#------------------------------------------------------------------------------ #$Date: 2019-11-10 15:31:44 +0200 (Sun, 10 Nov 2019) $ #$Revision: 225953 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/58/4515853.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4515853 loop_ _publ_author_name 'Chapovetsky, Alon' 'Welborn, Matthew' 'Luna, John M.' 'Haiges, Ralf' 'Miller, 3rd, Thomas F' 'Marinescu, Smaranda C.' _publ_section_title ; Pendant Hydrogen-Bond Donors in Cobalt Catalysts Independently Enhance CO2 Reduction. ; _journal_issue 3 _journal_name_full 'ACS central science' _journal_page_first 397 _journal_page_last 404 _journal_paper_doi 10.1021/acscentsci.7b00607 _journal_volume 4 _journal_year 2018 _chemical_formula_moiety 'C22 H22 Co N8 O, 2(B F4), C3 H6 O, H2 O' _chemical_formula_sum 'C25 H30 B2 Co F8 N8 O3' _chemical_formula_weight 723.12 _chemical_name_common Alon082916 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens mixed _cell_angle_alpha 106.688(8) _cell_angle_beta 101.505(8) _cell_angle_gamma 100.107(8) _cell_formula_units_Z 2 _cell_length_a 11.1267(14) _cell_length_b 11.9052(15) _cell_length_c 12.2051(16) _cell_measurement_reflns_used 4309 _cell_measurement_temperature 100.(2) _cell_measurement_theta_max 67.1706 _cell_measurement_theta_min 4.0065 _cell_volume 1470.1(3) _computing_cell_refinement 'APEX3 v2016.1-0 (Bruker AXS, 2016)' _computing_data_collection 'Bruker Instrument Service v2012.12.0.3 (Bruker AXS, 2012' _computing_data_reduction 'SAINT V8.37A (Bruker AXS, 2013)' _computing_molecular_graphics 'shelXle (C.B. Huebschle, rev 758)' _computing_publication_material 'SHELXTL XL 2014/7 (Bruker AXS, 2014)' _computing_structure_refinement 'SHELXTL XL 2014/7 (Bruker AXS, 2014)' _computing_structure_solution 'SHELXTL XT 2014/4 (Bruker AXS, 2014)' _diffrn_ambient_temperature 100.(2) _diffrn_detector_area_resol_mean 8.3333 _diffrn_measured_fraction_theta_full 0.984 _diffrn_measured_fraction_theta_max 0.984 _diffrn_measurement_device_type 'Bruker APEX II CCD' _diffrn_measurement_method 'omega- and phi-scans' _diffrn_radiation_monochromator 'multi-layer optics' _diffrn_radiation_type 'CuK\a ' _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.1232 _diffrn_reflns_av_unetI/netI 0.1893 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 29257 _diffrn_reflns_theta_full 68.22 _diffrn_reflns_theta_max 68.22 _diffrn_reflns_theta_min 3.92 _diffrn_source 'IuS microsource' _exptl_absorpt_coefficient_mu 5.446 _exptl_absorpt_correction_T_max 0.81 _exptl_absorpt_correction_T_min 0.64 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS 2014/5 (Bruker AXS, 2014)' _exptl_crystal_colour 'clear light orange-brown' _exptl_crystal_density_diffrn 1.634 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prism _exptl_crystal_F_000 738 _exptl_crystal_size_max 0.090 _exptl_crystal_size_mid 0.070 _exptl_crystal_size_min 0.040 _refine_diff_density_max 1.270 _refine_diff_density_min -1.364 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.005 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 449 _refine_ls_number_reflns 5297 _refine_ls_number_restraints 502 _refine_ls_restrained_S_all 0.983 _refine_ls_R_factor_all 0.2020 _refine_ls_R_factor_gt 0.0894 _refine_ls_shift/su_max 0.005 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1518P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2097 _refine_ls_wR_factor_ref 0.2724 _reflns_number_gt 2323 _reflns_number_total 5297 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file oc7b00607_si_003.cif _cod_data_source_block Alon082916 _cod_database_code 4515853 _shelx_res_file ; combined.res created by SHELXL-2014/7 TITL first_a.res in P-1 CELL 1.54178 11.1267 11.9052 12.2051 106.688 101.505 100.107 ZERR 2.000 0.0014 0.0015 0.0016 0.008 0.008 0.008 LATT 1 SFAC C H B N F CO O UNIT 50 60 4 16 16 2 6 TEMP -173.140 L.S. 10 BOND $H SHEL 999 0.83 SADI B2 F5 B2 F6 B2 F7 B2 F8 LIST 4 FMAP 2 RIGU ACTA SIZE 0.040 0.070 0.090 PLAN 5 EADP F5 F6 F7 F8 F5A F6A F7A F8A F5B F6B F7B F8B SUMP 1.0 0.001 1.0 2 1.0 3 1.0 4 DFIX 0.95 O1 H1W O1 H2W O2 H3W O2 H4W DFIX 1.515 H1W H2W H3W H4W WGHT 0.151800 FVAR 0.60558 0.50613 0.29612 0.19782 MOLE 1 C1 1 0.728570 0.496190 0.158632 11.00000 0.03333 0.02462 = 0.02701 0.00933 0.00998 0.00273 C2 1 0.680365 0.401098 0.054155 11.00000 0.03396 0.03158 = 0.03044 0.01189 0.00915 0.00547 AFIX 43 H2 2 0.734790 0.373335 0.007323 11.00000 -1.20000 AFIX 0 C3 1 0.552788 0.345968 0.017333 11.00000 0.04019 0.02903 = 0.02937 0.01012 0.00532 0.00045 AFIX 43 H3 2 0.518503 0.279603 -0.054579 11.00000 -1.20000 AFIX 0 C4 1 0.474950 0.388824 0.086893 11.00000 0.02775 0.03234 = 0.03372 0.01369 0.00437 -0.00076 AFIX 43 H4 2 0.386979 0.351293 0.064835 11.00000 -1.20000 AFIX 0 C5 1 0.528873 0.487165 0.188639 11.00000 0.02883 0.02472 = 0.03255 0.01464 0.00701 -0.00197 C6 1 0.338590 0.452203 0.257694 11.00000 0.03348 0.02906 = 0.03743 0.01328 0.01530 0.00235 AFIX 137 H6A 2 0.275410 0.437532 0.183296 11.00000 -1.50000 H6B 2 0.305605 0.487547 0.324887 11.00000 -1.50000 H6C 2 0.356891 0.375482 0.260982 11.00000 -1.50000 AFIX 0 C7 1 0.447420 0.657463 0.276345 11.00000 0.03089 0.03219 = 0.02527 0.01041 0.00747 0.00219 C8 1 0.333986 0.683904 0.245740 11.00000 0.03092 0.03997 = 0.03846 0.01666 0.00575 0.00906 AFIX 43 H8 2 0.257215 0.623030 0.222119 11.00000 -1.20000 AFIX 0 C9 1 0.332207 0.801107 0.249570 11.00000 0.03858 0.03801 = 0.03193 0.01171 0.00567 0.01095 AFIX 43 H9 2 0.254552 0.821434 0.225912 11.00000 -1.20000 AFIX 0 C10 1 0.445004 0.887039 0.288258 11.00000 0.03740 0.03499 = 0.03231 0.01401 0.00833 0.00883 AFIX 43 H10 2 0.446045 0.967992 0.291849 11.00000 -1.20000 AFIX 0 C11 1 0.557422 0.855830 0.322101 11.00000 0.03667 0.03118 = 0.02768 0.01502 0.00579 0.00679 C12 1 0.765784 0.958935 0.462455 11.00000 0.03060 0.03368 = 0.02851 0.01765 0.01332 0.00211 C13 1 0.824753 1.074633 0.538388 11.00000 0.03350 0.03400 = 0.03720 0.01416 0.01168 0.00261 AFIX 43 H13 2 0.802398 1.142474 0.521485 11.00000 -1.20000 AFIX 0 C14 1 0.915779 1.090227 0.638262 11.00000 0.03675 0.03429 = 0.03940 0.01239 0.01183 -0.00103 AFIX 43 H14 2 0.958262 1.169395 0.691375 11.00000 -1.20000 AFIX 0 C15 1 0.945855 0.990648 0.661793 11.00000 0.03162 0.03806 = 0.03064 0.00927 0.00551 -0.00089 AFIX 43 H15 2 1.006578 0.999888 0.732638 11.00000 -1.20000 AFIX 0 C16 1 0.885849 0.876795 0.580162 11.00000 0.03051 0.03526 = 0.02464 0.01005 0.00671 -0.00061 C17 1 0.965385 0.781841 0.723221 11.00000 0.05037 0.04133 = 0.03829 0.01711 0.00288 0.00322 AFIX 137 H17A 2 0.962070 0.700510 0.727679 11.00000 -1.50000 H17B 2 0.913930 0.820587 0.771604 11.00000 -1.50000 H17C 2 1.053264 0.830237 0.753009 11.00000 -1.50000 AFIX 0 C18 1 0.959063 0.694797 0.511377 11.00000 0.02573 0.03110 = 0.03788 0.01420 0.00153 -0.00017 C19 1 1.071728 0.665468 0.544419 11.00000 0.02578 0.04038 = 0.04246 0.02525 0.00572 0.00194 AFIX 43 H19 2 1.116807 0.690041 0.625591 11.00000 -1.20000 AFIX 0 C20 1 1.118691 0.597895 0.454607 11.00000 0.02993 0.04439 = 0.05349 0.02502 0.00923 0.00545 AFIX 43 H20 2 1.197740 0.578340 0.473406 11.00000 -1.20000 AFIX 0 C21 1 1.046279 0.560860 0.338222 11.00000 0.02360 0.03570 = 0.04651 0.01887 0.01008 0.00381 AFIX 43 H21 2 1.075831 0.516079 0.275706 11.00000 -1.20000 AFIX 0 C22 1 0.932087 0.589008 0.313661 11.00000 0.02396 0.02809 = 0.04059 0.01410 0.00798 0.00184 N1 4 0.654214 0.543810 0.226357 11.00000 0.03177 0.02257 = 0.02990 0.01006 0.00820 0.00321 N2 4 0.454404 0.535568 0.263519 11.00000 0.02995 0.02894 = 0.03780 0.01496 0.00975 0.00141 N3 4 0.562307 0.740564 0.315270 11.00000 0.03196 0.02712 = 0.03290 0.01607 0.00427 0.00171 N4 4 0.668189 0.945461 0.365705 11.00000 0.03397 0.03016 = 0.03083 0.01619 0.00581 0.00156 AFIX 43 H4N 2 0.677876 0.998805 0.328991 11.00000 -1.20000 AFIX 0 N5 4 0.795397 0.858669 0.478989 11.00000 0.03150 0.02728 = 0.02377 0.00916 0.00559 0.00082 N6 4 0.915853 0.773151 0.599602 11.00000 0.03540 0.03468 = 0.03074 0.01501 0.00632 0.00363 N7 4 0.884186 0.658432 0.397425 11.00000 0.02916 0.03034 = 0.03654 0.01765 0.00778 -0.00076 N8 4 0.857154 0.545998 0.198370 11.00000 0.02690 0.04003 = 0.03482 0.01654 0.01016 0.00309 AFIX 43 H8A 2 0.896472 0.551055 0.143494 11.00000 -1.20000 AFIX 0 CO1 6 0.723429 0.698755 0.356739 11.00000 0.02897 0.02782 = 0.03076 0.00993 0.00766 0.00283 MOLE 2 C23 1 0.786608 0.927103 -0.038366 11.00000 0.05439 0.04394 = 0.05601 0.02044 0.02373 0.01184 AFIX 137 H23A 2 0.730040 0.885126 -0.118187 11.00000 -1.50000 H23B 2 0.824671 0.869236 -0.009498 11.00000 -1.50000 H23C 2 0.853556 0.991112 -0.040936 11.00000 -1.50000 AFIX 0 C24 1 0.712983 0.981564 0.042978 11.00000 0.05795 0.04921 = 0.03988 0.02362 0.01276 0.01686 C25 1 0.665628 1.087190 0.025640 11.00000 0.08477 0.06519 = 0.07670 0.04852 0.04128 0.03895 AFIX 137 H25A 2 0.607000 1.062073 -0.053399 11.00000 -1.50000 H25B 2 0.737326 1.152320 0.032949 11.00000 -1.50000 H25C 2 0.621580 1.116268 0.086029 11.00000 -1.50000 AFIX 0 O3 7 0.689974 0.941510 0.120372 11.00000 0.10567 0.08083 = 0.06768 0.05277 0.04925 0.05499 MOLE 3 B1 3 1.000939 0.692389 0.024512 11.00000 0.03208 0.04545 = 0.03993 0.01867 0.01026 0.00277 F1 5 1.021151 0.646723 -0.088050 11.00000 0.05646 0.06588 = 0.04324 0.02511 0.02245 0.02540 F2 5 1.058833 0.637364 0.098242 11.00000 0.03844 0.05811 = 0.04870 0.03150 0.00563 0.00669 F3 5 1.049705 0.815278 0.069169 11.00000 0.04919 0.03880 = 0.06612 0.01505 0.00922 0.00215 F4 5 0.870238 0.665482 0.011910 11.00000 0.03401 0.05597 = 0.04398 0.02208 0.01116 0.01043 MOLE 4 B2 3 0.456398 0.758784 0.646721 11.00000 0.06119 0.04517 = 0.06388 0.01454 0.00536 0.01202 PART 1 F5 5 0.426967 0.637861 0.594890 21.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 F6 5 0.496032 0.797527 0.767810 21.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 F7 5 0.568995 0.802136 0.618026 21.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 F8 5 0.365578 0.816690 0.612599 21.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 PART 2 SAME F5 > F8 F5A 5 0.441270 0.642812 0.559155 31.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 F6A 5 0.546988 0.814339 0.742685 31.