#------------------------------------------------------------------------------ #$Date: 2020-03-28 00:25:28 +0200 (Sat, 28 Mar 2020) $ #$Revision: 249789 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/75/4517523.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4517523 loop_ _publ_author_name 'Xu, Wen-Bin' 'Ghorai, Samir' 'Huang, Wenyu' 'Li, Changkun' _publ_section_title ; Rh(I)/Bisoxazolinephosphine-Catalyzed Regio- and Enantioselective Allylic Substitutions ; _journal_name_full 'ACS Catalysis' _journal_page_first 4491 _journal_paper_doi 10.1021/acscatal.0c00712 _journal_year 2020 _chemical_absolute_configuration ad _chemical_formula_moiety 'C34 H40 Cl N2 O2 P Rh, C F3 O3 S' _chemical_formula_sum 'C35 H40 Cl F3 N2 O5 P Rh S' _chemical_formula_weight 827.08 _space_group_crystal_system tetragonal _space_group_IT_number 96 _space_group_name_Hall 'P 4nw 2abw' _space_group_name_H-M_alt 'P 43 21 2' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2016/6 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 10.9434(6) _cell_length_b 10.9434(6) _cell_length_c 60.442(4) _cell_measurement_reflns_used 9456 _cell_measurement_temperature 295(2) _cell_measurement_theta_max 68.35 _cell_measurement_theta_min 4.11 _cell_volume 7238.4(7) _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' _diffrn_ambient_temperature 295(2) _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0704 _diffrn_reflns_av_unetI/netI 0.0262 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 72 _diffrn_reflns_limit_l_min -71 _diffrn_reflns_number 87504 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 68.521 _diffrn_reflns_theta_min 2.924 _exptl_absorpt_coefficient_mu 5.960 _exptl_crystal_colour red _exptl_crystal_density_diffrn 1.518 _exptl_crystal_description block _exptl_crystal_F_000 3392 _exptl_crystal_size_max 0.240 _exptl_crystal_size_mid 0.220 _exptl_crystal_size_min 0.190 _exptl_transmission_factor_max 0.1665 _exptl_transmission_factor_min 0.0350 _refine_diff_density_max 0.340 _refine_diff_density_min -0.274 _refine_diff_density_rms 0.044 _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.034(8) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.996 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 448 _refine_ls_number_reflns 6650 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.996 _refine_ls_R_factor_all 0.0264 _refine_ls_R_factor_gt 0.0256 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0415P)^2^+1.9477P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0683 _refine_ls_wR_factor_ref 0.0692 _reflns_Friedel_coverage 0.673 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.997 _reflns_number_gt 6460 _reflns_number_total 6650 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs0c00712_si_003.cif _cod_data_source_block a_a _cod_original_cell_volume 7238.4(9) _cod_database_code 4517523 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.329 _shelx_estimated_absorpt_t_max 0.397 _shelx_res_file ; TITL a_a.res in P4(3)2(1)2 a_a.res created by SHELXL-2016/6 at 18:06:23 on 29-Nov-2018 REM Old TITL a in P4(3)2(1)2 REM SHELXT solution in P4(3)2(1)2 REM R1 0.194, Rweak 0.036, Alpha 0.013, Orientation as input REM Flack x = 0.188 ( 0.006 ) from Parsons' quotients REM Formula found by SHELXT: C33 Cl F3 N2 O7 P Rh S CELL 1.54178 10.9434 10.9434 60.4421 90.000 90.000 90.000 ZERR 8.000 0.0006 0.0006 0.0037 0.000 0.000 0.000 LATT -1 SYMM -X, -Y, 1/2+Z SYMM 1/2-Y, 1/2+X, 3/4+Z SYMM 1/2+Y, 1/2-X, 1/4+Z SYMM 1/2-X, 1/2+Y, 3/4-Z SYMM 1/2+X, 1/2-Y, 1/4-Z SYMM Y, X, -Z SYMM -Y, -X, 1/2-Z SFAC C H CL F N O P RH S UNIT 280 320 8 24 16 40 8 8 8 ACTA size 0.24 0.22 0.19 conf TEMP 22.130 L.S. 10 twin BOND $H LIST 6 FMAP 2 PLAN 20 WGHT 0.041500 1.947700 BASF 0.03447 FVAR 0.21850 RH1 8 0.823475 0.528639 0.418067 11.00000 0.04436 0.05218 = 0.04460 0.00053 0.00085 0.00073 C1 1 0.927646 0.709205 0.461930 11.00000 0.06173 0.05531 = 0.04608 -0.00169 -0.00066 -0.00524 O1 6 0.771190 0.171385 0.446955 11.00000 0.08377 0.05253 = 0.07572 -0.00002 0.01143 -0.00804 N1 5 0.824766 0.338069 0.427705 11.00000 0.05132 0.04862 = 0.05463 -0.00137 0.00261 0.00130 P1 7 0.894180 0.555868 0.452148 11.00000 0.04372 0.05058 = 0.04538 0.00018 0.00119 0.00039 F1 4 0.507105 -0.078076 0.418956 11.00000 0.22873 0.17657 = 0.13838 -0.01888 0.08196 0.03037 S1 9 0.460307 0.022260 0.456821 11.00000 0.07643 0.12841 = 0.07704 0.00735 -0.00616 -0.02293 CL1 3 0.772977 0.469080 0.379989 11.00000 0.06775 0.08135 = 0.05082 -0.00516 -0.00556 0.00092 F2 4 0.320691 -0.032293 0.423610 11.00000 0.17078 0.17888 = 0.12244 -0.01715 -0.07024 0.01010 N2 5 1.009074 0.540636 0.407436 11.00000 0.04690 0.05768 = 0.04880 0.00358 0.00828 -0.00290 O2 6 1.208733 0.501203 0.404304 11.00000 0.05254 0.09168 = 0.07181 0.00906 0.01917 0.00442 C2 1 1.047784 0.747781 0.463098 11.00000 0.06301 0.07088 = 0.07082 -0.01131 0.00655 -0.01281 AFIX 43 H2 2 1.110532 0.692771 0.460186 11.00000 -1.20000 AFIX 0 F3 4 0.394439 -0.185967 0.440190 11.00000 0.21132 0.09855 = 0.16475 -0.00040 -0.00342 -0.01437 O3 6 0.565236 -0.038803 0.465276 11.00000 0.10084 0.22705 = 0.18247 0.10604 -0.06464 -0.03904 C3 1 1.075726 0.867804 0.468573 11.00000 0.09279 0.08388 = 0.08783 -0.01019 0.00968 -0.03497 AFIX 43 H3 2 1.156927 0.892453 0.469402 11.00000 -1.20000 AFIX 0 C9 1 0.696185 0.464851 0.507063 11.00000 0.08245 0.08561 = 0.05902 0.00188 0.01799 0.00230 AFIX 43 H9 2 0.676566 0.500134 0.520602 11.00000 -1.20000 AFIX 0 C8 1 0.766088 0.529201 0.491939 11.00000 0.06362 0.07070 = 0.05334 -0.00288 0.00778 0.00131 AFIX 43 H8 2 0.793144 0.607576 0.495313 11.00000 -1.20000 AFIX 0 C7 1 0.795654 0.476894 0.471817 11.00000 0.04773 0.05839 = 0.04938 0.00337 0.00280 0.00038 C6 1 0.836253 0.795393 0.466739 11.00000 0.07281 0.06436 = 0.06325 -0.00805 -0.00971 0.00921 AFIX 43 H6 2 0.754664 0.771689 0.466398 11.00000 -1.20000 AFIX 0 C5 1 0.865345 0.913948 0.471932 11.00000 0.11156 0.06170 = 0.07000 -0.00731 -0.00750 0.01227 AFIX 43 H5 2 0.803774 0.970169 0.474909 11.00000 -1.20000 AFIX 0 O5 6 0.354461 0.015963 0.470298 11.00000 0.12089 0.19387 = 0.09189 -0.03883 0.03545 -0.05590 C4 1 0.985253 0.949181 0.472715 11.00000 0.13647 0.05643 = 0.07422 -0.00681 0.01026 -0.02055 AFIX 43 H4 2 1.004822 1.029712 0.476122 11.00000 -1.20000 AFIX 0 O4 6 0.481516 0.139352 0.446413 11.00000 0.10690 0.10391 = 0.13166 0.01261 0.00307 -0.02008 C10 1 0.655659 0.349173 0.502175 11.00000 0.08646 0.09457 = 0.06792 0.01457 0.02664 -0.01285 AFIX 43 H10 2 0.606753 0.307477 0.512242 11.00000 -1.20000 AFIX 0 C11 1 0.687145 0.294438 0.482390 11.00000 0.07301 0.06774 = 0.07608 0.00790 0.01590 -0.01068 AFIX 43 H11 2 0.661220 0.215243 0.479371 11.00000 -1.20000 AFIX 0 C13 1 0.787519 0.292489 0.446134 11.00000 0.05454 0.04898 = 0.06682 0.00032 0.00189 -0.00446 C12 1 0.757240 0.357064 0.467010 11.00000 0.05305 0.06248 = 0.05394 0.00671 0.00589 -0.00257 C14 1 0.777542 0.129642 0.424001 11.00000 0.07220 0.06311 = 0.08526 -0.01644 0.01050 -0.00854 AFIX 23 H14A 2 0.696388 0.117548 0.417929 11.00000 -1.20000 H14B 2 0.822897 0.053738 0.422881 11.00000 -1.20000 AFIX 0 C16 1 0.980066 0.213588 0.407595 11.00000 0.05956 0.06180 = 0.07635 -0.01222 0.00463 -0.00084 AFIX 13 H16 2 1.016719 0.294430 0.405447 11.00000 -1.20000 AFIX 0 C15 1 0.844252 0.233482 0.411996 11.00000 0.05780 0.05446 = 0.06145 -0.00779 0.00207 -0.00190 AFIX 13 H15 2 0.802541 0.250923 0.398000 11.00000 -1.20000 AFIX 0 C17 1 1.047694 0.153204 0.426787 11.00000 0.07700 0.07753 = 0.11071 -0.00039 -0.01559 0.00766 AFIX 137 H17A 2 1.017026 0.071852 0.428906 11.00000 -1.50000 H17B 2 1.035141 0.199988 0.440029 11.00000 -1.50000 H17C 2 1.133447 0.149794 0.423496 11.00000 -1.50000 AFIX 0 C19 1 1.037252 0.473071 0.456090 11.00000 0.04763 0.05788 = 0.05380 0.00079 -0.00212 0.00310 C18 1 0.996857 0.143158 0.385991 11.00000 0.06543 0.12111 = 0.11467 -0.05140 0.01166 0.00185 AFIX 137 H18A 2 0.960911 0.188431 0.374044 11.00000 -1.50000 H18B 2 0.957751 0.064901 0.387165 11.00000 -1.50000 H18C 2 1.082461 0.131876 0.383184 11.00000 -1.50000 AFIX 0 C20 1 1.061179 0.427223 0.476951 11.00000 0.05984 0.08437 = 0.05814 0.00566 -0.00200 0.00909 AFIX 43 H20 2 1.006100 0.440984 0.488400 11.00000 -1.20000 AFIX 0 C21 1 1.167679 0.360303 0.480933 11.00000 0.07114 0.10230 = 0.07160 0.01684 -0.00884 0.02373 AFIX 43 H21 2 1.182194 0.328345 0.494946 11.00000 -1.20000 AFIX 0 C22 1 1.250749 0.341459 0.464365 11.00000 0.05951 0.09084 = 0.08467 0.00909 -0.01107 0.01898 AFIX 43 H22 2 1.321863 0.297519 0.467136 11.00000 -1.20000 AFIX 0 C23 1 1.228756 0.387532 0.443706 11.00000 0.04969 0.07290 = 0.07566 -0.00135 0.00283 