Crystallography Open Database

Information card for entry 7024948

Preview

Coordinates	7024948.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C44 H87 Co N10 O3 S3
Calculated formula	C44 H87 Co N10 O3 S3
Title of publication	Metal complexes of thiobiurets and dithiobiurets: Novel single source precursors for metal sulfide thin film nanostructures.
Authors of publication	Ramasamy, Karthik; Malik, Mohammad A.; O'Brien, Paul; Raftery, James
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	6
Pages of publication	1460 - 1463
a	14.0552 ± 0.0017 Å
b	15.7278 ± 0.0019 Å
c	25.394 ± 0.003 Å
α	90°
β	96.686 ± 0.002°
γ	90°
Cell volume	5575.4 ± 1.2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1308
Residual factor for significantly intense reflections	0.0701
Weighted residual factors for significantly intense reflections	0.2003
Weighted residual factors for all reflections included in the refinement	0.2235
Goodness-of-fit parameter for all reflections included in the refinement	0.999
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179954 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/49.	7024948.cif
92758	2014-01-12	cif/ Adding structures of 7024946, 7024947, 7024948, 7024949, 7024950, 7024951 via cif-deposit CGI script.	7024948.cif