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Information card for entry 7042748
Preview
| Coordinates | 7042748.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C44 H36 Cl6 N2 O4 P4 Pd6 |
|---|---|
| Calculated formula | C44 H36 Cl6 N2 O4 P4 Pd6 |
| Title of publication | First examples of tri- and tetraphosphametacyclophanes: synthesis and isolation of an unusual hexapalladium complex containing pincer units with Pd—P covalent bonds |
| Authors of publication | Kashid, Vitthal S.; Radhakrishna, Latchupatula; Balakrishna, Maravanji Shivaramaiah |
| Journal of publication | Dalton Trans. |
| Year of publication | 2017 |
| a | 10.0974 ± 0.0002 Å |
| b | 10.1677 ± 0.0003 Å |
| c | 13.9117 ± 0.0003 Å |
| α | 102.789 ± 0.002° |
| β | 95.8839 ± 0.0019° |
| γ | 113.851 ± 0.002° |
| Cell volume | 1244.02 ± 0.06 Å3 |
| Cell temperature | 150 ± 2 K |
| Ambient diffraction temperature | 150 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0284 |
| Residual factor for significantly intense reflections | 0.0252 |
| Weighted residual factors for significantly intense reflections | 0.0626 |
| Weighted residual factors for all reflections included in the refinement | 0.0646 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.061 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | Yes |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 195681 (current) | 2017-04-22 | cif/ Adding structures of 7042748, 7042749, 7042750 via cif-deposit CGI script. |
7042748.cif |
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