#------------------------------------------------------------------------------ #$Date: 2020-04-09 06:48:06 +0300 (Thu, 09 Apr 2020) $ #$Revision: 250530 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/74/7157460.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7157460 loop_ _publ_author_name 'Sarkar, Parantap' 'Inaba, Yuya' 'Shirakura, Hayato' 'Yoneda, Tomoki' 'Inokuma, Yasuhide' _publ_section_title ; Modular synthesis of oligoacetylacetones via site-selective silylation of acetylacetone derivatives ; _journal_name_full 'Organic & Biomolecular Chemistry' _journal_paper_doi 10.1039/D0OB00501K _journal_year 2020 _chemical_formula_moiety 'C34 H50 O8' _chemical_formula_sum 'C34 H50 O8' _chemical_formula_weight 586.74 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _cell_angle_alpha 103.164(3) _cell_angle_beta 95.845(2) _cell_angle_gamma 95.145(2) _cell_formula_units_Z 1 _cell_length_a 7.3875(2) _cell_length_b 9.2832(3) _cell_length_c 11.5913(3) _cell_measurement_reflns_used 6794 _cell_measurement_temperature 123(2) _cell_measurement_theta_max 29.5420 _cell_measurement_theta_min 3.1200 _cell_volume 764.77(4) _computing_cell_refinement 'CrysAlisPro 1.171.39.43a (Rigaku OD, 2018)' _computing_data_collection 'CrysAlisPro 1.171.39.43a (Rigaku OD, 2018)' _computing_data_reduction 'CrysAlisPro 1.171.39.43a (Rigaku OD, 2018)' _computing_molecular_graphics 'Yadokari-XG 2009 (Wakita Nemoto et al., 2009)' _computing_publication_material 'Yadokari-XG 2009 (Wakita Nemoto et al., 2009)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 123(2) _diffrn_detector 'CCD plate' _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB AFC11 (RCD3): quarter-chi single' _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0226 _diffrn_reflns_av_unetI/netI 0.0215 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.993 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 12777 _diffrn_reflns_point_group_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.993 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 26.993 _diffrn_reflns_theta_min 2.269 _diffrn_source 'Rotating-anode X-ray tube (dual wavelength)' _diffrn_source_type 'Rigaku (Mo) X-ray DW Source' _exptl_absorpt_coefficient_mu 0.089 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.76417 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.39.43a (Rigaku Oxford Diffraction, 2018) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour colorless _exptl_crystal_density_diffrn 1.274 _exptl_crystal_density_method 'not measured' _exptl_crystal_description plate _exptl_crystal_F_000 318 _exptl_crystal_size_max 0.700 _exptl_crystal_size_mid 0.380 _exptl_crystal_size_min 0.040 _refine_diff_density_max 0.359 _refine_diff_density_min -0.156 _refine_diff_density_rms 0.038 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.046 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 193 _refine_ls_number_reflns 3318 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.046 _refine_ls_R_factor_all 0.0397 _refine_ls_R_factor_gt 0.0350 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0439P)^2^+0.2657P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0904 _refine_ls_wR_factor_ref 0.0932 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2958 _reflns_number_total 3318 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d0ob00501k3.cif _cod_data_source_block Compound8 _cod_database_code 7157460 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.940 _shelx_estimated_absorpt_t_max 0.996 _shelx_res_file ; TITL PS_ex80_1_a.res in P-1 PS_ex80_1_a.res created by SHELXL-2018/3 at 12:04:06 on 03-Feb-2020 REM Yadorkari-X generated CELL 0.71073 7.3875 9.2832 11.5913 103.1640 95.8450 95.1450 ZERR 1.0 0.0002 0.0003 0.0003 0.0030 0.0020 0.0020 LATT 1 REM SPGR P-1 triclinic SFAC C H O UNIT 34 50 8 SIZE 0.70 0.38 0.04 TEMP -150.0 L.S. 10 FMAP 2 PLAN -20 ACTA CONF LIST 4 OMIT -10.000000 54.000000 WGHT 0.043900 0.265700 FVAR 1.01170 C1 1 0.214123 0.360901 0.836579 11.00000 0.02138 0.02937 = 0.04244 0.00166 0.00742 0.00648 AFIX 137 H1 2 0.185827 0.342563 0.913138 11.00000 -1.50000 H2 2 0.178919 0.269645 0.773426 11.00000 -1.50000 H3 2 0.145924 0.440381 0.818149 11.00000 -1.50000 AFIX 0 C2 1 0.415825 0.407021 0.844272 11.00000 0.02291 0.01940 = 0.01686 0.00401 0.00376 0.00436 C3 1 0.541788 0.282168 0.817781 11.00000 0.01793 0.01492 = 0.01875 0.00302 0.00135 0.00174 C4 1 0.502527 0.220399 0.681613 11.00000 0.01452 0.01456 = 0.01991 0.00275 0.00101 0.00417 C5 1 0.601400 0.302767 0.603310 11.00000 0.01570 0.01735 = 0.01938 0.00359 0.00137 0.00061 AFIX 23 H4 2 0.729439 0.278913 0.604670 11.00000 -1.20000 H5 2 0.604476 0.411371 0.635825 11.00000 -1.20000 AFIX 0 C6 1 0.508688 0.261365 0.475117 11.00000 0.01720 0.01809 = 0.01807 0.00340 0.00323 0.00116 AFIX 23 H6 2 0.583547 0.309464 0.425110 11.00000 -1.20000 H7 2 0.500044 0.152161 0.443635 11.00000 -1.20000 AFIX 0 C7 1 0.318395 0.310340 0.467644 11.00000 0.01843 0.01171 = 0.01744 0.00621 0.00328 -0.00001 C8 1 0.178312 0.230038 0.359153 11.00000 0.01637 0.01217 = 0.01553 0.00491 0.00288 0.00133 C9 1 0.123512 0.076589 0.384239 11.00000 0.01483 0.01378 = 0.01490 0.00460 -0.00035 0.00062 C10 1 0.000837 0.072321 0.479878 11.00000 0.01632 0.01288 = 0.01888 0.00624 0.00368 0.00132 AFIX 23 H8 2 -0.125479 0.084225 0.448925 11.00000 -1.20000 H9 2 0.043372 0.156861 0.549394 11.00000 -1.20000 AFIX 0 C11 1 0.741973 0.347231 0.857148 11.00000 0.01850 0.02375 = 0.02130 0.00126 -0.00172 0.00162 AFIX 137 H10 2 0.762527 0.382463 0.944323 11.00000 -1.50000 H11 2 0.770018 0.430737 0.820711 11.00000 -1.50000 H12 2 0.821708 0.270202 0.831647 11.00000 -1.50000 AFIX 0 C12 1 0.490712 0.160545 0.883034 11.00000 0.03108 0.01965 = 0.02195 0.00677 0.00308 0.00283 AFIX 137 H13 2 0.575435 0.084764 0.869189 11.00000 -1.50000 H14 2 0.365291 0.114235 0.852671 11.00000 -1.50000 H15 2 0.498826 0.205048 0.968871 11.00000 -1.50000 AFIX 0 C13 1 0.011928 0.318298 0.352075 11.00000 0.01855 0.01459 = 0.02014 0.00636 0.00200 0.00352 AFIX 23 H16 2 -0.048266 0.324129 0.425238 11.00000 -1.20000 H17 2 0.054418 0.421111 0.348208 11.00000 -1.20000 AFIX 0 C14 1 -0.126767 0.245280 0.242714 11.00000 0.02143 0.02178 = 0.02614 0.00910 -0.00223 0.00349 AFIX 23 H18 2 -0.178306 0.146171 0.250310 11.00000 -1.20000 H19 2 -0.228698 0.307060 0.238916 11.00000 -1.20000 AFIX 0 C15 1 -0.037677 0.227675 0.127745 11.00000 0.03337 0.02643 = 0.02066 0.00842 -0.00476 0.00358 AFIX 23 H20 2 -0.128577 0.174636 0.059087 11.00000 -1.20000 H21 2 0.001394 0.327372 0.115520 11.00000 -1.20000 AFIX 0 C16 1 0.127592 0.141283 0.132510 11.00000 0.03165 0.02346 = 0.01588 0.00494 0.00262 0.00332 AFIX 23 H22 2 0.187526 0.138690 0.059581 11.00000 -1.20000 H23 2 0.085853 0.037372 0.133821 11.00000 -1.20000 AFIX 0 C17 1 0.267120 0.211047 0.242672 11.00000 0.02225 0.01763 = 0.01682 0.00607 0.00594 0.00152 AFIX 23 H24 2 0.321823 0.309584 0.235766 11.00000 -1.20000 H25 2 0.366819 0.147005 0.245782 11.00000 -1.20000 AFIX 0 O1 3 0.478293 0.536495 0.869852 11.00000 0.03281 0.01709 = 0.03197 0.00500 0.00777 0.00394 O2 3 0.390030 0.113128 0.638525 11.00000 0.02211 0.01914 = 0.02350 0.00254 -0.00006 -0.00410 O3 3 0.276571 0.408362 0.545263 11.00000 0.02483 0.01895 = 0.02326 -0.00173 0.00134 0.00588 O4 3 0.179894 -0.034646 0.330410 11.00000 0.02940 0.01421 = 0.02280 0.00477 0.00862 0.00536 HKLF 4 1 1 0 0 0 1 0 0 0 1 REM PS_ex80_1_a.res in P-1 REM wR2 = 0.0932, GooF = S = 1.046, Restrained GooF = 1.046 for all data REM R1 = 0.0350 for 2958 Fo > 4sig(Fo) and 0.0397 for all 3318 data REM 193 parameters refined using 0 restraints END WGHT 0.0439 0.2657 REM Highest difference peak 0.359, deepest hole -0.156, 1-sigma level 0.038 Q1 1 0.2542 0.2736 0.4096 11.00000 0.05 0.36 Q2 1 0.5272 0.2567 0.7508 11.00000 0.05 0.35 Q3 1 0.5547 0.2815 0.5366 11.00000 0.05 0.34 Q4 1 -0.0562 0.2828 0.2985 11.00000 0.05 0.33 Q5 1 0.2203 0.2158 0.3039 11.00000 0.05 0.33 Q6 1 0.4750 0.3379 0.8289 11.00000 0.05 0.32 Q7 1 0.1485 0.1590 0.3730 11.00000 0.05 0.32 Q8 1 0.0932 0.2742 0.3580 11.00000 0.05 0.31 Q9 1 0.1958 0.1782 0.1859 11.00000 0.05 0.31 Q10 1 0.5136 0.2191 0.8438 11.00000 0.05 0.29 Q11 1 0.6376 0.3188 0.8332 11.00000 0.05 0.29 Q12 1 0.0693 0.0748 0.4353 11.00000 0.05 0.28 Q13 1 0.4157 0.2844 0.4716 11.00000 0.05 0.28 Q14 1 0.5539 0.2634 0.6390 11.00000 0.05 0.26 Q15 1 0.0000 0.0000 0.5000 10.50000 0.05 0.24 Q16 1 0.0397 0.1773 0.1321 11.00000 0.05 0.24 Q17 1 0.3146 0.3719 0.8395 11.00000 0.05 0.23 Q18 1 -0.0763 0.2334 0.1848 11.00000 0.05 0.23 Q19 1 0.0464 0.3786 0.3310 11.00000 0.05 0.16 Q20 1 -0.0167 0.3535 0.4070 11.00000 0.05 0.15 ; _shelx_res_checksum 24655 _shelx_hkl_file ; 0 0 2 303.01 8.34 0 0 -2 278.14 8.34 0 0 3 2198.21 61.69 0 0 -3 2165.69 61.69 0 0 4 3559.92 101.40 0 0 -4 3617.38 101.40 0 0 5 145.15 4.45 0 0 5 144.72 4.24 0 0 -5 140.13 4.43 0 0 6 919.06 26.76 0 0 -6 959.87 27.02 0 0 6 976.75 27.03 0 0 -7 0.67 0.55 0 0 7 1.00 0.57 0 0 7 1.66 0.32 0 0 8 615.73 17.04 0 0 8 567.11 16.61 0 0 9 63.25 2.37 0 0 9 53.35 1.82 0 0 10 454.88 13.65 0 0 11 11.52 1.44 0 0 11 11.56 1.22 0 0 12 35.31 2.27 0 0 12 30.79 1.85 0 0 13 36.57 2.14 0 0 13 41.44 2.55 0 0 14 42.74 2.40 0 -1 14 35.79 2.27 0 -1 14 43.41 2.82 0 -1 13 32.57 2.39 0 -1 13 33.78 2.07 0 -1 12 4.81 1.12 0 -1 12 4.40 1.37 0 -1 11 0.62 0.86 0 1 -10 35.64 1.77 0 -1 10 36.18 1.83 0 1 -9 621.88 18.08 0 -1 9 613.65 18.15 0 1 -8 111.48 3.69 0 -1 8 108.58 3.72 0 -1 7 1143.37 33.11 0 1 -7 1166.56 33.08 0 1 -6 22.98 1.09 0 -1 6 21.55 1.09 0 1 -5 517.21 14.82 0 -1 5 509.29 14.87 0 1 -4 19.88 0.68 0 1 -4 20.69 0.88 0 -1 4 21.01 0.91 0 -1 3 1200.92 34.16 0 1 -3 1205.74 34.15 0 1 -2 425.92 12.68 0 -1 2 462.68 12.70 0 -1 0 1.77 0.22 0 -1 -1 501.05 13.69 0 1 1 476.78 13.79 0 1 1 462.15 13.66 0 -1 -2 99.76 3.06 0 1 3 2573.86 72.80 0 1 4 18.23 0.88 0 1 5 1116.07 31.88 0 1 6 19.66 1.05 0 1 7 8.00 0.78 0 1 8 518.15 15.27 0 1 9 255.58 7.68 0 1 9 261.84 8.04 0 1 10 30.13 1.28 0 1 10 32.52 1.74 0 1 10 30.07 1.92 0 1 11 24.10 1.09 0 1 11 24.41 1.61 0 1 12 10.45 1.53 0 1 12 9.73 1.29 0 1 13 4.89 1.15 0 -1 -13 4.25 1.31 0 1 13 3.88 1.47 0 -1 -14 10.67 1.69 0 1 14 7.83 1.37 0 -2 14 79.60 4.04 0 -2 14 77.32 3.50 0 -2 13 1.19 1.46 0 -2 13 -0.46 1.14 0 -2 12 121.20 4.54 0 2 -12 124.26 4.36 0 2 -11 6.28 0.95 0 -2 11 6.60 1.12 0 2 -10 12.34 