#------------------------------------------------------------------------------ #$Date: 2019-11-10 18:57:54 +0200 (Sun, 10 Nov 2019) $ #$Revision: 225968 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/58/4515876.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4515876 loop_ _publ_author_name 'Pagliari, Anderson B.' 'Orlando, Tain\'ara' 'Salbego, Paulo R. S.' 'Zimmer, Ge\'orgia C' 'H\"orner, Manfredo' 'Zanatta, Nilo' 'Bonacorso, Helio G.' 'Martins, Marcos A. P.' _publ_section_title ; Supramolecular Packing of a Series of N-Phenylamides and the Role of NH···O=C Interactions. ; _journal_issue 10 _journal_name_full 'ACS omega' _journal_page_first 13850 _journal_page_last 13861 _journal_paper_doi 10.1021/acsomega.8b01801 _journal_volume 3 _journal_year 2018 _chemical_absolute_configuration ad _chemical_formula_moiety 'C8 H6 F3 N O' _chemical_formula_sum 'C8 H6 F3 N O' _chemical_formula_weight 189.14 _chemical_melting_point ? _chemical_name_common 2,2,2-trifluoro-N-phenylacetamide _chemical_name_systematic 2,2,2-trifluoro-N-phenylacetamide _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _symmetry_cell_setting monoclinic _symmetry_Int_Tables_number 4 _symmetry_space_group_name_Hall 'P 2yb' _symmetry_space_group_name_H-M 'P 1 21 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_conform_dict_location ftp://ftp.iucr.org/pub/cif_core.dic _audit_conform_dict_name cif_core.dic _audit_conform_dict_version 2.4.3 _audit_creation_date 2018-04-15T07:34:25-00:00 _audit_creation_method 'WinGX routine CIF_UPDATE' _cell_angle_alpha 90 _cell_angle_beta 90.302(9) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 5.1753(14) _cell_length_b 19.084(4) _cell_length_c 8.2765(18) _cell_measurement_reflns_used 1417 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 24.86 _cell_measurement_theta_min 4.08 _cell_measurement_wavelength 0.71073 _cell_volume 817.4(3) _computing_cell_refinement 'Bruker Saint' _computing_data_collection 'Bruker Apex III' _computing_data_reduction 'Bruker Software' _computing_molecular_graphics 'Ortep-3 (Farrugia,2000' _computing_publication_material 'Shelxl-97 (Sheldrick, 1997)' _computing_structure_refinement 'SHELXL-2016/4 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 100(2) _diffrn_detector_area_resol_mean none _diffrn_measured_fraction_theta_full 0.989 _diffrn_measured_fraction_theta_max 0.979 _diffrn_measurement_device_type 'Bruker D8 Venture Photon 100 diffractometer' _diffrn_measurement_method '2\%\f &\w scans' _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0544 _diffrn_reflns_av_unetI/netI 0.1037 _diffrn_reflns_Laue_measured_fraction_full 0.989 _diffrn_reflns_Laue_measured_fraction_max 0.979 _diffrn_reflns_limit_h_max 6 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_k_min -24 _diffrn_reflns_limit_l_max 10 _diffrn_reflns_limit_l_min -10 _diffrn_reflns_number 3449 _diffrn_reflns_point_group_measured_fraction_full 0.828 _diffrn_reflns_point_group_measured_fraction_max 0.8 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.097 _diffrn_reflns_theta_min 2.461 _diffrn_source 'fine-focus sealed tube' _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.148 _exptl_absorpt_correction_T_max 0.7455 _exptl_absorpt_correction_T_min 0.6748 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details SADABS _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.537 _exptl_crystal_density_meas ? _exptl_crystal_density_method 'not measured' _exptl_crystal_description block _exptl_crystal_F_000 384 _exptl_crystal_size_max 0.283 _exptl_crystal_size_mid 0.276 _exptl_crystal_size_min 0.106 _refine_diff_density_max 0.667 _refine_diff_density_min -0.756 _refine_diff_density_rms 0.245 _refine_ls_abs_structure_details ; Flack x determined using 530 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.0(7) _refine_ls_extinction_coef 0.52(6) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method 'SHELXL-2016/4 (Sheldrick 2016)' _refine_ls_goodness_of_fit_ref 1.052 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_constraints 0 _refine_ls_number_parameters 236 _refine_ls_number_reflns 2899 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.052 _refine_ls_R_factor_all 0.1606 _refine_ls_R_factor_gt 0.0818 _refine_ls_shift/su_max 0 _refine_ls_shift/su_mean 0 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1496P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1846 _refine_ls_wR_factor_ref 0.2344 _reflns_Friedel_coverage 0.586 _reflns_Friedel_fraction_full 0.656 _reflns_Friedel_fraction_max 0.61 _reflns_number_gt 1718 _reflns_number_total 2899 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL mo_MMV0258_0m_a.res in P2(1) shelx.res created by SHELXL-2016/4 at 06:46:57 on 15-Apr-2018 CELL 0.71073 5.1753 19.0838 8.2765 90.000 90.302 90.000 ZERR 4.00 0.0014 0.0044 0.0018 0.000 0.009 0.000 LATT -1 SYMM - X, 1/2 + Y, - Z SFAC C 2.31000 20.84392 1.02000 10.20751 1.58860 0.56870 = 0.86500 51.65125 0.21560 0.003 0.002 11.500 0.770 12.011 SFAC H 0.49300 10.51091 0.32291 26.12573 0.14019 3.14236 = 0.04081 57.79977 0.00304 0.000 0.000 0.620 0.320 1.008 SFAC N 12.21261 0.00570 3.13220 9.89331 2.01250 28.99754 = 1.16630 0.58260 -11.52901 0.006 0.003 19.600 0.700 14.007 SFAC O 3.04850 13.27711 2.28680 5.70111 1.54630 0.32390 = 0.86700 32.90894 0.25080 0.011 0.006 32.500 0.660 15.999 SFAC F 3.53920 10.28251 2.64120 4.29440 1.51700 0.26150 = 1.02430 26.14763 0.27760 0.017 0.010 51.500 0.640 18.998 UNIT 32 24 4 4 12 MERG 2 OMIT 0 -8 0 OMIT 0 -4 0 OMIT 3 2 3 OMIT 1 7 0 OMIT -2 0 2 OMIT -1 3 6 FMAP -2 PLAN 15 ACTA BOND $H WPDB 2 L.S. 20 TEMP -173.00 WGHT 0.149600 EXTI 0.520817 FVAR 1.29024 F3 5 0.059532 0.368943 0.730792 11.00000 0.05818 0.06239 = 0.15657 0.02744 0.01698 -0.00732 O1 4 0.591079 0.471269 0.635022 11.00000 0.02849 0.05298 = 0.17292 0.02331 0.00640 -0.00034 C7 1 0.366342 0.455804 0.650223 11.00000 0.03277 0.03915 = 0.07205 0.00001 0.00570 -0.00021 F1' 5 0.440352 -0.132390 0.765576 11.00000 0.06317 0.06316 = 0.15917 -0.03351 0.01708 0.00671 F1 5 0.428029 0.368347 0.842408 11.00000 0.15474 0.09677 = 0.13315 0.05285 -0.06280 -0.02628 C8 1 0.308404 0.381116 0.708093 11.00000 0.04771 0.04634 = 0.07082 0.00895 0.00019 0.00556 F2 5 0.378922 0.334340 0.603095 11.00000 0.13896 0.04824 = 0.16025 -0.01325 0.05342 0.00168 F2' 5 0.125680 -0.167666 0.895579 11.00000 0.15272 0.04137 = 0.18187 0.00944 0.06937 0.00009 F3' 5 0.067071 -0.132259 0.659083 11.00000 0.15597 0.10969 = 0.15452 -0.06809 -0.06493 0.03761 MOLE 1 C6 1 0.362348 0.613322 0.629948 11.00000 0.03621 0.04462 = 0.05865 -0.00014 -0.00694 -0.00042 AFIX 43 H6 2 0.493038 0.597033 0.701698 11.00000 -1.20000 AFIX 0 C1 1 0.170248 0.567558 0.572637 11.00000 0.03182 0.03822 = 0.04554 -0.00058 0.01009 0.00093 C3 1 -0.021104 0.662126 0.423855 11.00000 0.05056 0.05356 = 0.05723 0.01051 -0.00088 0.00731 AFIX 43 H3 2 -0.154236 0.678888 0.354487 11.00000 -1.20000 AFIX 0 C5 1 0.358216 0.682303 0.580383 11.00000 0.04731 0.03976 = 0.06961 -0.00405 0.00396 -0.00830 AFIX 43 H5 2 0.489018 0.713396 0.617495 11.00000 -1.20000 AFIX 0 C2 1 -0.016881 0.592433 0.470691 11.00000 0.03879 0.04996 = 0.04758 -0.00249 0.00088 -0.00092 AFIX 43 H2 2 -0.146248 0.561429 0.431263 11.00000 -1.20000 AFIX 0 C4 1 0.168613 0.706950 0.478365 11.00000 0.04784 0.04004 = 0.05785 0.00400 0.00729 0.00255 AFIX 43 H4 2 0.168475 0.754664 0.445637 11.00000 -1.20000 AFIX 0 N1 3 0.162293 0.496194 0.623202 11.00000 0.03108 0.03474 = 0.05536 0.00027 0.00574 -0.00402 AFIX 43 H1 2 0.008949 0.477361 0.637704 11.00000 -1.20000 AFIX 0 MOLE 2 C2' 1 0.519345 0.110533 0.872740 11.00000 0.03663 0.04581 = 0.06013 0.00537 0.00454 -0.00081 AFIX 43 H2' 2 0.649634 0.093447 0.802558 11.00000 -1.20000 AFIX 0 C5' 1 0.138925 0.161498 1.074192 11.00000 0.04376 0.05437 = 0.05335 -0.00879 0.00449 0.00699 AFIX 43 H5' 2 0.008524 0.179272 1.143382 11.00000 -1.20000 AFIX 0 C3' 1 0.519233 0.180183 0.918923 11.00000 0.04421 0.04710 = 0.06688 0.00596 0.00093 -0.00709 AFIX 43 H3' 2 0.651648 0.210638 0.882097 11.00000 -1.20000 AFIX 0 C1' 1 0.328647 0.065513 0.929080 11.00000 0.02746 0.03752 = 0.04439 0.00122 -0.00461 0.00311 C6' 1 0.135738 0.091296 1.031204 11.00000 0.03742 0.04842 = 0.04958 -0.00013 0.00747 -0.00291 AFIX 43 H6' 2 0.004445 0.061068 1.070490 11.00000 -1.20000 AFIX 0 O1' 4 -0.093382 -0.031297 0.870845 11.00000 0.03098 0.05012 = 0.15177 -0.02248 -0.00093 0.00037 C4' 1 0.327288 0.205660 1.018421 11.00000 0.05250 0.04218 = 0.06091 -0.00143 -0.00637 0.00403 AFIX 43 H4' 2 0.325910 0.253742 1.048133 11.00000 -1.20000 AFIX 0 N1' 3 0.336611 -0.005661 0.879713 11.00000 0.02883 0.03892 = 0.05564 0.00014 0.00314 0.00207 AFIX 43 H1' 2 0.489955 -0.024428 0.864778 11.00000 -1.20000 AFIX 0 C7' 1 0.133213 -0.046162 0.854258 11.00000 0.03637 0.03745 = 0.06796 0.00441 0.00162 0.00089 C8' 1 0.193848 -0.120115 0.793208 11.00000 0.04772 0.04262 = 0.07186 -0.00941 -0.00055 -0.00415 HKLF 4 REM mo_MMV0258_0m_a.res in P2(1) REM R1 = 0.0818 for 1718 Fo > 4sig(Fo) and 0.1606 for all 2899 data REM 236 parameters refined using 1 restraints END WGHT 0.1491 0.0000 REM Highest difference peak 0.667, deepest hole -0.756, 1-sigma level 0.245 Q1 1 0.0420 -0.1411 1.0159 11.00000 0.05 -0.76 Q2 1 0.4392 0.3516 0.4347 11.00000 0.05 -0.75 Q3 1 0.6415 0.1688 0.7493 11.00000 0.05 -0.69 Q4 1 0.6770 0.2718 0.9883 11.00000 0.05 0.67 Q5 1 0.5634 0.3824 0.6384 11.00000 0.05 -0.66 Q6 1 0.7304 -0.1373 0.9141 11.00000 0.05 -0.66 Q7 1 -0.0712 -0.1261 0.8759 11.00000 0.05 -0.65 Q8 1 -0.1489 0.3474 0.8043 11.00000 0.05 -0.64 Q9 1 -0.1111 -0.2234 0.6109 11.00000 0.05 0.64 Q10 1 0.1822 -0.0326 0.8573 11.00000 0.05 0.63 Q11 1 0.3130 -0.2232 0.8668 11.00000 0.05 0.63 Q12 1 0.0537 -0.0387 0.8430 11.00000 0.05 0.63 Q13 1 0.7296 0.3776 0.5868 11.00000 0.05 -0.62 Q14 1 0.1033 0.1631 1.2412 11.00000 0.05 -0.61 Q15 1 0.1222 0.5713 0.5110 11.00000 0.05 0.61 ; _cod_data_source_file ao8b01801_si_005.cif _cod_data_source_block shelx _cod_depositor_comments ; The following automatic conversions were performed: data item '_chemical_melting_point' value 'none' was changed to '?' -- the value is undefined or not given. data item '_exptl_crystal_density_meas' value 'none' was changed to '?' -- the value is perceived as not measured. Automatic conversion script Id: cif_fix_values 6909 2019-04-08 15:41:33Z antanas ; _cod_original_sg_symbol_H-M 'P 21' _cod_database_code 4515876 _shelx_estimated_absorpt_t_min none _shelx_estimated_absorpt_t_max none _iucr_refine_reflections_details ; 1 0 0 -0.80 3.20 -1 0 0 -4.90 9.00 3 0 0 3.20 16.60 -3 0 0 3.20 21.10 5 0 0 2.10 2.40 6 0 0 198.58 9.10 1 -1 0 8.70 0.60 -2 -1 0 62.39 15.70 -2 1 0 94.39 18.30 -3 -1 0 -9.00 20.20 3 -1 0 -1.50 11.00 -3 1 0 -7.70 16.20 3 1 0 4.90 18.70 4 -1 0 355.26 11.80 5 -1 0 2.20 2.60 6 -1 0 4.60 3.50 6 1 0 10.10 3.60 1 -2 0 78.99 2.70 -1 2 0 79.29 2.70 2 -2 0 150.28 5.10 3 -2 0 0.90 1.20 4 -2 0 233.18 8.30 5 -2 0 -0.40 2.80 6 -2 0 131.99 7.80 6 2 0 129.69 8.10 0 -3 0 0.00 0.50 0 3 0 0.50 0.50 1 -3 0 48.50 1.80 -1 3 0 47.80 1.80 -2 -3 0 1533.65 64.49 3 -3 0 14.50 1.60 4 -3 0 289.27 10.00 5 -3 0 2.60 2.50 6 -3 0 3.10 4.20 0 -4 0 -0.10 4.00 0 4 0 3.50 4.10 1 -4 0 101.89 3.50 -1 4 0 101.69 3.40 2 -4 0 1428.16 43.40 3 -4 0 0.20 1.30 4 -4 0 189.48 7.10 5 -4 0 -3.50 2.70 6 -4 0 3.70 4.20 0 5 0 5.60 0.90 1 -5 0 6.80 0.80 -1 5 0 7.70 0.80 2 -5 0 1227.28 37.50 -2 5 0 1236.48 37.50 3 -5 0 1.80 1.40 4 -5 0 146.29 6.10 5 -5 0 -0.40 2.80 6 -5 0 -0.70 4.10 0 -6 0 1.50 6.10 1 -6 0 19.90 1.50 -1 6 0 18.90 1.40 2 -6 0 278.97 8.90 -2 6 0 270.37 8.90 3 -6 0 0.60 1.20 4 -6 0 138.39 5.80 5 -6 0 3.30 3.00 6 -6 0 28.00 4.90 0 -7 0 8.10 3.90 0 -7 0 -2.90 6.40 1 -7 0 6.60 1.10 -1 7 0 1.20 0.90 1 7 0 0.70 1.70 2 -7 0 20.30 1.90 -2 7 0 19.30 1.50 3 -7 0 1.60 1.50 4 -7 0 94.69 5.00 5 -7 0 -0.40 2.70 6 -7 0 6.00 5.00 0 -8 0 -0.40 7.30 1 -8 0 111.19 4.20 1 8 0 108.79 5.00 -1 8 0 106.49 4.00 2 -8 0 364.66 11.80 -2 8 0 367.46 11.70 3 -8 0 2.40 1.60 -3 8 0 1.00 1.30 4 -8 0 212.58 8.10 5 -8 0 -0.70 3.20 6 -8 0 4.40 5.80 0 -9 0 1.50 1.70 0 9 0 2.20 1.40 1 -9 0 69.59 3.20 -1 9 0 68.59 3.00 1 9 0 61.69 4.00 2 -9 0 835.32 25.70 -2 9 0 817.12 25.50 3 -9 0 3.80 1.80 -3 9 0 4.50 1.50 4 -9 0 27.80 3.00 5 -9 0 -4.40 3.30 6 -9 0 15.00 6.10 0 -10 0 5705.63 172.28 1 -10 0 156.78 5.80 1 10 0 152.98 6.30 -1 10 0 158.08 5.60 2 -10 0 357.26 11.90 -2 10 0 364.96 11.70 3 -10 0 1.70 1.80 4 -10 0 26.80 3.20 5 -10 0 -3.40 3.50 6 -10 0 44.20 6.30 0 -11 0 0.40 10.70 0 -11 0 16.80 7.80 1 -11 0 87.89 4.10 -1 11 0 82.29 3.80 1 11 0 87.79 4.80 2 -11 0 358.46 12.10 -2 11 0 370.46 11.90 3 -11 0 21.70 2.60 -3 11 0 20.30 2.20 4 -11 0 127.29 7.50 5 -11 0 5.20 3.90 0 -12 0 191.88 8.00 0 12 0 200.78 7.20 1 -12 0 227.38 8.40 -1 12 0 228.38 8.00 1 12 0 240.48 8.90 2 -12 0 265.17 9.40 2 12 0 266.77 11.00 -2 12 0 263.17 9.00 3 -12 0 -2.40 2.50 -3 12 0 1.30 1.70 4 -12 0 26.90 3.50 5 -12 0 6.30 4.40 0 -13 0 22.00 3.20 0 13 0 13.60 2.10 1 -13 0 73.69 4.40 1 13 0 63.59 4.70 -1 13 0 65.19 3.70 2 -13 0 459.35 15.60 2 13 0 477.55 16.70 -2 13 0 471.95 15.30 3 -13 0 39.90 3.40 3 13 0 33.30 5.20 -3 13 0 36.10 3.40 4 -13 0 233.78 9.70 5 -13 0 6.50 5.30 0 -14 0 97.39 6.10 0 14 0 87.19 4.70 1 -14 0 230.38 8.90 1 14 0 228.88 8.80 -1 14 0 224.38 8.30 2 -14 0 125.99 6.20 -2 14 0 134.39 5.50 2 14 0 123.59 7.10 3 -14 0 1.50 2.70 -3 14 0 3.90 2.30 3 14 0 4.70 5.40 4 -14 0 6.30 3.60 5 -14 0 7.90 5.30 0 -15 0 9.30 3.60 0 15 0 12.30 2.40 1 -15 0 44.00 3.90 1 15 0 41.00 3.80 -1 15 0 39.90 3.60 2 -15 0 659.43 21.50 -2 15 0 661.43 21.10 2 15 0 652.13 22.40 -3 15 0 19.40 2.70 3 15 0 25.30 5.30 4 -15 0 55.99 5.10 4 15 0 54.19 10.80 -4 15 0 57.79 5.20 5 -15 0 -2.70 5.90 0 -16 0 68.69 6.50 0 16 0 55.59 4.60 1 -16 0 129.79 7.20 -1 16 0 132.49 6.00 1 16 0 131.59 6.90 2 -16 0 219.78 9.30 -2 16 0 205.88 8.30 2 16 0 215.38 10.30 3 -16 0 1.40 3.50 3 16 0 1.60 5.90 -3 16 0 0.60 2.60 4 -16 0 23.10 4.80 -4 16 0 18.30 3.80 5 -16 0 1.30 6.00 0 -17 0 11.10 4.40 0 17 0 5.20 2.70 1 -17 0 21.30 4.10 -1 17 0 23.10 3.00 1 17 0 23.50 3.50 2 -17 0 122.89 8.00 -2 17 0 120.09 6.10 2 17 0 129.39 7.90 3 -17 0 16.90 4.10 -3 17 0 17.60 3.30 3 17 0 23.20 6.80 4 -17 0 5.00 5.10 -4 17 0 1.60 4.10 0 18 0 130.59 7.00 1 18 0 49.70 4.60 -1 18 0 36.40 3.60 2 -18 0 32.60 5.10 -2 18 0 40.60 3.70 2 18 0 37.20 5.70 3 -18 0 -3.60 4.30 -3 18 0 3.70 3.20 3 18 0 6.70 6.90 4 -18 0 13.30 6.10 -4 18 0 12.80 4.20 0 19 0 4.00 3.40 1 -19 0 9.00 4.70 1 19 0 20.00 4.20 -1 19 0 12.30 3.20 2 -19 0 26.70 5.60 2 19 0 28.50 5.80 -2 19 0 30.60 3.80 3 -19 0 4.10 5.10 -3 19 0 4.00 3.70 4 -19 0 56.09 7.80 0 20 0 55.29 5.00 1 -20 0 4.80 5.70 -1 20 0 7.10 4.00 1 20 0 0.70 4.40 2 -20 0 15.70 6.20 2 20 0 20.80 6.10 -2 20 0 12.90 3.80 3 -20 0 4.60 6.30 -3 20 0 0.70 4.50 0 21 0 14.80 5.00 1 -21 0 4.40 7.40 1 21 0 3.00 5.20 -1 21 0 5.80 4.00 2 -21 0 17.60 6.80 -2 21 0 17.70 4.30 3 -21 0 -3.40 6.40 -3 21 0 11.40 6.30 0 22 0 71.29 6.30 1 -22 0 2.30 8.40 1 22 0 4.50 5.70 -1 22 0 4.80 4.60 2 -22 0 0.10 6.80 -2 22 0 11.20 5.30 0 -23 0 -45.40 49.30 1 -23 0 22.20 8.80 -1 23 0 -1.30 5.70 2 -23 0 47.30 9.70 6 0 -1 13.40 3.80 5 0 -1 184.08 7.90 4 0 -1 35.40 2.90 2 0 -1 3.30 6.30 1 0 -1 9999.00 306.97 0 0 -1 1.20 0.20 0 0 1 0.90 0.20 1 0 1 1341.27 49.30 -1 0 -1 1308.87 46.10 -2 0 -1 115.79 21.20 -3 0 -1 15.20 26.30 3 0 1 1.10 17.60 -4 0 -1 -6.20 30.00 4 0 1 21.20 31.90 6 0 1 16.90 4.00 6 -1 -1 0.10 3.40 6 1 -1 -5.60 3.90 5 -1 -1 916.01 29.10 5 1 -1 913.91 29.00 4 -1 -1 71.29 3.70 3 -1 -1 316.27 10.40 2 -1 -1 178.48 5.90 1 -1 -1 6368.26 196.08 -1 -1 1 6333.37 197.68 0 -1 -1 3.20 0.40 0 1 1 2.80 0.40 -1 -1 -1 1121.79 44.60 1 -1 1 1117.89 39.50 2 -1 1 45.40 11.00 -2 -1 -1 46.40 9.90 2 1 1 25.30 15.90 3 -1 1 11.90 15.60 -3 -1 -1 49.90 28.40 -3 1 -1 45.50 24.70 3 1 1 58.09 26.50 -4 -1 -1 107.59 39.60 4 -1 1 33.00 28.30 -4 1 -1 79.89 36.40 4 1 1 0.90 31.20 5 -1 1 195.48 8.00 6 -1 1 5.30 3.90 6 1 1 3.00 4.00 6 -2 -1 7.00 3.90 6 2 -1 17.20 4.20 5 -2 -1 24.40 3.20 4 -2 -1 27.10 2.40 3 -2 -1 730.13 22.80 2 -2 -1 48.70 2.30 1 -2 -1 366.56 11.30 -1 2 1 364.06 11.30 0 -2 -1 2.30 0.50 0 2 1 2.50 0.40 -2 -2 -1 13.00 11.00 2 -2 1 13.00 9.00 2 2 1 -11.60 13.10 3 -2 1 137.89 22.10 -3 -2 -1 116.19 19.10 4 -2 1 16.00 2.00 5 -2 1 432.66 14.70 6 -2 1 18.80 4.20 6 -3 -1 -4.20 4.30 6 3 -1 -6.80 4.10 5 -3 -1 79.69 5.60 4 -3 -1 59.49 3.90 3 -3 -1 650.03 20.40 2 -3 -1 187.48 6.30 1 -3 -1 1029.80 31.80 -1 3 1 1067.89 31.80 0 -3 -1 3.60 0.70 0 3 1 4.20 0.60 0 3 -1 4.10 0.60 2 -3 1 93.19 3.40 3 -3 1 768.02 23.70 4 -3 1 71.59 3.90 5 -3 1 141.29 6.60 6 -3 1 5.40 4.00 6 -4 -1 8.00 4.60 6 4 -1 14.70 4.10 5 -4 -1 40.10 3.90 4 -4 -1 16.80 2.20 3 -4 -1 3205.18 96.99 2 -4 -1 66.69 2.90 -2 4 1 70.09 2.90 -1 4 1 2982.60 89.89 0 -4 -1 0.30 0.80 0 4 -1 0.60 0.60 0 4 1 0.80 0.70 1 -4 1 822.62 24.90 -1 4 -1 820.72 24.90 2 -4 1 89.19 3.30 3 -4 1 364.66 11.70 4 -4 1 21.00 2.20 5 -4 1 141.19 6.70 6 -4 1 11.70 4.30 6 -5 -1 7.40 4.20 5 -5 -1 192.08 8.00 4 -5 -1 25.80 2.60 3 -5 -1 257.67 8.80 2 -5 -1 65.19 3.00 -2 5 1 67.09 2.90 1 -5 -1 1422.36 43.10 -1 5 1 1413.56 43.00 0 -5 -1 0.50 0.90 0 5 -1 0.60 0.70 0 5 1 -0.50 0.70 1 -5 1 1118.39 34.10 1 5 1 1133.69 34.70 -1 5 -1 1127.59 34.10 2 -5 1 76.29 3.00 3 -5 1 146.59 5.40 4 -5 1 29.70 2.60 5 -5 1 25.40 3.20 6 -5 1 1.10 4.10 6 -6 -1 2.20 4.90 5 -6 -1 10.50 3.40 4 -6 -1 17.70 2.50 3 -6 -1 154.78 5.90 2 -6 -1 17.50 1.60 -2 6 1 19.90 1.80 1 -6 -1 4394.36 136.99 -1 6 1 4264.97 135.19 0 -6 1 5.30 1.20 0 -6 -1 5.10 1.10 0 6 1 5.30 1.00 0 6 -1 6.10 0.90 1 -6 1 678.03 21.10 1 6 1 693.33 21.80 -1 6 -1 702.93 21.10 2 -6 1 28.40 1.90 -2 6 -1 25.90 1.80 3 -6 1 1418.46 43.30 4 -6 1 14.00 2.10 5 -6 1 170.28 7.50 6 -6 1 -1.20 4.50 6 -7 -1 -1.00 5.00 5 -7 -1 169.78 8.10 4 -7 -1 7.50 2.40 3 -7 -1 1.20 1.60 -3 7 1 6.30 1.50 2 -7 -1 11.60 1.40 -2 7 1 11.20 1.30 1 -7 -1 1602.04 48.90 -1 7 1 1613.14 48.80 0 -7 1 8.90 1.40 0 -7 -1 8.40 1.40 0 7 1 8.10 1.30 0 7 -1 9.60 1.20 1 -7 1 521.95 16.20 1 7 1 512.75 16.70 -1 7 -1 529.55 16.10 2 -7 1 9.80 1.20 -2 7 -1 9.20 1.00 3 -7 1 15.90 1.80 4 -7 1 9.80 2.10 5 -7 1 41.20 3.70 6 -7 1 -0.10 4.50 6 -8 -1 -8.80 5.20 5 -8 -1 27.50 4.00 4 -8 -1 -10.90 46.30 -4 -8 1 10.30 20.90 4 8 -1 -1.70 23.30 -4 8 1 0.50 17.60 3 -8 -1 55.49 3.30 2 -8 -1 -0.70 1.30 -2 8 1 -0.70 1.00 1 -8 -1 1272.37 39.00 1 8 -1 1288.97 39.50 -1 8 1 1265.57 38.90 0 -8 -1 9.60 1.80 0 -8 1 12.70 1.80 0 8 1 12.60 1.50 0 8 -1 12.30 1.40 1 -8 1 550.64 17.20 1 8 1 543.65 17.80 -1 8 -1 565.54 17.10 2 -8 1 4.60 1.20 -2 8 -1 5.00 1.10 3 -8 1 75.69 3.70 4 -8 1 -0.50 2.00 5 -8 1 186.48 8.20 6 -8 1 6.50 4.80 6 -9 -1 0.50 5.60 5 -9 -1 155.78 8.10 4 -9 -1 9.50 2.80 3 -9 -1 210.68 7.90 -3 9 1 218.68 7.70 2 -9 -1 2.20 1.30 -2 9 1 0.20 1.10 1 -9 -1 1544.35 47.40 -1 9 1 1545.65 47.30 1 9 -1 1564.74 47.80 0 -9 1 17.20 2.00 0 -9 -1 16.20 2.10 0 9 -1 15.00 1.50 0 9 1 14.90 1.60 1 -9 1 220.08 7.50 1 9 1 216.48 8.10 -1 9 -1 228.78 7.30 2 -9 1 1.30 1.20 -2 9 -1 1.30 1.10 2 9 1 2.40 2.40 3 -9 1 12.40 2.00 4 -9 1 -1.00 2.20 5 -9 1 29.90 3.80 6 -9 1 2.90 4.90 6 -10 -1 2.40 6.00 5 -10 -1 50.39 4.60 4 -10 -1 16.80 3.00 3 -10 -1 204.38 7.80 -3 10 1 201.88 7.30 2 -10 -1 7.90 1.90 -2 10 1 5.90 1.50 1 -10 -1 989.50 30.50 -1 10 1 993.60 30.30 1 10 -1 963.40 30.70 0 -10 1 3.00 1.90 0 -10 -1 2.80 1.90 0 10 -1 3.40 1.40 0 10 1 3.60 1.50 1 -10 1 359.16 11.70 1 10 1 361.76 12.30 -1 10 -1 358.46 11.50 2 -10 1 16.00 1.90 2 10 1 18.60 3.40 -2 10 -1 17.00 1.60 3 -10 1 21.10 2.40 -3 10 -1 23.20 2.00 4 -10 1 15.50 2.60 5 -10 1 43.50 4.20 6 -10 1 5.80 5.90 5 -11 -1 32.70 4.80 4 -11 -1 9.90 3.10 3 -11 -1 233.78 8.90 -3 11 1 234.88 8.40 2 -11 -1 35.00 3.30 -2 11 1 31.40 2.80 1 -11 -1 278.77 9.60 1 11 -1 273.97 9.90 -1 11 1 276.17 9.30 0 -11 1 -2.00 2.10 0 -11 -1 0.30 2.10 0 11 -1 2.50 1.40 0 11 1 2.30 1.70 1 -11 1 503.05 16.40 -1 11 -1 519.15 16.10 1 11 1 515.45 16.90 2 -11 1 31.00 3.00 -2 11 -1 30.50 2.30 2 11 1 33.30 3.40 3 -11 1 153.08 6.10 3 11 1 151.48 8.50 -3 11 -1 151.88 5.80 4 -11 1 13.90 3.10 5 -11 1 17.00 4.30 5 -12 -1 1.20 4.40 4 -12 -1 34.30 4.00 3 -12 -1 613.34 19.90 -3 12 1 613.84 19.60 2 -12 -1 73.99 4.30 -2 12 1 66.69 4.30 2 12 -1 67.69 6.10 1 -12 -1 77.59 4.40 1 12 -1 67.49 4.50 -1 12 1 77.89 3.90 0 -12 -1 -1.60 2.20 0 -12 1 6.40 2.40 0 12 -1 0.70 1.40 0 12 1 0.90 1.80 1 -12 1 28.40 2.50 -1 12 -1 25.40 2.30 1 12 1 26.40 2.90 2 -12 1 20.80 2.50 2 12 1 23.20 3.60 -2 12 -1 24.80 2.40 3 -12 1 52.99 4.10 4 -12 1 39.00 3.60 5 -12 1 13.50 4.10 5 -13 -1 3.10 4.90 4 -13 -1 39.50 4.40 -4 13 1 30.20 3.40 3 -13 -1 666.53 22.00 -3 13 1 674.63 21.50 2 -13 -1 54.59 4.30 -2 13 1 46.10 3.50 2 13 -1 44.30 4.60 1 -13 -1 312.07 11.10 1 13 -1 321.27 11.30 -1 13 1 315.37 10.90 0 -13 -1 6.20 2.70 0 13 1 -1.30 1.90 0 13 -1 1.60 1.70 1 -13 1 276.57 10.20 1 13 1 290.27 10.50 -1 13 -1 285.37 9.60 2 -13 1 48.60 3.70 2 13 1 64.99 5.80 -2 13 -1 49.10 3.30 3 -13 1 333.27 11.70 -3 13 -1 338.87 11.30 -4 -13 -1 16.20 52.19 4 -13 1 51.29 60.59 4 13 1 0.00 33.40 -4 13 -1 11.10 20.70 5 -13 1 21.20 4.50 5 -14 -1 3.80 5.60 4 -14 -1 49.00 4.90 -4 14 1 49.30 4.10 3 -14 -1 532.25 17.90 3 14 -1 504.75 20.10 -3 14 1 539.75 17.40 2 -14 -1 72.59 5.10 -2 14 1 75.59 4.40 2 14 -1 77.19 6.40 1 -14 -1 476.75 16.50 -1 14 1 508.45 16.20 1 14 -1 490.85 16.70 0 -14 -1 5.90 3.00 0 14 -1 3.40 2.10 0 14 1 3.90 2.30 1 -14 1 190.58 7.70 1 14 1 184.68 8.10 -1 14 -1 194.98 7.10 2 -14 1 19.30 2.70 2 14 1 20.90 4.10 -2 14 -1 24.20 2.30 3 -14 1 720.43 23.70 -3 14 -1 751.12 23.30 4 -14 1 79.99 5.90 4 14 1 80.19 9.20 5 -14 1 39.50 5.20 5 -15 -1 19.90 6.30 4 -15 -1 42.30 5.00 -4 15 1 44.80 4.30 3 -15 -1 34.50 4.10 -3 15 1 32.80 3.30 3 15 -1 28.50 6.40 2 -15 -1 35.30 3.80 -2 15 1 31.40 3.00 2 15 -1 31.60 4.50 1 -15 -1 112.09 6.60 1 15 -1 123.79 6.20 -1 15 1 109.79 5.30 0 -15 -1 1.60 3.70 0 15 -1 0.80 2.30 0 15 1 0.60 2.20 1 -15 1 510.25 17.30 1 15 1 516.65 17.60 -1 15 -1 520.65 16.70 2 -15 1 65.09 5.00 2 15 1 71.89 6.10 3 -15 1 52.19 4.90 3 15 1 43.80 6.50 -3 15 -1 46.50 4.00 4 -15 1 16.50 4.20 5 -15 1 19.30 5.10 4 -16 -1 35.50 5.50 -4 16 1 41.20 4.50 3 -16 -1 39.80 5.00 3 16 -1 31.20 6.80 -3 16 1 38.90 3.70 -2 16 1 36.00 3.40 2 16 -1 49.30 4.90 1 -16 -1 643.74 22.00 -1 16 1 662.73 21.40 1 16 -1 675.33 21.80 0 -16 -1 5.50 4.20 0 16 1 -5.00 2.50 0 16 -1 -4.40 2.40 1 -16 1 127.89 6.70 1 16 1 134.59 6.70 -1 16 -1 111.29 6.60 2 -16 1 37.70 3.80 2 16 1 43.20 5.20 -2 16 -1 38.20 3.70 3 -16 1 169.28 8.00 3 16 1 177.48 11.50 -3 16 -1 176.18 7.10 4 -16 1 52.39 5.40 4 -17 -1 12.90 5.60 -4 17 1 8.70 4.90 3 -17 -1 8.90 4.20 -3 17 1 2.50 3.20 3 17 -1 3.20 6.50 2 -17 -1 6.90 3.90 2 17 -1 5.20 4.50 -2 17 1 11.90 2.90 1 17 -1 230.48 9.60 -1 17 1 230.68 9.20 0 17 1 3.90 2.60 0 17 -1 0.30 2.70 1 -17 1 118.39 7.60 -1 17 -1 118.59 5.60 1 17 1 124.19 7.30 2 -17 1 24.10 4.10 2 17 1 17.50 4.70 -2 17 -1 22.50 2.90 3 -17 1 66.49 6.50 -3 17 -1 54.79 4.50 3 17 1 65.59 7.80 4 -17 1 6.40 5.00 4 -18 -1 26.30 7.20 3 -18 -1 3.60 4.60 -3 18 1 3.00 3.70 3 18 -1 -10.70 6.50 2 -18 -1 33.50 4.90 2 18 -1 35.20 5.40 -2 18 1 35.30 3.70 1 -18 -1 103.69 7.90 -1 18 1 106.39 6.20 1 18 -1 99.09 7.00 0 -18 -1 9.60 4.50 0 18 -1 2.60 2.80 0 18 1 -2.30 3.10 1 -18 1 129.99 8.80 -1 18 -1 120.49 6.10 1 18 1 110.09 7.00 2 -18 1 11.80 4.30 2 18 1 -1.90 4.90 -2 18 -1 9.10 2.50 3 -18 1 -1.10 4.40 -3 18 -1 0.90 3.30 4 -18 1 22.00 5.10 4 -19 -1 0.50 6.80 3 -19 -1 49.40 6.90 -3 19 1 44.90 5.10 2 -19 -1 7.60 4.80 -2 19 1 4.40 3.40 2 19 -1 8.50 5.20 1 -19 -1 99.89 8.90 -1 19 1 109.59 6.70 1 19 -1 100.59 8.00 0 -19 -1 -0.60 5.50 0 19 1 0.90 3.60 0 19 -1 2.10 3.20 1 -19 1 47.70 6.30 1 19 1 41.10 5.10 -1 19 -1 54.39 4.20 2 -19 1 8.70 5.10 2 19 1 18.70 5.70 -2 19 -1 10.20 3.30 3 -19 1 -2.60 5.10 -3 19 -1 8.50 3.70 4 -19 1 5.50 6.40 -4 19 -1 4.60 4.40 2 -20 -1 -9.10 5.30 2 20 -1 13.50 6.10 -2 20 1 0.60 4.10 1 -20 -1 2.10 5.80 -1 20 1 11.00 4.00 1 20 -1 4.40 4.10 0 20 1 -3.80 3.80 0 20 -1 0.20 3.50 1 -20 1 27.40 6.10 -1 20 -1 37.10 4.30 1 20 1 39.80 5.60 2 -20 1 6.70 5.40 -2 20 -1 -2.20 3.10 3 -20 1 42.40 6.60 -3 20 -1 44.00 4.80 3 -21 -1 39.40 7.80 2 -21 -1 -5.70 7.10 2 21 -1 4.90 6.40 -2 21 1 1.40 4.40 1 -21 -1 19.00 6.60 1 21 -1 21.40 5.20 -1 21 1 26.10 5.00 0 21 1 11.00 4.90 0 21 -1 -2.80 3.80 1 -21 1 14.60 6.20 -1 21 -1 -3.30 3.50 1 21 1 1.50 5.30 2 -21 1 -1.90 6.00 -2 21 -1 -2.90 4.10 3 -21 1 4.50 6.80 -3 21 -1 7.60 4.70 2 -22 -1 2.70 7.40 1 -22 -1 11.10 8.10 1 22 -1 4.10 6.00 0 22 1 -4.30 6.10 0 22 -1 -0.90 4.40 -1 22 -1 37.90 5.10 2 -22 1 1.10 7.00 -2 22 -1 2.30 4.80 2 -23 -1 0.80 9.80 1 -23 -1 15.00 9.40 0 23 -1 -3.70 5.00 -1 23 -1 49.40 6.00 2 -23 1 -10.50 8.90 -2 23 -1 6.10 5.50 1 -24 -1 41.90 11.30 6 0 -2 85.39 6.80 5 0 -2 2.30 2.90 4 0 -2 -2.00 1.60 3 0 -2 123.49 4.90 2 0 -2 6.90 1.00 -1 0 2 2193.88 66.49 1 0 -2 2218.58 66.49 0 0 -2 314.07 9.70 0 0 2 318.27 9.70 1 0 2 24.60 12.10 -1 0 -2 39.00 10.10 -2 0 -2 502.65 27.20 2 0 2 421.36 36.90 3 0 2 51.79 27.60 -3 0 -2 129.99 36.60 4 0 2 17.80 35.30 -4 0 -2 140.39 43.40 5 0 2 13.90 59.89 -5 0 -2 17.00 46.40 6 0 2 36.60 4.40 6 -1 -2 21.70 4.90 6 1 -2 19.50 4.70 5 -1 -2 13.40 2.60 5 1 -2 9.90 3.10 4 -1 -2 26.90 2.70 4 1 -2 32.20 2.70 3 -1 -2 8.90 1.40 3 1 -2 11.00 1.50 2 -1 -2 37.50 2.20 2 1 -2 36.80 2.00 1 -1 -2 1540.55 49.50 -1 1 2 1651.33 49.50 1 1 -2 1727.23 49.50 1 -1 2 1211.88 49.10 -1 -1 -2 1134.79 51.99 -1 1 -2 1399.56 46.80 -2 -1 -2 123.89 16.60 2 -1 2 123.39 19.80 -3 -1 -2 10.30 18.80 3 -1 2 9.40 20.80 3 1 2 -12.50 23.00 -3 1 -2 10.10 27.50 5 -1 2 1.40 2.30 6 -1 2 32.60 4.50 6 -2 -2 10.60 4.70 6 2 -2 7.40 3.80 5 -2 -2 3.40 2.90 5 2 -2 1.60 2.80 4 -2 -2 185.08 7.20 4 2 -2 185.18 6.90 3 -2 -2 101.29 4.30 2 -2 -2 2512.65 75.99 1 -2 -2 1728.53 53.09 -1 2 2 1784.62 53.09 1 2 2 303.07 9.90 -2 -2 -2 377.66 28.40 2 -2 2 385.86 26.10 3 -2 2 27.10 18.10 -3 -2 -2 15.30 12.70 3 2 2 3.70 22.60 -3 2 -2 74.19 28.90 -4 -2 -2 163.98 52.49 -4 2 -2 249.78 43.90 5 -2 2 7.60 2.50 6 -2 2 35.70 4.60 6 -3 -2 19.00 4.80 6 3 -2 14.50 3.80 5 -3 -2 2.90 3.00 5 3 -2 11.70 3.10 4 -3 -2 385.46 12.90 3 -3 -2 12.00 1.70 2 -3 -2 295.57 9.40 -2 3 2 283.87 9.30 1 -3 -2 997.90 31.40 -1 3 2 1064.59 31.40 0 -3 -2 1632.14 49.70 0 3 2 1652.03 49.70 1 -3 2 1814.62 56.39 1 3 2 1938.91 56.99 2 -3 2 320.47 10.00 3 -3 2 28.90 2.10 4 -3 2 126.39 5.20 5 -3 2 3.70 2.40 6 -3 2 12.20 3.90 6 -4 -2 3.90 4.60 6 4 -2 4.60 3.80 5 -4 -2 2.20 2.90 4 -4 -2 168.98 6.70 3 -4 -2 46.50 3.10 2 -4 -2 630.84 19.70 -2 4 2 632.14 19.60 1 -4 -2 685.03 21.40 -1 4 2 702.63 21.30 0 -4 -2 1456.55 44.90 0 4 2 1500.25 44.90 1 -4 2 346.97 10.90 1 4 2 372.76 11.60 2 -4 2 271.87 8.60 3 -4 2 47.40 2.50 4 -4 2 138.59 5.50 5 -4 2 0.30 2.30 6 -4 2 3.40 4.40 6 -5 -2 9.00 4.90 6 5 -2 8.50 4.10 5 -5 -2 1.90 3.20 4 -5 -2 359.76 68.99 -4 -5 2 433.66 55.39 -4 5 2 445.36 32.40 3 -5 -2 19.40 2.00 2 -5 -2 191.18 6.50 -2 5 2 181.08 6.30 1 -5 -2 334.87 10.80 -1 5 2 340.97 10.70 0 -5 -2 2298.57 70.49 0 5 -2 2375.26 70.19 0 5 2 2310.57 70.39 1 -5 2 342.47 10.40 -1 5 -2 331.77 10.40 1 5 2 345.17 11.10 2 -5 2 285.07 9.00 3 -5 2 26.90 2.10 4 -5 2 22.40 2.30 5 -5 2 1.40 2.90 6 -5 2 18.10 4.40 6 -6 -2 -4.00 5.20 5 -6 -2 7.40 3.40 4 -6 -2 43.90 3.90 3 -6 -2 7.90 1.70 -3 6 2 8.10 1.70 2 -6 -2 133.49 5.00 -2 6 2 132.29 4.90 1 -6 -2 202.98 6.80 -1 6 2 195.68 6.70 0 -6 -2 384.06 12.20 0 6 -2 384.56 11.80 0 6 2 367.46 12.10 1 -6 2 253.77 7.90 1 6 2 256.57 8.70 -1 6 -2 247.18 7.80 2 -6 2 866.01 26.40 3 -6 2 16.50 1.60 4 -6 2 32.60 3.20 5 -6 2 -3.60 2.80 6 -6 2 22.10 5.00 6 -7 -2 -1.20 4.80 5 -7 -2 4.30 3.60 4 -7 -2 402.56 13.70 3 -7 -2 5.50 1.60 -3 7 2 3.90 1.50 2 -7 -2 469.45 15.10 -2 7 2 474.85 15.00 1 -7 -2 70.39 3.30 -1 7 2 68.09 3.10 0 -7 -2 4625.84 142.09 0 7 2 4788.02 141.99 1 -7 2 6.10 0.90 -1 7 -2 6.40 0.70 1 7 2 5.40 1.50 2 -7 2 692.13 21.20 2 7 2 687.33 22.50 3 -7 2 5.90 1.30 4 -7 2 26.20 2.40 5 -7 2 -1.30 3.10 6 -7 2 5.60 4.40 6 -8 -2 53.59 6.60 5 -8 -2 7.10 3.80 4 -8 -2 32.00 3.40 3 -8 -2 0.80 1.90 -3 8 2 -1.80 1.60 2 -8 -2 580.94 18.10 -2 8 2 554.94 17.90 1 -8 -2 53.19 3.10 -1 8 2 51.69 2.80 0 -8 -2 3543.15 108.79 0 8 2 3612.24 108.59 0 8 -2 3619.94 108.29 1 -8 2 61.19 2.60 -1 8 -2 60.99 2.30 1 8 2 54.19 3.40 2 -8 2 777.32 24.50 -2 8 -2 810.52 24.40 2 8 2 808.92 25.90 3 -8 2 -1.60 1.40 4 -8 2 52.19 3.60 5 -8 2 -4.80 3.20 6 -8 2 1.30 4.60 6 -9 -2 4.40 6.70 5 -9 -2 -0.20 4.00 4 -9 -2 144.89 7.00 3 -9 -2 7.30 2.00 -3 9 2 2.70 1.60 2 -9 -2 37.40 3.20 -2 9 2 39.60 2.60 1 -9 -2 50.89 3.00 -1 9 2 50.39 3.00 0 -9 -2 1261.17 39.30 0 9 2 1274.97 39.10 0 9 -2 1277.17 38.80 1 -9 2 81.09 3.40 -1 9 -2 78.99 3.00 1 9 2 75.29 4.30 2 -9 2 11.40 1.40 2 9 2 9.40 2.90 -2 9 -2 9.90 1.20 3 -9 2 3.80 1.60 4 -9 2 228.58 8.50 5 -9 2 1.50 3.40 6 -9 2 8.80 4.90 5 -10 -2 6.60 4.40 4 -10 -2 51.09 4.60 3 -10 -2 3.80 2.40 -3 10 2 5.30 1.80 2 -10 -2 900.41 28.20 1 -10 -2 82.09 4.20 -1 10 2 83.29 3.90 1 10 -2 74.19 4.50 0 -10 -2 449.76 15.40 0 10 -2 475.25 14.80 0 10 2 469.35 15.00 1 -10 2 3.80 1.30 -1 10 -2 3.40 1.00 1 10 2 2.80 2.10 2 -10 2 988.50 30.60 -2 10 -2 1000.50 30.40 2 10 2 996.70 31.90 3 -10 2 1.20 1.70 3 10 2 -2.40 3.60 4 -10 2 26.90 3.00 5 -10 2 -3.60 3.40 5 -11 -2 -1.50 3.90 4 -11 -2 32.00 4.00 -4 11 2 24.60 3.10 3 -11 -2 1.50 2.30 -3 11 2 5.60 2.30 2 -11 -2 84.99 4.70 -2 11 2 85.09 4.30 1 -11 -2 76.99 4.00 -1 11 2 71.09 3.80 1 11 -2 74.59 4.30 0 -11 -2 170.98 7.00 0 11 2 168.98 6.50 0 11 -2 170.28 6.10 1 -11 2 159.48 6.10 1 11 2 157.38 6.80 -1 11 -2 160.48 5.50 2 -11 2 147.09 5.60 -2 11 -2 149.99 5.40 2 11 2 148.39 7.20 3 -11 2 1.80 1.90 3 11 2 4.90 3.70 4 -11 2 87.99 5.30 5 -11 2 -1.20 3.70 5 -12 -2 5.60 5.00 4 -12 -2 173.78 8.50 -4 12 2 159.18 7.60 3 -12 -2 22.00 4.20 -3 12 2 16.40 2.70 2 -12 -2 489.55 16.30 -2 12 2 490.45 15.90 1 -12 -2 83.79 4.60 1 12 -2 84.79 5.00 0 -12 -2 809.82 26.30 0 12 2 827.02 26.00 0 12 -2 822.72 25.50 1 -12 2 41.20 3.40 -1 12 -2 51.09 2.80 1 12 2 46.10 3.80 2 -12 2 193.98 7.20 2 12 2 203.58 8.90 -2 12 -2 200.98 6.80 3 -12 2 3.70 2.10 4 -12 2 137.09 6.60 5 -12 2 -8.60 3.80 5 -13 -2 5.00 5.60 4 -13 -2 16.20 4.30 -4 13 2 13.30 3.40 3 -13 -2 0.30 3.00 -3 13 2 -2.00 2.40 2 -13 -2 127.69 6.30 2 13 -2 135.59 8.00 -2 13 2 126.09 5.70 1 -13 -2 56.99 4.30 -1 13 2 58.69 3.60 1 13 -2 58.09 4.70 0 -13 -2 423.16 14.60 0 13 -2 414.06 13.50 0 13 2 407.06 14.00 1 -13 2 82.69 4.80 1 13 2 75.39 5.20 -1 13 -2 82.29 3.70 2 -13 2 326.57 11.00 -2 13 -2 321.27 10.50 2 13 2 317.27 12.20 3 -13 2 16.80 2.60 -3 13 -2 17.50 2.10 4 -13 2 34.00 3.70 4 13 2 43.10 13.80 5 -13 2 -6.80 4.20 5 -14 -2 4.10 6.00 4 -14 -2 82.59 7.40 -4 14 2 82.69 6.50 3 -14 -2 9.90 3.70 -3 14 2 10.10 3.00 2 -14 -2 127.29 6.30 2 14 -2 99.19 7.90 -2 14 2 117.19 5.60 1 -14 -2 89.89 5.80 1 14 -2 85.59 5.50 -1 14 2 90.99 5.00 0 -14 -2 206.78 9.00 0 14 2 195.98 8.00 0 14 -2 194.88 7.40 1 -14 2 56.29 4.40 1 14 2 51.59 5.00 -1 14 -2 56.09 3.20 2 -14 2 800.02 24.80 -2 14 -2 762.72 24.20 3 -14 2 17.20 2.90 4 -14 2 21.10 3.70 4 14 2 38.70 8.40 5 -14 2 2.80 4.70 5 -15 -2 6.90 6.20 4 -15 -2 65.59 6.20 -4 15 2 75.69 6.70 3 -15 -2 4.80 3.80 3 15 -2 4.10 6.10 -3 15 2 1.60 2.80 2 -15 -2 332.47 12.20 -2 15 2 336.87 11.80 2 15 -2 325.27 13.10 1 -15 -2 103.39 6.60 -1 15 2 101.39 5.20 0 -15 -2 236.48 10.60 0 15 -2 247.78 8.70 0 15 2 237.88 9.10 1 -15 2 100.59 6.20 1 15 2 101.89 6.40 -1 15 -2 92.19 4.50 2 -15 2 -1.40 2.90 -2 15 -2 -0.40 1.80 3 -15 2 18.90 3.20 -3 15 -2 18.10 2.40 4 -15 