#------------------------------------------------------------------------------ #$Date: 2019-11-10 18:53:44 +0200 (Sun, 10 Nov 2019) $ #$Revision: 225959 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/58/4515859.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4515859 loop_ _publ_author_name 'Mondal, Sandip' 'Bera, Sachinath' 'Maity, Suvendu' 'Ghosh, Prasanta' _publ_section_title ; Orthometalated N-(Benzophenoxazine)-o-aminophenol: Phenolato versus Phenoxyl States. ; _journal_issue 10 _journal_name_full 'ACS omega' _journal_page_first 13323 _journal_page_last 13334 _journal_paper_doi 10.1021/acsomega.8b01983 _journal_volume 3 _journal_year 2018 _chemical_formula_sum 'C59 H44 Cl3 N2 O2 P2 Ru' _chemical_formula_weight 1082.32 _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_Hall '-C 2yc' _space_group_name_H-M_alt 'C 1 2/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/6 _cell_angle_alpha 90 _cell_angle_beta 121.360(13) _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 27.173(9) _cell_length_b 18.901(6) _cell_length_c 23.601(12) _cell_measurement_reflns_used 9174 _cell_measurement_temperature 273(2) _cell_measurement_theta_max 25.69 _cell_measurement_theta_min 2.85 _cell_volume 10351(7) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2014 (Sheldrick 2014)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 273(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.992 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0628 _diffrn_reflns_av_unetI/netI 0.0481 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.992 _diffrn_reflns_limit_h_max 33 _diffrn_reflns_limit_h_min -33 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_limit_l_min -28 _diffrn_reflns_number 52521 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.992 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.762 _diffrn_reflns_theta_min 2.380 _exptl_absorpt_coefficient_mu 0.564 _exptl_absorpt_correction_T_max 0.865 _exptl_absorpt_correction_T_min 0.785 _exptl_absorpt_correction_type multi-scan _exptl_crystal_colour black _exptl_crystal_density_diffrn 1.388 _exptl_crystal_description prism _exptl_crystal_F_000 4356 _exptl_crystal_size_max 0.356 _exptl_crystal_size_mid 0.105 _exptl_crystal_size_min 0.056 _exptl_transmission_factor_max 0.894 _exptl_transmission_factor_min 0.789 _refine_diff_density_max 1.537 _refine_diff_density_min -1.084 _refine_diff_density_rms 0.174 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.467 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 617 _refine_ls_number_reflns 9841 _refine_ls_number_restraints 2 _refine_ls_restrained_S_all 1.467 _refine_ls_R_factor_all 0.1073 _refine_ls_R_factor_gt 0.0631 _refine_ls_shift/su_max 0.008 _refine_ls_shift/su_mean 0.002 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.2589P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1825 _refine_ls_wR_factor_ref 0.2238 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6522 _reflns_number_total 9841 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file ao8b01983_si_002.cif _cod_data_source_block 1 _cod_original_sg_symbol_H-M 'C 2/c' _cod_database_code 4515859 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelxl_version_number 2014/6 _shelx_res_file ; TITL 1.res in C2/c CELL 0.71073 27.1729 18.9013 23.6008 90.000 121.360 90.000 ZERR 4.000 0.0085 0.0057 0.0115 0.000 0.013 0.000 LATT 7 SYMM -X, Y, 1/2-Z SFAC C H N O P Cl Ru UNIT 472 356 16 24 16 16 8 L.S. 10 ACTA BOND $H FMAP 2 PLAN 20 DFIX 1.54 0.02 CL3 C60 DFIX 1.54 0.02 CL4 C60 TEMP 0 WGHT 0.100000 0.258940 FVAR 0.09621 RU1 7 0.258846 0.758727 0.255611 11.00000 0.04112 0.02539 = 0.04768 0.00267 0.02347 0.00485 P2 5 0.253493 0.763215 0.354568 11.00000 0.03953 0.03144 = 0.04228 0.00344 0.02176 0.00692 P1 5 0.264838 0.760188 0.157594 11.00000 0.04077 0.03091 = 0.04682 0.00159 0.02495 0.00364 CL1 6 0.254455 0.882021 0.251074 11.00000 0.07483 0.02494 = 0.07248 0.00514 0.04178 0.00835 O1 4 0.170910 0.734868 0.192678 11.00000 0.04259 0.03485 = 0.07533 0.00900 0.01957 0.01065 O2 4 0.388953 0.450772 0.337838 11.00000 0.04285 0.02827 = 0.08824 0.00102 0.01639 0.00458 N1 3 0.260243 0.649183 0.259098 11.00000 0.02690 0.03093 = 0.03773 0.00246 0.01782 0.00177 C15 1 0.345554 0.739625 0.311507 11.00000 0.04000 0.03098 = 0.04860 -0.00450 0.02487 -0.00126 C16 1 0.360302 0.667886 0.322646 11.00000 0.04701 0.02337 = 0.05040 -0.00292 0.02709 -0.00540 N2 3 0.481146 0.545339 0.407704 11.00000 0.03795 0.04570 = 0.06682 -0.00182 0.01899 0.00316 C7 1 0.311608 0.617836 0.291926 11.00000 0.03787 0.02723 = 0.04709 -0.00036 0.02096 -0.00159 C9 1 0.378927 0.522429 0.334933 11.00000 0.04082 0.02839 = 0.06380 0.00323 0.02443 0.00543 C10 1 0.428617 0.568886 0.369702 11.00000 0.03341 0.03331 = 0.04536 -0.00066 0.01528 0.00285 C6 1 0.205076 0.619256 0.226448 11.00000 0.04085 0.03291 = 0.05731 -0.00079 0.02174 0.00457 C22 1 0.488713 0.472447 0.415033 11.00000 0.04247 0.03970 = 0.06157 0.00563 0.02494 0.01108 C8 1 0.324851 0.544723 0.298487 11.00000 0.03748 0.03118 = 0.06470 0.00134 0.01571 0.00081 AFIX 43 H8 2 0.295252 0.511886 0.276964 11.00000 -1.20000 AFIX 0 C29 1 0.212727 0.816880 0.088356 11.00000 0.05496 0.03794 = 0.04291 0.00210 0.02462 0.00300 C12 1 0.460899 0.694450 0.387684 11.00000 0.04165 0.04276 = 0.08782 -0.00461 0.02578 -0.00314 AFIX 43 H12 2 0.499159 0.680297 0.413671 11.00000 -1.20000 AFIX 0 C17 1 0.443010 0.425552 0.380021 11.00000 0.03763 0.04269 = 0.05753 0.00380 0.02147 0.00731 C1 1 0.160188 0.668801 0.190773 11.00000 0.04148 0.03703 = 0.06634 0.00332 0.02464 0.00086 C47 1 0.195520 0.817305 0.350208 11.00000 0.04814 0.04747 = 0.06071 0.00648 0.03110 0.01083 C11 1 0.417333 0.644301 0.360494 11.00000 0.03654 0.03604 = 0.05019 0.00174 0.01938 0.00221 C13 1 0.447498 0.764898 0.376207 11.00000 0.04379 0.03611 = 0.09529 -0.00974 0.02775 -0.00843 AFIX 43 H13 2 0.477114 0.798047 0.394337 11.00000 -1.20000 AFIX 0 C53 1 0.242016 0.676959 0.380425 11.00000 0.06452 0.04177 = 0.05205 0.00021 0.03315 -0.00542 C23 1 0.332101 0.791485 0.165921 11.00000 0.04787 0.06511 = 0.05872 0.00943 0.02984 -0.00194 C41 1 0.317127 0.799257 0.429150 11.00000 0.04899 0.05208 = 0.04752 -0.01048 0.02345 0.00160 C58 1 0.284753 0.624933 0.402899 11.00000 0.05734 0.04634 = 0.04919 0.00635 0.02088 0.00767 AFIX 43 H58 2 0.320377 0.636282 0.408640 11.00000 -1.20000 AFIX 0 C52 1 0.200853 0.849544 0.405564 11.00000 0.06469 0.05485 = 0.07040 -0.00066 0.04034 0.00925 AFIX 43 H52 2 0.235560 0.847024 0.445966 11.00000 -1.20000 AFIX 0 C5 1 0.190828 0.549280 0.228324 11.00000 0.04476 0.03759 = 0.12571 0.00711 0.02265 0.00344 AFIX 43 H5 2 0.219871 0.517462 0.255115 11.00000 -1.20000 AFIX 0 C51 1 0.154065 0.886091 0.401035 11.00000 0.09665 0.07462 = 0.08720 0.00447 0.06724 0.02072 AFIX 43 H51 2 0.157631 0.907209 0.438590 11.00000 -1.20000 AFIX 0 C35 1 0.249366 0.672650 0.118258 11.00000 0.06809 0.04048 = 0.07042 -0.00758 0.04566 -0.00469 C32 1 0.131281 0.894178 -0.020807 11.00000 0.09789 0.06515 = 0.04444 0.00624 0.02389 0.01861 AFIX 43 H32 2 0.103798 0.919120 -0.057857 11.00000 -1.20000 AFIX 0 C18 1 0.451278 0.354217 0.386450 11.00000 0.04566 0.03794 = 0.07010 0.00130 0.02116 0.00589 AFIX 43 H18 2 0.420419 0.323961 0.361238 11.00000 -1.20000 AFIX 0 C40 1 0.289213 0.617427 0.151079 11.00000 0.08456 0.04841 = 0.07112 0.00509 0.05401 0.00748 AFIX 43 H40 2 0.324577 0.627084 0.189125 11.00000 -1.20000 AFIX 0 C34 1 0.160438 0.835071 0.081422 11.00000 0.05685 0.08645 = 0.05810 0.02235 0.03083 0.02317 AFIX 43 H34 2 0.152561 0.822036 0.113902 11.00000 -1.20000 AFIX 0 C14 1 0.391021 0.788085 0.338326 11.00000 0.05537 0.02655 = 0.07751 -0.00112 0.03209 -0.00286 AFIX 43 H14 2 0.383314 0.836223 0.330693 11.00000 -1.20000 AFIX 0 C19 1 0.504226 0.326904 0.429382 11.00000 0.05991 0.03909 = 0.07609 0.00629 0.02904 0.01390 AFIX 43 H19 2 