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Information card for entry 7157484
Preview
| Coordinates | 7157484.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C22 H23 Cl N2 O3 |
|---|---|
| Calculated formula | C22 H23 Cl N2 O3 |
| Title of publication | Copper(i)/Ganphos catalysis: enantioselective synthesis of diverse spirooxindoles using iminoesters and alkyl substituted methyleneindolinones. |
| Authors of publication | Cui, Hao; Li, Ke; Wang, Yue; Song, Manman; Wang, Congcong; Wei, Donghui; Li, Er-Qing; Duan, Zheng; Mathey, François |
| Journal of publication | Organic & biomolecular chemistry |
| Year of publication | 2020 |
| Journal volume | 18 |
| Journal issue | 19 |
| Pages of publication | 3740 - 3746 |
| a | 24.1998 ± 0.0014 Å |
| b | 12.37 ± 0.0006 Å |
| c | 9.5879 ± 0.0006 Å |
| α | 90° |
| β | 119.944 ± 0.008° |
| γ | 90° |
| Cell volume | 2487 ± 0.3 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 5 |
| Hermann-Mauguin space group symbol | C 1 2 1 |
| Hall space group symbol | C 2y |
| Residual factor for all reflections | 0.0472 |
| Residual factor for significantly intense reflections | 0.0448 |
| Weighted residual factors for significantly intense reflections | 0.1259 |
| Weighted residual factors for all reflections included in the refinement | 0.1291 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.051 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 252912 (current) | 2020-06-05 | cif/ Updating files of 7157484 Original log message: Adding full bibliography for 7157484.cif. |
7157484.cif |
| 251169 | 2020-04-25 | cif/ Adding structures of 7157484 via cif-deposit CGI script. |
7157484.cif |
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Users of the data should acknowledge the original authors of the
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