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 F7A 5 0.363231 0.705133 0.708197 31.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 F8A 5 0.390266 0.815625 0.580949 31.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 PART 3 SAME F5 > F8 F5B 5 0.402635 0.641899 0.640138 41.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 F6B 5 0.591603 0.798418 0.680103 41.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 F7B 5 0.466712 0.749565 0.529001 41.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 F8B 5 0.371759 0.825302 0.670116 41.00000 0.06620 0.04801 = 0.06524 0.01633 0.00837 0.01438 PART 0 MOLE 5 O1 7 0.784538 0.777051 0.216118 11.00000 0.03609 0.03449 = 0.03496 0.01492 0.01154 0.00803 H1W 2 0.759934 0.838031 0.187332 11.00000 -1.20000 H2W 2 0.809473 0.726623 0.154234 11.00000 -1.20000 MOLE 6 O2 7 0.664611 0.615338 0.486462 11.00000 0.03431 0.03313 = 0.03120 0.00845 0.00617 0.00095 H3W 2 0.604281 0.540363 0.448150 11.00000 -1.20000 H4W 2 0.628542 0.664884 0.537972 11.00000 -1.20000 HKLF 4 REM first_a.res in P-1 REM R1 = 0.0894 for 2323 Fo > 4sig(Fo) and 0.2020 for all 5297 data REM 449 parameters refined using 502 restraints END WGHT 0.1508 0.0000 REM Highest difference peak 1.270, deepest hole -1.364, 1-sigma level 0.172 Q1 1 0.6636 0.6411 0.3040 11.00000 0.05 1.27 Q2 1 0.7772 0.7571 0.4059 11.00000 0.05 1.09 Q3 1 0.6015 0.7229 0.2669 11.00000 0.05 0.90 Q4 1 0.8085 0.6235 0.4760 11.00000 0.05 0.74 Q5 1 0.7728 0.5771 0.3660 11.00000 0.05 0.74 ; _shelx_res_checksum 50837 _shelx_hkl_file ; -1 0 0 69.9533 5.82611 23 1 0 0 76.1501 5.78929 23 1 0 0 64.9011 7.21086 4 -2 0 0 568.595 31.7916 22 -2 0 0 590.516 31.2494 23 -2 0 0 607.135 30.3417 21 -2 0 0 593.804 30.6111 20 2 0 0 538.452 31.6610 18 2 0 0 648.511 35.1939 4 2 0 0 554.750 30.8716 23 -3 0 0 983.005 52.3678 3 -3 0 0 1026.32 53.1880 22 -3 0 0 1048.44 52.2798 20 -3 0 0 1034.24 51.8529 21 -3 0 0 999.800 52.9709 23 -3 0 0 1031.25 51.6676 9 3 0 0 1016.96 50.8233 9 3 0 0 1035.72 57.9739 4 3 0 0 1006.44 52.7395 6 -4 0 0 79.5237 13.5258 3 -4 0 0 84.6866 12.3005 20 -4 0 0 73.5984 10.6797 7 -4 0 0 54.4729 11.9571 23 -4 0 0 87.8212 15.5526 5 -4 0 0 76.1927 13.2251 22 -4 0 0 74.0277 10.2239 9 -4 0 0 85.7381 11.7278 21 4 0 0 73.5601 8.06347 1 4 0 0 71.7295 17.5381 4 4 0 0 77.9111 11.9091 6 4 0 0 100.370 16.7317 18 4 0 0 83.4971 11.1229 2 4 0 0 77.2449 13.8377 24 -5 0 0 1004.55 53.3223 21 -5 0 0 1019.18 54.4458 3 -5 0 0 1016.53 53.9550 20 -5 0 0 935.927 60.4772 22 -5 0 0 983.811 57.9769 5 5 0 0 833.419 56.1017 18 5 0 0 1028.78 55.1197 6 5 0 0 976.617 52.6332 2 -6 0 0 83.0357 16.6489 20 -6 0 0 68.3227 15.5665 3 -6 0 0 76.6312 16.6501 21 6 0 0 65.9110 16.1262 6 6 0 0 75.2153 21.7112 18 -7 0 0 24.5148 19.1995 20 -7 0 0 30.0266 17.8215 3 -7 0 0 4.50160 17.8880 21 7 0 0 14.6358 23.2381 18 7 0 0 29.3124 18.8271 6 -8 0 0 406.838 41.0804 3 -8 0 0 352.623 81.4996 30 -8 0 0 405.613 38.8732 20 -8 0 0 311.909 38.2245 21 -8 0 0 354.146 57.5275 27 8 0 0 305.486 40.7267 6 8 0 0 261.485 70.0490 11 8 0 0 402.564 51.6912 18 -9 0 0 155.716 49.0807 27 -9 0 0 16.0874 68.1019 26 -9 0 0 40.5840 62.2645 30 -9 0 0 86.3092 26.7092 21 -9 0 0 90.9439 28.7764 3 -9 0 0 99.2213 26.9185 20 9 0 0 46.8504 31.1137 18 9 0 0 75.4014 64.9831 11 9 0 0 181.713 78.7331 30 9 0 0 129.046 32.0075 6 -10 0 0 50.5244 67.2945 26 10 0 0 327.749 96.1677 30 10 0 0 95.9494 69.5377 11 -11 0 0 22.9021 42.7243 27 -11 0 0 -6.3405 55.2506 26 11 0 0 39.7694 64.1694 30 11 0 0 1.99520 60.5348 11 -12 0 0 40.4292 35.3295 27 -12 0 0 36.0359 40.4877 26 12 0 0 66.8708 42.6515 26 12 0 0 8.56675 46.3921 11 12 0 0 6.90776 38.6024 30 12 -1 0 5.95653 46.2142 30 12 -1 0 129.012 44.4332 26 12 -1 0 36.4939 51.3957 11 -12 1 0 17.8760 41.5472 26 -12 1 0 85.4276 38.0582 27 11 -1 0 43.3837 71.3260 30 11 -1 0 0.94459 65.5213 11 -11 1 0 51.3251 43.6174 27 -11 1 0 -6.1389 55.5126 26 10 -1 0 -3.2111 69.5397 11 10 -1 0 125.575 81.3567 30 -10 1 0 -8.6624 63.7521 26 -10 1 0 81.9050 47.0247 27 9 -1 0 -3.1194 25.6225 6 9 -1 0 7.65437 63.2467 11 9 -1 0 -4.2844 28.7158 18 -9 1 0 14.2911 23.6090 3 -9 1 0 39.8419 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800.246 56.3644 20 -8 3 -1 927.468 61.4127 3 -8 3 -1 813.903 55.4312 21 8 -3 1 840.928 57.1926 2 8 -3 1 772.549 71.9471 18 8 -3 1 897.505 62.6380 6 -9 3 -1 -2.6769 22.4124 20 -9 3 -1 -9.1289 36.4039 27 -9 3 -1 32.1383 57.4711 30 -9 3 -1 9.25801 61.4673 26 -9 3 -1 4.29082 24.3957 3 9 -3 1 0.40220 32.9934 18 9 -3 1 -13.139 27.9827 6 9 -3 1 -9.6417 68.4969 11 -10 3 -1 -14.380 66.2734 30 -10 3 -1 27.2739 43.3193 27 -10 3 -1 -9.0571 58.8421 26 10 -3 1 -18.566 72.1432 11 -11 3 -1 6.35654 42.4659 27 -11 3 -1 -47.568 47.6182 26 11 -3 1 -3.5014 64.7897 11 11 -3 1 61.6871 71.4954 30 -12 3 -1 -7.5420 35.2521 26 -12 3 -1 78.4241 33.7984 27 12 -3 1 -3.4094 53.2989 30 12 -3 1 23.3250 52.1413 11 12 2 -1 3.99138 32.7416 26 -12 -2 1 25.1358 32.4692 27 11 2 -1 221.199 66.7647 26 11 2 -1 88.1890 54.4667 11 -11 -2 1 206.291 62.8162 27 10 2 -1 22.7601 61.2680 11 -10 -2 1 15.2600 43.6615 27 -10 -2 1 -8.8692 57.7799 26 9 2 -1 215.892 68.3462 11 9 2 -1 159.813 82.3700 30 -9 -2 1 236.813 73.8287 26 -9 -2 1 249.351 55.4802 27 8 2 -1 27.4255 25.2815 6 8 2 -1 20.6743 53.1185 11 8 2 -1 -6.7939 75.1988 30 8 2 -1 3.03556 28.2667 18 -8 -2 1 6.51943 55.9763 26 -8 -2 1 18.3068 22.5674 21 -8 -2 1 9.76855 39.8957 27 7 2 -1 10.4497 18.1560 6 7 2 -1 -1.3861 24.2409 18 -7 -2 1 7.73356 38.6122 27 -7 -2 1 1.13316 18.5261 20 -7 -2 1 11.4369 25.9025 5 -7 -2 1 -0.3936 17.3324 21 6 2 -1 623.549 56.0759 24 6 2 -1 627.755 42.8726 6 6 2 -1 703.282 50.3345 18 -6 -2 1 623.848 42.8570 21 -6 -2 1 528.920 45.2963 3 -6 -2 1 668.146 52.4900 5 -6 -2 1 597.678 41.6572 20 5 2 -1 88.0512 20.2667 18 5 2 -1 72.8792 15.0682 6 5 2 -1 118.433 15.0282 1 5 2 -1 58.4630 10.5888 9 -5 -2 1 99.3144 16.1444 20 -5 -2 1 82.2513 12.1203 1 -5 -2 1 75.4257 13.9537 3 -5 -2 1 84.4975 15.4342 21 -5 -2 1 97.5493 22.3844 5 4 2 -1 1238.91 60.8463 1 4 2 -1 1166.91 61.0685 2 4 2 -1 1202.06 60.4095 9 4 2 -1 1234.33 63.7016 6 4 2 -1 1097.56 71.1357 4 -4 -2 1 1191.89 61.9403 20 -4 -2 1 1243.74 62.9226 21 -4 -2 1 1238.07 68.9318 5 -4 -2 1 1113.82 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1306.68 72.8129 8 4 -2 1 1366.04 74.2698 18 4 -2 1 1386.74 71.7138 6 4 -2 1 1359.19 80.0772 4 4 -2 1 1349.96 72.2957 7 -5 2 -1 1714.27 91.8575 7 -5 2 -1 1820.77 94.9825 22 -5 2 -1 1729.26 89.8799 20 -5 2 -1 1796.77 88.7764 9 -5 2 -1 1785.40 89.4589 21 -5 2 -1 1781.07 91.4272 3 -5 2 -1 1747.26 95.5769 23 5 -2 1 1725.82 92.5014 7 5 -2 1 1658.51 93.3741 8 5 -2 1 1716.44 90.1028 2 5 -2 1 1708.23 91.0612 6 5 -2 1 1753.36 95.0085 18 -6 2 -1 91.9713 20.1654 22 -6 2 -1 59.9776 15.9387 20 -6 2 -1 67.1206 16.8530 21 -6 2 -1 68.5225 15.3139 7 -6 2 -1 86.6503 20.0047 3 6 -2 1 73.7702 15.6895 2 6 -2 1 71.8524 24.0286 18 6 -2 1 67.3965 16.9585 6 -7 2 -1 710.895 47.7369 20 -7 2 -1 674.528 49.7035 3 -7 2 -1 629.488 45.4046 21 7 -2 1 669.674 57.9732 18 7 -2 1 667.680 45.8076 2 7 -2 1 640.817 48.8174 6 -8 2 -1 85.2871 50.7384 30 -8 2 -1 43.1153 26.0852 3 -8 2 -1 45.1657 21.6467 21 -8 2 -1 36.1842 60.6894 26 -8 2 -1 5.04956 31.7888 27 -8 2 -1 41.7793 23.2225 20 8 -2 1 46.5319 25.6661 6 8 -2 1 26.9543 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67.8927 73.4531 30 9 1 -1 -2.1979 29.4319 18 9 1 -1 17.0185 30.8558 6 -9 -1 1 1.22206 22.8246 20 -9 -1 1 30.7588 66.0481 26 -9 -1 1 20.6057 45.9601 27 -9 -1 1 19.0822 26.0650 21 8 1 -1 317.712 41.8494 6 8 1 -1 335.533 47.9665 18 8 1 -1 282.610 62.4198 11 8 1 -1 445.995 87.3263 30 -8 -1 1 301.488 34.5230 21 -8 -1 1 384.845 61.5505 27 -8 -1 1 296.037 37.4350 20 -8 -1 1 281.228 69.9345 26 7 1 -1 38.3702 22.0372 18 7 1 -1 37.9389 18.5354 6 -7 -1 1 35.2858 17.2687 3 -7 -1 1 35.5991 17.4837 21 -7 -1 1 34.3943 20.0579 20 -7 -1 1 19.4613 21.5410 5 6 1 -1 22.6344 18.1265 18 6 1 -1 8.77236 13.4299 6 -6 -1 1 12.0323 15.9643 20 -6 -1 1 7.20161 16.8470 5 -6 -1 1 -1.4544 12.5896 3 -6 -1 1 1.98916 14.7221 21 5 1 -1 983.781 63.4448 24 5 1 -1 1014.74 55.2848 2 5 1 -1 1053.88 58.2111 6 5 1 -1 1139.57 61.1130 18 -5 -1 1 1014.18 56.4914 20 -5 -1 1 1080.43 63.5739 5 -5 -1 1 1001.38 56.0437 21 -5 -1 1 1000.40 56.3200 3 4 1 -1 325.175 19.6177 9 4 1 -1 311.780 30.1211 4 4 1 -1 312.858 20.1686 2 4 1 -1 297.771 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37.6244 6 5 -3 -2 558.063 39.7158 7 5 -3 -2 578.138 42.6124 3 5 -3 -2 627.645 52.1528 24 5 -3 -2 643.340 42.3957 8 5 -3 -2 551.725 47.1824 4 5 -3 -2 584.253 44.3113 18 5 -3 -2 619.919 37.7006 2 -5 3 2 615.205 37.0567 20 -5 3 2 591.750 42.2019 5 -5 3 2 624.142 41.1685 19 -5 3 2 642.162 45.2659 22 -5 3 2 512.827 34.2028 9 -5 3 2 652.930 49.9779 23 4 -3 -2 162.566 33.6388 24 4 -3 -2 156.733 27.2556 18 4 -3 -2 176.139 21.7489 8 4 -3 -2 148.612 15.9477 6 4 -3 -2 160.407 23.5041 3 4 -3 -2 194.012 22.6699 7 4 -3 -2 163.295 18.4305 2 4 -3 -2 171.993 24.2333 4 -4 3 2 171.798 23.7313 5 -4 3 2 177.498 18.0304 20 -4 3 2 187.757 31.8074 23 -4 3 2 168.876 23.3961 19 -4 3 2 175.485 15.1421 9 -4 3 2 155.525 24.9755 22 3 -3 -2 123.835 17.3600 4 3 -3 -2 143.241 27.8123 24 3 -3 -2 127.824 16.9150 7 3 -3 -2 102.867 16.8825 18 3 -3 -2 120.747 18.9239 8 3 -3 -2 115.130 12.5696 2 3 -3 -2 112.097 17.4837 3 -3 3 2 119.504 10.8562 9 -3 3 2 120.683 22.9296 22 -3 3 2 65.9349 19.1514 23 -3 3 2 129.950 23.1501 19 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2 16.4839 25.0734 7 -8 5 2 22.4579 48.5038 27 7 -5 -2 435.992 46.4642 8 7 -5 -2 432.286 52.6226 3 7 -5 -2 407.512 47.9036 7 7 -5 -2 398.165 55.6370 18 7 -5 -2 484.791 41.2815 2 -7 5 2 470.550 39.6377 20 -7 5 2 468.780 33.3500 9 -7 5 2 512.143 58.7570 22 6 -5 -2 235.071 31.6939 2 6 -5 -2 250.938 39.7050 3 6 -5 -2 255.454 35.5533 8 6 -5 -2 261.229 38.5840 7 6 -5 -2 248.107 40.1840 18 -6 5 2 276.724 23.1724 9 -6 5 2 232.296 36.5155 19 -6 5 2 270.906 42.2788 22 -6 5 2 263.397 27.7412 20 -6 5 2 226.066 41.8756 23 5 -5 -2 15.2090 24.6010 18 5 -5 -2 23.3836 20.6399 8 5 -5 -2 16.4943 19.7255 3 5 -5 -2 9.94882 27.3049 24 5 -5 -2 29.4816 20.1006 7 5 -5 -2 23.8760 14.9320 2 -5 5 2 16.6711 19.7993 20 -5 5 2 4.22944 21.7741 22 -5 