#------------------------------------------------------------------------------ #$Date: 2021-01-04 20:31:43 +0200 (Mon, 04 Jan 2021) $ #$Revision: 260475 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/12/77/7127766.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7127766 loop_ _publ_author_name 'Espinosa-Jalapa, Noel Angel' 'Berg, Nele' 'Seidl, Michael' 'Shenderovich, Ilya G.' 'Gschwind, Ruth M.' 'Bauer, Jonathan O.' _publ_section_title ; Complexation behaviour of LiCl and LiPF6- model studies in the solid-state and in solution using a bidentate picolyl-based ligand. ; _journal_issue 87 _journal_name_full 'Chemical communications (Cambridge, England)' _journal_page_first 13335 _journal_page_last 13338 _journal_paper_doi 10.1039/d0cc05682k _journal_volume 56 _journal_year 2020 _chemical_formula_moiety 'C48 H44 F12 Li2 N4 P2 Si2, 0.7(C1 H2 Cl2)' _chemical_formula_sum 'C48.7 H45.4 Cl1.4 F12 Li2 N4 P2 Si2' _chemical_formula_weight 1096.32 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2020-07-16 _audit_creation_method ; Olex2 1.3-alpha (compiled 2020.06.28 svn.raecde09e for OlexSys, GUI svn.r6132) ; _audit_update_record ; 2020-07-22 deposited with the CCDC. 2020-10-15 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 100.7840(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.57120(10) _cell_length_b 18.1992(2) _cell_length_c 27.2894(3) _cell_measurement_reflns_used 12030 _cell_measurement_temperature 123.15 _cell_measurement_theta_max 71.5640 _cell_measurement_theta_min 4.0830 _cell_volume 5157.42(10) _computing_cell_refinement 'CrysAlisPro 1.171.41.76a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.41.76a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.41.76a (Rigaku OD, 2020)' _computing_molecular_graphics 'Olex2 1.3-alpha (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-alpha (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_temperature 123.15 _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.2548 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 0.984 _diffrn_measured_fraction_theta_max 0.956 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -42.00 27.00 1.00 11.00 -- 40.72 -19.00 120.00 69 2 \w -42.00 27.00 1.00 11.00 -- 40.72 -19.00 60.00 69 3 \w -40.00 23.00 1.00 11.00 -- 40.72 -19.00-180.00 63 4 \w 85.00 175.00 1.00 50.00 -- 104.78 61.00 -90.00 90 5 \w 80.00 177.00 1.00 50.00 -- 104.78 77.00-180.00 97 6 \w 76.00 157.00 1.00 50.00 -- 104.78 45.00-120.00 81 7 \w 37.00 83.00 1.00 50.00 -- 104.78-111.00 150.00 46 8 \w 30.00 82.00 1.00 50.00 -- 104.78-111.00 120.00 52 9 \w 26.00 71.00 1.00 50.00 -- 104.78 -95.00-180.00 45 10 \w 40.00 68.00 1.00 50.00 -- 104.78 -61.00-150.00 28 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'Xcalibur, AtlasS2, Gemini ultra' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.1460156000 _diffrn_orient_matrix_UB_12 -0.0121477000 _diffrn_orient_matrix_UB_13 0.0047128000 _diffrn_orient_matrix_UB_21 0.0261742000 _diffrn_orient_matrix_UB_22 0.0696348000 _diffrn_orient_matrix_UB_23 0.0323793000 _diffrn_orient_matrix_UB_31 0.0012031000 _diffrn_orient_matrix_UB_32 -0.0465033000 _diffrn_orient_matrix_UB_33 0.0472714000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0171 _diffrn_reflns_av_unetI/netI 0.0230 _diffrn_reflns_Laue_measured_fraction_full 0.984 _diffrn_reflns_Laue_measured_fraction_max 0.956 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -12 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_limit_l_min -23 _diffrn_reflns_number 18202 _diffrn_reflns_point_group_measured_fraction_full 0.984 _diffrn_reflns_point_group_measured_fraction_max 0.956 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 71.860 _diffrn_reflns_theta_min 4.096 _diffrn_source 'fine-focus sealed X-ray tube' _diffrn_source_type 'Enhance Ultra (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 2.600 _exptl_absorpt_correction_T_max 0.846 _exptl_absorpt_correction_T_min 0.365 _exptl_absorpt_correction_type analytical _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.76a (Rigaku Oxford Diffraction, 2020) Analytical numeric absorption correction using a multifaceted crystal model based on expressions derived by R.C. Clark & J.S. Reid. (Clark, R. C. & Reid, J. S. (1995). Acta Cryst. A51, 887-897) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.412 _exptl_crystal_description plate _exptl_crystal_F_000 2246 _exptl_crystal_recrystallization_method 'Re-crystallisation from solvent: Dichloromethane/Pentane' _exptl_crystal_size_max 0.634 _exptl_crystal_size_mid 0.334 _exptl_crystal_size_min 0.082 _refine_diff_density_max 0.474 _refine_diff_density_min -0.360 _refine_diff_density_rms 0.045 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.022 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 677 _refine_ls_number_reflns 9665 _refine_ls_number_restraints 51 _refine_ls_restrained_S_all 1.022 _refine_ls_R_factor_all 0.0376 _refine_ls_R_factor_gt 0.0348 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0453P)^2^+2.5924P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0888 _refine_ls_wR_factor_ref 0.0910 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8917 _reflns_number_total 9665 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d0cc05682k2.cif _cod_data_source_block rx_318_mp_abs_ana _cod_original_formula_sum 'C48.70 H45.40 Cl1.40 F12 Li2 N4 P2 Si2' _cod_database_code 7127766 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula C48.6H45.1Cl1.1F12Li2N4P2Si2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _reflns_odcompleteness_completeness 98.28 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups 2. Restrained distances C23A-C22 \\sim C23B-C22 \\sim C24B-C23B \\sim C23A-C24A \\sim C24A-C19 \\sim C24B-C19 with sigma of 0.02 3. Uiso/Uaniso restraints and constraints C23B \\sim C23A \\sim C24B \\sim C24A: within 1.7A with sigma of 0.02 and sigma for terminal atoms of 0.04 within 1.7A 4. Others Sof(H22A)=Sof(C23B)=Sof(H23B)=Sof(C24B)=Sof(H24B)=1-FVAR(1) Sof(H22)=Sof(C24A)=Sof(H24A)=Sof(C23A)=Sof(H23A)=FVAR(1) Fixed Sof: Cl2(0.7) Cl1(0.7) C49(0.7) H49A(0.7) H49B(0.7) 5.a Secondary CH2 refined with riding coordinates: C12(H12A,H12B), C36(H36A,H36B), C6(H6A,H6B), C30(H30A,H30B), C49(H49A,H49B) 5.b Aromatic/amide H refined with riding coordinates: C1(H1), C4(H4), C7(H7), C10(H10), C14(H14), C2(H2), C38(H38), C48(H48), C42(H42), C8(H8), C9(H9), C20(H20), C3(H3), C25(H25), C15(H15), C34(H34), C46(H46), C18(H18), C31(H31), C28(H28), C39(H39), C44(H44), C26(H26), C41(H41), C21(H21), C47(H47), C40(H40), C27(H27), C16(H16), C32(H32), C33(H33), C22(H22), C22(H22A), C45(H45), C24A(H24A), C17(H17), C23A(H23A), C23B(H23B), C24B(H24B) ; _shelx_res_file ; TITL rx_318_mp_a.res in P2(1)/n rx_318_mp_abs_ana.res created by SHELXL-2018/3 at 11:11:42 on 16-Jul-2020 REM Old TITL Rx_318_mP in P2(1)/n REM SHELXT solution in P2(1)/n: R1 0.120, Rweak 0.012, Alpha 0.031 REM 1.011 for 309 systematic absences, Orientation as input REM Formula found by SHELXT: C50 B N4 F13 Si3 P2 CELL 1.54184 10.5712 18.1992 27.2894 90 100.784 90 ZERR 4 0.0001 0.0002 0.0003 0 0.001 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H Cl F Li N P Si UNIT 194.8 181.6 5.6 48 8 16 8 8 SADI C23A C22 C23B C22 C24B C23B C23A C24A C24A C19 C24B C19 SIMU 0.02 0.04 1.7 C23B C23A C24B C24A L.S. 10 PLAN 40 TEMP -150 CONF list 4 MORE -1 BOND $H fmap 2 53 acta REM REM REM WGHT 0.045300 2.592400 FVAR 2.94009 0.71028 P1 7 0.581660 0.264285 0.518526 11.00000 0.02097 0.02357 = 0.02694 -0.00145 0.00426 0.00285 P2 7 0.748184 0.169311 0.364355 11.00000 0.02984 0.02610 = 0.02694 0.00075 0.00333 0.00353 SI2 8 0.399513 0.492722 0.356896 11.00000 0.02121 0.01999 = 0.02304 0.00021 0.00320 0.00103 SI1 8 0.983228 0.097058 0.624250 11.00000 0.01946 0.02697 = 0.02401 0.00078 0.00303 0.00049 CL2 3 0.240681 0.298151 0.193991 10.70000 0.04620 0.03309 = 0.02915 0.00427 0.00944 -0.00289 CL1 3 0.425874 0.207382 0.260368 10.70000 0.04855 0.03668 = 0.03760 -0.00138 -0.00242 -0.00142 F1 4 0.660708 0.188827 0.512764 11.00000 0.02821 0.03023 = 0.04606 -0.00672 0.00876 0.00692 F3 4 0.503713 0.337965 0.522331 11.00000 0.04263 0.02987 = 0.06021 0.00153 0.01195 0.01380 F6 4 0.459613 0.216451 0.521915 11.00000 0.02846 0.03737 = 0.07034 0.00652 0.01957 -0.00152 F2 4 0.537131 0.265282 0.458411 11.00000 0.04805 0.05376 = 0.02854 0.00247 -0.00024 -0.00223 F5 4 0.705937 0.309863 0.512429 11.00000 0.03117 0.04039 = 0.06115 -0.00351 0.00602 -0.01080 F4 4 0.629223 0.260983 0.576730 11.00000 0.06585 0.05003 = 0.02876 -0.00379 0.00466 0.01628 F7 4 0.647964 0.236940 0.363836 11.00000 0.04173 0.05279 = 0.05548 -0.01647 0.01063 0.01838 F8 4 0.795389 0.183387 0.423701 11.00000 0.05695 0.07435 = 0.02723 0.00444 -0.00147 -0.02258 F12 4 0.852113 0.227820 0.354930 11.00000 0.04399 0.05645 = 0.06237 0.01386 0.02546 -0.00262 F10 4 0.698885 0.158820 0.306947 11.00000 0.06673 0.07359 = 0.03120 -0.01335 0.00116 0.02693 N2 6 0.813800 0.053475 0.508983 11.00000 0.02500 0.02232 = 0.02825 0.00064 0.00434 0.00123 N1 6 0.979722 0.222795 0.521667 11.00000 0.02165 0.02122 = 0.03139 -0.00019 0.00481 0.00164 N3 6 0.367904 0.300461 0.363733 11.00000 0.02608 0.02367 = 0.03693 -0.00064 0.00429 -0.00122 N4 6 0.666102 0.397586 0.409732 11.00000 0.02639 0.02218 = 0.03436 0.00219 0.00117 0.00140 C5 1 1.023644 0.226217 0.571215 11.00000 0.02128 0.01939 = 0.03393 -0.00123 0.00451 0.00345 C43 1 0.498518 0.563242 0.331098 11.00000 0.02407 0.02543 = 0.02203 0.00045 -0.00068 -0.00116 C29 1 0.308458 0.347054 0.328645 11.00000 0.02518 0.02252 = 0.03273 -0.00539 0.00454 0.00064 C11 1 0.895592 0.009949 0.539854 11.00000 0.02512 0.02308 = 0.02420 -0.00049 0.00735 0.00308 C35 1 0.621604 0.458878 0.428379 11.00000 0.02885 0.02346 = 0.02415 0.00342 -0.00058 0.00111 C12 1 1.016552 0.043545 0.568669 11.00000 0.02314 0.02457 = 0.02783 0.00100 0.00437 0.00244 AFIX 23 H12A 2 1.054475 0.076744 0.546565 11.00000 -1.20000 H12B 2 1.079851 0.004249 0.580266 11.00000 -1.20000 AFIX 0 C1 1 1.052634 0.252660 0.491288 11.00000 0.02726 0.02443 = 0.03508 0.00246 0.00902 0.00244 AFIX 43 H1 2 1.021058 0.251227 0.456341 11.00000 -1.20000 AFIX 0 C37 1 0.235370 0.530395 0.358203 11.00000 0.02336 0.01922 = 0.03028 0.00143 0.00601 0.00018 C36 1 0.478608 0.467033 0.422830 11.00000 0.02816 0.02634 = 0.02405 0.00096 0.00264 0.00256 AFIX 23 H36A 2 0.459491 0.505410 0.446105 11.00000 -1.20000 H36B 2 0.441592 0.420180 0.432037 11.00000 -1.20000 AFIX 0 C13 1 1.128114 0.099887 0.675744 11.00000 0.02312 0.02760 = 0.02801 0.00270 0.00220 -0.00120 C4 1 1.144014 0.256529 0.590741 11.00000 0.02367 0.02695 = 0.03657 -0.00546 0.00195 0.00210 AFIX 43 H4 2 1.174753 0.256858 0.625756 11.00000 -1.20000 AFIX 0 C7 1 0.702386 0.023745 0.485002 11.00000 0.02663 0.02714 = 0.03324 0.00159 0.00028 0.00239 AFIX 43 H7 2 0.644645 0.054299 0.463100 11.00000 -1.20000 AFIX 0 C6 1 0.939487 0.194999 0.604485 11.00000 0.02162 0.02749 = 0.02860 -0.00079 0.00406 0.00273 AFIX 23 H6A 2 0.848772 0.196407 0.586794 11.00000 -1.20000 H6B 2 0.946516 0.226141 0.634619 11.00000 -1.20000 AFIX 0 C10 1 0.866557 -0.063928 0.546949 11.00000 0.03141 0.02319 = 0.03120 0.00276 0.00590 0.00340 AFIX 43 H10 2 0.925656 -0.093844 0.568785 11.00000 -1.20000 AFIX 0 C30 1 0.386925 0.409615 0.314518 11.00000 0.02368 0.02363 = 0.02768 -0.00269 0.00401 0.00060 AFIX 23 H30A 2 0.348868 0.425360 0.280199 11.00000 -1.20000 H30B 2 0.474952 0.391450 0.314021 11.00000 -1.20000 AFIX 0 C14 1 1.118149 0.137998 0.719327 11.00000 0.02697 0.03510 = 0.03182 -0.00058 0.00412 0.00062 AFIX 43 H14 2 1.040093 0.162715 0.721279 11.00000 -1.20000 AFIX 0 C2 1 1.170668 0.285216 0.508158 11.00000 0.02783 0.02582 = 0.04621 0.00177 0.01394 -0.00081 AFIX 43 H2 2 1.218138 0.306548 0.485461 11.00000 -1.20000 AFIX 0 C38 1 0.139624 0.529717 0.315323 11.00000 0.02984 0.03582 = 0.03046 -0.00380 0.00274 0.00576 AFIX 43 H38 2 0.157591 0.508141 0.285672 11.00000 -1.20000 AFIX 0 C19 1 0.847364 0.049450 0.646647 11.00000 0.02710 0.03505 = 0.02533 -0.00147 0.00604 -0.00371 C48 1 0.584638 0.544064 0.300169 11.00000 0.02776 0.03041 = 0.04417 0.00274 0.01118 0.00172 AFIX 43 H48 2 0.596740 0.493672 0.293217 11.00000 -1.20000 AFIX 0 C42 1 0.205532 0.563524 0.400728 11.00000 0.03109 0.03049 = 0.03245 -0.00472 0.00315 0.00395 AFIX 43 H42 2 0.268498 0.564716 0.430534 11.00000 -1.20000 AFIX 0 C8 1 0.667267 -0.048506 0.490405 11.00000 0.02898 0.03052 = 0.03940 -0.00273 0.00308 -0.00539 AFIX 43 H8 2 0.587498 -0.067045 0.472892 11.00000 -1.20000 AFIX 0 C9 1 0.751956 -0.093108 0.522151 11.00000 0.03663 0.02189 = 0.03941 0.00019 0.00988 -0.00386 AFIX 43 H9 2 0.731314 -0.143130 0.526764 11.00000 -1.20000 AFIX 0 C20 1 0.874578 -0.007197 0.681054 11.00000 0.03367 0.03065 = 0.03409 -0.00310 0.00869 -0.00252 AFIX 43 H20 2 0.961551 -0.017459 0.695705 11.00000 -1.20000 AFIX 0 C3 1 1.218089 0.285988 0.558980 11.00000 0.02226 0.02634 = 0.05179 -0.00602 0.00648 -0.00340 AFIX 43 H3 2 1.300285 0.306458 0.571806 11.00000 -1.20000 AFIX 0 C25 1 0.299915 0.242816 0.376261 11.00000 0.03418 0.02893 = 0.04418 0.00489 0.00561 -0.00444 AFIX 43 H25 2 0.342207 0.209424 0.400703 11.00000 -1.20000 AFIX 0 C15 1 1.219378 0.140654 0.759827 11.00000 0.03632 0.03772 = 0.03165 -0.00528 0.00279 -0.00765 AFIX 43 H15 2 1.210384 0.166900 0.789072 11.00000 -1.20000 AFIX 0 C34 1 0.704707 0.514245 0.450276 11.00000 0.03546 0.02737 = 0.03919 -0.00411 -0.00222 0.00081 AFIX 43 H34 2 0.671535 0.556741 0.463663 11.00000 -1.20000 AFIX 0 C46 1 0.638196 0.670585 0.289563 11.00000 0.03526 0.04088 = 0.03775 0.00947 0.00056 -0.01458 AFIX 43 H46 2 0.683355 0.707024 0.274780 11.00000 -1.20000 AFIX 0 C18 1 1.244778 0.065268 0.673977 11.00000 0.02894 0.04548 = 0.03644 -0.00823 -0.00002 0.00807 AFIX 43 H18 2 1.255222 0.039707 0.644643 11.00000 -1.20000 AFIX 0 C31 1 0.794087 0.391551 0.412183 11.00000 0.02751 0.02749 = 0.05131 -0.00003 0.00168 0.00425 AFIX 43 H31 2 0.826040 0.348448 0.399080 11.00000 -1.20000 AFIX 0 C28 1 0.179279 0.336964 0.306548 11.00000 0.02672 0.03265 = 0.04797 0.00086 -0.00044 -0.00020 AFIX 43 H28 2 0.138199 0.370765 0.282138 11.00000 -1.20000 AFIX 0 C39 1 0.018819 0.559829 0.315011 11.00000 0.02835 0.03961 = 0.04259 -0.00524 -0.00372 0.00561 AFIX 43 H39 2 -0.045064 0.558230 0.285485 11.00000 -1.20000 AFIX 0 C44 1 0.487903 0.637365 0.341538 11.00000 0.05181 0.02946 = 0.04347 -0.00883 0.02124 -0.00876 AFIX 43 H44 2 0.431654 0.652262 0.363055 11.00000 -1.20000 AFIX 0 C26 1 0.172801 0.229721 0.355610 11.00000 0.03563 0.03482 = 0.05348 0.00165 0.00916 -0.01027 AFIX 43 H26 2 0.128649 0.188480 0.365569 11.00000 -1.20000 AFIX 0 C41 1 0.085433 0.594804 0.400290 11.00000 0.03794 0.03991 = 0.04330 -0.01182 0.01097 0.00952 AFIX 43 H41 2 0.067779 0.618135 0.429418 11.00000 -1.20000 AFIX 0 C21 1 0.776276 -0.049225 0.694422 11.00000 0.05093 0.03590 = 0.04420 0.00061 0.01647 -0.01033 AFIX 43 H21 2 0.796840 -0.087594 0.718181 11.00000 -1.20000 AFIX 0 C47 1 0.653064 0.597168 0.279329 11.00000 0.02861 0.04643 = 0.04295 0.00725 0.01061 -0.00198 AFIX 43 H47 2 0.710170 0.582863 0.258000 11.00000 -1.20000 AFIX 0 C40 1 -0.008439 0.592103 0.357635 11.00000 0.02711 0.03397 = 0.05497 -0.00747 0.00686 0.00744 AFIX 43 H40 2 -0.091274 0.612341 0.357640 11.00000 -1.20000 AFIX 0 C27 1 0.111387 0.278083 0.320099 11.00000 0.02553 0.04098 = 0.05793 -0.00171 0.00215 -0.00656 AFIX 43 H27 2 0.023592 0.270938 0.305191 11.00000 -1.20000 AFIX 0 C16 1 1.333197 0.104930 0.757357 11.00000 0.02869 0.04792 = 0.03952 -0.00110 -0.00834 -0.00464 AFIX 43 H16 2 1.402486 0.106056 0.785097 11.00000 -1.20000 AFIX 0 C32 1 0.881086 0.444510 0.432662 11.00000 0.02569 0.03847 = 0.06657 -0.00237 -0.00089 -0.00070 AFIX 43 H32 2 0.970588 0.438328 0.433242 11.00000 -1.20000 AFIX 0 C33 1 0.835338 0.506730 0.452311 11.00000 0.03384 0.03599 = 0.05834 -0.00792 -0.00607 -0.00670 AFIX 43 H33 2 0.893127 0.543964 0.467070 11.00000 -1.20000 AFIX 0 C22 1 0.649898 -0.035670 0.673554 11.00000 0.04203 0.05910 = 0.04354 -0.00550 0.01638 -0.02217 PART 1 AFIX 