0.00757 AFIX 43 H23 2 1.285265 0.374213 0.432470 11.00000 -1.20000 AFIX 0 C24 1 1.123214 0.454001 0.439229 11.00000 0.04179 0.05898 = 0.06275 -0.00105 0.00030 -0.00002 C25 1 1.106481 0.501356 0.416636 11.00000 0.04597 0.05838 = 0.05854 -0.00069 0.00953 -0.00015 C26 1 1.168275 0.530505 0.381862 11.00000 0.08466 0.10134 = 0.06753 0.01394 0.02953 0.00996 AFIX 23 H26A 2 1.163659 0.457296 0.372853 11.00000 -1.20000 H26B 2 1.223775 0.587896 0.374890 11.00000 -1.20000 AFIX 0 C27 1 1.043149 0.586690 0.384828 11.00000 0.06422 0.07285 = 0.04843 0.00490 0.01017 -0.01028 AFIX 13 H27 2 0.987176 0.551510 0.373891 11.00000 -1.20000 AFIX 0 C28 1 1.037339 0.724492 0.383375 11.00000 0.08320 0.07257 = 0.06537 0.01577 0.01385 -0.00443 AFIX 13 H28 2 0.953123 0.749499 0.386521 11.00000 -1.20000 AFIX 0 C29 1 1.068673 0.766313 0.359800 11.00000 0.12005 0.10391 = 0.07560 0.02943 0.00806 -0.01518 AFIX 137 H29A 2 1.017242 0.724358 0.349415 11.00000 -1.50000 H29B 2 1.152711 0.747934 0.356689 11.00000 -1.50000 H29C 2 1.055658 0.852794 0.358558 11.00000 -1.50000 AFIX 0 C30 1 1.121105 0.788322 0.400122 11.00000 0.19142 0.07831 = 0.08362 0.00365 -0.00180 -0.04655 AFIX 137 H30A 2 1.204880 0.772234 0.396419 11.00000 -1.50000 H30B 2 1.104301 0.757877 0.414704 11.00000 -1.50000 H30C 2 1.106557 0.874804 0.399725 11.00000 -1.50000 AFIX 0 C31 1 0.762232 0.710405 0.410535 11.00000 0.06581 0.05939 = 0.07403 0.01009 -0.00443 0.01059 AFIX 23 H31A 2 0.811287 0.776906 0.416340 11.00000 -1.20000 H31B 2 0.733503 0.724440 0.395567 11.00000 -1.20000 AFIX 0 C32 1 0.677790 0.656168 0.425391 11.00000 0.05203 0.06964 = 0.06593 -0.00529 0.00068 0.01525 AFIX 13 H32 2 0.672109 0.689182 0.440428 11.00000 -1.20000 AFIX 0 C33 1 0.618586 0.546035 0.420774 11.00000 0.04070 0.08140 = 0.06707 -0.00215 -0.00436 0.00622 AFIX 13 H33 2 0.580060 0.547724 0.406140 11.00000 -1.20000 AFIX 0 C34 1 0.538317 0.485408 0.437413 11.00000 0.04937 0.09490 = 0.07905 -0.00427 0.00433 -0.00279 AFIX 137 H34A 2 0.456858 0.517248 0.436183 11.00000 -1.50000 H34B 2 0.569187 0.501018 0.452009 11.00000 -1.50000 H34C 2 0.537225 0.398924 0.434759 11.00000 -1.50000 AFIX 0 C35 1 0.420224 -0.072927 0.433892 11.00000 0.12035 0.09635 = 0.08766 0.00099 0.01541 0.00926 HKLF 4 REM a_a.res in P4(3)2(1)2 REM R1 = 0.0256 for 6460 Fo > 4sig(Fo) and 0.0264 for all 6650 data REM 448 parameters refined using 0 restraints END WGHT 0.0318 2.0363 REM Highest difference peak 0.340, deepest hole -0.274, 1-sigma level 0.044 Q1 1 0.3975 0.0527 0.4433 11.00000 0.05 0.34 Q2 1 0.8192 0.5254 0.4339 11.00000 0.05 0.28 Q3 1 0.8281 0.5182 0.4647 11.00000 0.05 0.25 Q4 1 0.5607 -0.0937 0.4337 11.00000 0.05 0.20 Q5 1 0.6216 0.5054 0.4051 11.00000 0.05 0.19 Q6 1 0.8220 0.5342 0.4014 11.00000 0.05 0.18 Q7 1 0.9779 0.5057 0.4526 11.00000 0.05 0.17 Q8 1 0.8437 0.5290 0.3704 11.00000 0.05 0.17 Q9 1 0.5707 -0.0548 0.4502 11.00000 0.05 0.16 Q10 1 0.4664 -0.1525 0.4165 11.00000 0.05 0.15 Q11 1 0.3698 -0.1306 0.4380 11.00000 0.05 0.15 Q12 1 0.3570 -0.2682 0.4420 11.00000 0.05 0.15 Q13 1 1.1141 0.4013 0.4781 11.00000 0.05 0.15 Q14 1 0.4677 -0.1828 0.4481 11.00000 0.05 0.14 Q15 1 0.5959 -0.0593 0.4746 11.00000 0.05 0.14 Q16 1 0.3516 -0.0800 0.4750 11.00000 0.05 0.14 Q17 1 0.4380 -0.0909 0.4582 11.00000 0.05 0.14 Q18 1 0.4710 0.0409 0.4744 11.00000 0.05 0.14 Q19 1 0.3144 -0.0039 0.4204 11.00000 0.05 0.14 Q20 1 0.5200 0.0267 0.4715 11.00000 0.05 0.13 ; _shelx_res_checksum 68715 _shelx_hkl_file ; 1 0 0 0.90 0.30 1 0 0 1.20 0.30 2 0 0 3353.36 191.88 2 0 0 3640.44 191.88 -2 0 0 3001.70 192.68 -3 0 0 5.80 2.00 4 0 0 5067.89 268.67 -4 0 0 4239.18 270.47 -5 0 0 0.40 1.70 5 0 0 1.60 1.00 6 0 0 1787.92 97.39 -6 0 0 1500.75 100.69 -7 0 0 1.40 1.90 7 0 0 0.60 0.70 7 0 0 -1.80 1.20 -8 0 0 177.58 14.80 -8 0 0 181.08 17.50 8 0 0 196.18 14.10 8 0 0 199.38 13.90 9 0 0 -1.90 2.50 -9 0 0 1.80 1.50 9 0 0 -1.20 1.70 -9 0 0 4.50 2.90 9 0 0 1.80 1.50 -9 0 0 3.80 3.30 -10 0 0 46.70 5.90 10 0 0 49.80 5.40 -10 0 0 48.10 6.30 -10 0 0 39.00 6.20 11 0 0 -0.30 0.80 -11 0 0 0.30 1.50 -11 0 0 0.50 1.40 11 0 0 2.60 1.30 -12 0 0 10.40 2.80 -12 0 0 18.60 3.30 12 0 0 15.30 2.30 12 0 0 11.60 2.40 13 0 0 1.50 0.90 13 0 0 0.20 1.00 -13 0 0 -0.30 1.20 0 -1 0 0.10 0.30 0 -1 0 0.80 0.30 2 -1 0 588.54 34.80 -2 1 0 584.14 34.80 2 1 0 564.44 33.60 -3 -1 0 54.39 4.40 3 -1 0 58.39 5.00 -3 1 0 50.29 5.10 3 1 0 53.69 4.10 3 1 0 54.89 4.10 -4 -1 0 193.78 17.00 4 -1 0 244.18 15.50 4 1 0 234.38 14.20 -4 1 0 217.38 16.30 4 1 0 219.58 14.40 -5 -1 0 1191.88 79.39 5 -1 0 1413.46 76.99 5 1 0 1271.57 75.39 -5 1 0 1258.07 78.49 -6 -1 0 413.66 31.90 6 -1 0 498.65 29.70 6 1 0 466.65 28.20 -6 1 0 430.36 31.60 7 -1 0 61.49 6.10 -7 -1 0 57.59 7.90 7 -1 0 61.19 6.50 7 1 0 67.29 5.70 -7 1 0 62.09 8.40 8 -1 0 100.69 9.10 -8 -1 0 82.09 8.70 -8 -1 0 95.79 10.40 8 -1 0 106.69 8.50 -8 -1 0 88.89 10.60 8 1 0 96.59 8.00 -8 1 0 87.09 9.00 8 1 0 102.29 8.20 -8 1 0 83.99 11.40 9 -1 0 64.89 6.50 -9 -1 0 59.09 7.80 -9 -1 0 60.99 8.70 -9 -1 0 57.69 7.10 9 -1 0 59.29 6.70 9 -1 0 60.39 7.10 9 1 0 74.39 8.30 9 1 0 64.89 6.30 -9 1 0 60.09 7.10 -9 1 0 60.29 6.70 -9 1 0 64.09 8.10 10 -1 0 87.69 8.00 -10 -1 0 93.79 9.60 -10 -1 0 78.39 8.50 -10 1 0 86.19 8.90 -10 1 0 89.69 9.50 -10 1 0 90.49 8.10 10 1 0 96.99 7.90 11 -1 0 17.50 2.70 -11 -1 0 12.50 3.30 11 -1 0 12.70 2.50 -11 -1 0 17.70 3.40 -11 1 0 11.70 3.20 11 1 0 11.40 2.60 -11 1 0 9.10 2.70 -11 1 0 5.90 2.50 -12 -1 0 2.00 1.30 -12 -1 0 3.30 1.40 12 -1 0 1.40 1.40 12 1 0 2.50 1.20 -12 1 0 0.40 1.20 -12 1 0 3.10 1.40 13 -1 0 18.60 2.20 -13 -1 0 12.60 2.20 13 -1 0 17.00 2.30 13 1 0 15.80 2.20 13 1 0 21.00 2.60 0 -2 0 3237.68 183.88 0 -2 0 3015.80 183.98 0 2 0 3332.27 184.08 1 -2 0 561.54 34.40 -1 -2 0 541.55 33.20 -1 -2 0 561.84 33.70 -1 -2 0 597.64 35.10 -1 2 0 591.84 34.60 1 2 0 583.94 33.50 2 -2 0 411.76 25.00 -2 -2 0 391.26 25.70 -2 -2 0 372.16 24.30 -2 2 0 417.06 25.10 3 -2 0 670.53 38.30 -3 -2 0 555.44 39.00 3 2 0 626.84 36.00 -4 -2 0 126.69 9.40 4 -2 0 135.89 10.30 -4 -2 0 119.19 11.40 4 2 0 144.29 8.40 4 2 0 123.99 8.40 -5 -2 0 452.05 32.50 5 -2 0 502.55 30.60 -5 2 0 471.15 31.70 5 2 0 483.05 28.10 5 2 0 437.76 28.30 -6 -2 0 30.50 5.70 6 -2 0 26.60 5.10 6 -2 0 29.70 4.30 6 2 0 33.70 3.20 -6 2 0 30.40 5.50 7 -2 0 449.06 29.40 -7 -2 0 403.16 31.00 7 -2 0 441.56 29.10 7 -2 0 420.66 27.90 7 2 0 469.15 26.80 -7 2 0 406.46 31.30 8 -2 0 117.99 10.10 -8 -2 0 116.59 11.40 8 -2 0 107.19 9.20 8 -2 0 114.49 10.50 -8 -2 0 107.39 11.90 -8 -2 0 109.49 10.10 -8 2 0 103.89 10.10 -8 2 0 101.29 12.20 -8 2 0 107.89 10.20 9 -2 0 70.49 6.70 9 -2 0 69.59 7.20 -9 -2 0 49.00 8.60 -9 -2 0 64.69 7.80 9 -2 0 62.69 7.10 -9 -2 0 66.99 7.40 -9 2 0 55.29 8.00 -9 2 0 51.89 9.50 9 2 0 58.39 6.00 -9 2 0 67.59 7.30 -9 2 0 62.59 7.40 10 -2 0 19.50 3.50 -10 -2 0 17.10 4.10 -10 -2 0 26.90 4.60 10 -2 0 22.50 3.40 -10 2 0 19.60 3.90 10 2 0 25.50 3.50 -10 2 0 19.30 4.20 -10 2 0 17.10 4.20 11 -2 0 24.80 3.40 11 -2 0 17.90 3.10 -11 -2 0 24.70 4.30 -11 -2 0 20.70 4.00 -11 2 0 19.20 3.80 11 2 0 23.00 3.30 -11 2 0 25.70 3.90 -11 2 0 21.30 4.20 -12 -2 0 7.30 2.00 -12 -2 0 6.20 2.10 12 -2 0 5.50 1.50 12 -2 0 11.60 2.20 12 2 0 8.70 1.90 -12 2 0 4.80 2.20 -13 -2 0 4.90 1.40 13 -2 0 6.70 1.50 13 -2 0 4.50 1.30 0 -3 0 0.40 0.60 0 -3 0 1.00 0.60 0 3 0 0.10 0.50 -1 -3 0 48.10 4.10 -1 -3 0 48.20 5.00 1 -3 0 48.10 4.20 1 -3 0 52.49 4.80 1 3 0 48.70 3.90 -1 3 0 53.09 4.80 2 -3 0 657.43 39.60 -2 -3 0 689.73 40.60 -2 -3 0 600.04 38.50 -2 3 0 637.14 39.70 2 3 0 641.74 37.70 3 -3 0 5245.08 287.97 -3 -3 0 4963.40 289.17 -3 -3 0 4706.93 287.37 -4 -3 0 178.68 14.90 4 -3 0 185.78 13.70 -4 -3 0 171.18 12.90 4 -3 0 184.28 13.60 5 -3 0 16.60 3.30 -5 -3 0 21.60 4.70 -5 -3 0 20.30 3.10 5 -3 0 22.70 4.10 6 -3 0 157.58 12.90 6 -3 0 145.29 11.70 6 -3 0 158.68 13.00 -6 -3 0 156.68 14.70 -6 3 0 173.68 14.90 7 -3 0 126.29 11.20 7 -3 0 128.39 11.30 -7 -3 0 118.99 12.60 7 -3 0 119.19 10.00 -7 3 0 122.19 13.20 8 -3 0 17.70 4.80 -8 -3 0 21.20 4.40 8 -3 0 29.10 4.90 -8 -3 0 25.80 4.70 -8 -3 0 26.10 5.80 -8 -3 0 24.50 6.10 8 -3 0 32.30 4.80 8 -3 0 30.10 4.20 -8 -3 0 25.00 4.90 -8 3 0 22.30 4.80 -8 3 0 32.90 5.20 -8 3 0 25.00 6.20 -8 3 0 30.70 5.40 9 -3 0 6.10 2.20 9 -3 0 3.40 1.40 -9 -3 0 5.00 2.70 -9 -3 0 3.80 2.30 -9 3 0 4.30 2.20 -9 3 0 4.00 2.90 -9 3 0 2.40 2.40 10 -3 0 15.20 2.70 -10 -3 0 10.30 2.60 -10 -3 0 14.50 4.00 10 -3 0 13.40 2.80 -10 3 0 11.10 3.30 -10 3 0 17.90 4.10 10 3 0 11.20 2.90 -10 3 0 9.10 2.70 -11 -3 0 55.89 7.20 11 -3 0 59.89 5.90 11 -3 0 65.09 6.00 -11 -3 0 70.19 6.90 11 3 0 69.39 5.80 -11 3 0 56.19 6.20 -11 3 0 67.69 6.50 12 -3 0 37.00 3.90 -12 -3 0 32.80 4.60 12 -3 0 38.10 3.60 -12 -3 0 38.90 4.30 