5 2 17.8938 20.4348 3 -5 5 2 20.5246 9.34199 9 -5 5 2 15.4755 19.6467 5 -5 5 2 12.9996 25.5812 23 -5 5 2 12.7152 25.3847 19 4 -5 -2 7.80797 20.3645 18 4 -5 -2 26.3625 27.1365 24 4 -5 -2 31.6515 18.9917 3 4 -5 -2 29.9908 17.3313 8 4 -5 -2 36.7279 14.0950 2 4 -5 -2 42.9287 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57.9271 10.8398 10 -3 -5 3 48.2654 14.6589 18 2 5 -3 1977.46 99.4572 9 2 5 -3 1899.46 105.960 6 2 5 -3 2060.42 106.398 19 2 5 -3 1968.00 102.005 2 -2 -5 3 2083.38 104.357 18 -2 -5 3 2073.54 105.324 6 -2 -5 3 2024.46 102.746 21 -2 -5 3 2094.33 102.987 1 -2 -5 3 2104.16 100.647 10 -2 -5 3 1999.21 110.033 5 1 5 -3 995.152 55.3693 22 1 5 -3 1057.84 51.6322 9 1 5 -3 1032.58 58.8442 23 1 5 -3 1011.18 59.1482 19 -1 -5 3 1133.60 56.2803 1 -1 -5 3 985.795 56.0279 18 -1 -5 3 1042.62 57.8859 6 -1 -5 3 981.432 55.5577 21 -1 -5 3 1072.38 55.8387 2 -1 -5 3 994.852 60.2160 5 -1 -5 3 1095.24 53.9230 10 0 5 -3 399.928 20.5468 9 0 5 -3 346.614 27.1714 22 0 5 -3 363.182 31.1485 23 0 5 -3 388.976 30.3560 19 0 -5 3 350.563 25.7708 21 0 -5 3 431.469 26.0566 1 0 -5 3 359.386 27.0581 18 0 -5 3 368.572 29.0124 5 0 -5 3 377.933 23.8813 10 0 -5 3 410.857 29.7477 6 0 -5 3 396.296 28.7157 8 0 -5 3 380.769 25.8725 2 -1 5 -3 286.407 29.9812 23 -1 5 -3 293.118 25.6247 22 -1 5 -3 293.116 16.1816 9 -1 5 -3 303.221 27.0598 19 -1 5 -3 271.895 18.3091 20 1 -5 3 285.349 22.6427 1 1 -5 3 271.810 25.7753 18 1 -5 3 287.272 19.1800 15 1 -5 3 286.961 23.3836 7 1 -5 3 288.872 22.4571 21 1 -5 3 308.233 25.7015 6 1 -5 3 296.898 24.1041 2 1 -5 3 291.890 27.3044 8 1 -5 3 321.106 21.3032 10 1 -5 3 280.367 34.4924 4 -2 5 -3 31.0788 8.33291 20 -2 5 -3 40.6280 14.1184 22 -2 5 -3 33.3391 5.71923 9 -2 5 -3 37.8462 16.4448 23 -2 5 -3 45.0239 14.7166 19 -2 5 -3 0.78823 9.56213 7 -2 5 -3 5.19239 9.99628 3 2 -5 3 34.5297 14.2168 6 2 -5 3 29.7169 12.3117 7 2 -5 3 29.8721 13.6262 3 2 -5 3 32.2956 10.0550 1 2 -5 3 29.9384 15.0728 8 2 -5 3 26.2642 13.0219 21 2 -5 3 31.4277 9.63040 15 2 -5 3 32.1684 12.5819 2 2 -5 3 28.5551 15.3628 18 -3 5 -3 379.024 30.0952 3 -3 5 -3 463.131 36.6781 22 -3 5 -3 436.880 24.6844 9 -3 5 -3 410.043 33.7155 19 -3 5 -3 448.058 41.2536 23 -3 5 -3 441.902 27.3576 20 3 -5 3 458.076 33.7857 7 3 -5 3 395.139 38.1694 18 3 -5 3 416.130 26.2528 15 3 -5 3 450.661 36.2015 8 3 -5 3 431.015 31.6302 2 3 -5 3 417.250 35.0690 6 -4 5 -3 482.330 28.1685 9 -4 5 -3 458.226 35.1667 19 -4 5 -3 473.842 42.5505 23 -4 5 -3 475.829 37.4402 7 -4 5 -3 491.383 41.2197 22 -4 5 -3 464.285 32.8624 3 -4 5 -3 449.710 30.4659 21 -4 5 -3 463.417 31.0939 20 4 -5 3 455.345 35.9920 2 4 -5 3 469.395 39.0017 6 4 -5 3 384.195 40.6906 18 4 -5 3 457.571 40.5719 7 4 -5 3 491.086 39.9417 8 -5 5 -3 68.0981 12.3670 9 -5 5 -3 52.1914 14.9606 21 -5 5 -3 63.4108 25.2238 23 -5 5 -3 88.7956 21.3908 7 -5 5 -3 71.1358 17.9317 3 -5 5 -3 77.3190 23.7375 22 -5 5 -3 69.6247 15.7600 20 5 -5 3 91.1860 21.6109 2 5 -5 3 71.8455 23.3231 8 5 -5 3 80.5163 25.3931 7 5 -5 3 78.3892 29.1520 18 5 -5 3 72.8167 21.3192 6 -6 5 -3 51.5081 30.4381 8 -6 5 -3 53.8647 28.4420 23 -6 5 -3 64.7476 18.7744 20 -6 5 -3 66.3521 26.5903 22 -6 5 -3 62.6551 14.0712 9 -6 5 -3 56.6940 21.2561 3 -6 5 -3 69.6087 18.6350 21 -6 5 -3 64.8892 21.5685 7 6 -5 3 48.9980 23.4876 6 6 -5 3 95.2700 30.2848 18 6 -5 3 71.8578 24.3242 2 6 -5 3 54.6240 27.3483 8 -7 5 -3 44.9713 32.7466 8 -7 5 -3 244.526 37.2809 3 -7 5 -3 167.969 21.2283 9 -7 5 -3 214.805 36.8351 7 -7 5 -3 160.917 33.9513 22 -7 5 -3 236.273 31.0469 20 7 -5 3 241.513 38.8369 6 7 -5 3 223.337 33.2840 2 7 -5 3 206.550 38.1905 8 7 -5 3 -83.406 110.165 28 7 -5 3 158.541 38.0806 18 -8 5 -3 184.444 27.7777 20 -8 5 -3 148.475 35.7179 22 -8 5 -3 104.240 53.2877 30 -8 5 -3 214.728 35.3023 3 -8 5 -3 155.810 29.6745 7 8 -5 3 179.858 38.9424 6 8 -5 3 131.802 42.1361 18 8 -5 3 189.905 32.5269 2 8 -5 3 -31.201 115.077 28 -9 5 -3 42.9582 62.2551 30 9 -5 3 112.233 20.0690 15 9 -5 3 -69.695 146.700 28 9 -5 3 4.82838 69.9292 11 -10 5 -3 -5.5182 63.7551 30 10 -5 3 -0.9628 65.0709 11 -11 5 -3 -27.570 60.2562 30 11 -5 3 54.2314 63.4868 30 11 -5 3 23.9616 55.2345 11 12 -5 3 -9.7568 44.1039 30 12 -5 3 7.95376 38.3956 11 11 4 -3 28.6516 50.3626 26 -11 -4 3 48.2769 40.3978 27 10 4 -3 119.265 64.1388 26 -10 -4 3 60.8833 46.8985 27 9 4 -3 44.6295 65.8266 26 -9 -4 3 63.5117 49.6931 27 8 4 -3 509.271 87.1700 26 8 4 -3 352.676 61.5810 6 -8 -4 3 377.592 62.7844 5 -8 -4 3 396.654 72.1688 27 7 4 -3 -10.905 36.9354 24 7 4 -3 4.64743 24.0132 6 7 4 -3 -1.8131 55.5064 26 -7 -4 3 2.69810 19.9224 21 -7 -4 3 -4.0270 39.5534 27 -7 -4 3 -2.7208 57.7498 29 -7 -4 3 4.18726 30.1257 5 -7 -4 3 -7.0678 19.2438 13 -7 -4 3 -0.3803 50.1745 26 6 4 -3 103.389 17.9277 1 6 4 -3 162.110 32.4341 18 6 4 -3 115.730 37.8842 24 6 4 -3 127.720 23.8370 6 -6 -4 3 110.827 31.7589 5 -6 -4 3 163.165 26.6784 21 -6 -4 3 103.746 17.3886 1 5 4 -3 144.999 18.3795 9 5 4 -3 94.7463 21.8123 18 5 4 -3 145.186 23.3819 6 -5 -4 3 142.638 18.0932 1 -5 -4 3 164.974 26.4882 21 -5 -4 3 129.371 22.8519 18 -5 -4 3 115.382 27.2227 5 4 4 -3 158.702 24.2123 6 4 4 -3 165.451 16.2550 9 4 4 -3 166.730 19.1573 2 -4 -4 3 171.834 19.8864 1 -4 -4 3 184.154 23.1070 21 -4 -4 3 136.024 18.6999 20 -4 -4 3 162.914 30.7695 5 -4 -4 3 164.546 15.3389 10 -4 -4 3 157.263 24.5320 18 3 4 -3 1045.51 55.7353 2 3 4 -3 1114.42 60.3229 6 3 4 -3 1039.35 54.1626 9 3 4 -3 1010.11 58.7095 19 -3 -4 3 1129.27 65.6513 5 -3 -4 3 1091.44 56.2891 1 -3 -4 3 1082.88 57.5992 21 -3 -4 3 970.763 54.8852 20 -3 -4 3 989.713 57.3474 18 -3 -4 3 1056.93 53.8669 10 2 4 -3 53.3377 10.5737 2 2 4 -3 49.6002 7.54120 9 2 4 -3 44.7344 15.5856 6 2 4 -3 39.7243 19.3657 4 2 4 -3 60.7406 12.0536 23 2 4 -3 61.8875 14.0250 19 -2 -4 3 48.4179 10.7013 1 -2 -4 3 57.2150 14.4948 6 -2 -4 3 61.7562 16.2297 5 -2 -4 3 62.4457 11.0088 18 -2 -4 3 54.5596 11.9080 21 -2 -4 3 41.3604 8.44868 20 -2 -4 3 54.5255 8.62672 10 1 4 -3 128.218 18.4582 23 1 4 -3 49.1595 16.4478 6 1 4 -3 119.479 9.61470 9 1 4 -3 122.527 13.7264 8 1 4 -3 104.470 15.1841 2 1 4 -3 45.1711 22.0442 4 1 4 -3 112.107 17.9288 19 1 4 -3 110.051 13.9557 22 -1 -4 3 121.553 13.3713 10 -1 -4 3 114.984 17.5337 5 -1 -4 3 132.875 18.1104 6 -1 -4 3 114.338 12.9778 18 -1 -4 3 130.352 14.8965 2 -1 -4 3 102.282 13.8666 21 -1 -4 3 118.895 11.3746 20 -1 -4 3 113.737 15.7425 1 0 4 -3 421.316 27.6693 8 0 4 -3 420.889 30.8896 23 0 4 -3 393.037 23.0729 20 0 4 -3 427.890 27.3973 22 0 4 -3 339.782 23.8580 7 0 4 -3 453.727 22.1804 9 0 4 -3 421.527 29.5104 19 0 -4 3 407.594 25.1787 7 0 -4 3 442.399 27.9517 6 0 -4 3 391.619 27.1569 5 0 -4 3 459.066 24.4189 10 0 -4 3 412.870 26.0078 21 0 -4 3 443.019 27.9995 8 0 -4 3 394.352 26.3133 18 0 -4 3 455.232 26.4179 2 0 -4 3 443.268 27.0555 1 -1 4 -3 1784.83 89.2485 19 -1 4 -3 1636.66 85.8439 7 -1 4 -3 1687.87 83.8759 20 -1 4 -3 1667.03 87.9206 22 -1 4 -3 1646.46 90.5669 23 -1 4 -3 1730.35 82.7532 9 1 -4 3 1631.82 87.6625 18 1 -4 3 1701.65 85.9453 21 1 -4 3 1753.24 86.4288 2 1 -4 3 1728.75 88.6960 8 1 -4 3 1658.80 86.6268 7 1 -4 3 1747.99 97.1410 4 1 -4 3 1705.19 85.4449 1 1 -4 3 1734.27 87.9778 6 -2 4 -3 1751.26 95.8638 3 -2 4 -3 1977.59 93.6036 9 -2 4 -3 1899.74 98.8010 19 -2 4 -3 2109.39 111.600 4 -2 4 -3 1958.23 100.210 22 -2 4 -3 1987.11 95.0561 20 -2 4 -3 1942.57 103.158 23 2 -4 3 1668.18 106.026 4 2 -4 3 1868.19 95.4662 1 2 -4 3 1952.89 100.331 8 2 -4 3 1970.42 98.8870 7 2 -4 3 1968.86 99.3940 6 2 -4 3 1917.14 97.3450 2 2 -4 3 1882.81 99.9702 18 -3 4 -3 259.110 27.1837 22 -3 4 -3 267.553 31.3817 23 -3 4 -3 256.092 19.9146 21 -3 4 -3 242.578 21.1472 3 -3 4 -3 255.079 16.8830 9 -3 4 -3 241.678 19.6315 20 -3 4 -3 230.043 23.2685 19 3 -4 3 284.597 25.3697 7 3 -4 3 223.053 28.8467 18 3 -4 3 218.562 17.9743 1 3 -4 3 244.403 28.3062 8 3 -4 3 228.167 21.9608 2 3 -4 3 247.477 24.3922 6 -4 4 -3 1151.50 57.4957 9 -4 4 -3 1096.59 61.3926 3 -4 4 -3 1058.25 60.9615 19 -4 4 -3 1137.86 62.8310 7 -4 4 -3 1108.32 65.3277 22 -4 4 -3 1115.96 69.8408 23 -4 4 -3 1073.83 58.7529 21 -4 4 -3 1097.92 59.1165 20 4 -4 3 1075.54 68.5333 18 4 -4 3 1116.66 67.2119 8 4 -4 3 1081.42 64.2179 6 4 -4 3 1090.14 61.5375 2 4 -4 3 1069.03 64.9339 7 -5 4 -3 92.0345 23.7286 22 -5 4 -3 95.1564 25.7126 23 -5 4 -3 80.9797 18.0742 7 -5 4 -3 49.7006 11.4579 9 -5 4 -3 33.2638 22.3599 8 -5 4 -3 91.4799 16.7532 21 -5 4 -3 69.5988 15.1530 20 -5 4 -3 85.5135 19.2663 3 5 -4 3 82.2430 19.5505 2 5 -4 3 68.0323 23.4021 8 5 -4 3 86.6018 26.8564 18 5 -4 3 71.2442 20.6532 6 -6 4 -3 45.5153 16.5408 20 -6 4 -3 53.8038 18.4427 21 -6 4 -3 46.0168 19.2502 3 -6 4 -3 62.6889 21.5306 7 -6 4 -3 40.0720 23.0747 22 -6 4 -3 45.3028 26.4112 8 -6 4 -3 34.9856 23.8651 23 -6 4 -3 38.4593 13.2528 9 6 -4 3 74.3479 22.0439 2 6 -4 3 32.1722 25.9712 18 6 -4 3 48.1046 20.7372 6 6 -4 3 68.7680 26.0063 8 -7 4 -3 41.2970 59.5713 26 -7 4 -3 109.085 27.4732 3 -7 4 -3 90.1594 22.0111 21 -7 4 -3 115.075 30.6852 22 -7 4 -3 54.6630 40.4809 30 -7 4 -3 113.548 25.7939 7 -7 4 -3 117.162 24.0258 20 7 -4 3 -105.27 109.049 28 7 -4 3 80.9099 26.0903 2 7 -4 3 110.059 29.6692 6 7 -4 3 89.2780 32.5460 18 7 -4 3 13.6142 56.3956 11 -8 4 -3 0.72666 20.5589 20 -8 4 -3 1.83853 48.0186 30 -8 4 -3 36.6831 26.5278 3 -8 4 -3 17.0001 21.8063 21 -8 4 -3 11.3458 65.5358 26 -8 4 -3 6.74075 22.6417 7 8 -4 3 18.9327 64.8344 11 8 -4 3 30.5953 34.0136 18 8 -4 3 27.4134 28.1080 6 -9 4 -3 50.4981 61.5572 30 -9 4 -3 -4.2868 65.5744 26 9 -4 3 11.4725 66.1820 11 -10 4 -3 75.1325 65.2617 30 -10 4 -3 -8.3858 57.7015 26 10 -4 3 -1.3135 67.2558 11 -11 4 -3 -9.1692 43.9055 26 -11 4 -3 -0.1648 58.4787 30 11 -4 3 57.7612 57.5072 11 11 -4 3 157.394 68.6230 30 -12 4 -3 -13.605 37.2136 26 12 -4 3 -12.253 46.7184 30 12 -4 3 41.0341 39.8267 11 12 3 -3 -10.901 32.1202 26 -12 -3 3 48.6798 32.7005 27 11 3 -3 30.2667 51.6911 26 -11 -3 3 22.9112 41.8292 27 10 3 -3 -5.2180 61.1918 26 -10 -3 3 -3.7257 44.9733 27 9 3 -3 97.4359 68.3426 26 -9 -3 3 47.8912 47.7651 27 8 3 -3 203.412 35.2928 6 8 3 -3 169.935 62.6137 26 -8 -3 3 242.565 62.0563 26 -8 -3 3 139.000 41.6914 5 -8 -3 3 196.344 31.6370 21 -8 -3 3 172.592 49.2838 27 7 3 -3 701.904 54.9477 6 7 3 -3 651.002 72.3095 24 -7 -3 3 715.853 52.0337 20 -7 -3 3 757.345 52.8724 