#------------------------------------------------------------------------------ #$Date: 2020-05-30 06:33:03 +0300 (Sat, 30 May 2020) $ #$Revision: 252475 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/75/7157525.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7157525 loop_ _publ_author_name 'you, yong' 'Quan, Bao-Xue' 'Wang, Zhen-Hua' 'Zhao, Jian-Qiang' 'Yuan, Weicheng' _publ_section_title ; Divergent synthesis of oxindole derivatives via controllable reaction of isatin-derived para-quinone methides with sulfur ylides ; _journal_name_full 'Organic & Biomolecular Chemistry' _journal_paper_doi 10.1039/D0OB00979B _journal_year 2020 _chemical_formula_sum 'C31 H33 N O3' _chemical_formula_weight 467.58 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2013 _audit_update_record ; 2020-04-29 deposited with the CCDC. 2020-05-28 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 92.2310(10) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.00370(10) _cell_length_b 20.2706(2) _cell_length_c 13.21220(10) _cell_measurement_reflns_used 6595 _cell_measurement_temperature 290(2) _cell_measurement_theta_max 71.2840 _cell_measurement_theta_min 4.8790 _cell_volume 2677.15(4) _computing_cell_refinement 'CrysAlisPro (Rigaku OD, 2015)' _computing_data_collection 'CrysAlisPro (Rigaku OD, 2015)' _computing_data_reduction 'CrysAlisPro (Rigaku OD, 2015)' _computing_molecular_graphics 'Ortep-3 (L. J. Farrugia, 2001)' _computing_publication_material SHELXL-97 _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1997)' _diffrn_ambient_temperature 290(2) _diffrn_detector_area_resol_mean 5.2169 _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.972 _diffrn_measurement_device_type 'SuperNova, Dual, Cu at zero, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0209 _diffrn_reflns_av_unetI/netI 0.0243 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.972 _diffrn_reflns_limit_h_max 12 _diffrn_reflns_limit_h_min -8 _diffrn_reflns_limit_k_max 24 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_limit_l_min -15 _diffrn_reflns_number 10760 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.972 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 71.214 _diffrn_reflns_theta_min 3.996 _diffrn_source 'micro-focus sealed X-ray tube' _exptl_absorpt_coefficient_mu 0.582 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.74149 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.38.43f (Rigaku Oxford Diffraction, 2015) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_density_diffrn 1.160 _exptl_crystal_description block _exptl_crystal_F_000 1000 _exptl_crystal_size_max 0.290 _exptl_crystal_size_mid 0.270 _exptl_crystal_size_min 0.230 _refine_diff_density_max 0.617 _refine_diff_density_min -0.368 _refine_diff_density_rms 0.040 _refine_ls_extinction_coef 0.0117(7) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.053 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 324 _refine_ls_number_reflns 5046 _refine_ls_number_restraints 7 _refine_ls_restrained_S_all 1.108 _refine_ls_R_factor_all 0.0633 _refine_ls_R_factor_gt 0.0585 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0874P)^2^+0.7914P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1632 _refine_ls_wR_factor_ref 0.1690 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4498 _reflns_number_total 5046 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d0ob00979b2.cif _cod_data_source_block shelxl _cod_original_sg_symbol_H-M 'P 21/n' _cod_database_code 7157525 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.849 _shelx_estimated_absorpt_t_max 0.878 _shelxl_version_number 2013-4 _shelx_res_file ; TITL 161109_a.res in P2(1)/n CELL 1.54184 10.0037 20.2706 13.2122 90.000 92.231 90.000 ZERR 4.00 0.0001 0.0002 0.0001 0.000 0.001 0.000 LATT 1 SYMM 1/2 - X, 1/2 + Y, 1/2 - Z SFAC C H N O UNIT 124 132 4 12 MERG 2 MORE -1 isor 0.004 o3 delu 0.002 c20 o3 FMAP 2 PLAN 9 SIZE 0.23 0.27 0.29 ACTA BOND $H CONF LIST 6 L.S. 4 WGHT 0.087400 0.791400 EXTI 0.011663 FVAR 0.72985 O1 4 0.345389 0.488699 0.558417 11.00000 0.05552 0.06177 = 0.06617 0.01973 0.00400 0.00655 O2 4 0.384010 0.722428 0.461950 11.00000 0.07927 0.04961 = 0.08164 -0.01972 0.02168 -0.01248 N1 3 0.137506 0.531652 0.584601 11.00000 0.05497 0.05219 = 0.05421 0.00403 0.01487 -0.00650 C9 1 0.308280 0.568955 0.354647 11.00000 0.04071 0.03759 = 0.04391 -0.00130 0.00403 -0.00002 C22 1 0.350592 0.502103 0.329159 11.00000 0.04237 0.03665 = 0.05259 0.00138 0.00456 0.00138 AFIX 43 H22 2 0.395845 0.477164 0.378643 11.00000 -1.20000 AFIX 0 C18 1 0.241462 0.606734 0.273223 11.00000 0.04235 0.03561 = 0.05081 -0.00060 0.00211 0.00097 AFIX 43 H18 2 0.219235 0.650393 0.286176 11.00000 -1.20000 AFIX 0 C10 1 0.394603 0.607435 0.431724 11.00000 0.03904 0.04274 = 0.04237 -0.00038 0.00277 -0.00132 AFIX 13 H10 2 0.469154 0.581657 0.461417 11.00000 -1.20000 AFIX 0 C2 1 0.261412 0.586064 0.466484 11.00000 0.04204 0.04001 = 0.04539 -0.00119 0.00514 -0.00250 C3 1 0.136068 0.623525 0.482783 11.00000 0.04579 0.04294 = 0.05272 -0.00627 0.00840 -0.00170 C11 1 0.429990 0.678353 0.412313 11.00000 0.04362 0.04576 = 0.05176 -0.00244 0.00009 -0.00598 C19 1 0.210555 0.582624 0.182011 11.00000 0.04465 0.04593 = 0.04743 0.00120 0.00362 -0.00154 C1 1 0.258330 0.529124 0.540135 11.00000 0.04711 0.04727 = 0.04771 0.00199 0.00358 -0.00396 C21 1 0.326968 0.475382 0.237821 11.00000 0.04989 0.03927 = 0.05520 -0.00413 0.01078 -0.00001 C12 1 0.523987 0.691423 0.330116 11.00000 0.04358 0.05319 = 0.05564 0.00938 0.00039 -0.00540 C4 1 0.063188 0.586661 0.551054 11.00000 0.04974 0.05010 = 0.05750 -0.00765 0.01300 -0.00486 C8 1 0.080940 0.681066 0.444406 11.00000 0.06170 0.04793 = 0.07592 0.00074 0.01620 0.00897 AFIX 43 H8 2 0.129276 0.707613 0.401576 11.00000 -1.20000 AFIX 0 C23 1 0.143157 0.624312 0.098279 11.00000 0.06271 0.06193 = 0.05043 0.00604 -0.00412 0.00467 C27 1 0.383332 0.408002 0.208014 11.00000 0.07002 0.04620 = 0.07423 -0.01241 0.01725 0.00792 C20 1 0.245520 0.513052 0.161540 11.00000 0.09387 0.05714 = 0.05503 -0.01534 -0.01123 0.01328 C13 1 0.579593 0.640960 0.274681 11.00000 0.06550 0.06863 = 0.07636 0.01157 0.02455 0.00120 AFIX 43 H13 2 0.559971 0.597251 0.289503 11.00000 -1.20000 AFIX 0 C5 1 -0.064297 0.604375 0.577384 11.00000 