1.07 0 -2 10 10.58 1.18 0 -2 9 7.41 0.93 0 2 -9 7.41 0.91 0 -2 8 112.87 3.85 0 2 -8 109.11 3.68 0 -2 7 75.95 2.81 0 2 -7 79.01 2.71 0 2 -6 5.35 0.64 0 2 -6 5.35 0.36 0 -2 6 5.66 0.73 0 -2 5 1.93 0.59 0 2 -5 1.65 0.53 0 2 -4 2669.34 75.21 0 -2 4 2641.89 75.25 0 2 -3 281.16 8.34 0 -2 3 285.26 8.38 0 2 -2 2657.58 75.99 0 -2 2 2715.48 76.03 0 -2 1 753.35 20.50 0 2 -1 690.78 20.51 0 -2 1 701.46 20.58 0 2 0 3338.04 94.25 0 -2 0 3331.37 94.25 0 2 1 235.21 6.74 0 -2 -1 234.56 6.77 0 2 2 190.86 5.74 0 -2 -2 196.82 5.79 0 2 2 187.08 6.01 0 -2 -3 0.28 0.46 0 -2 -4 657.51 19.02 0 -2 -5 221.68 6.65 0 2 5 208.81 6.59 0 -2 -6 143.55 4.81 0 2 6 150.78 4.76 0 2 7 10.80 0.94 0 -2 -7 12.85 1.07 0 -2 -8 504.05 14.36 0 2 8 502.29 14.19 0 -2 -9 16.67 1.41 0 2 9 15.47 1.25 0 2 9 13.56 1.31 0 -2 -10 71.92 3.15 0 2 10 79.19 3.02 0 2 10 70.79 3.12 0 -2 -11 0.59 1.16 0 2 11 0.38 0.90 0 2 11 -0.12 1.00 0 2 11 0.32 0.61 0 2 12 70.09 3.06 0 2 12 72.27 3.34 0 -2 -12 72.36 3.36 0 2 13 1.35 1.17 0 2 13 0.90 1.37 0 -2 -13 0.43 1.30 0 -2 -14 0.48 1.52 0 -3 14 42.42 2.59 0 -3 14 46.42 3.19 0 3 -14 51.68 2.39 0 3 -13 67.74 2.84 0 -3 13 68.51 3.13 0 -3 12 11.46 1.43 0 3 -12 10.38 1.18 0 3 -11 323.60 9.90 0 -3 11 320.16 10.13 0 -3 10 1.10 0.96 0 3 -10 0.28 0.76 0 -3 9 851.34 25.04 0 3 -9 862.50 24.86 0 3 -8 0.08 0.29 0 -3 8 -0.76 0.71 0 3 -8 0.92 0.67 0 3 -7 141.00 4.33 0 -3 7 144.06 4.78 0 3 -7 150.53 4.68 0 -3 6 405.27 12.17 0 3 -6 408.80 12.04 0 -3 5 124.60 4.21 0 3 -5 126.61 4.08 0 3 -4 89.59 3.04 0 -3 4 86.74 3.11 0 3 -3 8.22 0.75 0 -3 3 9.14 0.84 0 -3 2 214.31 6.66 0 3 -2 219.67 6.60 0 3 -2 211.84 6.63 0 3 -1 3596.69 99.38 0 -3 1 3510.18 99.32 0 -3 1 3404.31 99.49 0 -3 0 144.65 4.54 0 3 0 144.19 4.55 0 -3 -1 0.09 0.51 0 3 1 0.39 0.66 0 3 1 0.04 0.49 0 -3 -2 5.13 0.67 0 3 2 6.18 0.89 0 3 2 4.70 0.63 0 -3 -3 0.05 0.57 0 3 3 0.13 0.48 0 -3 -4 0.06 0.62 0 3 4 -0.46 0.81 0 -3 -5 124.82 4.19 0 3 5 120.74 4.49 0 -3 -6 50.32 2.18 0 3 6 48.82 2.10 0 3 6 51.43 2.52 0 3 7 5.13 1.19 0 3 7 3.82 0.82 0 -3 -7 5.60 0.99 0 3 7 4.44 0.95 0 3 8 553.21 17.02 0 -3 -8 545.33 16.57 0 3 8 529.11 16.52 0 3 8 582.83 16.48 0 3 9 86.74 3.34 0 3 9 89.58 3.95 0 -3 -9 86.77 3.55 0 3 9 84.17 3.46 0 3 10 3.25 1.46 0 3 10 4.11 1.00 0 3 10 3.27 1.09 0 -3 -10 2.35 1.15 0 3 11 34.90 2.63 0 -3 -11 31.56 2.14 0 3 11 33.08 2.13 0 3 11 36.12 2.02 0 -3 -12 69.64 3.43 0 3 12 70.59 3.42 0 3 12 80.89 3.30 0 3 12 72.67 3.85 0 -3 -13 0.94 1.44 0 3 13 3.21 1.79 0 3 13 1.57 1.22 0 4 -14 25.96 1.77 0 -4 14 29.94 2.23 0 4 -13 1.11 0.91 0 -4 13 0.53 1.22 0 -4 12 19.76 1.76 0 4 -12 21.55 1.48 0 -4 11 6.23 1.26 0 4 -11 7.18 0.93 0 -4 10 39.41 2.22 0 4 -10 42.48 2.00 0 4 -9 102.74 3.67 0 -4 9 103.33 3.91 0 4 -9 102.70 3.23 0 -4 8 158.40 5.52 0 4 -8 166.24 5.34 0 4 -7 48.80 2.06 0 -4 7 46.97 2.27 0 4 -6 151.10 4.96 0 -4 6 152.96 5.14 0 4 -5 256.78 7.95 0 -4 5 259.31 8.11 0 -4 4 61.78 2.60 0 4 -4 62.36 2.51 0 4 -4 67.85 2.62 0 4 -3 614.53 17.83 0 4 -3 598.25 17.82 0 -4 3 606.75 17.89 0 4 -2 1389.83 40.07 0 -4 2 1445.69 40.25 0 4 -2 1365.73 40.13 0 4 -1 390.14 11.41 0 -4 1 394.97 11.36 0 -4 0 -0.06 0.65 0 4 0 0.36 0.69 0 4 1 77.68 3.11 0 -4 -1 79.27 2.85 0 4 1 77.09 2.83 0 4 2 13.26 1.28 0 4 2 10.82 0.91 0 -4 -2 12.63 1.02 0 -4 -3 0.14 0.63 0 4 3 0.27 0.55 0 4 3 0.20 0.94 0 4 4 434.46 13.13 0 -4 -4 417.23 12.75 0 -4 -5 384.75 11.40 0 4 5 399.26 11.83 0 4 6 40.57 2.38 0 -4 -6 37.50 1.96 0 4 6 38.92 2.04 0 4 7 313.70 10.03 0 4 7 320.48 10.50 0 -4 -7 312.21 10.03 0 4 7 335.05 9.97 0 -4 -8 68.55 2.98 0 4 8 61.73 3.31 0 4 8 65.43 2.78 0 4 8 66.95 2.94 0 4 9 4.93 1.06 0 4 9 6.57 1.70 0 4 9 6.39 1.22 0 -4 -9 2.22 1.16 0 -4 -10 155.92 5.72 0 4 10 164.57 6.24 0 4 10 156.01 5.66 0 4 10 151.10 5.44 0 4 11 95.68 3.78 0 4 11 95.62 3.97 0 4 11 84.27 4.37 0 -4 -11 92.87 4.01 0 4 12 34.53 2.21 0 -4 -12 35.65 2.55 0 4 12 39.42 2.99 0 4 13 11.45 2.34 0 4 13 10.25 1.61 0 -5 14 1.85 1.49 0 5 -14 1.33 1.16 0 -5 13 -0.73 1.39 0 5 -13 0.19 0.96 0 5 -12 4.25 1.08 0 -5 12 2.59 1.32 0 5 -11 2.33 0.93 0 -5 11 2.82 1.28 0 5 -11 1.25 0.38 0 -5 10 149.21 5.30 0 5 -10 142.26 4.87 0 5 -10 137.91 4.39 0 -5 9 799.31 24.03 0 5 -9 816.19 23.68 0 -5 8 67.38 3.13 0 5 -8 74.00 2.86 0 -5 7 41.71 2.26 0 5 -7 44.36 2.07 0 -5 6 42.80 2.22 0 5 -6 42.78 2.03 0 -5 5 201.76 6.78 0 5 -5 201.82 6.74 0 5 -5 209.11 6.63 0 -5 4 2.56 0.94 0 5 -4 2.89 0.88 0 5 -4 3.17 0.86 0 5 -3 220.98 7.09 0 -5 3 212.43 7.19 0 5 -3 226.18 7.15 0 -5 2 19.29 1.47 0 5 -2 18.54 1.37 0 5 -2 16.46 1.30 0 -5 1 703.18 20.90 0 5 -1 731.50 21.02 0 5 0 46.24 2.05 0 -5 0 46.62 2.03 0 5 1 5.94 1.11 0 -5 -1 4.73 0.85 0 5 1 6.56 0.88 0 5 2 529.29 15.62 0 5 2 532.19 16.10 0 -5 -2 527.85 15.75 0 -5 -3 113.42 3.98 0 5 3 107.53 3.78 0 5 3 113.83 4.36 0 -5 -4 265.25 8.02 0 5 4 257.61 8.41 0 5 5 31.49 2.22 0 -5 -5 33.94 1.92 0 5 5 30.68 1.91 0 5 6 11.61 1.64 0 5 6 10.27 1.33 0 -5 -6 11.10 1.32 0 5 7 386.58 12.35 0 5 7 368.80 11.79 0 -5 -7 382.18 11.85 0 5 8 53.67 3.21 0 5 8 56.05 2.64 0 -5 -8 57.61 2.82 0 5 8 57.08 2.74 0 -5 -9 22.37 1.93 0 5 9 23.57 1.68 0 5 9 19.75 2.16 0 5 9 22.40 1.78 0 5 10 7.08 1.40 0 5 10 8.07 1.98 0 -5 -10 11.23 1.57 0 5 10 8.99 1.38 0 -5 -11 74.31 3.73 0 5 11 80.05 4.24 0 5 11 82.53 3.51 0 5 12 55.50 2.90 0 5 12 55.91 3.73 0 -6 14 30.75 2.59 0 6 -14 28.63 1.92 0 -6 13 43.97 2.82 0 6 -13 35.87 2.11 0 6 -12 36.00 1.38 0 -6 12 37.29 2.56 0 -6 11 2.92 1.43 0 6 -11 3.04 0.67 0 6 -11 2.88 0.97 0 -6 10 36.68 2.45 0 6 -10 36.83 2.03 0 6 -9 14.38 1.31 0 -6 9 11.70 1.51 0 -6 8 0.25 1.14 0 6 -8 -0.58 0.91 0 6 -7 89.04 3.48 0 6 -7 86.97 3.72 0 -6 7 86.38 3.69 0 6 -6 362.92 11.12 0 6 -6 358.08 11.35 0 -6 6 352.79 11.37 0 6 -5 1.41 0.87 0 -6 5 1.41 1.05 0 6 -5 1.02 0.95 0 6 -4 259.13 8.34 0 6 -4 263.44 8.31 0 -6 4 245.26 8.41 0 -6 3 3.84 1.15 0 6 -3 2.57 0.98 0 6 -3 3.11 0.99 0 6 -2 105.45 3.95 0 6 -2 102.21 4.05 0 -6 2 111.03 4.26 0 6 -1 189.49 6.29 0 -6 1 190.48 6.20 0 -6 0 201.54 6.48 0 6 0 195.40 6.51 0 6 1 436.81 13.02 0 6 1 422.98 13.41 0 -6 -1 428.66 13.05 0 6 2 13.72 1.20 0 6 2 14.71 1.52 0 -6 -2 16.02 1.30 0 6 2 16.34 1.67 0 -6 -3 33.24 1.90 0 6 3 30.33 1.64 0 6 3 28.02 1.96 0 6 3 29.74 2.20 0 6 4 16.22 1.19 0 -6 -4 15.54 1.42 0 6 4 12.74 1.80 0 6 4 12.97 1.49 0 6 5 66.98 3.01 0 -6 -5 59.85 2.89 0 6 5 60.88 3.28 0 6 6 352.50 11.52 0 -6 -6 342.49 10.99 0 6 6 346.48 11.06 0 6 7 322.20 11.13 0 6 7 331.55 10.66 0 -6 -7 335.58 10.66 0 6 8 3.15 1.20 0 -6 -8 2.28 1.30 0 6 8 3.44 1.72 0 6 8 3.33 1.10 0 6 9 17.38 1.67 0 -6 -9 19.32 1.89 0 6 9 22.06 2.33 0 6 9 19.65 1.80 0 6 10 71.67 4.05 0 6 10 74.22 3.55 0 6 10 78.42 3.43 0 -6 -10 68.71 3.55 0 6 11 35.68 3.12 0 6 11 37.49 2.42 0 7 -14 6.04 1.36 0 -7 14 6.42 1.97 0 -7 13 82.65 4.23 0 7 -13 98.48 3.84 0 -7 12 1.18 1.45 0 7 -12 2.36 1.12 0 7 -11 8.09 1.30 0 7 -11 6.40 1.68 0 -7 11 7.31 1.59 0 7 -10 14.79 1.50 0 7 -10 11.27 1.67 0 -7 10 15.09 1.88 0 -7 9 42.17 2.78 0 7 -9 48.15 2.44 0 7 -9 45.31 2.70 0 7 -8 38.15 2.51 0 -7 8 45.46 2.75 0 7 -8 45.17 2.39 0 7 -7 87.03 3.63 0 -7 7 87.06 3.92 0 7 -7 95.26 4.02 0 7 -6 14.28 1.51 0 -7 6 14.80 1.72 0 7 -6 15.79 1.72 0 7 -5 1.95 1.31 0 7 -5 0.24 1.05 0 -7 5 -0.70 1.26 0 7 -4 70.80 3.24 0 -7 4 67.95 3.34 0 7 -4 74.48 3.24 0 7 -3 3.40 1.20 0 7 -3 3.58 1.16 0 -7 3 2.68 1.27 0 -7 2 77.68 3.47 0 7 -2 70.32 3.13 0 7 -2 67.90 3.25 0 -7 1 6.35 1.08 0 7 -1 6.10 1.18 0 7 0 0.93 0.91 0 7 0 0.84 1.19 0 -7 0 0.95 0.94 0 -7 -1 10.38 1.24 0 7 1 10.86 1.63 0 7 1 11.36 1.63 0 7 1 9.54 1.21 0 7 2 18.70 1.46 0 7 2 19.38 1.84 0 7 2 19.60 2.00 0 -7 -2 22.11 1.64 0 7 3 144.05 4.91 0 7 3 150.01 5.73 0 -7 -3 136.30 5.12 0 7 3 141.03 5.39 0 7 4 24.99 1.98 0 -7 -4 19.07 1.68 0 7 4 23.41 2.16 0 7 4 22.00 1.45 0 7 5 14.14 2.00 0 7 5 12.61 1.59 0 -7 -5 13.14 1.48 0 7 6 1.95 1.25 0 -7 -6 1.88 1.20 0 7 6 0.77 1.64 0 7 7 6.70 2.01 0 7 7 7.85 1.49 0 -7 -7 6.46 1.45 0 7 8 12.45 1.62 0 7 8 11.97 1.61 0 -7 -8 13.60 1.74 0 7 8 8.53 1.94 0 -7 -8 12.30 2.42 0 7 9 2.02 2.01 0 -7 -9 4.90 1.61 0 7 10 23.64 2.06 0 8 -14 43.02 2.51 0 -8 13 16.69 2.37 0 8 -13 18.20 1.70 0 8 -12 5.79 1.78 0 8 -12 3.76 1.26 0 -8 12 5.52 1.75 0 8 -11 1.18 1.69 0 -8 11 0.55 1.52 0 8 -11 1.11 1.23 0 8 -10 36.49 2.26 0 8 -10 34.51 2.64 0 -8 10 33.28 2.60 0 8 -9 25.81 2.23 0 8 -9 23.92 1.86 0 -8 9 24.75 2.33 0 8 -8 33.53 2.56 0 -8 8 36.70 2.57 0 8 -8 34.12 2.25 0 8 -7 21.92 2.12 0 8 -7 28.84 2.00 0 -8 7 23.45 2.28 0 -8 6 8.16 1.66 0 8 -6 7.46 1.55 0 8 -6 9.35 1.54 0 8 -5 6.46 1.50 0 -8 5 4.27 1.51 0 8 -5 5.23 1.51 0 8 -4 26.80 2.06 0 8 -4 24.99 2.08 0 -8 4 25.87 2.19 0 8 -3 56.10 2.97 0 8 -3 58.08 2.95 0 -8 3 57.38 3.18 0 -8 2 50.61 2.90 0 8 -2 45.41 2.76 0 8 -2 47.93 2.61 0 -8 1 35.64 2.06 0 8 -1 37.23 2.15 0 8 -1 33.86 2.49 0 8 0 12.04 1.48 0 -8 0 9.56 1.36 0 8 0 11.09 1.77 0 8 1 454.24 13.79 0 8 1 445.13 14.33 0 -8 -1 446.70 13.80 0 8 1 445.77 14.25 0 8 2 36.12 2.50 0 8 2 41.89 2.76 0 8 2 36.82 2.07 0 -8 -2 38.44 2.29 0 8 3 28.15 2.42 0 -8 -3 27.72 1.93 0 8 3 27.90 1.75 0 8 3 27.27 2.15 0 8 4 40.30 2.57 0 8 4 40.16 2.02 0 -8 -4 39.33 2.35 0 8 4 40.37 2.93 0 8 5 4.14 1.79 0 8 5 3.05 1.37 0 -8 -5 6.35 1.34 0 8 6 2.17 1.72 0 8 6 1.70 1.28 0 -8 -6 1.51 1.25 0 8 7 0.23 1.91 0 -8 -7 3.36 2.16 0 8 7 0.31 1.38 0 -8 -7 1.30 1.38 0 8 8 3.31 2.15 0 8 8 2.80 1.38 0 9 -13 19.53 1.97 0 -9 13 18.74 2.57 0 9 -12 3.54 1.34 0 -9 12 2.53 1.92 0 9 -11 4.12 1.81 0 -9 11 1.24 1.70 0 9 -11 2.61 1.38 0 9 -10 24.97 2.57 0 -9 10 21.14 2.40 0 9 -10 21.83 2.00 0 -9 9 28.54 2.68 0 9 -9 28.78 2.23 0 9 -9 32.00 2.67 0 9 -8 190.99 7.45 0 -9 8 208.02 7.67 0 9 -8 197.66 7.04 0 9 -7 76.85 3.58 0 9 -7 72.67 3.80 0 -9 7 70.89 3.90 0 -9 6 12.46 1.94 0 9 -6 14.07 1.82 0 9 -6 14.98 1.88 0 9 -5 2.75 1.37 0 -9 5 0.37 1.51 0 9 -5 -0.16 1.34 0 9 -4 138.66 5.62 0 9 -4 149.10 5.70 0 -9 4 150.76 6.02 0 9 -3 171.53 6.35 0 9 -3 166.38 6.12 0 9 -3 149.95 6.45 0 -9 3 166.41 6.48 0 -9 2 2.29 1.63 0 9 -2 1.16 1.61 0 9 -2 -2.67 1.45 0 9 -2 1.42 1.27 0 9 -1 2.22 1.51 0 9 -1 0.81 1.24 0 -9 0 16.75 1.62 0 9 0 21.25 2.10 0 9 0 17.03 1.64 0 -9 -1 1.77 1.18 0 9 1 -1.42 1.58 0 -9 -1 -1.46 1.89 0 9 1 1.19 1.07 0 9 1 0.94 1.55 0 9 2 189.56 7.07 0 9 2 188.11 6.84 0 9 2 171.79 6.17 0 -9 -2 175.62 6.33 0 9 3 51.67 2.52 0 9 3 49.97 3.04 0 9 3 50.83 3.27 0 -9 -3 57.98 2.82 0 9 4 1.52 1.83 0 9 4 2.72 1.01 0 -9 -4 1.20 1.24 0 9 4 1.18 1.45 0 -9 -5 3.76 1.46 0 9 5 7.02 2.05 0 -9 -5 8.08 2.40 0 9 5 5.71 1.49 0 9 6 12.49 2.44 0 -10 11 7.86 2.27 0 10 -11 