Crystallography Open Database

Information card for entry 7058761

Preview

Coordinates	7058761.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H32 Br2 Cl N3 Ni O2
Calculated formula	C22 H30 Br2 Cl N3 Ni O
Title of publication	Lewis acids in situ modulate pyridazine-imine Ni catalysed ethylene (co)polymerisation
Authors of publication	Wang, Guohong; Li, Min; Pang, Wenmin; Chen, Min; Tan, Chen
Journal of publication	New Journal of Chemistry
Year of publication	2019
Journal volume	43
Journal issue	34
Pages of publication	13630
a	23.206 ± 0.005 Å
b	23.206 ± 0.005 Å
c	8.801 ± 0.005 Å
α	90°
β	90°
γ	120°
Cell volume	4105 ± 3 Å³
Cell temperature	273 K
Ambient diffraction temperature	273 K
Number of distinct elements	7
Space group number	147
Hermann-Mauguin space group symbol	P -3
Hall space group symbol	-P 3
Residual factor for all reflections	0.0978
Residual factor for significantly intense reflections	0.0414
Weighted residual factors for significantly intense reflections	0.0916
Weighted residual factors for all reflections included in the refinement	0.1115
Goodness-of-fit parameter for all reflections included in the refinement	0.989
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
224966 (current)	2019-11-08	cif/ Updating files of 7058761 Original log message: Adding full bibliography for 7058761.cif.	7058761.cif
217538	2019-08-15	cif/ Adding structures of 7058761 via cif-deposit CGI script.	7058761.cif