0.05986 0.07027 = 0.08768 -0.00883 0.03065 -0.00327 AFIX 43 H5 2 -0.111803 0.579071 0.622413 11.00000 -1.20000 AFIX 0 C17 1 0.554299 0.756718 0.307503 11.00000 0.06774 0.06002 = 0.08483 0.01787 0.00399 -0.01017 AFIX 43 H17 2 0.517394 0.790888 0.344186 11.00000 -1.20000 AFIX 0 C31 1 0.099922 0.486536 0.664294 11.00000 0.08068 0.07519 = 0.06504 0.01597 0.02068 -0.01449 AFIX 137 H31A 2 0.159491 0.449388 0.666098 11.00000 -1.50000 H31B 2 0.009909 0.471555 0.650995 11.00000 -1.50000 H31C 2 0.105567 0.508899 0.728367 11.00000 -1.50000 AFIX 0 O3 4 0.212032 0.488092 0.081521 11.00000 0.26618 0.09887 = 0.10431 -0.05274 -0.09175 0.06611 C7 1 -0.047487 0.699156 0.470176 11.00000 0.07265 0.06447 = 0.10734 0.00150 0.02324 0.02469 AFIX 43 H7 2 -0.085456 0.737578 0.443473 11.00000 -1.20000 AFIX 0 C6 1 -0.118623 0.660860 0.534589 11.00000 0.05930 0.08511 = 0.11817 -0.00995 0.03132 0.01626 AFIX 43 H6 2 -0.205131 0.673210 0.549700 11.00000 -1.20000 AFIX 0 C16 1 0.639364 0.770536 0.230405 11.00000 0.09084 0.08979 = 0.11559 0.05034 0.02043 -0.01189 AFIX 43 H16 2 0.659426 0.814149 0.215283 11.00000 -1.20000 AFIX 0 C28 1 0.270544 0.359127 0.182669 11.00000 0.10769 0.05533 = 0.11624 -0.03309 -0.00165 -0.00085 AFIX 137 H28A 2 0.211981 0.356632 0.238403 11.00000 -1.50000 H28B 2 0.307870 0.316350 0.170547 11.00000 -1.50000 H28C 2 0.220958 0.373707 0.123141 11.00000 -1.50000 AFIX 0 C15 1 0.694506 0.720518 0.175953 11.00000 0.08530 0.13294 = 0.09732 0.05395 0.03579 0.00434 AFIX 43 H15 2 0.752316 0.730311 0.124593 11.00000 -1.20000 AFIX 0 C30 1 0.466629 0.377670 0.295304 11.00000 0.09946 0.05537 = 0.13536 -0.02169 -0.01683 0.02995 AFIX 137 H30A 2 0.542404 0.405364 0.311226 11.00000 -1.50000 H30B 2 0.496995 0.334721 0.275954 11.00000 -1.50000 H30C 2 0.412902 0.373837 0.353659 11.00000 -1.50000 AFIX 0 C14 1 0.664289 0.655554 0.197292 11.00000 0.08356 0.10851 = 0.09064 0.02093 0.04067 0.01186 AFIX 43 H14 2 0.700792 0.621695 0.159725 11.00000 -1.20000 AFIX 0 C24 1 0.004797 0.598220 0.071758 11.00000 0.09743 0.10344 = 0.13300 0.02179 -0.06200 -0.01373 AFIX 137 H24A 2 0.011088 0.553353 0.049177 11.00000 -1.50000 H24B 2 -0.035982 0.624657 0.018764 11.00000 -1.50000 H24C 2 -0.048671 0.600063 0.130474 11.00000 -1.50000 AFIX 0 C26 1 0.124758 0.694984 0.132239 11.00000 0.14851 0.06177 = 0.10307 0.01663 -0.05350 0.01477 AFIX 137 H26A 2 0.066790 0.695993 0.188440 11.00000 -1.50000 H26B 2 0.085745 0.720359 0.077305 11.00000 -1.50000 H26C 2 0.210076 0.713396 0.152496 11.00000 -1.50000 AFIX 0 C29 1 0.470517 0.416880 0.117329 11.00000 0.18500 0.08796 = 0.15526 -0.02169 0.11259 0.01853 AFIX 137 H29A 2 0.417285 0.433896 0.061209 11.00000 -1.50000 H29B 2 0.507834 0.375089 0.099159 11.00000 -1.50000 H29C 2 0.541501 0.447261 0.134340 11.00000 -1.50000 AFIX 0 C25 1 0.231408 0.625771 0.007099 11.00000 0.15639 0.22809 = 0.08037 0.07386 0.04573 0.08773 AFIX 137 H25A 2 0.321704 0.635890 0.029032 11.00000 -1.50000 H25B 2 0.199203 0.658888 -0.039723 11.00000 -1.50000 H25C 2 0.229007 0.583456 -0.025552 11.00000 -1.50000 AFIX 0 HKLF 4 REM 161109_a.res in P2(1)/n REM R1 = 0.0585 for 4498 Fo > 4sig(Fo) and 0.0633 for all 5046 data REM 324 parameters refined using 7 restraints END WGHT 0.0874 0.7914 REM Highest difference peak 0.617, deepest hole -0.368, 1-sigma level 0.040 Q1 1 0.1254 0.4745 0.1342 11.00000 0.05 0.62 Q2 1 0.1608 0.5849 -0.0050 11.00000 0.05 0.27 Q3 1 0.5246 0.4021 0.2415 11.00000 0.05 0.25 Q4 1 0.2270 0.4864 0.0589 11.00000 0.05 0.22 Q5 1 0.2081 0.6145 0.4757 11.00000 0.05 0.21 Q6 1 0.2655 0.4956 0.0828 11.00000 0.05 0.20 Q7 1 0.3138 0.5117 0.0842 11.00000 0.05 0.19 Q8 1 0.3524 0.4420 0.2226 11.00000 0.05 0.18 Q9 1 0.4982 0.7254 0.3013 11.00000 0.05 0.18 ; _shelx_res_checksum 20779 _shelx_hkl_file ; 0 0 2 913.01 16.36 0 0 3 7.86 0.68 0 0 4 230.24 5.61 0 0 5 4.27 0.67 0 0 6 7.06 0.92 0 0 7 -0.13 0.39 0 0 8 1879.90 36.04 0 0 9 1.23 0.50 0 0 9 2.15 0.89 0 0 10 125.30 3.55 0 0 10 122.19 5.55 0 0 10 121.13 3.84 0 0 11 -0.08 0.40 0 0 11 1.22 0.80 0 0 12 44.29 2.27 0 0 13 -0.32 0.50 0 0 14 4.51 0.66 0 0 15 -0.22 0.34 0 1 1 2971.91 49.29 0 -1 1 2838.53 49.30 0 -1 2 308.55 5.99 0 1 2 287.19 5.98 0 1 3 2000.41 34.34 0 -1 3 1900.32 34.18 0 -1 4 232.35 5.60 0 1 4 230.83 5.70 0 -1 5 50.18 2.28 0 1 5 49.75 2.37 0 1 6 691.60 14.75 0 -1 6 703.79 14.65 0 -1 7 235.25 6.86 0 -1 8 84.92 3.99 0 -1 8 77.03 3.63 0 -1 9 404.38 8.84 0 1 9 407.71 8.72 0 -1 9 413.41 11.22 0 1 9 400.04 10.94 0 -1 10 30.07 1.72 0 1 10 25.87 2.41 0 -1 10 29.81 2.65 0 1 10 27.82 1.63 0 1 11 184.65 7.42 0 1 11 202.61 5.07 0 1 11 192.71 5.38 0 -1 11 190.57 5.43 0 -1 11 199.71 7.82 0 -1 12 8.19 0.97 0 1 12 8.03 0.94 0 1 12 9.02 0.88 0 1 13 2.07 0.54 0 -1 13 3.36 0.67 0 1 14 7.94 0.88 0 -1 14 9.09 0.96 0 -1 15 4.51 0.62 0 1 15 4.40 0.61 0 1 16 0.50 0.22 0 -2 0 1745.75 29.65 0 -2 1 1391.79 24.47 0 -2 1 1425.39 24.32 0 -2 2 344.30 6.79 0 -2 3 951.79 17.45 0 -2 4 875.53 16.23 0 2 4 822.12 16.18 0 -2 5 54.02 2.37 0 -2 6 295.74 7.46 0 -2 7 236.35 6.86 0 -2 7 244.02 7.11 0 -2 8 76.20 3.77 0 -2 8 71.61 3.56 0 -2 9 33.24 1.75 0 -2 9 33.82 2.68 0 2 9 30.80 2.43 0 2 9 34.65 1.70 0 2 10 129.14 3.91 0 2 10 124.05 5.47 0 -2 10 126.00 4.05 0 -2 10 133.27 5.96 0 2 11 -0.41 0.55 0 -2 11 0.06 0.64 0 2 11 -0.61 0.46 0 2 11 -0.14 0.39 0 2 12 52.65 2.48 0 2 12 54.88 2.28 0 -2 12 56.39 2.58 0 2 13 23.35 1.39 0 2 13 23.26 1.56 0 -2 13 24.70 1.64 0 2 14 2.61 0.55 0 -2 14 2.97 0.66 0 2 15 12.81 0.95 0 -2 15 11.43 0.84 0 2 16 1.02 0.26 0 -3 0 -0.02 0.06 0 -3 1 53.39 1.72 0 -3 1 55.48 1.54 0 -3 2 53.31 1.69 0 -3 2 49.22 1.68 0 -3 3 1979.54 34.76 0 -3 4 1717.08 30.86 0 -3 5 35.04 1.87 0 -3 5 34.72 1.97 0 -3 6 130.85 4.31 0 -3 6 131.61 4.54 0 -3 7 309.56 8.39 0 -3 7 303.93 8.04 0 -3 8 9.79 1.22 0 -3 8 12.06 1.47 0 -3 9 61.02 2.48 0 -3 9 66.13 3.85 0 3 9 60.79 2.33 0 3 9 61.43 3.45 0 -3 9 54.06 3.10 0 -3 10 295.18 9.66 0 3 10 291.36 6.84 0 -3 10 281.10 7.05 0 3 10 277.20 8.77 0 3 11 30.61 1.66 0 3 11 29.63 1.73 0 -3 11 28.24 1.80 0 3 12 88.83 3.11 0 -3 12 90.23 3.46 0 3 12 91.09 3.33 0 -3 13 32.53 1.93 0 3 13 30.88 1.65 0 3 13 32.58 1.85 0 3 14 11.25 1.02 0 -3 14 11.03 1.07 0 3 14 10.09 0.84 0 -3 15 2.50 0.40 0 3 15 2.16 0.44 0 3 16 6.09 0.53 0 -4 0 917.22 16.16 0 -4 1 1476.64 25.56 0 -4 1 1446.26 26.03 0 -4 2 204.57 4.64 0 -4 2 204.80 4.59 0 -4 2 204.76 4.87 0 -4 3 1956.04 35.11 0 -4 3 2010.03 35.01 0 -4 4 892.51 17.49 0 -4 4 923.68 17.23 0 -4 5 553.76 11.39 0 -4 5 515.71 11.54 0 -4 6 53.33 2.72 0 -4 6 54.79 2.57 0 -4 7 38.39 2.52 0 -4 7 39.23 2.31 0 -4 8 147.10 5.70 0 -4 8 139.10 5.14 0 -4 9 52.54 3.50 0 4 9 55.09 3.19 0 4 9 51.37 2.12 0 -4 9 47.06 2.95 0 -4 9 53.62 2.34 0 4 10 278.86 6.67 0 -4 10 286.52 9.59 0 -4 10 285.69 7.06 0 4 10 261.89 8.43 0 -4 11 10.63 1.13 0 4 11 9.28 0.98 0 4 11 11.41 1.04 0 -4 12 30.86 1.93 0 4 12 28.96 1.66 0 4 12 30.26 1.79 0 -4 13 2.67 0.68 0 4 13 2.02 0.50 0 4 13 1.82 0.60 0 4 14 16.21 1.17 0 4 14 13.33 0.99 0 4 15 -0.18 0.24 0 -5 0 0.14 0.09 0 -5 -1 1584.92 27.21 0 -5 1 1543.44 27.58 0 -5 1 1586.36 28.20 0 -5 2 127.65 3.36 0 -5 2 121.76 3.57 0 -5 2 132.34 3.42 0 -5 3 105.89 3.24 0 -5 3 98.88 3.00 0 -5 4 3.17 0.57 0 -5 4 0.80 0.27 0 -5 5 22.73 1.51 0 -5 5 21.71 1.61 0 -5 6 15.13 1.30 0 -5 6 15.44 1.52 0 -5 7 1.12 0.44 0 -5 7 1.60 0.69 0 -5 8 72.03 2.68 0 -5 8 65.92 3.81 0 5 9 72.40 3.65 0 -5 9 71.82 2.81 0 5 9 73.02 2.58 0 -5 9 68.15 4.11 0 -5 9 69.43 3.69 0 -5 10 57.34 2.59 0 5 10 56.01 2.35 0 -5 10 56.59 3.96 0 -5 11 120.77 4.16 0 5 11 119.25 3.85 0 5 12 2.81 0.63 0 -5 12 3.10 0.72 0 5 12 3.51 0.67 0 5 13 26.41 1.54 0 -5 13 29.11 1.80 0 5 13 28.35 1.66 0 5 14 3.10 0.57 0 5 14 2.98 0.50 0 5 15 6.79 0.64 0 -6 0 189.22 4.23 0 -6 1 112.86 2.98 0 -6 -1 111.58 2.70 0 -6 1 113.25 3.50 0 -6 2 1.25 0.34 0 -6 2 3.03 0.48 0 -6 3 272.07 6.34 0 -6 3 281.52 6.61 0 -6 4 135.73 3.98 0 -6 4 140.70 4.40 0 -6 5 1478.93 27.93 0 -6 5 1446.58 27.11 0 -6 6 3.80 0.68 0 -6 6 3.65 0.81 0 -6 7 1050.49 21.91 0 -6 7 1012.96 20.69 0 -6 8 33.33 2.31 0 6 8 35.98 1.63 0 -6 8 37.15 2.86 0 -6 8 33.15 1.77 0 6 9 16.49 1.13 0 -6 9 14.34 1.89 0 -6 9 17.94 1.34 0 6 10 14.48 1.14 0 -6 10 13.25 1.99 0 -6 10 14.86 1.31 0 -6 11 21.41 1.60 0 6 11 20.31 1.41 0 -6 12 95.72 3.63 0 6 12 97.21 3.35 0 6 12 93.80 3.27 0 6 13 12.91 1.10 0 6 13 14.36 1.18 0 6 14 1.20 0.36 0 6 14 2.20 0.47 0 6 15 4.03 0.49 0 -7 0 0.23 0.18 0 -7 1 179.13 4.38 0 -7 1 183.31 5.11 0 -7 -1 183.27 4.05 0 -7 2 175.14 5.09 0 -7 2 192.37 4.81 0 -7 3 827.54 16.14 0 -7 3 846.45 16.40 0 -7 4 8.35 1.03 0 -7 4 10.12 0.97 0 -7 5 102.28 4.06 0 -7 5 102.68 3.59 0 -7 6 112.43 4.04 0 -7 6 106.38 4.50 0 -7 7 18.56 1.62 0 -7 7 19.52 1.95 0 -7 8 31.14 1.73 0 -7 8 28.43 2.53 0 7 8 33.01 1.58 0 7 9 0.14 0.33 0 -7 9 -0.21 0.86 0 -7 9 0.12 0.33 0 7 10 161.69 4.54 0 -7 10 168.90 5.06 0 -7 11 26.37 1.81 0 7 11 25.74 1.59 0 7 12 0.46 0.42 0 7 12 1.19 0.55 0 7 13 0.03 0.35 0 7 13 0.72 0.45 0 7 14 0.99 0.37 0 7 14 0.37 0.27 0 7 15 2.36 0.35 0 -8 0 2514.53 43.81 0 -8 1 174.26 5.23 0 -8 1 176.09 4.47 0 -8 -1 173.84 4.01 0 -8 2 322.19 7.28 0 -8 2 318.58 7.97 0 -8 3 868.08 16.85 0 -8 3 859.74 17.12 0 -8 4 448.80 9.88 0 -8 4 431.12 10.24 0 -8 5 443.19 10.04 0 -8 5 443.69 10.89 0 -8 6 57.06 3.30 0 -8 6 61.30 2.93 0 -8 7 70.58 3.93 0 -8 7 67.37 2.57 0 8 8 108.98 3.31 0 -8 8 110.05 5.34 0 -8 8 115.18 3.73 0 -8 9 38.26 3.29 0 -8 9 37.70 2.07 0 8 9 39.75 1.86 0 8 10 34.88 1.81 0 8 11 0.50 0.32 0 8 11 0.30 0.40 0 8 12 30.46 1.68 0 8 12 31.00 1.71 0 8 13 19.65 1.30 0 8 13 21.56 1.32 0 8 14 2.00 0.42 0 8 14 1.88 0.40 0 -9 0 0.79 0.29 0 -9 1 25.56 1.45 0 -9 1 26.79 1.90 0 -9 2 124.20 4.47 0 -9 2 128.99 3.93 0 -9 3 184.45 5.39 0 -9 3 196.79 5.39 0 -9 3 194.98 6.11 0 -9 4 309.12 7.54 0 -9 4 280.20 7.80 0 -9 5 405.48 9.42 0 -9 5 386.57 10.23 0 -9 6 4.80 1.04 0 -9 7 89.07 4.61 0 9 7 89.71 2.83 0 -9 8 16.86 2.15 0 9 8 17.53 1.17 0 -9 9 6.54 1.50 0 9 9 5.95 0.73 0 9 10 15.95 1.21 0 9 11 42.52 2.09 0 9 11 43.37 2.05 0 9 12 14.35 1.16 0 9 12 13.47 1.10 0 9 13 0.64 0.31 0 9 13 0.90 0.35 0 9 14 7.62 0.71 0 9 14 6.61 0.62 0 -10 0 3967.27 67.36 0 -10 0 3745.48 69.35 0 -10 1 335.14 8.87 0 -10 1 325.51 7.57 0 -10 2 435.25 9.85 0 -10 2 456.63 10.95 0 -10 3 54.95 3.06 0 -10 3 49.29 2.45 0 -10 4 99.35 3.68 0 -10 4 85.59 3.72 0 -10 5 2.94 0.76 0 10 6 8.47 0.79 0 -10 6 9.82 1.45 0 10 7 89.58 2.88 0 -10 7 89.58 4.80 0 -10 8 124.44 6.08 0 10 8 122.55 3.63 0 -10 9 38.18 3.44 0 10 9 42.57 1.96 0 10 10 96.71 3.24 0 10 11 9.33 0.91 0 10 11 9.12 0.97 0 10 12 38.66 1.79 0 10 12 33.84 1.77 0 10 13 1.09 0.32 0 10 13 1.64 0.41 0 10 14 0.15 0.24 0 10 14 0.68 0.23 0 -10 14 0.45 0.26 0 -11 0 0.16 0.38 0 -11 1 274.41 8.16 0 -11 2 81.27 3.24 0 -11 2 85.21 3.93 0 -11 3 2.43 0.59 0 -11 3 1.70 0.61 0 -11 3 2.02 0.60 0 -11 4 14.65 1.45 0 -11 5 2.17 0.67 0 11 5 3.58 0.52 0 -11 6 303.71 9.42 0 11 6 316.21 7.07 0 11 6 312.10 6.95 0 11 7 0.58 0.36 0 -11 7 1.25 0.74 0 11 8 8.61 0.85 0 -11 8 9.24 1.66 0 11 9 151.70 4.24 0 11 10 7.86 0.85 0 11 11 21.37 1.34 0 11 11 19.96 1.35 0 11 12 1.84 0.42 0 11 12 1.55 0.47 0 11 13 0.17 0.23 0 11 13 -0.36 0.31 0 11 14 0.96 0.26 0 11 14 1.67 0.33 0 -11 14 1.39 0.32 0 -12 0 357.54 10.15 0 -12 1 36.21 2.71 0 -12 -1 34.08 2.60 0 -12 2 54.20 3.26 0 -12 3 21.50 1.73 0 12 4 23.93 1.30 0 12 4 22.37 1.33 0 -12 4 20.94 1.84 0 12 5 48.99 2.02 0 -12 5 45.91 2.97 0 12 6 8.15 0.83 0 -12 6 8.24 1.37 0 12 6 6.66 0.73 0 -12 7 44.87 3.43 0 12 7 51.64 2.12 0 -12 8 347.74 11.47 0 12 8 373.58 8.10 0 12 9 8.10 0.85 0 12 10 9.97 0.99 0 12 10 8.19 0.84 0 12 11 42.48 1.87 0 12 11 41.93 1.98 0 12 12 5.00 0.64 0 12 12 5.78 0.62 0 12 13 0.00 0.19 0 12 13 0.18 0.28 0 -12 14 -0.13 0.19 0 12 14 0.04 0.18 0 -13 0 -0.08 0.47 0 -13 1 50.37 3.38 0 -13 -1 48.41 3.35 0 -13 2 42.82 3.06 0 13 2 44.38 1.97 0 13 3 39.03 1.72 0 13 3 37.98 1.81 0 13 4 6.58 0.76 0 13 4 6.24 0.70 0 13 5 59.39 2.36 0 13 6 1.87 0.48 0 13 6 2.46 0.56 0 13 7 122.58 3.64 0 13 8 122.81 3.65 0 13 9 1.70 0.43 0 13 10 3.66 0.68 0 13 10 2.70 0.49 0 13 11 77.94 2.59 0 13 11 79.37 2.79 0 13 12 1.16 0.30 0 13 12 0.80 0.34 0 -13 13 -0.34 0.28 0 13 13 0.00 0.22 0 14 0 1.30 0.43 0 14 0 2.09 0.40 0 -14 0 0.69 0.61 0 14 -1 74.48 2.81 0 -14 -1 71.01 4.35 0 -14 1 71.25 4.25 0 14 1 72.08 2.46 0 14 1 73.50 2.73 0 14 2 52.19 2.07 0 -14 -2 53.69 3.77 0 -14 2 54.66 3.68 0 14 2 57.61 2.36 0 14 3 41.76 1.99 0 14 3 40.45 1.82 0 14 4 17.21 1.19 0 14 4 16.58 1.23 0 14 5 58.90 2.41 0 14 6 494.85 10.52 0 14 6 492.30 10.24 0 14 7 145.91 4.10 0 14 8 0.59 0.29 0 14 9 10.50 0.89 0 14 9 10.39 0.99 0 14 10 22.33 1.42 0 14 10 22.34 1.28 0 14 11 10.41 0.93 0 14 11 10.58 0.80 0 14 12 -0.23 0.31 0 -14 13 1.35 0.32 0 14 13 1.06 0.29 0 15 0 0.62 