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Information card for entry 7061203
Preview
| Coordinates | 7061203.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C13 H16 O4 S |
|---|---|
| Calculated formula | C13 H16 O4 S |
| Title of publication | Regioselective direct sulfenylation of glycals using arylsulfonyl chlorides in the presence of triphenylphosphine: access to C2-thioaryl glycosides |
| Authors of publication | Kumar, Harikesh; Dubey, Atul; Prajapati, Gurudayal; Kant, Ruchir; Ampapathi, Ravi S.; Mandal, Pintu Kumar |
| Journal of publication | New Journal of Chemistry |
| Year of publication | 2022 |
| Journal volume | 46 |
| Journal issue | 7 |
| Pages of publication | 3426 - 3430 |
| a | 5.572 ± 0.002 Å |
| b | 18.599 ± 0.007 Å |
| c | 18.753 ± 0.008 Å |
| α | 90° |
| β | 92.336 ± 0.008° |
| γ | 90° |
| Cell volume | 1941.8 ± 1.3 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 4 |
| Hermann-Mauguin space group symbol | P 1 21 1 |
| Hall space group symbol | P 2yb |
| Residual factor for all reflections | 0.1361 |
| Residual factor for significantly intense reflections | 0.0713 |
| Weighted residual factors for significantly intense reflections | 0.1476 |
| Weighted residual factors for all reflections included in the refinement | 0.1719 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.919 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 273394 (current) | 2022-03-05 | cif/ Updating files of 7061203 Original log message: Adding full bibliography for 7061203.cif. |
7061203.cif |
| 272119 | 2022-01-19 | cif/ Adding structures of 7061203 via cif-deposit CGI script. |
7061203.cif |
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Users of the data should acknowledge the original authors of the
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