43 H22 2 0.583179 -0.061824 0.684937 21.00000 -1.20000 AFIX 43 PART 2 H22A 2 0.583655 -0.070096 0.675777 -21.00000 -1.20000 AFIX 0 PART 0 C45 1 0.557775 0.690417 0.321214 11.00000 0.06020 0.02661 = 0.05579 -0.00616 0.01647 -0.01120 AFIX 43 H45 2 0.549578 0.740725 0.329368 11.00000 -1.20000 AFIX 0 PART 1 C24A 1 0.717665 0.057685 0.623042 21.00000 0.02692 0.03955 = 0.02712 -0.00549 0.00435 -0.00332 AFIX 43 H24A 2 0.696553 0.093148 0.597263 21.00000 -1.20000 AFIX 0 PART 0 C17 1 1.346287 0.067668 0.714685 11.00000 0.02835 0.05946 = 0.05003 -0.00640 -0.00411 0.01037 AFIX 43 H17 2 1.424966 0.043458 0.712986 11.00000 -1.20000 AFIX 0 PART 1 C23A 1 0.619701 0.015555 0.636296 21.00000 0.02775 0.05419 = 0.02868 -0.01036 0.00513 -0.01191 AFIX 43 H23A 2 0.533014 0.022126 0.619791 21.00000 -1.20000 AFIX 0 PART 0 C49 1 0.278274 0.209743 0.218327 10.70000 0.04261 0.03108 = 0.05799 0.00412 -0.00090 -0.00523 AFIX 23 H49A 2 0.209009 0.192903 0.235561 10.70000 -1.20000 H49B 2 0.281940 0.175341 0.190526 10.70000 -1.20000 AFIX 0 LI2 5 0.557074 0.304540 0.396272 11.00000 0.02430 0.02347 = 0.03616 -0.00159 0.00322 0.00225 LI1 5 0.820658 0.163689 0.492922 11.00000 0.02406 0.02428 = 0.03126 -0.00001 0.00276 -0.00083 PART 2 C23B 1 0.623266 0.033135 0.648255 -21.00000 0.03059 0.09976 = 0.03041 0.00099 0.00079 -0.01837 AFIX 43 H23B 2 0.536610 0.049731 0.640562 -21.00000 -1.20000 AFIX 0 C24B 1 0.720034 0.077180 0.634318 -21.00000 0.02681 0.06911 = 0.03533 0.01804 0.00877 -0.00128 AFIX 43 H24B 2 0.701177 0.122803 0.617633 -21.00000 -1.20000 AFIX 0 PART 0 F9 4 0.851701 0.106616 0.365868 11.00000 0.06583 0.04451 = 0.09210 -0.00299 -0.01284 0.03109 F11 4 0.644033 0.114251 0.375884 11.00000 0.06886 0.06885 = 0.06677 0.00702 0.00048 -0.04204 HKLF 4 REM rx_318_mp_a.res in P2(1)/n REM wR2 = 0.0910, GooF = S = 1.022, Restrained GooF = 1.022 for all data REM R1 = 0.0348 for 8917 Fo > 4sig(Fo) and 0.0376 for all 9665 data REM 677 parameters refined using 51 restraints END WGHT 0.0453 2.5934 REM Highest difference peak 0.474, deepest hole -0.360, 1-sigma level 0.045 Q1 1 0.7852 0.0880 0.3766 11.00000 0.05 0.47 Q2 1 0.5454 0.2405 0.5741 11.00000 0.05 0.40 Q3 1 0.6871 0.3043 0.5417 11.00000 0.05 0.39 Q4 1 0.8466 0.1818 0.3437 11.00000 0.05 0.35 Q5 1 0.6088 0.1426 0.3922 11.00000 0.05 0.34 Q6 1 1.0670 0.0970 0.6551 11.00000 0.05 0.34 Q7 1 0.4887 0.6972 0.3027 11.00000 0.05 0.28 Q8 1 0.6744 0.2235 0.3969 11.00000 0.05 0.27 Q9 1 0.3873 0.4410 0.3348 11.00000 0.05 0.26 Q10 1 0.6574 0.1209 0.3568 11.00000 0.05 0.26 Q11 1 0.3063 0.5128 0.3566 11.00000 0.05 0.26 Q12 1 0.4643 0.5342 0.3427 11.00000 0.05 0.26 Q13 1 0.8143 0.1393 0.4225 11.00000 0.05 0.26 Q14 1 0.4517 0.3228 0.4979 11.00000 0.05 0.25 Q15 1 0.4510 0.4792 0.3976 11.00000 0.05 0.25 Q16 1 0.1480 0.2862 0.2975 11.00000 0.05 0.24 Q17 1 0.9659 0.1539 0.6136 11.00000 0.05 0.24 Q18 1 0.9410 0.1462 0.6040 11.00000 0.05 0.24 Q19 1 0.4210 0.6468 0.3239 11.00000 0.05 0.24 Q20 1 0.7016 0.0963 0.3999 11.00000 0.05 0.23 Q21 1 0.1964 0.3382 0.2817 11.00000 0.05 0.22 Q22 1 0.5460 0.4613 0.4235 11.00000 0.05 0.22 Q23 1 0.9516 0.0291 0.5538 11.00000 0.05 0.21 Q24 1 0.4990 0.6004 0.3395 11.00000 0.05 0.21 Q25 1 0.9128 0.0753 0.6416 11.00000 0.05 0.21 Q26 1 0.4408 0.2130 0.4832 11.00000 0.05 0.21 Q27 1 1.1280 0.2569 0.4997 11.00000 0.05 0.20 Q28 1 0.4561 0.1979 0.4934 11.00000 0.05 0.20 Q29 1 0.8215 0.0931 0.5098 11.00000 0.05 0.20 Q30 1 0.6206 0.3625 0.3997 11.00000 0.05 0.20 Q31 1 0.8865 -0.0252 0.5446 11.00000 0.05 0.19 Q32 1 0.7734 0.5141 0.4383 11.00000 0.05 0.19 Q33 1 1.0048 0.0773 0.5832 11.00000 0.05 0.19 Q34 1 0.1839 0.5218 0.3415 11.00000 0.05 0.19 Q35 1 0.5483 0.5583 0.3186 11.00000 0.05 0.18 Q36 1 0.6611 0.4849 0.4387 11.00000 0.05 0.18 Q37 1 0.7678 0.0398 0.5005 11.00000 0.05 0.17 Q38 1 0.1618 0.2415 0.3260 11.00000 0.05 0.17 Q39 1 0.8377 0.0392 0.5194 11.00000 0.05 0.17 Q40 1 0.4506 0.3078 0.3775 11.00000 0.05 0.17 ; _shelx_res_checksum 46164 _shelx_hkl_file ; 0 0 3 83.9017 19.9428 2 0 0 -3 27.4432 9.23991 3 0 0 4 79021.2 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6 17 1886.24 234.929 2 0 -6 17 1995.19 124.589 7 0 -6 17 2216.81 135.922 8 0 6 17 1787.97 108.448 6 0 6 17 1966.69 108.439 5 0 6 18 4909.14 385.175 2 0 -6 18 4770.19 197.910 7 0 -6 18 4655.00 204.796 8 0 6 18 4792.07 179.487 5 0 6 18 4763.25 183.463 6 0 6 19 30.5080 34.7865 5 0 6 19-16.0890 80.7874 2 0 -6 19 79.8275 55.8928 8 0 -6 19 46.3542 48.3741 7 0 6 20 27877.8 1006.15 2 0 -6 20 28364.6 604.821 8 0 -6 20 28664.9 592.345 7 0 6 20 28420.2 558.098 5 0 6 20 28816.6 574.593 6 0 -6 21 3353.17 175.639 7 0 -6 21 3333.61 178.812 8 0 6 21 3265.36 164.316 6 0 6 21 3146.29 154.558 5 0 -6 22 3730.69 184.665 7 0 -6 22 4048.48 197.822 8 0 6 22 3781.56 202.449 8 0 6 22 3793.72 180.553 6 0 6 23 861.982 107.709 8 0 -6 23 852.708 96.0780 8 0 -6 24 5195.65 222.374 8 0 6 24 5343.51 239.857 8 0 6 24 5092.40 214.762 7 0 6 25 14810.9 402.010 8 0 -6 25 13894.4 383.830 8 0 6 25 14110.4 369.357 7 0 6 26 462.579 81.0708 8 0 6 26 682.847 79.8968 7 0 6 27 122.668 63.0335 8 0 6 28 10651.1 291.605 8 0 6 29 356.197 60.4082 8 0 6 30 3433.58 137.411 8 0 6 31 2396.15 104.134 8 0 7 0 188.810 49.2614 2 0 7 1 33976.5 725.433 2 0 7 -1 36367.9 690.022 2 0 7 2 4529.35 229.037 2 0 7 -2 4403.81 180.628 2 0 7 -3 10524.9 272.863 2 0 7 3 11216.0 385.419 2 0 7 4 11893.1 417.690 2 0 7 -4 11691.4 271.275 2 0 7 5 3225.73 218.754 2 0 7 6 9039.97 382.393 2 0 7 7 57939.9 1200.08 2 0 7 8 35666.8 894.509 2 0 7 9 144.744 80.8684 2 0 7 10 46172.1 1097.59 2 0 7 11 56762.0 1286.35 2 0 7 12 17669.1 655.491 2 0 7 13 5040.89 348.546 2 0 7 14 672.010 144.374 2 0 7 15 776.608 155.102 2 0 7 16 3893.22 330.646 2 0 -7 16 4532.23 187.663 7 0 -7 16 4276.10 190.635 8 0 7 16 4233.49 169.333 6 0 7 17 2833.99 301.857 2 0 -7 17 2943.87 159.645 8 0 -7 17 2649.26 148.230 7 0 7 17 2674.88 130.642 5 0 7 17 2921.83 140.938 6 0 7 18 15665.4 742.016 2 0 -7 18 15394.7 410.072 8 0 -7 18 15310.3 393.810 7 0 7 18 16189.1 377.925 6 0 7 18 15265.7 354.648 5 0 7 19 998.595 192.251 2 0 -7 19 1129.24 106.145 8 0 -7 19 1158.56 109.967 7 0 7 19 1058.12 86.1260 5 0 7 19 1139.30 95.5041 6 0 7 20 47.8702 37.7509 5 0 7 20 121.570 89.1730 2 0 -7 20 73.5931 51.8675 8 0 7 20 31.1369 40.2836 6 0 -7 21 3175.86 176.424 8 0 7 21 3178.71 162.493 6 0 7 21 3429.30 158.621 5 0 -7 22 15463.9 419.432 8 0 7 22 15893.8 440.157 8 0 7 22 15637.0 403.413 6 0 7 23 15488.5 430.252 8 0 -7 23 14657.0 405.450 8 0 7 23 15093.1 391.923 6 0 7 24 2535.91 168.506 8 0 7 24 2595.31 151.086 7 0 7 25 5939.59 244.382 8 0 7 25 5723.81 216.069 7 0 7 26 300.962 73.0145 8 0 7 26 469.317 69.3575 7 0 7 27 964.629 92.1035 8 0 7 28 2549.68 134.716 8 0 7 29 280.979 59.7396 8 0 7 30 158.793 43.0100 8 0 7 31 2808.41 106.216 8 0 8 0 28189.6 637.943 2 0 8 -1 6311.27 253.762 2 0 8 1 6343.63 280.552 2 0 8 2 5449.50 268.812 2 0 8 -2 5727.66 221.041 2 0 8 -3 435.692 60.3978 2 0 8 3 231.288 63.4790 2 0 8 4 58022.0 1162.41 2 0 8 5 11615.0 446.663 2 0 8 6 8078.26 377.189 2 0 8 7 111645. 1976.99 2 0 8 8 30499.3 844.634 2 0 8 9 34553.2 934.933 2 0 8 10 109063. 2034.41 2 0 8 11 79838.2 1672.29 2 0 8 12 13746.0 603.574 2 0 8 13 8298.01 468.880 2 0 8 14 123.536 77.6296 2 0 8 15 46303.2 1268.53 2 0 8 15 47617.9 791.125 6 0 8 16 20980.8 832.283 2 0 8 16 20628.8 426.194 4 0 8 16 20441.0 438.392 6 0 8 17 4514.20 386.171 2 0 8 17 4793.38 188.432 6 0 8 18 4400.47 394.298 2 0 8 18 4383.13 172.174 5 0 8 18 4149.18 180.542 6 0 8 19 3820.32 365.645 2 0 8 19 4015.44 179.814 6 0 8 19 4068.51 170.281 5 0 8 20 708.014 87.4928 5 0 8 20 1078.82 98.3072 6 0 8 21 9826.77 305.007 6 0 8 22 2264.20 164.776 8 0 8 22 2198.11 146.302 6 0 8 23 186.495 79.2949 8 0 8 23 131.741 55.2186 6 0 8 24 39.8472 61.7350 8 0 8 25 2715.06 158.909 8 0 8 25 2735.39 143.302 7 0 8 26 152.274 68.3611 8 0 8 26 95.1115 47.8745 7 0 8 27 1453.63 106.808 8 0 8 28-71.3024 47.7829 8 0 8 29 3921.24 147.003 8 0 8 30 9082.99 217.070 8 0 9 0 47.9094 47.6905 2 0 9 -1 12237.9 390.244 2 0 9 1 12496.5 428.481 2 0 9 2 24785.3 661.006 2 0 9 -2 24849.0 564.351 2 0 9 3 25249.5 688.730 2 0 9 4 48954.3 1074.94 2 0 9 5 283.889 90.9418 2 0 9 6 618.064 133.559 2 0 9 7 1869.54 201.106 2 0 9 8 2504.08 231.348 2 0 9 9 184.992 80.1015 2 0 9 10 3693.54 300.769 2 0 9 11 119.610 78.6164 2 0 9 12 28131.3 923.779 2 0 9 13 29463.5 962.530 2 0 9 13 28917.4 542.681 6 0 9 14 11258.2 580.477 2 0 9 14 10919.3 283.334 4 0 9 14 11806.8 299.482 6 0 9 15 7295.16 485.903 2 0 9 15 7388.12 224.808 4 0 9 15 7398.52 234.689 6 0 9 16 457.823 57.5605 4 0 9 16 550.780 66.3258 6 0 9 17 7588.44 521.511 2 0 9 17 7354.22 231.733 4 0 9 17 7206.52 240.642 6 0 9 18 3192.55 152.405 4 0 9 18 3561.20 170.592 6 0 9 19 8377.78 272.349 6 0 9 20 2179.22 139.041 6 0 9 21 28914.0 600.109 6 0 9 22 71.3185 48.6407 6 0 9 23 4577.70 216.511 8 0 9 23 4520.05 203.802 6 0 9 24 1552.28 132.374 8 0 9 25 7055.03 253.822 8 0 9 25 6876.94 225.962 7 0 9 26 858.661 88.9563 8 0 9 27 1029.68 90.5135 8 0 9 28 574.506 64.3525 8 0 9 29 16.8371 34.3139 8 0 9 30 222.159 38.0717 8 0 10 0 19417.0 554.393 2 0 10 -1 418.099 81.7023 2 0 10 1 208.952 59.5399 2 0 10 2 10917.7 429.251 2 0 10 3 4599.63 287.117 2 0 10 4 15695.3 564.937 2 0 10 5 26999.1 793.004 2 0 10 6 10118.4 476.340 2 0 10 7 1421.01 190.422 2 0 10 8 44123.6 1151.89 2 0 10 9 2163.63 242.412 2 0 10 10 2639.37 267.090 2 0 10 11 297.728 104.136 2 0 10 12 11690.1 593.269 2 0 10 12 11504.1 287.659 4 0 10 12 11761.6 299.784 6 0 10 13 548.430 146.504 2 0 10 13 663.211 69.7993 4 0 10 13 592.763 69.3133 6 0 10 14 6899.57 482.011 2 0 10 14 6618.85 216.514 4 0 10 14 7127.01 229.614 6 0 10 15 1865.53 248.383 2 0 10 15 1912.42 114.792 4 0 10 15 2024.61 124.738 6 0 10 16 2185.23 287.033 2 0 10 16 1811.43 115.681 4 0 10 16 1820.66 119.502 6 0 10 17 52.7899 44.9127 4 0 10 17 66.4533 38.3794 6 0 10 18 2076.30 124.035 4 0 10 18 1997.05 130.437 6 0 10 19 8939.98 265.922 4 0 10 19 8529.87 282.189 6 0 10 20 2177.82 139.857 6 0 10 21 9163.81 294.459 6 0 10 22 7377.49 267.124 6 0 10 23 796.048 99.8072 8 0 10 23 878.458 95.1707 6 0 10 24 547.718 83.7845 8 0 10 25 808.225 93.9290 8 0 10 25 770.168 81.1035 7 0 10 26-18.7838 53.2692 8 0 10 27 3285.50 140.014 8 0 10 28 79.1550 42.2603 8 0 10 29 49.5407 29.9104 8 0 11 1 1815.51 176.095 2 0 11 2 452.968 86.1347 2 0 11 3 6451.61 349.035 2 0 11 4 5142.45 322.651 2 0 11 5 1886.54 201.057 2 0 11 6 15142.8 604.913 2 0 11 7 4994.97 356.580 2 0 11 8 15591.4 652.669 2 0 11 9 634.690 136.459 2 0 11 9 765.053 74.8093 4 0 11 10 371.445 123.989 2 0 11 10 400.898 58.0195 4 0 -11 10 494.483 73.4433 10 0 11 10 547.472 64.3659 6 0 11 11 9844.81 269.308 4 0 11 11 10042.5 552.239 2 0 -11 11 10123.6 309.070 10 0 11 11 10084.2 276.993 6 0 11 12 492.869 131.206 2 0 11 12 542.567 68.1586 4 0 11 12 549.561 66.8150 6 0 11 13 8354.27 537.911 2 0 11 13 8552.54 256.395 4 0 11 13 9313.67 270.058 6 0 11 14 89800.7 2066.26 2 0 11 14 85388.2 1304.13 4 0 11 14 87014.5 1321.56 6 0 11 15 0.77527 39.0738 4 0 11 15 31.9778 45.5482 6 0 11 16 15.7419 41.6875 4 0 11 16 57.7905 43.8531 6 0 11 17 8477.94 262.226 4 0 11 17 8300.87 274.343 6 0 11 18 762.520 84.2318 4 0 11 18 629.421 80.4836 6 0 11 19 10745.1 298.016 4 0 11 19 10776.9 322.642 6 0 11 20 654.737 73.4586 4 0 11 20 712.262 87.2809 6 0 11 21 18295.7 446.925 6 0 11 22 2588.10 154.491 6 0 11 23 957.733 103.940 8 0 11 23 825.680 92.2399 6 0 11 24 827.961 97.1112 8 0 11 25 7615.84 243.879 8 0 11 26 63.5665 43.0998 8 0 11 27 5110.56 166.891 8 0 11 28 2648.44 104.876 8 0 12 2 7939.67 411.583 2 0 12 3 18233.4 654.325 2 0 12 4 32475.5 925.951 2 0 12 5 20242.4 723.195 2 0 -12 5 20811.4 468.121 10 0 12 6 14099.9 610.795 2 0 -12 6 15523.9 391.866 10 0 12 7 7997.06 236.334 4 0 12 7 7716.13 454.674 2 0 -12 7 8343.09 276.937 10 0 12 7 7860.22 232.492 6 0 12 8 8969.04 256.809 4 0 12 8 8448.69 496.165 2 0 -12 8 9724.81 304.286 10 0 12 8 9229.27 259.495 6 0 12 9 188.940 94.9380 2 0 12 9 45.4962 33.6126 4 0 -12 9 166.294 53.6508 10 0 12 9 102.361 38.4960 6 0 12 10 5415.09 190.719 4 0 12 10 5151.10 408.074 2 0 -12 10 5352.37 223.901 10 0 12 10 4816.56 184.645 6 0 12 11 2293.71 126.187 4 0 12 11 2716.28 313.296 2 0 -12 11 2251.73 146.225 10 0 12 11 2237.34 127.674 6 0 12 12 28588.6 1047.16 2 0 12 12 27385.2 537.707 4 0 12 12 27862.2 549.584 6 0 12 13 1735.61 266.290 2 0 12 13 1376.20 103.953 4 0 12 14 1297.91 100.684 4 0 12 14 1350.66 105.815 6 0 12 15 557.724 68.4845 4 0 12 15 646.197 82.2018 6 0 12 16 4561.21 189.642 4 0 12 16 4362.70 193.557 6 0 12 17 3225.26 157.899 4 0 12 17 3076.43 164.377 6 0 12 18 6205.18 222.048 4 0 12 18 6203.15 236.784 6 0 12 19 9543.23 278.831 4 0 12 19 9337.22 298.481 6 0 12 20 1372.98 100.938 4 0 12 20 1361.06 113.054 6 0 12 21 417.095 74.3934 6 0 12 22 12758.4 355.153 8 0 12 22 12668.1 348.695 6 0 12 23 341.637 72.2225 8 0 12 24 866.550 94.2169 8 0 12 25 70.8152 44.4889 8 0 12 26 7028.49 200.234 8 0 12 27 1707.19 85.8353 8 0 -13 0 60.2473 38.5694 10 0 -13 1 15048.6 379.377 10 0 -13 -1 15062.8 377.626 10 0 -13 2 20498.0 469.386 10 0 -13 -2 21139.5 464.380 10 0 -13 -3 4894.43 196.887 10 0 -13 3 4833.31 202.408 10 0 13 4 10544.9 525.226 2 0 -13 -4 10539.3 302.104 10 0 -13 4 10711.4 318.284 10 0 13 5 10908.6 547.223 2 0 -13 5 10964.1 326.523 10 0 13 5 10849.5 279.186 6 0 13 6 41.1026 78.4977 2 0 -13 6 20.9513 42.7517 10 0 13 6 52.2097 38.2968 6 0 13 7 2667.23 135.849 4 0 13 7 2767.22 291.207 2 0 -13 7 2745.62 161.793 10 0 13 7 2801.40 136.734 6 0 13 8 6055.91 210.241 4 0 13 8 5930.37 436.550 2 0 -13 8 6531.97 252.235 10 0 13 8 5835.58 203.142 6 0 13 9 193.950 44.1899 4 0 13 9 140.061 101.492 2 0 -13 9 330.713 67.1309 10 0 13 9 349.253 56.9992 6 0 13 10 428.737 146.705 2 0 13 10 360.363 55.2534 4 0 -13 10 411.866 73.6423 10 0 13 10 327.875 55.6184 6 0 13 11 2217.99 287.615 2 0 13 11 2281.05 128.900 4 0 13 11 2238.87 129.059 6 0 13 12 2360.40 133.727 4 0 13 12 2498.72 138.025 6 0 13 13 42.3906 43.2363 4 0 13 13 95.6029 49.2680 6 0 13 14 530.790 68.0434 4 0 13 14 662.313 81.2821 6 0 13 15 1118.53 100.269 4 0 13 15 1088.49 99.9144 6 0 13 16 35661.9 671.267 4 0 13 16 36495.6 691.678 6 0 13 17 400.365 69.8512 4 0 13 17 434.636 73.0471 6 0 13 18 87.8640 47.6890 4 0 13 18 152.677 55.3431 6 0 13 19 111.943 52.2840 4 0 13 19 181.722 59.0094 6 0 13 20 33.1177 51.5565 6 0 13 21 41.2615 46.3634 6 0 13 22 3616.63 170.583 8 0 13 22 3675.01 172.594 6 0 13 23 4516.34 183.096 8 0 13 24 3916.24 157.906 8 0 13 25 85.1286 41.8889 8 0 13 26 2243.96 94.6003 8 0 -14 0 9927.57 307.874 10 0 -14 -1 3014.13 161.076 10 0 -14 1 3088.31 166.374 10 0 -14 -2 14341.9 381.104 10 0 -14 2 14732.7 391.293 10 0 -14 -3 14807.5 384.217 10 0 -14 3 13934.2 386.141 10 0 -14 4 28836.1 609.151 10 0 -14 -4 28264.5 585.760 10 0 14 5 173.899 54.2260 4 0 -14 5 253.372 63.6344 10 0 -14 -5 309.186 59.4285 10 0 14 6 1296.03 99.6043 4 0 -14 6 1421.22 122.820 10 0 14 6 1270.83 92.9134 6 0 14 7 279.821 56.8731 4 0 14 7 294.952 127.454 2 0 -14 7 328.969 75.4988 10 0 14 7 273.984 52.3224 6 0 14 8 9817.94 282.326 4 0 -14 8 9713.57 327.216 10 0 14 8 9975.05 279.313 6 0 14 9 11157.5 632.605 2 0 14 9 11727.9 315.524 4 0 14 9 11513.0 310.468 6 0 14 10 18207.5 423.326 4 0 14 10 18762.0 422.318 6 0 14 11 13904.1 352.990 4 0 14 11 13555.2 352.161 6 0 14 12 38.7603 45.0776 4 0 14 12-48.3372 44.9356 6 0 14 13 64.3294 45.7900 4 0 14 13 79.2229 49.2268 6 0 14 14 12920.1 343.217 4 0 14 14 12713.4 345.908 6 0 14 15 41320.1 743.907 4 0 14 15 40537.3 750.326 6 0 14 16 5059.96 202.504 4 0 14 16 5075.92 209.720 6 0 14 17 16934.2 404.390 4 0 14 17 17360.9 419.453 6 0 14 18 6054.27 214.140 4 0 14 18 6090.46 228.783 6 0 14 19 786.911 77.4998 4 0 14 19 825.529 92.1996 6 0 14 20 8509.01 242.952 4 0 14 20 9082.18 277.142 6 0 14 21 7605.50 248.617 6 0 14 22 100.742 49.9675 8 0 14 23 12123.2 296.528 8 0 14 24 3000.36 132.106 8 0 14 25 77.9561 29.1378 8 0 -15 0-11.7307 50.2437 10 0 -15 1 208.019 61.4581 10 0 -15 -1 304.385 63.9397 10 0 -15 2 1038.60 105.913 10 0 -15 -2 1009.23 113.034 10 0 -15 -3 40842.9 770.048 10 0 -15 3 40336.9 785.535 10 0 15 4 24813.6 