21 -7 -3 3 844.242 72.6439 26 -7 -3 3 720.848 72.2817 27 -7 -3 3 752.649 66.4124 5 6 3 -3 6.01919 18.7024 18 6 3 -3 -3.5104 27.7005 24 6 3 -3 10.1614 16.1484 6 -6 -3 3 8.41819 16.1556 20 -6 -3 3 3.55911 24.1925 5 -6 -3 3 15.3405 16.3177 21 5 3 -3 205.341 41.2018 24 5 3 -3 244.419 19.8639 9 5 3 -3 221.687 22.5892 2 5 3 -3 209.199 26.8263 18 5 3 -3 238.614 25.3863 6 -5 -3 3 235.928 24.1346 20 -5 -3 3 196.368 20.2862 1 -5 -3 3 220.640 25.4885 21 -5 -3 3 257.599 34.6763 5 4 3 -3 513.876 33.6616 6 4 3 -3 541.771 39.4847 19 4 3 -3 487.153 31.0931 2 4 3 -3 495.968 29.5720 9 -4 -3 3 493.826 28.7882 10 -4 -3 3 492.031 29.7823 1 -4 -3 3 514.999 39.3703 5 -4 -3 3 472.856 33.3642 18 -4 -3 3 459.883 31.6785 20 -4 -3 3 488.642 31.8296 21 3 3 -3 266.577 20.9294 23 3 3 -3 300.247 22.9516 6 3 3 -3 273.221 18.9504 2 3 3 -3 286.118 18.4117 9 3 3 -3 266.024 23.8572 19 3 3 -3 260.646 29.6540 4 -3 -3 3 265.087 20.7835 18 -3 -3 3 269.531 25.8748 5 -3 -3 3 249.108 18.2030 10 -3 -3 3 264.980 19.5990 1 -3 -3 3 249.531 19.4150 20 -3 -3 3 268.278 20.7966 21 2 3 -3 1388.46 66.7139 9 2 3 -3 1385.64 70.5189 23 2 3 -3 1268.31 68.2580 22 2 3 -3 1315.02 68.1638 2 2 3 -3 1412.21 80.7548 4 2 3 -3 1342.59 71.1537 6 2 3 -3 1321.21 70.5710 19 -2 -3 3 1322.16 68.2995 1 -2 -3 3 1310.01 67.5252 18 -2 -3 3 1369.23 69.9349 6 -2 -3 3 1273.47 71.9803 5 -2 -3 3 1337.81 67.3055 20 -2 -3 3 1445.59 69.1120 21 -2 -3 3 1293.84 66.4428 10 1 3 -3 398.539 23.9521 8 1 3 -3 351.259 35.5891 4 1 3 -3 359.527 24.1982 22 1 3 -3 368.199 27.1943 19 1 3 -3 373.564 20.7750 9 1 3 -3 385.334 27.3552 23 1 3 -3 397.713 24.2609 2 -1 -3 3 395.593 24.0742 2 -1 -3 3 395.622 24.9757 6 -1 -3 3 403.827 22.2480 10 -1 -3 3 390.607 23.7721 21 -1 -3 3 352.107 24.8507 5 -1 -3 3 372.416 22.4895 20 -1 -3 3 364.614 21.4332 18 -1 -3 3 380.271 23.6759 1 0 3 -3 1419.85 68.2833 9 0 3 -3 1468.33 74.8061 23 0 3 -3 1405.72 72.0916 8 0 3 -3 1348.29 69.0701 20 0 3 -3 1338.23 71.6167 22 0 3 -3 1416.40 73.2148 19 0 -3 3 1285.07 69.9141 18 0 -3 3 1449.83 72.8064 8 0 -3 3 1421.84 70.9271 21 0 -3 3 1398.02 71.9991 6 0 -3 3 1391.62 70.6559 2 0 -3 3 1428.97 70.6968 1 -1 3 -3 59.5511 9.34863 20 -1 3 -3 58.9844 12.0738 22 -1 3 -3 66.0978 12.6529 24 -1 3 -3 73.4037 14.8699 23 -1 3 -3 72.6978 13.1825 19 -1 3 -3 49.9506 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534.429 41.1285 23 -4 3 -3 574.436 35.7385 3 -4 3 -3 610.128 36.6819 7 -4 3 -3 546.947 39.1009 22 -4 3 -3 539.591 34.7399 21 -4 3 -3 486.289 40.4831 8 -4 3 -3 583.009 35.0362 20 4 -3 3 533.263 43.0496 18 4 -3 3 532.931 36.1343 2 4 -3 3 541.748 40.6626 8 4 -3 3 564.820 37.5996 6 -5 3 -3 170.315 25.9620 3 -5 3 -3 183.234 22.8838 20 -5 3 -3 175.231 22.4237 21 -5 3 -3 179.690 19.0244 9 -5 3 -3 157.796 22.9168 7 -5 3 -3 175.609 29.7969 23 -5 3 -3 175.720 28.4828 22 5 -3 3 170.554 26.8125 8 5 -3 3 158.746 26.6476 6 5 -3 3 150.758 26.7832 18 5 -3 3 155.476 22.9811 2 -6 3 -3 15.5050 15.2032 20 -6 3 -3 -1.1646 15.8996 21 -6 3 -3 11.2129 19.4738 22 -6 3 -3 7.33616 18.2886 7 -6 3 -3 -3.0572 16.8036 3 6 -3 3 -7.5211 23.3944 18 6 -3 3 -5.3982 15.1971 2 6 -3 3 21.9624 17.8923 6 -7 3 -3 688.541 50.9706 7 -7 3 -3 710.559 54.3010 3 -7 3 -3 667.248 48.9565 20 -7 3 -3 671.235 71.3640 30 -7 3 -3 680.853 48.5379 21 7 -3 3 684.317 52.3209 6 7 -3 3 631.539 65.1133 18 -8 3 -3 161.528 28.8620 20 -8 3 -3 136.661 52.9262 30 -8 3 -3 -8.0531 70.6268 26 -8 3 -3 116.920 25.1273 21 -8 3 -3 78.8259 29.0774 3 8 -3 3 2.28134 60.3419 11 8 -3 3 108.232 39.7486 18 8 -3 3 85.5154 27.9810 6 -9 3 -3 28.1857 72.2433 26 -9 3 -3 61.1969 63.0187 30 9 -3 3 24.5725 68.4390 11 -10 3 -3 64.1859 66.9746 30 -10 3 -3 3.56697 63.4844 26 10 -3 3 30.3307 66.2103 11 -11 3 -3 -13.918 47.9376 26 -11 3 -3 -10.971 56.3460 30 11 -3 3 188.255 63.2600 30 11 -3 3 30.4127 53.0087 11 -12 3 -3 -3.9140 28.6383 26 12 -3 3 -37.613 43.4474 30 12 -3 3 -6.2758 38.7189 11 12 2 -3 0.29880 34.1659 26 -12 -2 3 -6.3982 36.2017 27 11 2 -3 14.0138 50.6137 26 11 2 -3 -9.0205 50.0576 30 -11 -2 3 21.6768 42.3576 27 10 2 -3 15.8821 58.5974 30 10 2 -3 46.6571 61.1355 26 -10 -2 3 35.5149 48.0512 27 9 2 -3 48.7109 57.3759 26 9 2 -3 19.6263 56.8903 30 -9 -2 3 30.3806 46.1698 27 -9 -2 3 47.4425 61.8493 26 8 2 -3 54.2028 51.9387 30 8 2 -3 85.2510 27.5585 6 -8 -2 3 28.0199 40.1040 27 -8 -2 3 97.7747 25.8103 21 -8 -2 3 49.9116 24.3583 20 -8 -2 3 48.5339 34.6852 5 -8 -2 3 82.1057 53.2771 26 7 2 -3 1476.05 106.906 24 7 2 -3 1673.22 91.7869 6 7 2 -3 1509.78 91.6564 18 -7 -2 3 1656.03 101.197 5 -7 -2 3 1640.09 89.8920 20 -7 -2 3 1607.35 88.7538 21 6 2 -3 218.633 24.5350 2 6 2 -3 204.308 26.1348 6 6 2 -3 229.414 40.2571 24 6 2 -3 168.761 28.1980 18 -6 -2 3 205.336 27.5007 20 -6 -2 3 218.679 32.6446 5 -6 -2 3 215.312 26.6152 21 5 2 -3 6.29146 13.5786 18 5 2 -3 16.1014 24.0275 24 5 2 -3 21.0803 12.3908 2 5 2 -3 3.18147 8.91771 9 5 2 -3 15.4760 13.5917 6 -5 -2 3 11.3230 13.6371 20 -5 -2 3 11.3796 18.1241 5 -5 -2 3 22.9037 13.0610 21 -5 -2 3 7.32290 11.8297 1 4 2 -3 49.3256 11.9767 6 4 2 -3 60.4294 12.8370 19 4 2 -3 77.0647 12.4271 18 4 2 -3 44.1889 22.1647 24 4 2 -3 53.6942 11.8119 2 4 2 -3 53.7573 9.40885 9 4 2 -3 52.0802 19.5615 4 -4 -2 3 62.4782 12.9517 21 -4 -2 3 52.4519 12.3751 20 -4 -2 3 56.9430 9.53018 1 -4 -2 3 52.0267 8.23938 10 -4 -2 3 49.5151 16.2300 5 3 2 -3 15.0984 7.80829 8 3 2 -3 13.9222 9.42460 19 3 2 -3 10.0590 15.7864 24 3 2 -3 11.5205 7.29551 2 3 2 -3 27.3559 8.61981 18 3 2 -3 19.8883 15.8131 4 3 2 -3 17.6157 9.00958 6 3 2 -3 18.1418 6.70759 9 -3 -2 3 18.7305 9.08585 23 -3 -2 3 11.4451 5.29885 10 -3 -2 3 17.2178 12.0506 5 -3 -2 3 19.8869 7.84497 1 -3 -2 3 20.2006 8.68705 20 -3 -2 3 21.4281 8.77069 21 -3 -2 3 19.1339 8.74997 22 2 2 -3 217.468 15.6233 2 2 2 -3 255.868 18.8516 19 2 2 -3 203.353 18.1759 22 2 2 -3 237.501 14.9837 9 2 2 -3 227.257 19.8569 23 2 2 -3 256.165 20.9795 6 2 2 -3 203.678 25.2802 24 2 2 -3 273.276 27.3243 4 -2 -2 3 212.231 14.2115 18 -2 -2 3 215.386 20.2898 5 -2 -2 3 207.795 16.6133 21 -2 -2 3 218.988 18.8054 6 -2 -2 3 214.233 15.5816 20 -2 -2 3 203.237 14.3852 10 -2 -2 3 208.887 17.0427 1 1 2 -3 2531.87 133.444 24 1 2 -3 3022.30 138.591 4 1 2 -3 2531.73 127.871 2 1 2 -3 2560.17 129.516 19 1 2 -3 2817.02 131.295 23 1 2 -3 2713.72 126.729 9 1 2 -3 2657.58 129.405 22 -1 -2 3 2337.05 128.197 6 -1 -2 3 2508.19 127.827 2 -1 -2 3 2472.92 126.299 10 -1 -2 3 2793.72 127.802 20 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1176.99 59.7483 2 2 -2 3 1132.18 61.2411 6 2 -2 3 1115.92 67.9875 4 2 -2 3 1210.73 58.6054 1 2 -2 3 1202.79 61.6580 18 2 -2 3 1147.60 62.5840 8 -3 2 -3 84.8407 12.5355 20 -3 2 -3 78.1538 11.7168 21 -3 2 -3 97.8287 17.7050 23 -3 2 -3 92.7908 14.3280 7 -3 2 -3 63.6246 8.98647 9 -3 2 -3 47.7654 14.4582 8 -3 2 -3 80.9507 15.8371 22 -3 2 -3 70.2289 12.2044 19 -3 2 -3 80.5609 12.9545 3 3 -2 3 79.1348 15.5738 18 3 -2 3 85.9292 11.2734 1 3 -2 3 86.5206 13.7999 2 3 -2 3 70.2347 18.4270 4 3 -2 3 89.1550 16.2585 8 3 -2 3 97.0353 14.6661 6 -4 2 -3 1094.10 58.9623 9 -4 2 -3 1106.36 64.2120 22 -4 2 -3 1132.45 60.3168 21 -4 2 -3 1127.68 62.3027 3 -4 2 -3 1185.91 61.6645 7 -4 2 -3 1111.38 59.7890 20 -4 2 -3 1090.59 66.0804 23 4 -2 3 1053.08 62.9487 8 4 -2 3 1103.58 57.9337 1 4 -2 3 1103.07 60.5378 2 4 -2 3 1141.25 63.0288 6 4 -2 3 1195.25 66.6738 18 -5 2 -3 12.8753 14.3531 3 -5 2 -3 -8.3186 14.3206 23 -5 2 -3 4.71345 12.6954 21 -5 2 -3 1.78966 13.8006 7 -5 2 -3 3.85048 14.5663 22 -5 2 -3 4.60848 14.1800 20 5 -2 3 2.45285 18.6840 18 5 -2 3 8.33823 12.8227 2 5 -2 3 9.18460 15.1069 6 -6 2 -3 46.5771 16.7387 7 -6 2 -3 68.4226 19.2932 21 -6 2 -3 62.7862 18.8693 20 -6 2 -3 44.0502 19.8786 22 -6 2 -3 74.0855 21.2546 3 6 -2 3 40.8931 20.4623 6 6 -2 3 55.7257 23.4412 18 -7 2 -3 42.3366 20.0340 7 -7 2 -3 8.08882 57.8535 26 -7 2 -3 74.1868 20.5206 21 -7 2 -3 28.9345 21.7730 20 -7 2 -3 29.4146 38.4651 30 -7 2 -3 52.1782 24.2230 3 7 -2 3 50.2615 31.0851 18 7 -2 3 -16.634 48.6080 11 7 -2 3 54.4752 24.2851 6 -8 2 -3 30.0242 27.8324 3 -8 2 -3 71.6427 23.7849 21 -8 2 -3 51.5102 24.5834 20 -8 2 -3 84.6795 52.4030 30 -8 2 -3 6.68266 75.8941 26 8 -2 3 58.4294 25.6368 6 8 -2 3 60.2057 35.1372 18 8 -2 3 27.0320 60.3149 11 -9 2 -3 18.7871 62.5027 30 -9 2 -3 -6.3383 73.2042 26 9 -2 3 -0.8936 66.7867 11 -10 2 -3 -3.0588 65.5127 30 -10 2 -3 -8.1905 65.2090 26 10 -2 3 110.355 67.7986 11 -11 2 -3 20.4152 51.9776 26 11 -2 3 111.966 57.5924 11 11 -2 3 233.969 75.0135 30 -12 2 -3 -8.7662 26.2680 26 12 -2 3 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21 -6 -1 3 633.517 43.6313 20 -6 -1 3 672.990 49.4183 5 5 1 -3 11.9941 11.8479 2 5 1 -3 5.95816 12.0454 18 5 1 -3 5.96896 20.4186 24 5 1 -3 14.1786 11.2398 6 -5 -1 3 8.54672 17.2262 22 -5 -1 3 15.4998 13.5847 20 -5 -1 3 28.9409 16.1532 5 -5 -1 3 12.0337 11.6340 21 4 1 -3 1044.13 55.4871 8 4 1 -3 1003.06 54.5955 18 4 1 -3 999.154 54.3150 6 4 1 -3 1013.74 54.4557 19 4 1 -3 1026.68 64.1365 24 4 1 -3 986.678 52.5992 9 4 1 -3 1035.62 53.6546 2 -4 -1 3 1055.15 53.7275 21 -4 -1 3 976.309 50.3309 10 -4 -1 3 1084.41 59.8725 5 -4 -1 3 947.582 54.8747 22 -4 -1 3 1052.54 54.2257 20 -4 -1 3 922.027 51.2283 1 -4 -1 3 1011.56 55.6440 23 3 1 -3 440.617 35.7702 24 3 1 -3 331.942 23.3960 8 3 1 -3 374.699 21.6958 9 3 1 -3 330.964 28.5636 4 3 1 -3 314.154 21.4560 18 3 1 -3 429.814 23.2362 6 3 1 -3 334.191 21.5298 2 -3 -1 3 350.038 26.5654 5 -3 -1 3 342.773 21.1458 1 -3 -1 3 325.459 24.6409 23 -3 -1 3 307.564 19.1853 10 -3 -1 3 435.168 23.9253 20 -3 -1 3 323.189 21.6952 21 -3 -1 3 394.849 25.4192 22 2 1 -3 328.822 26.5668 4 2 1 -3 361.186 23.3059 19 2 1 -3 357.128 31.9351 24 2 1 -3 304.871 20.4473 8 2 1 -3 350.046 22.9615 22 2 1 -3 344.356 21.4972 6 2 1 -3 326.849 19.0343 9 2 1 -3 315.724 23.9029 23 2 1 -3 294.164 19.1745 2 -2 -1 3 321.864 21.3742 6 -2 -1 3 239.356 18.9248 21 -2 -1 3 282.089 19.6669 20 -2 -1 3 281.443 22.0025 5 1 1 -3 2430.65 110.894 23 1 1 -3 2132.91 106.457 9 1 1 -3 2231.41 106.929 20 1 1 -3 2268.59 113.859 24 1 1 -3 2267.75 113.863 4 1 1 -3 2179.98 108.899 19 1 1 -3 2389.70 109.450 22 1 1 -3 1877.16 110.558 4 -1 -1 3 1913.08 113.880 4 -1 -1 3 2248.32 107.421 21 0 1 -3 1488.65 78.4156 24 0 1 -3 1422.67 72.1061 9 0 1 -3 1506.09 80.0149 