47.0331 11.8177 2 7 -12 11 18.1669 8.9420 1 -7 -12 -11 25.0616 9.2045 5 7 12 11 13.2330 8.3546 2 -7 12 -11 8.72025 9.79368 2 11 -13 -11 2.70019 9.43232 5 10 -13 -11 63.8960 12.2564 5 -10 13 11 58.3625 11.3299 2 9 -13 -11 91.4636 13.5925 5 9 -13 -11 119.290 14.404 1 -9 13 11 109.723 14.045 2 8 -13 -11 45.4082 10.0087 1 8 -13 -11 28.1318 9.7057 5 -8 13 11 11.3978 8.8103 2 7 -13 -11 173.985 17.162 5 7 -13 -11 175.731 17.047 1 -7 -13 11 178.281 16.372 1 7 13 -11 162.769 15.408 2 -7 13 11 173.730 17.077 2 -6 -13 11 -3.4412 6.1399 1 6 -13 -11 -5.6001 7.1065 5 6 -13 -11 5.71842 7.07058 1 6 13 -11 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12.0140 2 -2 13 -11 65.6724 12.1021 2 -3 -13 -11 4.93032 7.37759 5 3 -13 11 2.19146 7.09349 1 3 13 11 3.78646 7.75108 2 -3 13 -11 4.09034 7.89551 2 4 -13 11 48.4299 10.2088 1 -4 -13 -11 45.1906 10.2150 5 -4 13 -11 27.0065 10.5518 2 4 13 11 25.3970 9.6953 2 8 -14 -11 170.280 17.927 5 -8 14 11 159.580 18.051 2 7 -14 -11 -3.5625 8.5942 5 -7 14 11 7.37465 8.72831 2 6 -14 -11 134.370 16.504 5 -6 -14 11 152.163 15.831 1 6 -14 -11 200.087 18.587 1 -6 14 11 205.436 18.752 2 6 14 -11 161.062 16.190 2 5 -14 -11 28.7499 9.4297 1 5 -14 -11 22.2241 9.6234 5 -5 -14 11 20.2594 8.6392 1 -5 14 11 19.9485 9.2522 2 5 14 -11 15.1200 8.6844 2 -4 -14 11 158.009 16.393 1 4 -14 -11 188.497 17.966 1 4 -14 -11 157.552 16.595 5 4 14 -11 167.789 16.601 2 -4 14 11 182.141 17.902 2 3 -14 -11 80.9913 12.5220 1 -3 -14 11 73.0174 12.0337 1 3 -14 -11 95.6896 13.6647 5 3 14 -11 75.3616 12.5589 2 -3 14 11 110.145 14.193 2 2 -14 -11 71.7143 11.7815 1 -2 -14 11 72.1699 12.3451 1 2 -14 -11 88.7272 13.0809 5 2 14 -11 76.0331 12.5253 2 -2 14 11 65.9993 12.0913 2 1 -14 -11 101.257 14.289 5 -1 -14 11 107.206 14.058 1 -1 14 11 78.5730 12.9723 2 1 14 -11 120.659 14.677 2 0 -14 11 30.9157 9.7840 1 0 -14 -11 17.3117 8.9246 5 0 14 -11 24.2284 9.7308 2 0 14 11 29.8910 9.4545 2 -1 -14 -11 53.3335 11.1796 5 -1 14 -11 46.4305 11.2579 2 21 0 -12 5.81486 8.61333 3 -20 0 12 370.278 25.424 5 20 0 -12 320.328 23.159 3 -19 0 12 4.60057 7.27341 5 19 0 -12 2.27631 6.40424 3 -18 0 12 747.953 38.854 5 18 0 -12 728.659 36.924 3 -17 0 12 -0.0620 5.3866 5 17 0 -12 4.38110 5.10192 3 16 0 -12 378.744 21.971 3 -16 0 12 396.889 24.076 5 -16 0 12 348.504 20.230 1 15 0 -12 -0.2918 4.2806 3 -15 0 12 -3.5114 4.2171 5 -15 0 12 -1.6324 4.1187 1 -14 0 12 26.2534 5.8787 1 -14 0 12 28.0451 7.0648 5 14 0 -12 20.5424 5.5613 3 -13 0 12 0.95907 3.65236 1 -13 0 12 3.43394 4.56810 5 13 0 -12 -2.6368 3.5087 3 12 0 -12 12.1385 4.8652 3 -12 0 12 10.6476 5.0556 5 -12 0 12 7.02766 4.13719 1 -11 0 12 -3.0565 3.6869 5 -11 0 12 -2.2072 3.3381 1 11 0 -12 3.12282 3.47585 3 -10 0 12 1165.65 47.61 1 10 0 -12 1163.46 47.16 3 -10 0 12 1095.28 47.75 5 -9 0 12 -3.3164 2.9587 