3.64 1.58 0 -10 10 2.74 1.93 0 10 -10 2.03 1.50 0 10 -10 3.63 2.03 0 10 -9 5.00 1.91 0 -10 9 3.59 2.12 0 10 -9 4.30 1.63 0 10 -8 28.29 2.38 0 -10 8 32.41 2.96 0 10 -8 33.34 2.77 0 -10 7 73.46 4.11 0 10 -7 77.41 4.13 0 10 -7 82.99 3.85 0 10 -6 0.56 1.51 0 -10 6 1.06 1.70 0 10 -6 3.72 1.66 0 10 -6 2.90 2.07 0 10 -5 57.19 3.32 0 10 -5 53.45 3.68 0 10 -5 59.86 3.25 0 -10 5 57.10 3.45 0 -10 4 2.10 1.63 0 10 -4 -1.14 1.90 0 10 -4 1.77 1.58 0 10 -4 0.34 1.46 0 -10 3 1.70 1.72 0 10 -3 1.14 1.42 0 10 -3 -0.37 1.57 0 10 -3 1.32 1.84 0 10 -2 127.07 5.18 0 -10 2 126.01 5.67 0 10 -2 127.04 5.66 0 10 -2 140.46 5.64 0 10 -1 78.99 4.10 0 10 -1 74.38 3.57 0 10 0 0.60 1.68 0 10 0 -0.14 1.23 0 10 1 76.77 3.46 0 -10 -1 71.88 3.37 0 10 1 77.69 4.14 0 10 1 81.38 4.06 0 10 2 31.75 2.14 0 -10 -2 33.36 2.21 0 10 2 37.18 2.93 0 10 2 31.42 2.57 0 10 3 47.47 2.50 0 10 3 44.80 3.04 0 -10 -3 54.82 2.81 0 -10 -3 50.61 3.71 0 10 3 46.59 3.35 0 -11 9 66.63 4.22 0 -11 8 1.93 2.01 0 11 -8 1.79 1.97 0 11 -8 1.60 1.54 0 11 -7 3.41 1.97 0 -11 7 6.18 2.14 0 11 -7 5.43 2.30 0 11 -7 4.51 1.76 0 11 -6 111.65 5.11 0 11 -6 113.09 4.91 0 -11 6 107.26 5.30 0 11 -6 104.60 5.47 0 11 -5 36.58 2.73 0 11 -5 34.61 3.17 0 -11 5 31.54 3.00 0 11 -5 35.39 2.75 0 -11 4 10.86 2.22 0 11 -4 5.70 1.88 0 11 -4 14.15 2.51 0 11 -4 9.98 1.98 0 11 -3 84.28 4.39 0 -11 3 86.65 4.65 0 11 -3 88.40 4.25 0 11 -3 91.99 4.76 0 11 -2 199.56 7.85 0 11 -2 188.38 7.52 0 11 -2 202.57 7.32 0 -11 2 195.60 7.88 0 11 -1 1.75 1.54 0 11 -1 1.57 1.80 0 11 0 101.09 4.82 0 11 0 89.23 4.07 0 11 1 117.33 4.69 0 12 -6 13.46 2.33 0 12 -5 53.24 3.50 0 12 -4 16.48 2.29 0 12 -3 70.10 3.81 0 12 -2 47.07 3.13 -1 12 0 -1.77 1.69 -1 12 -1 6.57 1.89 -1 12 -2 1.58 1.75 -1 12 -3 10.31 2.11 -1 12 -4 3.00 1.92 -1 12 -5 182.69 7.41 1 -11 -3 -0.17 1.55 -1 11 3 0.28 1.39 1 -11 -2 32.30 2.44 -1 11 2 33.15 2.42 -1 11 1 12.24 2.16 -1 11 1 11.99 1.76 1 -11 -1 16.39 2.70 1 -11 -1 12.06 1.78 1 -11 0 7.76 1.64 1 -11 0 10.53 2.36 -1 11 0 11.31 2.02 -1 11 0 11.75 2.14 1 -11 0 12.13 2.29 -1 11 0 10.72 1.87 -1 11 -1 -0.21 1.77 -1 11 -1 1.32 1.71 1 -11 1 -1.01 2.07 -1 11 -1 0.53 1.58 -1 11 -2 36.40 2.97 -1 11 -2 34.62 2.69 1 -11 3 11.88 2.30 -1 11 -3 11.69 2.06 -1 11 -3 10.63 2.25 1 -11 4 178.59 7.25 -1 11 -4 180.00 6.87 -1 11 -4 172.77 7.31 -1 11 -4 171.13 6.88 -1 11 -5 12.19 1.95 -1 11 -5 12.03 2.37 1 -11 5 18.50 2.48 -1 11 -5 13.16 2.12 -1 11 -6 1.04 2.09 -1 11 -6 4.12 1.94 -1 11 -6 3.29 1.76 1 -11 6 3.60 2.06 1 -11 7 40.96 3.29 -1 11 -7 37.40 3.30 -1 11 -7 41.28 2.91 -1 11 -7 40.15 3.18 1 -11 8 7.45 2.41 -1 11 -8 6.41 2.16 1 -10 -5 49.61 3.13 -1 10 4 9.14 2.21 -1 10 4 12.06 1.96 -1 10 4 7.92 1.42 1 -10 -4 8.43 2.33 1 -10 -4 8.14 1.74 -1 10 3 82.27 4.18 -1 10 3 68.47 3.40 -1 10 3 82.61 3.98 1 -10 -3 80.81 4.65 -1 10 2 32.33 2.58 -1 10 2 38.18 2.79 1 -10 -2 36.67 2.50 1 -10 -2 37.50 3.15 -1 10 2 35.01 2.33 1 -10 -1 30.32 2.97 -1 10 1 32.59 2.65 1 -10 -1 30.10 2.22 1 -10 -1 31.81 2.76 -1 10 1 32.33 2.29 -1 10 1 30.22 2.51 1 -10 0 9.36 1.62 -1 10 0 8.01 1.83 1 -10 0 6.09 2.06 -1 10 0 11.27 1.96 1 -10 0 6.86 1.98 -1 10 0 6.90 1.59 -1 10 -1 44.22 3.01 -1 10 -1 45.19 2.75 1 -10 1 40.54 2.56 -1 10 -1 38.30 2.87 1 -10 1 41.19 3.20 -1 10 -2 20.04 2.13 -1 10 -2 14.60 2.18 1 -10 3 12.25 1.97 -1 10 -3 11.15 1.87 -1 10 -3 12.83 2.13 1 -10 4 82.44 4.41 -1 10 -4 86.19 4.15 -1 10 -4 95.26 4.66 -1 10 -4 88.37 4.21 1 -10 5 392.43 13.46 -1 10 -5 404.92 13.59 -1 10 -5 394.55 13.20 -1 10 -5 404.99 13.04 -1 10 -6 48.75 3.20 -1 10 -6 47.78 3.43 -1 10 -6 53.77 3.03 1 -10 6 50.78 3.49 -1 10 -7 1.26 1.64 -1 10 -7 2.64 1.53 1 -10 7 1.33 1.97 -1 10 -7 -0.96 1.58 -1 10 -7 0.24 1.90 -1 10 -8 8.94 1.65 1 -10 8 9.59 2.07 -1 10 -8 6.83 2.00 -1 10 -8 6.97 1.87 -1 10 -8 10.39 2.38 -1 10 -9 109.84 5.18 -1 10 -9 126.13 5.67 -1 10 -9 133.24 6.09 1 -10 9 126.69 5.70 -1 10 -9 125.29 5.11 1 -10 10 26.95 2.88 -1 10 -10 27.89 2.33 1 -9 -7 21.58 2.34 -1 9 7 26.25 2.80 -1 9 6 7.46 1.74 1 -9 -6 5.38 1.69 -1 9 6 4.80 2.07 1 -9 -6 9.43 2.25 1 -9 -5 10.74 2.36 1 -9 -5 9.68 1.70 -1 9 5 11.82 1.75 -1 9 5 10.45 2.00 1 -9 -4 124.29 5.86 -1 9 4 125.26 5.62 1 -9 -4 134.03 5.34 -1 9 4 130.42 4.92 -1 9 3 0.13 1.13 -1 9 3 0.17 1.42 -1 9 3 1.54 1.58 1 -9 -3 2.45 1.80 1 -9 -3 -0.46 1.35 1 -9 -2 12.66 2.22 -1 9 2 17.94 1.70 -1 9 2 12.70 1.92 -1 9 2 17.25 1.94 1 -9 -2 13.97 1.81 1 -9 -2 12.80 2.10 -1 9 1 314.19 10.39 -1 9 1 309.73 10.40 1 -9 -1 313.53 10.89 1 -9 -1 290.60 10.03 1 -9 -1 304.64 10.61 -1 9 1 302.17 9.98 1 -9 0 56.89 3.32 1 -9 0 45.87 2.73 -1 9 0 46.61 2.95 1 -9 0 48.68 3.33 -1 9 0 52.81 2.86 -1 9 0 49.14 3.00 -1 9 -1 16.92 1.95 -1 9 -1 15.57 2.06 1 -9 1 15.44 1.69 1 -9 1 16.51 2.16 -1 9 -1 19.71 1.86 -1 9 -2 8.10 1.64 -1 9 -2 6.92 1.76 -1 9 -3 164.71 6.58 -1 9 -3 166.53 6.30 1 -9 3 172.75 6.63 -1 9 -4 9.35 1.63 -1 9 -4 6.80 1.86 1 -9 4 9.63 1.91 -1 9 -4 8.21 1.66 -1 9 -5 55.64 3.44 1 -9 5 54.37 3.31 -1 9 -5 56.85 3.21 -1 9 -5 59.19 3.10 -1 9 -6 4.61 1.39 -1 9 -6 3.30 1.62 1 -9 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10.63 -1 8 3 316.78 10.87 -1 8 2 78.50 3.65 1 -8 -2 68.92 3.69 -1 8 2 68.40 3.19 1 -8 -2 71.16 3.37 1 -8 -2 71.19 3.82 -1 8 2 70.64 3.50 1 -8 -1 36.04 2.33 -1 8 1 38.02 2.50 1 -8 -1 34.66 2.70 -1 8 1 40.83 2.33 1 -8 -1 38.22 2.66 -1 8 1 42.19 2.64 1 -8 0 34.99 2.51 -1 8 0 32.78 2.41 -1 8 0 37.48 2.32 -1 8 0 35.36 2.40 1 -8 0 41.14 2.78 1 -8 0 32.08 2.21 1 -8 1 458.31 14.53 -1 8 -1 466.97 14.74 -1 8 -1 477.05 14.66 1 -8 1 469.01 15.08 -1 8 -1 481.12 14.97 1 -8 2 299.43 10.03 -1 8 -2 315.97 10.25 -1 8 -2 324.73 10.54 -1 8 -3 334.02 11.06 -1 8 -3 320.32 10.72 1 -8 3 335.54 11.04 -1 8 -4 130.28 5.34 -1 8 -4 121.17 5.02 1 -8 4 128.75 5.26 -1 8 -4 127.44 4.95 -1 8 -5 18.43 1.78 -1 8 -5 20.14 1.99 1 -8 5 19.57 2.08 -1 8 -5 17.99 2.17 -1 8 -6 106.84 4.34 -1 8 -6 105.83 4.64 -1 8 -6 108.70 4.95 1 -8 6 104.63 4.67 -1 8 -7 214.53 7.55 -1 8 -7 204.74 7.66 -1 8 -7 212.91 7.31 -1 8 -7 222.64 8.07 1 -8 7 199.97 7.62 -1 8 -8 44.85 2.85 -1 8 -8 38.37 2.51 -1 8 -8 37.45 2.34 1 -8 8 40.85 2.74 -1 8 -8 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2.21 2 -8 -1 19.41 1.95 -2 8 1 15.59 1.83 2 -8 -1 21.59 2.19 -2 8 1 19.78 1.90 2 -8 0 63.06 3.37 2 -8 0 60.82 3.41 -2 8 0 62.71 3.20 -2 8 0 63.76 3.21 -2 8 0 62.77 3.21 2 -8 0 57.58 3.19 -2 8 -1 6.56 1.58 -2 8 -1 7.05 1.54 2 -8 1 6.42 1.62 -2 8 -1 8.63 1.49 2 -8 1 5.56 1.52 2 -8 1 6.97 1.68 2 -8 2 286.09 9.41 -2 8 -2 288.98 9.41 -2 8 -2 291.97 9.62 -2 8 -2 275.63 9.53 2 -8 2 261.14 9.60 -2 8 -3 329.71 10.76 2 -8 3 319.99 10.41 -2 8 -3 308.35 10.56 -2 8 -4 340.94 11.32 -2 8 -4 344.60 11.42 -2 8 -5 207.90 7.15 -2 8 -5 204.90 7.48 2 -8 5 193.53 7.48 -2 8 -5 213.97 7.70 2 -8 6 3.97 1.45 -2 8 -6 6.71 1.64 -2 8 -6 4.94 1.51 -2 8 -6 4.60 1.38 -2 8 -6 6.39 1.68 2 -8 7 33.69 2.58 -2 8 -7 34.35 2.22 -2 8 -7 37.15 2.71 -2 8 -7 29.99 2.25 -2 8 -7 32.39 2.70 -2 8 -8 46.62 2.75 -2 8 -8 41.31 3.12 2 -8 8 47.84 3.00 -2 8 -8 43.76 2.55 -2 8 -9 12.84 2.12 2 -8 9 15.33 2.02 -2 8 -9 10.95 1.57 -2 8 -9 13.01 1.64 -2 8 -10 25.05 1.97 -2 8 -10 23.70 2.54 2 -8 10 27.02 2.47 -2 8 -10 26.71 2.10 2 -8 11 73.59 3.92 -2 8 -11 73.65 3.42 -2 8 -11 67.04 3.01 -2 8 -11 63.94 3.38 -2 8 -12 17.10 1.79 2 -8 12 21.31 2.57 -2 7 10 12.91 2.11 -2 7 10 15.73 1.62 2 -7 -10 12.62 2.24 2 -7 -9 8.66 2.14 -2 7 9 8.29 1.93 -2 7 9 8.21 1.50 -2 7 9 8.52 1.44 2 -7 -9 7.72 1.89 2 -7 -8 47.94 3.32 -2 7 8 45.92 2.54 2 -7 -8 44.69 2.96 2 -7 -7 24.49 2.36 -2 7 7 25.87 2.34 2 -7 -7 25.67 2.50 -2 7 7 25.95 1.99 2 -7 -6 266.92 9.23 2 -7 -6 261.87 9.39 -2 7 6 252.99 9.07 -2 7 6 276.33 8.85 -2 7 5 562.59 17.76 2 -7 -5 569.32 17.83 2 -7 -5 571.17 18.09 -2 7 5 587.65 17.54 -2 7 5 577.56 17.42 2 -7 -4 307.73 10.49 -2 7 4 305.68 9.93 -2 7 4 316.56 10.05 -2 7 4 312.00 10.23 2 -7 -4 301.40 10.25 -2 7 3 56.45 2.96 2 -7 -3 57.36 3.17 2 -7 -3 55.26 3.16 2 -7 -3 53.37 2.99 -2 7 3 59.66 2.85 -2 7 3 62.35 2.94 -2 7 2 1.98 1.16 2 -7 -2 3.92 1.28 -2 7 2 0.63 1.17 2 -7 -2 2.71 1.46 -2 7 2 2.97 1.25 2 -7 -2 4.99 1.47 2 -7 -1 18.67 1.88 -2 7 1 19.10 1.74 2 -7 -1 19.25 1.95 2 -7 -1 22.67 1.88 -2 7 1 20.36 1.81 -2 7 1 22.94 1.87 -2 7 0 95.73 4.05 2 -7 0 99.75 4.16 -2 7 0 102.44 4.16 -2 7 0 99.79 4.13 2 -7 0 102.39 4.37 2 -7 0 99.78 4.31 -2 7 -1 359.85 11.30 -2 7 -1 352.83 11.41 -2 7 -1 354.73 11.39 2 -7 1 347.90 11.35 2 -7 1 366.46 11.55 2 -7 1 348.82 11.53 -2 7 -2 642.53 19.65 -2 7 -2 636.24 19.67 2 -7 2 631.12 19.56 -2 7 -2 675.86 19.55 -2 7 -3 78.16 3.57 2 -7 3 76.70 3.41 -2 7 -3 76.68 3.61 -2 7 -4 1.47 1.21 -2 7 -4 1.98 1.33 -2 7 -5 5.19 1.40 -2 7 -5 8.28 1.68 2 -7 5 6.60 1.44 -2 7 -5 6.47 1.29 -2 7 -6 143.65 5.24 -2 7 -6 143.12 5.72 -2 7 -6 142.71 5.38 2 -7 6 136.64 5.50 2 -7 7 0.31 1.29 -2 7 -7 -0.18 1.61 -2 7 -7 1.19 1.11 -2 7 -7 -0.52 1.20 2 -7 8 163.78 6.34 -2 7 -8 162.57 5.91 -2 7 -8 174.63 6.07 -2 7 -9 118.60 4.57 -2 7 -9 105.61 5.00 -2 7 -9 119.22 4.62 2 -7 9 124.95 5.09 -2 7 -10 80.88 3.28 -2 7 -10 75.52 3.55 -2 7 -10 84.88 4.20 -2 7 -10 87.84 3.62 2 -7 10 87.09 4.12 -2 7 -11 2.29 1.32 -2 7 -11 4.06 0.98 2 -7 11 2.88 1.63 -2 7 -11 2.50 1.24 -2 7 -11 3.05 1.63 2 -7 12 52.91 3.42 -2 7 -12 61.78 3.64 -2 7 -12 55.22 2.89 -2 7 -12 58.97 3.03 -2 7 -13 -0.27 1.22 2 -7 13 -0.80 1.78 -2 6 11 66.39 2.97 2 -6 -11 56.06 3.52 2 -6 -10 59.91 3.61 -2 6 10 52.62 3.24 -2 6 10 52.88 2.83 -2 6 10 58.91 2.72 2 -6 -10 57.89 3.44 2 -6 -9 21.58 2.30 -2 6 9 19.89 1.61 -2 6 9 25.61 2.29 -2 6 9 19.47 1.76 2 -6 -9 15.56 2.20 2 -6 -8 1.34 1.41 -2 6 8 1.29 1.43 2 -6 -8 1.12 1.48 -2 6 8 0.83 1.10 2 -6 -7 231.81 8.13 -2 6 7 227.82 7.61 2 -6 -7 224.20 8.18 -2 6 7 226.76 7.98 2 -6 -6 108.45 4.73 2 -6 -6 104.40 4.57 -2 6 6 109.90 4.24 -2 6 6 113.67 4.56 2 -6 -5 93.44 4.15 2 -6 -5 97.44 4.25 -2 6 5 98.47 3.81 -2 6 5 92.35 3.71 -2 6 5 90.57 3.94 2 -6 -4 83.29 3.85 2 -6 -4 86.11 3.82 -2 6 4 88.82 3.55 2 -6 -4 86.36 3.79 -2 6 4 82.92 3.66 -2 6 4 85.35 3.50 -2 6 3 1.20 1.19 -2 6 3 0.45 0.96 2 -6 -3 0.27 1.18 -2 6 3 1.22 0.98 2 -6 -3 0.14 1.27 2 -6 -3 1.82 1.17 -2 6 2 120.51 4.47 2 -6 -2 122.22 4.68 2 -6 -2 122.33 4.75 -2 6 2 111.42 4.44 2 -6 -2 122.69 4.69 -2 6 2 113.03 4.45 2 -6 -1 102.44 4.12 -2 6 1 95.71 3.91 2 -6 -1 100.08 4.05 -2 6 1 101.31 4.00 2 -6 -1 98.29 4.09 -2 6 1 103.45 3.98 2 -6 0 112.70 4.48 -2 6 0 110.80 4.34 2 -6 0 114.85 4.45 2 -6 0 115.80 4.49 -2 6 0 117.72 4.43 -2 6 0 112.57 4.31 -2 6 -1 22.34 1.61 2 -6 1 19.44 1.63 2 -6 1 