514.576 4 0 -15 -4 25759.9 552.895 10 0 -15 4 24777.9 568.387 10 0 15 5 37008.5 683.744 4 0 -15 5 37716.8 752.226 10 0 15 6 526.579 78.2262 4 0 -15 6 464.162 91.7286 10 0 15 7 96086.4 1452.29 4 0 15 7 97199.2 1433.76 6 0 15 8 627.219 85.1758 4 0 15 8 581.197 65.9316 6 0 15 9 1296.44 108.007 4 0 15 9 1340.36 99.9821 6 0 15 10 2962.70 153.185 4 0 15 10 3047.22 152.789 6 0 15 11 43496.3 772.397 4 0 15 11 43054.5 771.232 6 0 15 12 6399.92 230.163 4 0 15 12 6383.51 232.184 6 0 15 13 995.856 93.9496 4 0 15 13 741.804 86.0107 6 0 15 14 10654.8 305.627 4 0 15 14 10839.8 314.121 6 0 15 15 18882.0 433.447 4 0 15 15 19355.9 445.743 6 0 15 16 255.375 59.6542 4 0 15 16 323.419 67.3945 6 0 15 17 1098.11 92.9173 4 0 15 17 1172.42 101.358 6 0 15 18 903.842 83.0649 4 0 15 18 887.927 91.9338 6 0 15 19 401.899 62.2103 4 0 15 19 304.059 63.3300 6 0 15 20 22.0249 45.7122 6 0 15 21 79.2395 45.3771 8 0 15 22 7587.64 213.693 8 0 15 23 4607.82 147.399 8 0 16 1 18311.0 421.845 4 0 16 2 2129.06 129.350 4 0 16 3 940.917 91.0382 4 0 16 4 50.3637 51.4589 4 0 16 5 42482.6 760.935 4 0 16 6 43.3723 54.0891 4 0 16 7 380.468 69.6112 4 0 16 7 297.204 50.5007 6 0 16 8 309.027 64.5989 4 0 16 8 275.350 58.7931 6 0 16 9 11928.7 327.312 4 0 16 9 12045.2 319.823 6 0 16 10 22.8371 53.4980 4 0 16 10 62.3664 47.3107 6 0 16 11 23495.5 498.988 4 0 16 11 23507.9 498.003 6 0 16 12 285.176 65.2691 4 0 16 12 320.510 59.9759 6 0 16 13 11675.7 320.059 4 0 16 13 11987.6 326.606 6 0 16 14 184.835 64.5914 4 0 16 14 91.2549 47.5310 6 0 16 15 8669.15 263.094 4 0 16 15 8443.79 269.078 6 0 16 16 3434.39 156.974 4 0 16 16 2487.84 141.145 6 0 16 17 11210.3 293.330 4 0 16 17 11121.9 306.593 6 0 16 18 3418.84 146.307 4 0 16 18 3017.91 150.515 6 0 16 19 7869.95 218.048 4 0 16 20 8570.46 233.965 8 0 16 21 628.900 61.1696 8 0 17 0 49.0824 43.9976 4 0 17 -1 523.989 81.8192 4 0 17 1 334.535 65.1793 4 0 17 2 2519.76 139.602 4 0 17 -2 2608.04 135.651 4 0 17 -3 10603.4 284.601 4 0 17 3 11005.0 307.740 4 0 17 4 2446.54 137.840 4 0 17 -4 2300.63 121.758 4 0 17 5 7249.17 243.591 4 0 17 6 1275.95 107.136 4 0 17 7 4320.65 184.083 4 0 17 8 2614.80 144.855 4 0 17 9 2277.73 138.632 4 0 17 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18 53.5645 50.8950 8 1 3 19 21444.3 508.658 8 1 -3 19 22116.2 495.396 8 1 3 19 21463.0 455.659 5 1 -3 19 21707.2 451.583 5 1 -3 20 3341.70 177.127 8 1 3 20 3067.00 179.144 8 1 3 20 3289.74 153.702 5 1 -3 20 3189.59 150.406 5 1 3 21 12241.7 374.309 8 1 -3 21 11638.0 350.678 8 1 -3 21 12239.0 328.063 5 1 3 22 9645.12 329.736 8 1 -3 22 9687.72 311.738 8 1 -3 22 9172.71 283.785 5 1 3 22 9371.04 285.873 5 1 3 23 507.540 74.6503 5 1 -3 23 612.570 88.5998 8 1 3 23 559.874 93.8588 8 1 -3 24 2215.91 146.857 8 1 3 24 1980.30 145.439 8 1 3 24 1965.13 131.817 5 1 -3 25 4322.76 200.953 8 1 3 25 4174.02 199.044 8 1 3 26 3838.55 186.440 8 1 -3 26 4042.60 184.733 8 1 -3 27 3481.23 169.982 8 1 3 27 3627.69 172.849 8 1 3 28 1218.13 101.631 8 1 -3 28 1084.41 98.5972 8 1 -3 29-10.9909 45.6213 8 1 3 29 69.5718 50.6607 8 1 3 30 979.691 80.3690 8 1 3 31 8228.14 211.936 8 1 3 32 1247.97 70.9253 8 -1 4 32 3465.22 125.123 8 -1 4 31 2468.96 117.277 8 -1 4 30 9255.70 254.068 8 -1 4 29 2093.75 126.049 8 -1 -4 29 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1 4 24 358.498 73.9468 8 1 -4 24 400.468 73.8722 8 1 4 25-10.8988 58.4392 8 1 -4 25 80.8864 55.6443 8 1 4 26 518.107 82.9961 8 1 -4 26 581.480 82.0883 8 1 4 27 399.320 73.3281 8 1 -4 27 391.372 73.5772 8 1 4 28 351.482 65.2922 8 1 -4 28 314.031 61.2134 8 1 4 29 746.332 78.9982 8 1 4 30 2464.41 116.940 8 1 4 31 4307.33 142.312 8 -1 5 32 9223.27 213.113 8 -1 5 31 3.08955 36.0728 8 -1 5 30 544.723 65.0858 8 -1 5 29 54.1686 47.1333 8 -1 5 29 108.277 46.6585 7 -1 5 28 12013.4 314.280 7 -1 5 28 11884.6 319.993 8 -1 -5 27 1098.95 110.913 8 -1 5 27 1123.87 107.742 8 -1 5 27 1084.00 101.195 7 -1 5 26 2268.28 146.995 8 -1 -5 26 2332.16 151.599 8 -1 -5 26 2453.84 154.999 7 -1 5 26 2158.74 138.593 7 -1 5 25 8664.65 291.909 8 -1 -5 25 8887.26 301.572 7 -1 -5 25 8594.26 293.986 8 -1 5 25 8127.48 277.459 7 -1 -5 24 5835.19 238.782 8 -1 -5 24 5723.45 241.955 7 -1 5 24 5663.02 238.194 8 -1 5 24 5458.22 224.829 7 -1 -5 23 3442.84 187.551 7 -1 -5 23 3439.65 186.706 8 -1 5 23 3778.36 197.075 8 -1 -5 22 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316.919 8 1 5 19 9904.81 277.504 6 1 5 19 10275.1 281.904 5 1 -5 19 9881.17 277.113 5 1 5 20 19140.2 794.272 2 1 -5 20 18986.8 459.505 8 1 5 20 19173.2 424.696 5 1 5 20 18451.7 418.394 6 1 -5 21 1280.46 110.878 8 1 5 21 1283.80 131.072 8 1 5 21 1415.41 103.375 6 1 5 21 1260.46 103.130 5 1 5 22 81.9925 39.3232 5 1 5 22 100.170 94.6265 8 1 -5 22 155.195 65.6693 8 1 5 23 1084.70 122.634 8 1 -5 23 931.782 102.913 8 1 5 23 966.185 96.0103 5 1 5 24 25960.4 580.634 8 1 -5 24 25408.1 555.391 8 1 5 24 24735.9 528.959 5 1 -5 25 91.4358 68.6227 8 1 5 25-36.3417 66.8717 8 1 5 26 564.868 83.9437 8 1 -5 26 558.260 80.7949 8 1 5 27 3534.83 171.665 8 1 -5 27 3347.36 163.838 8 1 5 28 16492.4 380.839 8 1 5 29 2639.13 129.992 8 1 5 30 894.714 74.5578 8 1 5 31 671.882 58.9141 8 -1 6 32 110.721 31.0094 8 -1 6 31 26.2117 31.8809 8 -1 6 30 1972.31 106.894 8 -1 6 29 3348.08 144.149 7 -1 6 29 3367.87 148.922 8 -1 6 28 14165.9 342.027 7 -1 6 28 13979.0 346.701 8 -1 6 27 2772.91 153.129 8 -1 6 27 3013.80 154.025 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6 16 1472.07 206.666 2 1 6 16 1410.55 94.4235 6 1 6 17 7240.38 456.365 2 1 -6 17 7812.69 263.292 8 1 6 17 7527.45 230.060 6 1 6 17 7792.81 230.239 5 1 6 18 17867.5 741.070 2 1 -6 18 19669.7 459.819 8 1 -6 18 19028.6 432.052 7 1 6 18 18828.0 416.600 5 1 6 18 19147.2 417.319 6 1 6 19 1281.67 209.445 2 1 -6 19 1250.67 110.494 8 1 6 19 1148.67 92.4350 6 1 6 19 1037.45 85.0512 5 1 6 20 5449.11 424.813 2 1 -6 20 5296.25 223.891 8 1 6 20 5381.44 201.359 6 1 -6 21 5625.77 231.400 8 1 6 21 5734.17 213.875 6 1 6 21 5735.74 210.735 5 1 6 22 2803.28 176.031 8 1 -6 22 2697.88 161.108 8 1 6 22 2714.65 148.004 6 1 6 22 2574.52 141.929 5 1 6 23 1268.32 126.136 8 1 -6 23 1459.38 121.637 8 1 6 23 1231.59 103.623 5 1 6 23 1211.82 102.179 6 1 -6 24 819.537 92.9972 8 1 6 24 970.842 110.342 8 1 6 24 759.469 95.9524 5 1 -6 25 212.566 63.3765 8 1 6 25 145.408 66.6906 8 1 6 26 117.011 67.1512 8 1 6 27 186.730 61.0001 8 1 6 28 2041.86 121.367 8 1 6 29 144.359 48.7520 8 1 6 30 862.569 69.3029 8 1 6 31-4.08659 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47.5824 7 -2 9 28 76.7637 38.5145 8 -2 9 28 67.7312 44.7690 7 -2 9 27 1810.08 105.739 8 -2 9 27 1989.32 119.143 7 -2 9 26 1369.31 101.240 8 -2 9 26 1533.91 111.473 7 -2 9 25 1894.20 120.264 8 -2 9 24 320.918 73.5389 8 -2 9 23 4435.88 168.776 4 -2 9 23 4802.21 210.921 8 -2 9 22 18983.8 414.855 4 -2 9 22 19650.2 471.031 8 -2 9 21 1849.29 116.857 4 -2 9 21 1995.02 143.033 8 -2 9 20 17209.4 401.897 4 -2 9 20 16547.8 431.231 8 -2 9 20 16813.8 440.332 6 -2 9 19 17841.2 418.225 4 -2 9 19 18129.4 453.363 6 -2 9 18 15512.2 812.699 2 -2 9 18 14827.5 373.401 4 -2 9 18 14443.5 389.427 6 -2 9 17 6388.81 510.254 2 -2 9 17 5878.69 219.713 4 -2 9 17 6171.35 231.991 6 -2 9 16 344.245 152.813 2 -2 9 16 393.184 63.5385 4 -2 9 16 310.561 63.2211 6 -2 9 15 13.0152 39.4414 4 -2 9 15 58.8521 43.3829 6 -2 9 14 972.710 187.712 2 -2 9 14 1018.90 86.0887 4 -2 9 14 1163.25 92.6248 6 -2 9 13 261.790 50.5060 4 -2 9 13 275.092 47.6782 6 -2 9 12 9949.05 545.010 2 -2 9 11 8840.76 496.531 2 -2 9 10 705.873 145.871 2 -2 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98539.9 2039.90 2 -2 -12 5 94906.0 1462.49 10 -2 12 4 19533.7 763.650 2 -2 -12 4 19657.7 446.813 10 -2 -12 3 425.016 65.9355 10 2 12 1 61491.1 1389.83 2 2 12 2 970.549 158.508 2 2 12 3 2788.13 275.076 2 2 12 4 459.382 130.026 2 2 12 4 581.117 70.1631 6 2 12 5 7242.19 459.144 2 2 12 5 7196.35 230.787 6 2 12 6 25997.2 931.232 2 2 12 6 26482.7 523.470 6 2 12 7 16597.8 741.590 2 2 12 7 15798.4 375.903 6 2 12 8 3699.88 351.059 2 2 12 8 3925.70 170.785 6 2 12 9 33020.5 1119.56 2 2 12 9 32477.1 617.647 6 2 12 10 7279.21 510.145 2 2 12 10 7325.72 235.282 4 2 12 10 7401.86 242.668 6 2 12 11 8645.95 564.909 2 2 12 11 8872.24 259.798 4 2 12 11 8869.79 273.244 6 2 12 12 3502.67 155.622 4 2 12 12 3681.49 169.813 6 2 12 13 5321.32 199.703 4 2 12 13 5816.72 220.177 6 2 12 14 2031.26 118.399 4 2 12 14 1886.09 124.652 6 2 12 15 354.140 57.2385 4 2 12 15 446.510 68.7066 6 2 12 16 9638.18 270.824 4 2 12 16 9369.66 288.850 6 2 12 17 636.486 81.0039 6 2 12 18 94.6560 51.5718 6 2 12 19 2902.30 151.306 6 2 12 20 578.279 74.7320 6 2 12 21 245.413 60.9801 6 2 12 22 762.683 79.9362 6 2 12 23 2764.13 148.212 8 2 12 23 2807.96 135.920 6 2 12 24 1005.58 86.0086 8 2 12 25 97.8637 47.2256 8 2 12 26 5720.89 163.294 8 -2 13 27 2393.61 96.4278 7 -2 13 26 8849.39 219.447 7 -2 13 23 3327.82 128.728 4 -2 13 22 655.377 70.0191 4 -2 13 21 138.973 47.3127 4 -2 13 20 1669.66 112.087 4 -2 13 19 320.275 68.0497 4 -2 13 18 27845.7 568.758 4 -2 13 18 27670.1 598.162 6 -2 13 17 2972.14 163.710 4 -2 13 17 2993.06 171.450 6 -2 13 16 8890.15 284.559 4 -2 13 16 8530.45 294.115 6 -2 13 15 1893.83 132.450 4 -2 -13 15 1841.61 138.326 10 -2 13 15 1860.55 133.057 6 -2 13 14 7568.75 257.311 4 -2 -13 14 7098.31 269.361 10 -2 13 14 7288.81 260.284 6 -2 13 13 5924.53 225.643 4 -2 -13 13 5694.35 240.769 10 -2 13 13 5714.12 224.886 6 -2 13 12 8391.61 264.747 4 -2 -13 12 7750.64 283.088 10 -2 13 12 7540.01 257.609 6 -2 13 11 11887.4 323.505 4 -2 13 11 11161.6 683.500 2 -2 -13 11 11939.8 357.663 10 -2 13 11 11403.8 317.022 6 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14 12.9135 36.1120 5 3 9 14 30.1030 37.0587 6 3 9 15 3936.98 175.683 6 3 9 15 3760.67 157.805 5 3 9 16 16794.2 398.019 6 3 9 16 16417.4 376.364 5 3 9 17 4970.30 190.425 5 3 9 17 5273.80 201.229 6 3 9 18 81.8128 38.2578 5 3 9 18 132.237 47.0202 6 3 9 19 3753.32 162.147 5 3 9 19 3821.45 169.369 6 3 9 20 564.291 65.4751 5 3 9 20 522.031 70.0894 6 3 9 21 600.121 70.4855 5 3 9 21 483.108 65.1022 6 3 9 22 5359.94 231.281 8 3 9 22 5177.44 183.355 5 3 9 22 5273.56 190.044 6 3 9 23 63.6186 31.7839 5 3 9 23 70.8937 60.2117 8 3 9 24 104.719 58.2645 8 3 9 25 3781.08 161.415 8 3 9 26 8410.55 229.036 8 3 9 27 208.539 42.7881 8 -3 10 29 9326.99 223.033 7 -3 10 28 1740.16 99.6030 7 -3 10 27 173.118 52.5939 7 -3 10 26 2890.82 143.786 7 -3 10 24 509.961 60.3753 4 -3 10 23 297.815 54.4018 4 -3 10 22 54860.8 896.101 4 -3 10 21 4834.95 196.006 4 -3 10 20 1689.36 116.553 4 -3 10 19 10942.8 314.832 4 -3 10 18 21536.1 480.209 4 -3 10 17 219.837 61.6910 4 -3 10 16 10539.1 636.826 1 -3 10 16 10511.7 671.319 2 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41.9095 6 3 10 8 9348.68 555.506 2 3 10 8 9275.68 272.284 6 3 10 9 18169.2 805.712 2 3 10 9 17833.6 408.388 6 3 10 10 4464.75 392.652 2 3 10 10 4380.04 181.437 6 3 10 11 31715.8 1112.53 2 3 10 11 29436.8 584.520 6 3 10 12 1928.18 279.480 2 3 10 12 1985.59 123.553 6 3 10 13 19977.0 882.369 2 3 10 13 17850.3 421.949 6 3 10 14 23539.4 502.684 6 3 10 15 901.432 88.0220 6 3 10 16 1444.86 109.000 6 3 10 17 18327.1 424.536 6 3 10 18 5279.75 186.915 5 3 10 18 5200.78 203.032 6 3 10 19 1712.71 105.264 5 3 10 19 1681.58 115.948 6 3 10 20 5203.65 180.912 5 3 10 20 4851.31 190.718 6 3 10 21 41.6442 36.4312 5 3 10 21 32.9398 42.5690 6 3 10 22 124.507 38.4271 5 3 10 22 141.423 49.9021 6 3 10 23 310.043 71.6291 8 3 10 24 2135.56 128.309 8 3 10 25 509.801 66.2639 8 3 10 26 2907.87 121.689 8 -3 11 29 551.750 50.8446 7 -3 11 28 2714.40 112.151 7 -3 11 27 59.6276 43.6680 7 -3 11 26 477.384 64.6945 7 -3 11 24 191.523 44.3164 4 -3 11 23 5010.32 176.958 4 -3 11 22 173.520 54.6925 4 -3 11 21 485.329 71.1641 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2 -3 11 4 101.068 70.9170 2 -3 11 2 16358.8 673.279 1 3 11 -1 98.6481 60.7217 2 -3 11 1 148.381 83.1325 1 3 11 0 14385.6 609.976 2 -3 11 0 13993.2 594.254 1 3 11 1 7753.35 451.527 2 -3 11 -1 7497.61 416.437 1 3 11 2 1508.68 204.971 2 3 11 3 243.566 120.212 2 3 11 4 2441.55 272.767 2 3 11 4 2413.49 130.541 6 3 11 5 22051.4 860.778 2 3 11 5 21849.5 465.129 6 3 11 6 639.389 143.412 2 3 11 6 303.605 51.8848 6 3 11 7 7155.28 496.389 2 3 11 7 7292.87 242.575 6 3 11 8 14612.8 727.045 2 3 11 8 14488.4 362.451 6 3 11 9 654.130 151.598 2 3 11 9 567.576 72.8505 6 3 11 10 12328.6 671.963 2 3 11 10 11639.1 322.170 6 3 11 11 7475.54 528.624 2 3 11 11 7571.48 231.270 4 3 11 11 7676.70 253.920 6 3 11 12 113.078 107.507 2 3 11 12 131.959 52.8703 4 3 11 12 110.299 47.3981 6 3 11 13 20951.1 469.615 6 3 11 14 251.188 59.6469 6 3 11 15 616.256 81.4922 6 3 11 16 5764.81 219.289 6 3 11 17 259.360 59.1442 6 3 11 18 19892.5 449.460 6 3 11 19 6495.73 225.708 6 3 11 20 5641.63 204.761 6 3 11 21 153.177 53.0056 6 3 11 22 4782.10 177.859 6 3 11 23 10614.2 298.981 8 3 11 24 1384.53 98.7340 8 3 11 25 473.270 58.9065 8 3 11 26 2248.12 96.0373 8 -3 12 28 1411.22 74.8988 7 -3 12 27 316.341 48.9764 7 -3 12 26 1031.53 79.9896 7 -3 12 24 304.925 45.7967 4 -3 12 23 3765.98 150.246 4 -3 12 22 1662.70 106.408 4 -3 12 21 987.637 88.7259 4 -3 12 20 19221.7 433.313 4 -3 12 19 4691.69 195.864 4 -3 12 18 759.497 92.7007 4 -3 12 17 37442.6 710.543 4 -3 12 16 177.760 59.5451 4 -3 12 15 328.634 69.8229 4 -3 -12 15 356.953 69.1268 10 -3 12 14 5620.60 219.522 4 -3 -12 14 5286.06 228.567 10 -3 12 14 5301.13 223.329 6 -3 12 13 26542.5 547.842 4 -3 12 13 25009.3 1057.95 2 -3 -12 13 26274.3 581.227 10 -3 12 13 25755.8 552.196 6 -3 12 12 265.871 57.0222 4 -3 12 12 133.411 122.129 2 -3 -12 12 367.079 68.1845 10 -3 12 12 325.234 67.6561 6 -3 12 11 38800.8 702.531 4 -3 12 11 36637.2 1271.16 2 -3 -12 11 38218.7 742.646 10 -3 12 11 37840.8 705.683 6 -3 12 10 60.1322 50.0812 4 -3 12 10 48.4817 97.3970 2 -3 -12 10 202.114 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114.687 6 3 13 5 9461.93 574.887 2 -3 -13 -5 9406.59 291.410 10 3 13 5 9525.86 286.135 6 3 13 6 182.871 132.867 2 3 13 6 230.370 56.8843 6 3 13 7 848.239 185.245 2 3 13 7 913.761 89.3548 6 3 13 8 4156.62 186.051 6 3 13 9 472.048 71.4062 6 3 13 10 6433.14 219.669 4 3 13 10 6351.03 233.148 6 3 13 11 236.956 60.6794 4 3 13 11 247.964 61.1530 6 3 13 12 1640.40 108.080 4 3 13 12 1566.27 115.007 6 3 13 13 139.661 45.6866 4 3 13 13 92.7583 54.2413 6 3 13 14 16785.8 377.488 4 3 13 14 17002.9 410.995 6 3 13 15 15413.9 384.736 6 3 13 16 13835.0 357.770 6 3 13 17 1418.41 109.127 6 3 13 18 5210.66 198.425 6 3 13 19 3243.00 151.960 6 3 13 20 3719.22 156.406 6 3 13 21 415.297 59.6567 6 3 13 22 5300.98 189.397 8 3 13 22 4734.86 166.398 6 3 13 23 62.1484 45.9101 8 3 13 24-3.23069 32.7999 8 -3 14 26 4100.04 126.060 7 -3 14 25 48.5290 38.6192 7 -3 14 23 1386.24 80.6592 4 -3 14 22 55.9804 44.0902 4 -3 14 21 1534.54 98.2597 4 -3 14 20 1791.85 110.223 4 -3 14 19 61.6294 49.3636 4 -3 14 18 698.413 81.7783 4 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581.721 66.7396 6 5 13 18 1253.75 84.5635 6 5 13 19 6995.38 195.124 6 5 13 20 226.527 54.4208 8 -5 14 24-3.08653 25.9746 4 -5 14 24 21.1816 32.3823 7 -5 14 23 2060.74 92.6649 4 -5 14 22 4222.45 141.900 4 -5 14 21 3785.40 143.712 4 -5 14 20 7614.25 217.298 4 -5 14 19 2422.51 122.987 4 -5 14 18 468.686 69.6553 4 -5 14 17 943.374 87.3780 4 -5 14 16 3024.02 150.389 4 -5 -14 16 2978.25 157.669 10 -5 14 15 612.635 76.9186 4 -5 -14 15 689.685 88.5393 10 -5 14 14 8465.71 264.733 4 -5 -14 14 8597.78 296.230 10 -5 14 13 3657.38 170.887 4 -5 -14 13 3783.28 197.605 10 -5 14 12 2850.03 149.634 4 -5 -14 12 2941.72 179.321 10 -5 14 11 302.722 59.6219 4 -5 -14 11 313.054 79.1392 10 -5 14 10 503.034 67.8205 4 -5 -14 10 551.369 90.0977 10 -5 14 9 4823.12 198.814 4 -5 -14 9 4552.57 228.748 10 -5 14 8 19.7326 47.2177 4 -5 -14 8 83.9490 63.7802 10 -5 14 7 1340.52 101.974 4 -5 14 6 1299.36 99.2548 4 5 14 -5 6.60547 41.5698 6 5 14 -4 21900.6 487.945 6 5 14 -3 12435.9 344.738 6 5 14 -2 2771.88 152.934 6 5 14 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2626.08 138.336 4 -5 -15 13 2475.62 155.251 10 -5 15 12 17545.0 402.669 4 -5 -15 12 17611.7 457.058 10 -5 