Crystallography Open Database

Information card for entry 7127772

Preview

Coordinates	7127772.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H42 Cl8 Ni2 O14 P2
Calculated formula	C32 H42 Cl8 Ni2 O14 P2
Title of publication	Oxyphosphoranes as precursors to bridging phosphate-catecholate ligands.
Authors of publication	Yang, Xin; Wei, Rui; Shi, Yaping; Liu, Liu Leo; Wu, Yile; Zhao, Yufen; Stephan, Douglas W.
Journal of publication	Chemical communications (Cambridge, England)
Year of publication	2021
Journal volume	57
Journal issue	10
Pages of publication	1194 - 1197
a	8.911 ± 0.0005 Å
b	11.1675 ± 0.0006 Å
c	11.8597 ± 0.0007 Å
α	108.483 ± 0.0015°
β	97.6582 ± 0.0016°
γ	100.322 ± 0.0015°
Cell volume	1078.12 ± 0.11 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0329
Residual factor for significantly intense reflections	0.0325
Weighted residual factors for significantly intense reflections	0.0853
Weighted residual factors for all reflections included in the refinement	0.0856
Goodness-of-fit parameter for all reflections included in the refinement	1.06
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
262468 (current)	2021-03-05	cif/ Updating files of 7127772, 7127773, 7127774, 7127775 Original log message: Adding full bibliography for 7127772--7127775.cif.	7127772.cif
260500	2021-01-05	cif/ Adding structures of 7127772, 7127773, 7127774, 7127775 via cif-deposit CGI script.	7127772.cif