20.77 1.71 2 -6 1 19.03 1.68 -2 6 -1 21.28 1.69 -2 6 -1 24.40 1.73 2 -6 2 6.05 1.21 -2 6 -2 8.98 1.37 -2 6 -2 7.36 1.26 -2 6 -2 9.35 1.18 -2 6 -3 910.49 26.11 2 -6 3 875.93 25.95 -2 6 -3 850.24 26.05 -2 6 -4 254.60 8.56 2 -6 5 8.12 1.35 -2 6 -5 6.23 1.08 -2 6 -5 5.46 1.30 -2 6 -5 7.27 1.29 -2 6 -6 51.41 2.47 2 -6 6 51.61 2.76 -2 6 -6 50.56 2.53 -2 6 -6 51.22 2.86 -2 6 -7 0.62 0.93 -2 6 -7 0.44 1.05 2 -6 7 0.54 1.25 -2 6 -8 19.40 2.01 -2 6 -8 20.02 1.58 2 -6 8 20.21 1.86 -2 6 -8 23.40 1.67 -2 6 -9 26.33 1.62 -2 6 -9 28.66 1.85 -2 6 -9 26.48 1.90 2 -6 9 28.26 2.17 -2 6 -9 29.16 2.32 -2 6 -10 323.87 10.84 2 -6 10 328.83 10.68 -2 6 -10 314.27 9.89 -2 6 -10 314.24 10.22 -2 6 -10 327.64 10.27 -2 6 -11 372.83 11.57 -2 6 -11 386.18 12.03 -2 6 -11 387.32 12.08 2 -6 11 395.15 12.53 -2 6 -11 377.96 12.67 -2 6 -12 35.88 2.22 -2 6 -12 35.57 2.23 2 -6 12 35.25 2.70 -2 6 -12 36.89 2.79 -2 6 -12 36.24 1.75 -2 6 -13 17.69 1.70 -2 6 -13 18.02 1.81 -2 6 -13 16.99 2.28 2 -6 13 16.74 2.24 -2 6 -14 32.70 2.27 2 -6 14 29.73 2.64 2 -5 -12 12.09 2.10 2 -5 -11 66.08 3.80 -2 5 11 81.82 3.49 -2 5 11 72.08 3.71 -2 5 11 76.45 3.18 2 -5 -11 73.05 4.01 2 -5 -10 17.04 2.09 2 -5 -10 20.02 2.28 -2 5 10 16.09 1.89 -2 5 10 21.75 1.78 -2 5 10 24.09 1.62 -2 5 9 137.07 4.81 2 -5 -9 142.77 5.65 2 -5 -9 132.90 5.46 -2 5 9 137.35 5.00 -2 5 9 135.23 5.36 2 -5 -8 59.30 3.23 -2 5 8 60.00 2.79 -2 5 8 65.07 3.16 2 -5 -8 57.47 3.22 -2 5 7 81.98 3.57 2 -5 -7 83.96 3.65 -2 5 7 75.57 3.19 2 -5 -7 73.69 3.67 2 -5 -6 27.70 2.10 -2 5 6 25.83 2.00 2 -5 -6 27.79 2.04 -2 5 6 32.34 1.83 2 -5 -5 -0.26 1.15 -2 5 5 0.09 0.88 -2 5 5 0.58 0.96 2 -5 -5 1.52 1.14 -2 5 5 1.37 1.02 2 -5 -4 107.85 4.38 2 -5 -4 113.91 4.45 2 -5 -4 112.29 4.39 -2 5 4 116.26 4.22 -2 5 4 112.46 4.12 -2 5 4 115.29 4.28 -2 5 3 0.28 0.84 2 -5 -3 0.47 0.96 2 -5 -3 1.33 0.98 -2 5 3 -0.20 0.89 2 -5 -3 1.17 1.06 -2 5 3 0.60 0.94 2 -5 -2 2.34 1.10 2 -5 -2 2.18 1.04 -2 5 2 2.92 0.86 -2 5 2 2.12 0.88 -2 5 2 1.21 0.88 2 -5 -2 2.34 1.02 2 -5 -1 55.24 2.66 -2 5 1 55.11 2.51 2 -5 -1 53.77 2.62 2 -5 -1 57.80 2.68 -2 5 1 58.70 2.54 -2 5 1 59.76 2.62 -2 5 0 546.14 16.69 -2 5 0 550.91 16.55 2 -5 0 548.53 16.67 -2 5 0 557.13 16.62 2 -5 0 545.50 16.75 2 -5 0 576.88 16.74 2 -5 1 16.67 1.46 -2 5 -1 19.98 1.38 2 -5 1 16.89 1.39 -2 5 -1 17.93 1.43 2 -5 1 17.79 1.41 -2 5 -1 17.00 1.47 -2 5 -2 60.12 2.64 -2 5 -2 55.36 2.49 2 -5 2 59.63 2.66 -2 5 -3 386.17 10.85 2 -5 3 306.28 10.51 -2 5 -4 4.96 1.09 -2 5 -4 2.21 0.87 -2 5 -5 6.71 1.03 -2 5 -5 6.27 1.00 2 -5 5 7.11 1.15 -2 5 -6 122.70 4.34 -2 5 -6 112.88 4.57 2 -5 6 122.62 4.54 -2 5 -6 119.19 4.27 -2 5 -7 104.15 3.84 -2 5 -7 101.19 3.81 -2 5 -7 98.52 4.14 2 -5 7 106.16 4.11 -2 5 -8 89.15 3.30 -2 5 -8 92.20 3.94 2 -5 8 83.70 3.73 -2 5 -8 89.41 3.53 -2 5 -8 92.30 3.55 -2 5 -9 14.52 1.33 -2 5 -9 16.32 1.67 2 -5 9 13.54 1.63 -2 5 -9 11.77 1.09 -2 5 -9 10.63 1.24 -2 5 -10 176.09 6.02 -2 5 -10 176.89 6.52 2 -5 10 173.12 6.30 -2 5 -10 174.41 6.01 -2 5 -10 171.50 5.64 -2 5 -11 175.43 6.42 -2 5 -11 174.36 5.86 2 -5 11 154.17 6.08 -2 5 -11 160.13 5.31 -2 5 -11 163.51 5.81 -2 5 -12 44.98 2.49 -2 5 -12 50.57 2.61 -2 5 -12 50.10 3.07 2 -5 12 45.36 2.87 -2 5 -13 3.92 1.41 -2 5 -13 2.11 1.65 2 -5 13 2.70 1.62 -2 5 -13 3.80 1.27 -2 5 -14 34.41 2.27 2 -5 14 27.09 2.58 -2 4 12 6.64 1.19 2 -4 -12 3.10 1.74 -2 4 12 5.16 1.33 2 -4 -12 2.76 1.74 -2 4 11 2.23 0.97 2 -4 -11 -0.36 1.49 2 -4 -11 -0.34 1.50 -2 4 11 0.49 1.04 -2 4 11 3.51 1.42 -2 4 10 2.55 0.90 2 -4 -10 3.16 1.49 -2 4 10 3.58 1.33 2 -4 -10 2.67 1.45 -2 4 10 4.27 1.09 -2 4 9 382.16 11.44 2 -4 -9 374.46 12.18 -2 4 9 372.28 11.68 2 -4 -9 375.15 12.16 -2 4 9 375.47 11.95 2 -4 -8 1.25 1.16 -2 4 8 -0.15 0.72 -2 4 8 0.47 0.92 -2 4 8 -0.84 1.16 2 -4 -8 1.22 1.26 2 -4 -7 310.53 9.93 -2 4 7 308.81 9.49 -2 4 7 290.50 9.69 2 -4 -7 307.08 9.90 -2 4 6 18.97 1.51 2 -4 -6 19.55 1.69 -2 4 6 18.53 1.34 2 -4 -6 17.16 1.55 2 -4 -5 210.80 7.11 2 -4 -5 216.06 7.06 -2 4 5 210.59 6.74 -2 4 5 205.27 6.89 2 -4 -4 124.51 4.32 -2 4 4 111.51 4.05 2 -4 -4 117.33 4.33 -2 4 4 119.98 4.22 2 -4 -4 117.46 4.40 -2 4 4 118.49 4.23 2 -4 -3 629.44 19.23 -2 4 3 668.52 19.27 2 -4 -3 665.64 19.43 -2 4 3 670.66 19.11 -2 4 3 635.26 19.14 2 -4 -3 634.24 19.30 2 -4 -2 128.60 4.60 2 -4 -2 130.17 4.60 -2 4 2 132.56 4.47 -2 4 2 128.14 4.57 -2 4 2 128.77 4.45 2 -4 -2 135.73 4.73 2 -4 -1 300.81 9.20 2 -4 -1 279.04 9.07 -2 4 1 297.06 9.04 -2 4 1 285.44 9.15 -2 4 1 292.23 9.03 2 -4 -1 302.84 9.27 2 -4 0 483.41 14.58 2 -4 0 502.62 14.49 2 -4 0 477.13 14.42 -2 4 0 477.93 14.35 -2 4 0 472.37 14.37 2 -4 1 1428.36 39.55 -2 4 -1 1445.81 39.50 -2 4 -1 1389.32 39.55 2 -4 1 1401.41 39.61 -2 4 -2 0.41 0.79 -2 4 -2 0.89 0.71 -2 4 -3 849.76 24.88 -2 4 -4 1.26 0.85 -2 4 -4 1.31 0.73 -2 4 -5 12.05 1.20 -2 4 -5 14.30 1.10 -2 4 -5 10.62 1.00 2 -4 5 13.09 1.18 2 -4 6 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1.00 2 2 10 0.44 0.81 -2 -2 -10 0.73 1.23 2 2 10 0.23 1.02 2 2 10 1.59 1.03 2 2 11 8.13 1.08 2 2 11 7.28 1.33 -2 -2 -11 8.41 1.21 2 2 11 7.15 1.37 -2 -2 -11 8.10 1.57 2 2 12 114.46 4.73 -2 -2 -12 123.73 5.14 2 2 12 116.26 4.68 -2 -2 -12 121.96 4.54 2 2 13 131.92 5.21 -2 -3 14 54.79 3.49 2 3 -14 63.85 3.04 2 3 -13 3.79 1.17 -2 -3 13 4.88 1.72 -2 -3 13 5.85 1.17 2 3 -12 55.19 2.14 -2 -3 12 53.51 2.44 2 3 -12 56.59 2.62 -2 -3 12 56.57 3.17 2 3 -11 36.52 2.04 2 3 -11 39.55 1.63 -2 -3 11 35.47 1.85 -2 -3 11 36.30 2.45 2 3 -10 6.66 0.71 -2 -3 10 6.07 1.37 2 3 -10 9.45 1.16 -2 -3 10 6.08 0.96 2 3 -9 108.18 3.51 2 3 -9 114.22 3.96 -2 -3 9 105.87 3.75 -2 -3 9 107.86 4.31 2 3 -8 327.11 8.99 2 3 -8 330.32 9.42 -2 -3 8 336.01 9.25 2 3 -7 30.02 1.22 -2 -3 7 28.10 1.39 2 3 -7 27.66 1.07 2 3 -7 28.32 1.52 -2 -3 6 1.74 0.61 2 3 -6 3.05 0.52 2 3 -6 2.49 0.71 2 3 -5 886.79 26.08 2 3 -5 914.49 26.39 -2 -3 5 937.88 26.22 -2 -3 4 116.43 3.86 2 3 -4 113.91 3.81 2 3 -4 122.68 4.07 -2 -3 3 163.81 5.19 2 3 -3 160.41 5.42 2 3 -3 164.64 5.21 -2 -3 2 147.78 4.90 2 3 -2 152.44 5.02 2 3 -2 153.16 4.92 2 3 -1 183.81 5.91 -2 -3 1 189.53 5.98 2 3 -1 177.52 5.88 2 3 0 186.21 6.04 2 3 0 188.05 5.95 2 3 0 183.05 5.43 -2 -3 0 193.52 6.08 2 3 1 1382.42 41.83 2 3 1 1466.10 41.69 -2 -3 -1 1510.76 41.85 2 3 2 65.59 2.54 -2 -3 -2 63.63 2.67 -2 -3 -3 975.33 27.87 -2 -3 -3 969.83 28.55 2 3 3 1000.72 28.36 -2 -3 -4 2.22 0.45 2 3 4 2.25 0.71 2 3 4 2.21 0.72 -2 -3 -4 2.04 0.87 -2 -3 -5 43.45 1.71 2 3 5 44.54 2.05 2 3 5 44.49 2.05 -2 -3 -5 45.70 2.32 2 3 6 72.35 2.90 -2 -3 -6 69.91 2.58 -2 -3 -6 71.48 3.17 2 3 6 73.66 2.87 2 3 7 705.28 20.54 2 3 7 700.40 20.49 -2 -3 -7 701.13 20.92 -2 -3 -7 676.88 20.18 2 3 8 1.52 0.97 2 3 8 -0.20 0.88 -2 -3 -8 0.56 1.24 -2 -3 -8 1.83 0.80 2 3 9 3.98 0.99 2 3 9 2.93 1.01 -2 -3 -9 3.02 0.88 -2 -3 -9 3.23 1.40 2 3 9 2.97 1.05 2 3 10 23.48 1.76 -2 -3 -10 24.48 1.68 -2 -3 -10 21.35 2.18 2 3 10 26.39 1.85 2 3 10 23.89 1.63 2 3 11 284.74 9.11 -2 -3 -11 263.46 8.84 2 3 11 264.23 8.76 2 3 11 292.76 9.17 -2 -3 -11 272.70 9.66 2 3 12 33.69 2.40 2 4 -14 1.18 1.18 2 4 -13 32.98 2.17 -2 -4 13 31.89 2.04 2 4 -12 28.55 1.47 -2 -4 12 28.53 1.80 2 4 -12 31.58 1.90 -2 -4 11 47.31 2.24 2 4 -11 45.07 1.84 2 4 -11 43.09 2.26 -2 -4 10 2.94 0.89 2 4 -10 1.60 0.64 2 4 -10 3.23 0.98 2 4 -9 24.87 0.93 -2 -4 9 24.57 1.53 2 4 -9 26.12 1.65 2 4 -9 25.19 1.28 2 4 -8 211.35 6.63 2 4 -8 226.76 7.08 -2 -4 8 213.62 6.90 -2 -4 7 245.19 7.76 2 4 -7 249.74 7.57 2 4 -7 248.51 7.91 2 4 -6 326.15 10.01 2 4 -6 346.24 10.37 -2 -4 6 335.68 10.20 2 4 -5 680.10 19.60 2 4 -5 666.82 19.86 -2 -4 5 666.25 19.68 -2 -4 4 681.26 20.31 2 4 -4 702.30 20.64 2 4 -4 698.92 20.27 -2 -4 3 548.70 17.00 2 4 -3 601.96 17.29 2 4 -3 585.23 17.02 2 4 -2 40.37 2.04 -2 -4 2 37.25 1.92 -2 -4 2 39.03 1.98 2 4 -2 36.61 1.91 2 4 -1 6.58 1.04 2 4 -1 6.38 1.00 2 4 -1 5.49 0.58 -2 -4 1 7.49 1.13 2 4 0 127.72 4.65 2 4 0 131.95 4.00 2 4 0 123.25 4.52 -2 -4 0 135.76 4.72 -2 -4 -1 11.61 1.31 2 4 1 13.12 0.61 2 4 1 10.99 1.25 2 4 1 13.80 1.20 -2 -4 -2 234.31 7.64 -2 -4 -2 228.15 6.76 2 4 2 241.56 7.45 -2 -4 -3 36.28 1.38 -2 -4 -3 34.29 2.09 2 4 3 38.44 1.91 -2 -4 -4 197.15 6.01 2 4 4 195.65 6.93 -2 -4 -4 187.78 6.76 2 4 4 205.56 6.52 -2 -4 -5 63.42 2.42 2 4 5 66.74 2.80 -2 -4 -5 68.63 3.19 2 4 5 71.27 2.87 2 4 6 116.46 4.27 -2 -4 -6 118.19 4.74 -2 -4 -6 115.60 3.93 2 4 6 115.71 4.28 2 4 7 3.55 1.04 -2 -4 -7 2.39 0.80 -2 -4 -7 1.82 1.36 2 4 7 -0.21 0.93 -2 -4 -8 0.82 1.52 -2 -4 -8 0.08 0.82 2 4 8 -0.44 1.02 2 4 8 1.23 0.98 2 4 9 56.10 2.74 2 4 9 57.67 2.75 -2 -4 -9 55.10 3.23 -2 -4 -9 51.03 2.44 2 4 10 36.24 2.26 2 4 10 38.75 3.06 -2 -4 -10 36.51 2.82 2 4 10 39.47 2.37 2 4 10 40.58 2.18 -2 -4 -10 34.34 2.08 2 4 11 10.09 1.36 2 4 11 14.88 2.55 2 4 11 15.01 1.78 2 4 11 15.19 1.73 2 5 -13 80.10 3.03 -2 -5 13 81.60 3.51 2 5 -13 87.79 3.67 -2 -5 12 12.14 1.40 2 5 -12 12.08 1.05 2 5 -12 13.37 1.52 -2 -5 11 13.03 1.42 2 5 -11 13.74 1.05 2 5 -11 14.98 1.47 -2 -5 10 11.85 1.34 2 5 -10 10.89 1.00 2 5 -10 11.92 0.65 2 5 -9 58.68 2.38 2 5 -9 62.79 2.81 -2 -5 9 58.59 2.69 2 5 -8 159.38 5.56 2 5 -8 156.33 5.18 -2 -5 8 159.02 5.46 2 5 -7 523.48 15.96 2 5 -7 557.36 16.39 -2 -5 7 548.51 16.25 2 5 -6 566.44 17.44 2 5 -6 555.83 17.15 2 5 -6 578.24 16.86 -2 -5 6 571.38 17.01 -2 -5 5 -0.09 0.88 2 5 -5 1.04 1.05 2 5 -5 -0.25 0.79 2 5 -4 54.38 2.65 -2 -5 4 47.68 2.34 2 5 -4 52.50 2.34 2 5 -3 93.27 3.74 2 5 -3 95.77 3.29 -2 -5 3 85.67 3.53 2 5 -3 91.08 3.56 -2 -5 2 9.41 1.29 2 5 -2 9.14 0.85 2 5 -2 9.94 1.20 2 5 -2 9.40 1.34 -2 -5 2 7.16 1.16 2 5 -1 393.85 12.28 -2 -5 1 404.65 12.44 2 5 -1 390.13 11.70 2 5 -1 403.33 12.32 2 5 0 220.08 7.39 -2 -5 0 226.37 7.48 2 5 0 216.09 6.63 2 5 0 218.99 7.27 2 5 1 260.33 8.82 2 5 1 270.48 8.66 2 5 1 267.49 7.88 -2 -5 -1 272.18 8.89 -2 -5 -2 91.13 3.83 -2 -5 -2 85.60 2.80 2 5 2 91.06 3.55 -2 -5 -3 122.98 3.99 -2 -5 -3 121.75 4.92 2 5 4 62.46 3.36 -2 -5 -4 69.72 3.35 2 5 4 71.42 3.00 -2 -5 -4 67.97 2.45 -2 -5 -5 296.78 9.11 -2 -5 -5 300.48 10.10 2 5 5 289.12 10.11 2 5 5 312.20 9.66 2 5 5 308.38 9.58 2 5 6 204.82 6.84 -2 -5 -6 202.42 6.46 2 5 6 197.15 7.46 -2 -5 -6 196.16 7.34 2 5 6 209.43 6.90 2 5 7 24.20 1.79 2 5 7 30.06 2.51 -2 -5 -7 24.24 1.55 -2 -5 -7 23.01 2.19 2 5 7 30.77 1.94 2 5 8 13.28 1.49 2 5 8 14.12 1.56 -2 -5 -8 17.14 2.23 2 5 8 15.49 2.09 -2 -5 -8 12.15 1.28 2 5 9 5.62 1.28 -2 -5 -9 2.14 1.05 -2 -5 -9 5.65 1.76 2 5 9 4.13 1.87 2 5 9 2.34 1.20 2 5 10 4.53 1.37 -2 -5 -10 6.28 1.88 2 5 10 4.78 