4 0 1 -3 1456.45 75.2796 22 0 1 -3 1436.14 74.4197 19 0 1 -3 1412.89 76.8030 4 0 1 -3 1525.56 76.6697 23 0 1 -3 1472.14 74.8831 8 0 1 -3 1477.76 72.4336 20 0 -1 3 1435.79 72.6004 1 0 -1 3 1502.56 77.5798 4 -1 1 -3 791.522 42.4625 19 -1 1 -3 718.422 45.0722 24 -1 1 -3 836.936 41.0353 20 -1 1 -3 749.854 41.4527 7 -1 1 -3 774.483 43.8387 22 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23.6940 12.5654 3 -4 1 -3 17.8190 11.9764 22 -4 1 -3 37.4383 11.2880 20 -4 1 -3 36.2826 13.3231 21 -4 1 -3 27.9014 11.3957 7 -4 1 -3 25.8105 12.9341 23 4 -1 3 40.4624 9.53352 1 4 -1 3 46.9384 13.3626 6 4 -1 3 25.5462 16.0709 18 -5 1 -3 73.1371 16.3775 20 -5 1 -3 65.1284 17.7611 3 -5 1 -3 69.3668 15.9708 7 -5 1 -3 69.7984 15.5317 21 -5 1 -3 60.5380 16.3111 22 5 -1 3 61.2809 15.6644 1 5 -1 3 44.0389 20.8519 18 5 -1 3 63.4504 15.9442 6 -6 1 -3 131.059 21.7610 20 -6 1 -3 137.958 24.5851 3 -6 1 -3 141.121 22.8727 21 -6 1 -3 121.337 20.8665 7 6 -1 3 128.586 23.4768 6 6 -1 3 156.589 29.9260 18 -7 1 -3 334.552 39.4072 3 -7 1 -3 340.233 65.7114 30 -7 1 -3 278.359 32.5275 20 -7 1 -3 305.626 54.8914 27 -7 1 -3 273.271 35.3904 21 7 -1 3 390.192 40.1870 6 7 -1 3 257.720 63.1681 11 7 -1 3 263.781 47.0240 18 -8 1 -3 70.7870 53.4567 30 -8 1 -3 42.4010 29.2456 3 -8 1 -3 41.2094 22.5268 21 -8 1 -3 45.3482 39.5586 27 -8 1 -3 41.9083 74.8226 26 -8 1 -3 41.7924 23.1492 20 8 -1 3 35.2062 31.1110 18 8 -1 3 32.9890 25.7083 6 8 -1 3 30.3091 59.2742 11 -9 1 -3 119.718 66.7111 30 -9 1 -3 7.49775 75.3059 26 -9 1 -3 280.658 68.2005 27 9 -1 3 197.109 73.2324 11 -10 1 -3 -1.9504 60.4503 30 -10 1 -3 -6.6972 64.6949 26 10 -1 3 21.7712 60.5481 11 -11 1 -3 -25.466 46.4182 26 11 -1 3 2.37192 52.5636 30 11 -1 3 -16.894 48.4305 11 13 0 -3 2.20737 38.9747 26 13 0 -3 5.28224 27.9576 30 -13 0 3 17.6530 29.4531 27 12 0 -3 -9.3190 45.6538 30 12 0 -3 79.8530 45.6745 26 -12 0 3 166.071 43.8001 27 11 0 -3 0.27438 59.2701 11 11 0 -3 124.492 46.2422 26 11 0 -3 4.19100 58.0652 30 -11 0 3 129.908 48.2835 27 10 0 -3 120.031 63.3208 30 10 0 -3 -19.341 62.9505 11 10 0 -3 178.776 65.6175 26 -10 0 3 144.663 61.9060 26 -10 0 3 152.983 49.1721 27 9 0 -3 103.230 62.0826 30 9 0 -3 56.2435 26.4840 6 9 0 -3 42.6267 39.9965 2 9 0 -3 -22.798 58.4858 11 -9 0 3 51.8066 41.1926 27 -9 0 3 43.6853 56.0186 26 -9 0 3 37.3542 22.0973 21 -9 0 3 20.2525 25.0578 20 8 0 -3 92.2092 29.6589 18 8 0 -3 115.785 26.3783 6 8 0 -3 85.9835 54.5459 30 8 0 -3 117.931 26.8322 2 -8 0 3 165.632 84.6883 26 -8 0 3 103.740 27.7852 20 -8 0 3 99.5089 35.7514 27 -8 0 3 104.499 30.5386 5 -8 0 3 103.503 22.4580 21 7 0 -3 216.549 35.3663 18 7 0 -3 265.447 27.0501 2 7 0 -3 272.022 29.0275 6 -7 0 3 233.489 26.7645 21 -7 0 3 299.910 39.0959 5 -7 0 3 225.282 32.4464 20 6 0 -3 1.70655 12.1984 2 6 0 -3 -9.5966 15.2771 18 6 0 -3 1.09603 13.2978 6 6 0 -3 -3.8057 22.0584 24 -6 0 3 -5.2541 14.2325 20 -6 0 3 6.05924 11.9687 21 -6 0 3 0.15601 18.2905 5 -6 0 3 -0.4964 14.6218 22 5 0 -3 168.328 18.5356 2 5 0 -3 173.174 21.6631 8 5 0 -3 219.538 34.6545 24 5 0 -3 164.144 18.7386 6 5 0 -3 228.537 23.7386 18 -5 0 3 191.665 18.6305 21 -5 0 3 189.666 20.4311 20 -5 0 3 203.578 24.6882 22 -5 0 3 194.994 26.7053 5 -5 0 3 136.469 18.8381 3 4 0 -3 133.057 17.6405 19 4 0 -3 165.257 30.0855 24 4 0 -3 153.727 18.7769 8 4 0 -3 136.441 21.0038 4 4 0 -3 131.071 14.5834 2 4 0 -3 134.669 17.1860 18 4 0 -3 149.087 15.8260 6 -4 0 3 142.844 18.8436 5 -4 0 3 162.042 20.4364 22 -4 0 3 147.858 14.6256 21 -4 0 3 146.434 16.3081 20 -4 0 3 132.077 21.5398 23 -4 0 3 150.494 15.6733 3 -4 0 3 140.351 16.4811 9 3 0 -3 1923.84 101.041 8 3 0 -3 1865.50 98.7106 9 3 0 -3 2043.03 100.460 18 3 0 -3 1912.47 99.4240 6 3 0 -3 2168.39 102.273 19 3 0 -3 2004.44 99.8324 2 3 0 -3 2174.31 109.260 24 3 0 -3 1996.87 104.737 4 -3 0 3 2105.48 102.233 22 -3 0 3 1996.97 99.7858 20 -3 0 3 1921.08 103.100 5 -3 0 3 2197.50 103.451 23 -3 0 3 2020.71 98.8433 21 -3 0 3 1889.22 99.0390 9 2 0 -3 9261.33 447.204 8 2 0 -3 8979.97 447.887 19 2 0 -3 9010.78 448.980 4 2 0 -3 8959.84 445.258 9 2 0 -3 9497.20 445.770 2 -2 0 3 9087.98 449.051 5 -2 0 3 9815.87 445.300 21 -2 0 3 9322.38 445.320 9 -2 0 3 9999.99 446.073 20 1 0 -3 2349.64 110.245 24 1 0 -3 2014.17 100.447 9 1 0 -3 2026.43 104.960 23 1 0 -3 2096.71 103.649 19 1 0 -3 2067.21 103.565 22 1 0 -3 1997.14 103.827 4 1 0 -3 2020.48 103.130 4 1 0 -3 1937.76 101.954 8 -1 0 3 2239.30 101.043 21 -1 0 3 2042.41 100.242 9 -1 0 3 1978.02 104.918 4 0 0 -3 2676.02 131.078 20 0 0 -3 3001.97 133.762 4 0 0 -3 2597.09 133.315 22 0 0 -3 2817.53 138.759 24 0 0 -3 2481.00 131.585 7 0 0 -3 2833.62 131.163 18 0 0 -3 2480.48 134.514 4 0 0 -3 2697.69 130.875 21 0 0 -3 2876.92 134.022 19 0 0 -3 2511.79 132.276 8 0 0 -3 2809.29 135.352 23 0 0 -3 2646.61 131.019 9 0 0 3 2578.29 130.887 1 0 0 3 2756.30 130.661 9 0 0 3 2818.94 133.902 4 -1 0 -3 205.735 14.2383 21 -1 0 -3 202.549 17.3292 4 -1 0 -3 189.014 15.7500 3 -1 0 -3 193.328 16.0762 18 -1 0 -3 221.214 14.2925 9 -1 0 -3 181.656 14.7697 7 -1 0 -3 224.545 19.9654 23 -1 0 -3 201.848 13.8835 20 -1 0 -3 206.020 17.6662 19 -1 0 -3 206.243 17.9727 22 -1 0 -3 195.296 22.3394 24 -1 0 -3 192.239 15.3055 8 1 0 3 198.731 18.6237 4 1 0 3 184.106 12.7193 9 1 0 3 194.059 13.7048 1 -2 0 -3 925.764 49.8433 22 -2 0 -3 890.157 48.3767 19 -2 0 -3 976.982 50.6283 18 -2 0 -3 901.853 47.8168 8 -2 0 -3 827.200 46.6691 9 -2 0 -3 900.868 48.8495 3 -2 0 -3 899.136 47.9041 7 -2 0 -3 829.989 51.1459 24 -2 0 -3 937.194 51.1193 23 -2 0 -3 949.426 47.9570 21 -2 0 -3 922.083 47.0444 20 2 0 3 862.256 47.5425 6 2 0 3 877.767 53.2522 4 2 0 3 916.049 46.6348 1 -3 0 -3 51.5490 12.3088 23 -3 0 -3 52.9938 11.4091 7 -3 0 -3 51.1085 12.3962 21 -3 0 -3 63.5492 10.9161 20 -3 0 -3 42.1406 12.5872 3 -3 0 -3 40.3393 10.7743 22 3 0 3 33.8257 15.5005 18 3 0 3 49.1113 10.5815 6 3 0 3 48.5283 16.3929 4 3 0 3 59.6633 9.79857 1 -4 0 -3 56.8366 13.2338 22 -4 0 -3 69.9361 12.9996 7 -4 0 -3 67.4649 12.5464 20 -4 0 -3 84.5774 17.5665 3 -4 0 -3 75.5592 14.2525 21 4 0 3 85.9505 14.7652 6 4 0 3 69.5222 11.6521 1 4 0 3 51.1758 17.2885 18 -5 0 -3 220.240 23.8198 20 -5 0 -3 205.657 29.0130 3 -5 0 -3 167.169 21.7613 7 -5 0 -3 187.659 22.8101 21 5 0 3 177.347 19.3990 1 5 0 3 114.911 23.4453 18 5 0 3 173.515 24.0058 6 -6 0 -3 931.548 59.0563 21 -6 0 -3 1008.26 62.0885 3 -6 0 -3 950.984 57.9537 20 6 0 3 889.453 59.4552 6 -7 0 -3 585.915 52.3135 3 -7 0 -3 586.880 43.1263 13 -7 0 -3 617.668 77.0806 30 -7 0 -3 594.507 45.8399 20 -7 0 -3 634.313 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29.4335 5 2 -2 -3 240.507 16.0013 2 2 -2 -3 209.907 20.2191 3 2 -2 -3 217.916 19.7967 18 2 -2 -3 248.285 19.9082 8 2 -2 -3 220.445 34.6647 24 2 -2 -3 234.460 18.6528 7 2 -2 -3 165.662 22.4333 19 -2 2 3 180.058 28.3549 23 -2 2 3 250.696 15.1041 9 1 -2 -3 6.88296 7.79943 8 1 -2 -3 7.57108 7.42387 18 1 -2 -3 6.89585 12.8831 19 1 -2 -3 6.48933 9.33485 3 1 -2 -3 6.60015 7.24584 7 1 -2 -3 -2.1643 8.93415 5 1 -2 -3 -1.6475 18.9454 24 -1 2 3 2.50323 5.42741 21 -1 2 3 -5.9227 12.1373 22 -1 2 3 4.89051 4.85932 9 -1 2 3 2.12755 16.3318 23 -1 2 3 -5.3028 13.1015 5 -1 2 3 -3.6117 6.29451 20 -1 2 3 2.98037 5.32491 1 0 -2 -3 307.927 22.0360 8 0 -2 -3 309.895 26.4244 19 0 -2 -3 295.890 24.3462 22 0 -2 -3 324.892 18.4586 20 0 -2 -3 304.647 18.4676 21 0 -2 -3 329.402 36.1728 24 0 -2 -3 304.439 22.6681 3 0 -2 -3 318.212 21.7441 7 0 -2 -3 343.210 25.2994 5 0 -2 -3 342.853 22.4157 18 0 2 3 328.141 18.5581 9 0 2 3 302.416 19.9926 1 -1 -2 -3 320.117 24.0928 3 -1 -2 -3 353.120 24.0356 18 -1 -2 -3 318.564 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233.723 24.6889 24 -1 2 -4 281.769 22.6500 8 -1 2 -4 320.969 20.5307 21 -1 2 -4 256.255 18.1000 3 -1 2 -4 271.339 23.0971 19 -1 2 -4 331.812 28.3530 23 -1 2 -4 299.971 23.5435 22 -1 2 -4 301.559 18.3234 9 1 -2 4 300.359 22.6667 6 1 -2 4 273.225 19.8362 18 1 -2 4 284.799 19.0132 1 1 -2 4 266.568 27.5249 4 1 -2 4 311.612 20.8597 2 -2 2 -4 187.450 18.8490 19 -2 2 -4 200.239 16.1156 20 -2 2 -4 203.514 19.4255 8 -2 2 -4 185.353 23.0326 23 -2 2 -4 182.713 15.4978 9 -2 2 -4 186.093 16.6122 3 -2 2 -4 195.092 17.5567 7 -2 2 -4 186.516 22.0806 22 -2 2 -4 206.607 17.0676 21 2 -2 4 185.287 17.4616 2 2 -2 4 186.215 15.7665 1 2 -2 4 166.453 26.4072 4 2 -2 4 187.110 19.2021 6 2 -2 4 205.329 19.7825 18 -3 2 -4 615.146 36.9730 3 -3 2 -4 603.687 34.9213 20 -3 2 -4 593.178 40.3687 22 -3 2 -4 563.997 42.8960 23 -3 2 -4 598.705 35.5105 21 -3 2 -4 549.324 33.8263 9 -3 2 -4 602.722 37.5083 7 -3 2 -4 592.665 37.8869 8 -3 2 -4 559.079 35.9323 19 3 -2 4 596.976 35.6743 2 3 -2 4 633.767 34.8783 1 3 -2 4 622.140 40.4051 18 3 -2 4 517.694 46.0156 4 3 -2 4 615.365 39.3481 6 3 -2 4 579.376 39.1340 8 -4 2 -4 17.1755 13.1038 8 -4 2 -4 10.8077 9.18246 9 -4 2 -4 14.8312 15.2154 22 -4 2 -4 14.3408 12.5796 20 -4 2 -4 7.34783 15.9049 23 -4 2 -4 11.4507 13.6921 21 -4 2 -4 11.9773 12.6773 7 -4 2 -4 20.1990 14.4145 3 4 -2 4 11.9207 8.02042 15 4 -2 4 2.76464 14.7022 8 4 -2 4 3.42813 16.8494 18 4 -2 4 19.5079 10.4266 1 4 -2 4 4.72222 15.0987 6 -5 2 -4 108.393 23.1042 22 -5 2 -4 138.178 20.3486 20 -5 2 -4 110.566 21.1938 7 -5 2 -4 107.634 18.6121 21 -5 2 -4 132.344 23.5516 3 5 -2 4 105.994 21.7172 6 5 -2 4 107.575 26.6584 18 -6 2 -4 255.632 36.5047 3 -6 2 -4 229.872 27.8901 20 -6 2 -4 263.099 32.5328 7 -6 2 -4 226.249 30.4312 21 6 -2 4 241.405 37.9384 18 6 -2 4 232.503 34.0385 6 -7 2 -4 9.48910 21.6260 7 -7 2 -4 22.8663 39.6884 30 -7 2 -4 -0.4395 70.9160 26 -7 2 -4 36.8612 26.5396 3 -7 2 -4 16.2507 19.3028 21 -7 2 -4 43.4267 22.3201 20 7 -2 4 31.3855 24.1546 6 7 -2 4 -6.2480 52.8848 11 7 -2 4 2.69289 29.9992 18 -8 2 -4 36.0131 51.3131 30 -8 2 -4 -32.688 77.6047 26 8 -2 4 29.2512 61.0896 11 -9 2 -4 14.6963 74.2088 26 9 -2 4 127.925 68.9974 11 -10 2 -4 -44.998 61.7122 26 -10 2 -4 -41.365 55.6520 30 10 -2 4 9.38066 55.0094 11 -11 2 -4 -18.805 41.0170 26 11 -2 4 93.6024 48.3503 11 12 1 -4 8.61251 40.1151 30 12 1 -4 -7.7421 43.6751 26 -12 -1 4 17.2668 40.0904 27 11 1 -4 15.6231 45.6556 26 11 1 -4 10.8549 55.2306 30 -11 -1 4 26.0747 45.9486 27 10 1 -4 62.6979 48.7586 26 10 1 -4 19.6018 56.5276 30 -10 -1 4 53.2711 46.7727 27 9 1 -4 180.575 33.9872 6 9 1 -4 203.282 