1 9 0 -12 1.25678 3.16995 3 -9 0 12 -2.6149 2.6905 5 8 0 -12 1931.39 74.84 3 -8 0 12 1962.15 75.42 5 -8 0 12 1907.92 76.10 1 8 0 -12 2004.19 78.73 4 7 0 -12 -3.1830 2.3479 3 7 0 -12 -0.2330 1.9820 4 -7 0 12 0.39365 2.81877 1 -7 0 12 -2.3567 2.7037 5 6 0 -12 2127.93 80.70 3 -6 0 12 2097.66 80.42 5 6 0 -12 2248.75 87.60 4 -6 0 12 2082.11 82.45 1 5 0 -12 -0.0657 2.2848 4 -5 0 12 -0.1441 1.1303 2 -5 0 12 -1.7438 1.1876 2 5 0 -12 -1.2578 2.2616 3 -5 0 12 -1.6330 2.8178 1 4 0 -12 2412.99 88.66 5 -4 0 12 2388.07 84.65 2 4 0 -12 2502.96 99.07 4 -4 0 12 2290.90 91.30 1 4 0 -12 2401.42 89.37 3 3 0 -12 -1.1373 2.7641 4 -3 0 12 0.49183 2.67024 1 -3 0 12 -1.0410 1.7549 2 3 0 -12 2.47772 2.30426 5 3 0 -12 -0.6698 1.8896 3 2 0 -12 1427.44 54.88 3 -2 0 12 1432.36 56.76 1 2 0 -12 1420.14 53.54 5 2 0 -12 1418.96 61.86 4 -2 0 12 1438.57 52.67 2 -1 0 12 1.07676 2.94419 1 1 0 -12 -0.2843 2.5715 4 1 0 -12 -0.1883 1.5214 5 1 0 -12 0.39290 2.30408 3 -1 0 12 -0.1702 2.3904 2 0 0 12 112.045 8.271 2 0 0 -12 87.6417 6.1798 5 0 0 -12 98.4006 7.5123 3 0 0 -12 107.856 9.747 4 0 0 12 111.698 8.907 1 -1 0 -12 -0.7936 3.3928 4 1 0 12 -0.3980 2.9343 1 1 0 12 3.86705 3.36997 2 -1 0 -12 3.48593 2.79337 3 -1 0 -12 -0.3641 1.9275 5 2 0 12 132.337 10.136 1 -2 0 -12 140.632 12.429 4 -2 0 -12 157.460 9.943 3 -2 0 -12 139.361 8.305 5 2 0 12 165.150 11.342 2 3 0 12 1.69721 3.56183 2 -3 0 -12 -0.5688 3.6652 4 3 0 12 2.35306 3.63642 1 -3 0 -12 5.80002 2.97560 3 -3 0 -12 0.71585 2.03620 5 4 0 12 420.267 22.060 2 4 0 12 366.522 19.638 1 -4 0 -12 412.603 24.909 4 -4 0 -12 407.862 19.869 3 -4 0 -12 393.224 17.633 5 -5 0 -12 -0.1322 2.4873 5 -5 0 -12 0.35681 3.29855 3 5 0 12 -0.5749 3.4902 1 -5 0 -12 -2.2531 3.7182 4 5 0 12 0.73362 4.08314 2 -6 0 -12 1086.22 43.00 5 -6 0 -12 1114.06 45.82 3 6 0 12 1114.90 48.29 2 6 0 12 1052.26 44.62 1 -6 0 -12 1120.95 54.21 4 7 0 12 -2.7689 4.0661 1 -7 0 -12 -1.9207 2.8328 5 7 0 12 2.38794 4.79221 2 -7 0 -12 -3.2495 2.9693 3 -8 0 -12 1046.06 43.41 5 8 0 12 1155.44 49.57 2 -8 0 -12 1045.31 46.02 3 -9 0 -12 -5.0544 3.3621 3 9 0 12 -1.8403 5.4544 2 -10 0 -12 396.180 22.909 3 10 0 12 400.174 25.035 2 -11 0 -12 -2.6742 4.6595 3 11 0 12 -3.9036 5.4426 2 -12 0 -12 214.245 16.565 3 12 0 12 212.100 18.330 2 -13 0 -12 2.13430 5.67531 3 13 0 12 -3.2670 7.1843 2 14 0 12 22.5172 9.1500 2 -14 0 -12 13.9018 7.3558 3 15 0 12 -5.5702 8.1228 2 -15 0 -12 -0.0505 7.3904 3 21 -1 -12 186.343 18.270 3 -20 -1 12 3.91606 7.85671 5 20 -1 -12 -5.0460 6.8831 3 -20 1 12 -5.0040 7.4182 5 20 1 -12 -1.0682 7.2024 3 -19 -1 12 271.468 21.121 5 19 -1 -12 298.451 20.906 3 -19 1 12 265.726 21.765 5 19 1 -12 307.308 21.231 3 18 -1 -12 3.32294 6.19335 3 -18 -1 12 18.5641 8.1032 5 18 1 -12 17.4164 7.3812 3 -18 1 12 20.4828 7.7034 5 -17 -1 12 455.478 27.691 5 17 -1 -12 479.171 26.476 3 17 1 -12 461.335 26.366 3 -17 1 12 487.139 28.360 5 16 -1 -12 60.2852 9.1985 3 -16 -1 12 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2 14 371.975 17.487 2 0 2 -14 372.017 17.998 3 -1 -2 -14 281.211 14.140 5 1 -2 14 281.390 15.846 1 -1 -2 -14 259.646 18.246 4 1 -2 14 287.143 16.685 2 -1 -2 -14 254.340 14.250 3 1 2 14 293.659 15.547 2 -1 2 -14 297.511 15.592 3 -1 2 -14 240.989 11.490 5 1 2 14 262.118 16.168 1 -2 -2 -14 32.1011 5.2229 3 -2 -2 -14 50.3433 5.4665 5 2 -2 14 42.0955 7.1858 2 -2 -2 -14 46.0019 7.9825 4 2 -2 14 47.4295 6.5808 1 2 2 14 48.6478 7.0204 1 2 2 14 56.5916 7.0865 2 -2 2 -14 39.5344 5.9752 3 -3 -2 -14 293.266 16.013 3 3 -2 14 274.155 17.799 2 -3 -2 -14 282.965 14.946 5 -3 -2 -14 303.307 20.518 4 3 -2 14 254.241 15.937 1 -3 2 -14 299.347 16.438 3 3 2 14 315.015 17.819 2 3 2 14 291.918 16.874 1 4 -2 14 -0.8745 4.3600 2 -4 -2 -14 3.44109 3.15377 5 4 -2 14 3.81078 3.99515 1 -4 -2 -14 2.10181 3.61058 3 -4 -2 -14 1.76826 4.64664 4 4 2 14 1.22514 4.01058 2 4 2 14 3.40232 4.16289 1 -4 2 -14 5.97126 3.60335 3 -5 -2 -14 620.158 27.057 5 -5 -2 -14 606.199 28.027 3 5 -2 14 589.324 27.810 1 -5 -2 -14 583.620 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7 -14 257.697 17.810 3 6 7 14 284.624 19.955 2 -7 -7 -14 120.529 12.466 5 7 -7 14 126.665 15.418 2 -7 -7 -14 154.774 17.485 4 7 -7 14 131.297 13.088 1 -7 7 -14 144.825 13.402 3 7 7 14 143.866 15.071 2 8 -7 14 105.579 14.524 2 8 -7 14 97.0773 12.0683 1 -8 -7 -14 97.3653 11.6844 5 -8 -7 -14 102.234 15.322 4 8 7 14 88.7113 13.4842 2 -8 7 -14 104.012 12.000 3 9 -7 14 133.180 13.763 1 9 -7 14 101.650 14.889 2 -9 -7 -14 121.741 17.533 4 -9 -7 -14 123.701 13.850 5 -9 7 -14 147.084 14.354 3 9 7 14 130.648 15.602 2 -10 -7 -14 -0.2797 6.7343 5 10 -7 14 -2.2681 9.0146 2 10 7 14 0.68228 8.67970 2 -10 7 -14 -1.2877 6.7597 3 -11 -7 -14 81.8721 12.6786 5 11 -7 14 105.455 16.408 2 11 7 14 64.5644 13.7256 2 -11 7 -14 96.6357 12.9973 3 -12 -7 -14 35.5665 11.4876 5 17 -8 -14 -2.6739 8.1725 5 -17 -8 14 -7.1338 8.1079 5 17 8 -14 11.5581 8.6406 3 -17 8 14 4.83744 7.64621 1 -16 -8 14 108.200 14.816 5 16 -8 -14 91.4962 14.3686 5 -16 8 14 109.873 14.200 1 16 8 -14 99.0141 13.7716 3 15 -8 -14 62.5608 11.5402 5 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14 27.2702 7.1961 1 -6 9 14 11.6271 5.6392 2 6 9 -14 18.0526 5.6107 2 5 -9 -14 503.917 26.984 5 -5 -9 14 460.482 26.406 1 -5 9 14 530.632 25.795 2 5 9 -14 476.061 24.697 2 5 9 -14 531.338 26.717 3 -5 9 14 524.642 27.693 1 4 -9 -14 6.36986 4.97978 5 -4 -9 14 6.92973 4.71202 1 4 9 -14 -0.8888 4.8545 3 -4 9 14 11.8582 5.7143 1 -4 9 14 11.9151 5.4492 2 4 9 -14 9.75661 5.40956 2 -3 -9 14 663.836 32.919 1 3 -9 -14 651.209 32.169 5 3 9 -14 657.857 31.286 2 3 9 -14 660.797 31.894 3 -3 9 14 658.943 