Crystallography Open Database

Information card for entry 7125686

Preview

Coordinates	7125686.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C152 H254 As16 N16 Na6 O72 Sn14
Calculated formula	C152 H190 As16 N16 Na6 O60 Sn14
Title of publication	A core-shell type alkyl-Sn-oxo cluster of {Sn<sub>14</sub>As<sub>16</sub>} bridged by 4-aminophenylarsonate ligands and incorporated with a {Na<sub>6</sub>} cluster.
Authors of publication	Zhu, Yu; Zhang, Jian; Zhang, Lei
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2020
Journal volume	56
Journal issue	9
Pages of publication	1433 - 1435
a	28.003 ± 0.003 Å
b	38.235 ± 0.004 Å
c	26.324 ± 0.003 Å
α	90°
β	99.404 ± 0.002°
γ	90°
Cell volume	27806 ± 5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0615
Residual factor for significantly intense reflections	0.0535
Weighted residual factors for significantly intense reflections	0.1377
Weighted residual factors for all reflections included in the refinement	0.1433
Goodness-of-fit parameter for all reflections included in the refinement	1.027
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
247614 (current)	2020-02-04	cif/ Updating files of 7125686 Original log message: Adding full bibliography for 7125686.cif.	7125686.cif
245496	2019-12-22	cif/ Adding structures of 7125686 via cif-deposit CGI script.	7125686.cif