2 14.20 8.30 5 -15 2 -1.20 5.10 4 -16 -2 33.80 5.80 3 -16 -2 18.00 4.30 3 16 -2 14.40 6.50 -3 16 2 3.40 3.20 2 -16 -2 82.39 6.70 -2 16 2 84.19 5.60 2 16 -2 99.09 7.30 1 -16 -2 49.50 4.90 1 16 -2 53.69 4.10 -1 16 2 50.69 4.70 0 16 -2 195.78 7.80 0 16 2 200.48 8.50 1 -16 2 41.80 4.40 -1 16 -2 49.40 3.80 1 16 2 49.99 4.10 2 -16 2 121.69 6.90 -2 16 -2 123.79 5.60 3 -16 2 1.00 3.20 -3 16 -2 5.10 2.40 4 -16 2 28.50 4.40 4 -17 -2 42.00 6.60 3 -17 -2 6.80 4.50 3 17 -2 -0.30 6.20 -3 17 2 0.70 3.80 2 -17 -2 45.30 5.10 2 17 -2 46.40 5.50 -2 17 2 57.09 5.30 1 -17 -2 31.00 4.60 -1 17 2 20.70 3.00 1 17 -2 24.80 3.70 0 17 -2 348.67 12.20 0 17 2 349.07 12.90 1 -17 2 26.90 4.80 -1 17 -2 31.10 3.10 1 17 2 32.50 3.90 2 -17 2 51.49 4.90 2 17 2 51.29 5.50 -2 17 -2 47.20 4.00 3 -17 2 4.40 3.80 3 17 2 9.60 5.40 -3 17 -2 6.70 2.60 4 -17 2 11.70 5.10 4 -18 -2 44.30 7.00 3 -18 -2 4.20 5.40 3 18 -2 5.60 7.30 -3 18 2 3.70 4.10 2 -18 -2 37.30 5.30 2 18 -2 39.80 6.10 -2 18 2 31.50 4.10 1 -18 -2 10.00 4.90 -1 18 2 9.50 3.30 1 18 -2 8.20 3.70 0 -18 -2 23.00 5.20 0 18 2 19.40 3.90 0 18 -2 21.00 3.30 -1 18 -2 35.60 3.20 1 18 2 43.10 4.40 2 -18 2 105.99 7.60 -2 18 -2 123.29 5.70 2 18 2 119.29 9.40 3 -18 2 4.70 4.10 -3 18 -2 6.70 3.10 4 -18 2 37.40 5.60 3 -19 -2 11.30 6.10 3 19 -2 3.90 7.60 2 -19 -2 39.90 5.80 2 19 -2 51.79 6.30 -2 19 2 40.10 4.80 1 -19 -2 16.40 5.50 1 19 -2 9.20 3.80 -1 19 2 9.80 3.90 0 -19 -2 9.30 5.70 0 19 2 17.80 4.30 0 19 -2 22.60 3.40 -1 19 -2 11.90 2.90 1 19 2 10.10 4.10 2 -19 2 14.80 4.70 -2 19 -2 15.40 3.00 2 19 2 16.70 5.80 3 -19 2 6.00 4.80 -3 19 -2 3.80 3.30 3 -20 -2 7.50 6.70 2 -20 -2 -6.10 6.00 -2 20 2 0.60 4.90 2 20 -2 -4.00 5.60 1 -20 -2 13.50 6.30 1 20 -2 4.00 4.70 -1 20 2 4.10 4.30 0 -20 -2 29.40 7.40 0 20 -2 18.20 3.90 0 20 2 26.20 5.00 -1 20 -2 6.30 3.20 1 20 2 1.20 4.30 -2 20 -2 58.19 5.50 3 -20 2 0.30 5.50 -3 20 -2 3.10 3.70 3 -21 -2 1.60 7.70 2 -21 -2 17.80 7.30 2 21 -2 8.20 6.30 1 -21 -2 6.20 7.10 1 21 -2 -0.20 4.50 0 -21 -2 5.10 7.90 0 21 -2 2.30 4.10 0 21 2 5.10 5.70 -1 21 -2 3.50 3.70 2 -21 2 19.20 6.70 -2 21 -2 16.10 3.90 3 -21 2 2.80 6.50 -3 21 -2 -1.50 4.40 2 -22 -2 6.50 8.00 1 -22 -2 10.60 8.00 1 22 -2 -10.90 5.00 0 22 -2 13.50 4.90 -1 22 -2 7.20 4.20 2 -22 2 -3.10 7.20 -2 22 -2 12.50 4.20 1 -23 -2 16.70 9.70 1 23 -2 6.50 6.50 0 23 -2 18.80 5.50 -1 23 -2 1.80 4.70 6 0 -3 45.70 5.60 5 0 -3 199.28 8.80 3 0 -3 436.56 14.10 2 0 -3 17.60 1.50 1 0 -3 926.31 28.40 -1 0 3 933.41 28.30 0 0 3 2.90 0.60 0 0 -3 2.90 0.70 1 0 3 134.49 4.70 3 0 3 -0.40 25.90 -3 0 -3 79.29 32.00 -4 0 -3 -15.30 42.00 4 0 3 -16.20 45.00 -5 0 -3 47.60 61.19 5 0 3 -16.00 63.79 6 0 3 34.60 4.70 6 -1 -3 5.70 4.10 6 1 -3 9.60 4.70 5 -1 -3 27.50 3.90 5 1 -3 38.40 3.90 -4 -1 3 112.29 18.20 -4 1 3 118.69 18.40 3 -1 -3 363.46 11.90 3 1 -3 353.56 11.70 2 -1 -3 593.34 18.90 2 1 -3 617.54 18.80 1 -1 -3 46.30 2.20 -1 1 3 49.20 2.10 1 1 -3 45.70 2.00 0 -1 3 5.10 0.60 0 -1 -3 3.80 0.90 0 1 -3 4.30 0.60 0 1 3 4.10 0.80 1 -1 3 2174.28 66.59 1 1 3 2243.28 66.79 -2 -1 -3 61.49 14.50 2 -1 3 52.19 21.10 2 1 3 25.00 18.70 3 -1 3 18.30 26.00 -3 -1 -3 12.70 14.50 3 1 3 15.20 25.10 -3 1 -3 54.99 34.90 -4 -1 -3 226.58 57.09 5 -1 3 -1.80 56.89 -5 -1 -3 258.97 67.19 5 1 3 6.30 53.49 6 -1 3 23.80 4.20 6 -2 -3 43.10 5.50 6 2 -3 36.20 4.80 5 -2 -3 211.78 8.80 5 2 -3 210.48 9.00 4 -2 -3 142.39 6.80 3 -2 -3 158.58 5.90 3 2 -3 153.18 5.80 2 -2 -3 30.20 2.10 2 2 -3 31.00 2.10 -2 2 3 33.10 2.10 1 -2 -3 827.52 25.10 1 2 -3 809.42 24.90 -1 2 3 818.42 25.00 0 -2 -3 2.50 1.00 0 2 -3 1.70 0.50 0 2 3 2.00 0.80 1 -2 3 151.68 5.00 1 2 3 161.88 5.60 -2 -2 -3 125.29 20.90 2 -2 3 154.08 25.20 -3 -2 -3 36.70 15.30 3 -2 3 50.79 25.90 3 2 3 -0.50 23.50 -4 -2 -3 -1.20 42.60 4 -2 3 -3.30 43.30 4 2 3 32.80 37.90 -4 2 -3 26.40 37.10 5 -2 3 -1.30 2.40 6 -2 3 21.30 4.10 6 -3 -3 16.70 5.20 6 3 -3 5.50 4.10 5 -3 -3 37.00 4.00 5 3 -3 35.70 3.60 4 -3 -3 93.69 5.10 3 -3 -3 288.67 9.90 3 3 -3 289.17 9.70 2 -3 -3 382.06 12.50 -2 3 3 394.46 12.40 1 -3 -3 2051.89 63.49 1 3 -3 2113.89 63.29 -1 3 3 2124.89 63.39 0 -3 -3 10.00 1.20 0 3 3 9.80 1.10 0 3 -3 9.70 0.70 1 3 3 732.03 22.70 2 3 3 111.79 5.30 -3 -3 -3 82.39 20.40 3 -3 3 97.19 25.40 4 -3 3 215.88 7.70 5 -3 3 76.39 5.70 6 -3 3 13.60 4.50 6 -4 -3 5.40 4.60 6 4 -3 14.00 4.20 5 -4 -3 53.59 4.60 5 4 -3 52.29 4.20 4 -4 -3 86.29 5.20 3 -4 -3 220.48 8.00 2 -4 -3 73.49 3.40 -2 4 3 75.49 3.30 1 -4 -3 1013.00 31.20 -1 4 3 1023.20 31.20 0 -4 -3 0.10 1.10 0 4 3 1.10 1.00 1 4 3 1847.52 56.19 2 -4 3 171.98 5.70 2 4 3 181.18 7.20 3 -4 3 110.19 4.10 4 -4 3 33.50 3.10 5 -4 3 -39.70 64.69 -5 -4 -3 9.90 59.79 -5 4 -3 29.50 42.30 5 4 3 -31.90 49.30 6 -4 3 6.20 4.00 6 -5 -3 8.70 5.40 6 5 -3 12.70 4.80 5 -5 -3 73.89 6.40 5 5 -3 71.89 5.10 -4 -5 3 29.50 23.00 4 -5 -3 17.90 41.30 4 5 -3 -5.00 20.90 -4 5 3 43.90 14.70 3 -5 -3 145.09 6.00 -3 5 3 144.69 5.60 2 -5 -3 185.98 6.80 -2 5 3 190.28 6.60 1 -5 -3 221.38 7.50 -1 5 3 221.38 7.40 0 -5 -3 15.60 1.60 0 5 3 13.80 1.50 -1 -5 -3 35.20 3.50 1 5 3 36.50 2.80 2 -5 3 68.19 2.60 2 5 3 63.59 4.50 3 -5 3 65.59 3.00 4 -5 3 70.69 4.00 -5 -5 -3 -31.70 52.49 5 -5 3 43.50 52.29 5 5 3 6.80 50.09 -5 5 -3 17.20 40.40 6 -5 3 13.40 4.00 6 -6 -3 3.70 9.30 5 -6 -3 94.19 6.40 4 -6 -3 40.30 3.60 3 -6 -3 61.19 3.60 -3 6 3 60.39 3.30 2 -6 -3 72.99 3.70 -2 6 3 75.29 3.50 1 -6 -3 722.23 22.30 -1 6 3 707.33 22.20 0 -6 -3 0.00 1.40 0 6 -3 4.80 0.80 0 6 3 3.40 1.20 -1 -6 -3 598.84 19.30 1 6 3 588.74 18.90 2 -6 3 40.20 1.90 2 6 3 40.90 4.00 3 -6 3 72.79 3.10 4 -6 3 42.30 3.30 5 -6 3 -3.90 49.30 5 6 3 7.60 50.29 -5 6 -3 112.99 48.60 6 -6 3 4.70 4.50 5 -7 -3 14.30 4.10 4 -7 -3 17.20 3.20 3 -7 -3 248.08 8.80 -3 7 3 238.78 8.50 2 -7 -3 4.70 1.70 -2 7 3 4.00 1.30 1 -7 -3 26.60 2.20 -1 7 3 24.50 2.40 0 -7 -3 4.60 1.70 0 7 -3 4.20 0.90 0 7 3 4.90 1.40 1 -7 3 1032.80 30.60 -1 -7 -3 1011.10 31.80 1 7 3 979.50 31.30 2 -7 3 52.29 2.30 2 7 3 54.49 4.50 3 -7 3 39.80 2.60 3 7 3 49.50 4.60 4 -7 3 4.20 1.90 5 -7 3 -12.50 47.20 5 7 3 3.60 51.79 6 -7 3 13.80 4.90 5 -8 -3 45.90 4.70 4 -8 -3 17.90 3.00 3 -8 -3 93.79 4.80 -3 8 3 100.49 4.70 2 -8 -3 21.60 2.40 1 -8 -3 1904.61 58.49 -1 8 3 1923.21 58.29 0 -8 -3 3.20 1.60 0 8 3 6.10 1.60 0 8 -3 3.70 1.00 -1 -8 -3 160.98 7.00 1 -8 3 161.18 5.40 1 8 3 163.88 6.30 -1 8 -3 158.18 5.10 2 -8 3 22.80 1.70 2 8 3 21.60 2.80 3 -8 3 23.90 1.90 3 8 3 18.30 3.60 4 -8 3 41.60 3.00 5 -8 3 21.10 45.90 -5 8 -3 24.60 36.30 5 8 3 40.50 50.89 5 -9 -3 60.89 5.80 4 -9 -3 13.60 3.00 3 -9 -3 217.28 8.30 -3 9 3 204.78 7.90 2 -9 -3 31.20 2.90 -2 9 3 33.70 2.90 1 -9 -3 442.46 14.50 -1 9 3 438.36 14.30 0 -9 -3 -1.10 1.70 0 9 3 0.40 1.60 0 9 -3 0.10 1.10 1 -9 3 17.80 1.60 -1 -9 -3 21.90 3.20 -1 9 -3 19.60 1.30 1 9 3 24.70 2.60 2 -9 3 18.70 1.60 2 9 3 19.90 3.70 3 -9 3 23.80 2.00 3 9 3 25.80 4.50 4 -9 3 8.40 2.40 5 -9 3 19.80 4.00 5 -10 -3 21.00 4.40 4 -10 -3 26.90 3.60 -4 10 3 23.80 3.10 3 -10 -3 114.59 7.20 -3 10 3 145.79 5.90 2 -10 -3 25.20 2.70 -2 10 3 17.50 2.20 1 -10 -3 117.59 5.40 -1 10 3 112.39 5.00 0 -10 -3 2.10 2.30 0 10 3 -0.30 1.70 0 10 -3 0.80 1.20 1 -10 3 2.90 1.50 -1 -10 -3 -0.30 2.90 1 10 3 1.30 2.10 -1 10 -3 0.50 0.80 2 -10 3 50.19 2.70 2 10 3 46.70 4.00 3 -10 3 62.19 3.50 3 10 3 65.39 5.50 4 -10 3 16.80 2.50 5 -10 3 14.70 3.50 5 -11 -3 5.70 5.10 4 -11 -3 23.90 3.70 -4 11 3 22.20 3.60 3 -11 -3 778.22 25.10 -3 11 3 781.62 24.90 2 -11 -3 68.69 4.70 -2 11 3 63.79 3.80 1 -11 -3 185.38 7.40 1 11 -3 187.08 7.60 -1 11 3 195.48 7.10 0 -11 -3 3.70 2.70 0 11 -3 1.90 1.40 -1 -11 -3 139.69 7.60 1 11 3 135.49 6.40 -1 11 -3 147.79 4.90 2 -11 3 27.00 2.60 2 11 3 26.40 3.30 -2 11 -3 27.70 1.90 3 -11 3 129.39 5.20 3 11 3 115.69 8.50 4 -11 3 51.19 4.40 4 11 3 44.40 7.40 5 -11 3 29.60 3.90 5 -12 -3 4.60 4.90 4 -12 -3 37.30 4.70 -4 12 3 23.00 3.80 3 -12 -3 581.24 19.40 -3 12 3 578.94 19.10 2 -12 -3 0.80 2.20 -2 12 3 -0.80 2.00 1 -12 -3 343.67 12.30 1 12 -3 338.57 12.10 -1 12 3 356.66 11.90 0 -12 -3 2.00 2.80 0 12 -3 0.90 1.50 0 12 3 -1.40 1.70 -1 -12 -3 380.46 14.30 1 12 3 375.36 13.10 -1 12 -3 375.76 11.90 2 -12 3 52.69 3.50 2 12 3 55.29 5.10 -2 12 -3 51.69 2.70 3 -12 3 228.78 8.20 4 -12 3 6.60 2.60 4 12 3 11.00 6.80 5 -12 3 6.50 4.20 5 -13 -3 8.10 6.50 4 -13 -3 27.40 5.00 -4 13 3 19.90 3.80 3 -13 -3 88.49 5.90 -3 13 3 88.39 5.60 2 -13 -3 53.59 5.40 -2 13 3 71.49 4.20 1 -13 -3 79.79 5.50 -1 13 3 77.49 4.40 1 13 -3 78.19 4.80 0 -13 -3 3.90 3.10 0 13 -3 9.60 1.90 0 13 3 10.80 2.50 1 13 3 143.19 7.00 -1 13 -3 146.89 5.30 2 -13 3 34.30 2.80 2 13 3 38.80 4.40 -2 13 -3 31.90 2.60 3 -13 3 208.18 7.90 4 -13 3 49.90 3.90 4 13 3 45.80 7.60 5 -13 3 26.40 4.50 5 -14 -3 34.00 7.60 4 -14 -3 25.50 4.70 3 -14 -3 15.30 3.90 -3 14 3 7.40 3.10 2 -14 -3 0.60 2.80 2 14 -3 5.20 3.70 -2 14 3 0.80 2.50 1 -14 -3 340.07 13.70 -1 14 3 360.16 12.30 1 14 -3 359.86 12.50 0 -14 -3 1.20 3.50 0 14 -3 -2.00 1.80 0 14 3 3.10 2.20 -1 14 -3 320.67 10.50 2 -14 3 34.00 3.10 -2 14 -3 30.70 2.90 3 -14 3 18.20 2.90 4 -14 3 -1.90 3.20 5 -14 3 17.80 5.10 4 -15 -3 9.90 5.40 3 -15 -3 85.59 6.60 -3 15 3 79.09 6.30 2 -15 -3 46.30 4.40 -2 15 3 42.00 3.70 2 15 -3 41.40 5.00 1 -15 -3 55.29 5.30 1 15 -3 51.09 5.00 -1 15 3 45.20 4.30 0 -15 -3 4.20 4.00 0 15 -3 2.40 2.10 -1 15 -3 83.69 4.00 2 -15 3 7.60 2.70 -2 15 -3 3.90 1.70 3 -15 3 129.59 6.50 4 -15 3 27.40 4.10 4 -16 -3 14.80 6.10 3 -16 -3 5.40 4.80 -3 16 3 1.50 3.70 3 16 -3 7.90 6.50 2 -16 -3 -2.00 3.50 2 16 -3 -4.60 3.80 -2 16 3 0.70 2.60 1 -16 -3 176.48 8.80 -1 16 3 178.28 8.00 0 -16 -3 -3.20 4.30 0 16 -3 1.60 2.00 -1 16 -3 304.27 10.30 2 -16 3 15.90 3.30 -2 16 -3 13.50 2.00 3 -16 3 54.39 5.30 3 16 3 53.09 7.10 4 -16 3 0.50 4.20 4 -17 -3 5.90 5.80 3 -17 -3 62.39 6.50 3 17 -3 73.59 9.00 2 -17 -3 3.60 4.60 -2 17 3 5.00 3.50 2 17 -3 0.50 4.60 1 -17 -3 199.78 9.70 -1 17 3 190.88 8.90 1 17 -3 196.18 8.70 0 -17 -3 -5.30 4.00 0 17 -3 -1.50 2.70 0 17 3 0.90 3.90 -1 17 -3 45.10 3.80 2 -17 3 11.90 3.90 -2 17 -3 5.70 2.30 3 -17 3 23.60 4.40 4 -17 3 18.40 5.60 4 -18 -3 24.20 8.40 3 -18 -3 13.80 6.20 3 18 -3 14.40 8.70 2 -18 -3 -0.90 5.10 -2 18 3 2.20 3.80 2 18 -3 3.80 5.30 1 -18 -3 184.18 10.50 -1 18 3 171.88 8.90 1 18 -3 178.88 8.60 0 -18 -3 -3.60 4.80 0 18 -3 -1.40 3.10 0 18 3 6.00 3.40 -1 18 -3 54.79 4.50 1 18 3 52.39 5.50 2 -18 3 0.50 4.20 2 18 3 2.40 5.40 -2 18 -3 -0.60 2.40 3 -18 3 28.50 5.20 -3 18 -3 20.40 3.00 4 -18 3 0.50 5.70 3 -19 -3 11.40 7.00 3 19 -3 13.40 8.60 2 -19 -3 6.00 5.90 2 19 -3 13.00 5.90 1 -19 -3 31.60 6.50 -1 19 3 33.40 4.70 1 19 -3 36.10 4.50 