32.399 1 -3 9 14 639.920 31.141 2 2 -9 -14 79.6781 10.0016 5 -2 -9 14 95.0047 10.3994 1 2 9 -14 62.7150 8.7263 3 -2 9 14 62.4685 8.6746 1 2 9 -14 71.4712 9.4455 2 -2 9 14 91.1130 9.8582 2 1 -9 -14 345.519 20.904 5 -1 -9 14 390.911 22.128 1 -1 9 14 338.002 19.891 1 1 9 -14 346.172 20.530 3 -1 9 14 316.361 19.662 2 1 9 -14 342.872 21.009 2 0 -9 -14 64.8601 9.3001 5 0 -9 14 60.5121 9.4185 1 0 9 14 74.8217 8.8283 1 0 9 -14 57.7479 8.9675 2 0 9 -14 73.2048 9.2376 3 0 9 14 68.8162 9.2933 2 1 -9 14 57.9349 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1 -28 12.4011 8.9275 3 -11 -1 28 224.436 20.016 1 11 -1 -28 166.714 16.535 3 11 1 -28 213.544 18.533 3 -11 1 28 212.295 19.211 1 -10 -1 28 -5.6813 7.6168 1 10 -1 -28 -7.5453 6.8273 3 10 1 -28 -5.6023 6.9566 3 -10 1 28 2.17526 8.41969 1 9 -1 -28 292.362 21.209 3 -9 -1 28 286.447 23.567 1 -9 1 28 315.885 24.197 1 9 1 -28 346.916 23.014 3 8 -1 -28 0.85350 7.00789 3 -8 -1 28 -4.7275 7.7164 1 -8 1 28 2.23514 8.14681 1 8 1 -28 5.06041 7.19172 3 -7 -1 28 215.503 19.613 1 7 -1 -28 196.581 17.613 3 7 1 -28 204.768 17.765 3 -7 1 28 204.183 19.792 1 -6 -1 28 19.8765 9.6930 1 6 -1 -28 -1.5551 6.9732 3 6 1 -28 16.2543 7.9896 3 -6 1 28 6.59840 8.57499 1 5 -1 -28 130.692 14.357 3 -5 -1 28 127.537 16.657 1 5 1 -28 146.308 15.038 3 -5 1 28 156.525 17.534 1 -4 -1 28 52.9264 12.3053 1 4 -1 -28 37.7798 9.7294 3 -4 1 28 55.8362 12.4870 1 4 1 -28 57.3851 10.5496 3 -3 -1 28 52.0286 11.7449 1 3 -1 -28 24.4866 8.9388 3 3 1 -28 23.2631 8.8775 3 -3 1 28 36.8371 11.2554 1 2 -1 -28 37.9494 9.6448 3 -2 -1 28 25.4984 11.0192 1 -2 1 28 24.1249 10.6298 1 2 1 -28 24.1402 9.1241 3 -1 -1 28 -1.9180 9.9333 1 1 -1 -28 -5.3919 7.4190 3 1 1 -28 -2.8105 7.1991 3 -1 1 28 5.49531 9.47556 1 0 -1 28 17.8289 11.6524 1 0 -1 -28 35.0880 10.9614 3 13 -2 -28 12.1460 8.8936 5 12 -2 -28 35.3430 10.8045 5 12 2 -28 55.5675 11.2822 3 -11 -2 28 52.8072 11.3763 1 11 -2 -28 57.0293 11.4815 5 11 2 -28 38.7909 10.3785 3 -11 2 28 54.6673 12.1018 1 -10 -2 28 148.121 17.371 1 10 -2 -28 117.403 14.210 5 -10 2 28 143.156 16.804 1 10 2 -28 140.610 15.525 3 -9 -2 28 12.0612 9.2319 1 9 2 -28 10.1005 8.1009 3 -9 2 28 11.8486 9.1578 1 -8 -2 28 265.341 22.385 1 8 2 -28 294.761 21.263 3 -8 2 28 260.870 21.957 1 7 -2 -28 -1.4008 7.2301 3 -7 -2 28 0.17418 7.78599 1 7 2 -28 -3.2335 7.0290 3 -7 2 28 2.98710 8.00917 1 -6 -2 28 97.4365 14.7005 1 6 -2 -28 73.2742 11.7865 3 -6 2 28 93.7736 14.7032 1 6 2 -28 79.1308 11.4520 3 -5 -2 28 101.886 15.085 1 5 -2 -28 86.1899 12.6351 3 -5 2 28 108.418 15.969 1 5 2 -28 108.369 13.343 3 -4 -2 28 30.8345 11.0785 1 4 -2 -28 27.9846 9.1417 3 -4 2 28 42.6952 12.0482 1 4 2 -28 42.2972 9.6956 3 3 -2 -28 64.7412 10.8149 3 -3 -2 28 74.3110 13.7342 1 3 2 -28 73.0005 11.9555 3 -3 2 28 68.7354 13.4841 1 2 -2 -28 