0.509448 0.278160 0.434086 11.00000 -1.20000 AFIX 0 C57 1 0.275354 0.558035 0.416559 11.00000 0.09442 0.04750 = 0.06366 0.00994 0.03844 0.00617 AFIX 43 H57 2 0.304308 0.524250 0.430695 11.00000 -1.20000 AFIX 0 C42 1 0.340966 0.767572 0.491268 11.00000 0.06869 0.06032 = 0.05719 -0.00166 0.02943 0.01738 AFIX 43 H42 2 0.325149 0.726036 0.496088 11.00000 -1.20000 AFIX 0 C46 1 0.342496 0.861450 0.424552 11.00000 0.07210 0.06297 = 0.07186 -0.01032 0.03351 -0.01223 AFIX 43 H46 2 0.327461 0.883928 0.383759 11.00000 -1.20000 AFIX 0 C39 1 0.276282 0.550487 0.127525 11.00000 0.12281 0.04766 = 0.09525 -0.00132 0.07371 0.00686 AFIX 43 H39 2 0.302534 0.514312 0.150131 11.00000 -1.20000 AFIX 0 C21 1 0.543206 0.443595 0.458709 11.00000 0.03834 0.05600 = 0.08074 -0.00084 0.01735 0.00882 AFIX 43 H21 2 0.574677 0.473350 0.482812 11.00000 -1.20000 AFIX 0 C30 1 0.223876 0.840131 0.041099 11.00000 0.07211 0.07372 = 0.06378 0.00699 0.04218 0.01260 AFIX 43 H30 2 0.259115 0.829834 0.045347 11.00000 -1.20000 AFIX 0 C20 1 0.550305 0.371858 0.466042 11.00000 0.05228 0.05558 = 0.08083 0.00597 0.01683 0.02468 AFIX 43 H20 2 0.586423 0.353178 0.495932 11.00000 -1.20000 AFIX 0 C43 1 0.388073 0.797851 0.545658 11.00000 0.08082 0.09439 = 0.05245 -0.01166 0.01912 0.02416 AFIX 43 H43 2 0.403531 0.776518 0.587013 11.00000 -1.20000 AFIX 0 C54 1 0.190488 0.657791 0.373321 11.00000 0.07869 0.05461 = 0.12266 0.00605 0.07104 -0.00035 AFIX 43 H54 2 0.161047 0.690947 0.358826 11.00000 -1.20000 AFIX 0 C56 1 0.224853 0.540372 0.409852 11.00000 0.13388 0.03969 = 0.11654 0.00188 0.08058 -0.00555 AFIX 43 H56 2 0.219208 0.494861 0.420379 11.00000 -1.20000 AFIX 0 C31 1 0.183042 0.878849 -0.012935 11.00000 0.09996 0.08370 = 0.05309 0.01507 0.03987 0.01562 AFIX 43 H31 2 0.191421 0.894559 -0.044337 11.00000 -1.20000 AFIX 0 C48 1 0.144148 0.823222 0.291162 11.00000 0.07265 0.14958 = 0.05441 0.00835 0.03027 0.05062 AFIX 43 H48 2 0.140067 0.802752 0.253109 11.00000 -1.20000 AFIX 0 C2 1 0.103342 0.642266 0.153407 11.00000 0.04265 0.05166 = 0.10527 0.01139 0.02066 0.00839 AFIX 43 H2 2 0.073130 0.673354 0.128190 11.00000 -1.20000 AFIX 0 C33 1 0.119916 0.872573 0.026313 11.00000 0.07295 0.08648 = 0.06318 0.02335 0.03116 0.03114 AFIX 43 H33 2 0.084466 0.883162 0.021385 11.00000 -1.20000 AFIX 0 C28 1 0.363037 0.752847 0.145211 11.00000 0.07636 0.07292 = 0.11936 0.00067 0.07191 0.00062 AFIX 43 H28 2 0.351536 0.707067 0.129339 11.00000 -1.20000 AFIX 0 C50 1 0.103775 0.890743 0.342259 11.00000 0.08921 0.10239 = 0.09560 0.03311 0.06446 0.05175 AFIX 43 H50 2 0.072975 0.915496 0.339388 11.00000 -1.20000 AFIX 0 C4 1 0.135281 0.525788 0.191885 11.00000 0.05221 0.04092 = 0.18248 0.00253 0.03730 -0.00396 AFIX 43 H4 2 0.126717 0.478341 0.192920 11.00000 -1.20000 AFIX 0 C45 1 0.389458 0.889647 0.479798 11.00000 0.08980 0.08225 = 0.10286 -0.03551 0.05217 -0.02304 AFIX 43 H45 2 0.405793 0.931092 0.475688 11.00000 -1.20000 AFIX 0 C36 1 0.198187 0.657779 0.061156 11.00000 0.07781 0.06985 = 0.08564 -0.02258 0.03685 -0.01033 AFIX 43 H36 2 0.171773 0.693745 0.038350 11.00000 -1.20000 AFIX 0 C44 1 0.412584 0.858881 0.539926 11.00000 0.06542 0.10848 = 0.07819 -0.03569 0.02472 -0.00619 AFIX 43 H44 2 0.444545 0.878628 0.576834 11.00000 -1.20000 AFIX 0 C55 1 0.181794 0.589070 0.387618 11.00000 0.10979 0.06502 = 0.16280 -0.01338 0.09959 -0.02268 AFIX 43 H55 2 0.146428 0.576407 0.381951 11.00000 -1.20000 AFIX 0 C38 1 0.225652 0.535576 0.071520 11.00000 0.15774 0.05222 = 0.12364 -0.02222 0.09408 -0.02304 AFIX 43 H38 2 0.217554 0.489314 0.055868 11.00000 -1.20000 AFIX 0 C24 1 0.350136 0.858068 0.189387 11.00000 0.08441 0.07166 = 0.10109 -0.01563 0.06218 -0.02210 AFIX 43 H24 2 0.329519 0.884926 0.203095 11.00000 -1.20000 AFIX 0 C49 1 0.098089 0.859467 0.287519 11.00000 0.08111 0.17969 = 0.08758 0.02729 0.04207 0.07342 AFIX 43 H49 2 0.063216 0.862261 0.247329 11.00000 -1.20000 AFIX 0 C27 1 0.410467 0.781350 0.147845 11.00000 0.10859 0.11321 = 0.17757 0.00471 0.11384 0.00595 AFIX 43 H27 2 0.430504 0.755381 0.132792 11.00000 -1.20000 AFIX 0 C3 1 0.092051 0.573362 0.153530 11.00000 0.04376 0.05294 = 0.14587 -0.00581 0.02303 -0.01080 AFIX 43 H3 2 0.054358 0.557277 0.127264 11.00000 -1.20000 AFIX 0 C26 1 0.428672 0.848912 0.172936 11.00000 0.07202 0.15231 = 0.12794 0.01901 0.06363 -0.02583 AFIX 43 H26 2 0.461403 0.867965 0.175683 11.00000 -1.20000 AFIX 0 C25 1 0.398918 0.886622 0.193205 11.00000 0.10980 0.10674 = 0.12043 -0.02235 0.07366 -0.05168 AFIX 43 H25 2 0.410925 0.932046 0.209884 11.00000 -1.20000 AFIX 0 C37 1 0.185812 0.588285 0.037284 11.00000 0.09761 0.08491 = 0.10720 -0.03736 0.04062 -0.03653 AFIX 43 H37 2 0.151082 0.577702 -0.001276 11.00000 -1.20000 AFIX 0 CL2 6 0.060181 0.066460 0.281066 11.00000 0.11976 0.25743 = 0.20637 0.04621 0.07392 0.01455 C59 1 0.000000 0.114487 0.250000 10.50000 0.15759 0.08569 = 0.34799 0.00000 -0.04152 0.00000 AFIX 23 H59A 2 0.002838 0.144785 0.284756 10.50000 -1.20000 H59B 2 -0.002838 0.144785 0.215244 10.50000 -1.20000 AFIX 0 CL3 6 0.500000 0.800353 0.750000 10.50000 0.42594 0.30905 = 0.30872 0.00000 0.07029 0.00000 CL4 6 0.500000 0.944035 0.750000 10.50000 0.29586 0.26567 = 0.68004 0.00000 0.26947 0.00000 C60 1 0.526385 0.871816 0.744216 10.50000 2.00000 2.00000 = 2.00000 2.00000 2.00000 2.00000 AFIX 13 H60 2 0.499365 0.871816 0.696111 11.00000 -1.20000 AFIX 0 HKLF 4 REM 1.res in C2/c REM R1 = 0.0617 for 6522 Fo > 4sig(Fo) and 0.1060 for all 9841 data REM 628 parameters refined using 2 restraints END WGHT 0.1154 42.1354 REM Highest difference peak 1.537, deepest hole -1.084, 1-sigma level 0.174 Q1 1 0.2268 0.7530 0.2411 11.00000 0.05 0.90 Q2 1 0.2481 0.8817 0.3498 11.00000 0.05 0.67 Q3 1 0.0348 0.1304 0.2428 11.00000 0.05 0.64 Q4 1 0.2589 0.8815 0.1516 11.00000 0.05 0.59 Q5 1 0.2412 0.5408 0.3829 11.00000 0.05 0.53 Q6 1 -0.0223 0.4398 0.0639 11.00000 0.05 0.53 Q7 1 0.2614 0.4805 0.2578 11.00000 0.05 0.52 Q8 1 0.2146 0.8898 0.2316 11.00000 0.05 0.52 Q9 1 0.0000 0.2597 0.2500 10.50000 0.05 0.52 Q10 1 0.0614 0.6916 0.0193 11.00000 0.05 0.51 Q11 1 0.1971 0.5555 0.1913 11.00000 0.05 0.50 Q12 1 0.2405 0.5211 0.3197 11.00000 0.05 0.50 Q13 1 0.5397 0.7581 0.4674 11.00000 0.05 0.50 Q14 1 0.2692 0.4787 0.3489 11.00000 0.05 0.50 Q15 1 0.2970 0.4795 0.3103 11.00000 0.05 0.48 Q16 1 0.4324 0.8099 0.1883 11.00000 0.05 0.47 Q17 1 0.0340 0.6881 0.0228 11.00000 0.05 0.47 Q18 1 0.3001 0.4904 0.4933 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33.00 2 10 -4 278.67 16.00 -2 10 4 272.37 16.20 -2 10 4 283.77 15.90 -2 10 4 288.87 15.80 -2 -10 4 290.97 16.10 2 -10 -4 285.67 16.10 -4 10 6 852.51 44.50 -4 10 6 851.81 44.60 -4 10 6 808.22 44.80 4 10 -6 818.82 44.60 4 -10 -6 827.12 44.60 -4 -10 6 821.42 44.60 4 -10 -6 852.71 44.70 6 10 -8 604.34 32.60 -6 10 8 609.84 33.00 -6 10 8 596.94 32.80 6 -10 -8 632.64 32.90 6 -10 -8 578.64 32.80 -6 -10 8 594.44 32.80 -8 10 10 452.95 25.50 8 10 -10 465.15 25.10 -8 10 10 446.46 25.50 8 -10 -10 438.96 25.30 -8 -10 10 454.75 25.40 8 -10 -10 481.35 25.60 10 10 -12 135.29 8.60 -10 10 12 130.39 8.90 -10 10 12 119.59 9.40 10 -10 -12 134.99 9.30 10 -10 -12 130.19 9.70 -10 -10 12 134.39 9.40 -12 10 14 -4.00 2.80 -12 10 14 -0.90 2.40 12 10 -14 -3.60 2.10 12 -10 -14 0.10 2.90 -12 -10 14 0.00 2.70 14 10 -16 0.10 2.70 -14 10 16 4.70 3.30 -14 10 16 6.00 2.60 -14 -10 16 2.70 2.90 14 -10 -16 -1.30 3.10 -16 10 18 22.70 4.40 16 10 -18 28.40 4.40 16 -10 -18 28.00 4.90 -18 10 20 109.79 10.40 -18 10 20 113.79 10.40 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3.30 1.90 5 -11 -7 5.70 1.90 5 -11 -7 0.80 2.30 -7 11 9 5.60 2.50 -7 11 9 7.10 2.30 7 11 -9 3.60 2.20 7 -11 -9 3.30 2.80 7 -11 -9 3.00 2.30 -7 -11 9 6.80 2.30 -9 11 11 5.90 2.60 9 11 -11 7.60 2.40 -9 11 11 10.40 2.90 -9 -11 11 8.20 2.80 9 -11 -11 3.70 2.70 9 -11 -11 13.20 3.10 -11 11 13 -0.60 2.40 -11 11 13 -3.40 2.80 11 11 -13 3.50 2.20 -11 -11 13 0.50 2.60 11 -11 -13 3.00 2.90 -13 11 15 3.90 2.80 -13 11 15 -0.80 2.90 13 11 -15 -1.40 2.50 -13 -11 15 -1.10 2.70 15 11 -17 -3.20 2.70 -15 11 17 2.10 3.40 -15 11 17 -1.10 3.20 -15 -11 17 -3.80 3.00 -17 11 19 6.90 3.60 17 11 -19 7.70 2.40 17 11 -19 2.50 3.30 -17 11 19 7.90 4.20 17 -11 -19 9.00 4.10 -17 -11 19 7.80 3.90 -19 11 21 -3.80 4.40 -19 11 21 -2.70 3.60 -19 -11 21 -0.10 4.40 19 -11 -21 3.20 4.20 -21 11 23 -6.40 5.20 -21 11 23 -3.30 4.20 21 -11 -23 1.70 5.10 -24 -12 22 8.20 6.70 -22 12 20 23.70 4.10 -22 12 20 27.00 6.00 22 -12 -20 19.20 5.40 -22 -12 20 23.20 5.70 20 12 -18 34.60 5.90 -20 12 18 27.20 5.50 20 12 -18 41.80 6.20 20 -12 -18 29.90 5.30 18 12 -16 17.10 2.70 18 12 -16 13.50 3.40 -18 12 16 18.10 4.20 -18 12 16 11.60 4.20 -18 -12 16 9.10 3.90 -16 12 14 3.50 3.80 -16 12 14 7.40 2.90 16 12 -14 10.60 2.20 16 12 -14 12.50 3.10 -16 -12 14 4.40 3.20 16 -12 -14 7.80 3.70 -14 12 12 11.00 3.50 14 12 -12 9.10 2.90 -14 12 12 8.50 2.90 14 12 -12 13.10 2.70 -14 -12 12 8.30 3.30 14 -12 -12 9.10 3.40 -12 12 10 93.79 7.60 12 12 -10 97.19 7.40 12 12 -10 106.29 6.60 -12 12 10 93.39 8.30 12 -12 -10 87.59 8.00 12 -12 -10 101.69 8.80 -12 -12 10 108.69 8.30 -10 12 8 162.58 10.70 10 12 -8 166.58 10.70 -10 12 8 170.48 11.00 -10 -12 8 162.08 11.60 10 -12 -8 174.88 10.80 -8 12 6 3.80 2.20 8 12 -6 2.10 2.40 -8 12 6 5.20 2.20 8 12 -6 5.00 1.20 8 -12 -6 4.30 1.90 8 -12 -6 6.20 2.80 -8 -12 6 0.90 2.20 -6 12 4 9.30 2.10 6 12 -4 9.40 1.40 6 12 -4 5.70 2.30 -6 12 4 3.70 2.30 -6 -12 4 10.90 2.30 6 -12 -4 7.40 1.70 6 -12 -4 12.30 2.90 4 12 -2 33.90 3.10 4 12 -2 37.90 4.40 -4 12 2 31.30 4.40 -4 12 2 34.50 3.90 -4 -12 2 27.10 4.20 4 -12 -2 32.40 3.50 4 -12 -2 36.90 4.80 -2 12 0 274.37 14.90 2 12 0 262.27 14.70 -2 12 0 244.78 15.40 2 12 0 262.27 15.60 2 12 0 267.57 14.80 2 -12 0 281.87 15.60 -2 -12 0 268.67 15.40 2 -12 0 263.17 14.70 0 12 2 108.29 8.00 0 12 -2 118.59 7.20 0 12 -2 115.69 8.00 0 12 2 112.89 7.40 0 12 2 112.99 7.20 0 -12 -2 119.59 7.90 0 -12 2 114.79 7.90 2 12 -4 14.20 2.60 -2 12 4 11.60 2.50 -2 12 4 10.40 1.80 -2 12 4 15.30 2.40 2 -12 -4 11.10 2.70 -2 -12 4 14.00 2.50 -4 12 6 0.90 2.00 -4 12 6 1.10 2.00 4 12 -6 0.20 2.00 4 -12 -6 0.90 1.80 -4 -12 6 -0.30 1.80 4 -12 -6 -2.30 2.40 6 12 -8 17.80 3.00 -6 12 8 18.90 3.10 -6 12 8 26.30 4.30 -6 -12 8 23.70 4.40 6 -12 -8 14.80 2.70 6 -12 -8 15.80 3.20 -8 12 10 196.68 12.60 -8 12 10 185.28 12.30 8 12 -10 197.28 12.00 8 -12 -10 201.48 12.60 8 -12 -10 185.98 15.50 -10 12 12 69.39 7.30 10 12 -12 77.19 6.50 -10 12 12 77.79 6.80 -10 -12 12 73.29 7.20 10 -12 -12 84.39 7.30 12 12 -14 10.90 3.10 -12 12 14 8.30 3.50 -12 12 14 9.30 3.50 -12 -12 14 11.90 3.40 12 -12 -14 7.60 3.30 14 12 -16 3.30 3.20 -14 12 16 4.70 3.10 -14 -12 16 8.50 3.30 14 -12 -16 1.40 3.50 -16 12 18 11.90 3.50 -16 12 18 18.30 4.40 16 12 -18 13.50 3.80 -16 -12 18 12.40 4.00 16 -12 -18 9.80 4.00 -18 12 20 27.70 4.40 -18 12 20 20.90 5.20 18 -12 -20 27.60 5.10 -18 -12 20 23.40 5.00 -20 12 22 -1.30 5.10 -20 12 22 16.10 4.10 20 -12 -22 9.60 5.00 -20 -12 22 5.70 5.30 -23 13 21 20.30 6.90 23 -13 -21 -0.80 5.60 -23 -13 21 3.50 6.10 -21 13 19 20.90 6.00 -21 13 19 9.10 3.70 -21 -13 19 14.10 5.00 21 -13 -19 6.70 4.80 19 13 -17 4.00 3.50 -19 13 17 8.90 4.60 19 13 -17 10.60 3.80 -19 13 17 7.60 3.20 -19 -13 17 8.60 4.20 19 -13 -17 -2.20 4.10 -17 13 15 1.20 3.50 -17 13 15 -2.00 2.80 17 13 -15 -0.30 3.40 15 13 -13 3.30 3.00 -15 13 13 4.80 3.50 15 13 -13 3.50 1.90 -15 13 13 5.10 2.80 15 -13 -13 6.90 3.60 -15 -13 13 5.40 3.40 -13 13 11 9.00 3.50 13 13 -11 16.40 3.40 -13 13 11 7.80 5.40 -13 -13 11 12.10 3.30 13 -13 -11 9.90 3.40 11 13 -9 7.00 2.90 -11 13 9 4.20 3.60 -11 13 9 2.90 2.70 11 -13 -9 4.80 2.90 -11 -13 9 2.30 2.70 11 -13 -9 8.90 3.30 -9 13 7 7.50 2.90 9 13 -7 10.00 2.90 -9 13 7 10.00 3.00 -9 -13 7 11.50 3.20 9 -13 -7 9.00 2.40 9 -13 -7 12.80 3.40 -7 13 5 14.50 2.80 -7 13 5 12.70 3.00 7 13 -5 18.60 3.10 7 13 -5 15.90 2.80 7 -13 -5 15.60 2.30 -7 -13 5 11.80 2.80 7 -13 -5 18.60 3.50 5 13 -3 147.29 9.70 -5 13 3 151.88 9.30 5 13 -3 146.39 8.60 -5 13 3 146.69 9.80 -5 -13 3 140.59 9.60 5 -13 -3 144.79 10.00 5 -13 -3 148.99 9.00 3 13 -1 1.00 1.90 -3 13 1 1.50 2.30 3 13 -1 3.40 2.40 -3 13 1 -0.80 2.00 3 13 -1 0.40 1.20 3 -13 -1 5.00 2.50 -3 -13 1 3.90 2.30 3 -13 -1 0.30 1.30 1 13 1 24.50 3.20 -1 13 -1 25.70 4.40 -1 13 -1 22.50 3.50 1 13 1 26.80 3.50 1 13 1 19.10 3.20 1 -13 1 22.40 2.80 -1 -13 -1 25.30 4.50 1 -13 1 20.70 3.30 -1 13 3 11.50 2.30 -1 13 3 3.60 2.50 1 13 -3 7.30 2.60 -1 13 3 7.80 1.70 1 -13 -3 4.10 2.50 -1 -13 3 5.40 2.40 -3 13 5 1.50 2.10 -3 13 5 -3.10 2.20 3 13 -5 1.60 2.20 3 -13 -5 -1.60 2.40 -3 -13 5 -0.80 2.10 5 13 -7 -0.30 2.40 -5 13 7 3.00 2.40 -5 13 7 -2.40 2.30 5 -13 -7 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45.80 6.70 -12 14 8 43.20 6.10 12 14 -8 55.19 6.50 12 14 -8 53.39 4.80 -12 -14 8 53.09 6.40 12 -14 -8 51.99 7.20 12 -14 -8 57.09 6.60 -10 14 6 12.10 3.40 -10 14 6 12.30 3.50 10 14 -6 11.20 1.90 10 14 -6 8.20 3.50 10 -14 -6 10.10 2.60 -10 -14 6 11.00 3.10 10 -14 -6 13.80 3.70 -8 14 4 14.70 3.00 -8 14 4 16.00 4.20 8 14 -4 13.40 3.30 8 14 -4 19.90 3.40 -8 -14 4 11.50 3.00 8 -14 -4 10.90 2.10 8 -14 -4 9.30 3.40 6 14 -2 63.89 6.50 -6 14 2 62.69 5.70 6 14 -2 58.99 5.00 -6 14 2 58.19 10.40 -6 -14 2 68.09 4.40 -6 -14 2 46.60 7.90 6 -14 -2 63.29 7.90 6 -14 -2 72.49 5.20 4 14 0 413.06 22.10 4 14 0 397.66 21.90 -4 14 0 417.66 22.20 4 14 0 387.86 23.00 -4 -14 0 411.76 22.90 4 -14 0 412.86 21.80 4 -14 0 356.46 24.60 2 14 2 337.47 18.20 2 14 2 334.67 18.20 -2 14 -2 348.47 18.00 2 14 2 285.37 19.90 -2 -14 -2 325.57 18.80 2 -14 2 304.77 19.60 0 14 4 123.29 7.60 0 14 4 87.69 9.80 0 14 -4 98.89 11.20 0 14 4 117.99 7.70 0 -14 -4 111.39 8.50 -2 14 6 189.28 11.70 2 14 -6 178.48 12.40 -2 14 6 201.98 11.60 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141.59 10.60 -6 16 2 135.49 10.10 6 -16 -2 167.18 11.00 -6 -16 2 155.28 10.50 6 -16 -2 159.28 9.30 4 16 0 246.48 14.20 -4 16 0 248.78 14.50 -4 16 0 227.68 15.30 4 16 0 244.18 14.00 4 16 0 231.28 15.30 -4 -16 0 242.38 15.20 4 -16 0 250.67 15.40 4 -16 0 252.07 13.90 -2 16 -2 193.68 13.50 2 16 2 197.98 12.40 -2 16 -2 219.68 12.30 2 16 2 191.78 13.50 2 16 2 204.18 12.50 2 -16 2 216.68 13.60 -2 -16 -2 215.18 13.40 0 16 -4 87.89 7.90 0 16 4 86.09 7.20 0 16 4 81.89 7.80 0 16 4 95.29 7.20 0 -16 -4 82.89 7.90 0 -16 4 83.49 7.90 2 16 -6 34.90 5.70 -2 16 6 40.00 5.80 -2 16 6 38.50 5.80 -2 16 6 32.30 5.80 -2 -16 6 32.30 5.50 2 -16 -6 42.00 6.10 4 16 -8 195.08 13.10 -4 16 8 185.88 13.20 -4 16 8 201.68 13.30 4 -16 -8 199.68 13.20 -4 -16 8 212.78 13.00 -6 16 10 58.59 7.70 -6 16 10 57.19 7.20 6 16 -10 59.99 7.10 6 -16 -10 79.99 7.90 -6 -16 10 79.79 7.30 -8 16 12 26.10 4.80 8 16 -12 43.00 6.10 -8 16 12 34.70 5.70 8 -16 -12 41.40 6.70 -8 -16 12 28.60 4.40 -10 16 14 55.49 7.10 10 16 -14 57.59 6.90 -10 16 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6.30 2.60 11 11 -4 12.80 2.60 -11 11 4 9.90 2.60 -11 -11 4 12.00 2.60 11 -11 -4 7.70 1.90 11 -11 -4 14.80 3.00 -11 -11 4 14.70 2.20 9 11 -2 1.40 2.00 -9 11 2 2.10 2.20 -9 11 2 -1.90 1.80 9 11 -2 2.10 1.50 -9 -11 2 -0.10 1.30 9 -11 -2 -0.70 2.30 9 -11 -2 -0.50 1.30 -9 -11 2 1.40 1.80 -7 11 0 11.90 2.20 7 11 0 11.00 2.50 7 11 0 8.60 1.70 -7 11 0 10.80 2.50 7 -11 0 8.20 1.50 -7 -11 0 10.60 2.20 7 -11 0 12.70 2.60 -7 -11 0 16.00 2.50 -5 11 -2 77.79 6.00 -5 11 -2 74.39 5.30 5 11 2 82.79 5.60 5 11 2 81.09 6.20 5 -11 2 72.09 6.00 -5 -11 -2 67.89 5.70 3 11 4 15.60 2.40 3 11 4 16.10 2.80 -3 11 -4 15.40 2.80 3 11 4 22.20 3.30 -3 -11 -4 12.60 2.40 3 -11 4 14.50 2.60 1 11 6 5.30 1.70 1 11 6 5.10 2.10 -1 11 -6 2.50 2.10 1 11 6 1.90 2.20 1 -11 6 2.60 1.90 -1 -11 -6 2.80 2.10 -1 11 8 29.10 4.30 1 11 -8 20.00 3.10 -1 11 8 26.70 4.00 -1 11 8 30.40 4.50 1 -11 -8 21.30 3.20 -1 -11 8 27.20 4.00 -3 11 10 3.40 2.20 3 11 -10 0.30 2.20 -3 11 10 3.60 2.60 -3 11 10 0.50 2.50 -3 -11 10 