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Information card for entry 7032849
Preview
| Coordinates | 7032849.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C12 H13 N7 O5 Pb |
|---|---|
| Calculated formula | C12 H13 N7 O5 Pb |
| SMILES | [Pb]12(OC(=O)c3[n]1ccnc3N)[n]1c(C(=O)O2)c(ncc1)N.C(=O)NC |
| Title of publication | Synthesis, structure and catalytic application of lead(II) complexes in cyanosilylation reactions. |
| Authors of publication | Karmakar, Anirban; Hazra, Susanta; Guedes da Silva, M Fátima C; Pombeiro, Armando J. L. |
| Journal of publication | Dalton transactions (Cambridge, England : 2003) |
| Year of publication | 2015 |
| Journal volume | 44 |
| Journal issue | 1 |
| Pages of publication | 268 - 280 |
| a | 7.6487 ± 0.0005 Å |
| b | 12.27 ± 0.0007 Å |
| c | 18.3447 ± 0.0012 Å |
| α | 81.365 ± 0.002° |
| β | 87.259 ± 0.002° |
| γ | 73.959 ± 0.002° |
| Cell volume | 1635.82 ± 0.18 Å3 |
| Cell temperature | 296 ± 2 K |
| Ambient diffraction temperature | 296 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0504 |
| Residual factor for significantly intense reflections | 0.0384 |
| Weighted residual factors for significantly intense reflections | 0.1015 |
| Weighted residual factors for all reflections included in the refinement | 0.1102 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.141 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 193656 (current) | 2017-03-04 | cif/7: Fixing Z values and formulae |
7032849.cif |
| 180034 | 2016-03-25 | cif/7/03/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/03/28. |
7032849.cif |
| 131065 | 2015-02-04 | cif/ Updating files of 7032845, 7032846, 7032847, 7032848, 7032849, 7032850 Original log message: Adding full bibliography for 7032845--7032850.cif. |
7032849.cif |
| 125575 | 2014-10-21 | cif/ Adding structures of 7032845, 7032846, 7032847, 7032848, 7032849, 7032850 via cif-deposit CGI script. |
7032849.cif |
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Users of the data should acknowledge the original authors of the
structural data.