11.1838 7.7441 3 -2 -2 28 2.03174 8.62561 1 -2 2 28 7.9294 10.6570 1 2 2 -28 5.34425 7.83618 3 -1 -2 28 79.2478 14.8461 1 1 -2 -28 76.7419 12.0585 3 1 2 -28 86.5284 13.0571 3 0 -2 -28 10.6126 8.4781 3 0 -2 28 16.7501 11.0710 1 12 -3 -28 57.2220 11.5334 5 11 -3 -28 48.7278 10.7560 5 11 3 -28 60.3197 11.6422 3 10 -3 -28 35.4997 9.5622 5 -10 -3 28 30.8142 10.7059 1 -10 3 28 33.2465 11.1846 1 10 3 -28 33.6640 10.1851 3 9 -3 -28 150.665 15.692 5 -9 -3 28 164.238 18.139 1 9 3 -28 151.659 16.234 3 -9 3 28 170.332 18.566 1 8 -3 -28 6.71253 7.40620 5 -8 -3 28 4.09845 8.46827 1 8 3 -28 -10.633 6.414 3 -8 3 28 -1.4559 8.2067 1 -7 -3 28 70.3247 13.3839 1 7 3 -28 101.146 13.279 3 -7 3 28 96.3359 14.8946 1 -6 -3 28 21.2917 10.3161 1 -6 3 28 51.9221 12.2777 1 6 3 -28 16.1256 8.0773 3 -5 -3 28 37.9859 11.3541 1 5 3 -28 39.8660 9.4041 3 -5 3 28 43.4082 11.7420 1 -4 -3 28 174.497 18.630 1 4 3 -28 148.703 15.653 3 -4 3 28 140.277 18.091 1 -3 -3 28 -4.5433 8.4773 1 3 3 -28 2.61514 6.54941 3 -3 3 28 6.91794 9.53274 1 -2 -3 28 85.1604 14.4107 1 -2 3 28 69.7190 13.5562 1 -1 -3 28 5.44831 9.82149 1 0 -3 28 122.829 16.750 1 11 -4 -28 29.8853 10.2818 5 10 -4 -28 15.7670 8.7398 5 9 -4 -28 -3.3292 8.2349 5 9 4 -28 3.38243 7.78401 3 -9 4 28 -12.692 8.381 1 8 -4 -28 58.2052 11.5176 5 -8 -4 28 57.6952 12.9403 1 -8 4 28 100.744 15.516 1 8 4 -28 86.1579 12.4670 3 7 -4 -28 10.8544 8.0624 5 -7 -4 28 9.58921 9.50887 1 7 4 -28 28.7657 9.3659 3 -7 4 28 12.4611 9.9028 1 -6 -4 28 53.4889 12.2713 1 -6 4 28 33.5421 11.5353 1 6 4 -28 15.8331 7.4501 3 -5 -4 28 42.8790 12.1331 1 -5 4 28 52.3792 13.0970 1 5 4 -28 50.4074 9.8495 3 -4 -4 28 9.80740 9.89723 1 -4 4 28 11.5035 11.2823 1 -3 -4 28 169.815 19.310 1 -3 4 28 158.834 19.390 1 9 -5 -28 -5.7277 7.5231 5 8 -5 -28 -6.5083 8.2647 5 7 -5 -28 2.54884 8.44147 5 -7 5 28 6.8567 10.1682 1 6 -5 -28 69.6163 12.1238 5 -6 5 28 52.9205 13.9226 1 -5 5 28 -18.121 8.815 1 -4 5 28 139.564 18.205 1 12 0 -29 -1.8719 8.2017 3 11 0 -29 179.450 17.677 3 10 0 -29 -6.3946 8.2390 3 9 0 -29 6.90149 8.02433 3 -9 0 29 9.71344 8.83984 1 8 0 -29 10.5721 7.9655 3 -8 0 29 1.68977 7.87323 1 7 0 -29 -2.6883 7.1781 3 -7 0 29 5.05176 8.22957 1 -6 0 29 0.79081 8.87514 1 6 0 -29 -3.7218 7.2695 3 -5 0 29 49.2361 12.0709 1 5 0 -29 60.4799 11.4985 3 4 0 -29 -3.5529 7.5850 3 -4 0 29 -9.4493 8.6736 1 -3 0 29 170.909 19.198 1 3 0 -29 192.086 17.671 3 2 0 -29 -2.0145 8.0230 3 -2 0 29 2.75623 9.77153 1 11 -1 -29 -1.1371 9.0623 3 11 1 -29 5.24212 8.78841 3 10 -1 -29 21.0194 9.7630 3 10 1 -29 29.2406 9.8650 3 9 -1 -29 35.6491 10.0672 3 9 1 -29 51.3344 10.9543 3 -9 1 29 38.6862 11.6540 1 -8 -1 29 15.8224 9.4058 1 8 -1 -29 0.62581 7.42298 3 -8 1 29 10.9678 9.5727 1 8 1 -29 -2.0364 7.5364 3 -7 -1 29 72.2268 12.7777 1 7 -1 -29 38.2765 9.6639 3 7 1 -29 