1.43 2 5 10 2.54 1.89 -2 -6 13 12.58 1.66 2 6 -13 11.73 1.18 2 6 -13 12.09 1.59 -2 -6 12 7.04 1.40 2 6 -12 7.14 0.99 2 6 -12 6.88 1.35 -2 -6 11 13.53 1.66 2 6 -11 12.21 1.46 2 6 -11 14.56 1.22 2 6 -10 33.63 1.80 2 6 -10 36.79 2.27 -2 -6 10 36.73 2.30 -2 -6 9 15.67 1.59 2 6 -9 15.76 1.29 2 6 -9 15.39 1.59 2 6 -8 7.06 1.36 2 6 -8 5.42 1.60 -2 -6 8 9.22 1.40 2 6 -8 7.50 1.10 2 6 -7 124.74 4.88 2 6 -7 128.27 4.54 2 6 -7 130.34 5.22 -2 -6 7 125.17 4.76 -2 -6 6 298.58 9.73 2 6 -6 305.87 10.19 2 6 -6 311.37 9.61 2 6 -6 298.35 9.88 -2 -6 5 41.43 2.29 2 6 -5 42.88 2.26 2 6 -5 40.16 2.51 -2 -6 4 130.34 4.81 2 6 -4 131.76 5.06 2 6 -4 120.46 4.47 2 6 -4 133.99 4.74 2 6 -3 0.64 0.78 -2 -6 3 0.12 1.07 2 6 -3 0.68 1.03 2 6 -3 -0.96 1.24 2 6 -2 98.58 4.10 -2 -6 2 101.07 4.07 -2 -6 2 99.85 4.19 2 6 -2 101.42 4.06 2 6 -2 98.28 3.56 2 6 -1 4.77 1.25 -2 -6 1 4.20 1.41 2 6 -1 4.77 1.26 2 6 -1 3.22 0.77 2 6 0 -0.42 1.22 2 6 0 -0.12 1.05 2 6 0 0.61 0.61 -2 -6 0 -0.44 1.21 2 6 1 54.41 2.92 -2 -6 -1 58.47 3.02 2 6 1 54.44 2.75 2 6 1 51.49 1.96 2 6 2 213.76 7.13 -2 -6 -2 213.33 7.50 -2 -6 -2 203.06 6.29 2 6 2 208.79 6.23 -2 -6 -3 78.37 3.73 -2 -6 -3 71.35 2.54 2 6 3 68.71 3.19 2 6 4 9.02 1.35 -2 -6 -4 5.96 0.78 -2 -6 -4 7.59 1.65 2 6 4 6.88 1.65 -2 -6 -5 -0.89 1.47 -2 -6 -5 0.37 0.75 2 6 5 -0.25 1.04 2 6 5 -0.75 1.52 2 6 6 18.47 1.67 2 6 6 14.07 2.02 -2 -6 -6 17.54 2.10 -2 -6 -6 15.96 1.27 2 6 6 14.28 1.58 -2 -6 -7 2.51 0.96 2 6 7 2.66 1.26 2 6 7 0.84 1.64 -2 -6 -7 0.41 1.71 2 6 7 1.57 1.17 2 6 8 2.45 1.81 2 6 8 2.01 1.17 -2 -6 -8 4.29 1.76 2 6 8 5.29 1.32 2 6 9 100.89 5.10 2 6 9 107.59 4.40 -2 -6 -9 97.03 5.01 2 6 9 105.16 4.34 -2 -7 12 28.59 2.24 2 7 -12 24.45 1.66 2 7 -12 24.94 2.06 2 7 -11 89.52 3.50 -2 -7 11 89.20 4.01 2 7 -11 86.54 3.89 -2 -7 10 113.73 4.57 2 7 -10 99.64 4.88 2 7 -10 107.91 4.06 2 7 -10 109.80 4.47 2 7 -9 14.56 2.16 -2 -7 9 16.28 1.73 2 7 -9 15.49 1.47 2 7 -9 15.90 1.75 2 7 -8 1.92 1.55 2 7 -8 3.32 1.17 2 7 -8 1.45 1.25 -2 -7 8 3.97 1.35 -2 -7 7 1.89 1.25 2 7 -7 6.10 1.32 2 7 -7 4.19 1.16 2 7 -7 5.87 1.49 2 7 -7 6.32 1.79 -2 -7 6 1.62 1.35 2 7 -6 0.71 1.50 2 7 -6 -1.28 1.19 2 7 -6 1.40 1.15 -2 -7 5 311.33 10.37 2 7 -5 309.39 10.06 2 7 -5 333.68 10.32 2 7 -5 320.23 10.72 2 7 -4 60.13 2.75 -2 -7 4 62.20 3.07 2 7 -4 65.91 3.08 2 7 -3 15.55 1.71 2 7 -3 12.31 1.35 2 7 -3 12.86 1.72 -2 -7 3 13.92 1.63 2 7 -2 14.80 1.72 -2 -7 2 13.14 1.80 -2 -7 2 14.24 1.72 2 7 -2 13.96 1.29 2 7 -2 12.71 1.74 2 7 -1 189.54 6.43 2 7 -1 205.56 7.16 -2 -7 1 212.69 7.46 2 7 -1 202.99 7.22 2 7 0 0.29 1.23 -2 -7 0 1.04 1.44 2 7 0 0.66 0.73 2 7 0 -0.49 1.37 2 7 1 5.25 1.50 -2 -7 -1 2.46 1.55 2 7 1 3.88 0.72 2 7 1 3.25 1.32 2 7 2 206.29 7.14 -2 -7 -2 205.12 7.56 2 7 2 200.16 6.16 -2 -7 -3 3.37 1.62 2 7 3 4.02 1.22 -2 -7 -3 2.96 0.73 2 7 4 104.04 4.73 -2 -7 -4 97.23 4.71 -2 -7 -4 99.51 3.46 2 7 4 103.05 4.26 -2 -7 -5 247.55 9.60 2 7 5 275.54 9.11 2 7 5 271.30 9.72 -2 -7 -5 278.18 8.37 2 7 6 22.24 1.89 2 7 6 20.97 2.53 2 7 6 22.99 1.94 -2 -7 -6 21.34 2.44 -2 -7 -6 25.17 1.51 2 7 7 3.23 1.98 -2 -7 -7 2.29 1.88 2 7 7 2.09 1.23 2 7 7 1.74 1.26 2 7 8 8.00 1.50 2 7 8 7.31 2.13 -2 -8 12 0.66 1.63 2 8 -12 -0.24 1.73 2 8 -12 -1.26 1.13 2 8 -12 0.79 1.48 2 8 -11 4.40 1.98 2 8 -11 4.11 1.50 2 8 -11 2.06 1.15 -2 -8 11 4.26 1.62 -2 -8 10 24.61 2.24 2 8 -10 24.59 1.81 2 8 -10 25.24 2.23 2 8 -10 23.89 2.68 2 8 -10 24.50 2.14 2 8 -9 6.08 1.27 2 8 -9 5.77 1.93 2 8 -9 11.23 1.75 -2 -8 9 5.44 1.58 2 8 -9 6.14 1.58 -2 -8 8 227.14 7.99 2 8 -8 216.70 7.84 2 8 -8 230.56 8.55 2 8 -8 232.52 8.08 2 8 -8 223.77 7.59 -2 -8 7 82.50 3.93 2 8 -7 85.11 3.80 2 8 -7 93.24 4.49 2 8 -7 86.33 3.76 2 8 -7 93.45 4.18 -2 -8 6 38.91 2.57 2 8 -6 32.19 2.76 2 8 -6 39.89 2.43 2 8 -6 40.91 2.40 -2 -8 5 23.93 2.20 2 8 -5 23.72 1.85 2 8 -5 25.23 2.07 2 8 -5 21.41 2.31 -2 -8 4 133.29 5.42 2 8 -4 143.95 5.70 2 8 -4 137.24 5.29 2 8 -4 127.25 4.96 -2 -8 3 1.50 1.47 2 8 -3 0.78 1.35 2 8 -3 1.83 1.13 2 8 -3 0.90 1.46 -2 -8 2 533.10 16.84 -2 -8 2 556.61 17.08 2 8 -2 530.95 16.86 2 8 -2 525.86 16.72 2 8 -2 529.80 16.07 2 8 -1 26.75 1.70 2 8 -1 32.47 2.51 2 8 -1 29.55 2.37 2 8 0 -0.08 0.77 2 8 0 -1.45 1.52 2 8 0 0.49 1.42 -2 -8 0 -0.60 1.62 2 8 1 3.73 0.79 2 8 1 5.79 1.82 -2 -8 -1 2.42 1.66 2 8 1 0.48 1.32 2 8 2 496.69 14.65 2 8 2 502.69 15.74 -2 -8 -2 512.57 16.33 -2 -8 -3 -0.21 1.70 2 8 3 -0.62 1.29 -2 -8 -4 2.07 0.76 2 8 4 2.42 1.87 2 8 4 1.84 1.30 -2 -8 -4 0.66 1.79 2 8 5 99.04 4.23 -2 -8 -5 93.43 4.82 2 8 5 95.39 4.82 2 8 6 3.61 2.00 2 8 6 4.88 1.45 2 8 6 3.76 1.44 -2 -8 -6 2.18 1.97 2 9 -12 3.34 1.32 2 9 -11 48.94 2.60 -2 -9 11 42.03 3.04 2 9 -11 42.04 3.04 2 9 -10 14.86 2.42 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256.51 8.97 -2 -9 -4 12.59 2.55 2 9 4 15.85 2.45 2 9 4 7.45 1.60 -2 -10 11 43.59 3.18 2 10 -11 43.43 2.64 -2 -10 10 3.71 1.99 2 10 -10 3.25 1.57 2 10 -10 4.51 1.96 2 10 -9 75.00 3.67 2 10 -9 72.84 3.93 2 10 -9 73.88 4.51 -2 -10 9 80.85 4.19 -2 -10 8 0.62 1.73 2 10 -8 3.57 2.01 2 10 -8 0.37 1.72 2 10 -8 0.48 1.46 2 10 -8 2.86 1.89 2 10 -7 14.50 1.97 -2 -10 7 10.67 2.04 2 10 -7 14.95 2.37 2 10 -7 9.34 1.77 -2 -10 6 161.13 6.57 2 10 -6 162.37 6.24 2 10 -6 148.08 6.76 2 10 -6 169.12 6.36 2 10 -5 7.75 2.09 -2 -10 5 9.96 2.01 2 10 -5 7.14 1.60 2 10 -5 5.50 1.67 -2 -10 4 59.32 3.57 2 10 -4 60.20 3.78 2 10 -4 60.07 3.47 2 10 -4 56.09 3.01 2 10 -3 4.57 1.42 2 10 -3 4.45 1.93 2 10 -3 5.86 1.88 2 10 -2 9.63 1.92 2 10 -2 7.67 1.32 2 10 -2 13.31 2.01 2 10 -1 2.00 1.13 2 10 -1 0.86 1.68 2 10 -1 2.91 1.68 -2 -10 1 -0.48 1.99 2 10 0 37.88 3.02 2 10 0 39.78 2.95 -2 -10 0 39.45 3.28 2 10 0 37.69 2.00 2 10 1 0.23 1.86 -2 -10 -1 1.79 2.02 2 10 1 0.59 1.62 -2 -10 -2 101.43 5.31 2 10 2 93.96 4.55 -2 -11 10 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826.86 25.22 4 -6 -3 815.86 25.13 -4 6 3 846.36 24.73 -4 6 3 858.01 24.89 4 -6 -3 824.93 25.55 4 -6 -2 391.63 12.60 -4 6 2 406.37 12.31 -4 6 2 410.18 12.42 -4 6 2 374.53 12.68 4 -6 -2 398.49 13.02 4 -6 -2 425.91 12.80 -4 6 1 255.96 8.11 -4 6 1 255.29 8.15 4 -6 -1 240.01 8.72 4 -6 -1 256.12 8.51 4 -6 -1 246.13 8.28 4 -6 0 11.83 1.49 -4 6 0 14.25 1.39 -4 6 0 15.89 1.45 -4 6 -1 36.04 2.09 -4 6 -1 36.26 2.03 4 -6 1 41.04 2.40 -4 6 -2 25.04 2.05 -4 6 -2 23.88 1.79 -4 6 -2 25.52 1.71 4 -6 2 28.04 2.08 -4 6 -3 39.27 2.28 -4 6 -3 45.99 2.29 4 -6 3 41.54 2.61 4 -6 3 42.02 2.58 -4 6 -3 42.68 2.21 -4 6 -3 44.53 2.63 -4 6 -4 67.73 3.17 4 -6 4 71.58 3.35 4 -6 4 71.78 3.36 -4 6 -4 65.25 2.90 -4 6 -4 69.09 2.98 -4 6 -4 65.53 3.36 -4 6 -5 124.63 4.98 -4 6 -5 127.40 4.76 4 -6 5 114.48 4.77 -4 6 -5 117.92 4.33 -4 6 -5 112.45 4.40 -4 6 -6 13.71 1.42 -4 6 -6 19.23 1.86 -4 6 -6 13.91 1.79 -4 6 -6 15.66 1.35 -4 6 -7 58.14 2.73 -4 6 -7 52.61 3.13 -4 6 -7 55.53 2.56 -4 6 -8 86.19 3.77 4 -6 8 94.12 4.22 -4 6 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1.83 4 2 -4 49.16 2.04 4 2 -4 46.07 1.79 4 2 -4 47.67 2.01 4 2 -3 7.01 0.80 4 2 -3 10.27 0.61 4 2 -3 8.30 0.74 4 2 -3 7.53 0.80 4 2 -3 8.36 0.77 4 2 -3 7.84 0.67 4 2 -2 506.89 14.63 4 2 -2 501.78 14.54 4 2 -2 493.98 14.64 4 2 -2 499.22 14.90 4 2 -1 61.99 2.16 -4 -2 1 58.48 2.18 4 2 -1 55.83 2.11 4 2 -1 56.96 2.08 4 2 -1 55.64 2.38 4 2 0 19.76 1.12 -4 -2 0 20.04 1.20 4 2 0 20.24 1.04 4 2 0 18.72 0.89 4 2 1 100.41 3.37 4 2 1 94.70 3.16 -4 -2 -1 90.16 3.38 4 2 2 56.40 2.21 -4 -2 -2 48.93 2.25 4 2 2 50.54 1.97 4 2 2 53.92 2.37 4 2 3 20.56 1.35 -4 -2 -3 19.57 1.41 4 2 3 21.85 1.15 4 2 3 21.71 1.48 4 2 4 193.23 6.39 -4 -2 -4 203.12 6.55 4 2 4 195.19 6.14 4 2 4 193.43 6.56 -4 -2 -5 28.86 1.89 4 2 5 30.32 1.53 -4 -2 -5 27.66 1.18 4 2 5 26.19 1.78 4 2 6 125.08 4.41 -4 -2 -6 131.46 4.15 4 2 6 120.58 4.70 4 2 7 44.50 2.38 -4 -2 -7 43.91 2.50 -4 -2 -7 48.44 1.95 4 2 7 48.59 2.18 4 2 7 40.10 2.29 4 2 8 0.71 1.12 4 2 8 1.21 1.06 -4 -2 -8 0.84 1.22 4 2 8 0.97 0.92 -4 -2 -8 1.19 0.81 4 2 9 -0.61 1.01 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6.51 1.10 -4 -3 -3 6.95 1.26 4 3 3 6.55 0.91 4 3 4 10.55 1.32 -4 -3 -4 10.13 1.29 4 3 4 13.33 1.26 4 3 4 9.23 1.00 -4 -3 -5 142.15 5.26 4 3 5 141.94 4.80 4 3 5 136.78 5.15 -4 -3 -6 69.70 3.21 4 3 6 65.82 2.68 -4 -3 -6 61.11 2.01 -4 -3 -6 61.67 2.03 4 3 6 65.37 2.99 4 3 7 67.41 3.05 -4 -3 -7 76.89 3.54 4 3 7 70.84 2.91 -4 -3 -7 67.49 2.38 -4 -3 -7 65.73 2.32 4 3 7 76.17 3.21 4 3 8 5.30 1.30 -4 -3 -8 4.06 0.68 4 3 8 3.16 1.16 -4 -3 -8 3.40 1.47 4 3 8 4.72 1.07 -4 -3 -8 3.85 0.76 4 3 9 126.92 4.94 -4 -3 -9 119.05 5.22 4 3 9 127.70 4.75 4 3 9 127.70 4.89 4 3 10 10.90 1.59 4 3 10 10.08 1.60 -4 -3 -10 9.31 2.04 4 3 10 11.45 1.52 4 4 -14 2.51 1.26 4 4 -13 11.93 1.46 4 4 -12 24.83 1.74 4 4 -11 15.15 1.34 4 4 -10 2.46 0.36 4 4 -10 2.12 0.93 4 4 -9 4.53 0.69 4 4 -9 4.25 0.47 4 4 -8 27.45 1.17 4 4 -8 27.60 1.65 4 4 -8 26.14 1.38 4 4 -7 23.42 1.89 4 4 -7 23.38 1.18 4 4 -7 22.99 1.50 4 4 -7 23.75 1.36 4 4 -6 85.80 3.50 4 4 -6 79.92 2.92 4 4 -6 83.06 3.18 4 4 -6 79.93 3.04 4 4 -5 298.10 9.35 4 4 -5 282.62 8.89 4 4 -5 291.79 9.05 4 4 -4 0.25 0.79 4 4 -4 0.61 1.01 4 4 -3 32.50 1.91 4 4 -3 37.25 1.92 4 4 -2 184.87 6.13 4 4 -2 175.27 5.99 4 4 -1 71.18 3.12 -4 -4 1 76.29 3.10 4 4 -1 68.46 2.89 4 4 -1 72.46 2.27 4 4 -1 68.97 2.25 4 4 0 11.25 1.03 -4 -4 0 9.64 1.28 4 4 0 8.11 1.37 4 4 0 10.31 1.14 4 4 1 164.50 5.48 4 4 1 162.44 5.94 -4 -4 -1 156.24 5.76 4 4 1 169.98 5.52 4 4 2 124.73 4.44 -4 -4 -2 124.15 4.79 4 4 2 127.08 4.42 4 4 3 2.00 0.93 -4 -4 -3 2.92 1.23 4 4 3 3.16 0.97 4 4 4 15.39 1.41 -4 -4 -4 12.82 1.72 4 4 4 17.45 1.40 -4 -4 -5 279.49 9.67 4 4 5 294.08 9.13 4 4 6 19.14 1.72 -4 -4 -6 18.17 2.00 4 4 6 19.61 1.51 4 4 7 3.39 1.31 4 4 7 5.92 1.25 -4 -4 -7 4.47 1.58 4 4 7 2.52 0.98 4 4 8 150.63 5.42 -4 -4 -8 145.66 5.87 4 4 8 135.90 5.15 4 4 8 140.60 5.43 4 4 9 2.02 1.41 4 4 9 0.72 1.20 -4 -4 -9 1.79 1.78 4 4 9 3.36 1.16 4 4 10 1.78 1.44 4 5 -13 70.69 3.21 4 5 -12 212.16 7.22 4 5 -11 14.87 0.83 -4 -5 11 18.37 1.19 4 5 -11 15.54 1.55 4 5 -10 12.36 0.94 4 5 -10 13.12 0.84 -4 -5 10 15.95 1.15 4 5 -10 14.07 1.41 4 5 -9 3.56 0.75 4 5 -9 3.72 0.67 4 5 -9 2.77 1.02 4 5 -8 338.97 10.34 4 5 -8 351.85 11.41 4 5 -8 357.07 10.84 4 5 -8 344.08 10.47 4 5 -7 10.78 1.07 4 5 -7 10.65 1.37 4 5 -7 8.87 1.51 4 5 -6 649.57 19.17 4 5 -6 595.02 18.49 4 5 -6 656.30 18.83 4 5 -5 -0.18 0.93 4 5 -5 -0.38 1.24 4 5 -5 -0.85 1.02 4 5 -4 118.22 4.73 4 5 -4 132.69 4.68 4 5 -3 109.61 4.36 4 5 -3 118.07 4.41 4 5 -2 1052.07 30.65 4 5 -2 1041.04 30.53 