12 3 0 26.80 3.50 0 -4 0 4686.83 274.07 0 -4 0 4896.11 274.27 0 4 0 4683.73 274.67 1 -4 0 220.98 15.10 -1 -4 0 229.38 14.30 -1 -4 0 227.78 14.90 1 -4 0 229.78 15.50 1 4 0 232.68 14.90 -1 4 0 226.68 15.80 -2 -4 0 133.09 9.60 2 -4 0 132.19 10.40 2 -4 0 133.29 10.30 -2 -4 0 139.39 11.30 -2 4 0 143.59 10.90 2 4 0 123.49 8.80 3 -4 0 187.88 14.10 -3 -4 0 189.88 15.00 3 -4 0 189.48 13.90 -3 -4 0 179.38 13.20 -4 -4 0 60.59 6.70 4 -4 0 64.89 6.70 -4 -4 0 60.89 7.50 4 -4 0 66.89 6.90 5 -4 0 17.10 3.80 -5 -4 0 15.20 3.10 -5 -4 0 18.50 4.30 5 -4 0 10.80 3.00 5 -4 0 11.40 3.30 6 -4 0 274.37 18.60 -6 -4 0 257.67 21.50 6 -4 0 272.37 20.00 -6 -4 0 252.27 18.10 6 -4 0 284.77 19.90 -6 4 0 263.77 21.20 -7 -4 0 168.58 16.40 -7 -4 0 153.08 17.20 7 -4 0 166.28 13.90 7 -4 0 161.58 13.50 7 -4 0 176.08 13.90 -7 -4 0 165.88 15.60 7 -4 0 152.38 12.40 -7 -4 0 168.88 14.80 -7 4 0 170.48 14.20 -7 4 0 168.88 15.90 -7 4 0 155.38 13.90 8 -4 0 24.90 4.60 -8 -4 0 25.50 5.00 -8 -4 0 15.40 4.60 8 -4 0 25.50 4.40 -8 -4 0 20.50 6.10 -8 -4 0 26.60 4.80 8 -4 0 25.10 3.70 8 -4 0 23.20 4.50 -8 -4 0 33.10 5.90 8 -4 0 20.00 3.60 -8 4 0 26.80 4.90 -8 4 0 22.90 5.10 -8 4 0 16.70 5.60 -8 4 0 31.60 5.50 9 -4 0 17.30 4.40 9 -4 0 10.50 2.80 9 -4 0 9.50 2.50 -9 -4 0 7.60 3.30 9 -4 0 11.10 2.50 -9 4 0 5.90 3.30 -9 4 0 7.70 2.60 -9 4 0 5.10 2.50 -10 -4 0 12.80 3.30 10 -4 0 10.70 2.60 10 -4 0 8.10 2.40 -10 -4 0 10.10 3.20 -10 4 0 8.60 2.70 -10 4 0 11.30 3.10 -11 -4 0 64.09 6.40 -11 -4 0 56.69 6.90 11 -4 0 58.49 5.80 11 -4 0 66.19 6.00 -11 4 0 63.99 6.30 12 -4 0 0.40 0.90 12 -4 0 1.00 0.90 12 -4 0 0.20 1.10 -12 -4 0 -0.70 0.90 -12 -4 0 0.30 1.30 -12 4 0 0.20 1.30 0 -5 0 0.30 0.70 0 -5 0 3.40 1.50 0 -5 0 0.30 0.90 0 5 0 0.50 0.70 1 -5 0 1346.87 79.19 1 -5 0 1322.77 79.59 -1 -5 0 1300.17 78.89 -1 -5 0 1389.46 77.99 1 -5 0 1341.87 79.39 -1 5 0 1420.06 80.29 1 5 0 1239.08 78.89 2 -5 0 486.95 30.30 2 -5 0 450.05 29.70 -2 -5 0 445.26 29.40 2 -5 0 471.55 30.50 -2 -5 0 504.55 32.10 3 -5 0 21.50 3.30 -3 -5 0 24.30 4.70 -3 -5 0 29.30 3.70 3 -5 0 18.70 3.90 3 -5 0 19.50 3.80 -4 -5 0 19.90 4.40 4 -5 0 26.50 4.00 4 -5 0 19.30 3.90 -4 -5 0 18.90 4.30 5 -5 0 405.96 27.90 -5 -5 0 430.06 26.90 -5 -5 0 411.36 29.40 5 -5 0 392.36 26.00 5 -5 0 402.86 27.40 -5 5 0 375.76 25.80 -6 -5 0 173.78 12.40 -6 -5 0 163.78 15.30 6 -5 0 154.88 12.20 6 -5 0 155.88 13.80 6 -5 0 168.48 13.70 7 -5 0 33.20 4.80 -7 -5 0 28.40 6.50 7 -5 0 37.50 5.50 7 -5 0 37.60 5.80 7 -5 0 39.90 4.60 -7 -5 0 37.10 6.30 -7 -5 0 39.30 6.50 7 -5 0 37.90 5.60 -7 -5 0 42.10 7.10 -7 -5 0 37.80 6.30 -7 5 0 35.50 5.80 -7 5 0 39.20 7.50 -7 5 0 29.40 5.50 -8 -5 0 151.38 14.80 8 -5 0 135.59 11.20 -8 -5 0 133.59 12.10 -8 -5 0 138.29 11.80 8 -5 0 142.49 12.30 8 -5 0 118.69 11.20 -8 -5 0 153.08 14.00 8 -5 0 133.09 10.90 -8 -5 0 150.28 14.80 8 -5 0 141.69 12.20 -8 5 0 131.29 21.80 -8 5 0 132.39 16.30 -8 5 0 144.99 11.80 -8 5 0 130.19 12.40 9 -5 0 -0.70 1.20 -9 -5 0 5.10 2.40 -9 -5 0 1.40 2.10 9 -5 0 -0.10 1.40 9 -5 0 1.00 2.00 9 -5 0 0.40 1.30 -9 5 0 1.70 1.80 10 -5 0 4.30 2.40 10 -5 0 0.90 1.30 -10 -5 0 1.70 1.50 10 -5 0 1.20 1.20 -10 -5 0 2.30 1.80 -10 5 0 0.50 1.30 -11 -5 0 -0.90 1.20 -11 -5 0 0.30 1.70 11 -5 0 1.80 1.20 11 -5 0 1.70 1.60 -11 5 0 1.60 1.30 12 -5 0 54.19 5.00 -12 -5 0 48.80 5.30 12 -5 0 48.10 4.40 -12 5 0 52.69 5.10 0 -6 0 1758.52 103.29 0 -6 0 1765.22 102.99 0 -6 0 1735.63 102.79 1 -6 0 471.25 29.40 -1 -6 0 448.66 29.00 -1 -6 0 442.86 27.70 1 -6 0 460.95 29.60 1 -6 0 475.55 29.40 2 -6 0 31.90 4.20 -2 -6 0 24.80 3.70 2 -6 0 26.50 3.70 2 -6 0 27.80 4.40 -2 6 0 31.80 4.30 3 -6 0 170.28 13.10 -3 -6 0 160.18 12.60 3 -6 0 166.18 12.70 3 -6 0 149.99 13.10 -3 6 0 177.18 12.60 4 -6 0 268.37 20.00 -4 -6 0 273.07 21.60 4 -6 0 276.27 19.80 4 -6 0 259.97 19.10 -4 6 0 275.57 18.70 5 -6 0 161.18 12.40 -5 -6 0 166.58 15.00 5 -6 0 171.98 13.60 -5 -6 0 160.68 13.30 5 -6 0 168.68 13.10 5 -6 0 157.88 13.70 -5 6 0 157.98 12.20 6 -6 0 253.97 18.10 -6 -6 0 216.98 17.90 -6 -6 0 237.88 19.20 6 -6 0 224.08 17.50 6 -6 0 225.78 18.00 6 -6 0 233.78 17.20 -6 -6 0 242.28 20.10 -6 -6 0 243.18 19.80 -6 -6 0 239.68 16.90 6 -6 0 227.28 16.80 6 -6 0 220.48 16.20 -6 6 0 211.68 17.90 -6 6 0 222.88 17.00 7 -6 0 8.00 2.50 7 -6 0 14.00 3.40 -7 -6 0 8.80 3.00 -7 -6 0 4.80 3.00 7 -6 0 6.90 2.70 -7 -6 0 6.60 3.00 7 -6 0 7.20 2.90 7 -6 0 10.40 3.00 7 -6 0 8.70 2.40 -7 -6 0 3.50 3.30 -7 6 0 4.70 4.00 -7 6 0 9.40 3.30 -7 6 0 9.20 2.90 -8 -6 0 3.00 2.30 8 -6 0 1.10 1.50 -8 -6 0 1.10 2.10 -8 -6 0 -0.20 2.40 8 -6 0 3.00 1.50 8 -6 0 2.80 1.70 -8 -6 0 0.60 1.80 8 -6 0 0.30 1.70 -8 6 0 4.40 2.20 -8 6 0 -3.20 1.90 -9 -6 0 16.30 4.50 9 -6 0 15.40 3.40 9 -6 0 11.50 2.70 -9 -6 0 9.80 3.30 -9 -6 0 14.20 3.90 9 -6 0 13.80 3.50 -9 -6 0 11.00 2.90 -9 6 0 13.80 3.20 10 -6 0 1.70 1.20 10 -6 0 0.80 1.20 -10 -6 0 2.00 1.80 -10 6 0 1.00 1.10 -11 -6 0 11.70 3.00 11 -6 0 13.20 2.70 11 -6 0 14.60 2.50 -11 6 0 16.70 2.90 0 -7 0 1.00 1.10 0 7 0 1.70 1.60 1 -7 0 65.49 6.50 -1 -7 0 60.59 6.30 1 -7 0 72.29 7.30 -1 -7 0 66.49 5.20 1 -7 0 63.99 6.20 -1 7 0 66.99 6.30 2 -7 0 432.76 27.90 2 -7 0 448.26 28.00 2 -7 0 393.96 28.10 -2 -7 0 401.86 27.50 -2 7 0 436.16 27.60 -3 -7 0 115.99 10.50 3 -7 0 123.79 10.80 3 -7 0 127.19 10.60 3 -7 0 116.49 11.20 -3 7 0 141.99 10.60 4 -7 0 169.38 13.60 4 -7 0 154.08 13.70 -4 -7 0 168.68 15.30 4 -7 0 167.18 13.20 -4 7 0 172.68 12.70 -4 7 0 161.48 13.60 5 -7 0 34.70 7.30 5 -7 0 35.50 5.10 -5 -7 0 28.00 6.20 -5 -7 0 28.40 6.20 -5 -7 0 36.90 6.60 5 -7 0 28.70 4.80 5 -7 0 41.40 5.90 5 -7 0 37.40 5.20 -5 -7 0 36.50 7.10 5 -7 0 38.70 5.20 -5 7 0 35.60 5.10 -5 7 0 31.40 4.70 -5 7 0 20.70 5.70 -6 -7 0 8.60 3.70 6 -7 0 9.60 3.10 6 -7 0 16.70 3.60 6 -7 0 6.90 3.00 6 -7 0 5.00 2.30 6 -7 0 13.60 3.50 6 -7 0 8.60 2.90 -6 -7 0 6.90 3.50 -6 -7 0 3.80 3.30 -6 -7 0 7.90 3.40 -6 7 0 12.70 3.30 -6 7 0 6.10 2.90 -6 7 0 2.00 2.70 -7 -7 0 65.39 8.50 7 -7 0 59.09 7.10 -7 -7 0 71.19 9.10 7 -7 0 55.49 6.60 -7 -7 0 52.19 6.80 7 -7 0 65.59 6.90 -7 7 0 51.19 6.80 -7 7 0 53.09 6.60 -8 -7 0 1.60 1.90 8 -7 0 2.00 1.50 8 -7 0 -1.60 1.60 8 -7 0 0.10 1.20 -8 -7 0 -0.40 1.70 -8 7 0 1.80 1.50 -8 7 0 1.00 1.60 9 -7 0 18.20 3.80 -9 -7 0 24.60 4.50 -9 -7 0 18.90 3.60 9 -7 0 24.50 3.50 9 -7 0 23.20 4.20 -9 7 0 25.10 4.60 -9 7 0 23.70 3.90 10 -7 0 155.68 12.10 -10 -7 0 166.88 13.70 10 -7 0 162.48 11.70 10 -7 0 166.78 12.70 -10 7 0 150.38 12.30 11 -7 0 0.90 1.70 11 -7 0 1.50 0.90 -11 7 0 2.80 1.20 0 -8 0 203.48 14.70 0 -8 0 193.38 13.10 0 -8 0 173.28 16.30 0 8 0 196.78 14.00 -1 -8 0 87.89 10.50 1 -8 0 98.09 8.90 1 -8 0 104.09 8.20 1 -8 0 88.29 10.10 -1 -8 0 97.69 8.80 1 8 0 91.39 8.10 -1 8 0 104.49 8.40 -2 -8 0 118.89 10.30 2 -8 0 125.29 10.30 2 -8 0 109.19 9.50 -2 -8 0 95.99 12.10 2 8 0 97.49 8.90 -2 8 0 129.19 10.10 -2 8 0 126.79 10.60 3 -8 0 23.30 4.00 -3 -8 0 24.00 6.30 -3 -8 0 23.40 6.70 3 -8 0 23.90 4.20 3 -8 0 30.10 5.30 -3 -8 0 23.50 4.70 -3 8 0 30.90 5.00 -3 8 0 24.90 4.00 4 -8 0 29.90 4.40 4 -8 0 22.90 5.20 -4 -8 0 25.80 6.30 4 -8 0 29.50 4.60 4 -8 0 19.60 4.00 -4 -8 0 22.40 5.40 -4 -8 0 20.50 5.00 -4 -8 0 15.10 5.50 -4 8 0 15.20 4.20 -4 8 0 19.70 3.90 -4 8 0 27.80 3.80 5 -8 0 142.99 11.70 -5 -8 0 139.09 12.90 5 -8 0 138.89 11.30 5 -8 0 125.09 12.70 -5 -8 0 134.49 12.40 -5 -8 0 151.08 14.20 -5 -8 0 119.39 13.00 -5 8 0 130.49 11.50 -5 8 0 133.39 10.80 -5 8 0 132.19 13.10 -6 -8 0 3.40 3.10 6 -8 0 2.00 1.60 -6 -8 0 0.60 2.40 6 -8 0 -3.90 5.50 6 -8 0 6.40 1.90 -6 -8 0 1.60 2.20 -6 8 0 0.20 2.30 -6 8 0 4.90 2.40 -6 8 0 1.60 2.00 -7 -8 0 0.80 2.10 -7 -8 0 1.60 1.90 -7 -8 0 2.80 2.40 7 -8 0 -0.40 3.40 7 -8 0 0.70 1.30 7 -8 0 0.00 1.30 -7 8 0 -0.40 1.30 -7 8 0 -1.90 1.30 -8 -8 0 27.00 3.90 8 -8 0 21.20 4.60 -8 -8 0 20.50 4.60 8 -8 0 28.50 4.10 -8 -8 0 21.00 4.80 8 -8 0 22.40 4.00 -8 8 0 25.50 3.80 -8 8 0 23.80 4.20 9 -8 0 65.49 6.70 9 -8 0 71.19 7.60 9 -8 0 74.49 6.70 -9 -8 0 74.89 8.30 -9 8 0 64.29 6.80 -9 8 0 67.59 6.80 10 -8 0 2.80 1.20 10 -8 0 3.20 2.60 -10 8 0 4.30 1.40 0 -9 0 -0.40 2.10 0 -9 0 4.30 2.40 0 -9 0 -3.30 2.80 0 9 0 -0.50 2.80 0 9 0 0.90 1.20 1 -9 0 61.09 8.90 -1 -9 0 61.79 8.70 -1 -9 0 47.70 6.30 1 -9 0 45.60 7.40 1 -9 0 55.99 5.50 -1 -9 0 42.30 7.80 1 -9 0 66.79 7.10 -1 9 0 58.79 7.00 -1 9 0 67.59 6.40 1 9 0 60.89 5.80 2 -9 0 62.99 8.00 2 -9 0 61.69 6.10 2 -9 0 67.99 7.50 -2 -9 0 61.19 7.50 2 -9 0 51.89 8.80 -2 -9 0 57.99 8.90 -2 -9 0 67.59 9.30 2 9 0 53.19 5.90 -2 9 0 59.19 6.50 -2 9 0 62.69 7.10 -3 -9 0 -0.70 3.30 -3 -9 0 0.30 4.20 -3 -9 0 2.80 3.00 3 -9 0 7.30 2.10 3 -9 0 4.30 3.70 3 9 0 1.80 1.60 -3 9 0 4.40 1.70 -3 9 0 6.80 2.20 -4 -9 0 10.70 3.20 4 -9 0 6.30 2.00 -4 9 0 7.50 2.10 -4 9 0 7.20 2.20 -5 -9 0 2.80 2.30 5 -9 0 5.00 2.20 5 -9 0 2.00 