Crystallography Open Database

Information card for entry 7154166

Preview

Coordinates	7154166.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C35 H26 B F10 P
Calculated formula	C35 H26 B F10 P
Title of publication	1,1-Alkenylboration of diarylphosphino-enynes: convenient synthetic entry to vicinal P/B Lewis pairs at extended conjugated π-frameworks.
Authors of publication	Chen, Guo-Qiang; Kehr, Gerald; Daniliuc, Constantin G.; Erker, Gerhard
Journal of publication	Organic & biomolecular chemistry
Year of publication	2015
Journal volume	13
Journal issue	3
Pages of publication	764 - 769
a	11.546 ± 0.0002 Å
b	12.36 ± 0.0001 Å
c	12.765 ± 0.0002 Å
α	101.747 ± 0.001°
β	113.392 ± 0.002°
γ	95.129 ± 0.001°
Cell volume	1607.29 ± 0.05 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0448
Residual factor for significantly intense reflections	0.0401
Weighted residual factors for significantly intense reflections	0.1025
Weighted residual factors for all reflections included in the refinement	0.1067
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
180327 (current)	2016-03-26	cif/7/15/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/15/41.	7154166.cif
133516	2015-03-06	cif/ Updating files of 7154166, 7154167, 7154168, 7154169, 7154170, 7154171, 7154172, 7154173 Original log message: Adding full bibliography for 7154166--7154173.cif.	7154166.cif
125798	2014-10-24	cif/ Adding structures of 7154166, 7154167, 7154168, 7154169, 7154170, 7154171, 7154172, 7154173 via cif-deposit CGI script.	7154166.cif