15 11 1207.09 100.880 4 -5 -15 11 1357.70 125.620 10 -5 15 10 818.629 82.5404 4 -5 -15 10 848.221 103.638 10 -5 15 9 1078.94 92.9164 4 -5 -15 9 1005.12 116.115 10 -5 15 8 5191.85 196.290 4 -5 -15 8 5273.63 243.467 10 -5 15 7 180.024 49.2979 4 -5 -15 7 285.222 84.6083 10 -5 15 6 1643.42 111.856 4 -5 -15 6 1615.38 136.692 10 -5 -15 5 2933.82 183.172 10 -5 -15 4 23102.0 556.583 10 5 15 -4 23328.9 493.211 6 -5 -15 3 1081.18 115.547 10 5 15 -3 1191.73 100.109 6 -5 -15 2 4080.64 209.364 10 5 15 -2 4192.94 181.259 6 -5 -15 1 105.832 75.8509 10 5 15 -1 143.664 48.6943 6 -5 -15 0 3771.12 196.059 10 5 15 0 4005.18 181.338 6 -5 -15 -1 2682.68 162.643 10 5 15 1 2482.63 144.049 6 -5 -15 -2 389.713 73.4049 10 5 15 2 400.887 68.4755 6 -5 -15 -3 1925.67 132.116 10 5 15 3 1990.59 129.197 6 -5 -15 -4 7582.89 261.962 10 5 15 4 7235.94 251.695 6 -5 -15 -5 1120.06 99.5479 10 5 15 5 1092.94 99.6236 6 5 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611.522 5 7 -3 15 30739.9 585.654 5 7 -3 16 1.62357 42.7329 5 7 3 16 13.9086 51.1850 5 7 -3 17 74.5555 45.9919 5 7 3 17-6.70607 42.0097 5 7 -3 18 306.448 52.5977 5 7 3 18 165.234 52.8086 5 7 3 19 2582.85 133.671 5 7 3 20 2010.04 114.778 5 7 3 21 3458.95 143.167 5 7 3 22 1104.88 77.3881 5 7 3 23 2933.02 114.713 5 7 3 24 2447.62 95.9250 5 -7 4 29 1330.52 77.4097 7 -7 -4 28 1996.64 107.022 9 -7 4 28 2179.82 104.976 7 -7 -4 27 3807.34 158.870 9 -7 4 27 3768.39 147.168 7 -7 4 26 79.1895 51.0994 4 -7 -4 26 34.9674 54.1871 9 -7 4 26 15.5318 42.8595 7 -7 4 25 3994.67 169.791 4 -7 -4 25 3959.39 181.647 9 -7 4 25 4096.70 168.724 9 -7 4 25 3945.67 164.935 7 -7 4 24 963.171 94.4935 4 -7 4 24 1109.56 100.172 9 -7 -4 24 1076.82 104.583 9 -7 4 24 1055.62 91.5043 7 -7 -4 24 1026.99 93.3401 7 -7 4 23 1637.29 125.145 4 -7 4 23 1779.64 113.035 7 -7 -4 23 1835.79 139.590 9 -7 4 23 1624.58 116.578 9 -7 -4 23 1757.83 117.178 7 -7 4 22 3869.15 192.951 4 -7 -4 22 4854.89 219.381 9 -7 4 22 4617.64 197.003 9 -7 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1979.74 115.672 7 -7 5 24 15017.6 375.902 4 -7 5 24 15436.5 363.509 7 -7 5 24 16193.6 377.923 9 -7 5 23 3672.14 177.901 4 -7 -5 23 3918.09 192.381 9 -7 5 23 4079.53 176.969 9 -7 5 23 3856.70 166.495 7 -7 5 22 16298.7 404.663 4 -7 -5 22 17123.5 439.146 9 -7 5 22 16573.2 403.761 9 -7 5 22 16993.6 393.442 7 -7 -5 21 21812.5 526.833 9 -7 5 21 22510.3 475.459 7 -7 5 20 1884.90 125.764 4 -7 -5 20 1761.35 141.211 9 -7 5 20 1645.81 116.201 7 -7 5 19 1.62149 48.2667 4 -7 -5 19 35.3867 64.2077 9 -7 5 19 29.7161 45.0258 7 -7 -5 19 66.7761 44.1830 7 -7 5 18 547.918 76.3745 4 -7 -5 18 537.939 82.3852 9 -7 -5 18 468.379 71.3698 7 -7 5 17 19982.2 452.774 4 -7 -5 17 19904.3 498.037 9 -7 5 16 1690.62 116.115 4 -7 -5 16 1824.35 146.490 9 -7 5 15 261.473 62.2106 4 -7 -5 15 340.145 80.8532 9 -7 5 15 207.850 134.823 1 -7 5 14 97.4164 45.2251 4 -7 -5 14 106.241 54.8787 9 -7 5 14-49.9997 97.8983 1 -7 5 13 2423.56 131.543 4 -7 -5 13 2210.96 149.979 9 -7 5 13 2460.50 295.791 1 -7 5 12 10261.8 280.826 4 -7 -5 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6 26 6119.41 189.710 7 -7 6 25 539.630 71.0173 4 -7 -6 25 626.614 81.6179 9 -7 6 25 662.206 72.3470 7 -7 6 24 564.839 74.2312 4 -7 -6 24 486.274 83.3418 9 -7 6 24 621.842 73.1152 9 -7 6 24 419.488 62.3294 7 -7 -6 23 2103.15 142.524 9 -7 6 23 2026.09 124.780 9 -7 6 23 1899.24 114.835 7 -7 -6 22 4486.28 210.016 9 -7 6 22 4440.28 179.955 7 -7 6 21 13711.0 350.538 4 -7 -6 21 13655.8 391.291 9 -7 6 21 13469.0 340.242 7 -7 6 20 909.326 94.5626 4 -7 -6 20 1002.81 111.851 9 -7 6 20 890.894 85.3337 7 -7 6 19 2545.07 143.176 4 -7 -6 19 2217.92 159.650 9 -7 6 19 2266.78 130.480 7 -7 6 18 3794.76 176.058 4 -7 -6 18 3931.72 205.597 9 -7 6 17 218.671 61.8099 4 -7 -6 17 267.119 71.6096 9 -7 6 16-0.08245 43.9588 4 -7 -6 16 20.3919 65.5255 9 -7 6 15 7669.61 250.155 4 -7 -6 15 7483.36 283.712 9 -7 6 14 2085.74 126.979 4 -7 -6 14 1891.39 144.559 9 -7 6 13 1175.11 94.1378 4 -7 -6 13 1032.87 108.133 9 -7 6 13 1273.17 214.197 1 -7 6 12 7396.76 235.488 4 -7 -6 12 7304.36 274.169 9 -7 6 11 820.826 79.2273 4 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4197.67 202.121 6 -7 -6 -4 362.842 167.957 3 7 6 4 294.522 63.3301 5 7 6 4 349.204 69.2811 6 -7 -6 -5 15230.9 836.920 3 7 6 5 16387.5 416.773 5 7 6 5 16240.1 422.467 6 -7 -6 -6 43.3200 95.6250 3 7 6 6 136.628 59.3751 5 7 6 6 28.9765 42.7497 6 -7 -6 -7 15623.1 844.598 3 7 6 7 16524.4 417.818 5 7 6 7 16644.5 421.153 6 7 6 8 6123.12 235.884 5 7 6 8 6117.58 234.493 6 7 6 9 2758.61 157.536 5 7 6 9 3039.12 157.884 6 7 6 10 17495.0 420.191 6 7 6 10 17368.9 433.662 5 7 6 11 7924.72 256.135 6 7 6 11 7435.16 264.755 5 7 6 12 26031.7 552.047 5 7 6 12 25707.7 524.199 6 7 6 13 4250.55 192.495 5 7 6 14 6039.03 225.834 5 7 6 15 310.427 63.1174 5 7 6 16 3376.62 160.269 5 7 6 17 1503.57 104.266 5 7 6 18 11795.1 304.020 5 7 6 19 4692.42 172.916 5 7 6 20 113.704 42.2886 5 7 6 21 3731.39 135.365 5 7 6 22 264.750 40.7629 5 -7 7 28 246.167 40.3398 7 -7 7 27 286.805 49.6996 4 -7 7 27 326.238 44.7515 7 -7 7 26 1743.49 101.351 4 -7 7 26 1676.44 93.3227 7 -7 7 25 11431.9 289.720 4 -7 -7 25 12270.5 318.450 9 -7 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9738.39 665.861 3 7 7 4 10367.6 322.177 5 7 7 4 10716.0 340.043 6 -7 -7 -5 6238.45 533.255 3 7 7 5 6358.26 245.438 5 7 7 5 6625.31 258.805 6 7 7 6 5117.98 215.020 5 7 7 6 4862.71 214.842 6 7 7 7 44.0105 45.2691 5 7 7 7 100.937 54.6608 6 7 7 8 2496.36 149.065 5 7 7 8 2206.44 139.412 6 7 7 9 34879.6 688.240 5 7 7 9 35824.7 687.505 6 7 7 10 26926.7 576.508 5 7 7 10 27963.5 572.765 6 7 7 11 50724.6 897.869 5 7 7 11 52466.6 890.127 6 7 7 12 12292.2 328.433 6 7 7 12 12232.6 343.148 5 7 7 13 22901.6 478.586 6 7 7 13 23488.0 504.334 5 7 7 14 1626.74 116.583 5 7 7 15 138.460 48.5300 5 7 7 16 666.501 77.2306 5 7 7 17 51.0169 38.8042 5 7 7 18 3114.67 138.186 5 7 7 19 15661.2 339.328 5 7 7 20 2144.16 102.989 5 7 7 21 139.156 34.2881 5 7 7 22 26.5943 24.2883 5 -7 8 27 9444.77 222.166 4 -7 8 27 9298.04 212.830 7 -7 8 26 4483.23 153.650 4 -7 8 26 4564.29 146.769 7 -7 8 25 4151.59 155.411 4 -7 8 25 4254.85 149.863 7 -7 8 24 230.895 49.4017 4 -7 8 24 298.542 53.5958 7 -7 8 23 5506.21 201.675 4 -7 -8 23 5963.93 226.560 9 -7 8 23 5814.63 195.613 9 -7 8 23 5581.72 187.657 7 -7 8 22 4461.62 178.947 4 -7 -8 22 4469.78 203.044 9 -7 8 22 4492.87 170.700 7 -7 8 21 5942.97 210.243 4 -7 -8 21 5804.12 241.857 9 -7 8 21 5838.80 201.720 7 -7 8 20 1200.23 100.923 4 -7 -8 20 1272.47 123.571 9 -7 8 20 1210.86 96.5144 7 -7 8 19 3612.14 167.442 4 -7 -8 19 3651.93 196.749 9 -7 8 19 3893.42 166.266 7 -7 8 18 5328.33 206.748 4 -7 -8 18 5565.25 243.473 9 -7 8 17 477.899 67.7449 4 -7 -8 17 433.173 90.0011 9 -7 8 16 2910.67 149.920 4 -7 -8 16 2750.84 172.494 9 -7 8 15 412.155 68.1345 4 -7 -8 15 398.741 80.6329 9 -7 8 14 11488.4 307.628 4 -7 -8 14 10997.7 354.605 9 -7 8 13-0.85034 42.4351 4 -7 -8 13-43.4053 64.7965 9 -7 8 12 1702.32 111.152 4 -7 -8 12 1727.83 136.235 9 -7 8 11 911.142 82.1554 4 -7 -8 11 881.203 101.636 9 -7 8 10 9839.50 271.164 4 -7 -8 10 9693.40 319.892 9 -7 8 10 10662.6 617.570 1 -7 8 9 23391.2 469.460 4 -7 -8 9 23707.2 543.559 9 -7 8 9 24064.3 949.649 1 -7 8 8 23238.4 928.209 1 -7 -8 8 24718.7 1036.42 3 -7 8 8 23464.1 462.349 4 -7 8 7 7344.21 503.686 1 -7 -8 7 8181.16 593.512 3 -7 -8 6 4542.80 445.440 3 -7 8 6 5013.97 413.213 1 7 8 -6 4534.99 243.514 5 -7 -8 5 497.877 166.501 3 -7 8 5 565.259 149.007 1 7 8 -5 566.706 91.4642 5 -7 8 4 2800.68 319.389 1 -7 -8 4 3123.01 378.087 3 7 8 -4 3209.89 180.022 5 -7 8 3 24282.6 961.185 1 -7 -8 3 26803.4 1148.85 3 7 8 -3 25055.8 571.658 5 -7 8 2 4504.65 401.049 1 -7 -8 2 4885.56 487.063 3 7 8 -2 4818.47 219.672 5 -7 8 1 31323.4 1113.66 1 -7 -8 1 31906.9 1271.03 3 7 8 -1 30199.0 637.439 5 -7 -8 0-33.6491 152.777 3 7 8 0-27.4845 48.3648 5 -7 -8 -1 302.150 150.933 3 7 8 1 42.3915 47.9146 5 7 8 1 258.267 75.0932 6 -7 -8 -2 90.3934 98.5955 3 7 8 2 231.109 64.5316 5 7 8 2 232.558 62.4449 6 -7 -8 -3 9846.68 694.305 3 7 8 3 10311.2 317.234 5 7 8 3 10065.1 334.580 6 7 8 4 11145.9 328.135 5 7 8 4 10877.0 344.306 6 7 8 5 4049.67 187.843 5 7 8 5 3827.05 195.572 6 7 8 6 1473.93 116.432 5 7 8 6 1608.02 127.951 6 7 8 7 551.050 78.0605 5 7 8 7 541.689 83.3066 6 7 8 8 72174.4 1179.85 6 7 8 8 70597.7 1159.98 5 7 8 9 3983.20 185.431 5 7 8 9 3874.42 186.529 6 7 8 10 89.8079 53.5297 5 7 8 10 1.30051 44.4667 6 7 8 11 1496.17 112.062 5 7 8 11 1600.98 119.704 6 7 8 12 15224.6 375.491 6 7 8 12 15180.9 379.499 5 7 8 13 138.426 51.7262 5 7 8 13 55.6839 38.1608 6 7 8 14 28439.8 566.235 5 7 8 14 29415.3 548.913 6 7 8 15 4690.03 189.391 5 7 8 16 169.580 49.1046 5 7 8 17 4159.67 162.093 5 7 8 18 1138.22 80.7893 5 7 8 19 3081.83 127.750 5 7 8 20 4049.40 136.970 5 7 8 21 481.899 46.3838 5 -7 9 27 76.4916 31.3507 4 -7 9 26 610.076 57.5067 4 -7 9 26 643.696 55.9347 7 -7 9 25-7.20527 35.5434 4 -7 9 25 62.6291 34.8308 7 -7 9 24 404.960 58.2928 4 -7 9 24 391.989 55.3633 7 -7 9 23 152.359 47.2543 4 -7 9 23 242.091 49.9380 7 -7 9 22 96.6837 51.8238 4 -7 9 22 170.433 49.3489 7 -7 9 21 18698.6 409.091 4 -7 -9 21 19214.4 461.919 9 -7 9 21 19002.3 399.680 7 -7 9 20 2159.86 124.674 4 -7 -9 20 1874.69 141.580 9 -7 9 20 2002.33 115.418 7 -7 9 19 4882.41 190.498 4 -7 -9 19 5153.57 226.532 9 -7 9 18 180.663 53.9181 4 -7 -9 18 266.612 78.5244 9 -7 9 17 23830.8 493.738 4 -7 -9 17 23408.8 553.761 9 -7 9 16 1520.91 108.102 4 -7 -9 16 1582.20 135.965 9 -7 9 15 632.215 75.2276 4 -7 -9 15 629.441 95.4098 9 -7 9 14 485.341 71.0007 4 -7 -9 14 406.412 84.7648 9 -7 9 13 2631.21 143.271 4 -7 -9 13 2179.10 155.123 9 -7 9 12 2235.07 127.873 4 -7 -9 12 2264.60 156.150 9 -7 9 11 102.385 42.4920 4 -7 -9 11 275.498 92.1100 9 -7 9 10 4376.92 173.761 4 -7 -9 10 4357.19 208.141 9 -7 9 9 5252.16 185.737 4 -7 -9 9 4976.66 220.674 9 -7 9 8 258.080 53.1548 4 -7 -9 7 1863.38 315.884 3 -7 9 7 1763.26 245.848 1 7 9 -7 1886.70 151.541 5 -7 9 6 8564.66 555.608 1 -7 -9 6 9075.05 652.015 3 -7 -9 5 50303.3 1658.30 3 -7 9 5 47933.1 1400.77 1 7 9 -5 48369.5 908.408 5 -7 -9 4 241.691 105.033 3 -7 9 4 355.310 142.478 1 7 9 -4 440.834 77.2579 5 -7 9 3 5961.82 453.747 1 -7 -9 3 6244.36 571.879 3 7 9 -3 5869.67 240.241 5 -7 9 2 39563.9 1264.44 1 7 9 -2 41140.0 777.725 5 -7 -9 1 15215.5 893.224 3 7 9 -1 15215.6 399.437 5 7 9 -1 14797.4 422.034 6 -7 -9 0 2520.80 354.715 3 7 9 0 2713.50 155.731 5 7 9 0 2360.48 156.989 6 7 9 1 15688.2 405.503 5 7 9 1 15976.1 437.395 6 7 9 2 2547.77 148.220 5 7 9 2 2537.19 163.239 6 7 9 3 216.890 54.7688 5 7 9 3 214.586 63.1221 6 7 9 4 138.520 45.7980 5 7 9 4 250.676 64.2890 6 7 9 5 3743.65 177.267 5 7 9 5 3840.37 197.980 6 7 9 6 113.200 46.0113 5 7 9 6 39.6173 50.6761 6 7 9 7 1373.11 120.662 6 7 9 7 1273.43 107.610 5 7 9 8 2357.59 154.245 5 7 9 8 2385.27 149.467 6 7 9 9 786.960 87.8115 5 7 9 9 870.359 93.8280 6 7 9 10 700.682 80.2433 5 7 9 10 598.663 80.6327 6 7 9 11 2727.14 149.308 6 7 9 11 2553.70 140.080 5 7 9 12 4312.25 179.286 5 7 9 12 4298.10 183.751 6 7 9 13 5357.92 197.632 5 7 9 13 5256.45 196.898 6 7 9 14 245.653 48.1398 5 7 9 14 249.651 50.2925 6 7 9 15 325.748 52.0670 5 7 9 16 4443.87 164.306 5 7 9 17 24.1576 31.3469 5 7 9 18 203.030 39.1249 5 7 9 19 1439.50 79.9545 5 7 9 20 938.139 59.9871 5 -7 10 26 4903.56 144.758 4 -7 10 25 324.946 49.2653 4 -7 10 25 422.603 47.7159 7 -7 10 24 438.680 56.8071 4 -7 10 24 393.883 52.2494 7 -7 10 23 9207.81 243.625 4 -7 10 23 9067.77 230.493 7 -7 10 22 79.4731 46.8768 4 -7 10 22 115.807 39.9787 7 -7 10 21 48.3135 46.5164 4 -7 10 21 26.2824 39.7944 7 -7 10 20 832.101 82.4924 4 -7 10 20 754.080 72.7051 7 -7 10 19 14206.7 342.626 4 -7 10 18 718.803 80.8536 4 -7 10 17 9493.18 271.951 4 -7 -10 17 9329.45 317.243 9 -7 10 16 160.442 53.2891 4 -7 -10 16 315.858 79.3254 9 -7 10 15 2102.56 125.524 4 -7 -10 15 2355.73 166.279 9 -7 10 14 401.013 63.6032 4 -7 -10 14 417.723 82.5316 9 -7 10 13 284.747 53.2354 4 -7 -10 13 233.236 71.4655 9 -7 10 12 5270.36 194.923 4 -7 -10 12 5452.69 236.806 9 -7 10 11 1522.43 104.726 4 -7 -10 11 1596.17 134.876 9 -7 10 10 34.2957 36.9759 4 -7 -10 10 47.8648 56.6116 9 -7 10 9 67.6333 35.3218 4 -7 -10 9 106.728 49.1985 9 -7 10 8 3074.03 138.599 4 7 10 -5 26.5128 53.4766 5 7 10 -4 581.465 74.9808 5 7 10 -3 764.649 86.5750 5 7 10 -3 751.090 97.3571 6 7 10 -2 1044.88 103.079 5 7 10 -2 1024.41 113.063 6 7 10 -1 33135.9 650.644 5 7 10 -1 32438.2 694.580 6 7 10 0 658.837 79.8062 5 7 10 0 620.153 90.9229 6 7 10 1 28607.0 588.548 5 7 10 1 28556.8 630.820 6 7 10 2 97.0567 52.4678 5 7 10 2 67.3712 47.0665 6 7 10 3 2930.18 156.016 5 7 10 3 3135.28 179.169 6 7 10 4 3386.54 163.781 5 7 10 4 3455.47 185.777 6 7 10 5 10909.7 312.270 5 7 10 5 11225.0 348.013 6 7 10 6 21.4556 40.7489 5 7 10 6 42.3527 52.6684 6 7 10 7 379.364 62.5232 5 7 10 7 395.665 77.4957 6 7 10 8 1959.41 123.772 5 7 10 8 2189.24 146.317 6 7 10 9 231.847 53.0483 5 7 10 9 222.630 65.3910 6 7 10 10 2402.25 143.103 6 7 10 10 2521.77 135.338 5 7 10 11 156.006 50.5631 5 7 10 11 157.569 54.7454 6 7 10 12 2186.01 119.110 5 7 10 12 2214.34 129.688 6 7 10 13 104.546 39.3981 5 7 10 13 11.4838 43.5802 6 7 10 14 6659.44 212.324 6 7 10 14 6521.80 203.264 5 7 10 15 353.502 48.5580 5 7 10 15 395.717 53.5457 6 7 10 16 399.961 49.8723 5 7 10 17 246.494 39.7302 5 7 10 18 56.8341 30.2761 5 -7 11 25 205.382 37.0821 4 -7 11 24 871.654 68.9769 4 -7 11 24 876.132 60.7730 7 -7 11 23 1052.76 77.2332 4 -7 11 23 962.687 68.1763 7 -7 11 22 56.6678 40.1245 4 -7 11 22 39.3605 38.1930 7 -7 11 21 7638.12 218.941 4 -7 11 21 7355.40 205.739 7 -7 11 20 53.9322 41.0577 4 -7 11 20 58.3868 38.7671 7 -7 11 19 343.892 58.7648 4 -7 11 18 1834.21 113.644 4 -7 11 17-7.73822 43.1937 4 -7 11 16 8.18274 43.6723 4 -7 11 15 664.263 71.3378 4 -7 11 14 2138.07 123.812 4 -7 11 13 1633.66 105.858 4 -7 11 12 1013.80 83.2028 4 -7 11 11 1648.59 107.787 4 -7 11 10 25104.2 493.053 4 -7 11 9 1392.25 96.3881 4 7 11 -6 21537.1 547.166 6 7 11 -5 12008.3 383.302 6 7 11 -4 993.165 111.113 6 7 11 -3 55.8436 56.8246 6 7 11 -2 43333.5 842.767 6 7 11 -1 6214.80 257.624 6 7 11 0 176.442 70.6190 6 7 11 1 253.095 68.3343 6 7 11 2 4799.11 221.625 6 7 11 3 13766.6 391.918 6 7 11 4 635.039 88.9250 6 7 11 5 2217.99 150.631 6 7 11 6 1378.45 118.721 6 7 11 6 1385.75 100.526 5 7 11 7 168.464 47.1258 5 7 11 7 320.597 78.7594 6 7 11 8 52.8994 40.2839 5 7 11 8 19.0358 49.6562 6 7 11 9 19061.1 453.359 6 7 11 9 19291.8 411.394 5 7 11 10 5687.28 194.171 5 7 11 10 5351.84 214.777 6 7 11 11 2793.31 129.014 5 7 11 11 2925.44 151.629 6 7 11 12 15216.5 363.536 6 7 11 12 14499.6 325.104 5 7 11 13 4039.62 165.611 6 7 11 13 4204.44 153.438 5 7 11 14 15279.1 343.211 6 7 11 14 15207.5 319.272 5 7 11 15 3283.49 133.879 6 7 11 15 2938.17 116.561 5 -7 12 24 399.232 47.3192 4 -7 12 23 3009.43 116.198 4 -7 12 22 1692.06 94.1791 4 -7 12 22 1697.71 85.4263 7 -7 12 21 180.533 44.3577 4 -7 12 21 138.598 38.8838 7 -7 12 20 2115.39 110.518 4 -7 12 20 2046.13 100.033 7 -7 12 19 793.809 73.6641 4 -7 12 18 2611.12 126.553 4 -7 12 17 2352.20 123.009 4 -7 12 16 995.181 85.1485 4 -7 12 15 6735.15 214.944 4 -7 -12 15 6883.23 238.258 10 -7 12 14 7457.15 228.579 4 -7 -12 14 7570.81 260.627 10 -7 12 13 476.007 64.3167 4 -7 12 12 497.669 63.5794 4 7 12 -12 503.327 82.4162 6 -7 12 11 6396.74 208.949 4 7 12 -11 6348.60 257.817 6 -7 12 10 3639.45 152.716 4 7 12 -10 3765.16 199.592 6 -7 12 9 1714.94 104.983 4 7 12 -9 1647.63 137.081 6 7 12 -8 145.181 66.4571 6 7 12 -7 7582.02 295.245 6 7 12 -6 1771.59 141.483 6 7 12 -5 384.027 87.1778 6 7 12 -4 5483.13 243.369 6 7 12 -3 2.86809 55.0446 6 7 12 -2 158.867 61.8991 6 7 12 -1 1807.91 135.413 6 7 12 0 37.7197 53.4856 6 7 12 1 3574.35 188.683 6 7 12 2 3816.05 193.085 6 7 12 3 6455.55 253.733 6 7 12 4 190.015 56.7878 6 7 12 5 16048.6 416.336 6 7 12 6 165.299 61.9460 6 7 12 7 2180.02 140.261 6 7 12 8 13.4393 47.7881 6 7 12 9 1260.09 104.512 6 7 12 10 3330.92 161.290 6 7 12 11 1256.13 97.7359 6 7 12 12 2450.93 129.976 6 7 12 13 1545.89 98.8484 6 7 12 14 72.9286 36.8677 6 7 12 15 402.852 53.5259 6 -7 13 23 1409.40 75.3971 4 -7 13 22 1011.55 67.6107 4 -7 13 21 1783.13 92.2799 4 -7 13 20 804.334 67.9128 4 -7 13 19 94.6797 40.6908 4 -7 13 18 2269.51 113.483 4 -7 13 17 132.561 44.5979 4 -7 13 16 4552.60 166.572 4 -7 13 15 537.344 63.6540 4 -7 -13 15 599.591 73.6495 10 -7 -13 14 842.848 88.4483 10 -7 13 13 2177.16 113.901 4 -7 -13 13 2173.37 138.590 10 -7 13 12 4317.34 163.659 4 -7 13 11 534.749 65.5590 4 7 13 -11 440.932 69.8545 6 -7 13 10 1586.26 97.1528 4 7 13 -10 1814.10 129.019 6 -7 13 9 1985.33 107.121 4 7 13 -9 2011.91 139.655 6 7 13 -8 5145.29 225.028 6 7 13 -7 647.660 88.3689 6 7 13 -6 514.044 80.1655 6 7 13 -5 1464.94 128.981 6 7 13 -4 250.771 70.6813 6 7 13 -3 3239.62 180.332 6 7 13 -2 1617.43 130.712 6 7 13 -1 6130.60 246.192 6 7 13 0 272.188 74.4392 6 7 13 1 369.470 74.9873 6 7 13 2 3571.85 182.612 6 7 13 3 681.235 85.8698 6 7 13 4 380.794 70.8807 6 7 13 5 1118.59 102.295 6 7 13 6 706.717 85.2757 6 7 13 7 438.804 69.8338 6 7 13 8 0.83051 45.7643 6 7 13 9 177.529 60.0345 6 7 13 10 9107.46 266.287 6 7 13 11 8195.01 243.272 6 7 13 12 939.627 79.0925 6 7 13 13 2696.81 122.589 6 7 13 14 3480.79 133.774 6 7 13 15 2774.66 111.907 6 -7 14 22 12963.6 250.333 4 -7 14 21 513.603 47.3512 4 -7 14 20 485.111 48.7746 4 -7 14 19 2156.45 100.127 4 -7 14 18 1956.17 97.1417 4 -7 14 17 3993.68 144.879 4 -7 14 16 120.542 38.5979 4 -7 14 15 251.037 46.9813 4 -7 14 14 2148.88 108.586 4 -7 -14 14 2128.99 127.946 10 -7 14 13 209.193 44.8957 4 -7 -14 13 76.1909 45.0304 10 -7 14 12 264.385 48.8310 4 -7 -14 12 269.750 63.2919 10 -7 14 11 954.467 72.3963 4 -7 -14 11 917.127 100.519 10 -7 14 10 20727.0 403.552 4 -7 -14 10 20289.6 486.372 10 7 14 -9 4235.00 187.107 6 7 14 -8 1336.23 108.143 6 7 14 -7 13.1967 45.5716 6 7 14 -6 70.5140 49.6427 6 7 14 -5 1102.39 105.613 6 7 14 -4 2392.40 147.878 6 7 14 -3 4517.21 203.982 6 7 14 -2 24.7677 45.8132 6 7 14 -1 5738.20 228.017 6 7 14 0 332.182 65.1002 6 7 14 1 1429.88 112.823 6 7 14 2-2.10791 45.4374 6 7 14 3-6.08369 49.4158 6 7 14 4 2321.84 136.693 6 7 14 5 4074.87 179.896 6 7 14 6 2005.23 124.593 6 7 14 7 4771.39 188.666 6 7 14 8 284.347 58.0441 6 7 14 9 2539.44 130.102 6 7 14 10 4364.61 168.957 6 7 14 11 710.021 68.3794 6 7 14 12 219.987 44.3985 6 7 14 13 13856.2 299.458 6 7 14 14 2007.47 94.1201 6 -7 15 20 1903.99 79.8999 4 -7 15 19 214.414 37.5726 4 -7 15 18 277.217 39.5423 4 -7 15 17 737.796 58.9653 4 -7 15 16 974.143 68.4642 4 -7 15 15 31.9096 30.6590 4 -7 15 14 11531.3 260.608 4 -7 -15 14 11847.4 300.817 10 -7 15 13-20.1543 34.4471 4 -7 -15 13 54.4624 48.1302 10 -7 15 12 3970.77 140.365 4 -7 -15 12 4088.92 178.416 10 -7 15 11 236.945 45.5143 4 -7 -15 11 200.772 60.6637 10 -7 -15 10 524.490 80.2995 10 -7 -15 9-7.80283 51.7315 10 -7 -15 8-47.0568 60.1403 10 -7 -15 7 286.231 74.5997 10 7 15 -7 199.854 53.1461 6 -7 -15 6 1297.48 117.570 10 7 15 -6 1306.76 102.492 6 7 15 -5 1263.27 105.453 6 7 15 -4 1579.51 113.325 6 7 15 -3 1497.61 111.110 6 7 15 -2 468.652 65.1347 6 7 15 -1 4209.16 183.773 6 7 15 0 2642.40 146.120 6 7 15 1 5913.34 217.899 6 -7 -15 -2 8169.70 266.036 10 7 15 2 9070.53 272.791 6 -7 -15 -3 2537.51 139.088 10 7 15 3 2638.14 139.130 6 -7 -15 -4 7076.60 228.643 10 7 15 4 7723.60 240.667 6 -7 -15 -5 222.913 52.8963 10 7 15 5 335.583 61.2575 6 7 15 6 3046.30 142.615 6 7 15 7 638.735 72.4695 6 7 15 8 671.215 69.7952 6 7 15 9 134.536 41.5906 6 7 15 10 4134.94 150.148 6 7 15 11 1415.80 83.1705 6 7 15 12 67.4253 33.1596 6 7 15 13 1360.88 76.1722 6 -7 16 17 1593.14 71.8829 4 -7 16 16 2604.78 95.2061 4 -7 16 15 2443.49 96.1989 4 -7 16 14 1991.28 87.5866 4 -7 16 13 9661.53 216.033 4 -7 -16 13 10112.8 262.972 10 -7 16 12 2372.99 97.0948 4 -7 -16 12 2527.58 130.567 10 -7 -16 11 3057.38 147.406 10 -7 -16 10 933.050 91.5647 10 -7 -16 9 1.25691 53.1218 10 -7 -16 8 199.156 55.5195 10 -7 -16 7 5337.97 214.125 10 -7 -16 6 1697.52 122.739 10 7 16 -6 1811.61 106.465 6 -7 -16 5 3713.62 181.178 10 7 16 -5 3716.55 157.616 6 -7 -16 4 132.445 59.5346 10 7 16 -4 185.219 52.2400 6 -7 -16 3 4267.00 194.946 10 7 16 -3 4418.04 175.619 6 -7 -16 2 521.994 75.8561 10 7 16 -2 522.969 65.4220 6 -7 -16 1 32.0893 48.2289 10 7 16 -1 23.3450 39.3016 6 -7 -16 0 197.534 56.8599 10 7 16 0 179.859 46.3278 6 -7 -16 -1 419.185 64.3106 10 7 16 1 402.351 59.5061 6 -7 -16 -2 119.286 46.3321 10 7 16 2 266.020 55.2351 6 -7 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271.872 44.2234 6 7 17 7 143.511 36.6373 6 7 17 8 564.639 50.1701 6 -7 -18 11 2524.72 106.290 10 -7 -18 10 30.0639 32.9563 10 -7 -18 9 1316.21 85.5235 10 -7 -18 8 14470.6 322.206 10 -7 -18 7 1042.76 80.0831 10 -7 -18 6 3460.48 144.533 10 -7 -18 5 1204.65 88.6031 10 -7 -18 4 3807.98 154.110 10 -7 -18 3 180.309 46.2199 10 -7 -18 2 270.952 49.6806 10 -7 -18 1 101.501 38.6721 10 -7 -18 0 3490.74 137.429 10 7 18 1 1160.05 77.7781 4 -7 -18 -1 915.308 69.6752 10 7 18 1 1028.16 66.9604 6 7 18 2 2676.34 103.754 6 -8 0 27-3.57635 39.9608 9 -8 0 27 67.3362 37.1995 7 -8 0 26 181.542 59.0001 9 -8 0 26 119.004 39.0854 7 -8 0 25-26.3265 48.9879 9 -8 0 25-76.7833 46.5584 7 -8 0 24 3293.19 161.769 9 -8 0 23 22.6476 60.6036 9 -8 0 22 11280.7 330.255 9 -8 0 21 80.0801 70.9597 9 -8 0 20 17508.5 444.415 9 -8 0 19-3.96463 63.7660 9 -8 0 18 63911.4 1086.82 9 -8 0 17-26.7814 58.1658 9 -8 0 16 1213.64 116.126 4 -8 0 16 1294.45 114.639 9 -8 0 15 73.5345 61.4640 4 -8 0 14 19433.2 469.892 4 -8 0 13-0.49184 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525.072 1 -8 -4 5 9248.74 661.997 3 -8 4 5 9797.18 643.049 1 -8 -4 4 4401.10 459.675 3 -8 4 4 3991.97 423.151 1 8 4 -4 4448.50 227.442 5 -8 -4 3 6710.07 577.626 3 -8 4 3 7074.28 568.522 1 8 4 -3 7252.85 297.083 5 -8 -4 2 6663.77 583.249 3 -8 4 2 6717.88 566.568 1 8 4 -2 6901.11 286.040 5 -8 -4 1 22600.1 1095.74 3 -8 4 1 22478.5 1079.08 1 8 4 -1 23996.2 579.726 5 -8 -4 0 4382.31 479.259 3 -8 4 0 4006.75 459.013 1 8 4 0 3901.61 210.731 5 -8 -4 -1 11587.9 807.950 3 8 4 1 11674.6 365.693 5 -8 -4 -2 4658.89 510.831 3 -8 4 -2 3730.11 446.790 3 8 4 2 4594.92 219.088 5 -8 -4 -3 28293.6 1281.79 3 -8 4 -3 23357.8 1173.23 3 8 4 3 27073.3 594.961 5 8 4 3 24190.5 577.678 6 8 4 4 14184.7 401.257 5 8 4 4 14275.0 400.566 6 8 4 5 2212.07 149.290 5 8 4 5 2254.91 148.151 6 8 4 6 6367.44 255.967 5 8 4 6 6761.79 249.770 6 8 4 7 25581.4 573.328 5 8 4 8 365.738 79.8943 5 8 4 9 5814.09 235.630 5 8 4 10 13284.5 374.449 5 8 4 11 987.694 100.534 5 8 4 12 7088.76 254.455 5 8 4 13 18803.2 445.066 5 8 4 14 6238.63 226.493 5 8 4 15 2048.01 127.197 5 8 4 16 2995.35 145.639 5 8 4 17 1204.70 92.1392 5 8 4 18 593.049 65.0806 5 8 4 19 559.046 60.9833 5 8 4 20 271.593 42.8512 5 8 4 21 1083.60 66.4624 5 -8 -5 27 383.599 55.1088 9 -8 -5 26 1425.55 95.8843 9 -8 5 25 69.2953 48.2726 4 -8 -5 25-0.21452 48.2321 9 -8 5 25 119.906 51.3159 9 -8 5 24 1273.41 98.5061 4 -8 -5 24 1286.64 104.987 9 -8 5 24 1362.37 97.3303 9 -8 5 23 198.089 59.7911 4 -8 -5 23 179.999 65.6713 9 -8 5 23 225.579 66.2655 9 -8 5 22 12027.0 320.317 4 -8 -5 22 12253.1 346.731 9 -8 5 22 12341.1 328.750 9 -8 -5 21 12583.1 358.003 9 -8 5 21 12555.4 340.513 9 -8 5 20 33918.4 647.294 4 -8 -5 20 34110.8 689.374 9 -8 5 19 3190.60 164.288 4 -8 -5 19 3218.09 180.925 9 -8 5 18 10.0626 52.4115 4 -8 -5 18-24.8422 60.2307 9 -8 5 17 357.250 70.2466 4 -8 -5 17 223.790 70.5493 9 -8 5 16 1338.16 108.920 4 -8 -5 16 1420.09 123.522 9 -8 -5 15 2765.02 168.291 9 -8 5 14 9374.60 286.659 4 -8 -5 14 9374.44 315.888 9 -8 5 13 8489.00 263.916 4 -8 -5 13 8012.49 289.190 9 -8 5 12 1735.14 115.916 4 -8 -5 12 1765.29 132.420 9 -8 5 11 5223.09 198.570 4 -8 -5 11 5212.63 225.954 9 -8 5 10 5085.96 192.455 4 -8 -5 10 5098.75 221.274 9 -8 5 9 4653.00 183.208 4 -8 -5 9 4326.98 202.919 9 -8 -5 9 4463.28 441.015 3 -8 5 9 5259.53 454.600 1 -8 5 8 122.688 81.9533 1 -8 -5 8 243.850 105.554 3 -8 5 8 250.758 51.0177 4 -8 5 7 111.677 117.583 1 -8 -5 7 233.083 151.293 3 -8 -5 6 1806.14 293.916 3 -8 5 6 1716.50 265.120 1 -8 -5 5 698.226 209.879 3 -8 5 5 628.228 168.138 1 8 5 -5 345.206 84.4747 5 -8 -5 4 1511.96 286.928 3 -8 5 4 1304.14 254.853 1 8 5 -4 1309.07 135.552 5 -8 -5 3 5247.89 507.705 3 -8 5 3 5466.46 494.449 1 8 5 -3 5499.93 261.382 5 -8 -5 2 5850.35 541.344 3 -8 5 2 5613.87 498.213 1 8 5 -2 6234.63 276.756 5 -8 -5 1 1.83929 112.203 3 -8 5 1 349.485 168.284 1 8 5 -1 195.254 67.7313 5 -8 -5 0 626.707 184.958 3 -8 5 0 784.355 188.929 1 8 5 0 648.635 92.9671 5 -8 -5 -1 5408.85 549.617 3 8 5 1 5364.10 241.579 5 -8 -5 -2 363.789 174.590 3 8 5 2 384.976 83.2596 5 8 5 3 3170.39 184.384 5 8 5 3 3076.07 185.389 6 8 5 4 8247.03 299.947 5 8 5 4 8700.48 305.555 6 8 5 5 30786.2 661.387 5 8 5 5 31443.6 655.517 6 8 5 6 81029.6 1330.83 5 8 5 6 81767.2 1311.07 6 8 5 7 196.743 65.6292 5 8 5 7 216.486 55.5629 6 8 5 8 92.5083 52.4825 5 8 5 8 83.0743 51.4091 6 8 5 9 48495.9 883.537 5 8 5 10 3077.31 167.631 5 8 5 11 264.130 62.2904 5 8 5 12 13010.3 359.727 5 8 5 13 169.119 62.6257 5 8 5 14 573.330 77.2115 5 8 5 15 1295.24 104.200 5 8 5 16 73.7432 43.9133 5 8 5 17 2492.79 124.627 5 8 5 18 450.100 57.9706 5 8 5 19 68.0608 37.9374 5 8 5 20 87.6231 32.7326 5 8 5 21 61.2537 25.3636 5 -8 6 25 1432.48 94.5596 4 -8 -6 25 1440.11 101.710 9 -8 6 24 423.963 66.8471 4 -8 -6 24 491.858 74.4971 9 -8 6 24 420.098 60.3223 9 -8 6 23 1297.58 98.5211 4 -8 -6 23 1341.99 106.431 9 -8 6 23 1408.74 102.168 9 -8 6 22 782.423 90.1404 4 -8 6 22 1028.14 96.5690 9 -8 -6 22 750.602 94.1289 9 -8 6 21 8162.63 255.323 4 -8 -6 21 8428.19 280.994 9 -8 6 20 6583.37 241.979 4 -8 -6 20 7343.12 266.117 9 -8 6 19 672.994 88.8182 4 -8 -6 19 749.966 97.7034 9 -8 6 18 460.425 75.4903 4 -8 -6 18 503.051 86.2883 9 -8 6 17 539.010 81.5047 4 -8 -6 17 618.686 97.9145 9 -8 6 16 5151.06 206.770 4 -8 -6 16 4918.55 227.396 9 -8 6 15 990.767 91.9894 4 -8 -6 15 707.956 95.6960 9 -8 6 14 3772.20 174.832 4 -8 -6 14 4094.65 202.916 9 -8 6 13 474.024 74.4558 4 -8 -6 13 463.547 81.9251 9 -8 6 12 1236.07 97.8491 4 -8 -6 12 1146.23 115.012 9 -8 6 11 11044.4 300.169 4 -8 -6 11 11066.2 340.739 9 -8 6 10 15517.8 365.427 4 -8 -6 10 15154.6 409.615 9 -8 6 9 1001.53 86.0718 4 -8 -6 9 818.688 96.4916 9 -8 -6 8 56902.4 1725.31 3 -8 -6 7 4301.81 446.167 3 -8 6 7 4322.38 407.838 1 -8 -6 6 16568.9 896.614 3 -8 6 6 15880.3 794.301 1 8 6 -6 14013.7 435.720 5 -8 -6 5 19380.5 983.953 3 -8 6 5 18207.7 861.450 1 8 6 -5 17159.8 492.537 5 -8 -6 4 8206.83 644.374 3 -8 6 4 8823.05 605.006 1 8 6 -4 8102.91 327.693 5 -8 -6 3 1649.97 293.872 3 -8 6 3 1027.45 225.602 1 8 6 -3 1791.48 150.403 5 -8 -6 2 8465.22 670.922 3 -8 6 2 8736.01 624.323 1 8 6 -2 8609.91 329.691 5 -8 -6 1 1394.58 285.858 3 -8 6 1 1622.63 280.410 1 8 6 -1 1894.37 153.840 5 8 6 0 75.2291 64.8268 5 8 6 1 12748.2 395.086 5 8 6 2 611.673 91.1815 5 8 6 2 621.825 93.9917 6 8 6 3 6187.05 259.420 5 8 6 3 5979.88 257.432 6 8 6 4 4083.43 208.811 5 8 6 4 4272.95 210.696 6 8 6 5 249.266 72.6627 5 8 6 5 220.613 66.6106 6 8 6 6 3264.10 181.251 5 8 6 6 3236.94 176.542 6 8 6 7 393.570 72.0065 5 8 6 7 359.953 65.9268 6 8 6 8 3965.41 192.659 5 8 6 8 3691.76 180.109 6 8 6 9 46.3240 52.0576 5 8 6 9 105.260 60.0402 6 8 6 10 27888.7 557.265 6 8 6 10 26961.7 581.119 5 8 6 11 406.124 77.0408 5 8 6 12 17402.3 422.102 5 8 6 13 1274.81 104.635 5 8 6 14 10288.9 292.184 5 8 6 15 2617.56 136.929 5 8 6 16 620.579 69.8941 5 8 6 17 15296.2 341.666 5 8 6 18 19069.2 382.149 5 8 6 19 5303.31 163.480 5 8 6 20 44.4180 28.0373 5 -8 7 25-2.45258 38.6835 4 -8 7 24 1124.76 90.2220 4 -8 -7 24 1131.34 95.4710 9 -8 7 24 1270.89 88.9415 9 -8 7 23 6159.70 202.679 4 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15972.6 447.491 5 8 7 1 16221.8 466.142 6 8 7 2 8813.34 317.019 5 8 7 2 8552.70 323.216 6 8 7 3 5813.75 254.196 5 8 7 3 6143.28 265.265 6 8 7 4 80.4644 58.9398 5 8 7 4 44.7358 52.0955 6 8 7 5 7451.72 277.750 5 8 7 5 7322.50 280.173 6 8 7 6 14217.0 398.874 5 8 7 6 14762.3 407.553 6 8 7 7 1685.79 131.201 5 8 7 7 1834.87 132.673 6 8 7 8 9560.17 311.979 5 8 7 8 10241.5 314.624 6 8 7 9 6705.40 248.896 5 8 7 9 6629.81 239.805 6 8 7 10 7729.68 264.807 5 8 7 10 8018.35 258.408 6 8 7 11 6119.22 230.466 5 8 7 11 6430.30 220.840 6 8 7 12 903.062 93.5365 5 8 7 13 5010.95 199.280 5 8 7 14 1622.38 109.298 5 8 7 15 2256.97 122.715 5 8 7 16 13.3521 36.0412 5 8 7 17 1017.20 78.4055 5 8 7 18 146.822 36.3212 5 8 7 19 763.421 58.7934 5 -8 8 26 3063.03 116.113 4 -8 8 25 7817.08 208.488 4 -8 8 24 3074.15 129.423 4 -8 8 23 4692.74 169.406 4 -8 8 23 5059.99 172.173 9 -8 8 22 90.3646 48.7558 4 -8 -8 22 22.3786 52.8374 9 -8 8 22 106.849 44.2281 9 -8 8 21 4185.70 166.268 4 -8 -8 21 4197.59 185.019 9 -8 8 20 293.216 60.4006 4 -8 -8 20 357.455 73.7456 9 -8 8 19 506.177 69.0126 4 -8 -8 19 628.740 86.4647 9 -8 8 18 1091.93 93.5412 4 -8 -8 18 1043.90 110.667 9 -8 8 17 3120.68 153.848 4 -8 -8 17 2939.02 167.803 9 -8 8 16 19766.2 439.554 4 -8 -8 16 19727.7 483.756 9 -8 8 15 15754.1 375.439 4 -8 -8 15 14999.1 412.640 9 -8 8 14 1062.98 92.4563 4 -8 -8 14 1070.04 109.310 9 -8 8 13 270.259 58.4094 4 -8 -8 13 368.912 75.8839 9 -8 8 12 2434.77 130.928 4 -8 -8 12 2537.19 157.976 9 -8 8 11 12231.6 316.551 4 -8 -8 11 13784.5 381.071 9 -8 8 10 1235.09 91.8165 4 -8 -8 10 1160.91 111.548 9 -8 8 9 11211.8 288.896 4 8 8 -8 0.12204 51.2622 5 8 8 -7 114.358 58.3616 5 8 8 -6 846.799 105.317 5 8 8 -5 39326.5 837.186 5 8 8 -4 39.5267 61.9992 5 8 8 -3 1736.36 152.522 5 8 8 -2 3302.07 200.565 5 8 8 -1 17936.3 489.977 5 8 8 -1 18598.9 518.377 6 8 8 0 18.6657 55.4810 5 8 8 0 124.072 73.4362 6 8 8 1 12069.8 377.545 5 8 8 1 12417.0 398.758 6 8 8 2 602.296 84.5355 5 8 8 2 623.092 96.6386 6 8 8 3 3894.99 198.769 5 8 8 3 3647.91 203.513 6 8 8 4 619.533 88.7212 5 8 8 4 625.497 89.7632 6 8 8 5 550.000 81.6274 5 8 8 5 583.158 90.9585 6 8 8 6 12196.7 355.329 5 8 8 6 12908.9 376.840 6 8 8 7 8355.81 283.402 5 8 8 7 8654.89 294.172 6 8 8 8 12597.2 354.596 5 8 8 8 12887.9 362.019 6 8 8 9 478.182 72.0555 5 8 8 9 541.420 79.2834 6 8 8 10 10221.6 304.549 5 8 8 10 10724.1 305.210 6 8 8 11 1250.95 97.9013 6 8 8 11 1207.77 102.552 5 8 8 12 3134.34 153.990 5 8 8 13 5535.36 200.135 5 8 8 14 372.771 58.0780 5 8 8 15 3133.52 137.897 5 8 8 16 3251.05 132.764 5 8 8 17 7493.97 203.928 5 8 8 18 296.120 41.1594 5 -8 9 25 128.418 37.8399 4 -8 9 24 628.730 60.6545 4 -8 9 23 1224.70 87.5918 4 -8 9 22 82.7140 45.2165 4 -8 9 22 156.055 47.5368 9 -8 9 21 3449.56 150.575 4 -8 9 20 355.455 59.4337 4 -8 9 19 4402.33 174.412 4 -8 -9 19 4527.03 199.306 9 -8 9 18 245.368 57.7167 4 -8 -9 18 340.855 72.7661 9 -8 9 17 87.3198 44.0529 4 -8 -9 17 77.0146 58.6236 9 -8 9 16 192.427 57.3722 4 -8 -9 16 126.599 57.2295 9 -8 9 15 15508.5 365.218 4 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8 9 8 1415.57 111.765 5 8 9 9-10.1604 40.3951 5 8 9 9 15.5794 44.2120 6 8 9 10 2002.43 124.704 6 8 9 10 2063.92 123.172 5 8 9 11 12998.8 331.477 5 8 9 11 13526.9 339.356 6 8 9 12 8137.95 247.176 5 8 9 12 8812.28 250.400 6 8 9 13 20.6566 36.0600 5 8 9 14 3151.49 135.269 5 8 9 15 10306.8 255.850 5 8 9 16 1495.51 87.0246 5 8 9 17 2372.96 100.629 5 -8 10 25 40.1127 29.5671 4 -8 10 24 2026.11 95.2330 4 -8 10 23 2163.79 104.824 4 -8 10 22 439.489 57.5102 4 -8 10 21 1947.99 110.720 4 -8 10 19 2216.87 116.814 4 -8 10 18 4473.66 169.078 4 -8 10 17 178.800 48.4060 4 -8 10 16 1988.34 113.930 4 -8 10 15 1118.57 92.3814 4 8 10 -14 492.791 74.0806 5 -8 10 14 558.479 67.7465 4 8 10 -13 45.9778 40.5118 5 -8 10 13 27.1242 41.5366 4 8 10 -12 2309.82 143.030 5 -8 10 12 2971.14 138.385 4 8 10 -11 449.918 82.4597 5 -8 10 11 441.382 63.8714 4 8 10 -10 8538.71 298.155 5 -8 10 10 10846.6 274.494 4 8 10 -9 6649.77 258.469 5 8 10 -8 16026.6 433.823 5 8 10 -7 8386.69 305.575 5 8 10 -6 57211.0 1039.57 5 8 10 -5 5756.62 257.513 5 8 10 -5 5978.09 286.256 6 8 10 -4 68.5670 56.3508 5 8 10 -4 165.920 74.7890 6 8 10 -3 3334.66 188.255 5 8 10 -3 3463.60 211.287 6 8 10 -2 18447.7 474.694 5 8 10 -2 18271.9 509.160 6 8 10 -1 6658.60 258.998 5 8 10 -1 6511.56 283.320 6 8 10 0 1438.38 119.762 5 8 10 0 1524.93 140.304 6 8 10 1 638.398 84.1234 5 8 10 1 609.032 92.3444 6 8 10 2 3358.90 174.010 5 8 10 2 3375.01 191.785 6 8 10 3 158.433 49.2117 5 