0.30 0 -15 0 1.35 0.86 0 15 0 0.20 0.28 0 -15 1 140.50 6.37 0 15 1 146.67 4.32 0 15 -1 135.24 3.81 0 -15 -1 150.28 6.82 0 15 -1 146.89 4.38 0 15 1 141.02 3.92 0 15 2 2.15 0.45 0 -15 -2 0.73 0.54 0 15 -2 2.00 0.56 0 15 2 1.30 0.47 0 -15 2 2.52 1.06 0 15 3 155.41 4.29 0 15 3 157.26 4.53 0 -15 -3 154.17 7.13 0 15 4 3.46 0.66 0 15 4 2.85 0.60 0 15 5 157.29 4.50 0 15 6 2.91 0.66 0 15 6 2.35 0.46 0 15 7 80.67 2.77 0 15 8 13.86 1.04 0 15 8 16.80 1.24 0 15 9 0.57 0.32 0 15 9 1.10 0.42 0 15 10 38.41 1.63 0 15 10 38.83 1.85 0 15 11 0.63 0.28 0 -15 12 0.33 0.30 0 15 12 0.12 0.22 0 -16 0 10.73 1.70 0 16 0 12.03 1.13 0 16 0 10.84 0.92 0 -16 -1 19.19 2.46 0 16 1 18.32 1.22 0 16 1 19.40 1.41 0 -16 1 20.23 2.40 0 16 -1 19.72 1.47 0 16 -1 17.81 1.17 0 -16 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7 5.72 0.70 2 7 8 164.86 4.51 2 -7 8 148.72 6.60 2 -7 9 98.48 5.47 2 7 9 110.40 3.58 2 7 10 131.64 4.14 2 7 11 17.53 1.35 2 7 12 4.99 0.75 2 7 13 0.68 0.34 2 -7 13 0.80 0.39 2 -7 14 0.96 0.31 2 7 14 0.43 0.33 2 7 15 3.26 0.43 -2 8 15 0.03 0.19 -2 8 14 0.12 0.25 -2 8 14 0.13 0.30 -2 8 13 1.15 0.41 -2 8 13 0.41 0.35 -2 8 12 6.74 0.81 -2 8 11 8.59 0.95 -2 8 10 51.86 2.30 -2 -8 10 50.47 2.45 -2 8 9 10.24 0.94 -2 -8 9 10.16 1.74 -2 -8 9 11.28 1.71 -2 -8 9 9.92 1.01 -2 -8 8 1.53 0.79 -2 8 8 1.88 0.46 -2 -8 8 2.14 0.86 -2 -8 8 1.39 0.41 -2 -8 7 63.40 3.61 -2 -8 7 62.63 2.41 -2 8 7 65.79 2.39 -2 -8 7 65.70 3.79 -2 -8 6 0.25 0.48 -2 -8 6 0.98 0.54 -2 -8 5 1.51 0.55 -2 -8 5 2.03 0.62 -2 -8 4 46.69 2.35 -2 -8 4 46.13 2.79 -2 -8 3 13.76 1.41 -2 -8 3 16.11 1.17 -2 -8 2 147.33 4.35 -2 -8 2 164.74 4.01 2 -8 -1 4091.33 72.13 2 -8 -1 4155.69 71.54 -2 -8 1 4024.79 71.01 2 -8 0 1048.75 20.77 2 -8 0 997.87 19.95 2 -8 1 2.38 0.55 2 -8 1 2.77 0.65 2 -8 2 337.67 8.73 2 -8 2 303.17 8.12 2 -8 3 1.65 0.35 2 -8 4 29.09 2.16 2 -8 5 278.61 8.41 2 -8 6 10.19 1.54 2 8 7 165.09 4.37 2 -8 7 152.16 6.45 2 8 7 157.19 4.17 2 8 8 39.52 1.93 2 -8 8 40.65 3.36 2 -8 9 14.36 2.06 2 8 9 17.02 1.31 2 8 10 87.05 3.19 2 8 11 0.35 0.41 2 8 12 50.37 2.27 2 8 13 1.94 0.46 2 -8 13 1.68 0.43 2 8 14 0.38 0.29 2 -8 14 0.60 0.27 -2 9 14 0.58 0.25 -2 9 14 0.88 0.31 -2 9 13 0.07 0.31 -2 9 13 0.02 0.30 -2 9 12 0.31 0.35 -2 9 11 5.49 0.79 -2 9 10 171.68 4.82 -2 -9 9 0.47 0.71 -2 9 9 -0.05 0.46 -2 -9 8 112.79 5.40 -2 9 8 103.66 3.34 -2 -9 8 99.88 5.09 -2 -9 7 507.62 13.26 -2 -9 7 532.95 13.68 -2 9 7 527.56 10.75 -2 9 6 35.78 1.66 -2 -9 6 38.98 2.83 -2 -9 6 33.30 2.43 -2 -9 5 41.23 2.47 -2 -9 5 44.71 2.93 -2 -9 4 635.33 13.48 -2 -9 4 640.97 14.82 -2 -9 3 475.01 10.01 -2 -9 3 454.32 11.46 -2 -9 2 12.78 1.15 2 -9 -1 602.42 12.79 2 -9 -1 591.37 13.68 -2 -9 1 585.55 12.59 2 -9 0 375.25 9.79 2 -9 0 364.44 8.96 2 -9 1 22.77 1.90 2 -9 1 19.22 1.60 2 -9 2 27.87 2.17 2 -9 2 23.85 1.86 2 -9 3 105.04 4.33 2 -9 4 3.32 0.83 2 -9 5 61.73 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7 6.44 1.51 2 11 7 6.57 0.78 2 11 7 7.21 0.81 2 11 8 47.07 2.17 2 11 9 27.33 1.65 2 11 10 6.54 0.80 2 11 11 -0.30 0.43 2 -11 12 4.92 0.68 2 11 12 2.87 0.56 2 11 12 3.99 0.59 2 11 13 3.63 0.49 2 -11 13 3.16 0.49 -2 12 14 5.09 0.47 -2 12 13 7.94 0.69 -2 12 13 7.57 0.68 -2 12 12 0.38 0.34 -2 12 12 0.23 0.31 -2 12 11 0.98 0.44 -2 12 10 0.47 0.39 -2 12 9 87.17 3.10 -2 12 8 117.90 3.75 2 12 -7 54.53 2.20 -2 12 7 52.95 2.29 2 12 -6 47.12 2.01 -2 -12 6 51.35 3.46 2 12 -5 6.46 0.70 -2 -12 5 8.52 1.40 2 12 -4 224.42 5.33 -2 -12 4 225.73 7.76 -2 12 4 216.52 5.29 -2 -12 3 484.69 12.70 -2 -12 2 19.51 1.75 2 -12 -2 21.33 2.21 2 -12 -1 192.61 7.39 -2 -12 1 207.48 6.66 2 -12 0 14.26 1.46 2 -12 0 13.74 1.81 2 -12 1 29.80 2.58 2 -12 1 27.70 2.12 2 -12 2 167.56 6.76 2 -12 2 152.90 5.77 2 12 3 31.68 1.59 2 12 3 30.04 1.51 2 -12 3 28.80 2.41 2 12 4 89.16 2.89 2 12 4 89.97 3.00 2 -12 4 82.76 4.47 2 12 5 1.68 0.45 2 -12 5 2.20 0.97 2 12 5 1.43 0.46 2 12 6 42.53 1.96 2 12 6 39.25 1.86 2 12 7 2.93 0.59 2 12 7 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9 8 388.52 8.67 -4 -9 7 51.59 3.93 -4 9 7 49.40 2.17 -4 -9 6 1.15 0.88 -4 9 6 -0.36 0.36 4 -9 -5 11.56 1.59 -4 -9 5 9.53 1.55 4 -9 -4 -0.02 0.51 -4 -9 4 -0.05 0.49 4 -9 -3 37.32 2.77 -4 -9 3 36.82 2.92 4 -9 -2 59.04 3.50 4 -9 -1 78.24 3.99 4 -9 -1 77.79 3.89 4 -9 0 59.43 3.39 4 -9 0 61.59 3.50 4 -9 1 917.57 20.16 4 -9 2 2.41 0.78 4 -9 3 83.88 4.49 4 -9 4 0.52 0.30 4 -9 4 1.65 0.73 4 9 5 2.72 0.46 4 9 5 3.44 0.57 4 -9 5 3.70 0.61 4 -9 5 3.81 1.17 4 -9 6 10.36 1.03 4 9 6 10.66 0.99 4 -9 6 10.89 1.90 4 9 6 9.89 0.92 4 9 6 10.36 0.87 4 -9 7 88.81 3.31 4 9 7 85.48 3.22 4 -9 7 88.87 5.47 4 9 7 86.93 3.14 4 9 7 95.64 2.99 4 -9 8 281.33 7.05 4 9 8 275.25 7.01 4 9 8 269.55 6.81 4 -9 9 80.45 3.17 4 9 9 76.85 3.10 4 9 9 76.99 3.03 4 -9 10 276.63 6.93 4 9 10 269.49 6.78 4 9 11 0.79 0.41 4 -9 11 0.63 0.40 4 9 12 0.86 0.37 4 -9 12 0.91 0.33 4 9 13 0.52 0.29 4 -9 13 -0.03 0.19 -4 10 14 7.30 0.57 -4 10 13 0.97 0.33 -4 10 12 8.31 0.81 4 10 -12 9.31 0.79 -4 10 11 1.94 0.52 -4 10 10 23.08 1.47 -4 10 9 69.81 2.71 -4 10 8 1.97 0.51 -4 -10 7 500.23 14.53 -4 10 7 505.45 10.64 -4 -10 6 82.76 4.95 -4 10 6 77.67 2.79 4 -10 -5 83.97 4.68 -4 -10 5 93.28 5.14 -4 -10 4 75.24 4.45 4 -10 -4 69.77 4.16 -4 -10 3 285.74 9.52 4 -10 -3 299.29 9.46 4 -10 -2 -0.52 0.66 4 -10 -1 362.98 10.47 4 -10 -1 348.78 9.98 4 -10 0 7.23 1.27 4 -10 0 5.60 1.09 4 -10 1 27.17 2.39 4 -10 2 8.09 1.35 4 -10 3 81.50 2.83 4 -10 3 75.32 4.41 4 10 3 84.48 2.70 4 10 4 -0.36 0.34 4 -10 4 -0.04 0.29 4 -10 4 -0.21 0.63 4 -10 5 87.53 3.12 4 10 5 83.61 2.96 4 -10 5 83.17 5.03 4 10 5 88.58 2.86 4 -10 6 91.26 3.29 4 10 6 82.16 3.08 4 -10 6 81.96 5.23 4 10 6 91.42 2.94 4 -10 7 276.78 7.10 4 10 7 271.35 6.96 4 -10 7 275.71 10.65 4 10 7 300.45 6.68 4 -10 8 8.99 1.05 4 10 8 7.27 0.93 4 10 8 6.84 0.87 4 -10 9 99.49 3.63 4 10 9 97.19 3.42 4 -10 10 15.94 1.37 4 10 10 14.60 1.22 4 -10 11 29.27 1.68 4 10 11 28.49 1.58 4 -10 12 8.36 0.80 4 10 12 7.94 0.75 4 -10 13 5.46 0.55 4 10 13 5.40 0.53 -4 11 13 5.90 0.58 -4 11 13 5.27 0.55 -4 11 12 2.74 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4 -12 5 55.70 4.30 4 12 5 60.75 2.39 4 12 6 3.15 0.56 4 -12 6 2.30 0.58 4 -12 7 12.48 1.20 4 12 7 12.64 1.07 4 -12 8 50.90 2.46 4 -12 9 6.55 0.93 4 -12 10 2.18 0.59 4 -12 11 2.99 0.56 4 -12 12 8.97 0.77 -4 13 12 0.33 0.24 -4 13 11 0.90 0.40 4 13 -10 42.73 1.85 -4 13 10 