0 -19 -3 3.50 5.90 0 19 3 6.60 4.30 0 19 -3 -4.20 3.20 -1 19 -3 6.30 2.70 1 19 3 0.80 4.10 2 -19 3 0.50 4.80 -2 19 -3 0.60 2.70 3 -19 3 22.10 5.30 -3 19 -3 35.50 3.60 3 -20 -3 103.89 9.60 2 -20 -3 2.20 6.90 2 20 -3 -2.40 5.60 1 -20 -3 4.40 6.70 1 20 -3 6.50 4.60 0 -20 -3 4.90 7.50 0 20 -3 0.40 3.40 -1 20 -3 7.10 3.20 3 -20 3 24.40 6.50 2 -21 -3 12.60 7.70 2 21 -3 12.60 7.10 1 -21 -3 43.20 7.20 1 21 -3 61.49 6.00 0 -21 -3 -1.20 8.40 0 21 -3 0.40 3.80 -1 21 -3 2.90 3.10 -2 21 -3 -2.70 3.30 2 -22 -3 -0.20 9.00 2 22 -3 0.20 7.80 1 -22 -3 -13.30 8.70 1 22 -3 -3.50 5.40 0 -22 -3 -17.60 9.30 0 22 -3 7.70 4.70 -1 22 -3 19.00 4.20 -2 -22 -3 73.49 78.19 2 22 3 -23.60 68.59 1 -23 -3 11.80 16.40 1 23 -3 -6.90 6.20 0 23 -3 4.20 5.00 -1 -23 -3 -21.40 62.09 5 0 -4 -2.90 2.90 4 0 -4 7.10 2.50 3 0 -4 59.39 3.40 2 0 -4 15.80 1.60 -1 0 4 694.13 21.40 1 0 -4 702.03 21.50 0 0 -4 2419.76 73.69 0 0 4 2466.25 73.59 1 0 4 25.70 1.70 2 0 4 80.99 4.10 -3 0 -4 12.40 28.40 3 0 4 -7.90 28.80 5 0 4 -1.70 61.19 -5 0 -4 27.20 68.99 6 0 4 3.10 3.90 5 -1 -4 4.40 3.50 5 1 -4 11.90 3.10 4 -1 -4 128.39 6.20 4 1 -4 123.99 5.90 3 -1 -4 24.30 2.10 3 1 -4 20.40 2.00 2 -1 -4 31.80 2.50 2 1 -4 27.90 2.30 1 -1 -4 148.79 5.20 1 1 -4 145.39 5.00 -1 1 4 146.19 5.10 0 -1 -4 190.58 6.50 0 -1 4 196.58 6.20 0 1 4 193.18 6.30 0 1 -4 193.48 6.30 1 -1 4 832.72 25.50 1 1 4 846.62 25.70 2 -1 4 42.60 3.20 2 1 4 46.80 3.30 3 -1 4 0.60 34.20 -3 -1 -4 1.60 14.50 -3 1 -4 12.10 36.70 3 1 4 13.90 28.00 -4 -1 -4 62.29 51.69 4 -1 4 32.50 49.99 4 1 4 -3.50 39.40 -4 1 -4 103.39 49.60 5 -1 4 -36.50 61.89 -5 -1 -4 -1.30 62.09 5 1 4 12.70 68.69 6 -1 4 0.40 3.90 5 -2 -4 2.80 3.50 5 2 -4 -2.30 3.40 4 -2 -4 21.50 2.70 4 2 -4 23.20 2.90 3 -2 -4 35.60 3.20 3 2 -4 32.30 2.80 2 -2 -4 775.72 24.30 2 2 -4 779.62 24.10 -2 2 4 783.62 24.20 1 -2 -4 532.25 17.00 -1 2 4 550.64 17.00 1 2 -4 551.84 16.80 0 -2 -4 1010.20 31.40 0 -2 4 1053.79 31.00 0 2 4 1020.80 31.30 0 2 -4 1019.90 31.10 1 -2 4 42.30 1.70 1 2 4 40.80 2.50 2 2 4 422.76 14.00 -3 -2 -4 5.60 15.70 3 2 4 0.30 26.80 -3 2 -4 21.80 33.20 -4 -2 -4 223.48 50.49 -4 2 -4 369.06 59.19 5 -2 4 3.00 3.40 6 -2 4 15.00 4.40 5 -3 -4 7.40 3.80 5 3 -4 -1.10 3.00 4 -3 -4 32.40 3.10 4 3 -4 31.00 2.90 3 -3 -4 10.30 2.20 3 3 -4 17.60 1.90 2 -3 -4 989.00 31.10 2 3 -4 1020.30 30.90 -2 3 4 1009.20 31.00 1 -3 -4 162.48 5.70 1 3 -4 156.18 5.30 -1 3 4 156.98 5.50 0 -3 -4 74.49 3.40 0 3 4 76.49 3.20 0 3 -4 72.89 2.60 1 3 4 445.46 14.20 2 3 4 2411.16 73.49 -3 -3 -4 8.20 17.80 3 -3 4 8.10 32.20 3 3 4 7.30 25.90 -3 3 -4 23.60 29.80 4 -3 4 13.70 2.00 -5 -3 -4 7.00 72.09 5 -3 4 21.40 67.39 -5 3 -4 9.00 49.40 5 3 4 47.10 67.19 6 -3 4 8.80 4.40 5 -4 -4 -3.80 3.70 5 4 -4 6.00 3.50 4 -4 -4 170.78 7.50 4 4 -4 163.78 7.00 3 -4 -4 17.30 2.40 3 4 -4 15.50 1.80 2 -4 -4 179.78 6.60 -2 4 4 184.98 6.50 2 4 -4 184.48 6.30 1 -4 -4 254.67 8.40 1 4 -4 246.08 7.90 -1 4 4 246.28 8.20 0 -4 -4 303.37 10.00 0 4 4 304.97 9.80 0 4 -4 298.27 9.30 -1 -4 -4 144.49 6.20 1 4 4 135.99 5.40 2 -4 4 43.30 1.90 2 4 4 45.20 3.60 3 -4 4 8.30 1.20 3 4 4 9.10 3.20 4 -4 4 24.00 2.30 5 -4 4 -1.80 2.60 6 -4 4 11.00 4.50 5 -5 -4 1.40 3.50 5 5 -4 -0.40 3.40 4 -5 -4 226.58 9.10 4 5 -4 222.08 8.50 3 -5 -4 0.70 1.90 3 5 -4 5.10 1.70 -3 5 4 3.90 1.60 2 -5 -4 149.19 6.10 -2 5 4 161.78 6.00 2 5 -4 162.28 5.60 1 -5 -4 110.59 4.60 -1 5 4 110.59 4.30 1 5 -4 104.09 3.80 0 -5 -4 463.45 14.80 0 5 4 449.46 14.50 -1 -5 -4 36.30 3.00 1 5 4 35.20 2.80 2 -5 4 76.79 2.70 2 5 4 74.29 4.50 3 5 4 1.90 3.80 4 -5 4 11.20 2.00 5 -5 4 0.30 2.70 5 -6 -4 4.90 3.60 5 6 -4 -1.90 3.40 4 -6 -4 183.48 8.20 4 6 -4 183.98 7.40 3 -6 -4 7.20 2.40 -3 6 4 3.40 1.90 2 -6 -4 343.87 11.50 1 -6 -4 30.20 2.60 -1 6 4 33.30 2.50 0 -6 -4 2125.09 64.29 0 6 4 2092.79 64.09 -1 -6 -4 146.19 6.70 1 6 4 153.48 5.90 2 -6 4 384.06 11.90 2 6 4 389.66 13.30 3 -6 4 10.10 1.40 3 6 4 8.70 3.40 4 -6 4 2.30 1.90 5 -6 4 0.30 2.60 5 -7 -4 -3.70 4.30 5 7 -4 2.70 3.90 4 -7 -4 180.78 8.00 3 -7 -4 6.90 2.40 -3 7 4 6.20 1.90 2 -7 -4 37.00 3.50 -2 7 4 37.90 2.80 1 -7 -4 177.58 6.70 -1 7 4 173.08 6.30 0 -7 -4 37.00 3.00 0 7 4 36.30 2.90 0 7 -4 40.60 1.90 -1 -7 -4 20.10 3.20 1 7 4 16.40 2.20 2 7 4 142.89 6.60 3 -7 4 15.40 1.50 3 7 4 16.60 3.70 4 -7 4 89.49 4.40 5 -7 4 0.60 3.00 5 -8 -4 -3.40 4.60 5 8 -4 -2.10 3.40 4 -8 -4 19.90 3.30 3 -8 -4 3.00 2.30 2 -8 -4 45.10 3.80 -2 8 4 44.80 3.00 1 -8 -4 78.49 4.10 -1 8 4 76.69 3.90 0 -8 -4 122.09 5.60 0 8 -4 131.79 4.40 0 8 4 123.29 5.10 -1 -8 -4 179.28 8.10 1 8 4 185.18 7.20 2 -8 4 97.49 3.40 2 8 4 85.39 6.50 3 -8 4 6.40 1.30 3 8 4 -2.40 4.00 4 -8 4 65.79 3.90 5 -8 4 -0.60 3.10 5 -9 -4 4.20 5.20 4 -9 -4 21.10 3.90 3 -9 -4 15.70 2.80 2 -9 -4 221.58 8.60 -2 9 4 228.88 8.30 1 -9 -4 113.99 5.30 -1 9 4 117.39 5.00 0 -9 -4 226.58 8.50 0 9 4 219.08 8.00 0 9 -4 220.88 7.20 -1 -9 -4 80.19 6.00 1 9 4 83.79 5.20 2 -9 4 7.30 1.20 2 9 4 15.00 2.90 3 -9 4 12.80 1.70 3 9 4 8.50 3.90 4 -9 4 21.40 2.50 5 -9 4 7.40 3.10 5 -10 -4 6.80 5.40 4 -10 -4 29.50 4.00 -4 10 4 22.20 3.90 3 -10 -4 6.80 3.10 2 -10 -4 119.09 6.00 -2 10 4 119.79 5.40 1 -10 -4 108.89 5.30 -1 10 4 101.69 4.70 0 -10 -4 55.49 4.70 0 10 -4 53.89 2.60 0 10 4 54.49 3.70 -1 -10 -4 122.89 6.70 1 10 4 111.49 5.50 2 -10 4 28.90 2.20 2 10 4 32.90 3.60 3 -10 4 8.80 1.70 3 10 4 2.30 3.40 4 -10 4 178.78 6.80 4 10 4 155.88 10.30 5 -10 4 0.90 3.50 5 -11 -4 -5.10 5.10 4 -11 -4 45.20 5.10 -4 11 4 43.10 4.40 3 -11 -4 9.10 3.40 1 -11 -4 75.39 5.00 -1 11 4 74.19 4.30 1 11 -4 69.59 5.10 0 -11 -4 39.60 3.80 0 11 4 33.60 3.00 0 11 -4 31.90 2.40 -1 -11 -4 88.59 7.10 -1 11 -4 90.69 3.10 1 11 4 88.19 5.20 2 -11 4 408.46 12.90 2 11 4 409.76 14.50 3 -11 4 9.40 1.90 3 11 4 6.20 5.10 4 -11 4 4.20 2.60 4 11 4 9.30 6.70 5 -11 4 1.20 3.60 5 -12 -4 2.80 5.90 4 -12 -4 9.50 4.40 3 -12 -4 17.60 3.90 2 -12 -4 123.19 6.30 1 -12 -4 123.59 6.50 -1 12 4 110.29 5.50 1 12 -4 111.79 5.80 0 -12 -4 88.59 6.50 0 12 4 107.09 5.10 0 12 -4 98.09 4.10 -1 -12 -4 39.70 4.60 -1 12 -4 37.80 1.90 2 -12 4 136.19 5.20 2 12 4 120.49 6.90 3 -12 4 4.90 2.20 4 -12 4 21.80 3.00 4 12 4 23.40 7.10 5 -12 4 6.30 4.10 4 -13 -4 44.90 5.80 3 -13 -4 7.60 3.50 2 -13 -4 1.60 2.80 1 -13 -4 25.80 4.50 1 13 -4 28.30 3.20 0 -13 -4 101.19 6.60 0 13 4 86.09 5.40 0 13 -4 87.59 3.90 -1 13 -4 85.29 3.40 2 -13 4 358.36 11.80 2 13 4 352.26 13.60 3 -13 4 11.40 2.40 3 13 4 25.20 5.60 4 -13 4 16.60 3.20 -5 -13 -4 -34.10 74.49 -5 13 -4 16.60 49.80 4 -14 -4 15.30 5.00 3 -14 -4 6.80 3.80 -3 14 4 6.00 3.40 2 -14 -4 161.38 8.30 2 14 -4 145.19 8.60 1 -14 -4 36.80 4.10 1 14 -4 40.70 3.50 0 -14 -4 215.28 9.90 0 14 -4 197.48 7.20 -1 -14 -4 26.10 5.40 -1 14 -4 27.90 2.20 2 -14 4 77.89 4.70 3 -14 4 -0.40 2.60 3 14 4 1.70 5.10 4 -14 4 9.00 3.70 4 -15 -4 39.60 5.90 3 -15 -4 -3.80 3.90 -3 15 4 0.20 3.20 2 -15 -4 13.30 4.30 2 15 -4 10.50 4.30 1 -15 -4 8.60 3.50 1 15 -4 10.90 3.20 0 -15 -4 169.78 9.10 0 15 -4 174.08 6.60 -1 15 -4 19.10 1.80 -2 15 -4 25.00 1.90 3 -15 4 7.60 3.10 3 15 4 10.60 6.00 4 -15 4 11.00 3.90 4 -16 -4 20.90 6.10 3 -16 -4 6.70 4.70 3 16 -4 13.30 7.50 2 -16 -4 26.60 4.70 2 16 -4 21.70 5.20 -2 16 4 32.40 3.80 1 -16 -4 21.50 4.40 1 16 -4 19.10 3.30 0 -16 -4 33.70 5.00 0 16 -4 29.10 2.80 -1 16 -4 5.00 1.90 2 16 4 46.90 7.90 -2 16 -4 39.90 3.00 3 -16 4 1.60 3.80 -4 -16 -4 37.20 95.89 4 16 4 -17.20 70.89 -4 16 -4 41.00 33.00 4 -17 -4 -8.20 58.79 3 -17 -4 -2.50 5.90 3 17 -4 -12.00 7.80 2 -17 -4 -0.20 5.10 -2 17 4 -0.50 3.90 2 17 -4 7.70 4.90 1 -17 -4 3.60 5.20 -1 17 4 7.70 3.90 1 17 -4 7.30 3.90 0 -17 -4 140.99 10.10 0 17 -4 140.89 6.20 -1 17 -4 4.90 1.90 2 17 4 11.50 5.50 -2 17 -4 11.10 2.00 3 -17 4 6.00 4.00 -4 -17 -4 -72.19 88.39 4 17 4 29.10 79.59 -4 17 -4 29.80 36.90 3 -18 -4 -11.80 6.40 3 18 -4 3.30 7.50 2 -18 -4 9.10 6.00 2 18 -4 10.00 5.70 1 -18 -4 5.40 5.80 -1 18 4 -4.20 4.20 1 18 -4 -6.30 3.30 0 -18 -4 164.08 11.80 0 18 4 168.78 8.50 0 18 -4 165.48 7.30 1 18 4 2.00 4.70 -1 18 -4 2.80 2.10 -2 18 -4 26.60 2.70 3 -18 4 -0.90 4.80 3 -19 -4 -0.70 6.60 3 19 -4 -11.80 9.00 2 -19 -4 24.50 6.20 2 19 -4 26.10 5.70 1 -19 -4 0.40 5.90 1 19 -4 -5.80 4.10 0 -19 -4 41.40 8.50 0 19 -4 55.99 4.40 -1 19 -4 -2.70 2.40 -2 19 -4 -0.60 2.40 -3 -19 -4 10.20 72.49 3 19 4 -58.69 66.09 -3 19 -4 4.60 27.90 2 -20 -4 4.90 7.60 2 20 -4 -0.80 6.00 1 -20 -4 6.40 7.30 1 20 -4 3.40 4.20 0 -20 -4 2.40 7.10 0 20 -4 5.60 3.50 -1 20 -4 0.50 2.90 -2 -20 -4 15.40 69.39 -2 20 -4 11.80 22.50 2 20 4 -6.40 60.29 2 21 -4 47.60 7.70 1 -21 -4 -1.50 7.50 1 21 -4 -3.40 4.60 0 -21 -4 27.10 9.70 0 21 -4 9.10 4.00 -1 -21 -4 -4.00 29.40 -1 -21 -4 41.90 63.39 -2 -21 -4 69.89 78.79 2 21 4 -51.09 69.19 1 22 -4 7.10 5.30 0 -22 -4 -6.00 12.00 -1 -22 -4 -31.10 71.09 -1 -22 -4 -10.40 30.30 5 0 -5 -6.00 3.70 4 0 -5 45.70 4.20 3 0 -5 -1.40 1.80 2 0 -5 3.10 1.50 -1 0 5 51.29 2.50 1 0 -5 50.09 2.80 0 0 -5 1.90 1.20 0 0 5 2.60 0.90 1 0 5 283.27 9.10 2 0 5 79.29 3.80 3 0 5 35.20 3.50 4 0 5 67.39 48.90 5 0 5 2.90 78.99 -5 0 -5 144.19 83.59 5 -1 -5 126.49 8.10 5 1 -5 133.59 7.80 4 -1 -5 2.70 2.80 4 1 -5 3.40 2.70 3 -1 -5 116.69 5.30 3 1 -5 113.49 5.20 2 -1 -5 55.89 3.40 2 1 -5 59.29 3.20 1 -1 -5 657.03 20.20 -1 1 5 626.74 20.00 1 1 -5 654.93 20.00 0 -1 5 1.80 0.80 0 -1 -5 -0.50 1.40 0 1 5 0.30 0.90 0 1 -5 0.50 1.10 1 -1 5 283.37 9.00 1 1 5 285.27 9.20 2 -1 5 10.40 1.70 2 1 5 6.50 1.90 3 -1 5 100.09 5.60 3 1 5 83.99 5.60 4 -1 5 28.30 53.29 4 1 5 1.60 43.60 -4 1 -5 25.50 50.69 -5 -1 -5 83.09 88.09 5 -1 5 247.78 81.09 -5 1 -5 85.29 77.89 5 1 5 70.59 79.19 5 -2 -5 0.10 3.80 5 2 -5 -1.80 3.20 4 -2 -5 37.80 3.80 4 2 -5 41.40 3.60 3 -2 -5 341.07 11.90 3 2 -5 348.07 11.70 2 -2 -5 11.50 1.90 2 2 -5 11.50 1.60 -2 2 5 12.30 1.70 1 -2 -5 193.58 6.80 1 2 -5 191.98 6.40 -1 2 5 187.78 6.50 0 -2 5 5.30 0.80 0 -2 -5 3.90 1.40 0 2 5 5.90 1.20 0 2 -5 4.70 1.10 1 -2 5 201.08 6.30 1 2 5 195.98 6.80 2 -2 5 46.00 2.70 2 2 5 52.39 3.70 3 -2 5 340.37 11.90 3 2 5 331.57 12.10 4 -2 5 -28.30 49.60 -4 2 -5 14.00 46.40 4 2 5 4.60 43.10 -5 -2 -5 1.90 93.39 5 -2 5 6.40 73.29 5 2 5 2.00 74.09 -5 2 -5 78.09 73.29 5 -3 -5 3.40 4.40 5 3 -5 4.70 4.00 4 -3 -5 6.00 3.10 4 3 -5 5.70 2.70 3 -3 -5 213.88 8.20 3 3 -5 207.78 7.70 2 -3 -5 27.10 2.40 2 3 -5 33.50 2.50 -2 3 5 26.60 2.20 1 -3 -5 27.10 2.10 -1 3 5 33.00 2.40 1 3 -5 26.90 2.10 0 -3 -5 -2.40 1.60 0 3 -5 -0.80 0.80 0 3 5 -2.00 1.00 -1 -3 -5 649.54 21.20 1 3 5 670.73 20.70 2 -3 5 23.00 2.00 2 3 5 25.20 2.50 3 3 5 144.49 7.00 4 -3 5 12.60 2.10 5 -3 5 18.80 3.00 5 -4 -5 15.80 4.80 5 4 -5 19.50 4.40 4 -4 -5 8.30 3.20 4 4 -5 