53.3344 26 9 1 -4 177.581 61.5011 30 -9 -1 4 192.871 33.5149 20 -9 -1 4 201.971 50.0974 27 -9 -1 4 170.858 28.3670 21 -9 -1 4 119.476 38.9722 5 8 1 -4 251.869 74.8683 30 8 1 -4 303.558 59.3321 26 8 1 -4 298.314 34.9065 2 8 1 -4 354.860 40.8774 6 -8 -1 4 282.777 33.3583 21 -8 -1 4 289.197 54.5658 27 -8 -1 4 303.282 47.4822 5 -8 -1 4 304.655 61.1600 26 -8 -1 4 337.413 40.6824 20 7 1 -4 186.368 43.0982 24 7 1 -4 252.685 30.7656 2 7 1 -4 245.277 32.0673 6 -7 -1 4 263.986 38.5786 5 -7 -1 4 242.242 28.2885 21 -7 -1 4 217.454 33.5354 20 6 1 -4 111.561 20.6413 6 6 1 -4 93.9735 32.4758 24 6 1 -4 122.648 19.9668 2 -6 -1 4 107.714 25.6654 5 -6 -1 4 81.7584 17.3730 21 -6 -1 4 92.5684 21.0038 20 5 1 -4 1898.67 103.494 2 5 1 -4 1968.70 118.800 24 5 1 -4 2283.30 105.397 6 -5 -1 4 1899.52 110.686 5 -5 -1 4 2141.00 105.236 20 -5 -1 4 2091.20 106.424 22 -5 -1 4 1915.58 102.905 21 4 1 -4 1173.06 71.6710 2 4 1 -4 1532.38 73.3264 6 4 1 -4 1344.12 73.9995 8 4 1 -4 1544.76 75.1200 19 4 1 -4 1399.74 81.3281 4 4 1 -4 1411.87 87.2171 24 -4 -1 4 1503.49 76.6787 23 -4 -1 4 1249.52 71.1923 21 -4 -1 4 1630.31 74.0854 20 -4 -1 4 1188.14 76.6643 5 3 1 -4 2436.14 122.770 6 3 1 -4 2336.33 123.722 8 3 1 -4 2296.68 121.257 9 3 1 -4 2504.99 125.863 22 3 1 -4 2590.29 125.326 19 3 1 -4 2653.76 134.172 24 3 1 -4 2402.92 122.283 2 3 1 -4 2443.94 129.624 4 -3 -1 4 2591.16 122.303 21 -3 -1 4 2514.52 126.748 5 -3 -1 4 2487.13 122.619 20 -3 -1 4 2447.17 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8 -3 1 -4 48.2868 15.6021 23 -3 1 -4 57.5757 12.3685 21 -3 1 -4 46.4642 11.0039 20 -3 1 -4 53.5050 12.7825 7 -3 1 -4 50.8678 13.4043 3 -3 1 -4 36.3501 13.6095 22 3 -1 4 51.2410 19.6409 4 3 -1 4 31.3794 13.1129 6 3 -1 4 32.5528 9.32862 1 3 -1 4 51.5813 14.2603 18 -4 1 -4 100.202 17.8233 7 -4 1 -4 77.6154 15.7329 21 -4 1 -4 69.7256 16.9185 22 -4 1 -4 108.507 19.4925 3 -4 1 -4 95.0971 15.1074 20 -4 1 -4 91.9545 19.2766 23 4 -1 4 78.0056 20.1081 18 4 -1 4 97.2884 13.8995 1 4 -1 4 93.6352 17.8682 6 -5 1 -4 49.0429 18.9736 3 -5 1 -4 49.7754 16.4696 21 -5 1 -4 62.4888 18.4322 7 -5 1 -4 67.3989 17.3621 20 5 -1 4 42.2192 23.1209 18 5 -1 4 56.1468 18.7357 6 5 -1 4 59.6005 13.3744 1 -6 1 -4 430.020 43.3621 3 -6 1 -4 434.769 36.8239 20 -6 1 -4 433.924 37.6610 7 -6 1 -4 399.381 35.3122 21 6 -1 4 413.330 40.5874 6 6 -1 4 454.683 68.1881 11 6 -1 4 385.997 47.9501 18 -7 1 -4 83.7925 23.2181 20 -7 1 -4 67.1191 20.6291 21 -7 1 -4 53.4681 70.0157 26 -7 1 -4 28.5513 40.1629 30 -7 1 -4 78.8164 30.1274 3 7 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42.2203 5 -8 0 4 128.325 51.9034 26 -8 0 4 145.356 23.5558 21 -8 0 4 198.677 43.7300 27 -8 0 4 134.068 27.4293 20 7 0 -4 30.9412 32.7326 24 7 0 -4 51.4707 19.6763 2 7 0 -4 57.7497 19.6804 6 -7 0 4 49.0098 20.5091 20 -7 0 4 37.8047 15.9598 21 -7 0 4 54.4366 25.5727 5 6 0 -4 2719.59 160.322 24 6 0 -4 2954.16 144.992 6 6 0 -4 2962.84 145.044 2 -6 0 4 2931.18 145.960 20 -6 0 4 3147.52 153.883 5 -6 0 4 2679.08 142.401 21 -6 0 4 2612.30 147.870 22 5 0 -4 1900.06 97.7458 6 5 0 -4 1889.19 111.857 24 5 0 -4 1947.58 99.7311 19 5 0 -4 1828.84 97.7298 2 5 0 -4 1800.06 100.685 8 -5 0 4 2034.55 104.994 5 -5 0 4 1906.18 101.667 22 -5 0 4 1915.68 95.9952 21 -5 0 4 1858.73 98.0842 20 4 0 -4 701.038 43.7953 19 4 0 -4 691.238 39.8153 2 4 0 -4 676.148 47.8780 4 4 0 -4 645.922 39.3797 6 4 0 -4 690.798 54.6617 24 4 0 -4 711.013 43.5526 8 -4 0 4 712.133 40.7120 20 -4 0 4 666.119 38.8971 21 -4 0 4 715.429 47.0745 23 -4 0 4 710.864 45.7534 5 -4 0 4 775.216 45.5436 22 3 0 -4 32.3647 22.4807 24 3 0 -4 24.0755 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34.9381 66.3751 26 3 4 -10 85.2544 25.8085 2 3 4 -10 70.0525 31.5661 19 3 4 -10 83.1758 51.9516 30 3 4 -10 110.353 36.6158 22 3 4 -10 56.2132 38.3060 24 3 4 -10 125.286 127.527 25 3 4 -10 117.298 32.4346 8 3 4 -10 114.670 134.898 28 -3 -4 10 87.7795 30.0356 21 -3 -4 10 73.7713 28.7532 1 -3 -4 10 86.1490 29.1374 20 -3 -4 10 210.205 66.1182 29 2 4 -10 168.155 125.773 25 2 4 -10 85.3746 30.3914 19 2 4 -10 177.194 39.5161 22 2 4 -10 38.2118 70.0005 26 2 4 -10 194.577 28.4110 2 2 4 -10 130.334 52.7759 30 2 4 -10 129.016 30.2937 8 2 4 -10 244.196 140.784 28 -2 -4 10 137.732 30.7033 1 -2 -4 10 82.9438 30.1415 20 -2 -4 10 121.928 29.9649 21 1 4 -10 -22.850 134.035 28 1 4 -10 -9.1248 64.7846 26 1 4 -10 25.1099 28.7614 19 1 4 -10 -0.7335 126.208 25 1 4 -10 44.8045 28.1277 8 1 4 -10 40.7676 51.3360 30 1 4 -10 45.9609 22.0369 2 1 4 -10 56.0350 34.3142 22 -1 -4 10 12.1567 26.9987 1 -1 -4 10 28.0756 27.7419 20 -1 -4 10 26.6915 25.5843 21 0 4 -10 18.9729 27.9767 19 0 4 -10 42.9576 28.6912 8 0 4 -10 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-13 -26.072 87.9102 25 2 6 -13 38.5652 49.2350 30 1 6 -13 -13.880 54.4981 26 1 6 -13 -11.798 47.6548 30 1 6 -13 7.62149 92.6956 28 1 6 -13 18.7697 80.9795 25 0 6 -13 3.90306 94.5859 28 0 6 -13 20.8715 46.5282 30 0 6 -13 26.4423 70.2302 25 0 6 -13 19.6803 53.4583 26 -1 6 -13 -0.6749 47.8245 26 -1 6 -13 22.3412 85.5266 28 -1 6 -13 93.0620 45.8845 30 1 -6 13 57.7103 78.0426 25 -2 6 -13 128.931 44.4225 30 -2 6 -13 -32.539 74.5235 28 -2 6 -13 -8.1681 43.0370 26 -3 6 -13 0.69570 63.0329 28 -3 6 -13 -3.3417 34.6540 26 -3 6 -13 45.8370 37.7375 30 7 5 -13 0.96675 26.8652 30 7 5 -13 -6.2905 36.8858 26 -7 -5 13 -1.7672 41.3128 29 6 5 -13 13.9353 34.5725 30 6 5 -13 41.2621 61.7827 25 6 5 -13 6.10104 33.6886 26 -6 -5 13 1.50496 43.7337 29 5 5 -13 289.521 90.7497 25 5 5 -13 241.364 56.7778 30 -5 -5 13 37.4385 46.0500 29 4 5 -13 118.329 47.9808 30 4 5 -13 -12.317 42.3798 26 4 5 -13 62.6286 80.6833 28 4 5 -13 113.850 96.5685 25 3 5 -13 20.9371 94.5506 28 3 5 -13 -8.8568 90.2055 25 3 5 -13 17.2311 47.0744 30 3 5 -13 -10.865 46.0314 26 2 5 -13 3.52798 92.7211 28 2 5 -13 -3.7706 48.4084 26 2 5 -13 -8.3127 47.4912 30 2 5 -13 -49.659 86.0869 25 1 5 -13 55.6380 102.189 28 1 5 -13 38.7924 46.9835 30 1 5 -13 -0.5726 50.8862 26 1 5 -13 10.2467 81.6701 25 0 5 -13 33.7227 97.1625 28 0 5 -13 224.611 66.8037 30 0 5 -13 148.450 78.0381 25 -1 5 -13 56.8924 57.0718 25 -1 5 -13 -17.961 44.5529 26 -1 5 -13 -32.606 86.7797 28 -1 5 -13 96.1760 44.3948 30 -2 5 -13 3.77035 39.5084 26 -2 5 -13 121.664 43.3211 30 -2 5 -13 -4.9470 81.0758 28 -3 5 -13 0.45447 31.5826 26 -3 5 -13 -10.806 65.3214 28 -3 5 -13 24.7539 34.3878 30 8 4 -13 62.7549 27.6727 30 -8 -4 13 8.61002 35.0956 29 7 4 -13 55.5084 36.2931 30 7 4 -13 2.08349 36.0942 26 -7 -4 13 24.5712 43.5343 29 6 4 -13 46.7482 69.7559 25 6 4 -13 11.9592 33.3757 26 6 4 -13 34.3796 39.2042 30 -6 -4 13 13.7364 45.1444 29 5 4 -13 -3.5048 36.6940 26 5 4 -13 -8.1834 82.3711 25 5 4 -13 25.3460 43.7094 30 5 4 -13 28.2503 87.6316 28 -5 -4 13 11.4560 45.5677 29 4 4 -13 37.5730 97.1960 25 4 4 -13 13.8431 91.9103 28 4 4 -13 126.930 48.4955 30 4 4 -13 3.57118 41.7900 26 -4 -4 13 48.4129 57.9814 29 3 4 -13 0.77203 44.1795 26 3 4 -13 36.1355 45.8022 30 3 4 -13 4.59405 102.519 28 3 4 -13 -46.108 92.2206 25 2 4 -13 50.8584 104.210 28 2 4 -13 6.67508 88.5084 25 2 4 -13 11.3695 45.7372 26 1 4 -13 73.7870 47.8487 30 1 4 -13 -11.215 75.3830 25 1 4 -13 18.7727 104.902 28 1 4 -13 2.55865 45.9234 26 0 4 -13 -4.3117 45.4608 26 0 4 -13 22.0618 45.1002 30 0 4 -13 -21.617 58.9696 25 0 4 -13 5.36249 98.0989 28 -1 4 -13 295.795 97.7706 25 -1 4 -13 32.2951 93.5381 28 -1 4 -13 448.646 64.7673 30 -2 4 -13 15.6192 36.5887 26 -2 4 -13 30.5530 36.5968 30 -2 4 -13 18.3431 76.4106 28 -3 4 -13 10.8980 39.5484 26 -3 4 -13 22.7103 28.7148 30 -3 4 -13 -4.6088 59.5262 28 8 3 -13 106.686 31.5939 30 -8 -3 13 8.21868 38.5665 29 7 3 -13 10.7066 35.0819 30 -7 -3 13 14.9144 42.5151 29 6 3 -13 14.6870 71.7100 25 6 3 -13 100.141 41.6656 30 -6 -3 13 19.2914 46.2513 29 5 3 -13 -0.3222 90.4613 25 5 3 -13 44.9901 42.4977 30 5 3 -13 -11.863 84.2256 28 -5 -3 13 19.0144 45.8181 29 4 3 -13 1.36993 92.5253 25 4 3 -13 8.63487 89.9491 28 4 3 -13 5.86090 45.1838 26 4 3 -13 118.332 48.7641 30 -4 -3 13 44.5921 44.5290 29 3 3 -13 19.1727 88.9725 25 3 3 -13 13.0132 41.5404 26 3 3 -13 19.4985 100.051 28 2 3 -13 -13.634 92.8576 28 2 3 -13 9.61223 84.2377 25 2 3 -13 11.9660 43.1349 26 1 3 -13 -4.4143 101.604 28 1 3 -13 55.7588 45.6351 30 1 3 -13 -0.7120 41.5078 26 1 3 -13 18.0718 72.5996 25 0 3 -13 -11.172 39.1047 26 0 3 -13 66.5955 93.6773 28 0 3 -13 14.9898 42.3152 30 0 3 -13 -7.9716 56.0929 25 -1 3 -13 7.91538 36.6078 26 -1 3 -13 -8.1217 81.6763 28 -1 3 -13 2.65300 37.3080 30 -2 3 -13 89.9752 33.2912 30 -2 3 -13 0.59771 42.5409 26 -2 3 -13 -3.2596 67.6163 28 -3 3 -13 5.56780 34.2063 26 -3 3 -13 5.43332 24.9258 30 8 2 -13 14.5893 31.0564 30 -8 -2 13 -15.448 37.6530 29 7 2 -13 15.1171 57.7846 25 7 2 -13 22.9092 34.4797 30 -7 -2 13 11.7187 43.4950 29 6 2 -13 -9.6305 64.8916 25 6 2 -13 -31.942 78.3349 28 6 2 -13 9.34109 37.1849 30 -6 -2 13 -4.1830 46.0109 29 5 2 -13 34.2907 89.7066 28 5 2 -13 5.31836 89.3657 25 5 2 -13 71.6601 42.5395 30 -5 -2 13 12.8072 43.6202 29 4 2 -13 149.340 47.2759 30 4 2 -13 8.74022 96.9211 28 4 2 -13 4.94362 88.2516 25 3 2 -13 52.1783 88.9737 25 3 2 -13 13.6694 98.6319 28 2 2 -13 -7.9616 80.2740 25 2 2 -13 0.80356 100.805 28 2 2 -13 91.1688 46.8815 30 1 2 -13 -1.9325 65.4743 25 1 2 -13 16.5493 41.6598 30 1 2 -13 21.4141 97.2437 28 0 2 -13 -59.036 84.3057 28 0 2 -13 1.74545 37.8952 30 0 2 -13 -0.1448 48.5711 25 -1 2 -13 63.7605 32.7772 30 -1 2 -13 -24.612 80.0773 28 -2 2 -13 19.8390 25.4998 30 -2 2 -13 -14.970 59.9488 28 8 1 -13 64.9465 30.4107 30 -8 -1 13 6.72737 35.6244 29 7 1 -13 18.2561 34.5484 30 7 1 -13 -1.8471 63.6952 28 7 1 -13 26.8741 61.4909 25 -7 -1 13 5.17152 42.4118 29 6 1 -13 4.78997 70.0684 25 6 1 -13 22.5664 39.9453 30 6 1 -13 5.44191 80.8813 28 -6 -1 13 27.2048 46.5416 29 5 1 -13 2.92340 43.9590 30 5 1 -13 29.1380 91.8399 28 5 1 -13 -7.3555 85.2668 25 -5 -1 13 45.9226 47.4987 29 4 1 -13 39.4325 81.3943 25 4 1 -13 177.249 51.3858 29 4 1 -13 27.3445 87.3197 28 3 1 -13 145.964 45.0142 30 3 1 -13 17.8407 79.2112 25 3 1 -13 -46.435 96.4646 28 2 1 -13 36.9165 39.0452 30 2 1 -13 -10.437 88.1776 28 2 1 -13 21.3239 74.4982 25 1 1 -13 2.59067 35.1146 30 1 1 -13 7.35169 56.9627 25 1 1 -13 -13.365 84.2714 28 0 1 -13 -0.3184 30.3287 30 0 1 -13 