8 10 3 202.501 71.4711 6 8 10 4 1533.49 114.269 5 8 10 4 1514.62 130.794 6 8 10 5 103.125 48.9297 5 8 10 5 102.971 55.3236 6 8 10 6 11905.0 328.293 5 8 10 6 12837.3 367.522 6 8 10 7 127.017 49.4286 5 8 10 7 112.568 60.7795 6 8 10 8 2196.02 126.840 5 8 10 8 2373.88 147.149 6 8 10 9 9176.30 282.543 6 8 10 9 8963.01 261.864 5 8 10 10 335.598 53.5740 5 8 10 10 372.985 66.0588 6 8 10 11 2538.57 125.058 5 8 10 11 2359.01 129.560 6 8 10 12 11922.0 299.763 6 8 10 12 11998.1 290.932 5 8 10 13 2345.75 112.353 5 8 10 14 238.612 39.4625 5 8 10 15 2127.95 98.7104 5 8 10 16 8018.86 195.050 5 -8 11 24 11.5842 30.2240 4 -8 11 23 10839.6 239.493 4 -8 11 22 2007.99 97.2696 4 -8 11 21 7.78378 36.2812 4 -8 11 20 8863.57 232.920 4 -8 11 19 12244.1 288.778 4 -8 11 18 34.2067 38.4276 4 -8 11 17 3275.47 141.154 4 -8 11 16 2333.30 120.313 4 -8 11 15 14896.6 339.022 4 -8 11 14 5323.60 185.061 4 -8 11 13-7.88083 41.4224 4 -8 11 12 1639.32 101.403 4 -8 11 11 679.420 69.5218 4 8 11 -9 1433.76 133.092 6 8 11 -8 2262.53 168.573 6 8 11 -7 797.236 113.310 6 8 11 -6 169.073 77.4283 6 8 11 -5 4968.61 250.501 6 8 11 -4 28.7267 60.3910 6 8 11 -3 6638.02 283.190 6 8 11 -2 236.738 78.2418 6 8 11 -1 12033.5 342.361 5 8 11 -1 12271.8 392.173 6 8 11 0 159.771 48.1434 5 8 11 0 157.960 66.8474 6 8 11 1 40.4069 39.9491 5 8 11 1-2.10749 54.5250 6 8 11 2 1132.35 93.7385 5 8 11 2 1081.70 113.245 6 8 11 3 56.9187 35.0679 5 8 11 3 46.2789 56.7993 6 8 11 4 1285.22 118.740 6 8 11 4 1244.54 96.3902 5 8 11 5 443.650 60.6590 5 8 11 5 590.719 88.8626 6 8 11 6 1358.83 96.8762 5 8 11 6 1299.89 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56.8402 5 10 7 -4 62.5544 67.2172 6 10 7 -3 191.316 67.5344 5 10 7 -3 360.221 85.5657 6 10 7 -2 9080.38 322.900 5 10 7 -2 10028.2 355.920 6 10 7 -1 3271.44 192.314 5 10 7 -1 3621.24 207.981 6 10 7 0 5946.37 263.833 5 10 7 0 6820.65 285.760 6 10 7 1 45.2193 59.3406 5 10 7 1 111.034 71.6103 6 10 7 2 98.9289 68.1745 5 10 7 2 87.1065 65.3407 6 10 7 3 1337.02 130.075 5 10 7 3 1392.54 126.148 6 10 7 4 800.705 98.1821 5 10 7 4 756.861 95.8235 6 10 7 5 4286.33 210.530 5 10 7 5 4769.79 204.270 6 10 7 6 3306.03 178.275 5 10 7 7 97.3887 55.1690 5 10 7 8 1535.81 113.455 5 10 7 9 2431.88 137.192 5 10 7 10 139.140 49.0501 5 10 7 11 10604.0 278.218 5 10 7 12 932.084 76.6078 5 10 7 13 65.7344 32.0954 5 -10 8 22 28.5855 29.9185 9 10 8 -21 55.7003 27.5714 5 -10 8 21 82.2658 36.9116 9 10 8 -20 82.9745 35.5234 5 -10 8 20 29.1632 35.6089 9 10 8 -19 911.246 67.9620 5 -10 8 19 1108.57 79.2938 9 10 8 -18 7052.44 203.410 5 10 8 -17 22.1978 32.6714 5 10 8 -16 782.264 71.5862 5 10 8 -15 3720.31 156.234 5 10 8 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3424.46 170.942 5 10 9 4 3354.33 172.943 6 10 9 5 600.173 79.5975 5 10 9 5 675.417 83.6976 6 10 9 6 4866.17 194.987 5 10 9 6 5082.25 191.064 6 10 9 7 8006.51 247.238 5 10 9 8 75.5112 43.5773 5 10 9 9 10.3936 38.8938 5 10 9 10 86.9838 33.1223 5 -10 10 19 151.550 36.9815 9 10 10 -17 595.769 55.8402 6 10 10 -16 211.741 42.3710 6 10 10 -15 167.020 38.8475 5 10 10 -15 114.964 41.4666 6 10 10 -14 8531.48 246.699 6 10 10 -13 517.772 57.2303 5 10 10 -13 649.163 74.3365 6 10 10 -12 169.696 46.2171 5 10 10 -12 189.883 53.7391 6 10 10 -11 2326.17 119.961 5 10 10 -11 2383.17 138.982 6 10 10 -10 22551.2 459.255 5 10 10 -10 23312.2 506.173 6 10 10 -9 5420.56 192.957 5 10 10 -9 5654.02 221.597 6 10 10 -8 4179.38 171.311 5 10 10 -8 4581.11 204.181 6 10 10 -7 1018.80 87.7104 5 10 10 -7 1014.64 101.205 6 10 10 -6 320.900 60.2556 5 10 10 -6 265.183 69.0344 6 10 10 -5 467.166 67.7568 5 10 10 -5 458.909 75.8266 6 10 10 -4 8192.12 257.203 5 10 10 -4 8276.77 286.739 6 10 10 -3 61.6669 44.3386 5 10 10 -3 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128.048 6 10 11 -3 1563.62 98.7614 5 10 11 -3 1661.48 121.324 6 10 11 -2 530.055 61.0325 5 10 11 -2 643.295 79.9132 6 10 11 -1 6636.94 205.216 5 10 11 -1 7234.13 247.756 6 10 11 0 543.206 61.7586 5 10 11 0 674.600 80.5979 6 10 11 1 1673.35 119.379 6 10 11 1 1475.64 91.9807 5 10 11 2 5425.36 177.976 5 10 11 2 6294.73 221.499 6 10 11 3 1843.29 118.164 6 10 11 3 1500.56 89.7956 5 10 11 4 3673.53 156.444 6 10 11 4 3076.38 122.457 5 10 11 5 72.1695 36.8632 5 10 11 5 43.4582 40.5040 6 10 11 6 29.0664 36.3620 6 10 12 -13 365.103 44.6296 6 -10 -12 12 335.516 50.0854 10 10 12 -12 267.842 45.0901 6 10 12 -11 143.905 41.2254 6 10 12 -10 127.269 40.6790 6 10 12 -9 11308.6 286.674 6 10 12 -8 206.571 46.1452 6 10 12 -7 3639.78 156.833 6 10 12 -6 2323.86 125.784 6 10 12 -5 1492.73 102.855 6 10 12 -4 3479.44 159.101 6 10 12 -3 3534.10 158.825 6 10 12 -2 2411.61 131.769 6 10 12 -1 7160.02 230.415 6 10 12 0 1476.94 103.394 6 10 12 1 32.4693 40.5380 6 10 12 2 463.443 63.7205 6 10 12 3 2157.88 111.523 6 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595.216 71.6218 5 11 -1 5 608.040 66.6898 5 11 1 5 530.108 66.7014 5 11 1 6 128.394 44.9727 5 11 1 7 344.270 53.0419 5 11 1 8 2816.35 120.887 5 11 1 9 2950.61 119.828 5 11 1 11 323.670 38.7825 5 11 2 -22 17.7565 26.5283 5 -11 -2 22 14.1139 29.4924 9 -11 2 22 37.8330 30.3973 9 11 2 -21 10383.1 242.685 5 -11 -2 21 9780.64 230.785 9 -11 2 21 9841.06 234.294 9 11 2 -20 2737.71 122.616 5 -11 -2 20 2611.90 114.950 9 -11 2 20 2673.89 117.115 9 11 2 -19 1314.81 90.5952 5 -11 -2 19 1366.30 87.3441 9 -11 2 19 1449.84 90.9046 9 11 2 -18 1285.79 92.9695 5 -11 -2 18 1198.52 82.9311 9 -11 2 18 1395.06 92.8500 9 11 -2 -17 758.809 70.2359 5 11 2 -17 754.578 77.1403 5 -11 2 17 819.902 80.5480 9 -11 -2 17 813.212 73.0659 9 11 -2 -16 3194.11 136.964 5 11 2 -16 3214.06 153.595 5 -11 -2 16 2997.18 136.695 9 -11 2 16 3179.23 144.120 9 11 -2 -15 1489.08 100.447 5 11 2 -15 1471.84 106.406 5 -11 -2 15 1467.85 97.9668 9 -11 2 15 1529.47 101.642 9 11 -2 -14 10665.7 287.014 5 11 2 -14 10927.5 303.882 5 -11 -2 14 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62.0232 5 11 4 3 487.958 72.2363 5 11 4 4 332.365 65.9253 5 11 4 5 1075.96 94.0909 5 11 4 6 11145.5 294.945 5 11 4 7 1032.11 85.2140 5 11 4 8 11691.2 282.209 5 11 4 9 7712.62 209.814 5 11 4 10 1198.99 75.4653 5 11 4 11 87.6194 31.5998 5 11 5 -21 94.2428 31.8625 5 -11 5 21 187.336 37.5822 9 -11 -5 20 1724.27 82.3188 9 -11 5 20 1934.05 92.7069 9 11 5 -19 157.545 40.3092 5 -11 -5 19 164.257 35.8565 9 -11 5 19 214.144 43.4712 9 11 5 -18 76.9325 38.8069 5 -11 -5 18-8.43632 30.8093 9 -11 5 18 77.3381 40.0337 9 11 5 -17 2700.06 128.098 5 -11 -5 17 2919.62 119.535 9 -11 5 17 3104.21 128.083 9 11 5 -16 0.50844 34.9913 5 -11 -5 16 43.4809 37.1802 9 -11 5 16 12.6026 38.8171 9 11 5 -15 501.574 63.7175 5 -11 5 15 644.747 68.3196 9 11 5 -14 130.041 47.3195 5 -11 5 14 111.978 42.8748 9 11 5 -13 777.393 80.6650 5 -11 5 13 866.124 77.9745 9 11 5 -12 21.3645 45.4005 5 11 5 -11 138.175 50.2867 5 11 5 -10 389.388 68.6617 5 11 5 -9 5064.56 204.172 5 11 5 -8 1273.78 108.783 5 11 5 -7 293.589 61.2800 5 11 5 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5323.05 202.041 5 11 6 -8 1425.42 109.689 5 11 6 -7 11066.0 311.183 5 11 6 -6 5815.88 219.506 5 11 6 -6 6014.67 231.709 6 11 6 -5 3131.91 161.208 5 11 6 -5 3134.30 166.382 6 11 6 -4 2110.25 132.564 5 11 6 -4 2222.82 142.544 6 11 6 -3 431.810 73.3226 5 11 6 -3 488.287 76.3414 6 11 6 -2 1268.20 106.840 5 11 6 -2 1279.81 108.490 6 11 6 -1 1574.13 117.949 5 11 6 -1 1720.96 120.540 6 11 6 0 45.6029 49.9875 5 11 6 0 84.2479 48.7853 6 11 6 1 688.215 81.2055 5 11 6 2 6783.18 232.122 5 11 6 3 8883.71 266.734 5 11 6 4 1534.14 107.093 5 11 6 5 1775.88 106.720 5 11 6 6 2248.50 119.829 5 11 6 7 478.182 59.1631 5 11 6 8 428.131 51.3310 5 11 6 9 5221.01 157.627 5 -11 7 19 113.302 33.6381 9 11 7 -18 621.379 55.3702 5 -11 7 18 807.994 62.6603 9 11 7 -17 399.044 47.4125 5 -11 7 17 431.067 49.9672 9 11 7 -16 53.6531 31.0590 5 -11 7 16 97.2685 36.2131 9 11 7 -15 1416.40 88.4276 5 -11 7 15 1612.18 92.0680 9 11 7 -14 632.060 64.2703 5 11 7 -13 963.360 79.3673 5 11 7 -12 476.928 59.0641 5 11 7 -11 4268.55 169.171 5 11 7 -10 315.543 57.9094 5 11 7 -9 166.605 45.1309 5 11 7 -8 4611.14 185.470 5 11 7 -8 5189.19 207.365 6 11 7 -7-14.7517 41.9081 5 11 7 -7 56.7857 45.8658 6 11 7 -6 380.321 64.2680 5 11 7 -6 329.994 66.2913 6 11 7 -5 14925.8 368.369 5 11 7 -5 15011.3 385.067 6 11 7 -4 2482.23 137.505 5 11 7 -4 2554.25 147.210 6 11 7 -3 574.780 74.4671 5 11 7 -3 387.284 67.1125 6 11 7 -2 63.6417 47.6854 5 11 7 -2 20.5126 49.6243 6 11 7 -1 1022.07 92.0719 5 11 7 -1 1025.67 95.8066 6 11 7 0 206.471 49.1308 5 11 7 0 288.753 59.0528 6 11 7 1 43.0208 42.2629 5 11 7 1 53.3885 42.2917 6 11 7 2 91.9345 47.6700 5 11 7 3 3650.95 158.767 5 11 7 4 5624.47 192.637 5 11 7 5 825.629 75.9147 5 11 7 6 1006.69 79.0039 5 11 7 7 3834.54 141.698 5 11 7 8 299.815 44.4679 5 -11 8 18 135.846 35.2421 9 11 8 -17 539.678 48.4819 5 -11 8 17 614.574 54.6121 9 11 8 -17 602.883 56.1630 6 11 8 -16 1057.55 66.5445 5 -11 8 16 1296.90 77.2949 9 11 8 -16 1111.94 75.8370 6 11 8 -15 1243.17 74.8572 5 -11 8 15 1541.57 86.6592 9 11 8 -15 1386.65 87.7705 6 11 8 -14 32.2299 31.6079 5 11 8 -14 0.68352 35.8198 6 11 8 -13 149.512 41.6946 5 11 8 -13 90.1236 44.8004 6 11 8 -12 2024.87 107.634 5 11 8 -12 2213.79 122.375 6 11 8 -11 605.800 65.5512 5 11 8 -11 695.222 75.5283 6 11 8 -10 824.679 78.1325 5 11 8 -10 834.036 84.7958 6 11 8 -9 1492.00 99.6894 5 11 8 -9 1736.62 116.135 6 11 8 -8 8932.76 254.968 5 11 8 -8 9666.52 283.181 6 11 8 -7 1606.41 105.591 5 11 8 -7 1668.93 123.343 6 11 8 -6 190.295 52.0035 5 11 8 -6 217.481 55.2977 6 11 8 -5 460.453 65.6652 5 11 8 -5 315.852 59.7779 6 11 8 -4 3.93416 36.5671 5 11 8 -4 12.9334 44.5204 6 11 8 -3 163.683 48.3698 5 11 8 -3 193.674 56.9077 6 11 8 -2-2.63765 38.6633 5 11 8 -2 0.23239 42.9914 6 11 8 -1 4847.29 179.910 5 11 8 -1 4985.59 188.282 6 11 8 0 3375.71 150.278 5 11 8 0 3505.99 154.696 6 11 8 1 593.221 66.8069 5 11 8 1 625.928 68.9769 6 11 8 2 533.090 63.6367 5 11 8 3 1877.05 103.988 5 11 8 4 506.363 56.2319 5 11 8 5 1132.00 78.0914 5 11 8 6 304.427 44.7194 5 11 8 7 5736.08 163.703 5 -11 9 16-4.67067 28.5304 9 11 9 -16 47.5699 24.0917 6 -11 9 15 913.504 64.2566 9 11 9 -15 919.678 67.6987 6 11 9 -14 623.621 55.5953 5 11 9 -14 719.282 63.1269 6 11 9 -13 2061.10 95.7786 5 11 9 -13 2060.08 107.077 6 11 9 -12 15403.5 316.456 5 11 9 -12 15915.2 346.135 6 11 9 -11 468.539 55.2013 5 11 9 -11 454.110 61.0309 6 11 9 -10 812.551 66.6376 5 11 9 -10 793.767 77.8196 6 11 9 -9 1391.80 87.0691 5 11 9 -9 1410.07 101.052 6 11 9 -8 48.7800 37.7156 5 11 9 -8 37.9428 42.6869 6 11 9 -7 790.317 68.9159 5 11 9 -7 699.673 77.4253 6 11 9 -6 111.331 44.5109 5 11 9 -6 143.368 51.1741 6 11 9 -5 113.400 39.8041 5 11 9 -5 71.7638 40.5025 6 11 9 -4 2629.81 122.895 5 11 9 -4 2804.01 137.348 6 11 9 -3 115.271 34.6541 5 11 9 -3 208.961 51.0510 6 11 9 -2 596.608 62.3071 5 11 9 -2 682.656 73.9963 6 11 9 -1 2616.12 121.081 5 11 9 -1 2775.19 132.482 6 11 9 0 1108.89 79.3062 5 11 9 0 1011.80 82.0800 6 11 9 1 494.964 54.6299 5 11 9 1 445.540 57.5638 6 11 9 2 46.8922 31.3269 5 11 9 2-43.5312 33.0443 6 11 9 3 39.3286 29.7010 5 11 9 4 552.510 50.2875 5 11 9 5 683.112 53.8080 5 11 10 -14 976.471 63.0952 6 11 10 -13 42.6910 32.0136 6 11 10 -12 439.743 51.3633 6 11 10 -11 666.425 62.5124 6 11 10 -10 27.8937 27.1615 5 11 10 -10 20.8186 33.5289 6 11 10 -9 683.043 56.0176 5 11 10 -9 622.190 64.6446 6 11 10 -8 6086.47 171.587 5 11 10 -8 6513.65 200.642 6 11 10 -7 885.657 65.7230 5 11 10 -7 830.597 76.2338 6 11 10 -6 10507.9 243.474 5 11 10 -6 11156.3 280.530 6 11 10 -5 3244.20 123.442 5 11 10 -5 3429.70 144.898 6 11 10 -4 561.281 55.4988 5 11 10 -4 563.749 65.7243 6 11 10 -3 367.718 47.1515 5 11 10 -3 331.573 54.8603 6 11 10 -2 1902.81 92.8121 5 11 10 -2 2111.28 111.718 6 11 10 -1 417.108 48.0662 5 11 10 -1 542.123 61.2703 6 11 10 0 4457.04 152.641 6 11 10 0 4063.82 133.759 5 11 10 1 4061.22 130.921 5 11 10 1 4553.64 150.187 6 11 10 2 544.676 52.5048 6 11 11 -11 1228.84 70.3569 6 11 11 -10 311.147 42.7911 6 11 11 -9 4987.56 155.700 6 11 11 -8 1752.18 92.5676 6 11 11 -7 8096.49 215.080 6 11 11 -6 1444.28 86.7271 6 11 11 -5 160.296 39.6772 6 11 11 -4 118.420 42.7222 6 11 11 -3 2653.64 114.291 6 11 11 -2 3079.73 121.891 6 11 11 -1 127.328 35.7191 6 11 11 0 1123.97 69.3231 6 11 12 -5 850.395 58.3460 6 12 0 -17 2.38267 26.6323 5 12 0 -16 852.825 63.6818 5 12 0 -15 529.827 66.3030 5 12 0 -14 5983.67 179.143 5 12 0 -13 95.8263 46.2206 5 12 0 -12 12382.5 293.107 5 12 0 -11 14.7797 64.0466 5 12 0 -10 1229.16 90.1110 5 12 0 -9 0.26334 39.6273 5 12 0 -8 10423.4 275.991 5 12 0 -7-2.55615 45.8756 5 12 0 -6 5616.97 190.876 5 12 0 -5-6.88745 40.3756 5 12 0 -4 125.076 47.6250 5 12 0 -3 23.8166 36.6654 5 12 0 -2 399.756 55.5110 5 12 0 -1 45.6839 37.0764 5 12 0 0 5560.57 175.412 5 12 0 1 84.9574 37.0932 5 12 1 -17 183.329 35.2342 5 12 1 -16 6551.11 181.728 5 12 1 -15 179.300 42.1072 5 12 1 -14 33.7597 35.4603 5 12 1 -13 279.059 49.6574 5 12 1 -12 7410.31 218.236 5 12 1 -11-16.2803 40.7411 5 12 1 -10 2621.87 130.705 5 12 -1 -9 5330.96 180.338 5 12 1 -9 5359.39 190.765 5 12 1 -8 6397.91 209.317 5 12 1 -7 186.987 49.5629 5 12 1 -6 4778.36 179.722 5 12 1 -5 2067.92 116.614 5 12 1 -4-8.22527 37.7530 5 12 1 -3-25.9442 44.6715 5 12 1 -2 6432.50 201.636 5 12 1 -1 5796.48 188.582 5 12 1 0 1004.17 76.7446 5 12 1 1 8028.69 216.373 5 12 1 2 1634.53 92.0233 5 12 1 3 4078.79 138.687 5 12 1 4 812.190 59.9577 5 12 2 -18 64.0325 26.2507 5 12 2 -17 62.9200 30.6149 5 12 2 -16 3852.31 135.125 5 -12 2 16 3687.93 120.131 9 12 2 -15 247.174 46.7640 5 -12 2 15 278.162 39.7312 9 12 2 -14 753.117 68.3427 5 -12 2 14 699.235 57.0732 9 12 2 -13 1926.17 104.393 5 12 2 -12 5876.67 190.180 5 12 2 -11 447.298 60.3236 5 12 2 -10 1244.26 91.5096 5 12 2 -9 46.8763 40.9170 5 12 2 -8 134.753 46.5120 5 12 2 -7 3549.87 152.465 5 12 2 -6 571.120 72.8787 5 12 2 -5 2691.55 133.488 5 12 2 -4 4196.34 170.146 5 12 2 -3 575.017 68.2685 5 12 2 -2 1392.59 94.8322 5 12 2 -1 174.023 47.1645 5 12 2 0 556.626 63.1806 5 12 2 1 6348.71 192.195 5 12 2 2 5886.60 178.117 5 12 2 3 172.107 36.4865 5 12 2 4 18.9249 27.0066 5 12 2 5 449.186 47.0238 5 12 3 -17 123.776 31.3177 5 12 3 -16 2610.61 107.367 5 12 3 -15 6371.15 182.727 5 -12 3 15 6241.16 163.616 9 12 3 -14 4220.23 151.123 5 -12 3 14 4325.42 132.182 9 12 3 -13 1814.26 102.091 5 12 3 -12 10796.6 268.018 5 12 3 -11 5995.02 198.884 5 12 3 -10 3080.55 140.171 5 12 3 -9 1254.50 91.9720 5 12 3 -8 150.388 47.5599 5 12 3 -7 3124.17 140.658 5 12 3 -7 2802.62 132.719 6 12 3 -6 240.640 53.7393 5 12 3 -5 873.977 80.1159 5 12 3 -4 3349.30 150.743 5 12 3 -3 121.152 46.9501 5 12 3 -2 648.443 66.9288 5 12 3 -1 1399.97 91.7173 5 12 3 0 1565.17 95.6923 5 12 3 1 582.012 61.8498 5 12 3 2 2143.82 106.085 5 12 3 3 12632.8 276.256 5 12 3 4 636.361 55.8909 5 12 3 5 1297.51 71.1910 5 12 4 -16 1311.19 75.3359 5 12 4 -15-16.8192 32.7303 5 12 4 -14 3814.04 138.224 5 -12 4 14 3907.00 123.170 9 12 4 -13 10.2932 30.8706 5 -12 4 13 26.4998 27.7067 9 12 4 -12 958.044 72.8334 5 12 4 -11 468.552 59.6272 5 12 4 -10 1436.47 95.8198 5 12 4 -9 21259.5 425.082 5 12 4 -8 40.9011 57.6520 5 12 4 -8-12.8088 39.8822 6 12 4 -7 181.799 48.3412 5 12 4 -7 243.454 50.7818 6 12 4 -6 5999.53 197.056 5 12 4 -6 5749.90 188.949 6 12 4 -5 4350.08 165.663 5 12 4 -4 1098.92 84.4996 5 12 4 -3 290.660 51.4415 5 12 4 -2 557.594 62.4905 5 12 4 -1 137.391 43.1477 5 12 4 0 569.363 60.8672 5 12 4 1 77.5903 36.3860 5 12 4 2 3238.30 126.359 5 12 4 3 67.0963 32.8781 5 12 4 4 3993.82 131.289 5 12 4 5 3174.05 109.933 5 12 5 -14 151.768 37.2936 5 12 5 -13 29.7539 30.2467 5 12 5 -12 40.1205 33.7341 5 12 5 -11 211.168 45.2154 5 12 5 -11 69.6496 42.4686 6 12 5 -10 9116.04 235.709 5 12 5 -10 8602.72 236.631 6 12 5 -9 1243.53 91.7769 5 12 5 -9 1139.18 84.2961 6 12 5 -8 2478.57 118.934 5 12 5 -8 2205.69 112.936 6 12 5 -7 7826.04 221.124 5 12 5 -7 7562.56 218.895 6 12 5 -6 3422.58 139.778 5 12 5 -6 3082.77 132.807 6 12 5 -5 230.413 51.6853 5 12 5 -5 92.1515 37.4496 6 12 5 -4 74.5587 44.0220 5 12 5 -3 79.4462 39.2077 5 12 5 -2 6970.25 202.853 5 12 5 -1 86.1952 36.5808 5 12 5 0 1235.38 80.3938 5 12 5 1-16.6057 30.2064 