1.30 -5 -9 0 0.60 2.00 -5 9 0 1.40 1.70 -5 9 0 -1.90 2.10 -5 9 0 1.80 1.30 -6 -9 0 11.00 3.20 6 -9 0 11.60 2.90 -6 -9 0 7.80 3.30 6 -9 0 11.80 3.00 -6 9 0 12.00 3.20 -6 9 0 15.10 3.60 7 -9 0 22.00 3.40 7 -9 0 17.20 3.50 -7 -9 0 19.60 3.50 -7 9 0 19.50 3.70 -7 9 0 19.40 3.60 -8 -9 0 76.19 6.60 8 -9 0 71.09 6.90 -8 -9 0 65.39 7.20 8 -9 0 66.89 6.70 -8 9 0 77.49 6.80 -8 9 0 68.89 7.00 -9 9 0 0.20 1.00 0 -10 0 42.80 7.20 0 -10 0 46.60 7.00 0 10 0 47.20 6.00 0 10 0 44.70 5.50 -1 -10 0 101.29 10.50 1 -10 0 77.79 9.70 -1 -10 0 64.29 9.80 1 -10 0 83.79 9.60 1 10 0 85.79 8.00 -1 10 0 99.69 8.90 -1 10 0 88.19 8.30 1 10 0 97.39 8.70 2 -10 0 24.60 3.50 2 -10 0 17.50 4.60 2 -10 0 21.00 5.00 -2 -10 0 24.80 5.70 -2 10 0 22.40 3.60 2 10 0 22.40 3.40 -2 10 0 20.50 3.80 -3 -10 0 14.20 4.00 3 -10 0 13.20 3.20 3 -10 0 10.60 3.40 3 -10 0 10.60 3.60 3 10 0 14.40 3.00 -3 10 0 17.30 3.60 -3 10 0 16.20 3.00 -4 -10 0 5.80 3.00 4 -10 0 11.40 2.90 4 -10 0 6.90 2.60 4 -10 0 4.90 2.90 -4 10 0 11.40 2.80 4 10 0 11.90 3.00 -4 10 0 7.00 2.30 5 -10 0 -0.80 2.10 -5 -10 0 0.80 1.60 -5 -10 0 2.10 1.90 5 -10 0 0.60 1.30 -5 10 0 -0.90 1.10 -5 10 0 -0.10 2.40 -5 10 0 0.00 1.60 -6 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52.09 7.20 -8 -2 -28 48.80 7.80 -8 -2 -28 33.40 6.80 8 -2 28 36.90 6.40 -8 2 -28 48.20 8.10 8 2 28 41.60 6.10 -8 2 -28 43.40 8.40 -8 2 -28 43.30 7.20 -9 -2 -28 7.90 3.60 -9 -2 -28 10.90 3.90 9 -2 28 7.70 2.90 9 -2 28 19.10 5.10 -9 2 -28 10.20 3.40 9 2 28 4.80 2.50 -9 2 -28 9.30 3.30 -9 2 -28 8.90 3.70 -10 -2 -28 32.80 5.60 10 -2 28 33.80 5.60 -10 -2 -28 34.90 5.50 10 -2 28 28.60 4.80 -10 2 -28 25.20 4.80 10 2 28 31.20 4.50 -10 2 -28 32.40 5.90 -10 2 -28 22.90 3.90 11 -2 28 30.60 4.40 -11 -2 -28 38.10 4.90 11 -2 28 28.70 4.50 -11 -2 -28 41.90 5.10 -11 2 -28 40.90 5.60 11 2 28 33.00 4.10 12 -2 28 2.20 1.20 12 -2 28 2.50 1.10 -12 -2 -28 2.20 1.10 -12 -2 -28 2.60 1.20 -12 2 -28 2.50 1.10 -12 2 -28 4.30 1.20 11 -3 -28 11.80 2.40 11 -3 -28 11.80 2.30 -11 3 28 8.50 2.10 11 3 -28 6.90 2.40 11 3 -28 7.90 2.20 10 -3 -28 18.00 3.30 10 -3 -28 15.70 3.10 -10 3 28 16.00 3.40 10 3 -28 16.40 3.10 9 -3 -28 12.30 3.70 9 -3 -28 7.90 2.40 9 -3 -28 13.80 3.10 9 3 -28 15.20 3.30 -8 -3 28 5.30 3.00 8 -3 -28 5.60 2.50 8 -3 -28 4.50 1.90 8 -3 -28 2.80 2.00 -8 3 28 7.20 2.30 8 3 -28 11.40 2.90 -7 -3 28 9.80 3.60 7 -3 -28 10.70 3.10 7 -3 -28 7.80 2.70 7 -3 -28 8.80 2.40 -7 -3 28 5.20 3.00 7 -3 -28 8.70 2.30 -7 3 28 7.30 3.30 -7 3 28 9.50 2.60 7 3 -28 5.10 2.30 7 3 -28 9.00 2.40 -6 -3 28 29.20 5.90 6 -3 -28 28.00 4.80 6 -3 -28 34.70 4.50 6 -3 -28 28.00 4.50 6 -3 -28 28.20 4.90 -6 -3 28 27.80 6.00 -6 3 28 22.20 5.40 6 3 -28 29.20 4.50 -5 -3 28 44.60 6.40 5 -3 -28 43.70 5.70 5 -3 -28 42.90 5.40 5 -3 -28 47.50 5.80 -5 3 28 52.49 6.50 5 3 -28 61.69 6.40 5 3 -28 45.90 5.90 4 -3 -28 382.06 27.20 -4 -3 28 409.56 28.10 4 -3 -28 381.56 25.20 4 -3 -28 386.46 27.00 4 -3 -28 403.36 27.90 4 3 -28 431.06 27.70 -4 3 28 425.26 26.70 -4 3 28 445.46 28.10 4 3 -28 479.95 28.70 3 -3 -28 129.89 10.70 3 -3 -28 127.49 8.70 3 -3 -28 124.39 10.00 -3 -3 28 123.99 10.50 -3 3 28 117.69 9.70 3 3 -28 111.29 10.00 -3 3 28 126.99 10.10 3 3 -28 116.99 11.30 3 3 -28 140.39 11.60 2 -3 -28 1679.83 102.79 -2 -3 28 1697.63 102.99 2 -3 -28 1815.02 103.79 2 -3 -28 1759.02 101.39 -2 3 28 1650.23 102.09 2 3 -28 1896.51 105.99 2 3 -28 1677.73 104.49 1 -3 -28 64.89 5.40 1 -3 -28 54.09 6.00 -1 -3 28 64.59 5.00 -1 -3 28 70.29 6.30 1 -3 -28 56.29 6.60 1 3 -28 42.40 7.30 0 -3 -28 40.10 4.50 0 -3 -28 44.60 4.80 0 -3 -28 38.30 4.40 0 3 28 41.00 3.30 0 3 -28 36.10 6.60 0 3 -28 33.30 6.20 -1 -3 -28 43.80 4.50 -1 -3 -28 41.70 4.70 -1 -3 -28 42.90 4.60 -1 3 -28 59.09 8.40 -1 3 -28 59.99 8.10 -2 -3 -28 1539.15 83.89 -2 -3 -28 1501.65 83.79 -2 -3 -28 1194.18 84.59 -2 3 -28 1290.77 88.69 -2 3 -28 1556.04 88.89 -3 -3 -28 106.39 8.10 3 -3 28 95.49 10.90 -3 -3 -28 92.19 8.50 -3 3 -28 105.09 12.10 -3 3 -28 108.39 11.40 -4 -3 -28 387.26 23.90 -4 3 -28 343.57 28.00 -4 3 -28 367.26 27.40 5 -3 28 36.00 6.30 -5 -3 -28 46.80 5.10 5 3 28 38.10 3.90 -5 3 -28 38.20 6.50 -5 3 -28 51.89 8.30 -6 -3 -28 16.70 5.40 -6 -3 -28 14.00 3.40 6 -3 28 17.90 5.10 -6 -3 -28 20.90 5.90 -6 -3 -28 22.90 5.70 6 -3 28 8.60 3.60 -6 3 -28 24.60 5.10 6 3 28 15.40 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-28 21.90 3.90 9 4 -28 23.30 4.00 8 -4 -28 59.99 6.80 8 -4 -28 63.99 6.50 8 -4 -28 59.99 7.30 -8 4 28 62.49 6.30 8 4 -28 50.69 7.00 -8 4 28 63.69 7.00 8 4 -28 59.69 6.70 7 -4 -28 17.60 3.60 7 -4 -28 13.80 3.70 7 -4 -28 10.00 2.90 7 4 -28 12.50 4.60 7 4 -28 15.40 3.90 -7 4 28 20.30 4.20 -7 4 28 13.10 3.10 7 4 -28 5.50 3.90 -6 -4 28 65.59 9.70 6 -4 -28 72.89 7.40 -6 -4 28 80.19 9.00 6 -4 -28 87.19 8.40 6 -4 -28 72.79 7.70 6 -4 -28 78.39 8.40 6 4 -28 61.89 9.00 -6 4 28 76.39 8.80 -6 4 28 82.69 8.00 -6 4 28 86.09 8.20 5 -4 -28 41.70 5.80 5 4 -28 28.70 4.90 -5 4 28 22.10 4.40 -5 4 28 22.70 4.40 -5 4 28 34.00 5.20 5 4 -28 16.20 4.90 -5 4 28 31.10 4.70 4 -4 -28 0.90 1.70 4 -4 -28 2.70 3.00 4 -4 -28 4.90 2.00 -4 -4 28 2.90 1.90 4 -4 -28 4.20 1.60 4 4 -28 3.60 1.90 4 4 -28 -0.80 2.80 -4 4 28 4.80 1.90 -4 4 28 6.30 1.90 3 -4 -28 423.76 25.00 3 -4 -28 448.86 27.50 -3 -4 28 450.15 27.80 3 -4 -28 439.26 26.50 -3 4 28 355.16 25.60 3 4 -28 351.26 26.00 -3 4 28 397.96 26.50 3 4 -28 332.07 28.80 2 -4 -28 403.76 23.30 -2 -4 28 399.26 25.20 2 -4 -28 400.76 24.40 2 -4 -28 370.36 25.00 2 4 -28 329.67 27.00 2 4 -28 353.16 24.20 -2 4 28 326.17 23.50 -2 4 28 338.57 23.40 1 -4 -28 63.79 6.30 1 -4 -28 65.99 5.80 -1 -4 28 73.99 5.80 1 -4 -28 72.49 7.30 1 4 -28 49.50 8.90 -1 4 28 72.19 6.10 1 4 -28 57.59 8.40 -1 4 28 65.39 5.80 1 4 -28 76.69 7.10 0 -4 -28 276.47 18.70 0 -4 -28 302.17 18.70 0 -4 -28 264.97 19.10 0 4 -28 287.87 19.80 0 4 -28 276.37 22.50 0 4 28 288.47 17.50 0 4 28 267.27 18.40 0 4 -28 255.57 22.70 -1 -4 -28 75.59 5.90 -1 -4 -28 71.79 6.50 -1 -4 -28 62.59 6.20 -1 4 -28 66.79 9.50 -1 4 -28 63.19 7.40 -1 4 -28 50.39 9.00 -2 -4 -28 314.17 22.10 -2 -4 -28 326.57 21.50 -2 4 -28 334.97 23.30 -2 4 -28 386.96 27.20 -2 4 -28 333.77 27.10 3 -4 28 319.97 25.50 -3 -4 -28 350.56 23.50 -3 4 -28 393.16 29.20 -3 4 -28 425.76 28.60 -3 4 -28 339.57 24.50 -4 -4 -28 1.90 1.30 4 -4 28 2.60 2.90 4 4 28 2.30 1.80 -4 4 -28 8.10 3.70 -4 4 -28 2.60 3.00 -5 -4 -28 30.00 3.90 5 -4 28 34.20 8.10 5 -4 28 26.30 6.10 -5 -4 -28 24.90 5.80 -5 -4 -28 31.40 7.10 -5 -4 -28 22.50 4.30 -5 4 -28 37.20 8.20 -5 4 -28 44.30 6.80 -6 -4 -28 82.39 11.30 6 -4 28 72.79 9.10 -6 -4 -28 90.79 10.70 6 -4 28 82.09 14.80 6 -4 28 77.19 11.10 -6 -4 -28 67.79 9.40 6 -4 28 85.09 10.70 -6 -4 -28 77.89 7.30 6 -4 28 77.99 11.00 -6 4 -28 62.09 12.30 -6 4 -28 67.69 8.90 -6 4 -28 55.89 10.20 -6 4 -28 75.69 10.90 -7 -4 -28 11.20 4.70 -7 -4 -28 15.40 4.70 7 -4 28 11.50 4.40 7 -4 28 5.80 2.80 -7 -4 -28 14.40 3.30 -7 -4 -28 7.10 3.50 -7 4 -28 9.00 3.90 -7 4 -28 13.50 4.40 8 -4 28 48.30 9.30 -8 -4 -28 54.89 8.40 -8 -4 -28 49.80 7.80 8 -4 28 56.09 8.10 8 -4 28 38.20 6.60 -8 -4 -28 49.10 5.70 -8 -4 -28 64.79 8.30 -8 4 -28 46.30 7.30 8 4 28 43.00 5.40 -8 4 -28 55.79 8.20 -9 -4 -28 19.90 4.70 -9 -4 -28 14.70 3.80 9 -4 28 9.70 3.50 -9 -4 -28 11.50 3.40 -9 4 -28 15.90 4.10 -9 4 -28 15.00 3.90 9 4 28 12.60 3.70 -9 4 -28 17.90 4.50 10 -4 28 3.70 2.10 -10 -4 -28 6.10 2.30 -10 -4 -28 7.50 2.60 10 -4 28 3.20 2.00 -10 4 -28 6.00 2.10 -10 4 -28 6.10 2.10 -10 4 -28 4.10 2.30 10 4 28 8.00 2.70 -11 -4 -28 13.20 2.80 -11 -4 -28 9.80 2.50 11 -4 28 7.20 1.90 11 -4 28 14.00 2.70 -11 4 -28 10.50 2.80 -11 4 -28 10.20 2.30 11 -5 -28 6.20 1.60 11 -5 -28 5.20 1.60 11 5 -28 5.10 1.40 -11 5 28 7.80 1.80 10 -5 -28 3.30 1.50 10 -5 -28 3.50 3.60 10 -5 -28 2.20 1.80 10 5 -28 1.00 1.30 -10 5 28 1.80 1.30 9 -5 -28 5.30 2.00 9 -5 -28 5.20 2.30 9 5 -28 4.10 1.90 -9 5 28 4.40 2.00 8 -5 -28 14.20 3.50 8 -5 -28 13.40 3.40 8 -5 -28 15.20 3.50 -8 5 28 12.20 3.30 8 5 -28 12.10 3.30 -8 5 28 12.60 3.30 7 -5 -28 111.19 10.10 7 -5 -28 112.89 10.60 7 -5 -28 115.59 10.40 7 -5 -28 113.79 10.80 -7 5 28 111.49 10.30 7 5 -28 126.59 10.40 -7 5 28 136.29 10.90 6 -5 -28 58.09 6.40 -6 -5 28 59.39 8.00 6 -5 -28 71.19 7.50 6 -5 -28 57.49 7.70 6 -5 -28 60.79 7.70 -6 5 28 66.59 6.60 6 5 -28 50.79 8.70 -6 5 28 57.19 6.80 6 5 -28 59.19 6.80 -6 5 28 63.79 8.20 5 -5 -28 8.60 3.00 5 -5 -28 8.90 3.40 -5 -5 28 6.10 2.70 5 -5 -28 11.90 3.20 5 -5 -28 8.20 2.40 -5 -5 28 5.30 5.00 -5 5 28 9.00 2.80 5 5 -28 5.30 2.10 5 5 -28 6.00 3.20 -5 5 28 7.70 2.20 -4 -5 28 32.60 5.30 -4 -5 28 33.90 9.40 4 -5 -28 32.70 4.80 4 -5 -28 25.00 4.00 4 -5 -28 36.90 6.10 4 -5 -28 27.90 4.20 4 5 -28 33.70 7.00 -4 5 28 41.40 4.90 -4 5 28 38.00 4.80 3 -5 -28 50.79 4.60 3 -5 -28 