4 5 -2 1038.34 29.81 4 5 -1 53.26 2.73 4 5 -1 49.36 2.52 -4 -5 1 53.33 2.76 4 5 -1 51.64 1.66 4 5 -1 50.53 1.74 -4 -5 0 8.64 1.45 4 5 0 9.97 1.58 4 5 0 9.09 1.21 4 5 1 80.16 3.76 -4 -5 -1 75.56 3.63 4 5 2 561.15 16.80 -4 -5 -2 561.48 17.27 4 5 2 586.98 16.85 4 5 3 41.96 2.24 4 5 3 40.66 2.73 -4 -5 -3 41.76 2.61 4 5 3 40.99 2.22 4 5 4 29.15 1.88 -4 -5 -4 31.61 2.32 4 5 4 22.53 2.24 4 5 4 26.04 1.77 -4 -5 -5 68.45 3.66 4 5 5 72.65 3.12 -4 -5 -6 2.97 1.59 4 5 6 3.11 1.14 -4 -5 -7 1.18 1.60 4 5 7 2.33 1.27 4 5 7 1.36 1.86 4 5 7 1.17 1.03 4 5 8 23.54 2.08 4 5 8 26.94 2.02 4 5 8 18.94 2.58 -4 -5 -8 23.89 2.46 4 5 8 25.97 1.90 4 5 9 0.95 1.48 4 5 9 -0.54 1.30 4 5 10 1.45 1.61 4 6 -13 0.65 1.27 4 6 -12 0.38 1.18 4 6 -11 33.40 1.51 4 6 -11 34.65 2.15 4 6 -11 30.35 1.47 4 6 -10 16.86 2.24 4 6 -10 21.27 1.26 -4 -6 10 22.00 1.60 4 6 -10 20.98 1.72 4 6 -10 18.49 1.20 4 6 -9 8.67 1.04 4 6 -9 4.88 1.60 -4 -6 9 8.46 1.32 4 6 -9 8.40 1.02 4 6 -9 8.72 1.30 4 6 -8 28.15 2.36 4 6 -8 24.39 1.54 4 6 -8 26.88 1.96 4 6 -7 11.68 1.74 4 6 -7 12.66 1.62 4 6 -7 11.28 1.23 4 6 -6 31.40 1.93 4 6 -6 31.10 2.17 4 6 -6 30.16 2.34 4 6 -5 349.60 11.31 4 6 -5 344.36 10.92 4 6 -4 514.27 15.96 4 6 -4 514.19 15.79 4 6 -3 85.46 3.12 4 6 -3 92.52 3.85 4 6 -3 82.08 3.79 4 6 -2 0.96 0.63 4 6 -2 1.43 1.34 -4 -6 2 0.28 1.27 4 6 -2 2.21 1.24 4 6 -1 40.53 2.57 4 6 -1 36.96 1.37 4 6 -1 45.06 2.43 -4 -6 1 42.77 2.65 4 6 0 116.27 4.95 -4 -6 0 122.80 4.98 4 6 0 124.95 4.69 4 6 1 139.12 5.57 -4 -6 -1 133.76 5.49 4 6 1 140.34 5.13 4 6 2 232.38 8.56 4 6 2 249.45 7.98 -4 -6 -2 246.54 8.56 4 6 2 233.85 7.98 4 6 3 1.54 1.08 -4 -6 -3 -1.05 1.57 4 6 3 -0.38 1.64 4 6 3 0.59 1.12 4 6 4 104.16 4.30 4 6 4 117.68 5.09 -4 -6 -4 102.19 4.87 4 6 4 115.85 4.35 -4 -6 -5 2.94 1.78 4 6 5 2.07 1.14 4 6 6 30.62 2.06 -4 -6 -6 29.21 2.64 4 6 7 -0.30 1.29 -4 -6 -7 1.11 1.80 4 6 7 0.39 1.17 4 6 8 109.90 4.74 4 7 -12 14.33 2.38 4 7 -12 19.44 1.95 4 7 -11 59.68 3.09 4 7 -11 56.50 3.69 -4 -7 10 169.26 5.73 4 7 -10 154.47 6.51 4 7 -10 155.33 5.24 4 7 -10 160.38 5.81 4 7 -10 146.19 5.16 4 7 -9 3.85 1.79 -4 -7 9 3.37 1.28 4 7 -9 4.21 1.06 4 7 -9 5.44 1.46 4 7 -8 82.38 4.25 4 7 -8 86.53 3.45 4 7 -8 83.80 3.81 4 7 -7 34.49 2.66 4 7 -7 43.26 2.30 4 7 -7 37.43 2.52 4 7 -6 121.32 5.02 4 7 -6 113.88 4.53 4 7 -5 33.96 2.51 4 7 -5 36.46 1.99 4 7 -5 32.01 2.21 4 7 -4 163.55 6.16 4 7 -4 162.86 5.45 4 7 -4 154.17 5.92 4 7 -3 0.59 0.80 4 7 -3 0.15 1.37 4 7 -3 -0.94 1.51 4 7 -2 0.83 1.38 -4 -7 2 -0.17 1.53 4 7 -2 0.75 1.36 4 7 -2 0.72 0.68 4 7 -1 7.10 1.62 -4 -7 1 9.20 1.70 4 7 -1 9.43 0.62 4 7 -1 11.47 1.67 -4 -7 0 349.29 11.58 4 7 0 337.50 11.16 4 7 0 349.01 11.57 4 7 1 3.79 1.71 -4 -7 -1 8.47 1.82 4 7 1 5.66 1.41 4 7 2 107.35 5.02 -4 -7 -2 111.98 5.08 4 7 2 117.38 4.58 4 7 3 0.66 1.16 4 7 3 -0.21 1.71 -4 -7 -3 0.20 1.65 4 7 3 -1.20 1.23 4 7 4 7.79 1.47 4 7 4 9.62 2.02 -4 -7 -4 12.57 2.22 4 7 4 9.59 1.56 -4 -7 -5 22.38 2.64 4 7 5 22.85 1.91 -4 -7 -6 69.30 4.18 4 7 6 67.65 3.33 4 8 -11 48.77 3.65 4 8 -11 56.01 3.04 4 8 -10 29.02 2.94 4 8 -10 27.85 1.90 4 8 -10 25.87 2.32 4 8 -9 298.76 9.66 4 8 -9 311.04 10.29 4 8 -8 53.15 3.55 4 8 -8 64.59 3.16 4 8 -8 59.84 2.90 4 8 -8 60.13 3.32 4 8 -7 130.21 5.77 4 8 -7 138.25 5.20 4 8 -7 138.81 5.22 4 8 -7 138.11 5.62 4 8 -6 1.14 1.36 4 8 -6 -0.19 1.62 4 8 -6 0.48 1.14 4 8 -5 3.39 1.16 4 8 -5 2.43 1.38 4 8 -5 4.29 1.79 4 8 -4 16.02 1.91 4 8 -4 15.66 1.45 4 8 -4 14.98 1.99 4 8 -3 50.18 3.11 4 8 -3 52.45 2.35 4 8 -3 54.70 3.23 4 8 -2 2.62 0.80 4 8 -2 1.11 1.50 4 8 -2 1.68 1.52 4 8 -1 5.11 1.79 -4 -8 1 6.07 1.79 4 8 -1 4.12 1.48 4 8 -1 3.93 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3.37 -5 8 4 67.59 3.52 -5 8 4 63.92 2.90 -5 8 4 62.56 3.09 5 -8 -4 62.22 3.80 5 -8 -3 1.17 1.48 5 -8 -3 1.27 1.60 -5 8 3 0.36 1.42 5 -8 -3 1.52 1.80 -5 8 3 2.27 1.07 -5 8 3 0.67 1.28 5 -8 -2 38.50 2.55 5 -8 -2 33.42 2.62 5 -8 -2 38.63 2.96 -5 8 2 38.58 2.22 -5 8 2 38.67 2.39 -5 8 2 33.66 2.62 5 -8 -1 17.07 2.16 5 -8 -1 14.53 2.24 -5 8 1 13.90 1.59 -5 8 1 13.27 1.91 -5 8 1 17.81 1.73 5 -8 0 30.78 2.63 5 -8 0 32.49 2.64 -5 8 0 31.75 2.14 -5 8 0 26.87 2.01 5 -8 1 4.10 1.66 -5 8 -1 4.45 1.30 -5 8 -1 2.80 1.27 -5 8 -2 109.95 4.43 -5 8 -2 103.08 4.34 5 -8 2 107.48 4.86 5 -8 3 6.10 1.83 -5 8 -3 6.77 1.82 -5 8 -3 8.99 1.56 -5 8 -3 7.18 1.42 -5 8 -3 7.00 1.41 -5 8 -4 289.04 10.26 -5 8 -4 289.94 9.82 -5 8 -4 293.63 9.67 5 -8 4 301.47 10.21 5 -8 4 315.96 10.39 -5 8 -4 278.85 9.48 -5 8 -5 1.03 1.70 5 -8 5 -0.20 1.57 -5 8 -5 0.33 1.43 -5 8 -5 0.96 1.27 -5 8 -5 0.12 1.08 5 -8 6 10.57 2.01 -5 8 -6 10.24 1.65 -5 8 -6 8.56 1.78 -5 8 -6 9.81 1.43 -5 8 -6 10.70 1.99 -5 8 -6 11.53 1.40 -5 8 -7 2.54 1.29 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1.82 -5 7 -11 52.99 2.75 -5 7 -11 58.52 2.99 5 -6 -10 6.47 1.93 -5 6 10 6.67 1.38 5 -6 -9 -0.75 1.63 -5 6 9 0.85 1.02 5 -6 -8 4.46 2.05 5 -6 -8 8.35 1.75 -5 6 8 8.55 1.23 -5 6 8 5.31 1.26 5 -6 -7 1.71 1.64 5 -6 -7 -0.32 1.35 -5 6 7 -0.72 0.83 -5 6 7 0.10 0.96 5 -6 -6 3.70 1.74 5 -6 -6 4.67 1.54 -5 6 6 6.48 1.00 -5 6 6 8.92 1.21 -5 6 5 2.74 1.36 5 -6 -5 0.60 1.56 5 -6 -5 1.53 1.29 5 -6 -5 1.15 1.21 -5 6 5 1.61 0.83 -5 6 5 1.00 1.00 5 -6 -4 40.17 2.38 5 -6 -4 39.00 2.33 -5 6 4 38.45 2.09 -5 6 4 37.31 1.89 5 -6 -4 38.76 2.78 5 -6 -3 5.43 1.37 5 -6 -3 3.96 1.28 -5 6 3 4.75 0.91 -5 6 3 4.42 1.03 5 -6 -2 11.00 1.56 5 -6 -2 9.44 1.44 -5 6 2 10.89 1.15 -5 6 2 11.44 1.28 -5 6 1 104.37 3.81 -5 6 1 104.38 3.99 -5 6 1 103.11 4.47 5 -6 -1 107.00 4.35 -5 6 0 171.81 5.70 -5 6 0 170.72 5.84 -5 6 0 166.09 6.34 5 -6 0 159.92 6.50 5 -6 0 174.25 6.27 5 -6 1 21.41 1.97 5 -6 1 26.53 2.25 -5 6 -1 26.57 1.67 -5 6 -1 23.45 1.68 -5 6 -1 24.70 2.12 -5 6 -2 68.83 3.48 -5 6 -2 62.09 2.86 -5 6 -2 65.19 2.92 5 -6 2 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50.88 2.34 5 4 -5 129.88 4.27 5 4 -5 135.76 4.54 5 4 -5 138.77 4.91 5 4 -5 141.34 4.65 5 4 -5 128.93 4.57 5 4 -5 130.12 4.72 5 4 -4 47.28 1.87 5 4 -4 47.97 2.33 5 4 -4 43.79 2.13 5 4 -4 45.92 1.96 5 4 -4 42.82 2.22 5 4 -4 42.38 2.19 5 4 -3 241.20 7.77 5 4 -3 237.37 7.31 5 4 -3 241.97 7.67 5 4 -3 233.72 7.25 5 4 -3 230.52 7.73 5 4 -2 380.38 11.87 5 4 -2 381.44 11.38 5 4 -2 391.39 11.62 5 4 -2 367.54 11.11 5 4 -2 384.23 11.81 5 4 -1 28.14 1.11 5 4 -1 31.15 1.65 5 4 -1 32.84 2.08 -5 -4 1 31.48 1.89 5 4 -1 30.46 1.71 5 4 -1 33.52 1.96 5 4 0 2.35 0.98 5 4 0 3.62 0.84 -5 -4 0 1.76 1.15 5 4 0 1.49 1.31 5 4 0 2.63 0.91 5 4 1 0.36 0.83 -5 -4 -1 0.35 1.12 5 4 1 1.41 0.86 5 4 2 63.78 2.79 -5 -4 -2 65.41 3.05 5 4 2 64.35 2.63 5 4 2 62.07 3.01 5 4 3 59.30 2.72 -5 -4 -3 51.97 2.88 5 4 3 59.07 2.53 5 4 3 59.42 2.90 5 4 4 43.13 2.30 -5 -4 -4 41.01 2.63 5 4 4 43.15 2.10 5 4 4 40.08 2.43 5 4 5 4.61 1.33 5 4 5 6.67 1.30 -5 -4 -5 3.79 1.52 5 4 5 7.67 1.13 5 4 6 39.62 2.38 -5 -4 -6 44.72 2.85 5 4 6 46.86 2.25 5 4 6 40.21 2.59 5 4 7 9.46 1.70 -5 -4 -7 9.52 1.77 5 4 7 13.97 1.46 5 4 8 9.00 1.63 -5 -4 -8 9.26 1.84 5 4 8 6.40 1.31 5 4 9 0.66 1.44 -5 -4 -9 -0.42 1.83 5 4 9 1.52 1.29 5 5 -13 0.59 1.20 5 5 -12 84.14 3.53 5 5 -11 51.76 2.51 5 5 -10 0.14 0.73 5 5 -10 0.35 1.49 5 5 -10 0.95 0.34 5 5 -10 0.40 0.96 5 5 -9 44.04 2.75 5 5 -9 39.37 1.52 5 5 -9 37.92 2.09 5 5 -9 41.65 1.93 5 5 -8 1.12 0.86 5 5 -8 0.31 1.41 5 5 -8 0.15 0.64 5 5 -8 1.25 0.87 5 5 -7 3.21 0.93 5 5 -7 4.18 1.35 5 5 -7 3.39 1.03 5 5 -7 4.43 0.86 5 5 -6 53.18 2.86 5 5 -6 50.27 2.32 5 5 -6 51.92 2.49 5 5 -6 53.08 2.42 5 5 -5 74.48 3.36 5 5 -5 74.25 3.18 5 5 -5 74.18 3.11 5 5 -5 72.11 3.09 5 5 -4 46.17 2.43 5 5 -4 39.23 2.30 5 5 -4 43.12 2.26 5 5 -3 140.08 5.05 5 5 -3 135.15 4.36 5 5 -3 135.78 5.13 5 5 -2 2.04 0.85 5 5 -2 1.60 1.26 5 5 -2 1.70 1.03 5 5 -2 2.50 0.56 5 5 -2 0.92 0.50 5 5 -1 2.39 0.97 -5 -5 1 1.86 1.15 5 5 -1 2.31 1.26 5 5 -1 1.74 1.02 5 5 0 20.40 1.48 -5 -5 0 20.96 1.88 5 5 0 24.68 2.10 5 5 0 19.98 1.56 5 5 1 149.79 5.23 5 5 1 148.96 5.81 -5 -5 -1 148.68 5.63 5 5 1 148.81 5.22 5 5 2 17.87 1.50 -5 -5 -2 18.16 1.85 5 5 2 18.87 2.12 5 5 2 19.12 1.53 5 5 3 24.35 1.80 -5 -5 -3 24.88 2.22 5 5 3 22.30 2.28 5 5 3 25.44 1.73 5 5 4 20.21 1.82 5 5 4 23.90 1.83 -5 -5 -4 23.95 2.17 5 5 4 19.10 2.30 5 5 4 22.06 1.63 5 5 5 16.58 1.72 5 5 5 11.22 1.55 -5 -5 -5 12.96 1.98 5 5 5 14.65 2.14 5 5 5 11.73 1.33 5 5 6 10.57 1.79 5 5 6 10.93 1.53 -5 -5 -6 12.62 2.12 5 5 6 15.65 2.38 5 5 6 11.81 1.40 5 5 7 3.16 1.53 -5 -5 -7 3.34 1.86 5 5 7 2.70 1.17 5 5 8 2.23 1.43 -5 -5 -8 4.26 2.20 5 5 8 5.05 1.27 5 6 -13 17.35 2.53 5 6 -13 17.36 1.72 5 6 -12 10.39 2.19 5 6 -12 16.80 1.66 5 6 -11 88.28 4.40 5 6 -11 83.23 3.58 5 6 -10 0.40 0.79 5 6 -10 -0.19 1.71 5 6 -10 0.23 1.11 5 6 -9 39.54 2.80 5 6 -9 35.37 1.70 5 6 -9 37.70 2.18 5 6 -9 37.26 1.93 5 6 -8 18.66 1.40 5 6 -8 18.37 2.07 5 6 -8 16.12 1.27 5 6 -8 18.80 1.61 5 6 -7 6.93 1.10 5 6 -7 7.66 1.59 5 6 -7 7.78 1.34 5 6 -7 5.00 1.12 5 6 -6 102.00 4.43 5 6 -6 108.24 4.06 5 6 -6 102.13 4.16 5 6 -5 -0.47 1.15 5 6 -5 0.29 1.30 5 6 -4 -0.26 1.24 5 6 -4 1.11 1.29 5 6 -3 618.48 18.87 5 6 -3 619.13 18.08 5 6 -3 646.42 19.08 5 6 -3 614.02 17.93 5 6 -2 32.84 2.15 5 6 -2 31.56 1.26 5 6 -2 28.03 1.17 5 6 -2 35.34 2.43 -5 -6 1 7.40 1.58 5 6 -1 5.85 1.53 5 6 -1 4.16 1.23 5 6 0 62.27 3.34 5 6 0 58.75 2.71 -5 -6 0 62.76 3.23 5 6 0 57.04 2.85 5 6 1 73.55 3.97 5 6 1 80.09 3.38 -5 -6 -1 80.23 3.93 5 6 2 67.15 3.71 5 6 2 67.90 3.08 -5 -6 -2 68.46 3.58 5 6 2 65.03 2.98 5 6 3 11.17 1.47 -5 -6 -3 11.13 1.84 5 6 3 10.37 1.45 5 6 4 7.86 1.43 -5 -6 -4 4.98 1.77 5 6 4 8.66 1.89 5 6 4 7.15 1.31 5 6 5 54.96 2.95 5 6 5 53.15 3.57 -5 -6 -5 60.18 3.62 5 6 5 54.91 2.73 5 6 6 1.03 1.43 -5 -6 -6 -0.22 1.76 5 6 6 0.12 1.14 -5 -6 -7 4.18 1.99 5 6 7 5.30 1.38 5 7 -12 113.07 5.45 5 7 -12 112.32 4.56 5 7 -11 16.69 2.55 5 7 -11 20.24 1.90 5 7 -10 65.84 3.93 5 7 -10 67.31 3.18 5 7 -9 10.02 1.27 5 7 -9 10.61 1.96 5 7 -9 9.61 1.18 5 7 -8 0.88 1.01 5 7 -8 -0.19 1.62 5 7 -8 2.07 1.07 5 7 -8 1.63 1.33 5 7 -7 18.39 2.11 5 7 -7 15.46 1.74 5 7 -7 16.00 1.60 5 7 -6 14.22 1.64 5 7 -6 15.39 1.96 5 7 -6 14.37 1.77 5 7 -5 6.96 1.52 5 7 -5 5.08 1.58 5 7 -5 4.69 1.08 5 7 -4 5.20 1.49 5 7 -4 3.96 1.56 5 7 -4 3.22 0.94 5 7 -3 7.95 1.83 5 7 -3 7.14 0.89 5 7 -3 7.27 1.49 5 7 -2 35.75 1.25 5 7 -2 45.73 2.56 5 7 -2 41.91 2.73 5 7 -1 11.57 1.99 5 7 -1 10.29 1.60 5 7 0 5.39 1.23 5 7 0 8.26 1.81 -5 -7 0 3.26 1.72 5 7 0 5.08 1.29 5 7 1 0.62 1.11 5 7 1 2.42 1.66 5 7 1 -0.54 1.12 -5 -7 -1 2.08 1.67 5 7 2 11.58 1.48 5 7 2 13.24 2.05 -5 -7 -2 14.40 