5.37490 45.4529 25 0 1 -13 0.50632 78.7902 28 -1 1 -13 13.9617 38.4777 30 -1 1 -13 -20.275 68.4278 28 -8 0 13 -4.6085 31.7294 29 7 0 -13 20.5288 31.4713 30 7 0 -13 0.22803 54.5438 25 7 0 -13 -9.6554 65.0475 28 -7 0 13 7.95595 40.2929 29 6 0 -13 -32.964 77.8028 28 6 0 -13 13.4750 36.2686 30 6 0 -13 21.9456 71.6489 25 -6 0 13 19.7049 43.9199 29 5 0 -13 18.3567 78.1562 28 5 0 -13 -36.955 48.1408 29 5 0 -13 67.2857 40.7746 30 5 0 -13 33.1678 82.9585 25 4 0 -13 -22.237 87.0918 28 4 0 -13 41.1217 80.7190 25 4 0 -13 -6.4911 46.6003 29 4 0 -13 79.8324 36.0117 30 3 0 -13 -4.7879 87.1637 28 3 0 -13 3.24653 77.4963 25 2 0 -13 -3.5043 64.4271 25 2 0 -13 8.75348 78.7995 28 2 0 -13 10.5909 39.4238 30 1 0 -13 27.9557 49.2815 25 1 0 -13 -0.1651 82.4634 28 0 0 -13 4.73360 70.8684 28 7 -1 -13 -37.294 55.0384 28 7 -1 -13 -23.550 51.3154 25 -7 1 13 19.4582 35.4535 29 6 -1 -13 -6.1850 71.1065 28 6 -1 -13 31.4619 65.1786 25 6 -1 -13 -29.268 38.2683 29 5 -1 -13 -12.769 66.2405 25 5 -1 -13 -9.7192 45.1644 29 5 -1 -13 10.2399 77.1359 28 4 -1 -13 -5.6700 75.7594 28 4 -1 -13 32.9832 47.7392 29 4 -1 -13 3.23861 70.1840 25 3 -1 -13 -14.155 80.6392 28 3 -1 -13 18.2129 67.0692 25 3 -1 -13 8.02916 19.1978 16 2 -1 -13 44.9374 76.3096 28 2 -1 -13 12.5471 17.2014 16 2 -1 -13 -0.8440 51.8306 25 1 -1 -13 -5.2727 40.0195 25 1 -1 -13 -15.720 63.5368 28 6 -2 -13 14.8576 14.2334 16 6 -2 -13 -15.032 55.2244 25 6 -2 -13 24.0599 57.9547 28 6 -2 -13 -1.9443 32.4469 29 5 -2 -13 14.7601 67.1514 28 5 -2 -13 4.84499 60.8467 25 5 -2 -13 12.0168 15.9526 16 5 -2 -13 -7.0571 40.8802 29 4 -2 -13 105.714 25.5873 16 4 -2 -13 32.1303 39.0807 29 4 -2 -13 3.38186 69.5849 28 4 -2 -13 1.50515 56.9834 25 3 -2 -13 18.5852 54.8311 25 3 -2 -13 22.7240 16.0512 16 3 -2 -13 -0.3698 67.4045 28 2 -2 -13 24.5040 108.670 28 2 -2 -13 8.17278 40.8986 25 2 8 -14 -4.9190 32.3216 26 -2 -8 14 4.00612 54.9797 25 1 8 -14 -0.6846 32.2443 26 -1 -8 14 0.81210 57.8584 25 4 7 -14 10.6121 27.0653 26 -4 -7 14 3.98541 51.7338 25 3 7 -14 33.2524 29.8258 30 3 7 -14 -4.7571 29.4366 26 -3 -7 14 14.8822 58.4564 25 2 7 -14 -1.2723 31.8454 26 2 7 -14 -5.3623 31.0305 30 -2 -7 14 24.3262 60.9447 25 1 7 -14 -1.2000 31.7281 26 1 7 -14 35.7739 57.9266 28 1 7 -14 21.3348 32.9426 30 -1 -7 14 11.6672 60.5944 25 0 7 -14 31.0140 58.2033 28 0 7 -14 27.2011 33.9389 30 0 7 -14 5.49483 31.8563 26 0 -7 14 -19.366 48.3656 25 -1 7 -14 27.1736 36.9621 30 5 6 -14 9.05974 31.9140 30 5 6 -14 10.5261 33.2401 26 -5 -6 14 -12.587 47.9919 25 4 6 -14 28.2960 33.4713 30 4 6 -14 66.0416 57.6254 25 4 6 -14 -0.8996 38.2027 26 -4 -6 14 35.7714 59.2804 25 3 6 -14 8.95089 53.7990 25 3 6 -14 22.3133 36.7666 30 3 6 -14 30.6311 77.0528 28 3 6 -14 0.05197 33.4138 26 -3 -6 14 -6.4681 59.5508 25 2 6 -14 -2.3730 34.0648 26 2 6 -14 5.73233 36.8802 30 2 6 -14 -15.911 53.0057 25 2 6 -14 -23.729 64.4959 28 -2 -6 14 -14.560 62.3281 25 1 6 -14 -4.8622 32.7305 26 1 6 -14 6.96401 51.2707 25 1 6 -14 1.26053 66.3820 28 1 6 -14 9.97674 37.1244 30 -1 -6 14 16.4635 67.1516 25 0 6 -14 6.40060 64.3718 28 0 6 -14 36.0217 36.1048 30 0 6 -14 -6.5585 30.7453 26 0 -6 14 2.59460 59.1589 25 -1 6 -14 16.4318 55.4560 28 -1 6 -14 5.82382 35.0360 26 -1 6 -14 67.5035 32.8930 30 6 5 -14 3.98944 29.0672 30 5 5 -14 11.9792 32.1942 30 5 5 -14 -5.7906 34.5329 26 5 5 -14 25.2748 49.0918 25 4 5 -14 -8.0557 82.1092 28 4 5 -14 5.03443 71.2568 25 4 5 -14 16.1043 37.6085 30 4 5 -14 2.03550 40.1892 26 3 5 -14 11.5908 42.9900 26 3 5 -14 32.5038 61.1502 25 3 5 -14 36.4793 38.5877 30 3 5 -14 -35.487 64.0819 28 2 5 -14 -4.2853 61.6993 25 2 5 -14 -14.357 42.9967 26 2 5 -14 -10.056 66.3158 28 2 5 -14 27.3739 38.5669 30 1 5 -14 -3.9296 42.3482 26 1 5 -14 16.9274 55.0327 25 1 5 -14 67.0594 39.0135 30 1 5 -14 -12.695 73.0395 28 0 5 -14 9.19906 67.8575 28 0 5 -14 128.142 46.6634 25 0 5 -14 144.924 46.4491 30 0 -5 14 79.9716 63.6245 25 -1 5 -14 -0.6152 35.4356 26 -1 5 -14 28.0207 30.1780 30 -1 5 -14 -10.308 56.2248 28 6 4 -14 13.2148 29.4929 30 6 4 -14 10.1060 61.6754 25 5 4 -14 24.7571 34.3900 30 5 4 -14 14.3298 59.2758 25 4 4 -14 15.7576 38.2952 26 4 4 -14 46.4982 67.6357 25 4 4 -14 8.68768 66.6644 28 3 4 -14 16.0727 68.2625 28 3 4 -14 127.871 40.9379 30 3 4 -14 26.4731 67.0175 25 3 4 -14 24.7475 43.3804 26 2 4 -14 0.28352 42.7365 26 2 4 -14 -8.5383 71.8683 28 2 4 -14 24.1394 37.7586 30 2 4 -14 25.0364 64.2690 25 1 4 -14 6.61139 42.5012 26 1 4 -14 89.5389 37.2764 30 1 4 -14 17.7850 51.0787 25 1 4 -14 -9.3318 67.2550 28 0 4 -14 14.3205 39.2807 25 0 4 -14 -7.5736 31.8975 30 0 4 -14 -29.913 66.5382 28 0 4 -14 0.58487 37.9957 26 -1 4 -14 -7.2931 57.5224 28 -1 4 -14 71.1609 28.8364 30 6 3 -14 -7.9861 27.8806 30 6 3 -14 9.40836 51.6128 25 -6 -3 14 10.1030 33.1399 29 5 3 -14 16.3594 60.8939 28 5 3 -14 5.69335 35.4385 30 5 3 -14 15.6480 60.5614 25 -5 -3 14 20.9228 33.6041 29 4 3 -14 11.0571 65.4564 25 4 3 -14 53.4359 64.9123 28 3 3 -14 47.9778 76.1229 28 3 3 -14 43.8748 66.7207 25 3 3 -14 75.8936 34.4762 30 2 3 -14 19.9915 72.1523 28 2 3 -14 66.0178 35.2778 30 2 3 -14 -0.4949 60.5462 25 1 3 -14 26.6373 45.9310 25 1 3 -14 -2.5912 31.0766 30 1 3 -14 -6.5647 71.2536 28 0 3 -14 27.7189 48.1320 25 0 3 -14 8.96989 64.2594 28 0 3 -14 35.2755 28.0923 30 -1 3 -14 74.0428 35.6785 30 -1 3 -14 -19.295 73.4230 28 6 2 -14 15.5610 27.0223 30 6 2 -14 7.28528 46.9790 25 5 2 -14 21.3407 60.9939 25 5 2 -14 -16.998 64.3940 28 5 2 -14 57.3538 30.9337 30 -5 -2 14 17.7523 34.3355 29 4 2 -14 12.8487 64.1559 28 4 2 -14 77.5699 31.6243 30 4 2 -14 1.64191 61.4081 25 3 2 -14 -10.377 66.6318 28 3 2 -14 33.1266 30.9244 30 3 2 -14 -6.3250 59.5577 25 2 2 -14 2.26537 51.9557 25 2 2 -14 6.95425 26.8446 30 2 2 -14 -20.417 70.1583 28 1 2 -14 15.4173 39.6720 25 1 2 -14 38.3823 27.1249 30 1 2 -14 -0.7770 68.9413 28 0 2 -14 -14.718 59.5667 28 0 2 -14 41.8421 34.3935 30 6 1 -14 28.0546 47.1175 25 5 1 -14 26.9444 25.2353 30 5 1 -14 30.3666 56.3132 28 5 1 -14 8.56229 54.6490 25 4 1 -14 19.0376 63.1731 28 4 1 -14 93.7325 28.0865 30 4 1 -14 21.0715 58.6995 25 3 1 -14 36.4661 64.1800 28 3 1 -14 1.66138 53.6170 25 3 1 -14 56.5349 26.1016 30 2 1 -14 26.8028 24.8395 30 2 1 -14 6.73769 45.0638 25 2 1 -14 10.2290 67.1663 28 1 1 -14 -12.145 54.5135 28 5 0 -14 -14.391 52.8766 25 5 0 -14 -9.1121 53.5301 28 4 0 -14 -9.1908 50.1049 25 4 0 -14 12.5679 25.5408 16 4 0 -14 -19.674 56.3695 28 3 0 -14 -7.4291 60.0789 28 3 0 -14 21.5832 49.6088 25 2 0 -14 -8.0121 74.2076 28 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details 'SADABS 2014/5' _exptl_absorpt_correction_type multi-scan _exptl_absorpt_correction_T_max 0.7531 _exptl_absorpt_correction_T_min 0.5787 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 1.54192 11.124 11.898 12.222 106.737 101.642 100.177 ) ; _shelx_hkl_checksum 69906 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_type_symbol _atom_site_label _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_calc_flag _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_refinement_flags_posn _atom_site_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C C1 0.7286(7) 0.4962(6) 0.1586(6) 0.0285(16) Uani d U . . 1.0 . . C C2 0.6804(7) 0.4011(6) 0.0542(6) 0.0319(18) Uani d U . . 1.0 . . H H2 0.7348 0.3733 0.0073 0.038 Uiso calc U . R 1.0 . . C C3 0.5528(7) 0.3460(6) 0.0173(7) 0.0344(18) Uani d U . . 1.0 . . H H3 0.5185 0.2796 -0.0546 0.041 Uiso calc U . R 1.0 . . C C4 0.4749(7) 0.3888(6) 0.0869(6) 0.0323(17) Uani d U . . 1.0 . . H H4 0.387 0.3513 0.0648 0.039 Uiso calc U . R 1.0 . . C C5 0.5289(7) 0.4872(6) 0.1886(6) 0.0289(16) Uani d U . . 1.0 . . C C6 0.3386(6) 0.4522(6) 0.2577(6) 0.0327(18) Uani d U . . 1.0 . . H H6A 0.2754 0.4375 0.1833 0.049 Uiso calc U . R 1.0 . . H H6B 0.3056 0.4875 0.3249 0.049 Uiso calc U . R 1.0 . . H H6C 0.3569 0.3755 0.261 0.049 Uiso calc U . R 1.0 . . C C7 0.4474(7) 0.6575(6) 0.2763(6) 0.0300(17) Uani d U . . 1.0 . . C C8 0.3340(7) 0.6839(7) 0.2457(6) 0.0361(19) Uani d U . . 1.0 . . H H8 0.2572 0.623 0.2221 0.043 Uiso calc U . R 1.0 . . C C9 0.3322(7) 0.8011(7) 0.2496(6) 0.0365(19) Uani d U . . 1.0 . . H H9 0.2546 0.8214 0.2259 0.044 Uiso calc U . R 1.0 . . C C10 0.4450(7) 0.8870(7) 0.2883(6) 0.0344(18) Uani d U . . 1.0 . . H H10 0.446 0.968 0.2918 0.041 Uiso calc U . R 1.0 . . C C11 0.5574(7) 0.8558(6) 0.3221(6) 0.0313(17) Uani d U . . 1.0 . . C C12 0.7658(7) 0.9589(6) 0.4625(6) 0.0293(17) Uani d U . . 1.0 . . C C13 0.8248(7) 1.0746(6) 0.5384(6) 0.0348(18) Uani d U . . 1.0 . . H H13 0.8024 1.1425 0.5215 0.042 Uiso calc U . R 1.0 . . C C14 0.9158(7) 1.0902(7) 0.6383(7) 0.0378(19) Uani d U . . 1.0 . . H H14 0.9583 1.1694 0.6914 0.045 Uiso calc U . R 1.0 . . C C15 0.9459(7) 0.9906(6) 0.6618(6) 0.0356(19) Uani d U . . 1.0 . . H H15 1.0066 0.9999 0.7326 0.043 Uiso calc U . R 1.0 . . C C16 0.8858(7) 0.8768(6) 0.5802(6) 0.0314(17) Uani d U . . 1.0 . . C C17 0.9654(8) 0.7818(7) 0.7232(7) 0.045(2) Uani d U . . 1.0 . . H H17A 0.9621 0.7005 0.7277 0.067 Uiso calc U . R 1.0 . . H H17B 0.9139 0.8206 0.7716 0.067 Uiso calc U . R 1.0 . . H H17C 1.0533 0.8302 0.753 0.067 Uiso calc U . R 1.0 . . C C18 0.9591(7) 0.6948(6) 0.5114(7) 0.0330(17) Uani d U . . 1.0 . . C C19 1.0717(7) 0.6655(6) 0.5444(7) 0.0350(18) Uani d U . . 1.0 . . H H19 1.1168 0.69 0.6256 0.042 Uiso calc U . R 1.0 . . C C20 1.1187(7) 0.5979(7) 0.4546(7) 0.0414(19) Uani d U . . 1.0 . . H H20 1.1977 0.5783 0.4734 0.05 Uiso calc U . R 1.0 . . C C21 1.0463(7) 0.5609(6) 0.3382(7) 0.0345(18) Uani d U . . 1.0 . . H H21 1.0758 0.5161 0.2757 0.041 Uiso calc U . R 1.0 . . C C22 0.9321(7) 0.5890(6) 0.3137(7) 0.0310(17) Uani d U . . 1.0 . . N N1 0.6542(5) 0.5438(5) 0.2264(5) 0.0283(13) Uani d U . . 1.0 . . N N2 0.4544(5) 0.5356(5) 0.2635(5) 0.0320(14) Uani d U . . 1.0 . . N N3 0.5623(5) 0.7406(5) 0.3153(5) 0.0307(14) Uani d U . . 1.0 . . N N4 0.6682(5) 0.9455(5) 0.3657(5) 0.0316(15) Uani d U . . 1.0 . . H H4N 0.6779 0.9988 0.329 0.038 Uiso calc U . R 1.0 . . N N5 0.7954(5) 0.8587(5) 0.4790(5) 0.0285(14) Uani d U . . 1.0 . . N N6 0.9159(5) 0.7732(5) 0.5996(5) 0.0337(15) Uani d U . . 1.0 . . N N7 0.8842(5) 0.6584(5) 0.3974(5) 0.0318(14) Uani d U . . 1.0 . . N N8 0.8572(5) 0.5460(5) 0.1984(5) 0.0334(15) Uani d U . . 