63.8900 11.2078 3 -7 1 29 59.3190 12.7793 1 -6 -1 29 14.0321 10.1170 1 6 -1 -29 13.3103 8.0263 3 6 1 -29 14.9313 7.8696 3 -6 1 29 5.97595 9.44305 1 -5 -1 29 24.6223 10.4039 1 5 -1 -29 30.9649 9.4447 3 -5 1 29 42.5725 12.1046 1 5 1 -29 35.3316 9.7553 3 -4 -1 29 103.141 15.463 1 4 -1 -29 116.925 14.453 3 4 1 -29 102.163 14.065 3 -4 1 29 93.7524 15.5276 1 -3 -1 29 15.1096 9.9872 1 3 -1 -29 7.88148 8.02104 3 3 1 -29 1.68637 7.75738 3 -3 1 29 0.48102 9.60356 1 2 -1 -29 197.573 18.243 3 -2 -1 29 228.644 21.312 1 -2 1 29 187.115 20.623 1 10 2 -29 65.7276 11.8320 3 9 2 -29 22.1756 9.0877 3 8 2 -29 56.3931 11.2393 3 -8 2 29 82.9324 14.1089 1 -7 -2 29 14.0288 9.5858 1 7 2 -29 3.64211 7.23584 3 -7 2 29 -4.3906 8.3635 1 -6 -2 29 88.1748 14.8027 1 6 2 -29 99.8185 13.1474 3 -6 2 29 117.338 16.109 1 -5 -2 29 26.9619 10.6783 1 5 2 -29 34.2031 9.7897 3 -5 2 29 38.9869 12.2089 1 -4 -2 29 41.3041 11.9974 1 -4 2 29 56.4719 12.7662 1 -3 2 29 105.989 15.647 1 -2 2 29 6.58903 9.68888 1 10 -3 -29 89.3834 13.6496 5 -6 3 29 48.5739 12.4184 1 -5 3 29 168.158 18.969 1 -4 3 29 68.9855 14.2220 1 -3 3 29 15.1594 11.7287 1 9 -4 -29 16.3588 9.6284 5 9 0 -30 -2.8033 8.6177 3 8 0 -30 173.072 17.400 3 7 0 -30 -0.0156 8.1338 3 6 0 -30 281.315 21.780 3 8 -1 -30 -2.6728 8.5554 3 7 -1 -30 154.923 16.063 3 6 -1 -30 -6.2166 7.5115 3 5 -1 -30 140.963 16.148 3 0 0 0 0.00 0.00 0 ; _shelx_hkl_checksum 38889 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn W1 W 0.03588(2) 0.45204(2) 0.22477(2) 0.01494(4) Uani 1 1 d . Cl1 Cl 0.04313(6) 0.24816(7) 0.15628(4) 0.02570(14) Uani 1 1 d . Cl2 Cl 0.09886(6) 0.65731(7) 0.29334(4) 0.02369(13) Uani 1 1 d . O1 O 0.20687(16) 0.3866(2) 0.28855(11) 0.0217(4) Uani 1 1 d . O2 O 0.15210(16) 0.5273(2) 0.15827(11) 0.0207(4) Uani 1 1 d . N1 N -0.0142(2) 0.3801(3) 0.29091(14) 0.0215(5) Uani 1 1 d . N2 N -0.07392(18) 0.5215(2) 0.15487(13) 0.0168(4) Uani 1 1 d . C1 C 0.2372(3) 0.3622(4) 0.36852(18) 0.0349(8) Uani 1 1 d . H1A H 0.243438 0.449462 0.395159 0.041(7) Uiso 1 1 d GR H1B H 0.305206 0.314731 0.385459 0.041(7) Uiso 1 1 d GR H1C H 0.183536 0.305793 0.379439 0.041(7) Uiso 1 1 d GR C2 C 0.2881(2) 0.4576(3) 0.26907(18) 0.0266(6) Uani 1 1 d . H2A H 0.356125 0.408658 0.289448 0.032 Uiso 1 1 d R H2B H 0.296995 0.550908 0.290438 0.032 Uiso 1 1 d R C3 C 0.2547(2) 0.4635(4) 0.18456(18) 0.0276(6) Uani 1 1 d . H3A H 0.306085 0.517228 0.168347 0.033 Uiso 1 1 d R H3B H 0.251035 0.370328 0.163407 0.033 Uiso 1 1 d R C4 C 0.1119(3) 0.5276(3) 0.07690(16) 0.0265(6) Uani 1 1 d . H4A H 0.103048 0.433443 0.058333 0.033(6) Uiso 1 1 d GR H4B H 0.161689 0.575223 0.057173 0.033(6) Uiso 1 1 d GR H4C H 0.043579 0.574423 0.059853 0.033(6) Uiso 1 1 d GR C5 C -0.0925(2) 0.3474(3) 0.32610(17) 0.0241(6) Uani 1 1 d . H5 H -0.160734 0.391051 0.296151 0.029 