3.40 2.30 3 -11 -10 0.90 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12.00 3.00 18 12 -11 14.20 3.20 18 -12 -11 11.60 3.60 -16 12 9 56.29 6.50 -16 12 9 48.30 5.70 16 12 -9 57.99 6.00 16 12 -9 56.19 5.80 16 -12 -9 57.79 6.80 -16 -12 9 60.29 6.90 -14 12 7 93.79 9.30 14 12 -7 121.79 7.60 14 12 -7 108.19 8.10 -14 12 7 109.99 8.10 14 -12 -7 93.09 8.70 -14 -12 7 112.69 8.70 14 -12 -7 116.59 8.10 -12 12 5 -2.90 2.70 12 12 -5 -0.60 1.60 -12 12 5 -4.60 2.30 12 12 -5 -3.40 2.30 12 -12 -5 -0.30 1.80 -12 -12 5 0.90 2.40 12 -12 -5 -1.50 3.80 10 12 -3 -0.70 2.20 -10 12 3 -0.30 2.10 10 12 -3 -0.30 1.50 -10 12 3 -2.00 2.30 10 -12 -3 -3.20 2.60 10 -12 -3 -3.00 1.50 -10 -12 3 0.00 1.30 -10 -12 3 -0.40 2.10 8 12 -1 78.29 6.30 8 12 -1 76.69 5.60 -8 12 1 69.59 5.80 -8 12 1 73.49 6.30 -8 -12 1 72.29 6.10 -8 -12 1 79.09 5.00 8 -12 -1 80.59 6.50 8 -12 -1 68.09 5.10 -6 12 -1 210.78 12.80 6 12 1 207.48 13.00 -6 12 -1 211.08 12.10 6 12 1 211.98 12.20 6 -12 1 206.38 12.70 6 -12 1 217.08 11.60 -6 -12 -1 190.58 12.50 -6 -12 -1 211.58 11.90 4 12 3 47.30 4.30 4 12 3 43.20 5.00 -4 12 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125.89 10.80 -4 -14 11 112.39 9.00 -6 14 13 -5.80 3.00 -6 14 13 0.30 3.10 6 14 -13 2.20 2.70 -6 -14 13 -1.60 2.70 6 -14 -13 2.70 3.30 8 14 -15 0.10 2.90 -8 14 15 1.80 3.50 -8 14 15 -5.80 3.00 8 -14 -15 -2.10 3.30 -8 -14 15 -1.90 2.90 -10 14 17 4.60 3.80 10 14 -17 2.50 3.10 -10 14 17 2.20 3.60 10 -14 -17 1.50 3.80 -10 -14 17 5.10 3.60 -12 14 19 28.70 4.70 -12 14 19 25.10 5.50 12 14 -19 22.60 4.20 12 -14 -19 41.00 7.20 -12 -14 19 26.20 4.60 14 14 -21 18.10 4.20 -14 14 21 35.70 6.20 -14 14 21 26.80 4.80 -14 -14 21 28.90 5.10 14 -14 -21 26.50 5.50 -23 15 16 10.90 3.70 -23 15 16 11.50 5.70 -23 -15 16 13.70 5.30 23 -15 -16 7.00 5.20 21 15 -14 8.70 5.00 -21 15 14 4.50 3.50 -21 15 14 11.00 5.20 -21 -15 14 2.60 4.60 21 -15 -14 -1.80 4.50 -19 15 12 9.80 3.50 -19 15 12 15.80 4.60 19 15 -12 3.00 3.80 -19 -15 12 12.70 4.30 19 -15 -12 5.10 4.30 -17 15 10 12.60 4.00 -17 15 10 14.00 3.40 17 15 -10 14.60 5.30 17 15 -10 11.50 3.30 17 -15 -10 17.90 4.20 -17 -15 10 11.50 3.80 15 15 -8 19.40 4.60 15 15 -8 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25.90 4.30 -16 -14 8 24.80 4.30 16 -14 -8 32.40 6.00 14 14 -6 43.70 5.40 -14 14 6 51.69 5.80 -14 14 6 41.20 6.00 14 14 -6 40.70 6.20 14 -14 -6 44.20 6.30 14 -14 -6 43.60 5.60 -14 -14 6 33.60 6.10 12 14 -4 87.09 7.10 -12 14 4 93.29 8.90 -12 14 4 87.49 7.60 12 14 -4 79.89 7.90 -12 -14 4 83.79 7.60 12 -14 -4 92.49 6.50 12 -14 -4 85.59 8.00 -10 14 2 102.19 7.70 10 14 -2 102.89 8.70 10 14 -2 98.89 7.50 -10 14 2 102.99 8.30 -10 -14 2 83.49 8.00 10 -14 -2 116.19 6.90 10 -14 -2 103.99 8.50 -10 -14 2 99.09 6.40 -8 14 0 456.25 24.70 8 14 0 459.85 24.70 -8 14 0 422.26 25.30 -8 -14 0 443.06 24.20 8 -14 0 453.45 25.40 -8 -14 0 413.46 25.80 8 -14 0 466.05 24.10 6 14 2 103.59 8.50 -6 14 -2 114.69 7.40 -6 14 -2 113.79 8.50 6 14 2 120.39 7.80 -6 -14 -2 93.69 8.20 6 -14 2 92.29 10.10 -6 -14 -2 106.49 7.00 4 14 4 1.30 3.00 4 14 4 1.90 2.20 4 14 4 0.10 2.70 -4 14 -4 2.10 1.90 -4 14 -4 0.60 2.50 4 -14 4 -3.70 5.50 -4 -14 -4 -3.10 2.60 -2 14 -6 2.90 2.60 2 14 6 1.90 2.90 2 14 6 3.20 2.70 2 14 6 -0.10 2.50 2 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6.30 3.60 -20 12 11 5.40 2.80 20 12 -11 5.80 3.00 -20 -12 11 1.10 3.40 20 -12 -11 -3.90 3.40 -18 12 9 2.20 3.20 18 12 -9 3.00 2.60 18 12 -9 4.70 2.90 -18 12 9 9.40 3.00 -18 -12 9 5.50 3.30 18 -12 -9 2.10 3.20 16 12 -7 1.20 2.40 -16 12 7 -0.20 3.00 -16 12 7 -1.00 2.60 16 12 -7 -3.90 2.70 16 -12 -7 0.50 2.90 16 -12 -7 3.20 3.30 -16 -12 7 3.20 3.10 -16 -12 7 3.50 1.70 14 12 -5 -3.50 2.30 -14 12 5 -0.90 4.60 14 12 -5 -2.20 1.90 -14 -12 5 -1.70 1.50 14 -12 -5 -3.80 3.10 14 -12 -5 -3.70 1.90 -14 -12 5 -1.90 3.30 12 12 -3 -2.90 1.80 12 12 -3 -1.60 2.30 -12 -12 3 -2.00 1.40 12 -12 -3 1.20 3.00 -12 -12 3 -1.30 2.40 10 12 -1 131.99 8.30 10 12 -1 128.59 8.90 -10 12 1 120.79 8.40 -10 12 1 124.79 9.00 10 -12 -1 113.19 7.70 -10 -12 1 129.59 7.60 -10 -12 1 117.09 8.40 10 -12 -1 128.49 9.00 -8 12 -1 267.67 15.30 8 12 1 268.57 15.80 -8 12 -1 276.07 15.70 8 12 1 262.97 15.10 -8 -12 -1 262.77 14.70 -8 -12 -1 251.27 15.20 8 -12 1 240.78 15.50 8 -12 1 269.67 14.50 -6 12 -3 10.90 2.70 6 12 3 10.50 2.20 -6 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146.79 10.70 11 -15 0 160.58 11.10 -9 15 -2 49.10 5.40 -9 15 -2 49.70 6.10 9 15 2 43.80 6.30 -9 -15 -2 33.70 4.50 9 -15 2 49.00 6.30 -9 -15 -2 44.20 6.30 -7 15 -4 30.80 5.10 -7 15 -4 37.80 4.60 7 -15 4 26.20 4.10 -7 -15 -4 33.60 6.00 -7 -15 -4 31.60 4.50 -5 15 -6 29.60 5.20 5 15 6 23.30 4.50 -5 15 -6 38.10 4.30 -5 -15 -6 37.90 6.20 5 -15 6 32.10 5.40 3 15 8 12.00 3.90 -3 15 -8 11.80 3.20 3 15 8 9.80 3.70 3 -15 8 20.00 3.30 -3 -15 -8 19.80 3.80 -1 15 -10 32.80 5.50 1 15 10 26.40 4.60 1 15 10 27.70 5.00 -1 -15 -10 44.00 6.30 1 -15 10 38.90 5.70 -1 15 12 61.39 7.30 1 15 -12 49.60 6.00 -1 -15 12 42.00 6.20 1 -15 -12 49.60 8.60 -3 15 14 11.40 4.10 3 15 -14 15.10 3.40 -3 15 14 10.20 4.20 3 -15 -14 7.10 3.80 -3 -15 14 8.20 3.30 -5 15 16 10.50 4.30 -5 15 16 -4.40 3.70 5 15 -16 -0.50 3.30 5 -15 -16 11.00 4.10 -5 -15 16 0.90 3.20 -7 15 18 -1.70 4.10 7 15 -18 1.30 3.50 -7 15 18 0.00 4.40 -7 -15 18 0.20 3.50 7 -15 -18 5.90 4.20 -9 15 20 0.60 4.70 9 15 -20 -2.30 3.80 -9 15 20 1.20 5.00 -9 -15 20 7.10 3.80 9 -15 -20 4.90 4.50 22 16 -11 41.20 8.20 -22 16 11 24.30 4.20 -22 16 11 26.10 5.60 22 -16 -11 18.50 5.00 -22 -16 11 20.20 5.70 -20 16 9 63.59 7.10 20 16 -9 57.79 7.90 -20 16 9 46.70 8.10 20 -16 -9 66.19 8.10 -20 -16 9 64.29 8.50 -18 16 7 20.10 3.80 18 16 -7 14.70 4.40 -18 16 7 13.00 4.40 18 -16 -7 15.30 4.10 -18 -16 7 15.10 4.30 16 16 -5 -6.40 4.60 -16 16 5 3.70 3.30 -16 16 5 6.30 3.70 -16 -16 5 1.60 3.70 16 -16 -5 -1.10 3.80 14 16 -3 26.40 4.40 -14 16 3 21.70 4.20 -14 -16 3 27.20 4.50 14 -16 -3 30.30 4.80 -14 -16 3 33.40 3.80 14 -16 -3 26.50 4.20 12 16 -1 73.69 8.20 -12 16 1 77.49 7.90 -12 16 1 90.09 8.00 -12 -16 1 76.09 8.00 -12 -16 1 90.29 6.10 12 -16 -1 101.79 6.30 12 -16 -1 86.39 8.10 -10 16 -1 80.39 7.20 -10 16 -1 75.99 7.30 10 16 1 66.19 7.50 10 -16 1 75.69 7.70 -10 -16 -1 70.19 7.30 -10 -16 -1 75.59 5.70 -8 16 -3 51.69 6.10 -8 16 -3 49.70 5.90 -8 -16 -3 40.20 4.80 8 -16 3 50.09 6.20 -8 -16 -3 46.70 6.60 6 16 5 23.70 4.40 -6 16 -5 33.00 5.20 -6 -16 -5 18.80 4.10 -6 -16 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41.70 6.70 -22 14 10 25.40 4.80 -22 14 10 34.70 6.00 -22 -14 10 20.20 5.00 22 -14 -10 26.10 4.80 -20 14 8 43.00 7.60 20 14 -8 49.40 7.30 -20 14 8 42.80 6.10 -20 -14 8 52.49 4.70 20 -14 -8 44.90 6.80 -20 -14 8 61.19 7.90 18 14 -6 16.50 4.60 -18 14 6 19.60 3.60 -18 14 6 22.00 4.10 -18 -14 6 20.90 4.20 18 -14 -6 16.80 4.20 -18 -14 6 22.80 3.70 -16 14 4 30.50 5.40 16 14 -4 28.30 6.20 -16 14 4 26.60 4.10 -16 -14 4 21.50 2.90 16 -14 -4 35.90 5.90 -16 -14 4 30.90 4.60 16 -14 -4 41.60 5.40 14 14 -2 55.89 7.30 -14 14 2 64.59 6.80 -14 14 2 68.19 6.50 14 -14 -2 68.99 5.50 14 -14 -2 65.59 6.80 -14 -14 2 56.09 5.10 -14 -14 2 57.79 7.00 -12 14 0 76.39 6.90 12 14 0 64.19 7.50 -12 14 0 73.29 6.80 12 -14 0 74.59 7.10 -12 -14 0 61.89 5.40 12 -14 0 71.79 5.40 -12 -14 0 65.99 7.40 -10 14 -2 97.29 7.60 10 14 2 69.29 8.40 -10 14 -2 88.59 7.20 10 -14 2 98.99 8.10 -10 -14 -2 95.99 6.50 10 -14 2 97.39 5.90 -10 -14 -2 89.99 8.90 -8 14 -4 46.30 5.70 8 14 4 33.20 4.80 -8 14 -4 38.60 4.90 -8 -14 -4 44.60 6.30 8 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6.40 5.60 25 -15 -13 1.70 5.40 -25 -15 13 3.40 5.40 -23 15 11 13.40 3.80 -23 15 11 20.70 5.20 -23 -15 11 15.70 5.10 23 -15 -11 7.70 4.80 -21 15 9 18.30 3.80 21 15 -9 14.90 5.20 -21 15 9 17.50 4.70 -21 -15 9 20.30 4.70 21 -15 -9 23.90 4.50 -19 15 7 26.40 4.70 -19 15 7 26.00 4.10 19 15 -7 22.60 4.90 19 -15 -7 26.20 4.50 -19 -15 7 23.50 4.80 -17 15 5 9.40 3.40 17 15 -5 10.30 4.00 -17 15 5 11.00 3.60 -17 -15 5 13.30 3.90 -17 -15 5 5.60 2.30 17 -15 -5 7.90 3.70 -15 15 3 36.30 5.60 -15 15 3 44.50 6.30 15 15 -3 28.20 4.80 15 -15 -3 38.80 5.00 -15 -15 3 30.50 4.10 -15 -15 3 38.70 6.40 15 -15 -3 37.00 6.20 -13 15 1 23.90 3.90 -13 15 1 22.40 3.80 13 15 -1 14.70 4.20 -13 -15 1 18.90 4.00 13 -15 -1 29.90 4.10 -13 -15 1 23.50 3.10 13 -15 -1 23.40 4.00 -11 15 -1 52.49 6.60 -11 15 -1 65.69 6.50 11 15 1 41.80 7.30 -11 -15 -1 50.99 5.10 11 -15 1 61.59 6.80 -11 -15 -1 67.39 6.70 11 -15 1 69.59 4.60 9 15 3 3.50 3.40 -9 15 -3 10.50 2.90 -9 15 -3 15.50 3.20 -9 -15 -3 3.50 2.30 9 -15 3 10.30 3.40 -9 -15 -3 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19 9 -6 36.30 5.30 -19 9 6 37.90 5.90 -19 9 6 52.49 4.80 19 -9 -6 32.10 6.10 -19 -9 6 49.60 6.40 -19 -9 6 55.19 4.60 -17 9 4 -3.00 2.80 -17 9 4 -3.30 1.90 17 9 -4 0.30 2.50 17 9 -4 -4.90 2.50 -17 -9 4 -3.60 1.90 17 -9 -4 -3.00 2.70 17 -9 -4 0.20 2.10 -17 -9 4 -5.40 3.00 -15 9 2 6.80 3.00 15 9 -2 10.20 2.60 -15 9 2 13.60 2.60 15 9 -2 14.80 2.80 -15 -9 2 9.50 2.70 15 -9 -2 12.20 2.30 -13 9 0 139.29 9.20 13 9 0 144.49 9.70 13 9 0 143.09 9.40 -13 9 0 136.59 9.30 -13 -9 0 133.09 9.10 -13 -9 0 125.89 8.70 13 -9 0 142.89 9.10 13 -9 0 145.59 8.60 11 9 2 129.29 9.20 -11 9 -2 124.89 8.50 -11 9 -2 129.79 8.40 11 9 2 136.49 8.70 -11 -9 -2 128.09 8.10 11 -9 2 113.29 8.20 11 -9 2 131.19 7.70 -11 -9 -2 120.79 8.00 -9 9 -4 26.90 3.70 -9 9 -4 33.20 3.90 9 9 4 29.20 4.80 9 9 4 17.00 2.90 9 -9 4 26.30 2.60 -9 -9 -4 23.20 3.80 -9 -9 -4 25.70 3.50 -7 9 -6 43.20 4.50 7 9 6 40.50 5.20 -7 9 -6 36.00 4.20 7 9 6 53.79 5.60 -7 -9 -6 42.70 4.50 -7 -9 -6 46.30 4.60 7 -9 6 40.50 4.10 -5 9 -8 8.90 2.60 5 9 8 12.60 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416.16 23.90 -12 -10 -1 426.56 23.80 12 -10 1 430.56 23.40 -12 -10 -1 435.16 23.70 10 10 3 28.00 4.60 -10 10 -3 27.30 4.10 -10 10 -3 30.70 4.20 10 10 3 22.50 3.90 10 -10 3 21.50 3.10 -10 -10 -3 27.40 4.10 10 -10 3 28.40 2.90 -10 -10 -3 29.20 3.70 8 10 5 3.20 2.90 -8 10 -5 7.90 2.30 8 10 5 5.80 2.30 -8 10 -5 5.50 2.20 8 -10 5 4.30 2.00 -8 -10 -5 3.40 2.30 -8 -10 -5 6.00 2.10 -6 10 -7 85.09 6.20 -6 10 -7 85.79 7.30 6 10 7 88.19 7.50 6 10 7 90.89 7.90 -6 -10 -7 84.49 6.60 6 -10 7 83.29 6.20 -6 -10 -7 94.49 6.80 -4 10 -9 187.38 13.20 4 10 9 228.38 14.10 -4 10 -9 223.18 12.30 4 10 9 193.58 16.90 -4 -10 -9 214.28 13.00 -4 -10 -9 217.48 12.60 4 -10 9 209.28 12.50 2 10 11 114.49 10.10 -2 10 -11 142.29 8.10 -2 10 -11 129.99 9.10 2 10 11 138.49 9.70 2 -10 11 123.49 8.60 -2 -10 -11 133.29 8.70 0 10 -13 52.79 4.60 0 10 13 46.80 6.60 0 10 13 49.99 6.10 0 10 -13 49.99 5.50 0 -10 13 50.39 5.30 0 -10 -13 45.00 5.50 -2 10 15 64.59 6.70 -2 10 15 54.89 6.90 2 10 -15 56.19 6.00 -2 -10 15 58.99 5.80 2 -10 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8.00 2.70 -17 11 4 10.80 3.30 17 11 -4 3.40 3.10 -17 -11 4 11.60 3.50 -17 -11 4 12.00 2.30 17 -11 -4 8.00 2.30 17 -11 -4 9.90 3.70 -15 11 2 -0.20 3.40 15 11 -2 3.30 3.00 -15 11 2 -4.50 2.30 15 11 -2 -2.70 3.30 15 -11 -2 -3.00 1.80 -15 -11 2 -0.30 2.70 15 -11 -2 3.40 3.00 -15 -11 2 -2.30 1.90 13 11 0 141.39 10.20 -13 11 0 139.29 9.80 -13 11 0 135.09 9.60 13 11 0 138.29 10.00 -13 -11 0 142.19 8.80 -13 -11 0 143.59 9.50 13 -11 0 137.39 9.80 13 -11 0 144.19 8.60 -11 11 -2 94.39 7.00 -11 11 -2 98.69 7.50 11 11 2 87.29 8.20 11 11 2 93.09 7.60 11 -11 2 99.59 6.00 -11 -11 -2 92.79 6.90 11 -11 2 86.79 7.30 -11 -11 -2 93.79 6.60 9 11 4 36.50 5.40 -9 11 -4 25.10 4.10 9 11 4 20.00 4.10 9 -11 4 20.00 3.20 -9 -11 -4 29.60 4.50 -7 11 -6 -4.40 2.10 7 11 6 4.20 2.90 -7 11 -6 1.90 2.40 7 11 6 2.90 5.20 -7 -11 -6 -1.20 2.50 -7 -11 -6 -0.80 2.20 7 -11 6 -3.50 2.10 5 11 8 3.90 3.30 -5 11 -8 -2.40 2.00 -5 11 -8 -3.40 2.30 5 -11 8 -3.00 1.90 -5 -11 -8 -0.70 2.50 -5 -11 -8 1.00 2.60 -3 11 -10 42.40 5.30 3 11 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55.19 5.80 -8 -12 -5 54.69 5.80 -6 12 -7 24.30 3.70 6 12 7 32.10 5.90 -6 12 -7 24.10 3.80 6 -12 7 30.90 4.60 -6 -12 -7 33.20 5.20 -6 -12 -7 31.40 4.80 -4 12 -9 111.59 8.80 -4 12 -9 136.29 7.90 4 12 9 127.79 10.00 -4 -12 -9 122.49 8.80 -4 -12 -9 121.69 8.70 4 -12 9 106.09 8.30 2 12 11 61.89 6.40 2 12 11 49.60 6.90 -2 12 -11 53.09 5.70 2 -12 11 47.40 5.70 -2 -12 -11 54.59 6.10 0 12 13 10.10 3.60 0 12 13 11.10 3.70 0 12 -13 17.60 3.30 0 -12 -13 18.30 3.70 -2 12 15 -1.80 3.20 -2 12 15 5.50 3.50 2 12 -15 -0.50 2.60 -2 -12 15 -2.50 2.70 -4 12 17 1.10 3.40 -4 12 17 -2.70 3.50 4 12 -17 -1.40 2.80 -4 -12 17 -1.40 2.90 4 -12 -17 -2.10 3.50 -6 12 19 20.50 4.50 -6 12 19 24.60 4.80 6 12 -19 12.80 3.80 6 -12 -19 22.40 4.40 -6 -12 19 19.40 3.90 -8 12 21 19.60 5.20 8 12 -21 11.90 3.70 -8 12 21 6.90 4.50 -8 -12 21 14.00 4.10 8 -12 -21 14.20 4.40 -10 12 23 3.60 5.00 10 12 -23 -2.40 3.70 -10 12 23 -6.20 4.70 -10 -12 23 5.70 4.50 10 -12 -23 4.60 4.80 -27 13 14 -2.40 5.50 -27 -13 14 -3.30 5.20 -25 13 12 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6.60 4 4 -19 46.50 6.20 4 -4 -19 33.20 5.80 -4 -4 19 63.29 5.40 6 4 -21 5.30 3.20 6 4 -21 -2.40 3.30 6 4 -21 -0.90 2.80 -6 4 21 -5.10 3.30 -6 4 21 4.30 3.30 6 -4 -21 -0.80 3.10 -6 -4 21 -3.10 2.90 8 4 -23 -0.70 3.30 -8 4 23 7.10 3.40 -8 4 23 -5.20 3.50 8 4 -23 0.80 3.70 8 4 -23 -5.90 3.20 8 -4 -23 5.10 3.60 -8 -4 23 -3.20 3.30 10 4 -25 -1.40 3.60 10 4 -25 6.00 3.80 -10 4 25 0.90 3.80 -10 4 25 -2.50 3.90 -10 -4 25 -5.00 3.50 10 -4 -25 3.10 3.80 12 4 -27 -6.20 4.10 -12 4 27 0.70 4.60 12 4 -27 -0.80 4.00 -12 4 27 3.90 4.30 -12 -4 27 -0.30 3.80 12 -4 -27 2.50 4.60 -31 5 16 3.60 4.50 -31 -5 16 2.60 4.40 -31 -5 16 4.60 3.60 -29 -5 14 -6.10 3.10 29 -5 -14 -3.30 3.90 -29 -5 14 -5.10 3.50 -27 -5 12 -1.80 3.40 27 -5 -12 -1.70 3.50 -25 5 10 0.60 3.20 -25 -5 10 -2.00 3.10 25 -5 -10 0.20 3.40 -25 -5 10 -1.20 3.00 -23 5 8 43.80 3.70 -23 5 8 27.80 4.50 -23 -5 8 43.70 6.40 23 -5 -8 45.10 8.30 -23 -5 8 36.30 6.50 -21 5 6 42.10 3.90 -21 5 6 37.40 5.70 -21 -5 6 44.00 5.30 21 -5 -6 45.30 5.20 -21 -5 6 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6.70 1.80 -14 -6 -1 8.50 2.30 14 -6 1 8.10 2.00 12 6 3 0.80 1.90 -12 6 -3 1.30 1.70 12 6 3 -2.90 2.20 -12 6 -3 3.70 2.00 -12 -6 -3 0.00 1.70 12 -6 3 2.80 1.40 -12 -6 -3 -1.40 1.80 12 -6 3 0.90 1.70 -10 6 -5 0.10 1.60 10 6 5 -1.10 2.30 10 6 5 -1.20 1.80 -10 6 -5 1.50 1.90 10 -6 5 -0.40 1.20 -10 -6 -5 2.80 2.10 -10 -6 -5 -1.30 1.80 8 6 7 3.80 2.10 -8 6 -7 4.90 2.00 -8 6 -7 0.70 1.90 8 6 7 0.30 2.50 -8 -6 -7 3.50 2.10 8 -6 7 3.20 1.20 -6 6 -9 16.30 2.70 -6 6 -9 16.70 2.50 6 6 9 14.00 3.50 6 6 9 12.90 2.60 6 -6 9 13.50 1.70 -6 -6 -9 17.00 2.30 6 -6 9 21.00 2.80 -6 -6 -9 18.20 2.80 4 6 11 5.40 2.30 -4 6 -11 5.70 2.00 -4 6 -11 2.90 2.30 4 6 11 6.00 3.30 4 -6 11 3.20 1.20 -4 -6 -11 3.90 2.10 4 -6 11 3.10 1.70 -4 -6 -11 4.80 2.70 -2 6 -13 5.90 1.90 -2 6 -13 4.10 3.40 2 6 13 -4.90 5.10 2 6 13 2.50 2.60 -2 -6 -13 2.20 2.00 -2 -6 -13 -1.30 3.40 2 -6 13 -2.50 1.80 2 -6 13 1.90 1.30 0 6 15 42.90 5.80 0 6 -15 49.70 5.50 0 6 15 46.40 6.50 0 6 -15 51.39 4.70 0 -6 15 55.59 3.90 0 -6 -15 53.29 5.00 0 -6 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8 -1 25.30 4.70 -16 -8 1 21.20 3.20 -16 -8 1 21.40 3.20 16 -8 -1 25.40 4.20 14 8 1 234.28 14.60 -14 8 -1 240.28 14.10 -14 8 -1 225.88 14.10 14 8 1 252.77 14.60 14 -8 1 221.78 14.10 -14 -8 -1 230.08 13.80 14 -8 1 248.88 13.60 -14 -8 -1 238.48 13.70 -12 8 -3 2.20 1.90 12 8 3 1.00 2.10 12 8 3 -3.80 2.50 -12 8 -3 2.10 2.30 12 -8 3 -2.20 1.90 -12 -8 -3 0.80 1.90 -12 -8 -3 2.20 2.10 12 -8 3 3.70 1.40 -10 8 -5 -0.10 2.10 10 8 5 -0.10 2.60 -10 8 -5 -0.50 1.90 10 8 5 -1.10 1.90 10 -8 5 -0.10 1.20 -10 -8 -5 -1.10 1.90 10 -8 5 -1.90 1.80 -10 -8 -5 -1.70 2.00 8 8 7 7.90 3.00 -8 8 -7 6.80 2.30 8 8 7 3.90 2.40 -8 8 -7 5.10 2.20 8 -8 7 3.80 1.20 8 -8 7 6.60 1.80 -8 -8 -7 3.50 2.20 -8 -8 -7 2.80 2.30 6 8 9 73.29 7.90 -6 8 -9 84.69 6.20 -6 8 -9 72.69 8.20 6 8 9 90.49 7.70 -6 -8 -9 81.39 6.90 6 -8 9 86.29 5.80 -6 -8 -9 84.59 6.20 4 8 