43.90 6.10 3 -5 -28 46.90 5.20 -3 -5 28 51.19 6.50 3 5 -28 36.60 7.20 -3 5 28 38.70 5.50 -3 5 28 47.20 5.10 3 5 -28 41.80 5.60 2 -5 -28 35.10 4.20 2 -5 -28 39.50 5.70 2 -5 -28 39.60 4.60 2 5 -28 36.80 7.20 -2 5 28 44.50 4.60 -2 5 28 45.20 5.00 2 5 -28 42.50 5.20 1 -5 -28 217.28 14.30 1 -5 -28 180.18 15.40 1 -5 -28 214.78 14.80 -1 5 28 208.88 14.00 1 5 -28 190.58 18.60 1 5 -28 200.38 15.30 1 5 -28 202.28 19.70 0 -5 -28 409.06 27.80 0 -5 28 460.25 28.40 0 -5 -28 444.96 28.00 0 5 -28 434.86 32.90 0 5 -28 434.16 29.40 0 5 28 439.76 27.40 -1 -5 -28 205.48 13.50 -1 -5 -28 196.08 14.50 -1 5 -28 192.48 15.50 -1 5 -28 183.28 18.70 -1 5 -28 215.08 18.60 1 5 28 205.78 13.60 -2 -5 -28 42.10 4.60 -2 -5 -28 34.60 4.70 -2 5 -28 32.50 6.80 2 5 28 34.50 3.80 -2 5 -28 29.30 5.40 -2 5 -28 42.50 7.00 -3 -5 -28 45.70 5.20 3 -5 28 37.50 6.50 3 5 28 45.10 4.30 -3 5 -28 55.19 8.50 -3 5 -28 50.09 7.60 -3 5 -28 45.40 6.40 4 -5 28 47.20 7.20 -4 -5 -28 34.40 4.80 4 -5 28 35.70 8.00 -4 -5 -28 38.60 7.20 4 -5 28 30.30 7.70 4 5 28 27.70 3.40 -4 5 -28 26.90 7.10 -4 5 -28 36.70 6.90 -4 5 -28 22.00 4.50 -5 -5 -28 12.90 6.10 -5 -5 -28 10.70 3.80 5 -5 28 4.90 3.20 5 -5 28 4.20 3.70 -5 -5 -28 10.50 3.80 5 -5 28 8.30 3.80 -5 -5 -28 5.40 1.90 5 -5 28 8.00 4.40 5 -5 28 12.70 4.70 -5 -5 -28 5.40 2.10 -5 5 -28 4.40 4.60 -5 5 -28 3.30 4.00 -5 5 -28 8.80 3.40 -5 5 -28 0.20 4.80 6 -5 28 70.49 9.40 -6 -5 -28 55.49 7.70 6 -5 28 41.90 7.10 -6 -5 -28 49.99 5.90 6 -5 28 73.59 11.10 6 -5 28 71.09 9.30 -6 -5 -28 64.09 9.60 -6 5 -28 60.19 9.50 -6 5 -28 47.70 8.70 -6 5 -28 55.69 12.50 7 -5 28 96.49 12.00 -7 -5 -28 118.19 12.40 -7 -5 -28 91.69 11.40 -7 -5 -28 131.69 13.50 7 -5 28 115.09 12.70 -7 -5 -28 112.79 9.10 -7 5 -28 77.79 10.90 -7 5 -28 100.59 12.70 -8 -5 -28 10.30 2.40 -8 -5 -28 3.90 3.00 8 -5 28 8.70 3.90 -8 -5 -28 7.60 3.50 8 -5 28 9.50 4.20 -8 5 -28 10.80 3.90 9 -5 28 5.70 3.90 9 -5 28 2.60 2.40 -9 -5 -28 -0.60 1.70 -9 -5 -28 5.70 2.50 -9 -5 -28 6.00 2.30 -9 5 -28 -0.90 2.30 -9 5 -28 3.40 1.70 -10 -5 -28 2.00 1.40 10 -5 28 -0.20 1.00 10 -5 28 1.70 1.60 -10 -5 -28 1.60 1.50 10 -5 28 2.80 1.70 -10 5 -28 1.40 1.60 -10 5 -28 1.70 1.60 -11 -5 -28 3.60 1.20 11 -5 28 3.00 1.40 11 -5 28 2.90 1.20 -11 -5 -28 1.10 1.20 -11 5 -28 5.90 1.30 -11 5 -28 6.80 1.90 10 -6 -28 83.19 6.80 10 -6 -28 80.29 6.60 -10 6 28 67.89 6.20 10 6 -28 57.39 5.60 9 -6 -28 8.50 2.70 9 -6 -28 8.40 2.40 9 -6 -28 3.80 1.90 -9 6 28 7.30 2.10 9 6 -28 6.20 2.20 8 -6 -28 2.50 1.90 8 -6 -28 4.40 2.20 8 -6 -28 0.80 1.70 8 6 -28 2.90 1.70 -8 6 28 1.90 1.60 7 -6 -28 56.79 6.40 7 -6 -28 42.80 6.10 -7 6 28 43.60 5.30 7 6 -28 36.10 5.00 -7 6 28 44.40 5.60 6 -6 -28 2.10 2.30 6 -6 -28 2.40 3.00 6 -6 -28 4.60 1.70 6 6 -28 4.00 2.10 -6 6 28 2.40 1.50 -6 6 28 3.60 1.90 5 -6 -28 68.89 8.50 -5 -6 28 68.19 9.60 -5 -6 28 66.99 8.80 5 -6 -28 57.69 7.80 5 -6 -28 66.09 6.60 5 -6 -28 68.39 8.10 -5 6 28 63.69 6.20 -5 6 28 55.49 6.60 -5 6 28 46.30 7.80 -5 6 28 60.29 6.10 5 6 -28 56.59 6.60 4 -6 -28 68.39 8.70 4 -6 -28 80.59 7.00 4 -6 -28 76.99 8.70 4 -6 -28 84.29 9.20 4 -6 -28 91.19 7.60 -4 -6 28 77.49 11.00 -4 6 28 78.69 6.90 4 6 -28 56.59 9.30 4 6 -28 64.89 7.40 -4 6 28 72.99 7.10 -4 6 28 69.69 8.00 3 -6 -28 24.50 5.20 3 -6 -28 17.10 4.40 -3 -6 28 12.20 5.00 3 -6 -28 23.20 3.70 3 -6 -28 21.70 3.60 3 6 -28 14.30 5.80 -3 6 28 16.00 4.50 -3 6 28 27.10 3.70 -3 6 28 31.40 3.70 3 6 -28 28.00 4.50 2 -6 -28 147.69 10.90 -2 -6 28 155.38 16.50 2 -6 -28 134.79 12.70 2 -6 -28 152.38 11.40 2 6 -28 153.88 12.10 2 6 -28 108.89 13.80 -2 6 28 138.39 11.40 -2 6 28 131.59 10.60 -2 6 28 149.99 10.60 1 -6 -28 112.89 9.30 1 -6 -28 112.59 9.10 1 6 -28 110.19 13.80 -1 6 28 111.19 8.60 1 6 -28 110.59 10.20 1 6 -28 87.59 12.30 0 -6 -28 23.50 3.50 0 -6 -28 26.50 3.70 0 -6 28 20.00 4.70 0 6 -28 27.10 6.10 0 6 -28 15.00 4.70 0 6 28 22.20 3.10 1 -6 28 85.39 15.80 -1 -6 -28 97.79 9.10 1 -6 28 105.19 9.80 -1 -6 -28 109.49 7.80 -1 6 -28 107.99 12.70 1 6 28 97.99 7.90 -1 6 -28 119.79 12.80 -1 6 -28 101.89 9.90 -2 -6 -28 162.78 15.10 -2 -6 -28 125.69 11.50 -2 -6 -28 145.09 12.40 2 -6 28 160.08 12.80 2 -6 28 149.59 16.70 -2 6 -28 142.09 14.70 -2 6 -28 131.79 12.50 -2 6 -28 155.98 16.10 2 6 28 152.28 10.40 -2 6 -28 123.79 15.60 -3 -6 -28 26.50 5.00 3 -6 28 20.80 6.30 -3 -6 -28 22.50 5.40 3 -6 28 16.10 5.50 -3 -6 -28 25.20 4.00 -3 -6 -28 25.30 4.00 3 6 28 15.80 3.00 -3 6 -28 7.00 4.30 -3 6 -28 6.50 5.20 -3 6 -28 13.70 5.10 -4 -6 -28 61.59 8.80 -4 -6 -28 65.19 6.70 4 -6 28 84.89 10.60 -4 -6 -28 60.69 6.70 4 -6 28 86.69 11.70 -4 -6 -28 62.19 9.90 4 -6 28 78.59 10.90 4 -6 28 76.99 11.30 -4 6 -28 78.99 8.10 -4 6 -28 69.49 11.40 -4 6 -28 84.39 10.20 -4 6 -28 72.09 10.80 4 6 28 74.49 6.20 -4 6 -28 90.79 12.50 -5 -6 -28 58.79 5.90 5 -6 28 45.00 10.20 -5 -6 -28 65.49 9.60 5 -6 28 66.29 11.20 5 -6 28 59.39 9.30 -5 -6 -28 53.09 6.00 5 -6 28 63.89 9.30 -5 -6 -28 59.49 9.80 -5 -6 -28 51.29 7.70 -5 6 -28 50.39 8.80 -5 6 -28 54.09 10.80 -5 6 -28 61.79 10.20 -5 6 -28 64.99 8.90 6 -6 28 -4.50 3.10 6 -6 28 7.00 3.20 -6 -6 -28 2.60 2.60 -6 -6 -28 -1.90 3.40 -6 -6 -28 0.10 1.30 6 -6 28 6.60 2.90 -6 -6 -28 6.00 3.50 -6 6 -28 0.60 3.10 -6 6 -28 11.30 3.70 7 -6 28 26.40 7.00 -7 -6 -28 32.50 6.50 7 -6 28 31.90 6.20 -7 -6 -28 40.40 4.40 -7 -6 -28 39.90 6.50 -7 -6 -28 42.00 7.10 7 -6 28 26.00 6.50 -7 6 -28 34.10 7.30 -7 6 -28 22.20 5.70 8 -6 28 6.20 3.50 -8 -6 -28 1.90 2.30 8 -6 28 3.40 2.50 -8 -6 -28 0.90 1.00 -8 -6 -28 -2.00 1.80 8 -6 28 -1.10 1.70 -8 -6 -28 -0.60 1.80 -8 6 -28 0.50 2.30 9 -6 28 6.10 2.30 9 -6 28 2.20 2.30 9 -6 28 2.20 3.90 9 -6 28 2.60 1.90 -9 -6 -28 3.40 2.00 -9 -6 -28 2.30 2.10 -9 -6 -28 5.50 2.20 -9 6 -28 4.80 2.40 -9 6 -28 4.60 2.20 -10 -6 -28 63.39 5.80 10 -6 28 51.09 6.00 -10 -6 -28 56.99 5.80 10 -6 28 63.09 5.60 -10 6 -28 60.59 6.20 -10 6 -28 60.39 6.40 9 -7 -28 93.59 8.10 9 -7 -28 95.09 8.60 9 7 -28 119.49 7.90 -9 7 28 97.69 8.60 8 -7 -28 -0.50 1.30 8 -7 -28 -1.00 2.20 8 -7 -28 1.20 1.40 8 -7 -28 0.90 1.60 -8 7 28 0.60 1.20 8 7 -28 1.70 1.50 7 -7 -28 -1.90 1.70 7 -7 -28 1.90 1.40 7 -7 -28 2.90 1.70 7 -7 -28 2.30 2.50 7 7 -28 0.00 1.50 -7 7 28 2.10 1.50 6 -7 -28 31.10 6.20 6 -7 -28 37.80 4.60 6 -7 -28 36.00 5.60 6 7 -28 38.20 4.80 -6 7 28 36.40 4.70 -6 7 28 34.20 5.30 5 -7 -28 118.29 11.20 5 -7 -28 135.39 11.10 5 -7 -28 116.39 9.90 5 7 -28 112.89 9.90 -5 7 28 118.69 10.80 -5 7 28 111.99 9.60 -5 7 28 113.69 9.50 4 -7 -28 14.20 4.00 4 -7 -28 16.20 3.40 -4 -7 28 8.30 3.90 4 -7 -28 17.40 3.80 4 -7 -28 19.00 4.50 -4 7 28 27.90 5.30 -4 7 28 17.70 3.10 -4 7 28 11.10 4.20 4 7 -28 7.00 5.40 4 7 -28 18.70 3.70 4 7 -28 25.20 7.20 -4 7 28 13.10 3.00 3 -7 -28 16.90 3.90 -3 -7 28 3.60 3.40 3 -7 -28 8.10 2.30 3 -7 -28 7.90 2.20 -3 7 28 7.60 2.20 3 7 -28 15.70 6.10 -3 7 28 10.00 2.40 3 7 -28 5.70 3.60 -3 7 28 8.80 3.30 3 7 -28 8.10 2.40 2 -7 -28 26.30 4.60 2 -7 -28 30.00 4.20 -2 -7 28 33.10 7.10 2 -7 -28 27.80 4.30 -2 -7 28 25.60 4.90 2 7 -28 37.10 9.40 2 7 -28 30.40 4.90 -2 7 28 31.90 3.70 -2 7 28 29.70 3.70 2 7 -28 19.30 5.40 1 -7 -28 150.68 14.20 1 -7 -28 125.39 11.00 1 -7 -28 136.49 11.10 -1 -7 28 142.39 12.70 -1 -7 28 142.69 15.50 1 -7 -28 129.59 11.60 1 7 -28 155.88 15.50 -1 7 28 159.88 10.90 1 7 -28 149.49 13.10 1 7 -28 138.79 16.00 -1 7 28 140.89 10.70 0 -7 28 30.70 8.50 0 -7 -28 31.50 3.80 0 -7 28 32.90 6.20 0 -7 -28 32.60 6.70 0 -7 -28 32.00 4.60 0 7 -28 31.40 8.00 0 7 28 35.70 4.00 0 7 -28 28.10 5.20 0 7 28 38.80 4.70 0 7 -28 41.90 8.00 0 7 -28 39.30 8.00 1 -7 28 151.18 12.80 -1 -7 -28 145.89 12.30 -1 -7 -28 133.99 11.70 1 -7 28 163.18 14.50 1 -7 28 157.38 16.70 -1 -7 -28 161.28 12.80 -1 -7 -28 175.18 15.70 1 7 28 140.59 10.40 -1 7 -28 129.99 14.60 1 7 28 130.39 10.90 -1 7 -28 129.69 12.40 -1 7 -28 147.09 16.20 -1 7 -28 138.49 15.30 -2 -7 -28 25.60 4.70 -2 -7 -28 28.30 6.20 2 -7 28 26.10 6.20 2 -7 28 35.10 9.50 2 -7 28 25.00 6.10 -2 -7 -28 26.90 4.70 2 -7 28 25.40 7.20 -2 -7 -28 31.00 4.80 2 7 28 22.60 3.20 -2 7 -28 31.40 8.20 -2 7 -28 20.40 10.60 -2 7 -28 22.60 5.50 -2 7 -28 21.60 6.10 -2 7 -28 36.40 5.60 3 -7 28 13.30 4.90 -3 -7 -28 7.20 2.60 -3 -7 -28 9.80 2.90 3 -7 28 10.00 7.10 -3 -7 -28 7.30 3.10 3 -7 28 4.40 3.20 -3 -7 -28 11.20 2.90 3 -7 28 7.00 3.50 3 -7 28 4.50 4.10 -3 7 -28 8.70 3.90 -3 7 -28 8.60 4.70 3 7 28 9.30 2.50 -3 7 -28 6.50 2.60 -3 7 -28 7.90 4.30 -3 7 -28 18.40 7.50 4 -7 28 3.70 7.30 4 -7 28 6.60 4.50 4 -7 28 12.00 3.70 -4 -7 -28 12.80 3.80 -4 -7 -28 13.60 3.00 4 -7 28 15.10 5.00 -4 -7 -28 12.10 4.00 4 7 28 15.30 2.50 -4 7 -28 13.00 4.20 -4 7 -28 12.60 5.30 -4 7 -28 10.90 3.90 -4 7 -28 11.10 3.30 -5 -7 -28 95.29 8.80 -5 -7 -28 123.99 13.70 5 -7 28 107.29 12.20 5 -7 28 96.39 10.80 5 -7 28 125.19 13.00 -5 -7 -28 