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Information card for entry 7048012
Preview
Coordinates | 7048012.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H45 F6 N2 Ni P2 Sb |
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Calculated formula | C28 H45 F6 N2 Ni P2 Sb |
Title of publication | Redox-state dependent activation of silanes and ammonia with reverse polarity (PC<sub>carbene</sub>P)Ni complexes: electrophilic vs. nucleophilic carbenes. |
Authors of publication | LaPierre, Etienne A.; Piers, Warren E.; Gendy, Chris |
Journal of publication | Dalton transactions (Cambridge, England : 2003) |
Year of publication | 2018 |
Journal volume | 47 |
Journal issue | 46 |
Pages of publication | 16789 - 16797 |
a | 10.9965 ± 0.0003 Å |
b | 16.1517 ± 0.0004 Å |
c | 18.8351 ± 0.0004 Å |
α | 90° |
β | 101.979 ± 0.001° |
γ | 90° |
Cell volume | 3272.49 ± 0.14 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/n 1 |
Hall space group symbol | -P 2yn |
Residual factor for all reflections | 0.0434 |
Residual factor for significantly intense reflections | 0.0315 |
Weighted residual factors for significantly intense reflections | 0.0727 |
Weighted residual factors for all reflections included in the refinement | 0.0812 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.016 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
229647 (current) | 2019-11-17 | cif/ Updating files of 7048006, 7048007, 7048008, 7048009, 7048010, 7048011, 7048012 Original log message: Adding full bibliography for 7048006--7048012.cif. |
7048012.cif |
211865 | 2018-11-09 | cif/ Adding structures of 7048006, 7048007, 7048008, 7048009, 7048010, 7048011, 7048012 via cif-deposit CGI script. |
7048012.cif |
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Users of the data should acknowledge the original authors of the
structural data.