11 45.40 7.00 -4 8 -11 52.99 5.90 -4 8 -11 56.89 4.90 -4 -8 -11 41.30 6.10 -4 -8 -11 61.69 5.10 4 -8 11 47.60 4.70 2 8 13 8.50 3.60 -2 8 -13 14.70 2.90 2 8 13 13.70 3.30 -2 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65.29 7.50 -23 -9 8 70.39 6.30 23 -9 -8 74.89 7.20 -23 -9 8 69.79 7.60 -21 9 6 55.09 5.00 -21 9 6 48.30 6.50 21 9 -6 53.29 5.80 -21 -9 6 46.00 8.60 -21 -9 6 57.09 5.40 21 -9 -6 46.10 6.40 -19 9 4 0.30 2.30 -19 9 4 3.70 3.10 19 9 -4 3.60 2.80 -19 -9 4 2.50 2.90 19 -9 -4 -1.60 2.90 -19 -9 4 2.80 2.40 -17 9 2 54.59 5.40 17 9 -2 54.09 5.80 -17 9 2 47.90 6.00 17 -9 -2 48.80 5.40 -17 -9 2 46.90 5.20 -17 -9 2 40.50 5.50 17 -9 -2 56.59 5.60 -15 9 0 169.68 12.00 -15 9 0 175.78 11.00 15 9 0 184.98 11.60 15 -9 0 166.18 10.70 -15 -9 0 170.28 10.70 15 -9 0 177.38 10.60 -15 -9 0 165.68 10.80 13 9 2 77.39 7.70 -13 9 -2 73.79 6.10 -13 9 -2 70.09 6.30 13 9 2 63.49 7.10 -13 -9 -2 76.69 6.00 13 -9 2 73.89 5.90 -13 -9 -2 67.69 5.90 13 -9 2 74.09 5.30 11 9 4 1.80 3.00 -11 9 -4 5.30 2.40 -11 9 -4 6.60 2.30 11 9 4 6.20 2.70 11 -9 4 2.80 1.40 -11 -9 -4 7.40 2.30 11 -9 4 -1.20 2.10 -11 -9 -4 2.40 2.10 -9 9 -6 11.90 2.80 -9 9 -6 7.00 2.40 9 9 6 16.10 3.50 9 9 6 5.70 3.10 -9 -9 -6 2.20 2.20 -9 -9 -6 7.50 2.40 9 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-3.20 4.30 12 2 17 12.30 6.60 -12 2 -17 0.70 4.60 -12 -2 -17 1.40 4.50 -25 3 -4 -1.40 4.80 -25 3 -4 8.20 3.40 25 3 4 -0.80 5.20 -25 -3 -4 1.10 4.90 -23 3 -6 2.10 4.90 -23 3 -6 -5.10 3.40 23 3 6 1.20 5.50 -23 -3 -6 -5.80 4.60 -21 3 -8 3.90 3.40 -21 3 -8 -3.00 4.40 21 3 8 -3.30 5.20 -21 -3 -8 4.40 4.60 -19 3 -10 6.60 4.40 19 3 10 -6.00 5.30 -19 3 -10 -1.00 3.50 -19 -3 -10 0.20 4.60 17 3 12 -1.20 5.70 -17 3 -12 3.80 4.50 -17 3 -12 4.10 3.90 -17 -3 -12 5.10 4.90 15 3 14 -0.90 5.60 -15 3 -14 0.40 4.10 -15 3 -14 -1.20 4.20 -15 -3 -14 -1.90 4.50 -13 3 -16 4.80 4.20 13 3 16 -0.20 5.80 -13 3 -16 -3.50 4.40 -13 -3 -16 -3.80 4.40 -24 4 -5 1.10 3.50 24 4 5 -0.50 5.30 -24 -4 -5 -2.00 5.00 -22 4 -7 4.70 4.90 -22 4 -7 1.20 3.50 22 4 7 -0.30 5.30 -22 -4 -7 -3.00 4.90 -20 4 -9 -7.40 4.30 -20 4 -9 0.80 3.50 20 4 9 -1.50 5.10 -20 -4 -9 -3.70 4.60 -18 4 -11 -2.90 3.70 -18 4 -11 7.30 4.60 18 4 11 -6.40 5.50 -18 -4 -11 0.50 4.60 -16 4 -13 -0.60 3.80 -16 4 -13 5.20 4.50 16 4 13 -3.60 5.60 -16 -4 -13 1.60 4.70 -14 4 -15 -0.70 4.00 -14 4 -15 -8.20 4.40 14 4 15 1.10 5.80 -14 -4 -15 -8.60 4.30 -12 4 -17 -4.20 4.50 12 4 17 -5.80 6.00 -12 -4 -17 0.60 4.90 -23 5 -6 3.50 4.80 -23 5 -6 3.30 4.20 23 5 6 2.20 5.40 -21 5 -8 0.40 3.50 21 5 8 -9.50 5.40 -21 5 -8 0.10 4.70 -21 -5 -8 -9.00 4.70 -19 5 -10 -3.70 3.70 19 5 10 -1.00 5.50 -19 5 -10 1.40 4.70 -19 -5 -10 1.70 4.70 17 5 12 2.80 5.70 -17 5 -12 -0.50 3.80 -17 5 -12 7.40 4.70 -17 -5 -12 2.70 4.70 -15 5 -14 2.20 4.30 -15 5 -14 8.00 4.10 15 5 14 -5.10 5.70 -15 -5 -14 -5.20 4.80 -13 5 -16 -0.60 4.30 13 5 16 -4.70 5.90 -13 5 -16 -6.00 4.40 -13 -5 -16 -3.50 5.10 -22 6 -7 0.90 4.80 22 6 7 -5.70 5.30 -22 6 -7 0.90 3.60 -22 -6 -7 -4.00 4.90 -20 6 -9 -0.40 3.70 -20 6 -9 6.40 4.80 20 6 9 0.50 5.50 -20 -6 -9 -4.00 4.70 -18 6 -11 8.10 5.10 -18 6 -11 5.00 3.80 18 6 11 -6.60 5.70 -18 -6 -11 8.60 5.00 -16 6 -13 7.40 4.70 16 6 13 3.30 6.10 -16 6 -13 5.30 4.10 -16 -6 -13 2.90 5.00 -19 7 -10 21.00 4.40 -19 7 -10 17.10 5.30 19 7 10 18.60 6.40 -19 -7 -10 10.70 5.70 -24 0 -6 -3.60 5.30 -22 0 -8 0.10 5.20 -22 0 -8 0.70 3.70 -20 0 -10 -1.70 4.00 -20 0 -10 -9.60 5.00 18 0 12 2.20 5.70 -18 0 -12 -1.00 4.60 -16 0 -14 2.50 4.70 16 0 14 -4.60 5.90 -23 1 -7 2.70 3.70 -23 1 -7 -4.80 5.30 -23 -1 -7 -7.70 5.40 -23 -1 -7 -7.20 3.90 -21 1 -9 16.80 3.90 -21 1 -9 6.10 5.30 21 1 9 7.80 5.60 -21 -1 -9 12.60 5.50 -19 1 -11 63.29 8.80 19 1 11 49.80 9.50 -19 1 -11 54.49 7.70 -19 -1 -11 61.39 8.90 -17 1 -13 26.20 5.10 17 1 13 33.20 7.50 -17 1 -13 32.70 5.80 -17 -1 -13 29.80 5.70 15 1 15 -0.20 6.50 -15 1 -15 6.50 4.90 -15 1 -15 -1.70 4.60 -15 -1 -15 2.90 5.10 -22 2 -8 4.50 3.60 -22 2 -8 0.10 5.00 22 2 8 2.40 5.70 -22 -2 -8 -7.70 5.10 -20 2 -10 -2.30 3.70 20 2 10 -3.70 6.00 -20 2 -10 -3.10 4.90 -20 -2 -10 -2.60 5.20 -18 2 -12 3.10 4.00 -18 2 -12 -1.70 4.70 18 2 12 -5.50 5.80 -18 -2 -12 -1.50 4.90 16 2 14 2.80 6.20 -16 2 -14 2.20 4.30 -16 2 -14 -1.00 4.80 -16 -2 -14 -5.20 4.80 21 3 9 20.10 6.30 -21 3 -9 19.70 4.00 -21 3 -9 20.80 5.50 -21 -3 -9 14.90 5.90 -19 3 -11 33.90 6.00 -19 3 -11 43.50 7.20 19 3 11 38.30 7.40 -19 -3 -11 58.79 9.20 17 3 13 15.20 6.90 -17 3 -13 28.40 5.50 -17 3 -13 24.00 4.80 -17 -3 -13 31.20 6.00 -20 4 -10 3.30 5.00 20 4 10 -3.90 6.00 -20 -4 -10 -2.50 5.30 -18 4 -12 0.80 5.00 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 8134 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy Ru1 Ru 0.25885(2) 0.75873(2) 0.25561(2) 0.03789(17) Uani 1 1 d . . . P2 P 0.25349(6) 0.76322(6) 0.35457(6) 0.0375(3) Uani 1 1 d . . . P1 P 0.26484(6) 0.76019(6) 0.15759(7) 0.0385(3) Uani 1 1 d . . . Cl1 Cl 0.25446(6) 0.88202(7) 0.25107(7) 0.0558(4) Uani 1 1 d . . . O1 O 0.17091(16) 0.73487(18) 0.1927(2) 0.0562(10) Uani 1 1 d . . . O2 O 0.38895(15) 0.45077(17) 0.3378(2) 0.0616(11) Uani 1 1 d . . . N1 N 0.26024(14) 0.64918(19) 0.25910(17) 0.0314(8) Uani 1 1 d . . . C15 C 0.3456(2) 0.7396(2) 0.3115(2) 0.0390(11) Uani 1 1 d . . . C16 C 0.3603(2) 0.6679(2) 0.3226(2) 0.0394(11) Uani 1 1 d . . . N2 N 0.48115(18) 0.5453(2) 0.4077(2) 0.0541(12) Uani 1 1 d . . . C7 C 0.3116(2) 0.6178(2) 0.2919(2) 0.0379(11) Uani 1 1 d . . . C9 C 0.3789(2) 0.5224(2) 0.3349(3) 0.0457(12) Uani 1 1 d . . . C10 C 0.4286(2) 0.5689(2) 0.3697(2) 0.0398(11) Uani 1 1 d . . . C6 C 0.2051(2) 0.6193(2) 0.2264(3) 0.0455(12) Uani 1 1 d . . . C22 C 0.4887(2) 0.4724(3) 0.4150(3) 0.0489(13) Uani 1 1 d . . . C8 C 0.3249(2) 0.5447(3) 0.2985(3) 0.0496(13) Uani 1 1 d . . . H8 H 0.2953 0.5119 0.2770 0.060 Uiso 1 1 calc R U . C29 C 0.2127(2) 0.8169(3) 0.0884(3) 0.0457(12) Uani 1 1 d . . . C12 C 0.4609(2) 0.6945(3) 0.3877(3) 0.0612(16) Uani 1 1 d . . . H12 H 0.4992 0.6803 0.4137 0.073 Uiso 1 1 calc R U . C17 C 0.4430(2) 0.4256(3) 0.3800(3) 0.0475(13) Uani 1 1 d . . . C1 C 0.1602(2) 0.6688(3) 0.1908(3) 0.0499(13) Uani 1 1 d . . . C47 C 0.1955(2) 0.8173(3) 0.3502(3) 0.0508(13) Uani 1 1 d . . . C11 C 0.4173(2) 0.6443(2) 0.3605(2) 0.0424(11) Uani 1 1 d . . . C13 C 0.4475(3) 0.7649(3) 0.3762(3) 0.0624(17) Uani 1 1 d . . . H13 H 0.4771 0.7980 0.3943 0.075 Uiso 1 1 calc R U . C53 C 0.2420(3) 0.6770(3) 0.3804(3) 0.0514(13) Uani 1 1 d . . . C23 C 0.3321(2) 0.7915(3) 0.1659(3) 0.0562(14) Uani 1 1 d . . . C41 C 0.3171(2) 0.7993(3) 0.4292(3) 0.0503(13) Uani 1 1 d . . . C58 C 0.2848(3) 0.6249(3) 0.4029(3) 0.0542(14) Uani 1 1 d . . . H58 H 0.3204 0.6363 0.4086 0.065 Uiso 1 1 calc R U . C52 C 0.2009(3) 0.8495(3) 0.4056(3) 0.0608(15) Uani 1 1 d . . . H52 H 0.2356 0.8470 0.4460 0.073 Uiso 1 1 calc R U . C5 C 0.1908(3) 0.5493(3) 0.2283(4) 0.080(2) Uani 1 1 d . . . H5 H 0.2199 0.5175 0.2551 0.096 Uiso 1 1 calc R U . C51 C 0.1541(3) 0.8861(3) 0.4010(4) 0.077(2) Uani 1 1 d . . . H51 H 0.1576 0.9072 0.4386 0.092 Uiso 1 1 calc R U . C35 C 0.2494(3) 0.6726(3) 0.1183(3) 0.0551(14) Uani 1 1 d . . . C32 C 0.1313(3) 0.8942(3) -0.0208(3) 0.075(2) Uani 1 1 d . . . H32 H 0.1038 0.9191 -0.0579 0.090 Uiso 1 1 calc R U . C18 C 0.4513(2) 0.3542(3) 0.3864(3) 0.0555(14) Uani 1 1 d . . . H18 H 0.4204 0.3240 0.3612 0.067 Uiso 1 1 calc R U . C40 C 0.2892(3) 0.6174(3) 0.1511(3) 0.0616(16) Uani 1 1 d . . . H40 H 0.3246 0.6271 0.1891 0.074 Uiso 1 1 calc R U . C34 C 0.1604(3) 0.8351(3) 0.0814(3) 0.0667(17) Uani 1 1 d . . . H34 H 0.1526 0.8220 0.1139 0.080 Uiso 1 1 calc R U . C14 C 0.3910(2) 0.7881(3) 0.3383(3) 0.0543(14) Uani 1 1 d . . . H14 H 0.3833 0.8362 0.3307 0.065 Uiso 1 1 calc R U . C19 C 0.5042(3) 0.3269(3) 0.4294(3) 0.0614(15) Uani 1 1 d . . . H19 H 0.5094 0.2782 0.4341 0.074 Uiso 1 1 calc R U . C57 C 0.2754(3) 0.5580(3) 0.4166(3) 0.0698(18) Uani 1 1 d . . . H57 H 0.3043 0.5242 0.4307 0.084 Uiso 1 1 