8.00 2.50 3 -4 -5 99.89 5.40 3 4 -5 101.09 4.70 2 -4 -5 29.00 2.50 2 4 -5 28.70 2.40 -2 4 5 28.50 2.80 1 -4 -5 245.08 8.70 1 4 -5 255.17 8.10 -1 4 5 243.28 8.40 0 -4 -5 2.60 1.90 0 4 -5 0.20 0.80 0 4 5 3.70 1.30 -1 -4 -5 58.99 4.80 1 4 5 60.49 3.40 2 4 5 8.20 2.20 3 -4 5 154.08 5.30 4 -4 5 14.30 2.00 5 -4 5 20.60 3.20 5 4 5 21.80 8.00 5 -5 -5 36.10 4.80 5 5 -5 37.80 4.50 4 -5 -5 -1.50 3.10 4 5 -5 4.80 2.70 3 5 -5 223.38 8.20 -3 5 5 232.38 8.40 2 -5 -5 -0.90 1.60 -2 5 5 5.30 1.70 2 5 -5 2.60 1.20 1 -5 -5 25.40 2.40 -1 5 5 23.70 2.10 1 5 -5 23.90 1.80 0 -5 -5 4.60 1.90 -1 -5 -5 282.07 10.50 1 5 5 272.07 9.40 2 5 5 20.10 2.60 3 -5 5 160.38 5.50 4 -5 5 1.40 1.70 5 5 5 21.50 8.00 5 -6 -5 15.70 4.70 5 6 -5 17.90 4.30 4 -6 -5 7.70 3.70 4 6 -5 7.40 2.70 3 -6 -5 67.69 5.00 -3 6 5 67.99 4.00 3 6 -5 64.69 3.90 2 -6 -5 37.80 3.10 -2 6 5 36.00 2.90 2 6 -5 36.70 2.60 1 -6 -5 77.29 4.20 -1 6 5 77.59 3.90 1 6 -5 78.59 3.10 0 -6 -5 0.90 1.90 0 6 5 4.50 1.60 -1 -6 -5 118.19 6.40 1 6 5 123.19 5.20 2 6 5 7.00 2.40 3 -6 5 86.29 3.50 4 -6 5 12.50 2.00 5 -6 5 41.30 3.50 5 6 5 37.40 8.50 5 -7 -5 62.29 6.50 5 7 -5 73.19 6.60 4 -7 -5 16.90 3.60 4 7 -5 17.70 2.90 3 -7 -5 198.48 8.10 3 7 -5 199.38 7.40 -3 7 5 196.98 7.80 2 7 -5 5.60 1.50 -2 7 5 10.30 2.00 1 -7 -5 154.38 6.40 1 7 -5 158.08 5.30 0 -7 -5 4.50 2.20 0 7 5 3.20 1.80 -1 -7 -5 89.69 6.30 1 7 5 81.99 4.50 2 7 5 30.20 3.30 3 -7 5 90.59 3.60 4 -7 5 4.40 1.90 5 -7 5 25.40 3.60 5 -8 -5 41.60 6.30 5 8 -5 34.70 4.70 4 -8 -5 9.00 4.10 4 8 -5 14.40 2.80 3 -8 -5 145.29 7.30 3 8 -5 151.88 6.10 2 -8 -5 30.50 3.10 -2 8 5 24.90 2.50 1 -8 -5 138.79 6.30 -1 8 5 135.99 5.70 1 8 -5 141.99 4.80 0 -8 -5 2.20 2.50 -1 -8 -5 283.57 11.30 2 8 5 31.70 3.30 3 -8 5 65.49 3.00 4 -8 5 16.40 2.20 5 -8 5 16.40 3.50 5 -9 -5 5.00 5.80 5 9 -5 14.10 4.40 4 -9 -5 25.90 4.70 4 9 -5 28.20 3.20 3 -9 -5 81.29 6.00 2 -9 -5 37.70 5.10 -2 9 5 39.50 3.30 1 -9 -5 261.87 9.90 -1 9 5 276.07 9.60 0 -9 -5 1.10 2.50 0 9 5 2.90 1.70 -1 -9 -5 203.08 9.60 1 9 5 209.98 8.10 2 9 5 18.20 3.50 3 -9 5 38.10 2.40 4 -9 5 22.40 2.40 4 9 5 21.70 6.10 5 -9 5 27.50 3.90 5 10 -5 34.40 5.10 4 -10 -5 24.90 5.10 3 -10 -5 118.89 6.60 2 -10 -5 16.70 2.90 -2 10 5 16.00 2.50 1 -10 -5 163.18 7.50 -1 10 5 167.08 6.90 0 -10 -5 0.20 2.50 0 10 5 -0.20 2.20 -1 -10 -5 74.69 6.30 1 10 5 71.99 4.60 2 -10 5 8.20 20.10 -2 -10 -5 2.00 30.70 -2 10 -5 43.20 19.70 2 10 5 1.70 27.60 -3 -10 -5 -14.30 46.10 3 -10 5 -3.80 26.30 3 10 5 10.00 34.40 -3 10 -5 52.49 29.80 4 -10 5 38.60 3.80 4 10 5 39.20 6.80 -5 -10 -5 24.30 50.29 5 10 5 0.00 84.39 -5 10 -5 32.30 55.49 5 11 -5 6.40 4.50 4 -11 -5 18.00 5.00 3 -11 -5 51.89 4.60 2 -11 -5 27.20 3.50 1 -11 -5 77.29 7.60 -1 11 5 83.29 4.90 1 11 -5 75.49 5.30 0 -11 -5 -2.40 3.20 0 11 -5 1.70 1.00 0 11 5 1.00 2.40 -1 -11 -5 451.65 17.00 2 11 5 15.50 3.50 3 -11 5 -4.60 26.80 -3 11 -5 8.10 23.10 3 11 5 20.30 42.60 4 -11 5 22.30 2.80 4 11 5 11.50 7.90 -5 -11 -5 4.40 56.49 5 11 5 -17.80 90.19 -5 11 -5 -22.50 48.30 4 -12 -5 15.20 5.50 3 -12 -5 30.80 4.40 2 -12 -5 14.70 3.90 1 -12 -5 4.40 3.40 -1 12 5 6.90 2.80 1 12 -5 -0.40 2.70 0 12 -5 0.00 1.20 0 12 5 0.20 2.60 -1 -12 -5 164.28 9.40 1 12 5 177.08 7.70 2 12 5 35.00 4.90 3 12 5 12.10 4.50 4 -12 5 23.00 3.10 4 -13 -5 16.50 5.30 3 -13 -5 30.20 4.50 -3 13 5 19.90 4.20 2 -13 -5 17.60 3.70 1 -13 -5 21.70 3.80 1 13 -5 24.40 3.20 0 -13 -5 -1.80 3.60 0 13 5 1.70 2.90 0 13 -5 0.70 1.40 -1 -13 -5 275.97 13.10 1 13 5 268.27 10.80 2 -13 5 48.20 57.69 -2 13 -5 38.10 18.80 2 13 5 -10.40 30.00 3 13 5 7.70 5.60 4 -13 5 18.80 3.70 4 -14 -5 15.50 6.30 3 -14 -5 51.09 6.10 2 -14 -5 17.10 4.80 2 14 -5 19.50 4.80 1 -14 -5 24.00 4.70 1 14 -5 39.50 3.50 0 -14 -5 -3.20 4.40 0 14 -5 4.30 1.60 -1 -14 -5 2.10 5.60 2 14 5 4.70 4.30 3 14 5 65.19 7.00 -4 -14 -5 3.10 79.99 4 14 5 17.40 59.89 -4 14 -5 42.20 40.40 4 -15 -5 -0.80 52.49 3 -15 -5 32.50 6.10 2 -15 -5 -5.20 4.60 2 15 -5 5.30 4.80 1 -15 -5 24.70 5.20 1 15 -5 19.40 3.40 0 -15 -5 -1.70 5.00 0 15 -5 2.90 1.80 -1 -15 -5 110.99 9.70 1 15 5 109.79 7.50 2 15 5 -1.40 5.00 -3 -15 -5 13.90 61.79 -3 15 -5 49.70 28.90 3 15 5 21.80 54.89 -4 -15 -5 -70.79 84.19 4 15 5 -45.40 64.69 -4 15 -5 26.10 39.60 3 -16 -5 28.50 6.40 3 16 -5 26.10 8.50 2 -16 -5 11.70 4.80 2 16 -5 5.40 4.90 1 -16 -5 13.90 4.80 1 16 -5 17.50 3.60 0 -16 -5 5.90 4.90 0 16 -5 -0.80 2.00 1 16 5 39.50 5.30 2 16 5 8.20 5.00 -3 -16 -5 50.29 76.99 3 16 5 -38.30 59.19 -3 16 -5 25.80 29.00 3 -17 -5 6.90 7.20 3 17 -5 2.80 7.40 2 -17 -5 3.20 5.90 2 17 -5 -2.20 4.80 1 -17 -5 63.29 7.10 -1 17 5 39.30 5.80 1 17 -5 54.19 4.60 0 -17 -5 -3.00 5.90 0 17 -5 -0.30 2.30 0 17 5 6.00 4.40 -1 17 -5 15.80 1.70 -2 -17 -5 -27.70 58.99 2 17 5 -0.90 46.00 -2 17 -5 -1.70 20.50 -3 -17 -5 19.10 66.99 -3 17 -5 3.20 28.20 3 17 5 -6.40 56.19 3 18 -5 9.40 8.80 2 -18 -5 9.50 6.80 2 18 -5 6.90 5.40 1 -18 -5 49.40 6.60 0 -18 -5 12.80 7.20 -1 18 -5 16.10 2.00 -2 -18 -5 14.60 66.69 2 18 5 -36.80 57.99 -2 18 -5 34.30 21.70 -3 -18 -5 3.70 79.59 -3 18 -5 -19.70 30.40 3 18 5 -4.50 63.09 2 -19 -5 -1.40 7.60 2 19 -5 7.70 5.90 1 -19 -5 29.30 8.10 1 19 -5 39.10 4.70 0 -19 -5 -0.90 7.20 0 19 -5 -3.70 2.90 -1 19 -5 32.50 3.00 -2 -19 -5 -26.70 63.49 2 19 5 7.70 66.19 -2 19 -5 0.80 21.40 2 20 -5 5.90 6.80 1 -20 -5 16.20 8.40 1 20 -5 14.30 5.40 0 -20 -5 -1.20 9.40 -1 -20 -5 -2.10 66.09 -1 -20 -5 49.00 25.10 -2 -20 -5 22.90 72.49 2 20 5 -3.80 64.99 1 -21 -5 53.69 68.19 0 -21 -5 65.49 70.69 0 -21 -5 -12.30 35.10 -1 -21 -5 6.30 73.69 -1 -21 -5 51.09 34.50 5 0 -6 2.10 4.60 4 0 -6 27.70 3.70 3 0 -6 4.90 2.70 2 0 -6 0.30 1.90 -1 0 6 3.10 1.20 1 0 -6 3.80 1.60 0 0 -6 59.89 3.40 0 0 6 58.19 2.70 1 0 6 0.10 1.20 2 0 6 5.50 1.80 3 0 6 -11.80 34.30 -3 0 -6 -1.20 46.40 -4 0 -6 -9.80 74.49 4 0 6 25.90 52.49 -5 0 -6 50.49 96.29 5 0 6 33.20 105.19 5 -1 -6 8.60 5.00 5 1 -6 2.00 4.50 4 -1 -6 16.40 3.70 4 1 -6 21.20 3.50 3 1 -6 2.80 2.20 2 -1 -6 46.40 3.70 2 1 -6 42.80 3.40 1 -1 -6 6.60 1.70 -1 1 6 4.50 1.40 1 1 -6 3.30 1.40 0 -1 6 484.35 14.70 0 -1 -6 477.05 15.20 0 1 6 468.35 14.90 0 1 -6 471.05 15.00 1 -1 6 4.50 1.00 1 1 6 5.70 1.40 2 -1 6 171.18 6.00 2 1 6 170.08 6.40 3 -1 6 -1.70 2.40 3 1 6 0.10 2.70 4 -1 6 -5.10 53.39 -4 -1 -6 90.59 67.69 -4 1 -6 7.80 68.69 4 1 6 -2.90 57.49 -5 -1 -6 -17.40 86.99 -5 1 -6 71.49 91.29 5 1 6 -51.09 76.19 5 -2 -6 5.80 5.10 5 2 -6 2.30 4.40 4 -2 -6 5.40 3.40 4 2 -6 5.80 3.10 3 -2 -6 -1.10 3.00 3 2 -6 2.40 2.30 2 -2 -6 62.49 3.90 -2 2 6 60.69 3.50 2 2 -6 61.79 3.50 1 -2 -6 2.30 1.80 -1 2 6 1.80 1.30 1 2 -6 0.20 1.40 0 -2 -6 116.39 5.00 0 2 6 116.39 4.50 0 2 -6 107.39 4.40 1 -2 6 0.00 0.70 1 2 6 0.60 1.50 2 2 6 158.38 6.20 3 -2 6 5.00 2.50 3 2 6 -2.20 3.00 -4 -2 -6 24.60 64.39 4 -2 6 28.10 65.49 -4 2 -6 -10.90 64.59 4 2 6 38.10 50.39 5 -2 6 2.20 2.90 5 -3 -6 -2.30 4.40 5 3 -6 -6.00 4.30 4 -3 -6 63.29 6.30 4 3 -6 69.29 5.50 3 -3 -6 1.40 2.70 3 3 -6 0.50 2.10 2 -3 -6 174.48 6.80 2 3 -6 162.58 6.30 -2 3 6 166.68 6.30 1 -3 -6 2.00 2.00 1 3 -6 3.60 1.30 -1 3 6 3.30 1.40 0 -3 -6 116.39 5.30 0 3 6 117.79 4.70 0 3 -6 122.79 4.40 -1 -3 -6 -0.90 2.80 1 3 6 -0.60 1.50 2 3 6 64.69 4.00 3 -3 6 5.90 2.30 3 3 6 0.80 2.90 4 -3 6 72.79 3.90 5 -3 6 -5.20 3.00 5 3 6 5.00 9.00 5 -4 -6 -0.40 5.20 5 4 -6 1.90 4.40 4 -4 -6 26.50 3.80 4 4 -6 16.60 3.30 3 -4 -6 5.30 2.80 3 4 -6 -1.10 2.20 2 -4 -6 390.56 13.40 2 4 -6 397.86 12.80 -2 4 6 393.76 13.10 1 -4 -6 1.00 1.90 1 4 -6 2.30 1.20 -1 4 6 -0.50 1.60 0 -4 -6 50.19 3.80 0 4 -6 49.90 2.50 0 4 6 56.89 3.20 -1 -4 -6 2.00 2.90 1 4 6 4.40 1.70 2 4 6 48.90 4.10 3 -4 6 0.40 2.00 3 -4 6 2.30 1.20 4 -4 6 33.60 3.30 5 4 6 -19.20 7.40 5 -5 -6 14.80 5.60 5 5 -6 6.90 4.50 4 -5 -6 33.70 4.20 4 5 -6 35.30 3.70 3 -5 -6 -0.40 2.90 3 5 -6 2.80 2.20 2 -5 -6 21.10 2.90 2 5 -6 22.30 2.10 -2 5 6 23.10 2.70 1 -5 -6 1.20 2.30 1 5 -6 2.10 1.30 0 -5 -6 318.17 11.10 0 5 6 310.17 10.60 -1 -5 -6 5.80 3.20 1 5 6 6.20 2.10 2 5 6 410.16 14.40 3 -5 6 -2.50 1.70 3 -5 6 -0.10 1.00 4 -5 6 22.00 2.30 5 -5 6 6.20 3.30 5 5 6 3.50 8.20 5 -6 -6 -3.30 5.80 5 6 -6 -5.90 4.60 4 -6 -6 50.29 5.10 4 6 -6 53.59 5.20 3 -6 -6 2.00 3.10 3 6 -6 1.60 2.10 2 -6 -6 193.88 7.80 2 6 -6 197.98 7.00 1 -6 -6 21.10 2.80 1 6 -6 16.20 1.50 -1 6 6 14.90 2.10 0 -6 -6 113.79 6.10 0 6 6 126.89 5.30 -1 -6 -6 3.40 3.60 1 6 6 3.50 2.20 2 -6 6 17.60 38.70 -2 6 -6 67.09 30.10 2 6 6 -16.40 27.60 3 -6 6 -29.60 48.70 -3 -6 -6 -10.60 32.00 -3 6 -6 -26.60 34.50 3 6 6 13.90 34.50 4 -6 6 19.90 2.30 -5 -6 -6 31.40 66.19 -5 6 -6 -48.30 69.29 5 6 6 28.20 105.09 5 7 -6 7.30 4.90 4 -7 -6 10.40 4.60 4 7 -6 18.40 3.30 3 -7 -6 -4.80 3.30 3 7 -6 1.90 2.00 -2 7 6 10.80 2.20 2 7 -6 6.50 1.70 1 -7 -6 1.80 2.60 -1 7 6 1.70 1.90 1 7 -6 1.80 1.20 0 -7 -6 467.55 16.00 -1 -7 -6 32.80 4.20 1 7 6 34.60 3.60 -2 7 -6 55.99 26.40 2 7 6 2.80 29.50 -3 -7 -6 -1.10 45.50 3 -7 6 -5.20 47.50 -3 7 -6 5.70 33.60 3 7 6 23.70 42.70 4 -7 6 10.00 3.70 4 -7 6 15.10 2.00 -5 -7 -6 21.10 46.50 -5 7 -6 -2.70 72.29 5 8 -6 2.30 4.50 4 -8 -6 33.40 5.30 4 8 -6 36.50 3.80 3 -8 -6 1.30 3.70 3 8 -6 6.50 2.40 2 -8 -6 113.69 6.50 -2 8 6 110.99 5.60 2 8 -6 113.19 4.70 1 -8 -6 31.50 3.50 -1 8 6 32.70 2.80 1 8 -6 29.30 2.20 0 -8 -6 195.78 8.90 0 8 6 215.48 7.90 -1 -8 -6 5.80 3.90 1 8 6 10.60 2.50 -2 -8 -6 18.90 36.10 2 8 6 9.00 29.00 3 -8 6 1.00 45.20 -3 -8 -6 -40.70 43.40 3 8 6 5.50 36.60 -3 8 -6 -10.90 31.90 4 -8 6 28.40 3.80 4 -8 6 30.70 2.40 4 8 6 25.50 6.70 -5 -8 -6 -19.10 50.69 4 -9 -6 24.40 5.40 4 9 -6 20.50 3.80 3 -9 -6 6.70 3.90 3 9 -6 2.90 2.40 -3 9 6 5.80 3.40 2 -9 -6 7.50 3.10 -2 9 6 15.20 2.60 2 9 -6 10.80 2.00 1 -9 -6 10.00 3.30 -1 9 6 12.30 2.20 1 9 -6 13.20 1.40 0 -9 -6 38.90 4.20 -1 -9 -6 45.60 5.20 -2 -9 -6 -31.80 35.40 2 9 6 -2.60 26.50 -2 9 -6 56.29 22.80 3 -9 6 -11.80 44.20 -3 -9 -6 13.10 50.09 3 9 6 2.40 36.90 -3 9 -6 31.20 31.20 4 9 6 5.20 6.20 4 -10 -6 19.50 5.90 4 10 -6 15.50 3.50 3 -10 -6 2.90 3.70 3 10 -6 4.80 2.90 -3 10 6 8.40 3.80 2 -10 -6 65.89 5.20 2 10 -6 64.89 3.70 1 -10 -6 39.00 4.10 1 10 -6 38.20 2.30 -1 10 6 35.20 3.30 0 -10 -6 78.89 6.30 -1 -10 -6 21.90 5.40 -2 -10 -6 -20.50 37.90 2 10 6 -17.40 32.20 -2 10 -6 66.99 23.70 3 -10 6 40.00 44.60 -3 -10 -6 -47.00 62.39 3 10 6 -6.40 40.70 -3 10 -6 21.40 30.00 -4 -10 -6 17.80 64.39 -4 10 -6 35.20 46.00 4 10 6 1.20 68.39 4 -11 -6 18.30 5.40 4 11 -6 10.90 3.40 3 -11 -6 8.20 4.90 -3 11 6 7.30 3.60 2 -11 -6 44.80 4.90 2 11 -6 39.40 3.30 1 -11 -6 19.80 4.20 1 11 -6 23.50 2.20 -1 11 6 18.00 3.20 1 11 -6 16.40 3.10 0 -11 -6 193.48 9.20 0 11 6 190.48 7.90 -1 -11 -6 30.50 5.50 -2 -11 -6 