2.18 5 7 2 16.35 1.70 5 7 3 15.01 1.59 5 7 3 12.86 2.24 -5 -7 -3 12.22 2.16 5 7 3 12.64 1.62 5 7 4 0.30 1.30 5 7 4 0.24 1.97 -5 -7 -4 2.15 1.90 5 7 4 -0.13 1.31 -5 -7 -5 113.75 5.53 5 7 5 118.45 4.68 5 8 -11 83.36 4.63 5 8 -11 83.18 3.90 5 8 -10 2.05 2.02 5 8 -10 3.25 1.54 5 8 -9 0.95 1.15 5 8 -9 0.87 1.92 5 8 -9 2.13 1.45 5 8 -8 2.90 1.81 5 8 -8 4.46 1.38 5 8 -8 4.23 1.63 5 8 -7 114.83 5.10 5 8 -7 109.03 4.37 5 8 -7 107.25 4.46 5 8 -7 113.75 4.80 5 8 -6 1.47 1.43 5 8 -6 -0.38 1.75 5 8 -6 3.94 1.26 5 8 -5 138.93 5.71 5 8 -5 136.82 5.00 5 8 -5 138.22 5.54 5 8 -4 -0.25 0.92 5 8 -4 0.34 1.52 5 8 -4 0.18 1.55 5 8 -3 -0.92 1.69 5 8 -3 0.34 1.45 5 8 -3 -0.27 0.70 5 8 -2 1.77 1.79 5 8 -2 1.65 1.57 5 8 -1 7.40 2.00 -5 -8 1 4.11 1.82 5 8 -1 7.98 1.63 5 8 0 27.84 2.82 -5 -8 0 32.24 2.74 5 8 1 17.05 1.77 5 8 1 19.44 2.40 -5 -8 -1 21.90 2.63 5 8 1 17.70 1.93 5 8 2 33.66 2.29 5 8 2 29.38 2.81 -5 -8 -2 28.08 2.77 5 8 2 34.09 2.30 -5 -8 -3 -0.46 1.94 5 8 3 0.44 1.44 5 8 4 47.89 2.81 5 9 -9 2.13 1.95 5 9 -9 1.39 1.71 5 9 -8 160.46 6.78 5 9 -8 165.66 6.44 5 9 -7 78.94 4.41 5 9 -7 90.86 4.07 5 9 -7 88.71 4.39 5 9 -6 25.29 2.37 5 9 -6 25.85 2.64 5 9 -5 9.29 1.90 5 9 -5 8.53 1.99 5 9 -4 97.95 4.55 5 9 -4 81.98 4.33 5 9 -3 -0.61 1.96 5 9 -3 0.94 1.57 5 9 -2 -0.22 1.73 5 9 -2 3.68 1.75 5 9 -1 -0.45 1.95 -5 -9 1 0.44 1.99 5 9 -1 0.71 1.50 -5 -9 0 15.79 2.47 5 9 0 16.59 2.11 -5 -9 -1 -0.24 2.05 5 9 1 0.67 1.48 5 10 -6 5.83 2.00 5 10 -5 67.94 3.82 5 10 -4 15.25 2.45 5 10 -4 14.43 2.30 6 -10 -3 85.91 4.63 -6 10 3 77.44 3.92 6 -10 -2 0.70 2.14 -6 10 2 1.64 1.74 6 -10 -1 16.75 2.61 -6 10 1 19.16 2.14 -6 10 0 115.17 4.91 6 -10 0 114.40 5.54 6 -10 1 -0.25 2.11 6 -9 -4 18.69 2.43 -6 9 4 17.75 2.00 6 -9 -3 6.12 1.88 6 -9 -3 6.01 2.09 -6 9 3 4.40 1.55 6 -9 -2 18.63 2.40 -6 9 2 20.16 1.68 -6 9 2 19.79 2.03 6 -9 -1 14.12 2.18 -6 9 1 12.06 1.52 -6 9 1 14.13 1.82 -6 9 0 73.68 3.41 -6 9 0 77.29 3.59 6 -9 0 79.58 4.35 -6 9 -1 62.17 3.03 -6 9 -1 56.94 3.07 6 -9 1 61.53 3.81 -6 9 -2 14.51 2.23 6 -9 2 16.94 2.41 -6 9 -2 15.20 1.81 -6 9 -2 14.08 1.67 -6 9 -2 14.51 1.63 6 -9 3 1.78 1.77 -6 9 -3 3.17 1.51 -6 9 -3 -0.90 1.34 -6 9 -3 1.59 1.82 6 -9 3 -0.22 1.87 -6 9 -3 0.38 1.25 6 -9 4 0.23 1.84 -6 9 -4 -0.64 1.54 -6 9 -4 1.16 1.82 -6 9 -4 2.42 1.46 -6 9 -4 0.37 1.21 -6 9 -5 42.59 2.88 6 -9 5 36.26 3.18 -6 9 -5 44.26 2.84 -6 9 -5 36.58 2.25 -6 9 -6 20.95 2.32 -6 9 -6 21.77 1.77 -6 9 -7 31.13 2.70 6 -8 -5 31.05 2.59 6 -8 -5 32.90 2.55 -6 8 5 31.58 1.90 -6 8 5 30.60 2.14 6 -8 -4 56.25 3.33 6 -8 -4 56.87 3.21 -6 8 4 55.73 2.83 -6 8 4 52.96 2.54 -6 8 4 58.42 3.36 6 -8 -4 49.54 3.56 6 -8 -3 1.67 1.34 6 -8 -3 1.83 1.68 6 -8 -3 1.65 1.82 -6 8 3 2.05 1.02 -6 8 3 1.43 1.29 6 -8 -2 18.41 2.23 -6 8 2 16.07 1.47 -6 8 2 13.66 1.63 6 -8 -1 12.40 2.14 -6 8 1 8.05 1.31 -6 8 1 8.75 1.53 -6 8 0 70.13 3.06 -6 8 0 62.30 3.14 -6 8 0 73.21 3.83 6 -8 0 67.37 3.83 6 -8 1 8.55 2.13 6 -8 1 8.11 1.80 -6 8 -1 7.13 1.86 -6 8 -1 10.25 1.41 -6 8 -1 12.02 1.64 6 -8 2 5.37 1.92 6 -8 2 4.55 1.80 -6 8 -2 5.70 1.39 -6 8 -2 5.35 1.32 -6 8 -2 4.36 1.84 -6 8 -2 2.88 1.18 6 -8 3 1.80 1.80 -6 8 -3 0.27 1.29 -6 8 -3 -0.41 1.20 -6 8 -3 1.48 1.59 -6 8 -3 2.01 1.03 6 -8 3 -1.03 1.82 6 -8 4 0.82 1.83 -6 8 -4 1.84 1.35 -6 8 -4 2.15 1.72 -6 8 -4 1.87 1.41 -6 8 -4 2.22 1.32 6 -8 4 2.00 1.83 -6 8 -4 1.64 1.10 -6 8 -5 42.31 2.73 -6 8 -5 45.46 3.22 -6 8 -5 46.80 2.77 -6 8 -5 41.44 2.55 6 -8 5 42.86 3.18 -6 8 -5 48.00 2.34 -6 8 -6 65.40 3.45 -6 8 -6 61.51 3.81 -6 8 -6 64.34 3.43 -6 8 -6 61.08 3.23 6 -8 6 66.96 3.93 -6 8 -6 63.32 2.82 -6 8 -7 15.57 1.98 -6 8 -7 12.52 1.97 -6 8 -7 15.23 1.45 -6 8 -7 13.85 2.31 -6 8 -8 13.40 1.95 -6 8 -8 13.04 2.24 -6 8 -8 12.11 1.37 -6 8 -9 82.36 4.01 6 -7 -7 36.33 2.76 6 -7 -6 29.38 2.41 -6 7 6 30.68 1.78 -6 7 5 3.52 1.55 6 -7 -5 3.17 1.49 6 -7 -5 1.64 1.45 -6 7 5 1.89 0.89 -6 7 5 3.80 1.14 6 -7 -5 3.23 1.93 6 -7 -4 4.38 1.36 6 -7 -4 1.41 1.44 -6 7 4 2.51 0.90 -6 7 4 3.44 1.18 6 -7 -3 20.00 2.08 6 -7 -3 21.85 1.93 -6 7 3 19.47 1.42 -6 7 3 22.41 1.74 -6 7 2 1.62 1.52 6 -7 -2 2.35 1.43 -6 7 2 1.06 0.86 -6 7 2 1.13 1.12 -6 7 1 214.74 7.11 -6 7 1 204.71 6.79 -6 7 1 216.17 7.75 6 -7 -1 223.83 7.76 6 -7 0 34.36 2.86 -6 7 0 37.78 2.23 -6 7 0 34.11 1.94 -6 7 0 35.45 2.62 6 -7 0 39.29 2.63 6 -7 1 21.07 2.12 6 -7 1 20.18 2.39 -6 7 -1 22.62 2.25 -6 7 -1 24.87 1.66 -6 7 -1 23.89 1.83 6 -7 2 20.43 2.29 6 -7 2 21.11 2.24 -6 7 -2 19.97 1.66 -6 7 -2 21.40 1.69 -6 7 -2 18.21 2.08 -6 7 -2 16.86 1.37 -6 7 -3 141.81 5.61 -6 7 -3 146.91 6.04 -6 7 -3 150.77 5.37 -6 7 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1.36 7 3 5 1.01 1.36 -7 -3 -5 -0.57 1.38 7 3 5 1.20 0.89 7 3 6 25.83 1.69 7 4 -11 22.14 2.32 7 4 -10 1.43 1.46 7 4 -9 3.10 1.14 7 4 -9 1.10 1.30 7 4 -9 1.16 1.30 7 4 -8 19.30 1.63 7 4 -8 22.98 1.87 7 4 -8 20.09 1.84 7 4 -8 20.72 1.30 7 4 -7 3.11 1.14 7 4 -7 4.04 1.21 7 4 -7 3.86 1.16 7 4 -7 3.51 0.75 7 4 -6 0.78 1.07 7 4 -6 1.30 0.85 7 4 -6 1.02 0.56 7 4 -6 1.27 1.02 7 4 -6 0.79 0.64 7 4 -6 -0.11 1.04 7 4 -5 11.58 1.46 7 4 -5 10.18 1.28 7 4 -5 11.21 0.91 7 4 -5 12.29 1.18 7 4 -5 11.12 1.33 7 4 -5 9.61 0.90 7 4 -4 5.46 1.31 7 4 -4 7.10 1.13 7 4 -4 6.62 1.31 7 4 -4 6.37 0.85 7 4 -4 5.64 1.02 7 4 -4 6.36 0.86 7 4 -3 130.82 4.86 7 4 -3 122.59 4.24 7 4 -3 124.10 4.25 7 4 -3 122.66 4.19 7 4 -3 117.48 4.14 7 4 -3 123.40 4.92 7 4 -2 92.87 4.07 7 4 -2 92.75 3.46 7 4 -2 90.21 3.25 7 4 -2 93.45 3.11 7 4 -2 88.46 4.01 7 4 -1 49.08 2.94 7 4 -1 53.04 2.39 7 4 -1 53.52 2.14 7 4 -1 49.74 2.86 7 4 0 72.42 3.11 7 4 0 74.51 3.74 7 4 0 75.82 2.75 7 4 0 70.15 3.52 -7 -4 -1 -0.56 1.11 7 4 1 0.65 0.99 7 4 1 1.46 1.69 7 4 1 1.96 0.77 7 4 2 32.96 2.03 -7 -4 -2 29.61 2.08 7 4 2 32.16 1.63 7 4 3 27.60 2.26 7 4 3 30.02 2.02 -7 -4 -3 28.56 2.21 7 4 3 27.66 1.61 7 4 4 12.47 1.88 7 4 4 14.82 1.71 -7 -4 -4 11.99 1.72 7 4 4 12.52 1.17 7 4 5 79.05 3.16 7 5 -10 3.27 1.55 7 5 -9 8.04 1.31 7 5 -9 8.42 1.53 7 5 -8 19.29 1.71 7 5 -8 17.93 1.95 7 5 -8 16.64 1.74 7 5 -8 16.55 1.30 7 5 -7 5.17 1.29 7 5 -7 5.65 1.37 7 5 -7 5.20 1.23 7 5 -7 7.04 1.02 7 5 -6 20.20 1.79 7 5 -6 20.60 1.54 7 5 -6 21.45 1.65 7 5 -6 23.22 1.20 7 5 -6 21.32 1.76 7 5 -6 19.89 1.35 7 5 -5 -0.28 1.18 7 5 -5 -1.37 1.13 7 5 -5 0.59 0.67 7 5 -5 0.64 1.09 7 5 -5 -1.11 1.05 7 5 -5 0.47 0.81 7 5 -4 10.63 1.51 7 5 -4 11.85 1.20 7 5 -4 14.93 1.73 7 5 -4 12.33 1.14 7 5 -4 12.59 1.37 7 5 -4 10.28 1.16 7 5 -3 120.01 4.91 7 5 -3 117.78 3.93 7 5 -3 122.88 4.26 7 5 -3 115.88 4.31 7 5 -3 120.58 4.92 7 5 -2 57.61 3.15 7 5 -2 58.50 2.53 7 5 -2 52.05 2.43 7 5 -2 53.18 3.03 7 5 -1 1.97 1.40 7 5 -1 1.71 0.97 7 5 -1 2.26 1.48 7 5 -1 1.38 0.86 7 5 0 22.95 2.11 7 5 0 24.25 1.74 7 5 0 24.88 2.33 7 5 0 23.64 1.56 7 5 1 24.20 1.84 -7 -5 -1 25.45 2.05 7 5 1 25.71 2.52 7 5 1 24.22 1.56 7 5 2 72.28 3.16 7 5 2 59.75 3.75 -7 -5 -2 71.75 3.44 7 5 2 63.15 2.73 7 5 3 59.09 2.92 7 5 3 50.32 3.48 7 5 3 51.52 2.44 7 6 -9 3.15 1.43 7 6 -8 34.49 2.25 7 6 -7 4.95 1.37 7 6 -6 4.79 1.32 7 6 -6 7.04 1.51 7 6 -6 6.12 1.18 7 6 -5 3.99 1.33 7 6 -5 4.01 1.31 7 6 -5 6.27 0.97 7 6 -5 3.94 1.32 7 6 -5 4.77 1.13 7 6 -4 18.02 1.85 7 6 -4 16.16 1.93 7 6 -4 18.05 1.40 7 6 -4 16.78 1.75 7 6 -4 12.71 1.52 7 6 -3 25.23 2.17 7 6 -3 27.16 1.71 7 6 -3 23.91 2.32 7 6 -3 25.68 1.90 7 6 -2 6.21 1.64 7 6 -2 7.35 1.25 7 6 -2 4.65 1.66 7 6 -2 5.74 1.33 7 6 -1 21.42 2.15 7 6 -1 22.88 1.75 7 6 -1 22.71 2.37 7 6 -1 26.61 1.79 7 6 0 17.57 2.10 7 6 0 20.34 1.68 7 6 0 16.30 2.29 7 6 0 19.99 1.56 7 6 1 10.54 1.58 7 6 1 11.81 2.26 7 6 1 11.72 1.41 7 6 2 18.38 1.84 7 6 2 13.96 2.30 7 7 -8 100.53 4.26 7 7 -7 93.05 4.10 7 7 -6 0.33 1.38 7 7 -5 0.69 1.31 7 7 -4 52.12 2.49 7 7 -4 44.98 3.03 7 7 -4 47.15 3.06 7 7 -3 30.04 2.56 7 7 -3 33.09 2.10 7 7 -2 16.94 1.62 7 7 -2 15.93 2.28 7 7 -1 99.13 4.90 7 7 -1 95.01 4.02 7 7 0 19.73 1.87 7 7 0 24.69 2.62 7 8 -3 0.82 1.85 7 8 -3 0.13 1.35 7 8 -2 12.87 1.67 7 8 -2 11.26 2.40 8 -8 -1 13.33 2.33 8 -8 0 3.35 2.00 -8 8 0 2.26 1.37 -8 8 -1 63.56 3.26 8 -8 1 68.61 4.01 8 -8 2 0.65 1.89 8 -7 -2 2.51 1.72 8 -7 -1 0.92 1.70 -8 7 1 3.47 1.25 -8 7 0 80.95 3.55 8 -7 0 78.78 4.15 -8 7 -1 148.51 5.54 8 -7 1 152.04 6.25 -8 7 -1 148.59 6.25 8 -7 2 12.90 2.21 -8 7 -2 9.75 1.55 -8 7 -2 12.55 2.20 8 -7 3 -0.82 1.85 -8 7 -3 0.14 1.35 -8 6 5 36.43 2.70 -8 6 4 45.19 2.92 -8 6 3 61.57 3.56 8 -6 -3 63.15 3.38 -8 6 3 70.47 3.61 -8 6 2 14.95 1.98 8 -6 -2 21.45 2.12 8 -6 -2 19.57 2.61 -8 6 2 20.22 1.58 -8 6 2 16.95 2.10 -8 6 1 130.47 5.54 -8 6 1 133.21 4.82 8 -6 -1 131.01 5.87 8 -6 -1 140.00 5.47 -8 6 1 120.35 5.39 8 -6 0 39.39 3.24 -8 6 0 44.69 2.41 8 -6 0 44.24 2.88 -8 6 0 44.03 2.90 -8 6 0 40.78 2.87 8 -6 1 4.88 1.81 -8 6 -1 5.38 1.59 8 -6 1 6.56 2.02 -8 6 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2 3 32.88 2.61 8 2 3 33.67 2.29 8 2 4 4.95 1.48 8 3 -10 -1.63 1.82 8 3 -9 26.55 2.36 8 3 -8 1.74 1.48 8 3 -7 5.22 1.53 8 3 -6 0.86 1.15 8 3 -6 1.82 1.30 8 3 -5 27.79 2.14 8 3 -5 29.56 2.11 8 3 -4 41.35 2.22 8 3 -4 37.43 2.23 8 3 -4 36.51 1.77 8 3 -4 38.38 2.59 8 3 -3 105.39 4.42 8 3 -3 111.14 3.97 8 3 -3 112.06 4.16 8 3 -3 120.45 4.82 8 3 -2 85.05 3.89 8 3 -2 87.06 3.39 8 3 -2 92.84 4.16 8 3 -1 11.06 1.31 8 3 -1 8.43 1.75 8 3 0 50.74 2.51 8 3 0 51.88 3.08 8 3 1 9.90 1.38 8 3 2 29.36 2.03 8 3 3 15.12 1.73 8 4 -10 8.75 1.91 8 4 -9 1.92 1.47 8 4 -8 70.55 3.35 8 4 -8 72.40 3.53 8 4 -7 51.10 2.89 8 4 -7 60.71 3.06 8 4 -6 3.02 1.40 8 4 -6 5.29 1.37 8 4 -5 5.51 1.52 8 4 -4 166.61 5.53 8 4 -4 170.25 6.40 8 4 -4 171.39 6.09 8 4 -3 1.01 1.46 8 4 -3 -1.15 1.49 8 4 -3 0.51 0.87 8 4 -2 147.38 5.73 8 4 -2 148.56 5.10 8 4 -2 136.47 5.68 8 4 -1 5.16 1.60 8 4 -1 3.02 1.14 8 4 -1 3.82 1.71 8 4 0 6.60 1.74 8 4 0 6.71 1.30 8 4 0 3.76 1.69 8 4 1 31.69 2.09 8 4 1 32.25 2.82 8 4 2 119.92 4.75 8 4 2 123.01 5.50 8 5 -7 -0.15 1.36 8 5 -6 21.48 2.03 8 5 -5 1.63 1.33 8 5 -4 44.57 2.84 8 5 -3 -0.18 1.39 8 5 -3 0.48 1.52 8 5 -3 0.46 1.01 8 5 -2 1.59 1.74 8 5 -2 -0.71 1.06 8 5 -1 30.44 2.03 8 5 -1 33.86 2.77 8 5 0 81.89 4.17 8 5 0 76.36 3.41 8 5 1 2.84 1.36 8 5 1 2.36 2.11 8 6 -7 10.43 1.64 8 6 -6 46.36 2.81 8 6 -2 43.96 2.36 8 6 -2 43.18 3.12 8 6 -1 218.15 8.35 8 6 -1 226.75 7.54 8 6 0 2.28 1.30 8 6 0 1.77 2.04 9 -6 0 5.89 1.83 9 -6 1 41.76 3.06 -9 6 -1 44.14 2.47 -9 6 -2 2.97 1.38 9 -6 2 3.12 1.89 9 -5 -1 5.78 2.27 -9 5 1 6.42 1.81 -9 5 0 134.03 4.96 -9 5 0 131.47 5.58 9 -5 0 140.90 6.02 9 -5 0 140.03 5.61 9 -5 1 2.44 1.96 -9 5 -1 2.66 1.76 -9 5 -1 3.70 1.27 9 -5 