Uiso 1 1 d R C6 C -0.1086(3) 0.1942(4) 0.3256(2) 0.0404(9) Uani 1 1 d . H6A H -0.131956 0.161009 0.273370 0.049(7) Uiso 1 1 d GR H6B H -0.162296 0.172759 0.349050 0.049(7) Uiso 1 1 d GR H6C H -0.042006 0.149819 0.354060 0.049(7) Uiso 1 1 d GR C7 C -0.0576(3) 0.4070(4) 0.4059(2) 0.0358(8) Uani 1 1 d . H7A H 0.008000 0.362924 0.436509 0.042(7) Uiso 1 1 d GR H7B H -0.112630 0.391065 0.428848 0.042(7) Uiso 1 1 d GR H7C H -0.045779 0.505335 0.403469 0.042(7) Uiso 1 1 d GR C8 C -0.1657(2) 0.5607(3) 0.09874(15) 0.0159(5) Uani 1 1 d . C9 C -0.1699(2) 0.6929(3) 0.06721(15) 0.0190(5) Uani 1 1 d . C10 C -0.2574(2) 0.7277(3) 0.00580(16) 0.0237(6) Uani 1 1 d . H10 H -0.260874 0.815076 -0.016798 0.028 Uiso 1 1 d R C11 C -0.3405(2) 0.6351(4) -0.02307(17) 0.0261(6) Uani 1 1 d . H11 H -0.399198 0.658954 -0.065755 0.031 Uiso 1 1 d R C12 C -0.3368(2) 0.5086(3) 0.01077(17) 0.0239(6) Uani 1 1 d . H12 H -0.394465 0.447660 -0.008463 0.029 Uiso 1 1 d R C13 C -0.2508(2) 0.4684(3) 0.07230(15) 0.0181(5) Uani 1 1 d . C14 C -0.0830(2) 0.7953(3) 0.10317(16) 0.0206(5) Uani 1 1 d . H14 H -0.016268 0.742918 0.126364 0.025 Uiso 1 1 d R C15 C -0.1083(3) 0.8702(3) 0.16724(18) 0.0265(6) Uani 1 1 d . H15A H -0.176602 0.916439 0.146879 0.032(6) Uiso 1 1 d GR H15B H -0.053172 0.937710 0.189908 0.032(6) Uiso 1 1 d GR H15C H -0.111432 0.804269 0.205799 0.032(6) Uiso 1 1 d GR C16 C -0.0632(3) 0.8966(3) 0.04703(19) 0.0292(7) Uani 1 1 d . H16A H -0.048391 0.846406 0.006343 0.032(6) Uiso 1 1 d GR H16B H -0.002693 0.954397 0.073133 0.032(6) Uiso 1 1 d GR H16C H -0.125902 0.953655 0.025662 0.032(6) Uiso 1 1 d GR C17 C -0.2500(2) 0.3304(3) 0.10874(16) 0.0208(5) Uani 1 1 d . H17 H -0.184415 0.324590 0.153564 0.025 Uiso 1 1 d R C18 C -0.2465(3) 0.2149(3) 0.05461(19) 0.0310(7) Uani 1 1 d . H18A H -0.309877 0.218591 0.009866 0.034(6) Uiso 1 1 d GR H18B H -0.243742 0.126958 0.080076 0.034(6) Uiso 1 1 d GR H18C H -0.183707 0.225175 0.039209 0.034(6) Uiso 1 1 d GR C19 C -0.3443(3) 0.3124(4) 0.1368(2) 0.0341(7) Uani 1 1 d . H19A H -0.344758 0.386112 0.172046 0.050(7) Uiso 1 1 d GR H19B H -0.338680 0.224352 0.162685 0.050(7) Uiso 1 1 d GR H19C H -0.409759 0.314994 0.093766 0.050(7) Uiso 1 1 d GR loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 W1 0.01411(5) 0.01479(5) 0.01551(5) 0.00104(4) 0.00425(4) -0.00024(4) Cl1 0.0225(3) 0.0186(3) 0.0319(4) -0.0066(3) 0.0034(3) 0.0018(3) Cl2 0.0249(3) 0.0208(3) 0.0235(3) -0.0061(3) 0.0053(3) -0.0021(3) O1 0.0173(9) 0.0254(10) 0.0195(9) 0.0025(8) 0.0020(8) 0.0011(8) O2 0.0174(9) 0.0271(10) 0.0193(9) 0.0017(8) 0.0081(8) 0.0016(8) N1 0.0225(11) 0.0213(12) 0.0218(11) 0.0031(9) 0.0086(9) -0.0005(9) N2 0.0160(10) 0.0162(10) 0.0170(10) 0.0000(8) 0.0039(8) 0.0009(8) C1 0.0302(16) 0.048(2) 0.0205(14) 0.0088(14) 0.0003(12) 0.0040(15) C2 