46.56 2.01 4 13 -9 6.23 0.71 -4 13 9 7.23 0.83 4 13 -8 11.92 1.06 -4 13 8 11.47 1.07 4 13 -7 32.23 1.79 -4 13 7 36.38 1.90 4 13 -6 72.77 2.81 -4 13 6 75.37 2.88 4 13 -5 38.29 1.92 -4 -13 5 34.55 3.31 4 -13 -5 33.23 3.31 4 13 -4 15.34 1.18 -4 -13 4 14.96 2.20 4 -13 -4 14.45 2.17 4 13 -3 209.58 5.44 -4 -13 3 207.26 8.38 4 -13 -3 215.29 8.72 4 13 -2 3.56 0.59 4 -13 -2 2.91 1.09 4 13 -2 3.12 0.53 4 13 -1 26.63 1.51 4 -13 -1 28.02 2.86 4 13 -1 25.35 1.44 4 13 0 15.64 1.12 4 -13 0 18.90 2.44 4 -13 0 16.75 2.00 4 13 0 19.68 1.29 4 13 1 155.92 4.34 4 -13 1 160.45 4.34 4 13 1 149.40 4.21 4 13 2 271.75 6.41 4 -13 2 269.11 6.48 4 13 2 265.99 6.35 4 -13 2 254.49 9.15 4 13 3 170.69 4.62 4 -13 3 165.14 4.72 4 -13 3 157.98 7.12 4 13 4 5.43 0.74 4 -13 4 5.97 0.81 4 -13 4 6.58 1.57 4 -13 5 62.09 2.73 4 13 5 70.47 2.65 4 -13 6 17.97 1.42 4 13 6 18.82 1.31 4 -13 7 10.06 1.09 4 13 7 7.91 0.87 4 -13 8 1.11 0.54 4 -13 9 58.27 2.56 4 -13 10 19.69 1.37 4 -13 11 18.43 1.19 4 -13 12 22.07 1.13 -4 14 12 12.02 0.78 -4 14 12 12.35 0.79 -4 14 11 5.76 0.63 4 14 -10 3.58 0.49 -4 14 10 4.52 0.64 4 14 -9 0.00 0.26 -4 14 9 1.02 0.41 4 14 -8 2.88 0.55 -4 14 8 4.29 0.69 4 14 -7 5.41 0.71 -4 14 7 5.80 0.76 4 14 -6 3.80 0.63 -4 14 6 2.46 0.55 4 14 -5 93.75 3.24 4 14 -4 0.16 0.31 4 -14 -4 0.07 0.77 -4 -14 4 0.25 0.59 4 14 -3 23.94 1.49 -4 -14 3 26.39 2.87 4 -14 -3 25.49 2.91 4 14 -3 25.95 1.52 4 14 -2 6.79 0.80 4 14 -2 6.91 0.77 -4 -14 2 6.38 1.41 4 -14 -2 5.36 1.47 4 14 -1 38.49 1.88 4 14 -1 38.91 1.85 4 -14 -1 36.90 3.41 4 14 0 -0.06 0.42 4 14 0 1.00 0.42 4 -14 0 0.19 0.66 4 14 1 120.56 3.70 4 -14 1 108.09 5.47 4 14 1 113.89 3.58 -4 14 -1 120.97 3.66 4 14 2 81.46 2.92 4 -14 2 81.56 2.95 4 -14 2 74.91 4.60 4 -14 3 38.24 1.97 4 14 3 40.16 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3.64 5 12 3 229.76 5.65 5 -12 3 217.69 5.85 5 -12 3 215.80 8.74 5 -12 4 40.15 2.12 5 -12 4 37.13 3.48 5 12 4 40.89 1.93 5 -12 5 15.36 1.32 5 12 5 14.90 1.13 5 12 6 0.25 0.31 5 -12 6 0.11 0.47 5 12 7 2.21 0.49 5 -12 7 1.65 0.52 5 -12 8 17.03 1.39 5 -12 9 62.15 2.67 5 -12 10 18.78 1.31 5 -12 11 6.69 0.71 5 -12 12 2.34 0.38 -5 13 12 0.03 0.20 5 13 -11 70.46 2.18 -5 13 11 73.25 2.35 5 13 -10 10.39 0.86 -5 13 10 9.21 0.85 5 13 -9 4.79 0.69 -5 13 9 4.70 0.69 5 13 -8 76.57 2.90 -5 13 8 83.41 2.91 5 13 -7 2.49 0.60 -5 13 7 3.47 0.64 5 13 -6 0.25 0.35 -5 13 6 0.14 0.42 5 13 -5 0.23 0.42 5 13 -4 0.71 0.44 5 13 -3 356.89 8.15 -5 -13 3 343.34 11.90 5 -13 -3 331.89 11.41 5 13 -2 90.56 3.23 -5 -13 2 90.21 5.55 5 -13 -2 93.83 5.52 5 13 -1 146.64 4.34 5 -13 -1 153.99 7.34 5 -13 0 13.92 1.13 5 13 0 14.21 1.16 5 -13 1 55.68 2.39 5 13 1 55.72 2.36 5 -13 1 50.32 3.81 5 13 2 187.90 4.98 5 -13 2 182.71 5.07 5 13 3 112.97 3.59 5 -13 3 109.96 3.74 5 -13 4 29.33 1.80 5 13 4 33.11 1.73 5 -13 5 10.61 1.09 5 13 5 12.21 1.03 5 -13 6 16.93 1.42 5 13 6 16.58 1.20 5 13 7 1.06 0.38 5 -13 7 0.74 0.46 5 -13 8 21.07 1.51 5 -13 9 1.07 0.51 5 -13 10 7.32 0.81 5 -13 11 2.83 0.47 -5 14 11 4.89 0.55 5 14 -10 4.93 0.57 -5 14 10 5.05 0.62 5 14 -9 -0.26 0.38 -5 14 9 -0.15 0.32 5 14 -8 17.07 1.22 -5 14 8 17.82 1.24 5 14 -7 34.58 1.85 -5 14 7 36.42 1.86 5 14 -6 120.59 3.89 -5 14 6 125.63 3.89 5 14 -5 21.76 1.50 5 14 -4 92.77 3.31 5 14 -3 85.72 3.15 5 14 -2 37.00 1.94 5 14 -1 13.28 1.13 5 14 0 610.49 12.56 5 14 1 0.70 0.35 5 -14 1 0.24 0.30 5 14 2 11.88 1.06 5 -14 2 13.18 1.15 5 14 3 4.65 0.70 5 -14 3 3.98 0.68 5 14 4 0.83 0.42 5 -14 4 3.46 0.62 5 -14 5 12.26 1.19 5 14 5 13.83 1.12 5 14 6 0.34 0.31 5 -14 6 0.05 0.44 5 -14 7 12.39 1.20 5 14 7 13.20 1.02 5 -14 8 13.28 1.17 5 -14 9 4.71 0.71 5 -14 10 7.51 0.76 5 -14 11 2.03 0.37 -5 15 11 -0.02 0.19 5 15 -10 -0.22 0.25 -5 15 10 0.05 0.27 5 15 -9 0.26 0.23 -5 15 9 0.23 0.29 5 15 -8 0.79 0.33 -5 15 8 1.06 0.38 5 15 -7 12.68 1.05 -5 15 7 12.51 1.05 5 15 -6 -0.16 0.36 -5 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1 -13 0.27 0.39 -6 1 13 0.39 0.25 6 1 -12 0.56 0.47 6 -1 -12 0.44 0.49 -6 1 12 0.21 0.24 6 1 -11 175.03 5.25 6 -1 -11 184.16 5.30 -6 1 11 165.10 4.57 6 1 -10 11.89 1.28 6 -1 -10 10.86 1.24 -6 1 10 10.71 0.98 6 1 -9 54.04 2.73 6 -1 -9 55.93 2.76 6 1 -8 0.45 0.41 6 -1 -8 0.85 0.49 -6 -1 8 0.99 0.60 -6 1 8 0.66 0.63 6 1 -7 111.91 3.91 6 -1 -7 108.00 3.87 -6 -1 7 107.47 5.51 -6 1 7 102.12 5.18 6 1 -6 10.77 1.08 6 -1 -6 10.08 1.04 -6 -1 6 11.83 1.80 -6 1 6 11.66 1.66 6 1 -5 11.42 1.05 6 -1 -5 10.44 1.00 -6 -1 5 11.06 1.61 -6 1 5 9.42 1.36 6 1 -5 10.43 0.99 6 -1 -5 11.32 0.96 6 1 -4 11.34 1.00 6 -1 -4 11.36 1.00 -6 1 4 10.99 1.42 -6 -1 4 10.40 1.46 6 1 -4 10.94 0.91 6 -1 -4 10.84 0.91 -6 -1 3 7.73 1.23 -6 1 3 6.70 1.09 -6 1 2 424.33 10.03 -6 -1 2 377.41 10.27 -6 -1 1 449.58 11.36 -6 1 1 477.76 10.95 -6 -1 0 79.13 3.62 6 -1 1 5.59 1.06 6 1 2 30.66 2.21 6 -1 2 26.88 2.21 6 1 3 206.97 6.62 6 -1 3 191.29 6.81 6 -1 4 37.80 1.83 6 1 4 40.32 2.70 6 -1 4 37.51 2.85 6 -1 4 41.56 2.02 6 1 4 40.39 1.99 6 -1 5 -0.08 0.36 6 1 5 0.18 0.33 6 -1 5 1.01 0.65 6 -1 6 294.71 7.03 6 -1 6 295.41 9.82 6 -1 6 307.30 7.49 6 1 6 297.23 7.43 6 -1 7 165.44 5.08 6 1 7 163.59 5.09 6 -1 8 379.57 9.14 6 1 8 384.48 9.21 6 -1 9 200.47 5.85 6 1 9 195.68 5.87 6 -1 10 4.38 0.79 6 1 10 4.71 0.86 6 -1 11 0.48 0.36 6 1 11 -0.33 0.46 6 -1 12 -0.22 0.40 6 1 12 -0.27 0.40 6 -1 13 7.62 0.73 6 1 13 7.87 0.74 6 -2 -14 3.99 0.50 6 2 -14 4.23 0.50 6 2 -13 0.33 0.27 6 -2 -13 0.21 0.29 -6 2 13 0.00 0.22 6 2 -12 0.47 0.37 6 -2 -12 -0.27 0.35 -6 2 12 -0.38 0.29 6 2 -11 19.46 1.53 6 -2 -11 21.01 1.58 -6 2 11 17.26 1.21 6 -2 -10 9.52 1.13 6 2 -10 9.19 1.08 -6 2 10 9.91 0.93 6 2 -9 28.25 1.89 6 -2 -9 27.89 1.90 -6 2 9 27.45 1.54 6 2 -8 24.45 1.77 6 -2 -8 24.20 1.76 -6 -2 8 22.45 2.55 -6 2 8 23.20 2.45 6 -2 -7 6.20 0.88 -6 -2 7 6.00 1.38 -6 2 7 6.88 1.25 6 2 -7 7.06 0.95 6 2 -6 15.37 1.27 6 -2 -6 14.17 1.26 -6 2 6 14.68 1.79 -6 -2 6 14.20 1.94 6 -2 -6 14.42 1.14 6 2 -5 147.72 4.39 6 -2 -5 151.28 4.48 -6 -2 5 152.41 6.25 -6 2 5 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0.50 6 -3 6 0.47 0.30 6 -3 6 1.44 0.42 6 -3 7 87.98 3.23 6 -3 7 91.15 5.42 6 -3 7 96.58 3.59 6 3 7 91.83 3.54 6 -3 8 60.72 2.56 6 -3 8 65.48 2.92 6 3 8 63.48 2.94 6 -3 9 40.12 1.96 6 -3 9 44.28 2.34 6 3 9 41.45 2.33 6 -3 10 6.82 0.92 6 3 10 6.12 0.90 6 -3 11 16.90 1.30 6 3 11 17.92 1.39 6 -3 12 0.17 0.28 6 3 12 -0.59 0.44 6 -3 13 37.55 1.55 6 3 