Crystallography Open Database

Information card for entry 7112251

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Coordinates	7112251.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C69 H116 P28 Si16
Calculated formula	C69 H116 P28 Si16
Title of publication	Branched tetrasilane substituted phosphines ‒ synthesis and characterisation of PhSi(SiiPr2)3P and {PhSi(SiMe2)3}2P14
Authors of publication	Michael Feierabend; Carsten von Hanisch
Journal of publication	Chem.Commun.
Year of publication	2014
Journal volume	50
Pages of publication	4416
a	9.31 ± 0.002 Å
b	16.566 ± 0.004 Å
c	18.804 ± 0.004 Å
α	88.88 ± 0.019°
β	87.593 ± 0.019°
γ	77.702 ± 0.018°
Cell volume	2830.9 ± 1.1 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1656
Residual factor for significantly intense reflections	0.0716
Weighted residual factors for significantly intense reflections	0.1586
Weighted residual factors for all reflections included in the refinement	0.1803
Goodness-of-fit parameter for all reflections included in the refinement	0.742
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180236 (current)	2016-03-26	cif/7/11/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/11/22.	7112251.cif
108976	2014-04-07	cif/ Adding structures of 7112251, 7112252, 7112253 via cif-deposit CGI script.	7112251.cif