Crystallography Open Database

Information card for entry 7032846

Preview

Coordinates	7032846.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C28 H32 N14 O11 Pb2
Calculated formula	C22 H16 N12 O8 Pb2
Title of publication	Synthesis, structure and catalytic application of lead(II) complexes in cyanosilylation reactions.
Authors of publication	Karmakar, Anirban; Hazra, Susanta; Guedes da Silva, M Fátima C; Pombeiro, Armando J. L.
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2015
Journal volume	44
Journal issue	1
Pages of publication	268 - 280
a	7.8443 ± 0.0004 Å
b	22.1845 ± 0.0013 Å
c	21.7657 ± 0.0013 Å
α	90°
β	90.842 ± 0.002°
γ	90°
Cell volume	3787.3 ± 0.4 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0862
Residual factor for significantly intense reflections	0.0526
Weighted residual factors for significantly intense reflections	0.1172
Weighted residual factors for all reflections included in the refinement	0.1269
Goodness-of-fit parameter for all reflections included in the refinement	1.047
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
180034 (current)	2016-03-25	cif/7/03/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/03/28.	7032846.cif
131065	2015-02-04	cif/ Updating files of 7032845, 7032846, 7032847, 7032848, 7032849, 7032850 Original log message: Adding full bibliography for 7032845--7032850.cif.	7032846.cif
125575	2014-10-21	cif/ Adding structures of 7032845, 7032846, 7032847, 7032848, 7032849, 7032850 via cif-deposit CGI script.	7032846.cif