13 40.04 1.71 6 4 -14 0.10 0.19 6 -4 -14 0.03 0.20 6 4 -13 5.87 0.67 6 -4 -13 5.64 0.65 -6 4 13 5.71 0.59 6 4 -12 0.94 0.39 6 -4 -12 1.10 0.40 -6 4 12 1.08 0.33 6 4 -11 3.80 0.67 6 -4 -11 3.81 0.68 -6 4 11 3.47 0.52 6 4 -10 66.01 2.89 6 -4 -10 61.60 2.81 -6 4 10 61.78 2.45 6 4 -9 8.67 1.06 6 -4 -9 8.58 1.01 -6 4 9 9.85 0.91 6 4 -8 153.87 4.85 6 -4 -8 147.98 4.78 -6 4 8 154.92 4.25 6 4 -7 22.06 1.58 6 -4 -7 20.08 1.53 -6 -4 7 23.69 2.66 -6 4 7 20.57 2.17 -6 4 7 22.14 1.32 6 4 -6 692.48 14.03 6 -4 -6 674.92 14.04 -6 -4 6 696.74 17.60 -6 4 6 671.78 16.09 6 -4 -6 683.16 13.49 6 4 -5 144.12 4.27 6 -4 -5 144.52 4.32 -6 -4 5 152.36 6.50 6 -4 -5 139.99 3.98 6 4 -4 341.77 7.80 6 -4 -4 341.77 7.85 -6 -4 4 356.77 10.79 6 -4 -4 353.39 7.64 -6 -4 3 317.72 9.79 6 4 -3 316.66 7.20 6 4 -3 320.55 7.13 6 -4 -3 326.50 7.18 -6 -4 2 129.66 5.52 -6 -4 1 148.42 5.87 6 -4 0 344.07 9.99 6 -4 1 73.34 4.03 6 -4 2 2.22 0.46 6 -4 2 1.17 0.64 6 -4 3 132.57 3.98 6 -4 3 130.57 3.52 6 4 3 142.70 3.69 6 -4 3 126.53 5.77 6 -4 3 139.82 4.13 6 4 3 130.64 4.00 6 -4 4 3.15 0.58 6 4 4 3.80 0.60 6 -4 4 1.87 0.42 6 -4 4 3.09 1.08 6 -4 5 78.13 2.96 6 -4 5 81.39 4.85 6 -4 5 84.88 3.18 6 4 5 76.96 3.04 6 -4 6 1.38 0.48 6 4 6 0.82 0.45 6 -4 6 0.64 0.36 6 -4 6 1.19 0.83 6 -4 7 51.97 2.42 6 -4 7 51.46 4.09 6 -4 7 58.05 2.69 6 4 7 53.31 2.59 6 -4 8 27.11 1.66 6 -4 8 28.90 1.88 6 4 8 27.49 1.87 6 -4 9 12.29 1.05 6 -4 9 11.72 1.18 6 4 9 13.91 1.33 6 -4 10 0.26 0.40 6 4 10 0.76 0.46 6 -4 10 0.31 0.28 6 -4 11 3.44 0.60 6 4 11 4.06 0.72 6 -4 12 9.99 0.88 6 4 12 10.04 0.94 6 4 13 11.76 0.87 6 5 -13 5.12 0.59 6 -5 -13 5.17 0.60 -6 5 13 4.66 0.52 6 5 -12 14.78 1.13 6 -5 -12 14.59 1.11 -6 5 12 15.41 1.04 6 5 -11 -0.18 0.41 6 -5 -11 0.18 0.33 -6 5 11 0.26 0.28 6 5 -10 23.73 1.66 6 -5 -10 20.92 1.55 -6 5 10 20.84 1.34 6 5 -9 122.01 4.19 6 -5 -9 120.31 4.16 -6 5 9 121.42 3.68 6 5 -8 21.07 1.58 6 -5 -8 20.78 1.57 -6 5 8 21.35 1.34 6 5 -7 197.64 5.57 6 -5 -7 191.98 5.54 -6 -5 7 207.11 8.42 -6 5 7 196.70 4.98 6 5 -6 70.33 2.85 6 -5 -6 69.56 2.86 -6 -5 6 68.10 4.45 -6 5 6 75.01 2.52 6 -5 -6 69.88 2.57 6 -5 -5 1.92 0.44 6 5 -5 1.74 0.52 6 -5 -5 1.75 0.48 -6 -5 5 1.75 0.61 6 -5 -4 3.13 0.59 6 5 -4 2.25 0.53 6 -5 -4 2.05 0.52 6 5 -3 57.62 2.27 -6 -5 3 55.21 3.70 6 -5 -3 55.79 2.22 6 -5 -2 173.91 4.66 -6 -5 2 162.25 6.56 6 -5 -2 166.39 4.48 -6 -5 1 51.39 3.36 6 -5 0 5.86 1.22 6 -5 1 264.90 6.29 6 -5 1 248.77 8.45 6 -5 2 120.09 3.78 6 5 2 131.37 3.51 6 -5 2 120.73 5.60 6 -5 2 131.60 3.92 6 -5 3 0.11 0.31 6 5 3 0.30 0.26 6 -5 3 0.05 0.28 6 5 3 0.71 0.35 6 -5 3 0.40 0.70 6 -5 4 0.45 0.30 6 5 4 1.06 0.37 6 -5 4 0.94 0.39 6 -5 4 0.74 0.51 6 -5 5 51.62 2.36 6 -5 5 53.76 3.93 6 -5 5 52.84 2.45 6 5 5 49.89 2.36 6 -5 6 0.70 0.43 6 5 6 1.10 0.45 6 -5 6 1.22 0.51 6 -5 6 1.78 0.90 6 -5 7 7.05 0.88 6 -5 7 9.76 1.07 6 5 7 8.67 1.03 6 -5 8 5.69 0.88 6 5 8 5.98 0.90 6 -5 8 5.28 0.76 6 -5 9 7.98 0.97 6 5 9 8.63 1.03 6 -5 9 7.35 0.86 6 -5 10 4.61 0.74 6 5 10 4.43 0.77 6 -5 10 4.21 0.61 6 -5 11 0.87 0.38 6 5 11 0.21 0.40 6 -5 12 9.20 0.80 6 5 12 9.05 0.87 6 5 13 42.30 1.67 6 6 -13 16.05 0.96 6 -6 -13 15.02 0.93 -6 6 13 15.87 0.93 6 6 -12 4.20 0.60 6 -6 -12 4.60 0.63 -6 6 12 4.87 0.60 6 6 -11 0.56 0.36 6 -6 -11 0.92 0.38 -6 6 11 1.20 0.35 6 6 -10 13.20 1.23 6 -6 -10 12.15 1.15 -6 6 10 12.20 1.03 6 6 -9 2.42 0.65 6 -6 -9 1.35 0.53 -6 6 9 1.59 0.44 6 6 -8 175.68 5.20 6 -6 -8 172.28 5.14 -6 6 8 175.50 4.68 6 6 -7 272.02 6.91 6 -6 -7 258.90 6.80 -6 -6 7 285.58 10.24 -6 6 7 272.26 6.34 6 6 -6 14.44 1.23 6 -6 -6 13.11 1.18 -6 -6 6 13.49 1.99 -6 6 6 15.11 1.07 6 -6 -6 16.65 1.17 6 6 -5 22.48 1.45 6 -6 -5 16.84 1.26 -6 -6 5 17.74 2.23 -6 6 5 18.65 1.15 6 -6 -5 19.73 1.27 6 6 -4 643.35 12.92 6 -6 -4 638.11 12.89 -6 -6 4 639.08 16.65 6 -6 -4 641.95 12.71 6 -6 -3 0.24 0.27 6 6 -3 0.47 0.30 6 -6 -3 0.21 0.28 -6 -6 3 0.95 0.54 -6 -6 2 53.37 3.64 6 6 -2 56.99 2.21 6 -6 -2 56.76 2.26 6 -6 -1 52.16 2.21 6 -6 -1 51.90 2.18 6 -6 0 55.61 2.26 6 -6 0 44.76 3.27 6 -6 1 22.93 1.42 6 6 1 21.82 1.21 6 -6 1 20.46 2.20 6 -6 1 23.04 1.42 6 -6 2 22.66 1.45 6 6 2 23.49 1.27 6 -6 2 20.06 2.23 6 -6 2 23.18 1.46 6 6 2 21.54 1.38 6 -6 3 134.41 4.15 6 6 3 146.28 3.79 6 -6 3 131.07 6.18 6 -6 3 147.00 4.29 6 6 3 133.46 4.10 6 -6 4 64.53 2.67 6 -6 4 66.97 4.37 6 -6 4 71.78 2.83 6 6 4 63.39 2.64 6 -6 5 12.07 1.14 6 -6 5 11.65 1.12 6 -6 5 10.59 1.87 6 6 5 12.11 1.12 6 -6 6 7.91 0.94 6 -6 6 9.15 1.03 6 -6 6 9.66 1.76 6 6 6 8.15 0.97 6 -6 7 20.55 1.52 6 -6 7 21.31 1.56 6 6 7 17.97 1.46 6 -6 8 8.90 0.99 6 -6 8 8.24 1.00 6 6 8 8.68 1.04 6 -6 9 19.24 1.41 6 -6 9 23.06 1.59 6 6 9 19.25 1.52 6 -6 10 0.65 0.41 6 6 10 0.23 0.37 6 -6 10 0.26 0.29 6 6 11 0.34 0.31 6 -6 11 0.37 0.31 6 -6 11 0.24 0.25 6 6 12 0.17 0.28 6 6 13 5.98 0.58 6 -7 -13 -0.19 0.22 -6 7 13 0.35 0.23 6 -7 -12 2.53 0.44 6 7 -12 3.07 0.48 -6 7 12 3.05 0.48 6 7 -11 12.76 1.06 6 -7 -11 13.45 1.10 -6 7 11 13.58 1.01 6 7 -10 36.20 1.95 6 -7 -10 37.49 1.97 -6 7 10 34.83 1.75 6 7 -9 140.23 4.42 6 -7 -9 135.43 4.34 -6 7 9 139.94 4.03 6 7 -8 64.96 2.78 6 -7 -8 60.99 2.70 -6 7 8 63.23 2.47 6 7 -7 50.72 2.42 6 -7 -7 48.98 2.34 -6 7 7 50.48 2.13 6 7 -6 195.78 5.42 6 -7 -6 197.13 5.38 -6 -7 6 199.66 8.26 -6 7 6 199.16 5.03 6 -7 -6 198.33 5.03 6 7 -5 36.00 1.87 6 -7 -5 32.28 1.75 -6 -7 5 32.42 3.13 -6 7 5 33.40 1.62 6 -7 -5 32.98 1.65 6 7 -4 15.40 1.20 6 -7 -4 16.02 1.18 -6 -7 4 19.82 2.43 -6 7 4 15.80 1.08 6 -7 -4 17.22 1.17 6 7 -3 37.75 1.81 -6 -7 3 37.81 3.17 6 -7 -3 35.89 1.75 6 -7 -2 0.25 0.35 6 7 -2 0.39 0.26 -6 -7 2 -0.18 0.68 6 7 -1 349.47 7.86 6 7 -1 374.30 7.89 6 -7 -1 371.72 8.20 6 -7 -1 369.27 8.16 6 -7 0 106.64 3.42 6 7 0 99.08 3.10 6 7 0 106.66 3.11 6 -7 0 100.58 5.10 6 -7 0 110.68 3.44 6 -7 1 54.25 2.28 6 7 1 51.30 1.97 6 7 1 49.52 1.92 6 -7 1 48.66 2.15 6 -7 2 121.71 3.86 6 7 2 126.46 3.43 6 -7 2 114.21 5.69 6 -7 2 125.79 3.85 6 -7 3 220.06 5.80 6 -7 3 208.20 8.23 6 -7 3 234.61 5.88 6 7 3 217.28 5.67 6 -7 4 69.26 2.86 6 -7 4 69.70 4.56 6 -7 4 78.91 2.97 6 7 4 66.33 2.71 6 -7 5 25.11 1.65 6 -7 5 24.59 2.76 6 -7 5 27.76 1.72 6 7 5 25.17 1.60 6 -7 6 4.98 0.75 6 7 6 3.99 0.65 6 -7 6 3.45 0.64 6 -7 6 5.08 1.41 6 -7 7 13.28 1.27 6 -7 7 12.91 1.22 6 7 7 11.72 1.15 6 -7 8 16.19 1.35 6 -7 8 16.78 1.36 6 7 8 13.35 1.23 6 -7 9 6.77 0.82 6 7 9 6.29 0.87 6 -7 9 6.30 0.84 6 7 10 4.64 0.73 6 -7 10 