97.39 10.50 -5 7 -28 101.19 14.10 -5 7 -28 111.79 12.40 -6 -7 -28 32.20 4.10 -6 -7 -28 36.30 6.30 6 -7 28 27.30 5.80 6 -7 28 34.80 6.80 -6 -7 -28 45.90 7.20 -6 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-4 8 28 60.79 5.90 -4 8 28 52.99 5.70 4 8 -28 51.09 9.40 4 8 -28 63.89 7.00 3 -8 -28 8.40 2.70 -3 -8 28 10.10 3.50 -3 8 28 4.20 1.50 -3 8 28 3.20 1.50 3 8 -28 5.50 4.50 3 8 -28 4.00 2.60 -2 -8 28 63.39 8.10 2 -8 -28 46.10 5.70 2 -8 -28 60.79 7.90 2 -8 -28 47.30 6.00 2 8 -28 39.00 9.10 2 8 -28 51.79 6.80 -2 8 28 47.30 5.20 -2 8 28 58.39 5.30 1 -8 -28 27.80 5.00 1 -8 -28 31.20 4.00 -1 -8 28 37.10 5.40 1 -8 -28 30.70 5.90 -1 -8 28 35.20 7.30 1 8 -28 24.40 6.50 -1 8 28 24.80 3.30 1 8 -28 23.20 4.60 0 -8 -28 0.70 1.90 0 -8 -28 2.00 2.70 0 -8 28 -0.20 2.90 0 -8 28 -0.60 2.10 0 8 28 -1.60 1.30 0 8 28 1.20 1.00 0 8 -28 -3.00 3.70 -1 -8 -28 27.50 5.80 -1 -8 -28 23.00 4.30 1 -8 28 34.00 6.10 -1 -8 -28 25.50 4.30 -1 8 -28 33.00 7.40 1 8 28 37.00 4.60 -1 8 -28 23.30 6.40 -1 8 -28 33.80 5.40 1 8 28 34.20 3.70 -2 -8 -28 42.10 5.70 -2 -8 -28 48.40 6.30 2 -8 28 48.10 8.50 2 -8 28 52.89 7.50 -2 -8 -28 62.69 8.20 -2 8 -28 49.70 9.40 -2 8 -28 46.30 6.30 -2 8 -28 54.89 9.10 2 8 28 51.39 4.90 3 -8 28 8.40 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2.10 1 2 68 11.10 2.10 -1 2 -68 7.40 1.90 2 -2 68 57.19 6.00 2 -2 68 58.89 5.20 2 2 68 56.49 5.20 -2 2 -68 50.79 5.00 2 2 68 44.90 4.60 3 -2 68 12.50 3.50 3 -2 68 17.30 2.60 3 2 68 17.90 2.50 3 2 68 11.50 2.20 4 -2 68 18.50 2.60 4 2 68 16.70 3.00 -3 3 68 62.79 5.00 3 3 -68 67.89 5.40 -2 -3 68 16.00 3.00 -2 3 68 15.80 2.20 2 3 -68 16.50 2.30 -1 -3 68 26.20 3.80 1 3 -68 22.30 2.90 -1 3 68 24.60 2.80 0 -3 68 1.90 1.40 0 3 -68 2.30 1.20 0 3 -68 3.30 1.90 0 3 68 4.30 1.30 1 -3 68 17.30 2.90 1 -3 68 24.10 3.50 -1 3 -68 23.10 3.00 -1 3 -68 21.30 4.10 1 3 68 22.70 2.80 2 -3 68 18.30 2.60 2 -3 68 14.80 3.10 2 3 68 18.80 2.50 2 3 68 15.60 2.30 3 -3 68 61.29 5.20 3 -3 68 60.29 5.60 3 3 68 64.69 5.20 3 3 68 53.19 4.50 -2 -4 68 23.20 3.10 2 4 -68 29.60 2.90 -2 4 68 24.70 2.60 -1 -4 68 26.50 3.50 1 4 -68 26.60 2.90 -1 4 68 23.20 2.70 0 -4 68 1.80 1.20 0 4 68 1.70 0.80 0 4 -68 0.50 0.90 1 -4 68 25.90 3.50 1 -4 68 23.60 3.00 1 4 68 29.90 3.00 -1 4 -68 30.40 2.80 2 -4 68 24.60 2.80 2 -4 68 26.10 3.30 2 4 68 23.90 2.90 4 0 -69 4.90 1.20 3 0 -69 0.40 0.90 -3 0 69 -0.60 1.00 -3 0 69 2.00 1.60 2 0 -69 3.20 1.20 -2 0 69 -0.20 1.40 2 0 -69 1.00 1.30 -1 0 69 14.20 2.40 1 0 -69 11.10 2.60 0 0 69 -0.80 1.70 0 0 -69 2.20 1.40 0 0 69 -0.60 0.80 1 0 69 20.30 2.90 1 0 69 14.70 4.10 -1 0 -69 13.70 2.70 2 0 69 3.20 1.20 3 0 69 -0.70 0.80 4 0 69 6.20 1.60 -4 -1 69 -0.80 1.00 -4 1 69 0.40 1.00 -3 1 69 3.80 1.10 3 1 -69 3.30 1.20 2 -1 -69 42.20 4.80 -2 -1 69 45.60 4.10 -2 1 69 45.00 4.30 2 1 -69 47.50 4.10 1 -1 -69 1.80 1.60 -1 -1 69 -1.60 1.40 -1 -1 69 1.80 1.10 1 1 -69 0.30 1.10 -1 1 69 -1.60 1.70 -1 1 69 0.50 1.00 1 1 -69 1.00 1.30 0 -1 69 13.50 2.40 0 -1 69 13.20 3.50 0 -1 -69 9.70 2.20 0 1 -69 14.70 2.90 0 1 69 17.60 2.50 1 -1 69 -0.20 1.40 1 -1 69 -0.10 1.00 -1 1 -69 1.40 1.50 1 1 69 1.40 1.10 2 -1 69 40.30 5.50 2 -1 69 49.30 4.60 2 1 69 48.70 4.60 3 -1 69 5.20 1.40 3 1 69 7.80 1.80 4 -1 69 17.80 2.40 4 1 69 16.60 2.40 2 2 -69 5.10 1.30 -1 -2 69 47.40 4.00 1 2 -69 43.20 4.00 1 2 -69 33.60 6.90 -1 2 69 47.70 4.30 0 -2 69 5.70 1.90 0 -2 69 3.00 1.20 0 2 -69 2.90 1.70 0 2 69 4.20 1.20 0 2 -69 2.30 1.30 1 -2 69 43.90 5.20 1 -2 69 47.50 4.40 1 2 69 44.70 4.40 -1 2 -69 40.00 4.80 2 -2 69 6.70 2.10 2 -2 69 10.40 2.00 2 2 69 12.00 2.10 3 -2 69 11.50 2.10 3 2 69 12.30 2.00 -2 -3 69 10.60 2.30 -2 3 69 10.00 1.70 -1 -3 69 5.30 1.70 -1 3 69 7.50 1.70 1 3 -69 7.50 1.80 0 -3 69 1.10 1.20 0 -3 69 1.00 1.50 0 3 69 0.20 0.60 0 3 -69 0.70 1.00 1 -3 69 8.50 2.30 1 -3 69 5.50 1.50 1 3 69 4.90 1.40 2 -3 69 9.20 2.40 2 -3 69 9.60 2.00 2 3 69 10.70 1.90 3 -3 69 22.40 3.20 -1 -4 69 16.60 2.70 -1 4 69 15.20 2.00 1 4 -69 15.80 2.20 0 -4 69 4.40 1.40 0 4 69 5.90 1.30 0 4 -69 4.10 1.20 1 -4 69 19.30 2.80 1 4 69 16.00 2.30 3 0 -70 8.90 1.80 -2 0 70 37.30 3.50 2 0 -70 32.30 3.10 1 0 -70 2.20 2.50 -1 0 70 -1.20 1.60 0 0 70 -1.00 0.80 0 0 70 -0.40 1.60 0 0 -70 1.30 1.90 1 0 70 6.50 2.30 2 0 70 38.80 4.00 3 0 70 8.90 1.90 -2 -1 70 3.50 1.50 2 1 -70 6.40 1.50 -1 -1 70 3.30 1.20 -1 1 70 0.80 1.90 -1 1 70 2.40 1.10 1 1 -70 1.10 1.20 0 -1 70 5.20 1.70 1 -1 70 7.00 2.20 1 -1 70 2.20 1.10 1 1 70 1.90 1.00 2 -1 70 3.30 2.40 2 -1 70 8.60 2.00 2 1 70 6.70 1.70 3 -1 70 32.60 3.40 3 1 70 27.40 3.10 -3 -2 70 -1.50 0.90 -3 2 70 0.30 0.90 3 2 -70 -0.30 0.60 -3 2 70 -0.10 1.20 -2 -2 70 0.90 1.20 -2 2 70 -1.40 1.50 -2 2 70 2.90 1.20 -1 -2 70 6.30 1.70 1 2 -70 9.70 1.90 -1 2 70 9.10 1.90 0 -2 70 47.00 4.70 0 -2 70 36.60 3.70 0 2 -70 38.00 3.80 0 2 70 37.90 3.80 1 -2 70 6.80 2.00 1 -2 70 9.70 2.00 1 2 70 7.40 1.90 2 -2 70 4.20 1.70 2 -2 70 3.90 1.40 2 2 70 3.40 1.10 3 -2 70 -0.90 0.80 3 2 70 0.30 0.70 2 3 -70 0.40 0.70 -2 3 70 0.80 0.60 -1 -3 70 35.30 4.00 1 3 -70 26.00 2.80 -1 3 70 29.00 3.00 0 -3 70 15.90 2.80 0 3 -70 8.60 2.10 0 3 70 12.10 1.90 1 -3 70 28.30 3.30 1 -3 70 30.40 3.70 1 3 70 31.80 3.30 2 -3 70 -1.70 1.10 2 -3 70 -0.80 1.20 2 3 70 0.50 0.70 -2 0 71 6.10 1.30 -1 0 71 2.30 1.10 -1 0 71 -0.80 1.40 0 0 71 1.70 1.50 0 0 71 -0.20 0.80 1 0 71 3.60 1.20 1 0 71 1.50 2.20 2 0 71 8.00 1.80 -1 -1 71 23.60 2.60 -1 -1 71 16.40 3.20 0 -1 71 1.80 1.00 0 -1 71 1.70 1.50 0 1 71 -0.40 1.80 0 1 71 1.70 0.90 1 -1 71 22.00 2.90 1 -1 71 30.00 3.90 1 1 71 27.80 3.00 2 -1 71 6.70 1.60 -2 -2 71 -1.10 0.90 -2 2 71 0.00 1.60 -2 2 71 0.00 0.70 2 2 -71 1.30 0.80 -1 -2 71 8.00 2.00 -1 2 71 3.70 2.50 1 2 -71 9.10 2.00 -1 2 71 13.20 2.00 0 -2 71 7.20 1.90 0 -2 71 7.10 1.50 0 2 71 6.80 1.70 1 -2 71 10.20 2.10 1 2 71 9.90 2.00 2 -2 71 2.40 1.00 2 -2 71 2.80 1.50 2 2 71 3.00 0.90 -2 0 72 1.80 1.30 0 0 72 7.80 1.90 0 0 72 10.80 1.90 1 0 72 29.50 3.20 2 0 72 2.80 1.10 -1 -1 72 4.90 1.20 -1 -1 72 3.90 1.40 0 -1 72 27.70 3.50 0 -1 72 27.40 2.80 0 1 72 28.30 2.90 1 -1 72 5.90 2.10 1 -1 72 7.00 1.60 1 1 72 8.00 1.60 0 -2 72 1.80 1.10 0 -2 72 3.70 1.60 0 2 72 2.00 0.90 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 55605 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' '-y+1/2, x+1/2, z+3/4' 'y+1/2, -x+1/2, z+1/4' '-x+1/2, y+1/2, -z+3/4' 'x+1/2, -y+1/2, -z+1/4' 'y, x, -z' '-y, -x, -z+1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Rh1 Rh 0.82348(2) 0.52864(2) 0.41807(2) 0.04705(9) Uani 1 1 d . . . . . C1 C 0.9276(4) 0.7092(4) 0.46193(6) 0.0544(8) Uani 1 1 d . . . . . O1 O 0.7712(3) 0.1714(3) 0.44695(5) 0.0707(7) Uani 1 1 d . . . . . N1 N 0.8248(3) 0.3381(3) 0.42770(5) 0.0515(6) Uani 1 1 d . . . . . P1 P 0.89418(8) 0.55587(8) 0.45215(2) 0.04656(19) Uani 1 1 d . . . . . F1 F 0.5071(6) -0.0781(5) 0.41896(9) 0.181(2) Uani 1 1 d . . . . . S1 S 0.46031(13) 0.02226(17) 0.45682(2) 0.0940(4) Uani 1 1 d . . . . . Cl1 Cl 0.77298(10) 0.46908(11) 0.37999(2) 0.0666(2) Uani 1 1 d . . . . . F2 F 0.3207(5) -0.0323(5) 0.42361(8) 0.1574(19) Uani 1 1 d . . . . . N2 N 1.0091(3) 0.5406(3) 0.40744(5) 0.0511(7) Uani 1 1 d . . . . . O2 O 1.2087(2) 0.5012(3) 0.40430(5) 0.0720(8) Uani 1 1 d . . . . . C2 C 1.0478(4) 0.7478(4) 0.46310(7) 0.0682(10) Uani 1 1 d . . . . . H2 H 1.110532 0.692771 0.460186 0.082 Uiso 1 1 calc R U . . . F3 F 0.3944(6) -0.1860(4) 0.44019(8) 0.1582(18) Uani 1 1 d . . . . . O3 O 0.5652(5) -0.0388(7) 0.46528(11) 0.170(3) Uani 1 1 d . . . . . C3 C 1.0757(6) 0.8678(5) 0.46857(9) 0.0882(16) Uani 1 1 d . . . . . H3 H 1.156927 0.892453 0.469402 0.106 Uiso 1 1 calc R U . . . C9 C 0.6962(5) 0.4649(5) 0.50706(7) 0.0757(12) Uani 1 1 d . . . . . H9 H 0.676566 0.500134 0.520602 0.091 Uiso 1 1 calc R U . . . C8 C 0.7661(4) 0.5292(4) 0.49194(6) 0.0626(9) Uani 1 1 d . . . . . H8 H 0.793144 0.607576 0.495313 0.075 Uiso 1 1 calc R U . . . C7 C 0.7957(3) 0.4769(3) 0.47182(6) 0.0518(7) Uani 1 1 d . . . . . C6 C 0.8363(4) 0.7954(4) 0.46674(7) 0.0668(10) Uani 1 1 d . . . . . H6 H 0.754664 0.771689 0.466398 0.080 Uiso 1 1 calc R U . . . C5 C 0.8653(6) 0.9139(4) 0.47193(8) 0.0811(14) Uani 1 1 d . . . . . H5 H 0.803774 0.970169 0.474909 0.097 Uiso 1 1 calc R U . . . O5 O 0.3545(5) 0.0160(6) 0.47030(7) 0.136(2) Uani 1 1 d . . . . . C4 C 0.9853(7) 0.9492(4) 0.47272(8) 0.0890(17) Uani 1 1 d . . . . . H4 H 1.004822 1.029712 0.476122 0.107 Uiso 1 1 calc R U . . . O4 O 0.4815(4) 0.1394(4) 0.44641(8) 0.1142(13) Uani 1 1 d . . . . . C10 C 0.6557(5) 0.3492(5) 0.50217(8) 0.0830(14) Uani 1 1 d . . . . . H10 H 0.606753 0.307477 0.512242 0.100 Uiso 1 1 calc R U . . . C11 C 0.6871(4) 0.2944(4) 0.48239(7) 0.0723(11) Uani 1 1 d . . . . . H11 H 0.661220 0.215243 0.479371 0.087 