0.0154(12) 0.0332(16) 0.0291(15) -0.0009(13) 0.0044(11) -0.0004(11) C3 0.0161(13) 0.0385(18) 0.0297(15) 0.0048(13) 0.0097(12) 0.0046(12) C4 0.0299(15) 0.0345(17) 0.0169(13) 0.0020(12) 0.0099(12) 0.0053(13) C5 0.0231(14) 0.0281(15) 0.0231(13) 0.0070(12) 0.0104(11) 0.0018(12) C6 0.049(2) 0.0338(18) 0.043(2) 0.0061(16) 0.0220(18) -0.0111(17) C7 0.0341(18) 0.046(2) 0.0310(17) 0.0033(15) 0.0160(15) 0.0019(16) C8 0.0142(11) 0.0198(12) 0.0147(11) 0.0004(9) 0.0061(9) 0.0037(9) C9 0.0201(13) 0.0215(13) 0.0177(12) 0.0022(10) 0.0092(10) 0.0051(10) C10 0.0238(14) 0.0271(15) 0.0214(13) 0.0058(11) 0.0089(11) 0.0092(11) C11 0.0197(13) 0.0376(17) 0.0195(13) 0.0035(12) 0.0042(11) 0.0080(12) C12 0.0182(13) 0.0317(15) 0.0205(13) -0.0025(12) 0.0046(11) 0.0011(11) C13 0.0160(12) 0.0229(13) 0.0161(11) -0.0031(10) 0.0060(10) 0.0014(10) C14 0.0227(13) 0.0170(12) 0.0242(13) 0.0032(10) 0.0106(11) 0.0013(10) C15 0.0292(15) 0.0260(15) 0.0275(15) -0.0021(12) 0.0134(12) 0.0017(12) C16 0.0381(18) 0.0227(14) 0.0314(16) 0.0055(12) 0.0177(14) -0.0012(13) C17 0.0193(12) 0.0222(13) 0.0204(13) -0.0015(10) 0.0057(10) -0.0035(10) C18 0.0367(18) 0.0248(15) 0.0317(16) -0.0051(13) 0.0115(14) -0.0004(13) C19 0.0313(17) 0.0370(18) 0.0395(19) 0.0048(15) 0.0191(15) -0.0036(14) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' W W -0.8490 6.8722 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle Cl1 W1 O2 80.37(5) Cl2 W1 Cl1 157.30(3) Cl2 W1 O2 81.06(5) O1 W1 Cl1 80.66(6) O1 W1 Cl2 80.70(6) O1 W1 O2 69.57(7) N1 W1 Cl1 97.78(9) N1 W1 Cl2 96.30(9) N1 W1 O1 93.89(10) N1 W1 O2 163.45(10) N1 W1 N2 105.26(11) N2 W1 Cl1 95.46(8) N2 W1 Cl2 97.89(8) N2 W1 O1 160.82(9) N2 W1 O2 91.29(9) C1 O1 W1 118.80(19) C2 O1 W1 116.24(17) C2 O1 C1 111.4(2) C3 O2 W1 113.36(17) C4 O2 W1 117.74(17) C4 O2 C3 110.4(2) C5 N1 W1 157.1(2) C8 N2 W1 173.1(2) O1 C2 C3 107.2(2) O2 C3 C2 107.5(2) N1 C5 C6 109.9(3) N1 C5 C7 108.9(3) C6 C5 C7 112.5(3) N2 C8 C9 118.3(2) N2 C8 C13 120.2(2) C13 C8 C9 121.4(2) C8 C9 C14 119.9(2) C10 C9 C8 118.5(3) C10 C9 C14 121.5(3) C9 C10 C11 120.7(3) C12 C11 C10 119.8(3) C11 C12 C13 121.8(3) C8 C13 C17 121.9(2) C12 C13 C8 117.6(3) C12 C13 C17 120.5(3) C9 C14 C15 109.2(2) C9 C14 C16 113.8(2) C16 C14 C15 111.0(2) C13 C17 C18 111.1(2) C13 C17 C19 112.0(3) C19 C17 C18 110.4(3) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance W1 Cl1 2.3935(7) W1 Cl2 2.3882(7) W1 O1 2.304(2) W1 O2 2.405(2) W1 N1 1.738(2) W1 N2 1.757(2) O1 C1 1.438(4) O1 C2 1.436(4) O2 C3 1.444(4) O2 C4 1.441(3) N1 C5 1.445(4) N2 C8 1.387(3) C2 C3 1.498(4) C5 C6 1.517(5) C5 C7 1.528(5) C8 C9 1.417(4) C8 C13 1.414(4) C9 C10 1.391(4) C9 C14 1.519(4) C10 C11 1.402(5) C11 C12 1.386(5) C12 C13 1.395(4) C13 C17 1.513(4) C14 C15 1.535(4) C14 C16 1.530(4) C17 C18 1.531(4) C17 C19 1.528(4)