4.83 0.67 6 7 11 4.22 0.63 6 -7 11 4.10 0.56 6 7 12 12.33 0.92 6 8 -13 10.87 0.70 -6 8 13 10.05 0.68 6 8 -12 0.18 0.24 6 -8 -12 0.36 0.23 -6 8 12 0.27 0.24 6 8 -11 77.27 2.68 6 -8 -11 83.25 2.77 -6 8 11 77.67 2.63 6 8 -10 8.99 0.93 6 -8 -10 9.35 0.92 -6 8 10 7.83 0.82 6 8 -9 4.54 0.70 6 -8 -9 4.75 0.73 -6 8 9 3.94 0.62 6 8 -8 18.89 1.40 6 -8 -8 17.14 1.34 -6 8 8 18.01 1.26 6 8 -7 289.21 7.06 6 -8 -7 274.45 6.85 -6 8 7 275.69 6.55 6 8 -6 93.77 3.32 -6 -8 6 91.36 5.47 -6 8 6 87.06 2.98 6 8 -5 128.27 3.94 -6 8 5 122.35 3.65 6 -8 -5 123.51 3.64 -6 -8 5 127.62 6.54 6 8 -4 20.29 1.35 -6 -8 4 22.21 2.59 6 -8 -4 20.83 1.30 6 8 -3 41.90 1.91 -6 -8 3 43.37 3.51 6 -8 -3 40.20 1.88 6 8 -2 8.27 0.78 -6 -8 2 6.98 1.36 6 -8 -2 8.99 0.87 6 8 -1 29.69 1.59 6 8 -1 32.81 1.56 6 -8 -1 30.02 1.65 6 -8 0 14.64 1.16 6 8 0 14.46 1.03 6 8 0 15.49 1.03 6 -8 0 14.84 1.13 6 -8 0 12.28 1.78 6 8 1 0.50 0.32 6 -8 1 0.11 0.28 6 8 1 1.60 0.36 6 -8 1 0.24 0.62 6 -8 1 0.28 0.31 6 8 2 526.24 10.73 6 -8 2 531.51 11.34 6 8 2 548.56 10.67 6 -8 2 512.91 14.61 6 -8 2 557.39 11.28 6 -8 3 10.30 1.04 6 -8 3 10.66 1.00 6 -8 3 8.47 1.56 6 -8 4 0.62 0.33 6 8 4 0.41 0.30 6 -8 4 1.29 0.45 6 -8 5 -0.16 0.31 6 8 5 0.62 0.29 6 -8 5 0.36 0.33 6 -8 5 -0.49 0.64 6 -8 6 24.37 1.68 6 8 6 23.41 1.58 6 8 7 1.63 0.39 6 -8 7 0.39 0.50 6 -8 8 13.44 1.22 6 8 8 13.70 1.23 6 -8 9 14.31 1.23 6 8 9 13.06 1.16 6 8 10 -0.23 0.39 6 -8 10 -0.19 0.32 6 8 11 1.64 0.40 6 -8 11 2.05 0.45 6 8 12 0.40 0.25 6 -8 12 0.30 0.21 6 9 -12 6.74 0.64 -6 9 12 6.55 0.63 -6 9 11 34.22 1.60 -6 9 10 11.92 0.98 6 9 -9 5.64 0.76 -6 9 9 5.75 0.72 6 9 -8 59.45 2.52 -6 9 8 54.42 2.27 6 9 -7 17.78 1.33 -6 9 7 17.87 1.25 -6 9 6 121.54 3.69 -6 -9 5 0.41 0.77 -6 9 5 -0.62 0.45 -6 -9 4 332.06 11.53 6 -9 -4 347.72 7.65 6 -9 -3 2.17 0.40 -6 -9 3 1.17 0.72 6 9 -2 63.05 2.52 -6 -9 2 59.30 4.19 6 -9 -2 60.94 2.43 6 9 -1 51.73 2.22 6 -9 -1 52.24 2.27 6 9 0 0.15 0.27 6 -9 0 0.27 0.27 6 -9 0 0.75 0.55 6 -9 0 0.08 0.30 6 -9 1 134.69 4.12 6 9 1 129.93 3.78 6 -9 1 127.08 6.16 6 -9 1 142.38 4.03 6 9 2 48.34 2.00 6 -9 2 46.89 2.25 6 -9 2 44.22 3.63 6 9 3 16.31 1.10 6 -9 3 15.07 1.24 6 -9 3 14.53 2.10 6 -9 4 119.09 3.98 6 -9 4 113.58 6.17 6 -9 5 14.16 1.27 6 -9 6 12.35 1.20 6 9 6 12.45 1.15 6 9 7 4.30 0.67 6 -9 7 4.46 0.69 6 9 8 -0.43 0.56 6 -9 8 -0.55 0.64 6 9 9 7.32 0.86 6 -9 9 7.45 0.89 6 -9 10 23.89 1.47 6 9 10 20.73 1.36 6 9 11 0.82 0.32 6 -9 11 0.96 0.34 6 9 12 4.25 0.48 6 10 -12 6.81 0.61 -6 10 12 7.23 0.62 6 10 -11 8.80 0.81 -6 10 11 8.37 0.75 -6 10 10 1.75 0.41 -6 10 9 6.56 0.74 -6 10 8 1.22 0.39 -6 10 7 53.89 2.27 -6 10 6 160.58 4.49 -6 -10 5 2.40 0.94 -6 10 5 1.14 0.36 -6 -10 4 2.64 1.14 6 10 -3 93.31 3.35 -6 -10 3 97.05 5.62 6 -10 -3 92.21 3.08 6 10 -2 14.52 1.18 -6 -10 2 13.31 1.99 6 -10 -2 14.23 1.09 6 10 -1 39.86 1.94 6 -10 -1 40.86 1.98 6 -10 0 15.13 1.21 6 10 0 15.50 1.14 6 -10 0 14.59 2.06 6 -10 1 58.39 2.50 6 10 1 61.36 2.36 6 10 2 5.13 0.68 6 -10 2 5.61 0.80 6 -10 2 4.54 1.29 6 10 3 309.37 6.93 6 -10 3 308.49 7.51 6 10 4 6.46 0.71 6 -10 4 4.55 0.78 6 -10 5 45.41 2.33 6 -10 6 12.90 1.21 6 -10 7 33.93 2.01 6 10 8 0.91 0.31 6 -10 8 -0.21 0.52 6 10 9 0.78 0.38 6 -10 9 0.25 0.36 6 10 10 1.61 0.46 6 -10 10 1.18 0.43 6 -10 11 8.11 0.75 6 10 11 7.12 0.66 6 11 -12 9.21 0.63 -6 11 12 9.04 0.65 6 11 -11 1.09 0.32 -6 11 11 1.79 0.41 6 11 -10 11.76 0.99 -6 11 10 10.77 0.87 6 11 -9 29.32 1.70 -6 11 9 31.56 1.60 -6 11 8 12.01 1.01 -6 11 7 5.93 0.73 -6 11 6 146.66 4.25 6 11 -5 174.52 5.10 -6 11 5 164.55 4.64 6 11 -4 31.03 1.87 6 11 -3 -0.13 0.44 -6 -11 3 0.38 0.75 6 11 -2 78.10 2.98 -6 -11 2 71.05 4.92 6 -11 -2 79.05 2.85 6 11 -1 237.39 6.02 6 -11 -1 236.33 6.00 6 11 0 49.75 2.18 6 -11 0 47.41 2.22 6 11 1 -0.45 0.43 6 -11 1 -0.19 0.42 6 -11 1 0.19 0.69 6 11 2 92.52 3.09 6 -11 2 96.85 3.46 6 -11 2 90.77 5.37 6 11 3 269.46 6.37 6 -11 3 269.68 6.89 6 11 4 0.29 0.32 6 -11 4 0.79 0.40 6 -11 5 26.37 1.79 6 11 5 31.48 1.58 6 -11 6 5.25 0.79 6 -11 7 48.96 2.45 6 -11 8 5.24 0.76 6 -11 9 41.48 2.04 6 -11 10 14.82 1.12 6 -11 11 -0.19 0.28 6 12 -11 13.59 0.87 -6 12 11 12.58 0.83 6 12 -10 6.72 0.74 -6 12 10 6.43 0.67 6 12 -9 -0.49 0.47 -6 12 9 -0.13 0.31 6 12 -8 -0.82 0.55 -6 12 8 -0.13 0.33 6 12 -7 8.67 0.98 -6 12 7 9.67 0.92 6 12 -6 18.24 1.46 -6 12 6 18.95 1.32 6 12 -5 60.66 2.70 -6 12 5 55.97 2.39 6 12 -4 71.45 2.95 6 12 -3 131.47 4.22 6 12 -2 21.93 1.51 -6 -12 2 17.09 2.44 6 -12 -2 20.61 1.34 6 12 -1 136.30 4.17 6 -12 -1 135.97 4.08 6 12 0 41.20 2.03 6 -12 0 40.69 2.03 6 -12 1 37.93 2.00 6 12 1 36.76 1.86 6 12 2 131.16 3.92 6 -12 2 128.46 4.14 6 12 3 249.15 6.08 6 -12 3 249.35 6.53 6 -12 4 35.30 2.03 6 12 4 34.73 1.74 6 12 5 1.48 0.44 6 -12 5 1.20 0.46 6 -12 6 0.46 0.42 6 -12 7 3.82 0.70 6 -12 8 1.56 0.53 6 -12 9 4.09 0.67 6 -12 10 0.49 0.33 6 -12 11 3.32 0.44 6 13 -11 21.13 1.00 -6 13 11 22.98 1.07 6 13 -10 1.59 0.38 -6 13 10 2.15 0.42 6 13 -9 7.85 0.80 -6 13 9 6.66 0.73 6 13 -8 25.31 1.56 -6 13 8 26.13 1.44 6 13 -7 52.71 2.39 -6 13 7 50.39 2.15 6 13 -6 16.28 1.34 -6 13 6 17.79 1.27 6 13 -5 7.05 0.95 -6 13 5 6.07 0.79 6 13 -4 -0.17 0.45 6 13 -3 33.24 1.91 6 13 -2 3.20 0.67 6 13 -1 11.45 1.07 6 -13 -1 10.78 0.95 6 13 0 7.11 0.85 6 -13 0 7.47 0.86 6 -13 1 64.48 2.67 6 13 1 62.56 2.56 6 13 2 -0.07 0.35 6 -13 2 -0.20 0.42 6 13 3 49.70 2.17 6 -13 3 48.69 2.38 6 13 4 1.46 0.37 6 -13 4 1.83 0.48 6 -13 5 22.85 1.61 6 13 5 22.67 1.36 6 -13 6 11.33 1.14 6 13 6 13.30 0.98 6 -13 7 12.15 1.16 6 -13 8 0.19 0.37 6 -13 9 0.79 0.41 6 -13 10 8.41 0.75 6 14 -10 33.52 1.39 -6 14 10 32.55 1.36 6 14 -9 21.70 1.25 -6 14 9 23.39 1.22 6 14 -8 14.97 1.12 -6 14 8 16.55 1.10 6 14 -7 24.01 1.52 -6 14 7 24.56 1.42 6 14 -6 0.21 0.46 -6 14 6 0.61 0.32 6 14 -5 56.24 2.50 -6 14 5 53.45 2.31 6 14 -4 1.01 0.52 6 14 -3 166.63 4.89 6 14 -2 165.02 4.82 6 14 -1 3.05 0.67 6 14 0 59.64 2.53 6 -14 0 58.04 2.43 6 14 1 23.68 1.52 6 -14 1 27.24 1.64 6 14 2 15.03 1.18 6 -14 2 16.76 1.31 6 14 3 57.59 2.39 6 -14 3 59.50 2.62 6 -14 4 25.92 1.69 6 14 4 24.33 1.45 6 -14 5 9.31 1.02 6 14 5 10.67 0.92 6 -14 6 11.23 1.14 6 14 6 13.77 1.00 6 -14 7 -0.22 0.38 6 -14 8 6.84 0.82 6 -14 9 6.92 0.73 6 -14 10 0.13 0.25 -6 15 10 0.02 0.20 6 15 -9 30.63 1.38 -6 15 9 30.34 1.34 6 15 -8 3.87 0.55 -6 15 8 3.77 0.55 6 15 -7 8.43 0.86 -6 15 7 6.44 0.70 6 15 -6 15.33 1.19 -6 15 6 15.18 1.11 6 15 -5 