Uiso 1 1 calc R U . . . C13 C 0.7875(4) 0.2925(3) 0.44613(7) 0.0568(9) Uani 1 1 d . . . . . C12 C 0.7572(4) 0.3571(4) 0.46701(6) 0.0565(9) Uani 1 1 d . . . . . C14 C 0.7775(5) 0.1296(4) 0.42400(8) 0.0735(11) Uani 1 1 d . . . . . H14A H 0.696388 0.117548 0.417929 0.088 Uiso 1 1 calc R U . . . H14B H 0.822897 0.053738 0.422881 0.088 Uiso 1 1 calc R U . . . C16 C 0.9801(4) 0.2136(4) 0.40759(7) 0.0659(10) Uani 1 1 d . . . . . H16 H 1.016719 0.294430 0.405447 0.079 Uiso 1 1 calc R U . . . C15 C 0.8443(4) 0.2335(4) 0.41200(6) 0.0579(9) Uani 1 1 d . . . . . H15 H 0.802541 0.250923 0.398000 0.069 Uiso 1 1 calc R U . . . C17 C 1.0477(5) 0.1532(5) 0.42679(9) 0.0884(15) Uani 1 1 d . . . . . H17A H 1.017026 0.071852 0.428906 0.133 Uiso 1 1 calc R U . . . H17B H 1.035141 0.199988 0.440029 0.133 Uiso 1 1 calc R U . . . H17C H 1.133447 0.149794 0.423496 0.133 Uiso 1 1 calc R U . . . C19 C 1.0373(3) 0.4731(4) 0.45609(6) 0.0531(8) Uani 1 1 d . . . . . C18 C 0.9969(5) 0.1432(6) 0.38599(10) 0.1004(19) Uani 1 1 d . . . . . H18A H 0.960911 0.188431 0.374044 0.151 Uiso 1 1 calc R U . . . H18B H 0.957751 0.064901 0.387165 0.151 Uiso 1 1 calc R U . . . H18C H 1.082461 0.131876 0.383184 0.151 Uiso 1 1 calc R U . . . C20 C 1.0612(4) 0.4272(4) 0.47695(7) 0.0675(10) Uani 1 1 d . . . . . H20 H 1.006100 0.440984 0.488400 0.081 Uiso 1 1 calc R U . . . C21 C 1.1677(5) 0.3603(5) 0.48093(8) 0.0817(14) Uani 1 1 d . . . . . H21 H 1.182194 0.328345 0.494946 0.098 Uiso 1 1 calc R U . . . C22 C 1.2507(4) 0.3415(5) 0.46437(8) 0.0783(13) Uani 1 1 d . . . . . H22 H 1.321863 0.297519 0.467136 0.094 Uiso 1 1 calc R U . . . C23 C 1.2288(4) 0.3875(4) 0.44371(7) 0.0661(10) Uani 1 1 d . . . . . H23 H 1.285265 0.374213 0.432470 0.079 Uiso 1 1 calc R U . . . C24 C 1.1232(3) 0.4540(4) 0.43923(6) 0.0545(8) Uani 1 1 d . . . . . C25 C 1.1065(3) 0.5014(3) 0.41664(6) 0.0543(8) Uani 1 1 d . . . . . C26 C 1.1683(5) 0.5305(5) 0.38186(8) 0.0845(14) Uani 1 1 d . . . . . H26A H 1.163659 0.457296 0.372853 0.101 Uiso 1 1 calc R U . . . H26B H 1.223775 0.587896 0.374890 0.101 Uiso 1 1 calc R U . . . C27 C 1.0431(4) 0.5867(4) 0.38483(6) 0.0618(9) Uani 1 1 d . . . . . H27 H 0.987176 0.551510 0.373891 0.074 Uiso 1 1 calc R U . . . C28 C 1.0373(5) 0.7245(4) 0.38338(7) 0.0737(11) Uani 1 1 d . . . . . H28 H 0.953123 0.749499 0.386521 0.088 Uiso 1 1 calc R U . . . C29 C 1.0687(6) 0.7663(6) 0.35980(8) 0.0999(18) Uani 1 1 d . . . . . H29A H 1.017242 0.724358 0.349415 0.150 Uiso 1 1 calc R U . . . H29B H 1.152711 0.747934 0.356689 0.150 Uiso 1 1 calc R U . . . H29C H 1.055658 0.852794 0.358558 0.150 Uiso 1 1 calc R U . . . C30 C 1.1211(8) 0.7883(6) 0.40012(9) 0.118(3) Uani 1 1 d . . . . . H30A H 1.204880 0.772234 0.396419 0.177 Uiso 1 1 calc R U . . . H30B H 1.104301 0.757877 0.414704 0.177 Uiso 1 1 calc R U . . . H30C H 1.106557 0.874804 0.399725 0.177 Uiso 1 1 calc R U . . . C31 C 0.7622(4) 0.7104(4) 0.41054(7) 0.0664(10) Uani 1 1 d . . . . . H31A H 0.811287 0.776906 0.416340 0.080 Uiso 1 1 calc R U . . . H31B H 0.733503 0.724440 0.395567 0.080 Uiso 1 1 calc R U . . . C32 C 0.6778(4) 0.6562(4) 0.42539(7) 0.0625(9) Uani 1 1 d . . . . . H32 H 0.672109 0.689182 0.440428 0.075 Uiso 1 1 calc R U . . . C33 C 0.6186(3) 0.5460(4) 0.42077(7) 0.0631(10) Uani 1 1 d . . . . . H33 H 0.580060 0.547724 0.406140 0.076 Uiso 1 1 calc R U . . . C34 C 0.5383(4) 0.4854(5) 0.43741(7) 0.0744(12) Uani 1 1 d . . . . . H34A H 0.456858 0.517248 0.436183 0.112 Uiso 1 1 calc R U . . . H34B H 0.569187 0.501018 0.452009 0.112 Uiso 1 1 calc R U . . . H34C H 0.537225 0.398924 0.434759 0.112 Uiso 1 1 calc R U . . . C35 C 0.4202(7) -0.0729(6) 0.43389(10) 0.1015(18) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Rh1 0.04436(13) 0.05218(15) 0.04460(13) 0.00053(10) 0.00085(10) 0.00073(10) C1 0.062(2) 0.055(2) 0.0461(17) -0.0017(14) -0.0007(15) -0.0052(16) O1 0.0838(19) 0.0525(15) 0.0757(17) 0.0000(14) 0.0114(15) -0.0080(15) N1 0.0513(15) 0.0486(15) 0.0546(15) -0.0014(13) 0.0026(14) 0.0013(13) P1 0.0437(4) 0.0506(5) 0.0454(4) 0.0002(3) 0.0012(3) 0.0004(3) F1 0.229(6) 0.177(5) 0.138(4) -0.019(3) 0.082(4) 0.030(4) S1 0.0764(7) 0.1284(12) 0.0770(7) 0.0074(7) -0.0062(6) -0.0229(8) Cl1 0.0677(5) 0.0813(6) 0.0508(4) -0.0052(4) -0.0056(4) 0.0009(5) F2 0.171(4) 0.179(4) 0.122(3) -0.017(3) -0.070(3) 0.010(3) N2 0.0469(15) 0.0577(16) 0.0488(14) 0.0036(13) 0.0083(12) -0.0029(13) O2 0.0525(15) 0.092(2) 0.0718(16) 0.0091(15) 0.0192(13) 0.0044(13) C2 0.063(2) 0.071(3) 0.071(2) -0.011(2) 0.0066(19) -0.013(2) F3 0.211(5) 0.099(3) 0.165(4) 0.000(3) -0.003(4) -0.014(3) O3 0.101(3) 0.227(7) 0.182(5) 0.106(5) -0.065(3) -0.039(4) C3 0.093(4) 0.084(3) 0.088(3) -0.010(3) 0.010(3) -0.035(3) C9 0.082(3) 0.086(3) 0.059(2) 0.002(2) 0.018(2) 0.002(3) C8 0.064(2) 0.071(2) 0.0533(19) -0.0029(18) 0.0078(17) 0.0013(19) C7 0.0477(18) 0.0584(19) 0.0494(17) 0.0034(15) 0.0028(13) 0.0004(15) C6 0.073(3) 0.064(2) 0.063(2) -0.0081(18) -0.010(2) 0.009(2) C5 0.112(4) 0.062(3) 0.070(3) -0.007(2) -0.008(3) 0.012(3) O5 0.121(3) 0.194(6) 0.092(3) -0.039(3) 0.035(2) -0.056(4) C4 0.136(5) 0.056(2) 0.074(3) -0.007(2) 0.010(3) -0.021(3) O4 0.107(3) 0.104(3) 0.132(3) 0.013(3) 0.003(3) -0.020(2) C10 0.086(3) 0.095(4) 0.068(2) 0.015(2) 0.027(2) -0.013(3) C11 0.073(3) 0.068(3) 0.076(3) 0.008(2) 0.016(2) -0.011(2) C13 0.055(2) 0.049(2) 0.067(2) 0.0003(16) 0.0019(17) -0.0045(15) C12 0.053(2) 0.062(2) 0.0539(19) 0.0067(16) 0.0059(16) -0.0026(17) C14 0.072(3) 0.063(2) 0.085(3) -0.016(2) 0.011(2) -0.009(2) C16 0.060(2) 0.062(2) 0.076(2) -0.0122(19) 0.005(2) -0.0008(19) C15 0.058(2) 0.054(2) 0.061(2) -0.0078(16) 0.0021(16) -0.0019(17) C17 0.077(3) 0.078(3) 0.111(4) 0.000(3) -0.016(3) 0.008(3) C19 0.0476(17) 0.0579(19) 0.0538(18) 0.0008(16) -0.0021(15) 0.0031(16) C18 0.065(3) 0.121(5) 0.115(4) -0.051(4) 0.012(3) 0.002(3) C20 0.060(2) 0.084(3) 0.058(2) 0.006(2) -0.0020(18) 0.009(2) C21 0.071(3) 0.102(4) 0.072(3) 0.017(2) -0.009(2) 0.024(3) C22 0.060(2) 0.091(3) 0.085(3) 0.009(3) -0.011(2) 0.019(2) C23 0.050(2) 0.073(3) 0.076(2) -0.001(2) 0.0028(19) 0.0076(19) C24 0.0418(16) 0.059(2) 0.063(2) -0.0011(16) 0.0003(15) 0.0000(16) C25 0.0460(17) 0.058(2) 0.0585(19) -0.0007(16) 0.0095(16) -0.0002(16) C26 0.085(3) 0.101(4) 0.068(2) 0.014(3) 0.030(2) 0.010(3) C27 0.064(2) 0.073(2) 0.0484(18) 0.0049(17) 0.0102(17) -0.0103(19) C28 0.083(3) 0.073(3) 0.065(2) 0.016(2) 0.014(2) -0.004(2) C29 0.120(5) 0.104(4) 0.076(3) 0.029(3) 0.008(3) -0.015(4) C30 0.191(8) 0.078(4) 0.084(3) 0.004(3) -0.002(4) -0.047(4) C31 0.066(2) 0.059(2) 0.074(2) 0.0101(19) -0.004(2) 0.0106(19) C32 0.052(2) 0.070(2) 0.066(2) -0.0053(18) 0.0007(17) 0.0153(19) C33 0.0407(17) 0.081(3) 0.067(2) -0.002(2) -0.0044(16) 0.0062(18) C34 0.049(2) 0.095(3) 0.079(3) -0.004(2) 0.004(2) -0.003(2) C35 0.120(5) 0.096(4) 0.088(4) 0.001(3) 0.015(4) 0.009(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Rh Rh 0.0927 3.6045 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.3331 0.5567 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag N2 Rh1 C31 100.15(15) . . ? N2 Rh1 C32 136.29(15) . . ? C31 Rh1 C32 38.41(16) . . ? N2 Rh1 N1 97.70(12) . . ? C31 Rh1 N1 161.99(15) . . ? C32 Rh1 N1 124.80(15) . . ? N2 Rh1 P1 86.53(8) . . ? C31 Rh1 P1 100.43(13) . . ? C32 Rh1 P1 88.88(11) . . ? N1 Rh1 P1 82.96(8) . . ? N2 Rh1 C33 164.23(14) . . ? C31 Rh1 C33 68.11(17) . . ? C32 Rh1 C33 36.76(16) . . ? N1 Rh1 C33 93.91(14) . . ? P1 Rh1 C33 105.53(11) . . ? N2 Rh1 Cl1 87.04(8) . . ? C31 Rh1 Cl1 88.68(13) . . ? C32 Rh1 Cl1 101.37(11) . . ? N1 Rh1 Cl1 89.88(8) . . ? P1 Rh1 Cl1 169.65(4) . . ? C33 Rh1 Cl1 82.34(11) . . ? C2 C1 C6 117.5(4) . . ? C2 C1 P1 119.4(3) . . ? C6 C1 P1 123.0(3) . . ? C13 O1 C14 105.5(3) . . ? C13 N1 C15 107.3(3) . . ? C13 N1 Rh1 127.2(3) . . ? C15 N1 Rh1 124.4(2) . . ? C1 P1 C7 110.18(17) . . ? C1 P1 C19 104.08(19) . . ? C7 P1 C19 100.77(16) . . ? C1 P1 Rh1 119.75(12) . . ? C7 P1 Rh1 109.59(12) . . ? C19 P1 Rh1 110.70(12) . . ? O5 S1 O3 115.5(4) . . ? O5 S1 O4 115.1(4) . . ? O3 S1 O4 116.3(3) . . ? O5 S1 C35 102.5(3) . . ? O3 S1 C35 101.7(4) . . ? O4 S1 C35 102.6(3) . . ? C25 N2 C27 107.6(3) . . ? C25 N2 Rh1 130.0(2) . . ? C27 N2 Rh1 122.0(2) . . ? C25 O2 C26 105.2(3) . . ? C1 C2 C3 120.7(5) . . ? C1 C2 H2 119.7 . . ? C3 C2 H2 119.7 . . ? C4 C3 C2 120.3(5) . . ? C4 C3 H3 119.8 . . ? C2 C3 H3 119.8 . . ? C10 C9 C8 120.3(4) . . ? C10 C9 H9 119.8 . . ? C8 C9 H9 119.8 . . ? C7 C8 C9 120.0(4) . . ? C7 C8 H8 120.0 . . ? C9 C8 H8 120.0 . . ? C8 C7 C12 119.8(3) . . ? C8 C7 P1 121.1(3) . . ? C12 C7 P1 118.9(3) . . ? C5 C6 C1 121.1(5) . . ? C5 C6 H6 119.4 . . ? C1 C6 H6 119.4 . . ? C4 C5 C6 119.8(5) . . ? C4 C5 H5 120.1 . . ? C6 C5 H5 120.1 . . ? C3 C4 C5 120.6(5) . . ? C3 C4 H4 119.7 . . ? C5 C4 H4 119.7 . . ? C9 C10 C11 120.4(4) . . ? C9 C10 H10 119.8 . . ? C11 C10 H10 119.8 . . ? C10 C11 C12 120.3(4) . . ? C10 C11 H11 119.9 . . ? C12 C11 H11 119.9 . . ? N1 C13 O1 117.3(4) . . ? N1 C13 C12 128.5(3) . . ? O1 C13 C12 114.2(3) . . ? C11 C12 C7 119.2(4) . . ? C11 C12 C13 117.3(4) . . ? C7 C12 C13 123.6(3) . . ? O1 C14 C15 103.9(3) . . ? O1 C14 H14A 111.0 . . ? C15 C14 H14A 111.0 . . ? O1 C14 H14B 111.0 . . ? C15 C14 H14B 111.0 . . ? H14A C14 H14B 109.0 . . ? C15 C16 C17 113.7(4) . . ? C15 C16 C18 109.8(4) . . ? C17 C16 C18 111.9(4) . . ? C15 C16 H16 107.0 . . ? C17 C16 H16 107.0 . . ? C18 C16 H16 107.0 . . ? N1 C15 C16 110.9(3) . . ? N1 C15 C14 101.4(3) . . ? C16 C15 C14 116.1(4) . . ? N1 C15 H15 109.3 . . ? C16 C15 H15 109.3 . . ? C14 C15 H15 109.3 . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? H17A C17 H17B 109.5 . . ? C16 C17 H17C 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? C20 C19 C24 118.8(3) . . ? C20 C19 P1 117.5(3) . . ? C24 C19 P1 123.7(3) . . ? C16 C18 H18A 109.5 . . ? C16 C18 H18B 109.5 . . ? H18A C18 H18B 109.5 . . ? C16 C18 H18C 109.5 . . ? H18A C18 H18C 109.5 . . ? H18B C18 H18C 109.5 . . ? C19 C20 C21 120.4(4) . . ? C19 C20 H20 119.8 . . ? C21 C20 H20 119.8 . . ? C22 C21 C20 120.5(4) . . ? C22 C21 H21 119.8 . . ? C20 C21 H21 119.8 . . ? C21 C22 C23 119.7(4) . . ? C21 C22 H22 120.1 . . ? C23 C22 H22 120.1 . . ? C22 C23 C24 121.1(4) . . ? C22 C23 H23 119.5 . . ? C24 C23 H23 119.5 . . ? C23 C24 C19 119.5(3) . . ? C23 C24 C25 117.9(3) . . ? C19 C24 C25 122.6(3) . . ? N2 C25 O2 117.0(3) . . ? N2 C25 C24 128.8(3) . . ? O2 C25 C24 114.2(3) . . ? O2 C26 C27 104.7(3) . . ? O2 C26 H26A 110.8 . . ? C27 C26 H26A 110.8 . . ? O2 C26 H26B 110.8 . . ? C27 C26 H26B 110.8 . . ? H26A C26 H26B 108.9 . . ? N2 C27 C26 101.3(3) . . ? N2 C27 C28 112.1(3) . . ? C26 C27 C28 115.9(4) . . ? N2 C27 H27 109.0 . . ? C26 C27 H27 109.0 . . ? C28 C27 H27 109.0 . . ? C27 C28 C30 113.0(4) . . ? C27 C28 C29 110.0(4) . . ? C30 C28 C29 110.1(4) . . ? C27 C28 H28 107.9 . . ? C30 C28 H28 107.9 . . ? C29 C28 H28 107.9 . . ? C28 C29 H29A 109.5 . . ? C28 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C28 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C28 C30 H30A 109.5 . . ? C28 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C28 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C32 C31 Rh1 71.4(2) . . ? C32 C31 H31A 116.5 . . ? Rh1 C31 H31A 116.5 . . ? C32 C31 H31B 116.5 . . ? Rh1 C31 H31B 116.5 . . ? H31A C31 H31B 113.4 . . ? C33 C32 C31 122.5(4) . . ? C33 C32 Rh1 75.2(2) . . ? C31 C32 Rh1 70.2(2) . . ? C33 C32 H32 118.3 . . ? C31 C32 H32 118.3 . . ? Rh1 C32 H32 118.3 . . ? C32 C33 C34 121.5(4) . . ? C32 C33 Rh1 68.1(2) . . ? C34 C33 Rh1 126.6(3) . . ? C32 C33 H33 111.3 . . ? C34 C33 H33 111.3 . . ? Rh1 C33 H33 111.3 . . ? C33 C34 H34A 109.5 . . ? C33 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? C33 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? F1 C35 F3 108.2(6) . . ? F1 C35 F2 106.6(6) . . ? F3 C35 F2 105.8(7) . . ? F1 C35 S1 112.4(6) . . ? F3 C35 S1 111.9(5) . . ? F2 C35 S1 111.6(5) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Rh1 N2 2.134(3) . ? Rh1 C31 2.148(4) . ? Rh1 C32 2.165(4) . ? Rh1 N1 2.165(3) . ? Rh1 P1 2.2205(9) . ? Rh1 C33 2.256(4) . ? Rh1 Cl1 2.4550(9) . ? C1 C2 1.383(6) . ? C1 C6 1.405(6) . ? C1 P1 1.816(4) . ? O1 C13 1.338(5) . ? O1 C14 1.462(5) . ? N1 C13 1.287(5) . ? N1 C15 1.502(5) . ? P1 C7 1.823(3) . ? P1 C19 1.825(4) . ? F1 C35 1.312(7) . ? S1 O5 1.418(4) . ? S1 O3 1.423(5) . ? S1 O4 1.446(5) . ? S1 C35 1.788(7) . ? F2 C35 1.331(8) . ? N2 C25 1.277(5) . ? N2 C27 1.503(4) . ? O2 C25 1.345(4) . ? O2 C26 1.462(6) . ? C2 C3 1.389(7) . ? C2 H2 0.9300 . ? F3 C35 1.325(8) . ? C3 C4 1.355(8) . ? C3 H3 0.9300 . ? C9 C10 1.373(7) . ? C9 C8 1.384(6) . ? C9 H9 0.9300 . ? C8 C7 1.383(5) . ? C8 H8 0.9300 . ? C7 C12 1.407(6) . ? C6 C5 1.372(7) . ? C6 H6 0.9300 . ? C5 C4 1.368(8) . ? C5 H5 0.9300 . ? C4 H4 0.9300 . ? C10 C11 1.381(7) . ? C10 H10 0.9300 . ? C11 C12 1.386(5) . ? C11 H11 0.9300 . ? C13 C12 1.484(5) . ? C14 C15 1.533(6) . ? C14 H14A 0.9700 . ? C14 H14B 0.9700 . ? C16 C15 1.525(6) . ? C16 C17 1.526(7) . ? C16 C18 1.527(6) . ? C16 H16 0.9800 . ? C15 H15 0.9800 . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? C19 C20 1.382(5) . ? C19 C24 1.403(5) . ? C18 H18A 0.9600 . ? C18 H18B 0.9600 . ? C18 H18C 0.9600 . ? C20 C21 1.397(6) . ? C20 H20 0.9300 . ? C21 C22 1.368(7) . ? C21 H21 0.9300 . ? C22 C23 1.368(6) . ? C22 H22 0.9300 . ? C23 C24 1.392(5) . ? C23 H23 0.9300 . ? C24 C25 1.472(5) . ? C26 C27 1.512(7) . ? C26 H26A 0.9700 . ? C26 H26B 0.9700 . ? C27 C28 1.512(6) . ? C27 H27 0.9800 . ? C28 C30 1.534(8) . ? C28 C29 1.535(6) . ? C28 H28 0.9800 . ? C29 H29A 0.9600 . ? C29 H29B 0.9600 . ? C29 H29C 0.9600 . ? C30 H30A 0.9600 . ? C30 H30B 0.9600 . ? C30 H30C 0.9600 . ? C31 C32 1.419(6) . ? C31 H31A 0.9700 . ? C31 H31B 0.9700 . ? C32 C33 1.397(6) . ? C32 H32 0.9800 . ? C33 C34 1.491(6) . ? C33 H33 0.9800 . ? C34 H34A 0.9600 . ? C34 H34B 0.9600 . ? C34 H34C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C2 C1 P1 C7 128.1(3) . . . . ? C6 C1 P1 C7 -57.3(4) . . . . ? C2 C1 P1 C19 20.8(4) . . . . ? C6 C1 P1 C19 -164.6(3) . . . . ? C2 C1 P1 Rh1 -103.5(3) . . . . ? C6 C1 P1 Rh1 71.1(3) . . . . ? C6 C1 C2 C3 -0.8(6) . . . . ? P1 C1 C2 C3 174.1(4) . . . . ? C1 C2 C3 C4 -0.4(8) . . . . ? C10 C9 C8 C7 -0.2(7) . . . . ? C9 C8 C7 C12 -1.7(6) . . . . ? C9 C8 C7 P1 -176.7(3) . . . . ? C1 P1 C7 C8 -6.1(4) . . . . ? C19 P1 C7 C8 103.4(3) . . . . ? Rh1 P1 C7 C8 -139.9(3) . . . . ? C1 P1 C7 C12 178.8(3) . . . . ? C19 P1 C7 C12 -71.7(3) . . . . ? Rh1 P1 C7 C12 45.0(3) . . . . ? C2 C1 C6 C5 1.4(6) . . . . ? P1 C1 C6 C5 -173.3(3) . . . . ? C1 C6 C5 C4 -0.7(7) . . . . ? C2 C3 C4 C5 1.1(8) . . . . ? C6 C5 C4 C3 -0.5(8) . . . . ? C8 C9 C10 C11 1.9(8) . . . . ? C9 C10 C11 C12 -1.8(8) . . . . ? C15 N1 C13 O1 -2.2(5) . . . . ? Rh1 N1 C13 O1 165.6(3) . . . . ? C15 N1 C13 C12 179.0(4) . . . . ? Rh1 N1 C13 C12 -13.2(6) . . . . ? C14 O1 C13 N1 -11.9(5) . . . . ? C14 O1 C13 C12 167.1(4) . . . . ? C10 C11 C12 C7 -0.1(7) . . . . ? C10 C11 C12 C13 180.0(4) . . . . ? C8 C7 C12 C11 1.8(6) . . . . ? P1 C7 C12 C11 176.9(3) . . . . ? C8 C7 C12 C13 -178.3(4) . . . . ? P1 C7 C12 C13 -3.1(5) . . . . ? N1 C13 C12 C11 162.1(4) . . . . ? O1 C13 C12 C11 -16.7(6) . . . . ? N1 C13 C12 C7 -17.8(7) . . . . ? O1 C13 C12 C7 163.4(4) . . . . ? C13 O1 C14 C15 19.9(5) . . . . ? C13 N1 C15 C16 -109.5(4) . . . . ? Rh1 N1 C15 C16 82.2(4) . . . . ? C13 N1 C15 C14 14.4(4) . . . . ? Rh1 N1 C15 C14 -153.9(3) . . . . ? C17 C16 C15 N1 74.7(5) . . . . ? C18 C16 C15 N1 -159.1(4) . . . . ? C17 C16 C15 C14 -40.3(5) . . . . ? C18 C16 C15 C14 85.8(5) . . . . ? O1 C14 C15 N1 -20.4(4) . . . . ? O1 C14 C15 C16 99.9(4) . . . . ? C1 P1 C19 C20 82.5(4) . . . . ? C7 P1 C19 C20 -31.7(4) . . . . ? Rh1 P1 C19 C20 -147.6(3) . . . . ? C1 P1 C19 C24 -97.4(4) . . . . ? C7 P1 C19 C24 148.4(3) . . . . ? Rh1 P1 C19 C24 32.5(4) . . . . ? C24 C19 C20 C21 -1.7(7) . . . . ? P1 C19 C20 C21 178.4(4) . . . . ? C19 C20 C21 C22 1.3(8) . . . . ? C20 C21 C22 C23 -0.6(9) . . . . ? C21 C22 C23 C24 0.3(8) . . . . ? C22 C23 C24 C19 -0.7(7) . . . . ? C22 C23 C24 C25 179.6(4) . . . . ? C20 C19 C24 C23 1.4(6) . . . . ? P1 C19 C24 C23 -178.7(3) . . . . ? C20 C19 C24 C25 -178.9(4) . . . . ? P1 C19 C24 C25 1.0(6) . . . . ? C27 N2 C25 O2 -4.7(5) . . . . ? Rh1 N2 C25 O2 167.8(3) . . . . ? C27 N2 C25 C24 176.0(4) . . . . ? Rh1 N2 C25 C24 -11.6(6) . . . . ? C26 O2 C25 N2 -9.0(5) . . . . ? C26 O2 C25 C24 170.4(4) . . . . ? C23 C24 C25 N2 163.5(4) . . . . ? C19 C24 C25 N2 -16.2(6) . . . . ? C23 C24 C25 O2 -15.8(5) . . . . ? C19 C24 C25 O2 164.4(4) . . . . ? C25 O2 C26 C27 18.3(5) . . . . ? C25 N2 C27 C26 15.6(5) . . . . ? Rh1 N2 C27 C26 -157.6(3) . . . . ? C25 N2 C27 C28 -108.7(4) . . . . ? Rh1 N2 C27 C28 78.2(4) . . . . ? O2 C26 C27 N2 -20.0(5) . . . . ? O2 C26 C27 C28 101.6(4) . . . . ? N2 C27 C28 C30 58.5(6) . . . . ? C26 C27 C28 C30 -57.2(6) . . . . ? N2 C27 C28 C29 -178.1(4) . . . . ? C26 C27 C28 C29 66.2(5) . . . . ? Rh1 C31 C32 C33 -56.5(4) . . . . ? C31 C32 C33 C34 174.8(4) . . . . ? Rh1 C32 C33 C34 120.5(4) . . . . ? C31 C32 C33 Rh1 54.2(3) . . . . ? O5 S1 C35 F1 179.0(5) . . . . ? O3 S1 C35 F1 -61.3(6) . . . . ? O4 S1 C35 F1 59.3(6) . . . . ? O5 S1 C35 F3 -59.1(6) . . . . ? O3 S1 C35 F3 60.6(6) . . . . ? O4 S1 C35 F3 -178.7(5) . . . . ? O5 S1 C35 F2 59.3(6) . . . . ? O3 S1 C35 F2 179.0(5) . . . . ? O4 S1 C35 F2 -60.4(6) . . . . ?