1 5.67 1.78 -9 5 -2 10.06 1.48 9 -5 2 13.43 2.06 9 -5 2 9.99 2.06 -9 5 -2 12.66 1.97 -9 5 -3 -0.53 1.32 -9 5 -3 -1.45 1.74 9 -5 3 -0.91 1.73 9 -5 3 0.57 1.76 -9 5 -4 6.86 1.90 -9 4 3 4.11 1.51 9 -4 -3 3.60 2.05 -9 4 2 11.53 1.82 9 -4 -2 14.97 2.38 -9 4 1 84.96 4.00 9 -4 -1 86.18 3.92 9 -4 -1 88.90 4.57 9 -4 0 5.06 1.81 -9 4 0 4.37 1.24 -9 4 0 4.42 1.56 9 -4 0 1.80 1.58 -9 4 -1 93.68 3.77 -9 4 -1 87.71 4.10 9 -4 1 86.46 4.11 9 -4 1 88.82 4.39 -9 4 -2 23.53 2.19 -9 4 -2 24.70 1.94 9 -4 2 21.60 2.17 9 -4 2 21.29 2.25 -9 4 -3 102.01 4.20 9 -4 3 99.29 4.52 9 -4 3 101.69 4.65 -9 4 -3 103.32 4.48 -9 3 7 76.17 3.76 -9 3 6 12.28 1.91 -9 3 5 52.63 3.09 9 -3 -5 54.05 3.69 -9 3 4 7.18 1.63 9 -3 -4 12.20 2.27 -9 3 3 5.90 1.67 9 -3 -3 7.76 2.07 -9 3 2 42.71 2.60 9 -3 -2 40.77 2.97 -9 3 2 42.81 2.86 -9 3 1 19.78 2.13 -9 3 1 19.96 1.87 -9 3 1 22.13 1.59 9 -3 -1 24.66 2.38 9 -3 -1 19.34 1.82 -9 3 0 93.49 3.76 -9 3 0 96.35 4.13 9 -3 0 98.07 4.16 9 -3 0 93.86 4.43 9 -3 1 10.58 1.84 -9 3 -1 9.40 1.38 -9 3 -1 12.38 1.70 9 -3 1 8.43 1.66 -9 3 -2 78.25 3.53 -9 3 -2 85.94 3.76 9 -3 2 79.33 3.79 9 -3 2 80.66 3.85 -9 3 -3 20.49 1.94 9 -3 3 22.18 2.27 -9 3 -4 8.05 1.61 9 -3 4 8.15 1.93 9 -2 -6 5.23 2.12 9 -2 -5 33.76 3.01 9 -2 -4 45.15 3.10 -9 2 4 45.15 2.85 -9 2 3 17.88 2.05 9 -2 -3 19.18 2.36 -9 2 2 11.54 1.76 9 -2 -2 12.11 1.53 -9 2 1 15.52 1.35 9 -2 -1 13.31 1.94 -9 2 1 14.15 1.67 9 -2 -1 15.82 1.64 -9 2 0 130.84 4.82 9 -2 0 139.45 5.40 -9 2 0 141.71 5.01 9 -2 1 10.78 1.75 -9 2 -1 9.22 1.33 -9 2 -1 9.24 1.42 9 -2 1 9.44 1.67 -9 2 -2 27.61 2.03 9 -2 2 24.21 2.19 -9 2 -3 52.21 2.74 9 -2 3 48.73 3.01 -9 2 -4 0.68 1.24 9 -2 4 1.19 1.67 9 -1 -7 5.10 1.94 9 -1 -6 32.17 2.79 9 -1 -5 26.94 2.59 9 -1 -4 2.79 1.69 9 -1 -3 -0.18 1.62 9 -1 -2 92.41 3.81 9 -1 -2 111.31 4.54 9 -1 -1 69.52 3.10 9 -1 -1 69.80 3.46 9 -1 0 32.02 2.27 9 -1 0 27.74 2.03 9 -1 1 -0.13 1.35 9 -1 2 1.15 1.34 9 -1 3 22.00 2.08 9 -1 4 18.47 2.14 9 0 -7 0.62 1.86 9 0 -6 17.14 2.20 9 0 -5 2.61 1.74 9 0 -4 2.56 1.57 9 0 -3 67.67 3.49 9 0 -2 28.16 2.12 9 0 -2 19.09 1.61 9 0 -1 28.76 2.12 9 0 -1 29.47 1.94 9 0 0 30.43 2.05 9 0 1 -0.52 1.27 9 0 2 12.86 1.71 9 0 3 13.64 1.88 9 1 -8 -0.61 1.83 9 1 -7 2.52 1.79 9 1 -6 1.46 1.68 9 1 -5 -0.51 1.59 9 1 -4 27.54 2.28 9 1 -3 24.63 2.06 9 1 -2 7.44 1.15 9 1 -1 -1.06 1.10 9 1 0 30.77 2.08 9 1 1 7.90 1.52 9 1 2 136.02 5.25 9 1 3 235.93 8.20 9 2 -3 123.00 5.22 9 2 -2 1.47 1.50 9 2 -1 12.91 1.48 9 2 0 10.24 1.48 9 2 1 73.81 3.43 9 2 2 14.49 1.79 9 3 -5 28.81 2.39 9 3 -4 33.16 2.60 9 3 0 5.60 1.97 9 3 0 5.02 1.38 9 3 1 7.03 1.52 10 -3 -2 68.12 3.93 0 0 0 0.00 0.00 TITL PS_ex80_1 in P-1 REM P-1 (#2 in standard setting) CELL 0.71073 7.387450 9.283227 11.591312 103.1637 95.8453 95.1445 ZERR 3.00 0.000231 0.000282 0.000348 0.0026 0.0025 0.0025 LATT 1 SFAC C H N O UNIT 33.00 30.00 3.00 3.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 8642 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group C1 C 0.21412(17) 0.36090(15) 0.83658(13) 0.0317(3) Uani 1 1 d . . . . . H1 H 0.185827 0.342563 0.913138 0.048 Uiso 1 1 calc R U . . . H2 H 0.178919 0.269645 0.773426 0.048 Uiso 1 1 calc R U . . . H3 H 0.145924 0.440381 0.818149 0.048 Uiso 1 1 calc R U . . . C2 C 0.41582(15) 0.40702(12) 0.84427(10) 0.0196(2) Uani 1 1 d . . . . . C3 C 0.54179(14) 0.28217(12) 0.81778(9) 0.0174(2) Uani 1 1 d . . . . . C4 C 0.50253(14) 0.22040(12) 0.68161(9) 0.0165(2) Uani 1 1 d . . . . . C5 C 0.60140(14) 0.30277(12) 0.60331(9) 0.0177(2) Uani 1 1 d . . . . . H4 H 0.729439 0.278913 0.604670 0.021 Uiso 1 1 calc R U . . . H5 H 0.604476 0.411371 0.635825 0.021 Uiso 1 1 calc R U . . . C6 C 0.50869(14) 0.26136(12) 0.47512(9) 0.0179(2) Uani 1 1 d . . . . . H6 H 0.583547 0.309464 0.425110 0.022 Uiso 1 1 calc R U . . . H7 H 0.500044 0.152161 0.443635 0.022 Uiso 1 1 calc R U . . . C7 C 0.31839(14) 0.31034(11) 0.46764(9) 0.0155(2) Uani 1 1 d . . . . . C8 C 0.17831(14) 0.23004(11) 0.35915(9) 0.0144(2) Uani 1 1 d . . . . . C9 C 0.12351(13) 0.07659(11) 0.38424(9) 0.0145(2) Uani 1 1 d . . . . . C10 C 0.00084(14) 0.07232(11) 0.47988(9) 0.0155(2) Uani 1 1 d . . . . . H8 H -0.125479 0.084225 0.448925 0.019 Uiso 1 1 calc R U . . . H9 H 0.043372 0.156861 0.549394 0.019 Uiso 1 1 calc R U . . . C11 C 0.74197(15) 0.34723(13) 0.85715(10) 0.0222(2) Uani 1 1 d . . . . . H10 H 0.762527 0.382463 0.944323 0.033 Uiso 1 1 calc R U . . . H11 H 0.770018 0.430737 0.820711 0.033 Uiso 1 1 calc R U . . . H12 H 0.821708 0.270202 0.831647 0.033 Uiso 1 1 calc R U . . . C12 C 0.49071(17) 0.16054(13) 0.88303(10) 0.0240(2) Uani 1 1 d . . . . . H13 H 0.575435 0.084764 0.869189 0.036 Uiso 1 1 calc R U . . . H14 H 0.365291 0.114235 0.852671 0.036 Uiso 1 1 calc R U . . . H15 H 0.498826 0.205048 0.968871 0.036 Uiso 1 1 calc R U . . . C13 C 0.01193(14) 0.31830(12) 0.35207(10) 0.0173(2) Uani 1 1 d . . . . . H16 H -0.048266 0.324129 0.425238 0.021 Uiso 1 1 calc R U . . . H17 H 0.054418 0.421111 0.348208 0.021 Uiso 1 1 calc R U . . . C14 C -0.12677(16) 0.24528(13) 0.24271(10) 0.0229(2) Uani 1 1 d . . . . . H18 H -0.178306 0.146171 0.250310 0.027 Uiso 1 1 calc R U . . . H19 H -0.228698 0.307060 0.238916 0.027 Uiso 1 1 calc R U . . . C15 C -0.03768(18) 0.22768(14) 0.12775(11) 0.0269(3) Uani 1 1 d . . . . . H20 H -0.128577 0.174636 0.059087 0.032 Uiso 1 1 calc R U . . . H21 H 0.001394 0.327372 0.115520 0.032 Uiso 1 1 calc R U . . . C16 C 0.12759(17) 0.14128(13) 0.13251(10) 0.0236(2) Uani 1 1 d . . . . . H22 H 0.187526 0.138690 0.059581 0.028 Uiso 1 1 calc R U . . . H23 H 0.085853 0.037372 0.133821 0.028 Uiso 1 1 calc R U . . . C17 C 0.26712(15) 0.21105(12) 0.24267(9) 0.0184(2) Uani 1 1 d . . . . . H24 H 0.321823 0.309584 0.235766 0.022 Uiso 1 1 calc R U . . . H25 H 0.366819 0.147005 0.245782 0.022 Uiso 1 1 calc R U . . . O1 O 0.47829(12) 0.53650(9) 0.86985(8) 0.0271(2) Uani 1 1 d . . . . . O2 O 0.39003(11) 0.11313(9) 0.63852(7) 0.02262(19) Uani 1 1 d . . . . . O3 O 0.27657(11) 0.40836(9) 0.54526(7) 0.02336(19) Uani 1 1 d . . . . . O4 O 0.17989(11) -0.03465(8) 0.33041(7) 0.02153(18) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 C1 0.0214(6) 0.0294(7) 0.0424(7) 0.0017(6) 0.0074(5) 0.0065(5) C2 0.0229(5) 0.0194(5) 0.0169(5) 0.0040(4) 0.0038(4) 0.0044(4) C3 0.0179(5) 0.0149(5) 0.0187(5) 0.0030(4) 0.0013(4) 0.0017(4) C4 0.0145(5) 0.0146(5) 0.0199(5) 0.0027(4) 0.0010(4) 0.0042(4) C5 0.0157(5) 0.0173(5) 0.0194(5) 0.0036(4) 0.0014(4) 0.0006(4) C6 0.0172(5) 0.0181(5) 0.0181(5) 0.0034(4) 0.0032(4) 0.0012(4) C7 0.0184(5) 0.0117(5) 0.0174(5) 0.0062(4) 0.0033(4) 0.0000(4) C8 0.0164(5) 0.0122(5) 0.0155(5) 0.0049(4) 0.0029(4) 0.0013(4) C9 0.0148(5) 0.0138(5) 0.0149(5) 0.0046(4) -0.0003(4) 0.0006(4) C10 0.0163(5) 0.0129(5) 0.0189(5) 0.0062(4) 0.0037(4) 0.0013(4) C11 0.0185(5) 0.0238(6) 0.0213(5) 0.0013(4) -0.0017(4) 0.0016(4) C12 0.0311(6) 0.0196(6) 0.0219(6) 0.0068(4) 0.0031(4) 0.0028(5) C13 0.0185(5) 0.0146(5) 0.0201(5) 0.0064(4) 0.0020(4) 0.0035(4) C14 0.0214(5) 0.0218(6) 0.0261(6) 0.0091(5) -0.0022(4) 0.0035(4) C15 0.0334(6) 0.0264(6) 0.0207(6) 0.0084(5) -0.0048(5) 0.0036(5) C16 0.0316(6) 0.0235(6) 0.0159(5) 0.0049(4) 0.0026(4) 0.0033(5) C17 0.0223(5) 0.0176(5) 0.0168(5) 0.0061(4) 0.0059(4) 0.0015(4) O1 0.0328(5) 0.0171(4) 0.0320(5) 0.0050(3) 0.0078(4) 0.0039(3) O2 0.0221(4) 0.0191(4) 0.0235(4) 0.0025(3) -0.0001(3) -0.0041(3) O3 0.0248(4) 0.0189(4) 0.0233(4) -0.0017(3) 0.0013(3) 0.0059(3) O4 0.0294(4) 0.0142(4) 0.0228(4) 0.0048(3) 0.0086(3) 0.0054(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 C2 C1 121.56(10) . . ? O1 C2 C3 120.89(10) . . ? C1 C2 C3 117.55(10) . . ? C11 C3 C12 110.12(9) . . ? C11 C3 C4 111.86(9) . . ? C12 C3 C4 110.58(9) . . ? C11 C3 C2 109.90(9) . . ? C12 C3 C2 110.12(9) . . ? C4 C3 C2 104.12(8) . . ? O2 C4 C5 121.19(10) . . ? O2 C4 C3 120.94(10) . . ? C5 C4 C3 117.79(9) . . ? C4 C5 C6 111.76(9) . . ? C7 C6 C5 110.95(9) . . ? O3 C7 C6 121.09(9) . . ? O3 C7 C8 120.85(9) . . ? C6 C7 C8 118.05(9) . . ? C17 C8 C7 110.69(8) . . ? C17 C8 C13 110.23(8) . . ? C7 C8 C13 109.98(8) . . ? C17 C8 C9 110.42(8) . . ? C7 C8 C9 103.99(8) . . ? C13 C8 C9 111.37(8) . . ? O4 C9 C10 121.76(9) . . ? O4 C9 C8 121.04(9) . . ? C10 C9 C8 117.18(8) . . ? C9 C10 C10 112.09(11) . 2_556 ? C14 C13 C8 111.53(9) . . ? C15 C14 C13 111.18(9) . . ? C16 C15 C14 111.35(9) . . ? C15 C16 C17 111.98(9) . . ? C16 C17 C8 111.79(9) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag C1 C2 1.5009(16) . ? C2 O1 1.2066(14) . ? C2 C3 1.5470(15) . ? C3 C11 1.5287(15) . ? C3 C12 1.5362(15) . ? C3 C4 1.5391(15) . ? C4 O2 1.2134(13) . ? C4 C5 1.5143(15) . ? C5 C6 1.5199(14) . ? C6 C7 1.5160(14) . ? C7 O3 1.2112(13) . ? C7 C8 1.5420(14) . ? C8 C17 1.5418(14) . ? C8 C13 1.5426(14) . ? C8 C9 1.5449(14) . ? C9 O4 1.2107(13) . ? C9 C10 1.5067(14) . ? C10 C10 1.5179(19) 2_556 ? C13 C14 1.5283(15) . ? C14 C15 1.5279(17) . ? C15 C16 1.5228(17) . ? C16 C17 1.5323(15) . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C2 C3 C11 13.04(14) . . . . ? C1 C2 C3 C11 -167.13(10) . . . . ? O1 C2 C3 C12 134.52(11) . . . . ? C1 C2 C3 C12 -45.65(13) . . . . ? O1 C2 C3 C4 -106.92(11) . . . . ? C1 C2 C3 C4 72.91(12) . . . . ? C11 C3 C4 O2 147.14(10) . . . . ? C12 C3 C4 O2 24.01(14) . . . . ? C2 C3 C4 O2 -94.24(11) . . . . ? C11 C3 C4 C5 -36.04(12) . . . . ? C12 C3 C4 C5 -159.17(9) . . . . ? C2 C3 C4 C5 82.58(11) . . . . ? O2 C4 C5 C6 14.75(14) . . . . ? C3 C4 C5 C6 -162.06(9) . . . . ? C4 C5 C6 C7 64.65(11) . . . . ? C5 C6 C7 O3 21.80(14) . . . . ? C5 C6 C7 C8 -157.28(9) . . . . ? O3 C7 C8 C17 136.32(10) . . . . ? C6 C7 C8 C17 -44.60(12) . . . . ? O3 C7 C8 C13 14.26(13) . . . . ? C6 C7 C8 C13 -166.66(9) . . . . ? O3 C7 C8 C9 -105.10(11) . . . . ? C6 C7 C8 C9 73.98(11) . . . . ? C17 C8 C9 O4 13.51(13) . . . . ? C7 C8 C9 O4 -105.26(11) . . . . ? C13 C8 C9 O4 136.33(10) . . . . ? C17 C8 C9 C10 -167.74(9) . . . . ? C7 C8 C9 C10 73.49(10) . . . . ? C13 C8 C9 C10 -44.92(12) . . . . ? O4 C9 C10 C10 14.53(16) . . . 2_556 ? C8 C9 C10 C10 -164.20(10) . . . 2_556 ? C17 C8 C13 C14 55.46(11) . . . . ? C7 C8 C13 C14 177.78(8) . . . . ? C9 C8 C13 C14 -67.47(11) . . . . ? C8 C13 C14 C15 -56.51(12) . . . . ? C13 C14 C15 C16 55.58(13) . . . . ? C14 C15 C16 C17 -54.55(13) . . . . ? C15 C16 C17 C8 54.28(12) . . . . ? C7 C8 C17 C16 -176.04(9) . . . . ? C13 C8 C17 C16 -54.13(11) . . . . ? C9 C8 C17 C16 69.35(11) . . . . ?