11.10 41.00 2 11 6 -14.90 31.40 3 11 6 5.30 5.40 -4 -11 -6 38.80 74.69 4 11 6 -28.70 60.79 -4 11 -6 -19.00 44.30 4 -12 -6 11.20 6.60 4 12 -6 8.90 4.00 3 -12 -6 0.40 4.20 3 12 -6 3.80 2.60 2 -12 -6 21.90 4.10 -2 12 6 23.10 3.90 1 -12 -6 20.30 4.40 1 12 -6 26.70 3.30 1 12 -6 21.70 1.80 0 -12 -6 149.99 8.90 -1 -12 -6 26.20 5.80 -2 -12 -6 13.80 44.60 2 12 6 -16.40 31.80 -2 12 -6 51.29 22.30 3 12 6 9.70 5.30 -4 -12 -6 -51.39 80.29 4 12 6 39.50 68.59 -4 12 -6 29.50 38.90 4 13 -6 9.20 3.90 3 -13 -6 -7.20 5.50 2 -13 -6 12.30 4.80 -2 13 6 2.10 3.30 1 -13 -6 23.10 4.30 -1 13 6 21.20 4.50 1 13 -6 19.40 3.20 0 -13 -6 4.60 4.60 -1 -13 -6 12.20 6.00 2 13 6 25.50 4.90 -3 -13 -6 7.10 66.19 -3 13 -6 -1.30 29.80 3 13 6 2.40 58.49 -4 -13 -6 32.70 79.99 4 13 6 -67.19 90.09 -4 13 -6 38.80 43.50 3 -14 -6 8.80 6.10 2 -14 -6 16.30 5.20 2 14 -6 8.60 5.70 1 -14 -6 -1.90 5.00 -1 14 6 0.50 3.80 1 14 -6 -0.60 3.10 0 -14 -6 8.80 5.40 0 14 6 3.30 3.60 -1 -14 -6 20.00 6.00 1 14 6 15.40 4.40 2 14 6 28.30 4.80 -3 -14 -6 40.30 81.59 3 14 6 4.40 61.49 -3 14 -6 -10.00 29.90 3 -15 -6 13.60 6.00 2 -15 -6 62.89 7.20 2 15 -6 73.69 6.50 1 -15 -6 18.40 6.00 -1 15 6 20.00 3.90 1 15 -6 22.20 3.30 0 -15 -6 47.10 6.70 0 15 6 48.00 5.00 1 15 6 11.80 4.70 -2 -15 -6 -15.10 53.99 -2 15 -6 15.20 18.50 2 15 6 -12.70 44.80 -3 -15 -6 -70.49 72.39 3 15 6 58.49 68.79 -3 15 -6 6.10 30.50 3 16 -6 13.90 8.60 2 -16 -6 -6.60 5.70 2 16 -6 10.40 5.30 1 -16 -6 10.50 5.50 1 16 -6 -3.00 3.00 0 -16 -6 23.10 6.20 1 -16 6 11.00 30.40 -1 -16 -6 3.10 52.79 1 16 6 13.30 42.90 -1 16 -6 17.80 15.60 -2 -16 -6 -55.09 66.89 -2 16 -6 21.60 20.90 2 16 6 42.80 58.79 -3 -16 -6 15.60 81.09 -3 16 -6 7.50 31.70 2 -17 -6 17.80 7.40 2 17 -6 2.30 5.70 1 -17 -6 14.30 7.20 1 17 -6 7.30 3.40 0 -17 -6 -2.90 7.20 -1 -17 -6 12.50 52.69 -1 17 -6 1.00 16.40 1 17 6 15.20 53.89 -2 -17 -6 11.90 75.49 -2 17 -6 -5.80 22.50 2 17 6 -18.70 62.19 2 -18 -6 7.40 49.60 1 -18 -6 4.50 8.30 0 -18 -6 53.49 9.80 -1 -18 -6 -36.40 65.39 -2 -18 -6 2.10 82.59 1 -19 -6 -7.90 9.50 0 -19 -6 32.30 10.40 -1 -19 -6 29.50 65.69 0 -20 -6 8.60 74.99 5 0 -7 35.80 6.30 4 0 -7 -0.70 3.70 3 0 -7 18.50 3.10 2 0 -7 3.50 2.40 1 0 -7 106.99 4.90 -1 0 7 100.99 4.20 0 0 7 0.70 1.30 0 0 -7 1.30 2.10 1 0 7 55.29 2.70 2 0 7 4.70 1.70 3 0 7 -11.30 45.60 -3 0 -7 -20.40 60.19 4 0 7 -4.70 79.49 -4 0 -7 16.00 88.09 5 -1 -7 8.50 5.90 5 1 -7 29.00 6.10 4 -1 -7 6.10 4.00 4 1 -7 3.40 3.80 3 -1 -7 0.50 2.80 3 1 -7 3.00 3.00 2 -1 -7 -0.60 2.50 2 1 -7 7.30 2.30 1 -1 -7 17.70 2.40 -1 1 7 14.40 1.90 1 1 -7 17.50 2.30 0 -1 7 -1.20 1.10 0 -1 -7 -1.50 2.20 0 1 7 1.50 1.30 0 1 -7 0.10 2.00 1 -1 7 72.69 3.00 1 1 7 69.19 3.50 2 -1 7 1.80 1.50 2 1 7 1.40 2.10 -3 -1 -7 -8.40 39.60 3 -1 7 -33.70 44.50 -3 1 -7 51.39 55.09 3 1 7 44.50 47.80 -4 -1 -7 18.90 91.49 4 1 7 -1.30 75.59 -4 1 -7 -30.70 66.89 4 -2 -7 4.20 4.30 4 2 -7 0.20 3.70 3 -2 -7 76.09 5.70 3 2 -7 78.89 5.30 2 -2 -7 7.30 2.50 2 2 -7 9.30 2.20 1 -2 -7 32.00 2.70 -1 2 7 26.10 2.30 1 2 -7 27.40 2.30 0 -2 -7 0.50 2.30 0 2 -7 3.50 1.80 0 2 7 1.40 1.40 1 -2 7 4.00 1.00 1 2 7 4.30 1.70 2 -2 7 2.70 1.20 3 -2 7 56.69 3.70 -4 -2 -7 -1.30 73.69 4 2 7 45.00 67.99 -4 2 -7 13.20 77.69 4 -3 -7 8.30 4.40 4 3 -7 11.50 4.10 3 -3 -7 36.80 4.00 3 3 -7 32.40 3.80 2 -3 -7 10.60 2.70 2 3 -7 7.60 2.20 1 -3 -7 56.79 4.30 1 3 -7 46.90 3.40 0 -3 -7 0.00 2.50 0 3 7 0.80 1.70 0 3 -7 -1.20 1.70 1 3 7 40.40 3.20 2 3 7 2.10 2.30 3 -3 7 47.60 3.10 4 -3 7 9.60 2.00 4 -4 -7 4.40 4.40 4 4 -7 7.10 4.00 3 -4 -7 45.90 4.40 2 -4 -7 2.20 2.80 2 4 -7 4.10 2.00 1 -4 -7 18.70 3.00 1 4 -7 13.30 1.90 0 -4 -7 -1.10 2.70 0 4 7 -1.60 1.80 0 4 -7 -1.30 1.50 1 4 7 3.10 2.00 2 4 7 5.00 2.30 -3 -4 -7 19.60 32.10 3 -4 7 4.30 54.09 -3 4 -7 43.30 49.60 3 4 7 9.70 39.20 4 -4 7 10.90 3.80 4 -4 7 9.90 2.10 4 -5 -7 13.50 4.90 4 5 -7 6.30 4.00 3 -5 -7 77.49 6.80 2 -5 -7 11.30 3.10 2 5 -7 6.00 1.90 1 -5 -7 86.29 5.30 1 5 -7 84.69 3.90 0 -5 -7 -1.00 2.70 -1 -5 -7 115.19 7.70 1 5 7 128.99 6.20 -2 -5 -7 27.20 33.40 -2 5 -7 15.40 31.00 2 5 7 1.00 31.60 3 -5 7 14.00 56.49 -3 -5 -7 35.20 39.30 3 5 7 -39.70 45.40 -3 5 -7 53.59 46.00 4 -5 7 6.20 2.10 4 -6 -7 6.40 4.50 4 6 -7 8.70 3.90 3 -6 -7 191.08 9.20 -3 6 7 188.38 8.40 2 -6 -7 5.00 3.20 2 6 -7 0.10 2.10 1 -6 -7 10.90 3.00 1 6 -7 5.80 1.60 0 -6 -7 0.00 3.20 -1 -6 -7 48.20 5.20 -2 -6 -7 16.40 44.40 -2 6 -7 26.50 32.80 2 6 7 33.40 33.30 3 -6 7 -1.60 60.89 -3 -6 -7 12.90 44.10 3 6 7 3.50 42.90 -3 6 -7 121.89 47.10 -4 -6 -7 0.30 44.00 -4 6 -7 -22.00 57.69 4 -7 -7 7.00 5.70 4 7 -7 3.80 3.60 3 -7 -7 22.00 4.50 -3 7 7 19.10 3.80 2 -7 -7 11.80 3.50 2 7 -7 6.50 2.20 1 -7 -7 48.40 4.50 1 7 -7 41.00 2.80 0 -7 -7 7.80 3.30 -1 -7 -7 72.99 5.70 -2 -7 -7 -3.60 50.29 2 7 7 4.50 33.90 -2 7 -7 8.50 27.30 3 -7 7 20.90 64.79 -3 -7 -7 -11.50 41.80 -3 7 -7 -8.00 32.40 3 7 7 -24.40 51.09 -4 -7 -7 -33.50 50.89 -4 7 -7 8.40 57.79 4 -8 -7 21.30 5.90 4 8 -7 12.40 4.10 3 -8 -7 34.30 4.70 -3 8 7 39.00 4.30 2 -8 -7 0.10 3.50 2 8 -7 0.50 2.10 1 -8 -7 48.30 4.50 1 8 -7 46.30 2.80 0 -8 -7 -1.40 3.50 -1 -8 -7 51.89 5.60 -2 -8 -7 9.90 45.20 2 8 7 27.00 37.40 -2 8 -7 23.20 28.00 -3 -8 -7 35.50 49.30 -3 8 -7 14.30 38.80 3 8 7 9.00 53.99 4 8 7 -7.60 6.30 4 -9 -7 4.30 6.10 4 9 -7 4.20 3.80 3 -9 -7 5.30 4.90 -3 9 7 8.30 4.40 3 9 -7 5.20 3.30 2 -9 -7 7.70 4.10 2 9 -7 6.40 2.10 1 -9 -7 69.49 6.60 1 9 -7 75.89 3.40 0 -9 -7 -2.90 3.80 -1 -9 -7 41.80 5.90 -2 -9 -7 21.70 53.89 -2 9 -7 -20.10 23.10 2 9 7 10.80 39.10 -3 -9 -7 6.10 61.89 -3 9 -7 8.40 35.50 3 9 7 7.90 54.29 -4 -9 -7 24.50 64.99 -4 9 -7 13.90 49.90 4 -10 -7 -10.90 6.60 4 10 -7 -3.70 4.30 3 -10 -7 25.60 5.50 3 10 -7 17.80 3.10 2 -10 -7 7.00 4.30 -2 10 7 -0.60 3.40 2 10 -7 1.20 2.10 1 -10 -7 -4.60 3.90 1 10 -7 2.70 1.50 0 -10 -7 -1.40 4.20 -1 -10 -7 167.68 10.70 -2 -10 -7 -43.70 55.59 -2 10 -7 14.40 23.20 2 10 7 -22.70 42.20 3 10 7 8.20 5.70 -4 -10 -7 -18.20 61.89 -4 10 -7 -32.30 51.29 4 11 -7 -1.30 4.00 3 -11 -7 7.90 5.70 3 11 -7 5.10 3.10 2 -11 -7 2.20 4.70 -2 11 7 2.10 3.80 2 11 -7 5.30 2.30 1 -11 -7 67.59 5.90 1 11 -7 59.29 4.90 1 11 -7 57.99 3.10 0 -11 -7 -8.80 4.40 -1 -11 -7 52.29 6.90 2 -11 7 17.00 43.20 -2 -11 -7 42.60 55.09 2 11 7 8.60 44.90 -2 11 -7 -1.10 24.90 3 11 7 5.30 5.50 3 -12 -7 12.10 6.30 3 12 -7 9.00 3.20 2 -12 -7 0.60 5.30 -2 12 7 7.20 4.70 2 12 -7 -1.10 2.20 1 -12 -7 8.50 4.30 1 12 -7 9.10 2.60 1 12 -7 10.00 1.70 -1 12 7 9.10 3.90 0 -12 -7 -0.60 5.10 0 12 7 3.00 4.10 -1 -12 -7 -4.70 6.30 2 12 7 5.00 4.60 -3 -12 -7 -4.00 79.99 -3 12 -7 3.20 33.60 3 -13 -7 27.00 7.10 3 13 -7 25.00 3.90 2 -13 -7 6.20 5.00 2 13 -7 0.40 2.40 1 -13 -7 5.50 4.80 -1 13 7 7.60 4.20 1 13 -7 4.40 1.60 1 13 -7 2.80 2.70 0 -13 -7 2.10 5.80 0 13 7 -2.00 4.10 -1 -13 -7 9.50 7.00 1 13 7 10.40 4.50 2 13 7 -2.20 6.10 -3 -13 -7 52.59 85.39 -3 13 -7 19.00 34.70 3 14 -7 8.10 3.70 2 -14 -7 16.80 6.70 2 14 -7 2.90 2.70 1 -14 -7 4.00 6.10 1 14 -7 9.20 2.70 1 14 -7 7.00 1.90 0 -14 -7 -9.50 6.30 0 14 7 -0.50 3.80 1 14 7 6.80 5.60 -2 -14 -7 53.59 76.09 -3 -14 -7 -12.20 87.69 2 -15 -7 6.00 7.20 2 15 -7 6.90 7.70 2 15 -7 -2.70 2.70 1 -15 -7 21.40 7.00 1 15 -7 7.60 2.00 1 15 -7 5.20 2.70 0 -15 -7 2.60 7.40 -1 -15 -7 14.80 53.09 -1 15 -7 6.30 16.80 -2 -15 -7 -34.40 66.89 -2 15 -7 0.50 24.00 2 -16 -7 -24.30 7.90 2 16 -7 -0.40 2.80 1 -16 -7 -6.60 7.60 0 -16 -7 -3.50 7.80 -1 -16 -7 -8.80 66.69 -1 16 -7 -7.90 17.30 -2 -16 -7 65.49 89.29 1 -17 -7 13.20 9.00 0 -17 -7 8.40 9.30 -1 -17 -7 -16.80 65.29 -1 17 -7 22.50 19.80 0 -18 -7 -17.20 67.99 4 0 -8 6.70 4.80 3 0 -8 -3.30 3.20 2 0 -8 2.20 2.90 1 0 -8 6.10 2.70 0 0 -8 -0.60 2.80 1 0 8 7.40 1.60 2 0 8 3.60 2.10 -3 0 -8 -17.80 79.59 -4 0 -8 19.60 103.39 4 -1 -8 4.30 5.00 4 1 -8 2.90 4.60 3 -1 -8 0.90 3.50 3 1 -8 1.50 3.10 2 -1 -8 -1.20 3.00 2 1 -8 -0.50 2.70 1 -1 -8 9.30 2.90 1 1 -8 -0.10 2.60 0 -1 -8 39.90 3.80 0 1 8 50.49 4.90 0 1 -8 48.80 4.40 1 -1 8 4.80 1.40 2 -1 8 3.90 1.50 -3 -1 -8 34.60 72.39 -3 1 -8 60.89 72.49 -4 -1 -8 60.49 111.99 -4 1 -8 12.00 93.09 4 -2 -8 16.40 5.80 4 2 -8 15.30 4.70 3 -2 -8 -1.30 3.70 3 2 -8 1.80 3.40 2 2 -8 2.50 2.60 1 -2 -8 11.60 2.90 1 2 -8 10.80 2.50 0 -2 -8 22.40 3.40 0 2 8 24.00 2.40 0 2 -8 21.50 2.80 1 2 8 11.50 1.90 -2 -2 -8 -7.90 23.00 -2 2 -8 -9.80 48.60 2 2 8 20.50 36.90 3 -2 8 1.80 1.90 -4 -2 -8 8.60 106.69 -4 2 -8 109.99 86.69 4 -3 -8 3.00 6.20 4 3 -8 0.70 5.00 3 -3 -8 -4.20 4.00 3 3 -8 2.60 3.40 2 -3 -8 5.60 3.20 2 3 -8 7.50 2.70 1 -3 -8 24.90 3.60 1 3 -8 20.90 2.70 0 -3 -8 47.90 4.10 0 3 -8 41.20 3.00 0 3 8 39.60 3.30 1 3 8 13.10 2.30 -2 -3 -8 11.00 29.30 2 3 8 16.20 36.50 -2 3 -8 45.90 44.40 -3 -3 -8 -20.80 32.70 -3 3 -8 -23.60 58.29 -4 -3 -8 -72.29 99.69 -4 3 -8 44.20 82.29 4 -4 -8 -5.90 5.70 4 4 -8 -0.20 4.40 3 -4 -8 8.80 4.40 3 4 -8 3.60 3.30 2 -4 -8 107.29 7.20 -2 4 8 104.49 6.50 2 4 -8 94.99 5.40 1 -4 -8 11.60 3.10 1 4 -8 15.20 2.40 0 -4 -8 28.50 3.90 -1 -4 -8 36.60 35.50 -1 4 -8 39.00 31.10 -2 -4 -8 -21.00 33.10 -2 4 -8 -19.70 37.50 2 4 8 19.00 37.70 -3 -4 -8 5.60 37.20 -3 4 -8 -7.40 54.69 -4 -4 -8 0.30 64.99 -4 4 -8 6.90 74.89 4 -5 -8 14.60 6.30 4 5 -8 8.00 5.00 3 -5 -8 6.10 4.40 3 5 -8 -0.50 3.30 2 -5 -8 47.00 4.60 2 5 -8 43.30 4.20 1 -5 -8 37.50 4.40 1 5 -8 35.30 2.80 0 -5 -8 76.99 6.20 1 -5 8 -5.60 29.80 -1 -5 -8 21.50 47.70 -1 5 -8 26.90 29.60 2 -5 8 13.00 45.40 -2 -5 -8 70.49 44.00 -2 5 -8 117.19 44.40 -3 -5 -8 5.60 40.60 -3 5 -8 -13.80 49.30 -4 -5 -8 -18.00 52.49 -4 5 -8 8.00 75.59 4 -6 -8 17.20 6.40 4 6 -8 -2.70 4.80 3 -6 -8 1.00 4.80 3 6 -8 5.00 3.50 2 -6 -8 14.00 4.20 2 6 -8 23.20 2.80 1 -6 -8 4.70 4.10 1 6 -8 6.80 2.10 0 -6 -8 33.30 4.40 -1 -6 -8 -37.80 49.60 1 -6 8 18.00 31.40 -1 6 -8 -15.10 26.20 2 -6 8 17.80 46.90 -2 -6 -8 -13.00 47.60 2 6 8 11.50 41.90 -2 6 -8 37.80 33.30 -3 -6 -8 12.10 43.10 -3 6 -8 8.10 53.79 4 6 8 4.10 7.90 3 -7 -8 2.50 5.30 3 7 -8 7.30 3.30 2 -7 -8 24.10 5.10 -2 7 8 19.30 4.40 2 7 -8 35.70 3.10 1 -7 -8 27.40 4.30 1 7 -8 26.80 2.40 0 -7 -8 7.90 35.60 0 7 -8 24.30 12.80 1 -7 8 -6.50 33.00 -1 -7 -8 -18.60 45.50 1 7 8 1.90 30.40 -1 7 -8 27.50 22.20 -2 -7 -8 11.30 55.79 -2 7 -8 41.10 36.50 2 7 8 16.70 42.90 -3 -7 -8 -14.40 55.99 -3 7 -8 -26.20 50.79 3 -8 -8 -4.90 5.50 3 8 -8 -2.10 3.50 2 -8 -8 13.00 4.70 2 8 -8 6.30 2.60 -2 8 8 9.90 3.80 1 -8 -8 2.30 4.20 1 8 -8 3.30 1.90 0 -8 -8 112.39 8.80 -1 -8 -8 13.90 49.20 1 -8 8 10.80 41.20 1 8 8 -4.00 33.60 -1 8 -8 5.30 19.90 -2 -8 -8 30.60 65.89 -2 8 -8 9.30 31.90 -3 -8 -8 -28.00 62.19 -3 8 -8 -10.90 43.90 3 -9 -8 -4.20 5.80 3 9 -8 -1.70 3.50 2 -9 -8 7.60 5.10 2 9 -8 6.60 2.60 -2 