Crystallography Open Database

Information card for entry 7125676

Preview

Coordinates	7125676.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H41 N O P
Calculated formula	C32 H41 N O P
Title of publication	Isolable cyclic (alkyl)(amino)carbene-phosphonyl radical adducts.
Authors of publication	Livshits-Kritsman, Yulia; Tumanskii, Boris; Ménard, Gabriel; Dobrovetsky, Roman
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2020
Journal volume	56
Journal issue	9
Pages of publication	1341 - 1344
a	10.5072 ± 0.0003 Å
b	14.0611 ± 0.0003 Å
c	18.7738 ± 0.0005 Å
α	90°
β	103.585 ± 0.001°
γ	90°
Cell volume	2696.09 ± 0.12 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0539
Residual factor for significantly intense reflections	0.0415
Weighted residual factors for significantly intense reflections	0.1056
Weighted residual factors for all reflections included in the refinement	0.1129
Goodness-of-fit parameter for all reflections included in the refinement	1.036
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
247617 (current)	2020-02-04	cif/ Updating files of 7125674, 7125675, 7125676, 7125677 Original log message: Adding full bibliography for 7125674--7125677.cif.	7125676.cif
245463	2019-12-21	cif/ Adding structures of 7125674, 7125675, 7125676, 7125677 via cif-deposit CGI script.	7125676.cif