calc R U . C42 C 0.3410(3) 0.7676(3) 0.4913(3) 0.0637(16) Uani 1 1 d . . . H42 H 0.3251 0.7260 0.4961 0.076 Uiso 1 1 calc R U . C46 C 0.3425(3) 0.8615(3) 0.4246(3) 0.0709(17) Uani 1 1 d . . . H46 H 0.3275 0.8839 0.3838 0.085 Uiso 1 1 calc R U . C39 C 0.2763(4) 0.5505(4) 0.1275(4) 0.080(2) Uani 1 1 d . . . H39 H 0.3025 0.5143 0.1501 0.097 Uiso 1 1 calc R U . C21 C 0.5432(2) 0.4436(3) 0.4587(3) 0.0648(16) Uani 1 1 d . . . H21 H 0.5747 0.4734 0.4828 0.078 Uiso 1 1 calc R U . C30 C 0.2239(3) 0.8401(3) 0.0411(3) 0.0666(16) Uani 1 1 d . . . H30 H 0.2591 0.8298 0.0453 0.080 Uiso 1 1 calc R U . C20 C 0.5503(3) 0.3719(3) 0.4660(3) 0.0714(18) Uani 1 1 d . . . H20 H 0.5864 0.3532 0.4959 0.086 Uiso 1 1 calc R U . C43 C 0.3881(3) 0.7979(4) 0.5457(3) 0.083(2) Uani 1 1 d . . . H43 H 0.4035 0.7765 0.5870 0.100 Uiso 1 1 calc R U . C54 C 0.1905(3) 0.6578(3) 0.3733(4) 0.076(2) Uani 1 1 d . . . H54 H 0.1610 0.6909 0.3588 0.092 Uiso 1 1 calc R U . C56 C 0.2249(4) 0.5404(3) 0.4099(4) 0.089(2) Uani 1 1 d . . . H56 H 0.2192 0.4949 0.4204 0.107 Uiso 1 1 calc R U . C31 C 0.1830(3) 0.8788(4) -0.0129(3) 0.079(2) Uani 1 1 d . . . H31 H 0.1914 0.8946 -0.0443 0.095 Uiso 1 1 calc R U . C48 C 0.1441(3) 0.8232(5) 0.2912(3) 0.094(3) Uani 1 1 d . . . H48 H 0.1401 0.8028 0.2531 0.112 Uiso 1 1 calc R U . C2 C 0.1033(3) 0.6423(3) 0.1534(4) 0.075(2) Uani 1 1 d . . . H2 H 0.0731 0.6734 0.1282 0.090 Uiso 1 1 calc R U . C33 C 0.1199(3) 0.8726(4) 0.0263(3) 0.076(2) Uani 1 1 d . . . H33 H 0.0845 0.8832 0.0214 0.091 Uiso 1 1 calc R U . C28 C 0.3630(3) 0.7528(3) 0.1452(4) 0.080(2) Uani 1 1 d . . . H28 H 0.3515 0.7071 0.1293 0.095 Uiso 1 1 calc R U . C50 C 0.1038(3) 0.8907(4) 0.3423(4) 0.088(2) Uani 1 1 d . . . H50 H 0.0730 0.9155 0.3394 0.106 Uiso 1 1 calc R U . C4 C 0.1353(3) 0.5258(3) 0.1919(5) 0.103(3) Uani 1 1 d . . . H4 H 0.1267 0.4783 0.1929 0.124 Uiso 1 1 calc R U . C45 C 0.3895(4) 0.8896(4) 0.4798(4) 0.091(2) Uani 1 1 d . . . H45 H 0.4058 0.9311 0.4757 0.109 Uiso 1 1 calc R U . C36 C 0.1982(3) 0.6578(4) 0.0612(4) 0.080(2) Uani 1 1 d . . . H36 H 0.1718 0.6937 0.0384 0.097 Uiso 1 1 calc R U . C44 C 0.4126(3) 0.8589(5) 0.5399(4) 0.090(2) Uani 1 1 d . . . H44 H 0.4445 0.8786 0.5768 0.108 Uiso 1 1 calc R U . C55 C 0.1818(4) 0.5891(4) 0.3876(5) 0.099(3) Uani 1 1 d . . . H55 H 0.1464 0.5764 0.3820 0.119 Uiso 1 1 calc R U . C38 C 0.2257(5) 0.5356(4) 0.0715(5) 0.101(3) Uani 1 1 d . . . H38 H 0.2176 0.4893 0.0559 0.122 Uiso 1 1 calc R U . C24 C 0.3501(3) 0.8581(4) 0.1894(4) 0.079(2) Uani 1 1 d . . . H24 H 0.3295 0.8849 0.2031 0.095 Uiso 1 1 calc R U . C49 C 0.0981(4) 0.8595(5) 0.2875(4) 0.117(3) Uani 1 1 d . . . H49 H 0.0632 0.8623 0.2473 0.140 Uiso 1 1 calc R U . C27 C 0.4105(4) 0.7814(5) 0.1478(5) 0.114(3) Uani 1 1 d . . . H27 H 0.4305 0.7554 0.1328 0.137 Uiso 1 1 calc R U . C3 C 0.0921(3) 0.5734(3) 0.1535(4) 0.093(3) Uani 1 1 d . . . H3 H 0.0544 0.5573 0.1273 0.112 Uiso 1 1 calc R U . C26 C 0.4287(4) 0.8489(6) 0.1729(5) 0.112(3) Uani 1 1 d . . . H26 H 0.4614 0.8680 0.1757 0.134 Uiso 1 1 calc R U . C25 C 0.3989(4) 0.8866(5) 0.1932(4) 0.106(3) Uani 1 1 d . . . H25 H 0.4109 0.9320 0.2099 0.127 Uiso 1 1 calc R U . C37 C 0.1858(4) 0.5883(4) 0.0373(4) 0.103(3) Uani 1 1 d . . . H37 H 0.1511 0.5777 -0.0013 0.123 Uiso 1 1 calc R U . Cl2 Cl 0.06018(15) 0.0665(3) 0.2811(2) 0.1997(17) Uani 1 1 d . . . C59 C 0.0000 0.1145(9) 0.2500 0.279(17) Uani 1 2 d S T P H59A H 0.0028 0.1448 0.2848 0.335 Uiso 0.5 1 calc R U P H59B H -0.0028 0.1448 0.2152 0.335 Uiso 0.5 1 calc R U P Cl3 Cl 0.5000 0.8004(7) 0.7500 0.405(7) Uani 1 2 d DS T P Cl4 Cl 0.5000 0.9440(5) 0.7500 0.406(7) Uani 1 2 d DS T P C60 C 0.5264(11) 0.8718(10) 0.7442(13) 1.54(6) Uani 0.5 1 d D . P H60 H 0.4994 0.8718 0.6961 1.852 Uiso 1 1 calc R U . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Ru1 0.0411(3) 0.0254(2) 0.0477(3) 0.00267(16) 0.0235(2) 0.00485(14) P2 0.0395(7) 0.0314(6) 0.0423(7) 0.0034(5) 0.0218(6) 0.0069(5) P1 0.0408(7) 0.0309(6) 0.0468(7) 0.0016(5) 0.0249(6) 0.0036(5) Cl1 0.0748(10) 0.0249(6) 0.0725(9) 0.0051(6) 0.0418(8) 0.0084(5) O1 0.043(2) 0.035(2) 0.075(3) 0.0090(17) 0.020(2) 0.0106(15) O2 0.043(2) 0.0283(18) 0.088(3) 0.0010(18) 0.016(2) 0.0046(14) N1 0.0269(19) 0.031(2) 0.038(2) 0.0025(15) 0.0178(17) 0.0018(14) C15 0.040(3) 0.031(2) 0.049(3) -0.004(2) 0.025(2) -0.0013(19) C16 0.047(3) 0.023(2) 0.050(3) -0.003(2) 0.027(2) -0.0054(19) N2 0.038(3) 0.046(3) 0.067(3) -0.002(2) 0.019(2) 0.0032(19) C7 0.038(3) 0.027(2) 0.047(3) 0.000(2) 0.021(2) -0.0016(18) C9 0.041(3) 0.028(2) 0.064(3) 0.003(2) 0.024(3) 0.005(2) C10 0.033(3) 0.033(3) 0.045(3) -0.001(2) 0.015(2) 0.0029(19) C6 0.041(3) 0.033(3) 0.057(3) -0.001(2) 0.022(3) 0.005(2) C22 0.042(3) 0.040(3) 0.062(3) 0.006(2) 0.025(3) 0.011(2) C8 0.037(3) 0.031(3) 0.065(3) 0.001(2) 0.016(3) 0.001(2) C29 0.055(3) 0.038(3) 0.043(3) 0.002(2) 0.025(3) 0.003(2) C12 0.042(3) 0.043(3) 0.088(4) -0.005(3) 0.026(3) -0.003(2) C17 0.038(3) 0.043(3) 0.058(3) 0.004(2) 0.021(3) 0.007(2) C1 0.041(3) 0.037(3) 0.066(4) 0.003(2) 0.025(3) 0.001(2) C47 0.048(3) 0.047(3) 0.061(3) 0.006(3) 0.031(3) 0.011(2) C11 0.037(3) 0.036(3) 0.050(3) 0.002(2) 0.019(2) 0.002(2) C13 0.044(3) 0.036(3) 0.095(5) -0.010(3) 0.028(3) -0.008(2) C53 0.065(4) 0.042(3) 0.052(3) 0.000(2) 0.033(3) -0.005(2) C23 0.048(3) 0.065(4) 0.059(3) 0.009(3) 0.030(3) -0.002(3) C41 0.049(3) 0.052(3) 0.048(3) -0.010(2) 0.023(3) 0.002(2) C58 0.057(4) 0.046(3) 0.049(3) 0.006(2) 0.021(3) 0.008(2) C52 0.065(4) 0.055(3) 0.070(4) -0.001(3) 0.040(3) 0.009(3) C5 0.045(4) 0.038(3) 0.126(6) 0.007(3) 0.023(4) 0.003(2) C51 0.097(6) 0.075(5) 0.087(5) 0.004(4) 0.067(5) 0.021(4) C35 0.068(4) 0.040(3) 0.070(4) -0.008(3) 0.046(3) -0.005(3) C32 0.098(6) 0.065(4) 0.044(3) 0.006(3) 0.024(4) 0.019(4) C18 0.046(3) 0.038(3) 0.070(4) 0.001(3) 0.021(3) 0.006(2) C40 0.085(4) 0.048(3) 0.071(4) 0.005(3) 0.054(4) 0.007(3) C34 0.057(4) 0.086(5) 0.058(4) 0.022(3) 0.031(3) 0.023(3) C14 0.055(3) 0.027(3) 0.078(4) -0.001(2) 0.032(3) -0.003(2) C19 0.060(4) 0.039(3) 0.076(4) 0.006(3) 0.029(3) 0.014(3) C57 0.094(5) 0.047(4) 0.064(4) 0.010(3) 0.038(4) 0.006(3) C42 0.069(4) 0.060(4) 0.057(4) -0.002(3) 0.029(3) 0.017(3) C46 0.072(4) 0.063(4) 0.072(4) -0.010(3) 0.034(4) -0.012(3) C39 0.123(7) 0.048(4) 0.095(5) -0.001(4) 0.074(5) 0.007(4) C21 0.038(3) 0.056(4) 0.081(4) -0.001(3) 0.017(3) 0.009(2) C30 0.072(4) 0.074(4) 0.064(4) 0.007(3) 0.042(4) 0.013(3) C20 0.052(4) 0.056(4) 0.081(4) 0.006(3) 0.017(3) 0.025(3) C43 0.081(5) 0.094(6) 0.052(4) -0.012(4) 0.019(4) 0.024(4) C54 0.079(5) 0.055(4) 0.123(6) 0.006(4) 0.071(5) 0.000(3) C56 0.134(7) 0.040(4) 0.117(6) 0.002(4) 0.081(6) -0.006(4) C31 0.100(6) 0.084(5) 0.053(4) 0.015(3) 0.040(4) 0.016(4) C48 0.073(5) 0.150(8) 0.054(4) 0.008(4) 0.030(4) 0.051(5) C2 0.043(3) 0.052(4) 0.105(5) 0.011(3) 0.021(4) 0.008(3) C33 0.073(5) 0.086(5) 0.063(4) 0.023(4) 0.031(4) 0.031(4) C28 0.076(5) 0.073(5) 0.119(6) 0.001(4) 0.072(5) 0.001(3) C50 0.089(6) 0.102(6) 0.096(6) 0.033(5) 0.064(5) 0.052(4) C4 0.052(4) 0.041(3) 0.182(9) 0.003(4) 0.037(5) -0.004(3) C45 0.090(6) 0.082(5) 0.103(6) -0.036(5) 0.052(5) -0.023(4) C36 0.078(5) 0.070(4) 0.086(5) -0.023(4) 0.037(4) -0.010(4) C44 0.065(5) 0.108(7) 0.078(5) -0.036(5) 0.025(4) -0.006(4) C55 0.110(6) 0.065(5) 0.163(8) -0.013(5) 0.100(6) -0.023(4) C38 0.158(9) 0.052(5) 0.124(7) -0.022(5) 0.094(7) -0.023(5) C24 0.084(5) 0.072(5) 0.101(5) -0.016(4) 0.062(5) -0.022(4) C49 0.081(6) 0.180(9) 0.088(6) 0.027(6) 0.042(5) 0.073(6) C27 0.109(7) 0.113(7) 0.178(10) 0.005(7) 0.114(8) 0.006(6) C3 0.044(4) 0.053(4) 0.146(7) -0.006(4) 0.023(4) -0.011(3) C26 0.072(5) 0.152(9) 0.128(8) 0.019(7) 0.064(6) -0.026(6) C25 0.110(7) 0.107(7) 0.120(7) -0.022(5) 0.074(6) -0.052(5) C37 0.098(6) 0.085(6) 0.107(6) -0.037(5) 0.041(5) -0.037(5) Cl2 0.120(3) 0.257(5) 0.206(4) 0.046(3) 0.074(3) 0.015(3) C59 0.158(19) 0.086(12) 0.35(3) 0.000 -0.042(18) 0.000 