Crystallography Open Database

Information card for entry 7157524

Preview

Coordinates	7157524.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H12 Br2 N2 O4 Te
Calculated formula	C16 H12 Br2 N2 O4 Te
Title of publication	Reaction of ketone hydrazones with TeCl<sub>4</sub>: isolation and reactions of novel divinyl telluride.
Authors of publication	Okuma, Kentaro; Qu, Yuxuan; Suetome, Aoi; Nagahora, Noriyoshi
Journal of publication	Organic & biomolecular chemistry
Year of publication	2020
Journal volume	18
Journal issue	24
Pages of publication	4583 - 4589
a	15.726 ± 0.01 Å
b	10.425 ± 0.005 Å
c	13.63 ± 0.008 Å
α	90°
β	121.565 ± 0.008°
γ	90°
Cell volume	1903.9 ± 1.9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0437
Residual factor for significantly intense reflections	0.0339
Weighted residual factors for significantly intense reflections	0.072
Weighted residual factors for all reflections included in the refinement	0.0764
Goodness-of-fit parameter for all reflections included in the refinement	1.041
Diffraction radiation wavelength	0.71075 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
253974 (current)	2020-07-06	cif/ Updating files of 7157523, 7157524 Original log message: Adding full bibliography for 7157523--7157524.cif.	7157524.cif
252474	2020-05-30	cif/ Adding structures of 7157523, 7157524 via cif-deposit CGI script.	7157524.cif