1.0 . . H H8A 0.8965 0.5511 0.1435 0.04 Uiso calc U . R 1.0 . . Co Co1 0.72343(10) 0.69876(9) 0.35674(10) 0.0297(4) Uani d U . . 1.0 . . C C23 0.7866(8) 0.9271(7) -0.0384(7) 0.049(2) Uani d U . . 1.0 . . H H23A 0.73 0.8851 -0.1182 0.074 Uiso calc U . R 1.0 . . H H23B 0.8247 0.8692 -0.0095 0.074 Uiso calc U . R 1.0 . . H H23C 0.8536 0.9911 -0.0409 0.074 Uiso calc U . R 1.0 . . C C24 0.7130(8) 0.9816(7) 0.0430(7) 0.047(2) Uani d U . . 1.0 . . C C25 0.6656(9) 1.0872(8) 0.0256(8) 0.064(3) Uani d U . . 1.0 . . H H25A 0.607 1.0621 -0.0534 0.096 Uiso calc U . R 1.0 . . H H25B 0.7373 1.1523 0.0329 0.096 Uiso calc U . R 1.0 . . H H25C 0.6216 1.1163 0.086 0.096 Uiso calc U . R 1.0 . . O O3 0.6900(6) 0.9415(6) 0.1204(5) 0.0703(19) Uani d U . . 1.0 . . B B1 1.0009(9) 0.6924(9) 0.0245(9) 0.039(2) Uani d U . . 1.0 . . F F1 1.0212(4) 0.6467(4) -0.0880(4) 0.0509(12) Uani d U . . 1.0 . . F F2 1.0588(4) 0.6374(4) 0.0982(4) 0.0470(12) Uani d U . . 1.0 . . F F3 1.0497(4) 0.8153(4) 0.0692(4) 0.0540(13) Uani d U . . 1.0 . . F F4 0.8702(4) 0.6655(4) 0.0119(4) 0.0434(11) Uani d U . . 1.0 . . B B2 0.4564(9) 0.7588(9) 0.6467(9) 0.059(2) Uani d U . D 1.0 . . F F5 0.4270(14) 0.6379(9) 0.5949(11) 0.0617(17) Uani d U P D 0.506(7) A 1 F F6 0.4960(10) 0.7975(9) 0.7678(8) 0.0617(17) Uani d U P D 0.506(7) A 1 F F7 0.5690(9) 0.8021(8) 0.6180(10) 0.0617(17) Uani d U P D 0.506(7) A 1 F F8 0.3656(11) 0.8167(12) 0.6126(11) 0.0617(17) Uani d U P D 0.506(7) A 1 F F5A 0.441(2) 0.6428(17) 0.5592(16) 0.0617(17) Uani d U P D 0.296(6) A 2 F F6A 0.5470(17) 0.8143(16) 0.7427(17) 0.0617(17) Uani d U P D 0.296(6) A 2 F F7A 0.3632(15) 0.7051(14) 0.7082(14) 0.0617(17) Uani d U P D 0.296(6) A 2 F F8A 0.390(2) 0.8156(19) 0.5809(18) 0.0617(17) Uani d U P D 0.296(6) A 2 F F5B 0.403(3) 0.642(2) 0.640(3) 0.0617(17) Uani d U P D 0.198(6) A 3 F F6B 0.592(2) 0.798(2) 0.680(3) 0.0617(17) Uani d U P D 0.198(6) A 3 F F7B 0.467(2) 0.750(2) 0.5290(19) 0.0617(17) Uani d U P D 0.198(6) A 3 F F8B 0.372(2) 0.825(2) 0.670(2) 0.0617(17) Uani d U P D 0.198(6) A 3 O O1 0.7845(5) 0.7771(4) 0.2161(4) 0.0342(12) Uani d U . D 1.0 . . H H1W 0.760(6) 0.838(4) 0.187(5) 0.041 Uiso d U . D 1.0 . . H H2W 0.809(6) 0.727(4) 0.154(4) 0.041 Uiso d U . D 1.0 . . O O2 0.6646(4) 0.6153(4) 0.4865(4) 0.0348(13) Uani d U . D 1.0 . . H H3W 0.604(4) 0.540(3) 0.448(5) 0.042 Uiso d U . D 1.0 . . H H4W 0.629(5) 0.665(4) 0.538(5) 0.042 Uiso d U . D 1.0 . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 C1 0.033(3) 0.025(3) 0.027(4) 0.003(3) 0.010(3) 0.009(3) C2 0.034(4) 0.032(4) 0.030(4) 0.005(3) 0.009(3) 0.012(3) C3 0.040(4) 0.029(4) 0.029(4) 0.000(3) 0.005(3) 0.010(3) C4 0.028(4) 0.032(4) 0.034(4) -0.001(3) 0.004(3) 0.014(3) C5 0.029(3) 0.025(3) 0.033(4) -0.002(3) 0.007(3) 0.015(3) C6 0.033(4) 0.029(4) 0.037(5) 0.002(3) 0.015(3) 0.013(3) C7 0.031(3) 0.032(3) 0.025(4) 0.002(3) 0.007(3) 0.010(3) C8 0.031(4) 0.040(4) 0.038(5) 0.009(3) 0.006(3) 0.017(3) C9 0.039(4) 0.038(4) 0.032(5) 0.011(3) 0.006(3) 0.012(3) C10 0.037(4) 0.035(4) 0.032(4) 0.009(3) 0.008(3) 0.014(3) C11 0.037(4) 0.031(3) 0.028(4) 0.007(3) 0.006(3) 0.015(3) C12 0.031(4) 0.034(3) 0.029(4) 0.002(3) 0.013(3) 0.018(3) C13 0.034(4) 0.034(4) 0.037(4) 0.003(3) 0.012(3) 0.014(3) C14 0.037(4) 0.034(4) 0.039(4) -0.001(3) 0.012(3) 0.012(3) C15 0.032(4) 0.038(4) 0.031(4) -0.001(3) 0.006(3) 0.009(3) C16 0.031(4) 0.035(3) 0.025(4) -0.001(3) 0.007(3) 0.010(3) C17 0.050(5) 0.041(5) 0.038(4) 0.003(4) 0.003(4) 0.017(4) C18 0.026(4) 0.031(4) 0.038(4) 0.000(3) 0.002(3) 0.014(3) C19 0.026(4) 0.040(4) 0.042(4) 0.002(3) 0.006(3) 0.025(3) C20 0.030(4) 0.044(5) 0.053(4) 0.005(3) 0.009(3) 0.025(4) C21 0.024(4) 0.036(4) 0.047(4) 0.004(3) 0.010(3) 0.019(3) C22 0.024(3) 0.028(4) 0.041(4) 0.002(3) 0.008(3) 0.014(3) N1 0.032(3) 0.023(3) 0.030(3) 0.003(2) 0.008(2) 0.010(2) N2 0.030(3) 0.029(3) 0.038(4) 0.001(2) 0.010(3) 0.015(3) N3 0.032(3) 0.027(3) 0.033(3) 0.002(2) 0.004(2) 0.016(2) N4 0.034(3) 0.030(3) 0.031(3) 0.002(2) 0.006(3) 0.016(3) N5 0.032(3) 0.027(3) 0.024(3) 0.001(2) 0.006(2) 0.009(2) N6 0.035(4) 0.035(3) 0.031(3) 0.004(3) 0.006(3) 0.015(3) N7 0.029(3) 0.030(3) 0.037(3) -0.001(2) 0.008(2) 0.018(2) N8 0.027(3) 0.040(3) 0.035(3) 0.003(3) 0.010(2) 0.017(3) Co1 0.0290(7) 0.0278(7) 0.0308(8) 0.0028(5) 0.0077(6) 0.0099(6) C23 0.054(5) 0.044(5) 0.056(5) 0.012(4) 0.024(4) 0.020(4) C24 0.058(5) 0.049(5) 0.040(5) 0.017(4) 0.013(4) 0.024(4) C25 0.085(7) 0.065(5) 0.077(7) 0.039(5) 0.041(6) 0.049(5) O3 0.106(5) 0.081(4) 0.068(4) 0.055(4) 0.049(4) 0.053(4) B1 0.032(4) 0.045(4) 0.040(5) 0.003(3) 0.010(4) 0.019(4) F1 0.056(3) 0.066(3) 0.043(3) 0.025(2) 0.022(2) 0.025(2) F2 0.038(3) 0.058(3) 0.049(3) 0.007(2) 0.006(2) 0.031(2) F3 0.049(3) 0.039(2) 0.066(3) 0.002(2) 0.009(2) 0.015(2) F4 0.034(2) 0.056(3) 0.044(3) 0.010(2) 0.011(2) 0.022(2) B2 0.061(4) 0.045(4) 0.064(5) 0.012(3) 0.005(4) 0.015(3) F5 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F6 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F7 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F8 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F5A 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F6A 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F7A 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F8A 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F5B 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F6B 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F7B 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) F8B 0.066(3) 0.048(2) 0.065(4) 0.0144(19) 0.008(3) 0.016(3) O1 0.036(3) 0.034(3) 0.035(3) 0.008(2) 0.012(2) 0.015(2) O2 0.034(3) 0.033(3) 0.031(3) 0.001(2) 0.006(2) 0.008(2) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Co Co -2.3653 3.6143 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N1 C1 C2 122.7(7) N1 C1 N8 117.9(6) C2 C1 N8 119.4(7) C1 C2 C3 119.8(7) C1 C2 H2 120.1 C3 C2 H2 120.1 C2 C3 C4 119.0(7) C2 C3 H3 120.5 C4 C3 H3 120.5 C5 C4 C3 118.1(7) C5 C4 H4 120.9 C3 C4 H4 120.9 N1 C5 C4 124.0(7) N1 C5 N2 115.1(6) C4 C5 N2 120.9(6) N2 C6 H6A 109.5 N2 C6 H6B 109.5 H6A C6 H6B 109.5 N2 C6 H6C 109.5 H6A C6 H6C 109.5 H6B C6 H6C 109.5 C8 C7 N3 124.3(7) C8 C7 N2 120.8(6) N3 C7 N2 114.8(6) C7 C8 C9 118.9(7) C7 C8 H8 120.5 C9 C8 H8 120.5 C10 C9 C8 118.5(7) C10 C9 H9 120.7 C8 C9 H9 120.7 C9 C10 C11 120.0(7) C9 C10 H10 120.0 C11 C10 H10 120.0 N3 C11 N4 118.9(6) N3 C11 C10 122.7(6) N4 C11 C10 118.4(7) N5 C12 C13 123.8(7) N5 C12 N4 118.7(6) C13 C12 N4 117.6(7) C14 C13 C12 118.9(7) C14 C13 H13 120.6 C12 C13 H13 120.6 C13 C14 C15 119.7(7) C13 C14 H14 120.2 C15 C14 H14 120.2 C14 C15 C16 118.7(7) C14 C15 H15 120.7 C16 C15 H15 120.7 N5 C16 C15 122.8(7) N5 C16 N6 116.7(6) C15 C16 N6 120.5(6) N6 C17 H17A 109.5 N6 C17 H17B 109.5 H17A C17 H17B 109.5 N6 C17 H17C 109.5 H17A C17 H17C 109.5 H17B C17 H17C 109.5 N7 C18 C19 125.1(7) N7 C18 N6 115.6(6) C19 C18 N6 119.2(7) C18 C19 C20 118.3(7) C18 C19 H19 120.9 C20 C19 H19 120.9 C21 C20 C19 118.1(7) C21 C20 H20 120.9 C19 C20 H20 120.9 C22 C21 C20 119.8(8) C22 C21 H21 120.1 C20 C21 H21 120.1 C21 C22 N7 124.3(7) C21 C22 N8 119.5(7) N7 C22 N8 116.2(6) C5 N1 C1 116.3(6) C5 N1 Co1 122.7(5) C1 N1 Co1 120.4(4) C5 N2 C7 116.1(5) C5 N2 C6 116.1(5) C7 N2 C6 116.3(6) C11 N3 C7 115.4(6) C11 N3 Co1 121.4(5) C7 N3 Co1 123.2(5) C11 N4 C12 125.6(6) C11 N4 H4N 117.2 C12 N4 H4N 117.2 C12 N5 C16 116.1(6) C12 N5 Co1 121.4(5) C16 N5 Co1 122.3(5) C16 N6 C18 118.1(6) C16 N6 C17 116.8(6) C18 N6 C17 117.4(6) C18 N7 C22 114.2(6) C18 N7 Co1 123.3(5) C22 N7 Co1 122.5(5) C1 N8 C22 128.0(6) C1 N8 H8A 116.0 C22 N8 H8A 116.0 N7 Co1 N3 179.5(2) N7 Co1 N5 89.2(2) N3 Co1 N5 90.5(2) N7 Co1 N1 91.2(2) N3 Co1 N1 89.0(2) N5 Co1 N1 176.1(2) N7 Co1 O2 87.2(2) N3 Co1 O2 93.3(2) N5 Co1 O2 92.5(2) N1 Co1 O2 91.4(2) N7 Co1 O1 91.8(2) N3 Co1 O1 87.7(2) N5 Co1 O1 89.9(2) N1 Co1 O1 86.2(2) O2 Co1 O1 177.43(18) C24 C23 H23A 109.5 C24 C23 H23B 109.5 H23A C23 H23B 109.5 C24 C23 H23C 109.5 H23A C23 H23C 109.5 H23B C23 H23C 109.5 O3 C24 C23 121.9(8) O3 C24 C25 120.6(8) C23 C24 C25 117.4(7) C24 C25 H25A 109.5 C24 C25 H25B 109.5 H25A C25 H25B 109.5 C24 C25 H25C 109.5 H25A C25 H25C 109.5 H25B C25 H25C 109.5 F3 B1 F2 110.5(7) F3 B1 F4 109.7(7) F2 B1 F4 110.0(7) F3 B1 F1 109.5(7) F2 B1 F1 108.9(7) F4 B1 F1 108.1(7) F5 B2 F6 114.4(9) F6A B2 F8A 124.5(15) F5 B2 F8 116.0(10) F6 B2 F8 109.1(9) F8B B2 F5B 107.2(17) F5 B2 F7 105.2(10) F6 B2 F7 101.3(9) F8 B2 F7 109.7(9) F8B B2 F6B 128.2(16) F5B B2 F6B 117.8(17) F8B B2 F7B 107.3(15) F5B B2 F7B 105.4(16) F6B B2 F7B 84.9(15) F6A B2 F5A 128.0(16) F8A B2 F5A 101.8(14) F6A B2 F7A 95.5(13) F8A B2 F7A 105.8(12) F5A B2 F7A 92.8(11) Co1 O1 H1W 131.(4) Co1 O1 H2W 119.(3) H1W O1 H2W 105.(3) Co1 O2 H3W 112.(4) Co1 O2 H4W 112.(4) H3W O2 H4W 107.(3) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance C1 N1 1.363(9) C1 C2 1.371(9) C1 N8 1.376(8) C2 C3 1.377(9) C2 H2 0.95 C3 C4 1.390(10) C3 H3 0.95 C4 C5 1.376(9) C4 H4 0.95 C5 N1 1.359(8) C5 N2 1.422(9) C6 N2 1.458(8) C6 H6A 0.98 C6 H6B 0.98 C6 H6C 0.98 C7 C8 1.360(10) C7 N3 1.372(8) C7 N2 1.432(9) C8 C9 1.386(10) C8 H8 0.95 C9 C10 1.371(9) C9 H9 0.95 C10 C11 1.385(10) C10 H10 0.95 C11 N3 1.362(8) C11 N4 1.375(8) C12 N5 1.351(8) C12 C13 1.376(9) C12 N4 1.385(8) C13 C14 1.363(10) C13 H13 0.95 C14 C15 1.377(10) C14 H14 0.95 C15 C16 1.385(9) C15 H15 0.95 C16 N5 1.364(8) C16 N6 1.404(9) C17 N6 1.466(9) C17 H17A 0.98 C17 H17B 0.98 C17 H17C 0.98 C18 N7 1.372(8) C18 C19 1.374(10) C18 N6 1.431(9) C19 C20 1.411(10) C19 H19 0.95 C20 C21 1.386(10) C20 H20 0.95 C21 C22 1.368(10) C21 H21 0.95 C22 N7 1.378(9) C22 N8 1.380(9) N1 Co1 1.963(5) N3 Co1 1.953(6) N4 H4N 0.88 N5 Co1 1.962(5) N7 Co1 1.939(6) N8 H8A 0.88 Co1 O2 2.238(5) Co1 O1 2.332(5) C23 C24 1.489(11) C23 H23A 0.98 C23 H23B 0.98 C23 H23C 0.98 C24 O3 1.224(9) C24 C25 1.498(11) C25 H25A 0.98 C25 H25B 0.98 C25 H25C 0.98 B1 F3 1.370(10) B1 F2 1.382(10) B1 F4 1.400(10) B1 F1 1.404(10) B2 F6A 1.294(18) B2 F5 1.345(11) B2 F8B 1.35(2) B2 F6 1.367(10) B2 F8A 1.38(2) B2 F8 1.383(11) B2 F5B 1.39(2) B2 F7 1.418(11) B2 F6B 1.43(2) B2 F7B 1.44(2) B2 F5A 1.44(2) B2 F7A 1.549(19) O1 H1W 0.950(19) O1 H2W 0.943(19) O2 H3W 0.94(2) O2 H4W 0.94(2)