5 12 5 2 502.169 51.7915 5 12 5 3 8498.00 205.002 5 12 5 4 577.295 49.2749 5 12 6 -15 237.500 39.7078 6 12 6 -14 852.623 59.3612 5 12 6 -14 846.304 63.4053 6 12 6 -13 2624.03 106.131 5 12 6 -13 2744.87 114.861 6 12 6 -12 2046.19 96.3275 5 12 6 -12 2057.37 100.751 6 12 6 -11 1132.17 77.4316 5 12 6 -11 1141.22 79.5136 6 12 6 -10 17.4679 34.6898 5 12 6 -10-26.7116 35.3070 6 12 6 -9 2138.65 104.249 5 12 6 -9 1980.89 104.930 6 12 6 -8 72.1196 37.2196 5 12 6 -8 95.2607 38.1123 6 12 6 -7 1727.62 95.3174 5 12 6 -7 1626.98 94.9496 6 12 6 -6 9150.37 235.794 5 12 6 -6 8695.95 229.221 6 12 6 -5 8328.90 219.358 5 12 6 -5 7816.04 211.757 6 12 6 -4 3800.08 140.304 5 12 6 -4 3578.16 134.867 6 12 6 -3-31.4778 34.8333 5 12 6 -2 6860.28 192.225 5 12 6 -1 837.320 65.8504 5 12 6 0 540.524 54.0506 5 12 6 1 463.488 50.0381 5 12 6 2 5425.47 154.093 5 12 6 3 905.223 57.9736 5 12 7 -13 437.213 46.3924 6 12 7 -12 186.596 32.8036 5 12 7 -12 229.522 41.1395 6 12 7 -11 3258.62 115.262 5 12 7 -11 3027.60 118.752 6 12 7 -10 10140.1 229.732 5 12 7 -10 9962.89 238.301 6 12 7 -9 340.516 57.0602 5 12 7 -9 313.093 44.3650 6 12 7 -8 3923.46 135.926 5 12 7 -8 4064.78 142.514 6 12 7 -7 9.75648 29.1892 5 12 7 -7-29.8633 33.3920 6 12 7 -6 2424.88 104.721 5 12 7 -6 2392.52 107.205 6 12 7 -5 26.3595 33.1020 5 12 7 -5 53.6688 31.7008 6 12 7 -4 2313.51 101.031 5 12 7 -4 2145.40 97.7590 6 12 7 -3 428.372 47.4907 5 12 7 -2 102.254 30.5587 5 12 7 -1 2345.83 99.7496 5 12 7 0 3071.50 112.269 5 12 7 1 84.3783 28.4919 5 12 8 -11 5548.00 154.463 6 12 8 -10 108.107 32.2863 6 12 8 -9 23.0791 26.5442 6 12 8 -8 2338.25 90.8116 5 12 8 -8 2438.10 102.239 6 12 8 -7 195.210 35.8133 5 12 8 -7 187.517 36.3735 6 12 8 -6 3703.46 118.333 5 12 8 -6 3550.77 124.640 6 12 8 -5 1625.29 76.9107 5 12 8 -5 1433.99 77.4069 6 12 8 -4 2782.78 101.198 5 12 8 -4 2695.36 104.887 6 12 8 -3 1218.06 66.1053 5 0 0 0 0.00 0.00 0 TITL Rx_318_mP_abs_ana in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 10.571207 18.199210 27.289409 90.0000 100.7841 90.0000 ZERR 4.00 0.000135 0.000216 0.000296 0.0000 0.0011 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H Li N F Si P Cl UNIT 194.40 180.40 8.00 16.00 48.00 8.00 8.00 4.40 SIZE 0.08 0.33 0.63 TREF HKLF 4 END ; _shelx_hkl_checksum 33281 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.405 _oxdiff_exptl_absorpt_empirical_full_min 0.715 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group P1 P 0.58166(4) 0.26429(2) 0.51853(2) 0.02385(9) Uani 1 1 d . . . . . P2 P 0.74818(4) 0.16931(2) 0.36436(2) 0.02788(10) Uani 1 1 d . . . . . Si2 Si 0.39951(4) 0.49272(2) 0.35690(2) 0.02154(9) Uani 1 1 d . . . . . Si1 Si 0.98323(4) 0.09706(2) 0.62425(2) 0.02362(10) Uani 1 1 d . . . . . Cl2 Cl 0.24068(6) 0.29815(3) 0.19399(2) 0.03584(13) Uani 0.7 1 d . . P . . Cl1 Cl 0.42587(7) 0.20738(4) 0.26037(2) 0.04229(15) Uani 0.7 1 d . . P . . F1 F 0.66071(9) 0.18883(5) 0.51276(4) 0.0346(2) Uani 1 1 d . . . . . F3 F 0.50371(11) 0.33796(6) 0.52233(5) 0.0439(3) Uani 1 1 d . . . . . F6 F 0.45961(10) 0.21645(6) 0.52192(5) 0.0441(3) Uani 1 1 d . . . . . F2 F 0.53713(11) 0.26528(7) 0.45841(4) 0.0444(3) Uani 1 1 d . . . . . F5 F 0.70594(10) 0.30986(6) 0.51243(5) 0.0446(3) Uani 1 1 d . . . . . F4 F 0.62922(13) 0.26098(7) 0.57673(4) 0.0488(3) Uani 1 1 d . . . . . F7 F 0.64796(11) 0.23694(7) 0.36384(5) 0.0498(3) Uani 1 1 d . . . . . F8 F 0.79539(13) 0.18339(8) 0.42370(4) 0.0541(3) Uani 1 1 d . . . . . F12 F 0.85211(12) 0.22782(7) 0.35493(5) 0.0523(3) Uani 1 1 d . . . . . F10 F 0.69889(13) 0.15882(8) 0.30695(4) 0.0582(4) Uani 1 1 d . . . . . N2 N 0.81380(13) 0.05347(7) 0.50898(5) 0.0253(3) Uani 1 1 d . . . . . N1 N 0.97972(12) 0.22279(7) 0.52167(5) 0.0248(3) Uani 1 1 d . . . . . N3 N 0.36790(13) 0.30046(7) 0.36373(5) 0.0291(3) Uani 1 1 d . . . . . N4 N 0.66610(13) 0.39759(7) 0.40973(5) 0.0282(3) Uani 1 1 d . . . . . C5 C 1.02364(14) 0.22622(8) 0.57122(6) 0.0250(3) Uani 1 1 d . . . . . C43 C 0.49852(15) 0.56324(9) 0.33110(5) 0.0245(3) Uani 1 1 d . . . . . C29 C 0.30846(15) 0.34705(9) 0.32865(6) 0.0269(3) Uani 1 1 d . . . . . C11 C 0.89559(15) 0.00995(8) 0.53985(5) 0.0238(3) Uani 1 1 d . . . . . C35 C 0.62160(15) 0.45888(9) 0.42838(6) 0.0262(3) Uani 1 1 d . . . . . C12 C 1.01655(15) 0.04354(9) 0.56867(6) 0.0252(3) Uani 1 1 d . . . . . H12A H 1.054475 0.076744 0.546565 0.030 Uiso 1 1 calc R U . . . H12B H 1.079851 0.004249 0.580266 0.030 Uiso 1 1 calc R U . . . C1 C 1.05263(16) 0.25266(9) 0.49129(6) 0.0285(3) Uani 1 1 d . . . . . H1 H 1.021058 0.251227 0.456341 0.034 Uiso 1 1 calc R U . . . C37 C 0.23537(15) 0.53039(8) 0.35820(6) 0.0242(3) Uani 1 1 d . . . . . C36 C 0.47861(15) 0.46703(9) 0.42283(6) 0.0265(3) Uani 1 1 d . . . . . H36A H 0.459491 0.505410 0.446105 0.032 Uiso 1 1 calc R U . . . H36B H 0.441592 0.420180 0.432037 0.032 Uiso 1 1 calc R U . . . C13 C 1.12811(15) 0.09989(9) 0.67574(6) 0.0266(3) Uani 1 1 d . . . . . C4 C 1.14401(15) 0.25653(9) 0.59074(7) 0.0295(3) Uani 1 1 d . . . . . H4 H 1.174753 0.256858 0.625756 0.035 Uiso 1 1 calc R U . . . C7 C 0.70239(16) 0.02375(9) 0.48500(6) 0.0297(3) Uani 1 1 d . . . . . H7 H 0.644645 0.054299 0.463100 0.036 Uiso 1 1 calc R U . . . C6 C 0.93949(15) 0.19500(9) 0.60449(6) 0.0260(3) Uani 1 1 d . . . . . H6A H 0.848772 0.196407 0.586794 0.031 Uiso 1 1 calc R U . . . H6B H 0.946516 0.226141 0.634619 0.031 Uiso 1 1 calc R U . . . C10 C 0.86656(16) -0.06393(9) 0.54695(6) 0.0286(3) Uani 1 1 d . . . . . H10 H 0.925656 -0.093844 0.568785 0.034 Uiso 1 1 calc R U . . . C30 C 0.38693(15) 0.40961(8) 0.31452(6) 0.0251(3) Uani 1 1 d . . . . . H30A H 0.348868 0.425360 0.280199 0.030 Uiso 1 1 calc R U . . . H30B H 0.474952 0.391450 0.314021 0.030 Uiso 1 1 calc R U . . . C14 C 1.11815(16) 0.13800(10) 0.71933(6) 0.0315(3) Uani 1 1 d . . . . . H14 H 1.040093 0.162715 0.721279 0.038 Uiso 1 1 calc R U . . . C2 C 1.17067(16) 0.28522(9) 0.50816(7) 0.0324(4) Uani 1 1 d . . . . . H2 H 1.218138 0.306548 0.485461 0.039 Uiso 1 1 calc R U . . . C38 C 0.13962(16) 0.52972(10) 0.31532(6) 0.0324(4) Uani 1 1 d . . . . . H38 H 0.157591 0.508141 0.285672 0.039 Uiso 1 1 calc R U . . . C19 C 0.84736(16) 0.04945(10) 0.64665(6) 0.0290(3) Uani 1 1 d D . . . . C48 C 0.58464(16) 0.54406(10) 0.30017(7) 0.0335(4) Uani 1 1 d . . . . . H48 H 0.596740 0.493672 0.293217 0.040 Uiso 1 1 calc R U . . . C42 C 0.20553(17) 0.56352(9) 0.40073(6) 0.0317(4) Uani 1 1 d . . . . . H42 H 0.268498 0.564716 0.430534 0.038 Uiso 1 1 calc R U . . . C8 C 0.66727(17) -0.04851(10) 0.49040(7) 0.0334(4) Uani 1 1 d . . . . . H8 H 0.587498 -0.067045 0.472892 0.040 Uiso 1 1 calc R U . . . C9 C 0.75196(17) -0.09311(9) 0.52215(7) 0.0323(4) Uani 1 1 d . . . . . H9 H 0.731314 -0.143130 0.526764 0.039 Uiso 1 1 calc R U . . . C20 C 0.87458(17) -0.00720(9) 0.68105(6) 0.0325(4) Uani 1 1 d . . . . . H20 H 0.961551 -0.017459 0.695705 0.039 Uiso 1 1 calc R U . . . C3 C 1.21809(16) 0.28599(9) 0.55898(7) 0.0335(4) Uani 1 1 d . . . . . H3 H 1.300285 0.306458 0.571806 0.040 Uiso 1 1 calc R U . . . C25 C 0.29992(18) 0.24282(10) 0.37626(7) 0.0360(4) Uani 1 1 d . . . . . H25 H 0.342207 0.209424 0.400703 0.043 Uiso 1 1 calc R U . . . C15 C 1.21938(18) 0.14065(10) 0.75983(7) 0.0357(4) Uani 1 1 d . . . . . H15 H 1.210384 0.166900 0.789072 0.043 Uiso 1 1 calc R U . . . C34 C 0.70471(17) 0.51424(10) 0.45028(7) 0.0352(4) Uani 1 1 d . . . . . H34 H 0.671535 0.556741 0.463663 0.042 Uiso 1 1 calc R U . . . C46 C 0.63820(18) 0.67058(11) 0.28956(7) 0.0388(4) Uani 1 1 d . . . . . H46 H 0.683355 0.707024 0.274780 0.047 Uiso 1 1 calc R U . . . C18 C 1.24478(17) 0.06527(11) 0.67398(7) 0.0377(4) Uani 1 1 d . . . . . H18 H 1.255222 0.039707 0.644643 0.045 Uiso 1 1 calc R U . . . C31 C 0.79409(17) 0.39155(10) 0.41218(7) 0.0362(4) Uani 1 1 d . . . . . H31 H 0.826040 0.348448 0.399080 0.043 Uiso 1 1 calc R U . . . C28 C 0.17928(17) 0.33696(10) 0.30655(7) 0.0367(4) Uani 1 1 d . . . . . H28 H 0.138199 0.370765 0.282138 0.044 Uiso 1 1 calc R U . . . C39 C 0.01882(17) 0.55983(11) 0.31501(7) 0.0382(4) Uani 1 1 d . . . . . H39 H -0.045064 0.558230 0.285485 0.046 Uiso 1 1 calc R U . . . C44 C 0.4879(2) 0.63737(10) 0.34154(7) 0.0400(4) Uani 1 1 d . . . . . H44 H 0.431654 0.652262 0.363055 0.048 Uiso 1 1 calc R U . . . C26 C 0.17280(19) 0.22972(11) 0.35561(8) 0.0412(4) Uani 1 1 d . . . . . H26 H 0.128649 0.188480 0.365569 0.049 Uiso 1 1 calc R U . . . C41 C 0.08543(19) 0.59480(11) 0.40029(7) 0.0399(4) Uani 1 1 d . . . . . H41 H 0.067779 0.618135 0.429418 0.048 Uiso 1 1 calc R U . . . C21 C 0.7763(2) -0.04922(11) 0.69442(8) 0.0427(4) Uani 1 1 d . . . . . H21 H 0.796840 -0.087594 0.718181 0.051 Uiso 1 1 calc R U . . . C47 C 0.65306(17) 0.59717(11) 0.27933(7) 0.0388(4) Uani 1 1 d . . . . . H47 H 0.710170 0.582863 0.258000 0.047 Uiso 1 1 calc R U . . . C40 C -0.00844(17) 0.59210(10) 0.35764(8) 0.0388(4) Uani 1 1 d . . . . . H40 H -0.091274 0.612341 0.357640 0.047 Uiso 1 1 calc R U . . . C27 C 0.11139(18) 0.27808(11) 0.32010(8) 0.0422(4) Uani 1 1 d . . . . . H27 H 0.023592 0.270938 0.305191 0.051 Uiso 1 1 calc R U . . . C16 C 1.33320(18) 0.10493(11) 0.75736(7) 0.0406(4) Uani 1 1 d . . . . . H16 H 1.402486 0.106056 0.785097 0.049 Uiso 1 1 calc R U . . . C32 C 0.88109(18) 0.44451(11) 0.43266(8) 0.0448(5) Uani 1 1 d . . . . . H32 H 0.970588 0.438328 0.433242 0.054 Uiso 1 1 calc R U . . . C33 C 0.83534(19) 0.50673(11) 0.45231(8) 0.0446(5) Uani 1 1 d . . . . . H33 H 0.893127 0.543964 0.467070 0.054 Uiso 1 1 calc R U . . . C22 C 0.6499(2) -0.03567(13) 0.67355(8) 0.0471(5) Uani 1 1 d D . . . . H22 H 0.583179 -0.061824 0.684937 0.057 Uiso 0.71(2) 1 calc R U P A 1 H22A H 0.583655 -0.070096 0.675777 0.057 Uiso 0.29(2) 1 calc R U P A 2 C45 C 0.5578(2) 0.69042(11) 0.32121(8) 0.0468(5) Uani 1 1 d . . . . . H45 H 0.549578 0.740725 0.329368 0.056 Uiso 1 1 calc R U . . . C24A C 0.7177(5) 0.0577(4) 0.6230(2) 0.0313(10) Uani 0.71(2) 1 d D U P A 1 H24A H 0.696553 0.093148 0.597263 0.038 Uiso 0.71(2) 1 calc R U P A 1 C17 C 1.34629(19) 0.06767(13) 0.71469(8) 0.0474(5) Uani 1 1 d . . . . . H17 H 1.424966 0.043458 0.712986 0.057 Uiso 1 1 calc R U . . . C23A C 0.6197(6) 0.0156(3) 0.6363(2) 0.0369(11) Uani 0.71(2) 1 d D U P A 1 H23A H 0.533014 0.022126 0.619791 0.044 Uiso 0.71(2) 1 calc R U P A 1 C49 C 0.2783(3) 0.20974(15) 0.21833(12) 0.0452(7) Uani 0.7 1 d . . P . . H49A H 0.209009 0.192903 0.235561 0.054 Uiso 0.7 1 calc R U P . . H49B H 0.281940 0.175341 0.190526 0.054 Uiso 0.7 1 calc R U P . . Li2 Li 0.5571(3) 0.30454(15) 0.39627(10) 0.0283(5) Uani 1 1 d . . . . . Li1 Li 0.8207(3) 0.16369(14) 0.49292(10) 0.0268(5) Uani 1 1 d . . . . . C23B C 0.6233(17) 0.0331(10) 0.6483(8) 0.054(4) Uani 0.29(2) 1 d D U P A 2 H23B H 0.536610 0.049731 0.640562 0.065 Uiso 0.29(2) 1 calc R U P A 2 C24B C 0.7200(11) 0.0772(13) 0.6343(8) 0.043(3) Uani 0.29(2) 1 d D U P A 2 H24B H 0.701177 0.122803 0.617633 0.052 Uiso 0.29(2) 1 calc R U P A 2 F9 F 0.85170(15) 0.10662(7) 0.36587(6) 0.0710(4) Uani 1 1 d . . . . . F11 F 0.64403(15) 0.11425(8) 0.37588(6) 0.0697(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 P1 0.02097(19) 0.02357(19) 0.0269(2) -0.00145(14) 0.00426(15) 0.00285(14) P2 0.0298(2) 0.0261(2) 0.0269(2) 0.00075(15) 0.00333(16) 0.00353(16) Si2 0.02121(19) 0.01999(19) 0.02304(19) 0.00021(15) 0.00320(15) 0.00103(15) Si1 0.01946(19) 0.0270(2) 0.0240(2) 0.00078(15) 0.00303(15) 0.00049(15) Cl2 0.0462(3) 0.0331(3) 0.0291(3) 0.0043(2) 0.0094(2) -0.0029(2) Cl1 0.0485(4) 0.0367(3) 0.0376(3) -0.0014(2) -0.0024(3) -0.0014(3) F1 0.0282(5) 0.0302(5) 0.0461(6) -0.0067(4) 0.0088(4) 0.0069(4) F3 0.0426(6) 0.0299(5) 0.0602(7) 0.0015(5) 0.0119(5) 0.0138(5) F6 0.0285(5) 0.0374(6) 0.0703(8) 0.0065(5) 0.0196(5) -0.0015(4) F2 0.0481(6) 0.0538(7) 0.0285(5) 0.0025(5) -0.0002(4) -0.0022(5) F5 0.0312(5) 0.0404(6) 0.0611(7) -0.0035(5) 0.0060(5) -0.0108(5) F4 0.0658(8) 0.0500(7) 0.0288(5) -0.0038(5) 0.0047(5) 0.0163(6) F7 0.0417(6) 0.0528(7) 0.0555(7) -0.0165(6) 0.0106(5) 0.0184(5) F8 0.0570(7) 0.0744(9) 0.0272(5) 0.0044(5) -0.0015(5) -0.0226(6) F12 0.0440(6) 0.0564(7) 0.0624(8) 0.0139(6) 0.0255(6) -0.0026(6) F10 0.0667(8) 0.0736(9) 0.0312(6) -0.0133(6) 0.0012(5) 0.0269(7) N2 0.0250(6) 0.0223(6) 0.0282(6) 0.0006(5) 0.0043(5) 0.0012(5) N1 0.0217(6) 0.0212(6) 0.0314(7) -0.0002(5) 0.0048(5) 0.0016(5) N3 0.0261(7) 0.0237(7) 0.0369(7) -0.0006(6) 0.0043(6) -0.0012(5) N4 0.0264(7) 0.0222(6) 0.0344(7) 0.0022(5) 0.0012(5) 0.0014(5) C5 0.0213(7) 0.0194(7) 0.0339(8) -0.0012(6) 0.0045(6) 0.0035(6) C43 0.0241(7) 0.0254(8) 0.0220(7) 0.0004(6) -0.0007(6) -0.0012(6) C29 0.0252(8) 0.0225(7) 0.0327(8) -0.0054(6) 0.0045(6) 0.0006(6) C11 0.0251(7) 0.0231(7) 0.0242(7) -0.0005(6) 0.0073(6) 0.0031(6) C35 0.0288(8) 0.0235(7) 0.0242(7) 0.0034(6) -0.0006(6) 0.0011(6) C12 0.0231(7) 0.0246(7) 0.0278(8) 0.0010(6) 0.0044(6) 0.0024(6) C1 0.0273(8) 0.0244(8) 0.0351(8) 0.0025(6) 0.0090(7) 0.0024(6) C37 0.0234(7) 0.0192(7) 0.0303(8) 0.0014(6) 0.0060(6) 0.0002(6) C36 0.0282(8) 0.0263(8) 0.0241(7) 0.0010(6) 0.0026(6) 0.0026(6) C13 0.0231(7) 0.0276(8) 0.0280(8) 0.0027(6) 0.0022(6) -0.0012(6) C4 0.0237(8) 0.0269(8) 0.0366(9) -0.0055(7) 0.0019(6) 0.0021(6) C7 0.0266(8) 0.0271(8) 0.0332(8) 0.0016(6) 0.0003(6) 0.0024(6) C6 0.0216(7) 0.0275(8) 0.0286(8) -0.0008(6) 0.0041(6) 0.0027(6) C10 0.0314(8) 0.0232(8) 0.0312(8) 0.0028(6) 0.0059(6) 0.0034(6) C30 0.0237(7) 0.0236(7) 0.0277(7) -0.0027(6) 0.0040(6) 0.0006(6) C14 0.0270(8) 0.0351(9) 0.0318(8) -0.0006(7) 0.0041(7) 0.0006(7) C2 0.0278(8) 0.0258(8) 0.0462(10) 0.0018(7) 0.0139(7) -0.0008(6) C38 0.0298(8) 0.0358(9) 0.0305(8) -0.0038(7) 0.0027(7) 0.0058(7) C19 0.0271(8) 0.0351(9) 0.0253(7) -0.0015(6) 0.0060(6) -0.0037(7) C48 0.0278(8) 0.0304(8) 0.0442(10) 0.0027(7) 0.0112(7) 0.0017(7) C42 0.0311(8) 0.0305(8) 0.0325(8) -0.0047(7) 0.0031(7) 0.0040(7) C8 0.0290(8) 0.0305(8) 0.0394(9) -0.0027(7) 0.0031(7) -0.0054(7) C9 0.0366(9) 0.0219(8) 0.0394(9) 0.0002(7) 0.0099(7) -0.0039(7) C20 0.0337(9) 0.0306(8) 0.0341(9) -0.0031(7) 0.0087(7) -0.0025(7) C3 0.0223(8) 0.0263(8) 0.0518(10) -0.0060(7) 0.0065(7) -0.0034(6) C25 0.0342(9) 0.0289(9) 0.0442(10) 0.0049(7) 0.0056(8) -0.0044(7) C15 0.0363(9) 0.0377(10) 0.0317(9) -0.0053(7) 0.0028(7) -0.0076(8) C34 0.0355(9) 0.0274(8) 0.0392(9) -0.0041(7) -0.0022(7) 0.0008(7) C46 0.0353(9) 0.0409(10) 0.0377(9) 0.0095(8) 0.0006(7) -0.0146(8) C18 0.0289(9) 0.0455(10) 0.0364(9) -0.0082(8) 0.0000(7) 0.0081(8) C31 0.0275(8) 0.0275(8) 0.0513(11) 0.0000(7) 0.0017(7) 0.0042(7) C28 0.0267(8) 0.0326(9) 0.0480(10) 0.0009(8) -0.0004(7) -0.0002(7) C39 0.0284(9) 0.0396(10) 0.0426(10) -0.0052(8) -0.0037(7) 0.0056(7) C44 0.0518(11) 0.0295(9) 0.0435(10) -0.0088(8) 0.0212(9) -0.0088(8) C26 0.0356(10) 0.0348(10) 0.0535(11) 0.0016(8) 0.0092(8) -0.0103(8) C41 0.0379(10) 0.0399(10) 0.0433(10) -0.0118(8) 0.0110(8) 0.0095(8) C21 0.0509(11) 0.0359(10) 0.0442(10) 0.0006(8) 0.0165(9) -0.0103(9) C47 0.0286(9) 0.0464(11) 0.0429(10) 0.0072(8) 0.0106(7) -0.0020(8) C40 0.0271(8) 0.0340(9) 0.0550(11) -0.0075(8) 0.0069(8) 0.0074(7) C27 0.0255(8) 0.0410(10) 0.0579(12) -0.0017(9) 0.0022(8) -0.0066(8) C16 0.0287(9) 0.0479(11) 0.0395(10) -0.0011(8) -0.0083(7) -0.0046(8) C32 0.0257(9) 0.0385(10) 0.0666(13) -0.0024(9) -0.0009(8) -0.0007(7) C33 0.0338(10) 0.0360(10) 0.0583(12) -0.0079(9) -0.0061(9) -0.0067(8) C22 0.0420(11) 0.0591(13) 0.0435(11) -0.0055(9) 0.0164(9) -0.0222(10) C45 0.0602(13) 0.0266(9) 0.0558(12) -0.0062(8) 0.0165(10) -0.0112(9) C24A 0.0269(15) 0.040(2) 0.027(2) -0.0055(15) 0.0043(12) -0.0033(12) C17 0.0283(9) 0.0595(13) 0.0500(11) -0.0064(10) -0.0041(8) 0.0104(9) C23A 0.0278(16) 0.054(2) 0.029(2) -0.0104(16) 0.0051(16) -0.0119(14) C49 0.0426(15) 0.0311(13) 0.0580(17) 0.0041(12) -0.0009(13) -0.0052(11) Li2 0.0243(13) 0.0235(13) 0.0362(14) -0.0016(11) 0.0032(11) 0.0023(10) Li1 0.0241(13) 0.0243(13) 0.0313(13) 0.0000(10) 0.0028(10) -0.0008(10) C23B 0.031(4) 0.100(9) 0.030(6) 0.001(6) 0.001(4) -0.018(6) C24B 0.027(4) 0.069(8) 0.035(7) 0.018(6) 0.009(4) -0.001(5) F9 0.0658(9) 0.0445(7) 0.0921(11) -0.0030(7) -0.0128(8) 0.0311(7) F11 0.0689(9) 0.0689(9) 0.0668(9) 0.0070(7) 