Cl3 0.426(18) 0.309(12) 0.309(12) 0.000 0.070(11) 0.000 Cl4 0.296(12) 0.266(11) 0.68(2) 0.000 0.269(14) 0.000 C60 2.00(9) 2.00(10) 2.00(9) 2.00(8) 2.00(8) 2.00(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 C15 Ru1 N1 78.87(16) . . C15 Ru1 O1 157.09(16) . . N1 Ru1 O1 78.72(13) . . C15 Ru1 Cl1 102.71(13) . . N1 Ru1 Cl1 178.28(10) . . O1 Ru1 Cl1 99.76(10) . . C15 Ru1 P1 89.46(15) . . N1 Ru1 P1 92.33(10) . . O1 Ru1 P1 86.78(12) . . Cl1 Ru1 P1 88.38(4) . . C15 Ru1 P2 90.65(14) . . N1 Ru1 P2 90.33(10) . . O1 Ru1 P2 94.15(12) . . Cl1 Ru1 P2 88.96(4) . . P1 Ru1 P2 177.30(4) . . C53 P2 C47 103.0(3) . . C53 P2 C41 104.5(3) . . C47 P2 C41 101.5(2) . . C53 P2 Ru1 113.51(18) . . C47 P2 Ru1 116.56(18) . . C41 P2 Ru1 116.01(19) . . C23 P1 C35 107.4(3) . . C23 P1 C29 99.8(2) . . C35 P1 C29 101.9(3) . . C23 P1 Ru1 117.66(19) . . C35 P1 Ru1 111.36(18) . . C29 P1 Ru1 116.96(17) . . C1 O1 Ru1 112.9(3) . . C17 O2 C9 119.4(4) . . C7 N1 C6 129.7(4) . . C7 N1 Ru1 117.4(3) . . C6 N1 Ru1 112.9(3) . . C14 C15 C16 116.8(5) . . C14 C15 Ru1 128.8(4) . . C16 C15 Ru1 114.4(3) . . C11 C16 C15 122.8(4) . . C11 C16 C7 121.5(4) . . C15 C16 C7 115.7(4) . . C10 N2 C22 117.4(4) . . N1 C7 C8 128.9(4) . . N1 C7 C16 113.7(4) . . C8 C7 C16 117.4(4) . . C8 C9 O2 117.9(4) . . C8 C9 C10 124.3(4) . . O2 C9 C10 117.7(4) . . N2 C10 C11 120.5(4) . . N2 C10 C9 122.9(4) . . C11 C10 C9 116.6(4) . . C5 C6 N1 127.3(5) . . C5 C6 C1 118.8(5) . . N1 C6 C1 113.9(4) . . N2 C22 C17 121.9(4) . . N2 C22 C21 120.6(5) . . C17 C22 C21 117.6(5) . . C9 C8 C7 120.9(5) . . C9 C8 H8 119.6 . . C7 C8 H8 119.6 . . C30 C29 C34 118.1(5) . . C30 C29 P1 120.9(4) . . C34 C29 P1 121.0(4) . . C13 C12 C11 119.9(5) . . C13 C12 H12 120.1 . . C11 C12 H12 120.1 . . O2 C17 C18 118.7(5) . . O2 C17 C22 120.0(4) . . C18 C17 C22 121.3(5) . . O1 C1 C2 121.6(5) . . O1 C1 C6 121.0(5) . . C2 C1 C6 117.4(5) . . C48 C47 C52 118.5(5) . . C48 C47 P2 119.5(5) . . C52 C47 P2 121.9(4) . . C12 C11 C16 118.2(5) . . C12 C11 C10 122.7(4) . . C16 C11 C10 119.1(4) . . C12 C13 C14 121.8(5) . . C12 C13 H13 119.1 . . C14 C13 H13 119.1 . . C54 C53 C58 117.0(5) . . C54 C53 P2 122.5(5) . . C58 C53 P2 120.2(4) . . C24 C23 C28 118.5(6) . . C24 C23 P1 118.1(5) . . C28 C23 P1 123.3(5) . . C42 C41 C46 117.8(6) . . C42 C41 P2 122.6(5) . . C46 C41 P2 119.6(5) . . C57 C58 C53 121.5(6) . . C57 C58 H58 119.3 . . C53 C58 H58 119.3 . . C47 C52 C51 120.1(6) . . C47 C52 H52 119.9 . . C51 C52 H52 119.9 . . C4 C5 C6 121.7(6) . . C4 C5 H5 119.1 . . C6 C5 H5 119.1 . . C50 C51 C52 120.2(6) . . C50 C51 H51 119.9 . . C52 C51 H51 119.9 . . C36 C35 C40 119.0(6) . . C36 C35 P1 122.0(5) . . C40 C35 P1 118.8(5) . . C31 C32 C33 119.0(6) . . C31 C32 H32 120.5 . . C33 C32 H32 120.5 . . C19 C18 C17 120.6(5) . . C19 C18 H18 119.7 . . C17 C18 H18 119.7 . . C39 C40 C35 120.4(7) . . C39 C40 H40 119.8 . . C35 C40 H40 119.8 . . C33 C34 C29 120.2(6) . . C33 C34 H34 119.9 . . C29 C34 H34 119.9 . . C13 C14 C15 120.4(5) . . C13 C14 H14 119.8 . . C15 C14 H14 119.8 . . C18 C19 C20 119.7(5) . . C18 C19 H19 120.1 . . C20 C19 H19 120.1 . . C56 C57 C58 120.7(7) . . C56 C57 H57 119.7 . . C58 C57 H57 119.7 . . C43 C42 C41 119.9(7) . . C43 C42 H42 120.0 . . C41 C42 H42 120.0 . . C45 C46 C41 120.4(7) . . C45 C46 H46 119.8 . . C41 C46 H46 119.8 . . C38 C39 C40 120.8(7) . . C38 C39 H39 119.6 . . C40 C39 H39 119.6 . . C20 C21 C22 120.3(6) . . C20 C21 H21 119.9 . . C22 C21 H21 119.9 . . C29 C30 C31 120.5(6) . . C29 C30 H30 119.7 . . C31 C30 H30 119.7 . . C21 C20 C19 120.5(5) . . C21 C20 H20 119.7 . . C19 C20 H20 119.7 . . C44 C43 C42 121.3(7) . . C44 C43 H43 119.4 . . C42 C43 H43 119.4 . . C53 C54 C55 120.6(6) . . C53 C54 H54 119.7 . . C55 C54 H54 119.7 . . C57 C56 C55 120.0(7) . . C57 C56 H56 120.0 . . C55 C56 H56 120.0 . . C32 C31 C30 121.2(6) . . C32 C31 H31 119.4 . . C30 C31 H31 119.4 . . C47 C48 C49 120.7(7) . . C47 C48 H48 119.6 . . C49 C48 H48 119.6 . . C3 C2 C1 121.4(6) . . C3 C2 H2 119.3 . . C1 C2 H2 119.3 . . C32 C33 C34 120.9(7) . . C32 C33 H33 119.6 . . C34 C33 H33 119.6 . . C27 C28 C23 120.6(7) . . C27 C28 H28 119.7 . . C23 C28 H28 119.7 . . C51 C50 C49 120.2(6) . . C51 C50 H50 119.9 . . C49 C50 H50 119.9 . . C5 C4 C3 119.1(6) . . C5 C4 H4 120.5 . . C3 C4 H4 120.5 . . C44 C45 C46 121.8(8) . . C44 C45 H45 119.1 . . C46 C45 H45 119.1 . . C35 C36 C37 119.8(7) . . C35 C36 H36 120.1 . . C37 C36 H36 120.1 . . C45 C44 C43 118.8(7) . . C45 C44 H44 120.6 . . C43 C44 H44 120.6 . . C56 C55 C54 120.3(7) . . C56 C55 H55 119.9 . . C54 C55 H55 119.9 . . C39 C38 C37 120.7(7) . . C39 C38 H38 119.6 . . C37 C38 H38 119.6 . . C23 C24 C25 121.0(7) . . C23 C24 H24 119.5 . . C25 C24 H24 119.5 . . C50 C49 C48 120.3(8) . . C50 C49 H49 119.9 . . C48 C49 H49 119.9 . . C28 C27 C26 120.0(8) . . C28 C27 H27 120.0 . . C26 C27 H27 120.0 . . C2 C3 C4 121.2(6) . . C2 C3 H3 119.4 . . C4 C3 H3 119.4 . . C25 C26 C27 119.7(7) . . C25 C26 H26 120.2 . . C27 C26 H26 120.2 . . C26 C25 C24 120.2(8) . . C26 C25 H25 119.9 . . C24 C25 H25 119.9 . . C38 C37 C36 119.4(8) . . C38 C37 H37 120.3 . . C36 C37 H37 120.3 . . Cl2 C59 Cl2 114.1(10) 2 . Cl2 C59 H59A 108.7 2 . Cl2 C59 H59A 108.7 . . Cl2 C59 H59B 108.7 2 . Cl2 C59 H59B 108.7 . . H59A C59 H59B 107.6 . . C60 Cl3 C60 61.1(11) . 2_656 C60 Cl4 C60 60.5(14) . 2_656 Cl3 C60 Cl4 119.2(11) . . Cl3 C60 C60 59.5(6) . 2_656 Cl4 C60 C60 59.7(7) . 2_656 Cl3 C60 H60 90.0 . . Cl4 C60 H60 90.0 . . C60 C60 H60 90.1 2_656 . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Ru1 C15 2.046(5) . Ru1 N1 2.072(4) . Ru1 O1 2.104(4) . Ru1 Cl1 2.3331(15) . Ru1 P1 2.4022(18) . Ru1 P2 2.4159(17) . P2 C53 1.824(5) . P2 C47 1.835(5) . P2 C41 1.840(5) . P1 C23 1.832(6) . P1 C35 1.836(5) . P1 C29 1.848(5) . O1 C1 1.278(6) . O2 C17 1.362(6) . O2 C9 1.376(6) . N1 C7 1.332(6) . N1 C6 1.399(6) . C15 C14 1.397(7) . C15 C16 1.400(6) . C16 C11 1.399(7) . C16 C7 1.474(6) . N2 C10 1.307(6) . N2 C22 1.390(6) . C7 C8 1.416(6) . C9 C8 1.327(7) . C9 C10 1.454(7) . C10 C11 1.450(6) . C6 C5 1.385(7) . C6 C1 1.416(7) . C22 C17 1.394(7) . C22 C21 1.401(7) . C8 H8 0.9300 . C29 C30 1.371(8) . C29 C34 1.386(8) . C12 C13 1.370(7) . C12 C11 1.386(7) . C12 H12 0.9300 . C17 C18 1.362(7) . C1 C2 1.413(8) . C47 C48 1.371(8) . C47 C52 1.379(8) . C13 C14 1.385(8) . C13 H13 0.9300 . C53 C54 1.370(8) . C53 C58 1.398(7) . C23 C24 1.359(8) . C23 C28 1.381(8) . C41 C42 1.393(8) . C41 C46 1.395(8) . C58 C57 1.362(8) . C58 H58 0.9300 . C52 C51 1.401(8) . C52 H52 0.9300 . C5 C4 1.365(8) . C5 H5 0.9300 . C51 C50 1.351(10) . C51 H51 0.9300 . C35 C36 1.371(9) . C35 C40 1.410(8) . C32 C31 1.351(10) . C32 C33 1.362(9) . C32 H32 0.9300 . C18 C19 1.359(8) . C18 H18 0.9300 . C40 C39 1.353(8) . C40 H40 0.9300 . C34 C33 1.384(8) . C34 H34 0.9300 . C14 H14 0.9300 . C19 C20 1.382(8) . C19 H19 0.9300 . C57 C56 1.339(10) . C57 H57 0.9300 . C42 C43 1.380(9) . C42 H42 0.9300 . C46 C45 1.371(10) . C46 H46 0.9300 . C39 C38 1.351(11) . C39 H39 0.9300 . C21 C20 1.368(8) . C21 H21 0.9300 . C30 C31 1.386(9) . C30 H30 0.9300 . C20 H20 0.9300 . C43 C44 1.373(11) . C43 H43 0.9300 . C54 C55 1.393(9) . C54 H54 0.9300 . C56 C55 1.361(11) . C56 H56 0.9300 . C31 H31 0.9300 . C48 C49 1.390(9) . C48 H48 0.9300 . C2 C3 1.338(9) . C2 H2 0.9300 . C33 H33 0.9300 . C28 C27 1.368(10) . C28 H28 0.9300 . C50 C49 1.354(11) . C50 H50 0.9300 . C4 C3 1.379(9) . C4 H4 0.9300 . C45 C44 1.349(11) . C45 H45 0.9300 . C36 C37 1.400(10) . C36 H36 0.9300 . C44 H44 0.9300 . C55 H55 0.9300 . C38 C37 1.381(12) . C38 H38 0.9300 . C24 C25 1.390(10) . C24 H24 0.9300 . C49 H49 0.9300 . C27 C26 1.386(12) . C27 H27 0.9300 . C3 H3 0.9300 . C26 C25 1.339(12) . C26 H26 0.9300 . C25 H25 0.9300 . C37 H37 0.9300 . Cl2 C59 1.670(9) . C59 Cl2 1.670(10) 2 C59 H59A 0.9700 . C59 H59B 0.9700 . Cl3 C60 1.568(18) . Cl3 C60 1.568(18) 2_656 Cl4 C60 1.580(15) . Cl4 C60 1.581(15) 2_656 C60 C60 1.59(3) 2_656 C60 H60 0.9800 .