9 8 13.50 4.00 1 -9 -8 14.20 5.20 0 -9 -8 84.49 8.40 -1 -9 -8 -45.80 51.49 1 -9 8 -6.50 39.90 -1 9 -8 19.10 20.70 1 9 8 4.80 34.90 -2 -9 -8 -0.80 70.69 -2 9 -8 23.70 32.00 3 9 8 3.00 5.20 3 -10 -8 -3.50 6.60 3 10 -8 4.90 3.70 2 -10 -8 24.60 5.90 1 -10 -8 5.20 5.10 -1 10 8 -0.60 3.70 0 -10 -8 87.69 7.20 1 -10 8 1.90 44.50 -1 -10 -8 6.20 56.09 -1 10 -8 10.10 18.60 2 10 8 14.30 4.50 -3 -10 -8 74.49 80.69 -3 10 -8 -1.20 44.40 3 -11 -8 -1.80 7.00 3 11 -8 4.70 3.50 2 -11 -8 12.30 5.90 2 11 -8 11.80 2.90 1 -11 -8 -2.90 5.40 -1 11 8 -1.10 4.10 0 -11 -8 14.50 6.00 0 11 8 13.90 4.30 1 11 8 2.80 4.30 2 11 8 5.70 5.50 -3 -11 -8 96.69 97.59 2 -12 -8 6.70 6.60 2 12 -8 3.60 2.80 1 -12 -8 9.20 6.30 0 -12 -8 18.60 6.50 0 12 8 10.70 4.80 1 12 8 18.40 5.40 -2 -12 -8 -1.70 84.39 -2 12 -8 15.80 29.20 2 -13 -8 21.20 7.80 1 -13 -8 -2.90 6.60 0 -13 -8 -3.30 7.50 -1 -13 -8 19.10 69.19 -1 13 -8 -2.90 16.40 -2 -13 -8 5.80 75.69 2 -14 -8 11.70 9.00 1 -14 -8 -3.10 7.50 0 -14 -8 12.50 8.00 -1 -14 -8 24.60 73.69 -1 14 -8 16.60 18.20 -2 -14 -8 40.90 79.29 1 -15 -8 1.10 8.50 0 -15 -8 7.90 9.10 -1 -15 -8 -41.00 78.09 0 -16 -8 4.90 10.10 3 0 -9 7.30 4.90 2 0 -9 6.30 3.70 1 0 -9 3.70 3.50 0 0 -9 -0.80 3.90 -1 0 -9 4.80 50.19 1 0 9 -3.50 32.30 2 0 9 -0.10 1.90 -3 0 -9 18.00 92.69 3 -1 -9 10.30 4.70 3 1 -9 5.80 4.70 2 -1 -9 -1.00 3.90 2 1 -9 3.00 4.40 1 -1 -9 -0.30 3.40 1 1 -9 4.80 3.40 0 -1 -9 -3.00 3.90 0 1 -9 0.60 3.40 1 -1 9 0.40 32.40 -1 -1 -9 -5.10 25.40 -1 1 -9 16.50 54.99 1 1 9 0.40 36.30 -2 -1 -9 21.90 57.09 -2 1 -9 -66.59 70.49 -3 -1 -9 -20.30 96.19 -3 1 -9 -44.90 77.99 3 -2 -9 -1.40 5.20 3 2 -9 8.40 4.50 2 -2 -9 1.80 4.20 2 2 -9 4.60 3.80 1 -2 -9 13.30 3.80 1 2 -9 1.90 3.20 0 -2 -9 -6.60 4.20 0 2 -9 -0.50 3.60 1 -2 9 -38.80 31.50 -1 -2 -9 13.50 26.90 -1 2 -9 12.20 48.90 -2 -2 -9 -0.90 34.00 -2 2 -9 -0.70 62.99 -3 -2 -9 34.40 88.69 -3 2 -9 33.30 77.49 3 -3 -9 -4.80 4.90 3 3 -9 4.70 4.40 2 -3 -9 8.20 4.60 2 3 -9 2.70 3.50 1 -3 -9 2.30 4.40 1 3 -9 4.50 3.20 0 -3 -9 8.80 4.50 1 -3 9 -16.80 31.00 -1 -3 -9 14.70 28.70 -1 3 -9 21.70 43.70 -2 -3 -9 20.60 31.50 -2 3 -9 1.80 51.09 -3 -3 -9 -37.60 60.89 -3 3 -9 -10.80 71.49 3 -4 -9 25.80 6.40 3 4 -9 18.90 4.50 2 -4 -9 5.70 5.00 2 4 -9 6.50 3.40 1 -4 -9 25.10 4.60 1 4 -9 17.90 3.20 0 -4 -9 3.50 4.40 -1 -4 -9 5.10 35.10 1 -4 9 -12.80 36.90 -1 4 -9 21.60 37.00 -2 -4 -9 31.30 37.40 -2 4 -9 22.10 45.30 -3 -4 -9 -11.60 43.20 3 -5 -9 -3.50 5.70 3 5 -9 3.80 4.50 2 -5 -9 4.40 4.80 -2 5 9 10.90 3.80 2 5 -9 10.40 3.60 1 -5 -9 9.00 4.80 1 5 -9 3.90 2.90 0 -5 -9 7.50 5.20 -1 -5 -9 43.10 47.90 -1 5 -9 -5.50 29.40 -2 -5 -9 14.00 44.20 -2 5 -9 19.50 41.20 -3 -5 -9 -9.60 49.70 3 -6 -9 3.40 6.10 3 6 -9 18.20 4.70 2 -6 -9 8.30 4.90 -2 6 9 5.50 3.70 2 6 -9 7.90 3.50 1 -6 -9 47.70 5.40 1 6 -9 49.00 4.60 0 -6 -9 6.30 5.30 -1 -6 -9 11.10 56.99 -1 6 -9 33.10 30.70 -2 -6 -9 36.50 53.19 -2 6 -9 -40.10 36.70 2 -7 -9 7.90 5.40 2 7 -9 10.20 3.60 1 -7 -9 1.70 4.90 1 7 -9 -1.40 2.50 -1 7 9 4.40 4.90 0 -7 -9 5.90 5.00 -1 -7 -9 11.20 58.39 -1 7 -9 43.70 28.50 -2 -7 -9 45.50 61.49 -2 7 -9 28.00 41.80 2 -8 -9 1.10 5.80 2 8 -9 5.70 3.10 1 -8 -9 20.70 5.70 -1 8 9 17.10 4.10 0 -8 -9 -1.20 5.50 -1 -8 -9 -87.39 63.79 -1 8 -9 -17.50 25.50 -2 -8 -9 -64.99 65.89 -2 8 -9 23.50 33.50 2 -9 -9 -4.00 6.40 1 -9 -9 2.40 6.70 -1 9 9 -1.20 4.60 0 -9 -9 -7.80 6.10 0 9 9 -4.00 3.80 -1 -9 -9 -27.00 67.89 -1 9 -9 21.50 24.10 2 9 9 0.60 5.50 2 -10 -9 8.80 7.10 1 -10 -9 -2.40 6.60 0 -10 -9 1.40 7.60 0 10 9 -1.10 4.90 1 10 9 8.40 5.00 1 -11 -9 -0.80 7.30 0 -11 -9 5.30 7.40 -1 -11 -9 19.80 78.79 -1 11 -9 33.00 22.30 1 -12 -9 3.40 8.90 0 -12 -9 -10.00 8.00 2 0 -10 -3.80 5.50 1 0 -10 -4.20 4.40 0 0 -10 3.30 5.20 -1 0 -10 23.80 76.29 2 -1 -10 -6.60 5.20 2 1 -10 -1.40 5.00 1 -1 -10 3.20 5.30 1 1 -10 -1.20 4.70 0 -1 -10 4.20 5.90 -1 -1 -10 18.40 67.99 -1 1 -10 -17.20 63.19 2 -2 -10 7.30 5.40 2 2 -10 2.80 4.70 1 -2 -10 6.40 5.50 1 2 -10 2.00 4.10 0 -2 -10 -1.10 6.10 -1 -2 -10 6.10 39.20 -1 2 -10 37.50 57.69 2 -3 -10 0.20 5.90 1 -3 -10 0.10 5.70 1 3 -10 1.50 6.70 0 -3 -10 1.80 6.30 -1 -3 -10 -40.80 30.90 -1 3 -10 13.70 49.10 1 -4 -10 -0.30 5.80 0 -4 -10 -0.60 6.50 -1 -4 -10 -22.80 40.70 -1 4 -10 30.20 42.20 1 -5 -10 24.70 6.40 -1 5 10 14.20 6.00 0 -5 -10 8.60 7.10 -1 5 -10 -18.80 36.70 1 -6 -10 5.40 6.70 -1 6 10 5.90 4.40 0 -6 -10 2.20 7.00 -1 6 -10 1.90 33.50 1 -7 -10 19.90 7.50 0 -7 -10 47.70 8.20 0 7 10 48.40 5.00 0 -8 -10 9.20 8.50 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp F3 F 0.0595(9) 0.3689(2) 0.7308(7) 0.0923(16) Uani 1 1 d . . O1 O 0.5911(8) 0.4713(3) 0.6350(8) 0.0848(18) Uani 1 1 d . . C7 C 0.3663(11) 0.4558(3) 0.6502(7) 0.0480(15) Uani 1 1 d . . F1' F 0.4404(10) -0.1324(2) 0.7656(8) 0.0951(17) Uani 1 1 d . . F1 F 0.4280(15) 0.3683(3) 0.8424(8) 0.128(3) Uani 1 1 d . . C8 C 0.3084(13) 0.3811(3) 0.7081(8) 0.0550(16) Uani 1 1 d . . F2 F 0.3789(14) 0.3343(2) 0.6031(8) 0.116(2) Uani 1 1 d . . F2' F 0.1257(15) -0.1677(2) 0.8956(8) 0.125(3) Uani 1 1 d . . F3' F 0.0671(16) -0.1323(4) 0.6591(9) 0.140(3) Uani 1 1 d . . C6 C 0.3623(11) 0.6133(3) 0.6299(7) 0.0465(14) Uani 1 1 d . . H6 H 0.493038 0.597033 0.701698 0.056 Uiso 1 1 calc R U C1 C 0.1702(10) 0.5676(3) 0.5726(6) 0.0385(13) Uani 1 1 d . . C3 C -0.0211(12) 0.6621(3) 0.4239(7) 0.0538(15) Uani 1 1 d . . H3 H -0.154236 0.678888 0.354487 0.065 Uiso 1 1 calc R U C5 C 0.3582(12) 0.6823(3) 0.5804(8) 0.0522(15) Uani 1 1 d . . H5 H 0.489018 0.713396 0.617495 0.063 Uiso 1 1 calc R U C2 C -0.0169(11) 0.5924(3) 0.4707(6) 0.0454(14) Uani 1 1 d . . H2 H -0.146248 0.561429 0.431263 0.055 Uiso 1 1 calc R U C4 C 0.1686(13) 0.7069(3) 0.4784(7) 0.0486(15) Uani 1 1 d . . H4 H 0.168475 0.754664 0.445637 0.058 Uiso 1 1 calc R U N1 N 0.1623(9) 0.4962(2) 0.6232(5) 0.0404(11) Uani 1 1 d . . H1 H 0.008949 0.477361 0.637704 0.048 Uiso 1 1 calc R U C2' C 0.5193(11) 0.1105(3) 0.8727(7) 0.0475(14) Uani 1 1 d . . H2' H 0.649634 0.093447 0.802558 0.057 Uiso 1 1 calc R U C5' C 0.1389(11) 0.1615(3) 1.0742(7) 0.0505(15) Uani 1 1 d . . H5' H 0.008524 0.179272 1.143382 0.061 Uiso 1 1 calc R U C3' C 0.5192(12) 0.1802(3) 0.9189(8) 0.0527(16) Uani 1 1 d . . H3' H 0.651648 0.210638 0.882097 0.063 Uiso 1 1 calc R U C1' C 0.3286(10) 0.0655(3) 0.9291(6) 0.0365(12) Uani 1 1 d . . C6' C 0.1357(11) 0.0913(3) 1.0312(6) 0.0451(14) Uani 1 1 d . . H6' H 0.004445 0.061068 1.07049 0.054 Uiso 1 1 calc R U O1' O -0.0934(8) -0.0313(2) 0.8708(8) 0.0776(16) Uani 1 1 d . . C4' C 0.3273(13) 0.2057(3) 1.0184(8) 0.0519(16) Uani 1 1 d . . H4' H 0.32591 0.253742 1.048133 0.062 Uiso 1 1 calc R U N1' N 0.3366(9) -0.0057(2) 0.8797(5) 0.0411(11) Uani 1 1 d . . H1' H 0.489955 -0.024428 0.864778 0.049 Uiso 1 1 calc R U C7' C 0.1332(11) -0.0462(3) 0.8543(7) 0.0473(14) Uani 1 1 d . . C8' C 0.1938(13) -0.1201(3) 0.7932(8) 0.0541(16) Uani 1 1 d . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 F3 0.058(3) 0.062(3) 0.157(5) 0.027(3) 0.017(3) -0.007(2) O1 0.028(2) 0.053(3) 0.173(5) 0.023(3) 0.006(3) 0.000(2) C7 0.033(3) 0.039(3) 0.072(4) 0.000(3) 0.006(3) 0.000(2) F1' 0.063(3) 0.063(3) 0.159(5) -0.034(3) 0.017(3) 0.007(2) F1 0.155(6) 0.097(4) 0.133(5) 0.053(4) -0.063(4) -0.026(4) C8 0.048(4) 0.046(3) 0.071(4) 0.009(3) 0.000(3) 0.006(3) F2 0.139(6) 0.048(3) 0.160(5) -0.013(3) 0.053(5) 0.002(3) F2' 0.153(6) 0.041(3) 0.182(6) 0.009(3) 0.069(5) 0.000(3) F3' 0.156(7) 0.110(5) 0.155(6) -0.068(5) -0.065(5) 0.038(4) C6 0.036(3) 0.045(3) 0.059(4) 0.000(3) -0.007(3) 0.000(2) C1 0.032(3) 0.038(3) 0.046(3) -0.001(2) 0.010(2) 0.001(2) C3 0.051(4) 0.054(4) 0.057(3) 0.011(3) -0.001(3) 0.007(3) C5 0.047(4) 0.040(3) 0.070(4) -0.004(3) 0.004(3) -0.008(3) C2 0.039(3) 0.050(3) 0.048(3) -0.002(3) 0.001(2) -0.001(2) C4 0.048(4) 0.040(3) 0.058(3) 0.004(3) 0.007(3) 0.003(3) N1 0.031(2) 0.035(2) 0.055(3) 0.0003(19) 0.0057(19) -0.0040(17) C2' 0.037(3) 0.046(3) 0.060(3) 0.005(3) 0.005(3) -0.001(2) C5' 0.044(3) 0.054(4) 0.053(3) -0.009(3) 0.004(3) 0.007(3) C3' 0.044(4) 0.047(3) 0.067(4) 0.006(3) 0.001(3) -0.007(3) C1' 0.027(3) 0.038(3) 0.044(3) 0.001(2) -0.005(2) 0.003(2) C6' 0.037(3) 0.048(3) 0.050(3) 0.000(3) 0.007(2) -0.003(3) O1' 0.031(2) 0.050(3) 0.152(5) -0.022(3) -0.001(2) 0.000(2) C4' 0.052(4) 0.042(3) 0.061(4) -0.001(3) -0.006(3) 0.004(3) N1' 0.029(2) 0.039(2) 0.056(3) 0.000(2) 0.0031(19) 0.0021(17) C7' 0.036(3) 0.037(3) 0.068(4) 0.004(3) 0.002(3) 0.001(2) C8' 0.048(4) 0.043(3) 0.072(4) -0.009(3) -0.001(3) -0.004(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.003 0.002 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.006 0.003 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.011 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.017 0.01 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle O1 C7 N1 127.4(6) O1 C7 C8 116.7(5) N1 C7 C8 115.9(5) F1 C8 F2 108.1(7) F1 C8 F3 107.9(6) F2 C8 F3 104.6(7) F1 C8 C7 110.5(6) F2 C8 C7 111.9(5) F3 C8 C7 113.6(5) C5 C6 C1 118.9(5) C5 C6 H6 120.5 C1 C6 H6 120.5 C2 C1 C6 119.4(6) C2 C1 N1 119.5(5) C6 C1 N1 121.1(5) C4 C3 C2 119.6(6) C4 C3 H3 120.2 C2 C3 H3 120.2 C4 C5 C6 121.3(5) C4 C5 H5 119.4 C6 C5 H5 119.4 C1 C2 C3 121.1(6) C1 C2 H2 119.5 C3 C2 H2 119.5 C5 C4 C3 119.6(6) C5 C4 H4 120.2 C3 C4 H4 120.2 C7 N1 C1 125.5(5) C7 N1 H1 117.2 C1 N1 H1 117.2 C3' C2' C1' 120.0(5) C3' C2' H2' 120 C1' C2' H2' 120 C4' C5' C6' 121.0(6) C4' C5' H5' 119.5 C6' C5' H5' 119.5 C4' C3' C2' 120.3(6) C4' C3' H3' 119.9 C2' C3' H3' 119.9 C2' C1' C6' 119.6(5) C2' C1' N1' 118.2(5) C6' C1' N1' 122.1(5) C5' C6' C1' 119.1(6) C5' C6' H6' 120.4 C1' C6' H6' 120.4 C5' C4' C3' 119.9(6) C5' C4' H4' 120 C3' C4' H4' 120 C7' N1' C1' 125.5(5) C7' N1' H1' 117.2 C1' N1' H1' 117.2 O1' C7' N1' 127.9(6) O1' C7' C8' 116.9(5) N1' C7' C8' 115.3(5) F2' C8' F3' 107.1(7) F2' C8' F1' 104.9(6) F3' C8' F1' 107.6(6) F2' C8' C7' 111.9(5) F3' C8' C7' 109.9(6) F1' C8' C7' 114.9(5) loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance F3 C8 1.323(8) O1 C7 1.207(7) C7 N1 1.325(8) C7 C8 1.534(8) F1' C8' 1.318(8) F1 C8 1.293(9) C8 F2 1.299(8) F2' C8' 1.292(8) F3' C8' 1.307(10) C6 C5 1.379(7) C6 C1 1.404(8) C6 H6 0.95 C1 C2 1.366(8) C1 N1 1.425(7) C3 C4 1.376(9) C3 C2 1.385(8) C3 H3 0.95 C5 C4 1.374(9) C5 H5 0.95 C2 H2 0.95 C4 H4 0.95 N1 H1 0.88 C2' C3' 1.383(8) C2' C1' 1.391(8) C2' H2' 0.95 C5' C4' 1.371(9) C5' C6' 1.386(8) C5' H5' 0.95 C3' C4' 1.382(9) C3' H3' 0.95 C1' C6' 1.401(7) C1' N1' 1.419(7) C6' H6' 0.95 O1' C7' 1.215(7) C4' H4' 0.95 N1' C7' 1.322(8) N1' H1' 0.88 C7' C8' 1.532(8)