0.0005(7) -0.0420(8) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.3639 0.7018 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Li Li 0.0008 0.0003 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.2541 0.3302 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -1 -8 13 0.1363 2 10 5 0.2815 2 9 9 0.2951 1 1 17 0.2900 -2 -11 -4 0.2826 -1 -1 -17 0.2134 0 4 -17 0.1594 -6 1 12 0.0514 6 0 -12 0.0200 6 -5 -6 0.0903 -6 5 4 0.0902 1 7 -15 0.1213 7 1 -6 0.1192 3 10 -1 0.2493 0 -9 10 0.1354 3 -11 -1 0.1789 -5 7 11 0.1482 -6 4 9 0.0763 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag F3 P1 F1 178.25(6) . . ? F3 P1 F2 90.04(6) . . ? F3 P1 F5 90.88(6) . . ? F6 P1 F1 88.87(6) . . ? F6 P1 F3 91.27(6) . . ? F6 P1 F2 88.83(7) . . ? F6 P1 F5 176.73(7) . . ? F6 P1 F4 91.73(7) . . ? F2 P1 F1 88.21(6) . . ? F5 P1 F1 88.90(6) . . ? F5 P1 F2 88.70(6) . . ? F4 P1 F1 89.57(6) . . ? F4 P1 F3 92.17(6) . . ? F4 P1 F2 177.70(7) . . ? F4 P1 F5 90.65(7) . . ? F7 P2 F8 88.13(7) . . ? F12 P2 F7 87.72(7) . . ? F12 P2 F8 87.87(7) . . ? F10 P2 F7 89.38(7) . . ? F10 P2 F8 177.50(8) . . ? F10 P2 F12 91.75(8) . . ? F10 P2 F9 92.14(8) . . ? F9 P2 F7 176.89(8) . . ? F9 P2 F8 90.33(8) . . ? F9 P2 F12 89.52(8) . . ? F11 P2 F7 90.27(8) . . ? F11 P2 F8 89.83(7) . . ? F11 P2 F12 176.99(8) . . ? F11 P2 F10 90.46(8) . . ? F11 P2 F9 92.43(10) . . ? C43 Si2 C36 110.32(7) . . ? C43 Si2 C30 107.33(7) . . ? C37 Si2 C43 109.94(7) . . ? C37 Si2 C36 108.55(7) . . ? C37 Si2 C30 110.16(7) . . ? C30 Si2 C36 110.54(7) . . ? C12 Si1 C6 109.18(7) . . ? C13 Si1 C12 111.51(7) . . ? C13 Si1 C6 108.01(7) . . ? C19 Si1 C12 107.01(7) . . ? C19 Si1 C13 109.66(7) . . ? C19 Si1 C6 111.50(7) . . ? P1 F1 Li1 136.10(10) . . ? P1 F2 Li2 148.62(11) . . ? P2 F7 Li2 151.92(12) . . ? P2 F8 Li1 157.80(12) . . ? C11 N2 C7 117.89(14) . . ? C11 N2 Li1 131.52(13) . . ? C7 N2 Li1 110.49(13) . . ? C5 N1 C1 118.01(14) . . ? C5 N1 Li1 121.24(13) . . ? C1 N1 Li1 120.31(14) . . ? C29 N3 C25 118.05(15) . . ? C29 N3 Li2 125.39(14) . . ? C25 N3 Li2 116.38(14) . . ? C35 N4 Li2 121.96(13) . . ? C31 N4 C35 117.87(15) . . ? C31 N4 Li2 117.98(14) . . ? N1 C5 C4 121.29(15) . . ? N1 C5 C6 117.33(14) . . ? C4 C5 C6 121.37(15) . . ? C48 C43 Si2 121.92(12) . . ? C44 C43 Si2 121.08(13) . . ? C44 C43 C48 117.00(15) . . ? N3 C29 C30 117.03(14) . . ? N3 C29 C28 120.89(16) . . ? C28 C29 C30 122.08(15) . . ? N2 C11 C12 118.22(14) . . ? N2 C11 C10 121.31(15) . . ? C10 C11 C12 120.40(14) . . ? N4 C35 C36 117.45(14) . . ? N4 C35 C34 121.56(15) . . ? C34 C35 C36 120.94(15) . . ? Si1 C12 H12A 109.4 . . ? Si1 C12 H12B 109.4 . . ? C11 C12 Si1 111.22(10) . . ? C11 C12 H12A 109.4 . . ? C11 C12 H12B 109.4 . . ? H12A C12 H12B 108.0 . . ? N1 C1 H1 118.2 . . ? N1 C1 C2 123.60(16) . . ? C2 C1 H1 118.2 . . ? C38 C37 Si2 120.65(12) . . ? C42 C37 Si2 121.91(12) . . ? C42 C37 C38 117.35(15) . . ? Si2 C36 H36A 109.2 . . ? Si2 C36 H36B 109.2 . . ? C35 C36 Si2 112.21(11) . . ? C35 C36 H36A 109.2 . . ? C35 C36 H36B 109.2 . . ? H36A C36 H36B 107.9 . . ? C14 C13 Si1 118.04(12) . . ? C18 C13 Si1 124.44(13) . . ? C18 C13 C14 117.50(15) . . ? C5 C4 H4 120.1 . . ? C3 C4 C5 119.79(16) . . ? C3 C4 H4 120.1 . . ? N2 C7 H7 118.1 . . ? N2 C7 C8 123.89(15) . . ? C8 C7 H7 118.1 . . ? Si1 C6 H6A 109.0 . . ? Si1 C6 H6B 109.0 . . ? C5 C6 Si1 112.87(10) . . ? C5 C6 H6A 109.0 . . ? C5 C6 H6B 109.0 . . ? H6A C6 H6B 107.8 . . ? C11 C10 H10 120.1 . . ? C9 C10 C11 119.81(15) . . ? C9 C10 H10 120.1 . . ? Si2 C30 H30A 108.4 . . ? Si2 C30 H30B 108.4 . . ? C29 C30 Si2 115.35(11) . . ? C29 C30 H30A 108.4 . . ? C29 C30 H30B 108.4 . . ? H30A C30 H30B 107.5 . . ? C13 C14 H14 119.2 . . ? C15 C14 C13 121.68(16) . . ? C15 C14 H14 119.2 . . ? C1 C2 H2 120.9 . . ? C1 C2 C3 118.30(16) . . ? C3 C2 H2 120.9 . . ? C37 C38 H38 119.2 . . ? C39 C38 C37 121.55(16) . . ? C39 C38 H38 119.2 . . ? C20 C19 Si1 119.30(13) . . ? C20 C19 C24A 116.7(3) . . ? C20 C19 C24B 119.5(6) . . ? C24A C19 Si1 122.7(3) . . ? C24B C19 Si1 120.6(6) . . ? C43 C48 H48 119.3 . . ? C47 C48 C43 121.41(17) . . ? C47 C48 H48 119.3 . . ? C37 C42 H42 119.4 . . ? C41 C42 C37 121.22(16) . . ? C41 C42 H42 119.4 . . ? C7 C8 H8 121.0 . . ? C7 C8 C9 117.97(16) . . ? C9 C8 H8 121.0 . . ? C10 C9 C8 119.13(15) . . ? C10 C9 H9 120.4 . . ? C8 C9 H9 120.4 . . ? C19 C20 H20 119.5 . . ? C19 C20 C21 120.98(17) . . ? C21 C20 H20 119.5 . . ? C4 C3 C2 118.92(15) . . ? C4 C3 H3 120.5 . . ? C2 C3 H3 120.5 . . ? N3 C25 H25 118.1 . . ? N3 C25 C26 123.73(17) . . ? C26 C25 H25 118.1 . . ? C14 C15 H15 120.2 . . ? C16 C15 C14 119.60(17) . . ? C16 C15 H15 120.2 . . ? C35 C34 H34 120.3 . . ? C33 C34 C35 119.42(17) . . ? C33 C34 H34 120.3 . . ? C47 C46 H46 120.3 . . ? C45 C46 H46 120.3 . . ? C45 C46 C47 119.39(17) . . ? C13 C18 H18 119.6 . . ? C17 C18 C13 120.84(17) . . ? C17 C18 H18 119.6 . . ? N4 C31 H31 118.3 . . ? N4 C31 C32 123.49(17) . . ? C32 C31 H31 118.3 . . ? C29 C28 H28 119.9 . . ? C27 C28 C29 120.14(17) . . ? C27 C28 H28 119.9 . . ? C38 C39 H39 120.0 . . ? C40 C39 C38 119.97(17) . . ? C40 C39 H39 120.0 . . ? C43 C44 H44 119.2 . . ? C43 C44 C45 121.53(17) . . ? C45 C44 H44 119.2 . . ? C25 C26 H26 120.9 . . ? C25 C26 C27 118.19(17) . . ? C27 C26 H26 120.9 . . ? C42 C41 H41 119.9 . . ? C40 C41 C42 120.24(17) . . ? C40 C41 H41 119.9 . . ? C20 C21 H21 119.7 . . ? C22 C21 C20 120.56(19) . . ? C22 C21 H21 119.7 . . ? C48 C47 H47 119.9 . . ? C46 C47 C48 120.16(17) . . ? C46 C47 H47 119.9 . . ? C39 C40 C41 119.64(16) . . ? C39 C40 H40 120.2 . . ? C41 C40 H40 120.2 . . ? C28 C27 C26 118.99(17) . . ? C28 C27 H27 120.5 . . ? C26 C27 H27 120.5 . . ? C15 C16 H16 120.0 . . ? C17 C16 C15 119.99(17) . . ? C17 C16 H16 120.0 . . ? C31 C32 H32 120.8 . . ? C31 C32 C33 118.47(18) . . ? C33 C32 H32 120.8 . . ? C34 C33 C32 119.18(17) . . ? C34 C33 H33 120.4 . . ? C32 C33 H33 120.4 . . ? C21 C22 H22 119.9 . . ? C21 C22 H22A 121.8 . . ? C21 C22 C23B 116.4(7) . . ? C23A C22 C21 120.2(3) . . ? C23A C22 H22 119.9 . . ? C23B C22 H22A 121.8 . . ? C46 C45 C44 120.46(18) . . ? C46 C45 H45 119.8 . . ? C44 C45 H45 119.8 . . ? C19 C24A H24A 119.0 . . ? C23A C24A C19 122.1(5) . . ? C23A C24A H24A 119.0 . . ? C18 C17 H17 119.8 . . ? C16 C17 C18 120.37(18) . . ? C16 C17 H17 119.8 . . ? C22 C23A C24A 119.1(5) . . ? C22 C23A H23A 120.5 . . ? C24A C23A H23A 120.5 . . ? Cl2 C49 H49A 109.1 . . ? Cl2 C49 H49B 109.1 . . ? Cl1 C49 Cl2 112.32(15) . . ? Cl1 C49 H49A 109.1 . . ? Cl1 C49 H49B 109.1 . . ? H49A C49 H49B 107.9 . . ? F2 Li2 N3 96.46(13) . . ? F2 Li2 N4 107.84(14) . . ? F7 Li2 F2 109.14(14) . . ? F7 Li2 N3 108.54(14) . . ? F7 Li2 N4 107.82(14) . . ? N3 Li2 N4 125.80(14) . . ? F1 Li1 N2 95.97(12) . . ? F1 Li1 N1 118.29(14) . . ? F8 Li1 F1 105.58(14) . . ? F8 Li1 N2 113.17(14) . . ? F8 Li1 N1 103.76(13) . . ? N1 Li1 N2 119.66(14) . . ? C22 C23B H23B 118.6 . . ? C24B C23B C22 122.8(13) . . ? C24B C23B H23B 118.6 . . ? C19 C24B H24B 122.0 . . ? C23B C24B C19 116.0(13) . . ? C23B C24B H24B 122.0 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag P1 F1 1.6304(10) . ? P1 F3 1.5874(10) . ? P1 F6 1.5734(11) . ? P1 F2 1.6200(11) . ? P1 F5 1.5885(11) . ? P1 F4 1.5749(11) . ? P2 F7 1.6223(11) . ? P2 F8 1.6233(11) . ? P2 F12 1.5852(12) . ? P2 F10 1.5675(12) . ? P2 F9 1.5761(13) . ? P2 F11 1.5636(13) . ? Si2 C43 1.8745(16) . ? Si2 C37 1.8723(16) . ? Si2 C36 1.8953(16) . ? Si2 C30 1.8935(15) . ? Si1 C12 1.8903(16) . ? Si1 C13 1.8756(16) . ? Si1 C6 1.8943(16) . ? Si1 C19 1.8750(17) . ? Cl2 C49 1.758(3) . ? Cl1 C49 1.756(3) . ? F1 Li1 1.925(3) . ? F2 Li2 1.888(3) . ? F7 Li2 1.881(3) . ? F8 Li1 1.892(3) . ? N2 C11 1.346(2) . ? N2 C7 1.349(2) . ? N2 Li1 2.057(3) . ? N1 C5 1.346(2) . ? N1 C1 1.348(2) . ? N1 Li1 2.026(3) . ? N3 C29 1.344(2) . ? N3 C25 1.351(2) . ? N3 Li2 2.032(3) . ? N4 C35 1.347(2) . ? N4 C31 1.347(2) . ? N4 Li2 2.043(3) . ? C5 C4 1.398(2) . ? C5 C6 1.497(2) . ? C43 C48 1.397(2) . ? C43 C44 1.388(2) . ? C29 C30 1.501(2) . ? C29 C28 1.398(2) . ? C11 C12 1.500(2) . ? C11 C10 1.401(2) . ? C35 C36 1.498(2) . ? C35 C34 1.396(2) . ? C12 H12A 0.9900 . ? C12 H12B 0.9900 . ? C1 H1 0.9500 . ? C1 C2 1.380(2) . ? C37 C38 1.397(2) . ? C37 C42 1.395(2) . ? C36 H36A 0.9900 . ? C36 H36B 0.9900 . ? C13 C14 1.398(2) . ? C13 C18 1.394(2) . ? C4 H4 0.9500 . ? C4 C3 1.381(3) . ? C7 H7 0.9500 . ? C7 C8 1.382(2) . ? C6 H6A 0.9900 . ? C6 H6B 0.9900 . ? C10 H10 0.9500 . ? C10 C9 1.379(2) . ? C30 H30A 0.9900 . ? C30 H30B 0.9900 . ? C14 H14 0.9500 . ? C14 C15 1.388(2) . ? C2 H2 0.9500 . ? C2 C3 1.384(3) . ? C38 H38 0.9500 . ? C38 C39 1.388(2) . ? C19 C20 1.388(2) . ? C19 C24A 1.410(5) . ? C19 C24B 1.418(12) . ? C48 H48 0.9500 . ? C48 C47 1.391(2) . ? C42 H42 0.9500 . ? C42 C41 1.389(2) . ? C8 H8 0.9500 . ? C8 C9 1.386(3) . ? C9 H9 0.9500 . ? C20 H20 0.9500 . ? C20 C21 1.393(3) . ? C3 H3 0.9500 . ? C25 H25 0.9500 . ? C25 C26 1.377(3) . ? C15 H15 0.9500 . ? C15 C16 1.380(3) . ? C34 H34 0.9500 . ? C34 C33 1.378(3) . ? C46 H46 0.9500 . ? C46 C47 1.380(3) . ? C46 C45 1.369(3) . ? C18 H18 0.9500 . ? C18 C17 1.393(3) . ? C31 H31 0.9500 . ? C31 C32 1.376(3) . ? C28 H28 0.9500 . ? C28 C27 1.378(3) . ? C39 H39 0.9500 . ? C39 C40 1.381(3) . ? C44 H44 0.9500 . ? C44 C45 1.392(3) . ? C26 H26 0.9500 . ? C26 C27 1.378(3) . ? C41 H41 0.9500 . ? C41 C40 1.382(3) . ? C21 H21 0.9500 . ? C21 C22 1.373(3) . ? C47 H47 0.9500 . ? C40 H40 0.9500 . ? C27 H27 0.9500 . ? C16 H16 0.9500 . ? C16 C17 1.377(3) . ? C32 H32 0.9500 . ? C32 C33 1.379(3) . ? C33 H33 0.9500 . ? C22 H22 0.9500 . ? C22 H22A 0.9500 . ? C22 C23A 1.372(5) . ? C22 C23B 1.432(13) . ? C45 H45 0.9500 . ? C24A H24A 0.9500 . ? C24A C23A 1.390(6) . ? C17 H17 0.9500 . ? C23A H23A 0.9500 . ? C49 H49A 0.9900 . ? C49 H49B 0.9900 . ? C23B H23B 0.9500 . ? C23B C24B 1.407(13) . ? C24B H24B 0.9500 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag P1 F2 Li2 F7 103.2(2) . . . . ? P1 F2 Li2 N3 -144.61(17) . . . . ? P1 F2 Li2 N4 -13.7(3) . . . . ? P2 F7 Li2 F2 -25.4(3) . . . . ? P2 F7 Li2 N3 -129.4(2) . . . . ? P2 F7 Li2 N4 91.5(3) . . . . ? P2 F8 Li1 F1 -81.7(3) . . . . ? P2 F8 Li1 N2 22.0(4) . . . . ? P2 F8 Li1 N1 153.2(3) . . . . ? Si2 C43 C48 C47 176.90(14) . . . . ? Si2 C43 C44 C45 -177.81(16) . . . . ? Si2 C37 C38 C39 -177.58(14) . . . . ? Si2 C37 C42 C41 176.43(14) . . . . ? Si1 C13 C14 C15 177.79(14) . . . . ? Si1 C13 C18 C17 -177.46(16) . . . . ? Si1 C19 C20 C21 -172.83(14) . . . . ? Si1 C19 C24A C23A 172.2(3) . . . . ? Si1 C19 C24B C23B 173.3(8) . . . . ? F1 P1 F2 Li2 -102.6(2) . . . . ? F3 P1 F2 Li2 77.2(2) . . . . ? F6 P1 F1 Li1 165.89(15) . . . . ? F6 P1 F2 Li2 168.5(2) . . . . ? F2 P1 F1 Li1 77.02(15) . . . . ? F5 P1 F1 Li1 -11.72(15) . . . . ? F5 P1 F2 Li2 -13.6(2) . . . . ? F4 P1 F1 Li1 -102.37(15) . . . . ? F7 P2 F8 Li1 113.8(3) . . . . ? F8 P2 F7 Li2 -14.7(3) . . . . ? F12 P2 F7 Li2 -102.6(3) . . . . ? F12 P2 F8 Li1 -158.4(3) . . . . ? F10 P2 F7 Li2 165.6(3) . . . . ? N2 C11 C12 Si1 78.31(15) . . . . ? N2 C11 C10 C9 -0.3(2) . . . . ? N2 C7 C8 C9 -0.4(3) . . . . ? N1 C5 C4 C3 2.3(2) . . . . ? N1 C5 C6 Si1 95.88(14) . . . . ? N1 C1 C2 C3 1.3(2) . . . . ? N3 C29 C30 Si2 -83.17(16) . . . . ? N3 C29 C28 C27 -0.9(3) . . . . ? N3 C25 C26 C27 0.1(3) . . . . ? N4 C35 C36 Si2 -75.52(16) . . . . ? N4 C35 C34 C33 0.9(3) . . . . ? N4 C31 C32 C33 0.8(3) . . . . ? C5 N1 C1 C2 1.3(2) . . . . ? C5 C4 C3 C2 0.4(2) . . . . ? C43 Si2 C37 C38 81.87(14) . . . . ? C43 Si2 C37 C42 -94.69(14) . . . . ? C43 Si2 C36 C35 -41.60(13) . . . . ? C43 Si2 C30 C29 -178.96(11) . . . . ? C43 C48 C47 C46 0.9(3) . . . . ? C43 C44 C45 C46 0.9(3) . . . . ? C29 N3 C25 C26 -0.9(3) . . . . ? C29 C28 C27 C26 0.0(3) . . . . ? C11 N2 C7 C8 0.2(2) . . . . ? C11 C10 C9 C8 0.1(2) . . . . ? C35 N4 C31 C32 0.0(3) . . . . ? C35 C34 C33 C32 -0.1(3) . . . . ? C12 Si1 C13 C14 179.68(13) . . . . ? C12 Si1 C13 C18 -1.65(18) . . . . ? C12 Si1 C6 C5 -42.66(13) . . . . ? C12 Si1 C19 C20 87.99(14) . . . . ? C12 Si1 C19 C24A -78.6(3) . . . . ? C12 Si1 C19 C24B -100.9(13) . . . . ? C12 C11 C10 C9 176.67(15) . . . . ? C1 N1 C5 C4 -3.1(2) . . . . ? C1 N1 C5 C6 178.03(13) . . . . ? C1 C2 C3 C4 -2.1(2) . . . . ? C37 Si2 C43 C48 -142.61(14) . . . . ? C37 Si2 C43 C44 36.55(16) . . . . ? C37 Si2 C36 C35 -162.12(11) . . . . ? C37 Si2 C30 C29 -59.28(13) . . . . ? C37 C38 C39 C40 0.7(3) . . . . ? C37 C42 C41 C40 1.5(3) . . . . ? C36 Si2 C43 C48 97.71(14) . . . . ? C36 Si2 C43 C44 -83.13(16) . . . . ? C36 Si2 C37 C38 -157.38(13) . . . . ? C36 Si2 C37 C42 26.07(15) . . . . ? C36 Si2 C30 C29 60.68(13) . . . . ? C36 C35 C34 C33 -176.44(17) . . . . ? C13 Si1 C12 C11 152.26(11) . . . . ? C13 Si1 C6 C5 78.76(13) . . . . ? C13 Si1 C19 C20 -33.10(16) . . . . ? C13 Si1 C19 C24A 160.3(3) . . . . ? C13 Si1 C19 C24B 138.0(13) . . . . ? C13 C14 C15 C16 0.0(3) . . . . ? C13 C18 C17 C16 -0.5(3) . . . . ? C4 C5 C6 Si1 -83.00(16) . . . . ? C7 N2 C11 C12 -176.91(14) . . . . ? C7 N2 C11 C10 0.1(2) . . . . ? C7 C8 C9 C10 0.2(3) . . . . ? C6 Si1 C12 C11 -88.48(12) . . . . ? C6 Si1 C13 C14 59.72(15) . . . . ? C6 Si1 C13 C18 -121.61(16) . . . . ? C6 Si1 C19 C20 -152.68(13) . . . . ? C6 Si1 C19 C24A 40.7(3) . . . . ? C6 Si1 C19 C24B 18.5(13) . . . . ? C6 C5 C4 C3 -178.87(15) . . . . ? C10 C11 C12 Si1 -98.72(15) . . . . ? C30 Si2 C43 C48 -22.79(15) . . . . ? C30 Si2 C43 C44 156.37(14) . . . . ? C30 Si2 C37 C38 -36.22(15) . . . . ? C30 Si2 C37 C42 147.23(13) . . . . ? C30 Si2 C36 C35 76.95(13) . . . . ? C30 C29 C28 C27 178.99(17) . . . . ? C14 C13 C18 C17 1.2(3) . . . . ? C14 C15 C16 C17 0.7(3) . . . . ? C38 C37 C42 C41 -0.2(3) . . . . ? C38 C39 C40 C41 0.6(3) . . . . ? C19 Si1 C12 C11 32.34(13) . . . . ? C19 Si1 C13 C14 -61.97(15) . . . . ? C19 Si1 C13 C18 116.69(16) . . . . ? C19 Si1 C6 C5 -160.69(11) . . . . ? C19 C20 C21 C22 0.3(3) . . . . ? C19 C24A C23A C22 0.1(6) . . . . ? C48 C43 C44 C45 1.4(3) . . . . ? C42 C37 C38 C39 -0.9(3) . . . . ? C42 C41 C40 C39 -1.7(3) . . . . ? C20 C19 C24A C23A 5.3(5) . . . . ? C20 C19 C24B C23B -15.6(17) . . . . ? C20 C21 C22 C23A 5.3(4) . . . . ? C20 C21 C22 C23B -15.3(12) . . . . ? C25 N3 C29 C30 -178.59(15) . . . . ? C25 N3 C29 C28 1.3(2) . . . . ? C25 C26 C27 C28 0.4(3) . . . . ? C15 C16 C17 C18 -0.5(3) . . . . ? C34 C35 C36 Si2 101.96(16) . . . . ? C18 C13 C14 C15 -1.0(3) . . . . ? C31 N4 C35 C36 176.56(15) . . . . ? C31 N4 C35 C34 -0.9(2) . . . . ? C31 C32 C33 C34 -0.8(3) . . . . ? C28 C29 C30 Si2 96.93(17) . . . . ? C44 C43 C48 C47 -2.3(3) . . . . ? C21 C22 C23A C24A -5.4(6) . . . . ? C21 C22 C23B C24B 15.2(16) . . . . ? C47 C46 C45 C44 -2.3(3) . . . . ? C22 C23B C24B C19 0.2(17) . . . . ? C45 C46 C47 C48 1.4(3) . . . . ? C24A C19 C20 C21 -5.4(4) . . . . ? Li2 N3 C29 C30 -3.6(2) . . . . ? Li2 N3 C29 C28 176.32(16) . . . . ? Li2 N3 C25 C26 -176.38(18) . . . . ? Li2 N4 C35 C36 -20.6(2) . . . . ? Li2 N4 C35 C34 161.94(16) . . . . ? Li2 N4 C31 C32 -163.52(19) . . . . ? Li1 N2 C11 C12 -0.8(2) . . . . ? Li1 N2 C11 C10 176.20(15) . . . . ? Li1 N2 C7 C8 -176.66(16) . . . . ? Li1 N1 C5 C4 169.34(14) . . . . ? Li1 N1 C5 C6 -9.6(2) . . . . ? Li1 N1 C1 C2 -171.21(15) . . . . ? C24B C19 C20 C21 15.9(13) . . . . ? F9 P2 F8 Li1 -68.9(3) . . . . ? F11 P2 F7 Li2 75.2(3) . . . . ? F11 P2 F8 Li1 23.6(3) . . . . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -1.3552 -8.0065 12.9776 -0.0395 -0.1728 0.9842 2.2462 10.3950 4.9347 0.2250 0.9424 -0.2474 2.0349 8.8977 9.2458 0.2326 0.9722 0.0257 0.5058 0.6043 17.0804 0.1470 0.6084 0.7799 -2.2612 -10.5310 -4.3514 -0.2227 -0.9334 0.2813 -0.6316 -1.2338 -16.9208 -0.1570 -0.6503 -0.7433 0.4625 4.0476 -16.5221 -0.0595 -0.2410 -0.9687 -5.8913 0.9123 11.6532 -0.8164 0.2867 0.5013 5.7058 -0.2991 -12.4003 0.7783 -0.2730 -0.5654 6.2537 -4.5374 -5.5681 0.9420 -0.3326 -0.0447 -6.1829 5.0142 4.4984 -0.9425 0.3330 -0.0280 0.9192 6.6046 -14.6773 -0.0152 0.0087 -0.9998 6.7705 1.1318 -5.5506 0.9487 0.0763 -0.3069 3.4026 10.2513 -0.8196 0.3684 0.7764 -0.5114 0.3354 -9.3504 10.4400 0.2118 -0.3043 0.9287 2.6037 -10.9323 -1.2843 0.5069 -0.7347 0.4508 -4.6755 6.5826 10.5063 -0.7131 0.6762 0.1849 -5.9517 3.7846 9.4872 -0.8703 0.4149 0.2653