83.63 3.06 -6 15 5 80.77 2.90 6 15 -4 20.38 1.51 6 15 -3 33.69 1.88 6 15 -2 95.07 3.38 6 15 -1 260.44 6.54 6 15 0 12.04 1.10 6 15 1 19.44 1.37 6 -15 1 20.48 1.39 6 15 2 3.50 0.62 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4.30 7 -6 -6 138.44 4.06 7 6 -5 335.10 7.81 7 -6 -5 321.96 7.69 -7 -6 5 331.06 11.24 7 -6 -5 320.69 7.48 7 6 -4 69.77 2.76 7 -6 -4 70.97 2.75 -7 -6 4 70.73 4.67 7 -6 -4 72.88 2.73 7 6 -3 285.35 6.75 7 -6 -3 271.56 6.64 -7 -6 3 284.66 9.97 7 -6 -3 287.85 6.81 7 6 -2 151.78 4.25 7 -6 -2 147.59 4.17 -7 -6 2 145.13 6.69 7 -6 -2 153.17 4.43 7 6 -1 22.64 1.33 7 -6 -1 21.59 1.29 7 6 -1 21.41 1.33 7 -6 -1 24.67 1.57 7 6 -1 21.62 1.38 -7 -6 1 17.64 2.16 7 -6 -1 21.37 1.44 -7 -6 0 66.89 4.26 7 -6 0 73.68 2.52 7 6 0 74.59 2.58 7 -6 0 75.25 2.90 7 6 0 67.89 2.68 7 -6 0 70.84 2.82 7 -6 1 8.45 0.76 7 6 1 9.14 0.85 7 -6 1 10.62 1.70 7 -6 1 8.05 0.92 7 6 1 7.62 0.84 7 -6 1 8.50 0.91 7 -6 2 7.89 0.92 7 6 2 6.74 0.84 7 -6 2 9.37 0.80 7 6 2 6.86 0.74 7 -6 2 7.86 1.56 7 -6 2 6.56 0.82 7 -6 3 22.70 1.57 7 -6 3 19.54 2.38 7 -6 3 22.17 1.56 7 6 3 19.39 1.43 7 -6 4 0.99 0.55 7 6 4 0.03 0.31 7 -6 4 0.22 0.32 7 -6 4 0.12 0.63 7 -6 5 1.92 0.53 7 6 5 0.86 0.46 7 -6 5 1.12 0.47 7 -6 6 41.65 2.24 7 -6 6 46.37 2.39 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5.42 0.68 7 7 -1 7.27 0.77 -7 -7 1 4.96 1.12 7 7 0 3.13 0.51 7 -7 0 2.36 0.56 7 7 0 3.11 0.51 7 -7 0 3.43 0.63 7 7 1 119.66 3.47 7 -7 1 116.99 3.85 7 -7 1 120.07 3.93 7 -7 2 55.49 2.53 7 7 2 55.11 2.14 7 -7 2 48.70 3.82 7 -7 2 57.81 2.54 7 7 2 54.75 2.40 7 -7 3 28.03 1.79 7 -7 3 29.58 1.80 7 7 3 29.45 1.74 7 -7 4 14.59 1.29 7 -7 4 15.73 1.35 7 7 4 14.94 1.27 7 -7 5 116.42 4.11 7 7 5 112.47 3.97 7 -7 6 34.45 2.04 7 -7 6 38.39 2.13 7 7 6 31.86 1.96 7 -7 7 2.75 0.61 7 7 7 2.44 0.60 7 -7 7 1.97 0.53 7 -7 8 18.55 1.41 7 -7 8 19.62 1.42 7 7 8 18.06 1.42 7 -7 9 4.31 0.64 7 7 9 4.53 0.67 7 -7 9 5.77 0.75 7 -7 10 7.89 0.76 7 7 10 9.12 0.89 7 7 11 2.68 0.45 7 -7 11 2.96 0.39 7 8 -12 0.26 0.26 7 8 -11 15.40 0.95 -7 8 11 14.38 0.89 7 8 -10 6.82 0.75 7 -8 -10 6.84 0.72 -7 8 10 6.27 0.65 7 8 -9 4.03 0.62 7 -8 -9 4.08 0.62 -7 8 9 4.28 0.58 7 8 -8 11.75 1.06 7 -8 -8 14.21 1.20 -7 8 8 11.95 0.95 7 8 -7 4.26 0.67 7 -8 -7 6.01 0.78 -7 8 7 5.87 0.71 7 -8 -6 3.95 0.65 7 8 -6 2.76 0.55 -7 8 6 3.08 0.54 7 8 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9 2.46 0.47 7 9 -8 9.09 0.89 -7 9 8 8.81 0.83 7 9 -7 5.07 0.68 -7 9 7 5.55 0.66 7 9 -6 21.78 1.43 -7 9 6 19.76 1.25 7 9 -5 12.31 1.09 -7 9 5 10.85 0.92 7 -9 -5 11.27 1.00 -7 9 4 143.46 4.07 7 -9 -4 146.76 4.22 7 9 -3 167.54 4.88 7 9 -3 177.43 4.67 -7 -9 3 157.31 7.60 7 -9 -3 160.53 4.61 7 9 -2 3.18 0.58 7 -9 -2 2.02 0.53 7 9 -2 3.03 0.53 -7 -9 2 1.70 0.84 7 9 -1 3.73 0.62 7 -9 -1 2.95 0.58 7 9 -1 4.49 0.61 -7 -9 1 3.73 1.05 7 9 0 75.66 2.55 7 -9 0 71.68 2.88 7 9 1 10.77 0.91 7 9 1 11.86 0.94 7 -9 1 11.77 1.09 7 -9 1 9.82 1.79 7 -9 1 10.75 1.11 7 -9 2 2.95 0.63 7 -9 2 3.03 0.61 7 -9 3 111.80 3.94 7 -9 3 115.16 3.78 7 -9 4 28.02 1.82 7 -9 4 28.84 1.74 7 -9 5 76.87 3.20 7 -9 6 8.24 0.99 7 9 6 9.04 0.96 7 9 7 0.36 0.34 7 -9 7 -0.26 0.53 7 -9 8 23.56 1.58 7 9 8 22.51 1.45 7 9 9 1.05 0.38 7 -9 9 1.75 0.47 7 9 10 1.05 0.32 7 -9 10 0.77 0.32 7 -9 11 -0.08 0.18 7 10 -11 1.00 0.33 -7 10 11 0.98 0.28 7 10 -10 66.23 2.41 -7 10 10 61.20 2.08 -7 10 9 39.86 1.69 -7 10 8 11.11 0.92 -7 10 7 39.35 1.79 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1.92 0.59 7 11 3 11.75 0.95 7 -11 3 12.02 1.21 7 -11 4 7.78 0.95 7 -11 5 0.88 0.50 7 -11 6 70.57 2.97 7 -11 7 25.51 1.66 7 -11 8 13.09 1.13 7 -11 9 9.56 0.90 7 -11 10 3.37 0.48 7 12 -10 16.55 1.01 -7 12 10 15.72 0.87 7 12 -9 0.13 0.29 -7 12 9 0.35 0.27 7 12 -8 0.76 0.39 -7 12 8 0.60 0.33 7 12 -7 5.78 0.82 -7 12 7 6.13 0.70 7 12 -6 0.10 0.49 -7 12 6 0.37 0.27 7 12 -5 76.47 3.05 -7 12 5 70.36 2.59 7 12 -4 1.57 0.54 -7 12 4 1.02 0.41 7 12 -3 100.40 3.57 7 -12 -3 98.39 3.16 7 12 -2 8.34 0.97 7 -12 -2 7.52 0.84 7 12 -1 0.37 0.40 7 -12 -1 0.24 0.39 7 12 0 229.96 5.90 7 -12 0 236.95 6.10 7 12 1 19.92 1.33 7 -12 1 19.71 1.45 7 12 2 47.90 2.06 7 -12 2 47.41 2.34 7 12 3 25.22 1.43 7 -12 3 28.17 1.77 7 -12 4 0.02 0.44 7 -12 5 34.47 1.97 7 -12 6 18.72 1.43 7 -12 7 0.00 0.35 7 -12 8 4.04 0.67 7 -12 9 6.64 0.73 7 -12 10 12.05 0.80 7 13 -10 0.84 0.28 -7 13 10 0.86 0.22 7 13 -9 3.90 0.56 -7 13 9 3.10 0.42 7 13 -8 36.58 1.75 -7 13 8 31.84 1.44 7 13 -7 8.63 0.91 -7 13 7 7.94 0.74 7 13 -6 3.65 0.67 -7 13 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0.52 7 20 -1 1.98 0.34 7 20 0 2.42 0.38 7 20 1 92.06 2.48 8 0 -12 7.18 0.67 8 0 -11 -0.35 0.33 8 0 -10 16.49 1.28 8 0 -9 0.16 0.42 8 0 -8 20.80 1.58 8 0 -7 -0.10 0.43 8 0 -6 29.22 1.89 8 0 -5 0.06 0.44 8 0 -4 11.58 1.13 8 0 -4 11.00 1.11 8 0 -3 0.35 0.37 8 0 -3 0.00 0.35 8 0 -2 35.12 1.87 8 0 -2 35.03 2.02 8 0 -2 35.20 1.88 8 0 -1 0.83 0.40 8 0 -1 -0.15 0.28 8 0 -1 -0.01 0.40 8 0 0 108.93 3.47 8 0 0 106.44 3.77 8 0 0 106.91 3.57 8 0 1 -0.26 0.37 8 0 1 -0.28 0.42 8 0 1 -0.64 0.50 8 0 2 160.92 4.41 8 0 2 155.57 4.89 8 0 2 156.76 4.59 8 0 3 0.70 0.55 8 0 3 0.09 0.37 8 0 3 0.48 0.43 8 0 4 60.72 2.85 8 0 4 63.90 2.60 8 0 5 -0.16 0.50 8 0 5 -0.30 0.28 8 0 6 4.47 0.80 8 0 7 0.32 0.50 8 0 8 31.51 2.00 8 0 9 0.59 0.43 8 0 10 13.49 1.14 8 0 11 -0.06 0.27 8 1 -12 2.05 0.41 8 -1 -12 2.06 0.39 8 1 -11 0.82 0.37 8 -1 -11 1.14 0.37 8 1 -10 0.15 0.32 8 -1 -10 0.18 0.36 8 1 -9 0.56 0.39 8 -1 -9 0.08 0.38 8 1 -8 1.97 0.59 8 -1 -8 2.53 0.67 8 1 -7 11.64 1.23 8 -1 -7 14.04 1.33 8 1 -6 17.21 1.45 8 -1 -6 16.73 1.42 8 1 -5 35.65 2.05 8 -1 -5 36.11 2.06 8 -1 -5 37.40 1.97 8 1 -4 19.58 1.48 8 -1 -4 21.49 1.54 8 1 -4 23.31 1.56 8 -1 -4 22.08 1.52 8 1 -3 5.19 0.77 8 -1 -3 5.38 0.77 8 1 -3 3.88 0.63 8 -1 -3 4.72 0.72 8 1 -2 5.00 0.79 8 -1 -2 4.95 0.74 8 1 -2 4.04 0.69 8 -1 -2 3.53 0.60 8 -1 -2 4.67 0.79 8 1 -2 4.69 0.77 8 -1 -1 43.47 2.07 8 1 -1 42.89 2.05 8 -1 -1 44.43 2.29 8 1 -1 43.98 2.23 8 1 -1 45.26 2.12 8 -1 -1 45.89 2.16 8 -1 0 72.23 2.70 8 1 0 70.39 2.66 8 -1 0 67.00 2.89 8 1 0 68.67 2.90 8 1 0 69.28 2.71 8 -1 0 70.46 2.78 8 1 1 3.65 0.59 8 -1 1 2.99 0.54 8 -1 1 3.07 0.54 8 1 1 2.62 0.52 8 -1 1 3.00 0.62 8 1 1 3.50 0.64 8 -1 2 15.76 1.16 8 1 2 15.93 1.16 8 -1 2 15.00 1.33 8 1 2 16.61 1.38 8 1 2 16.53 1.24 8 -1 2 14.96 1.24 8 -1 3 217.74 5.43 8 1 3 216.61 5.46 8 -1 3 210.72 6.04 8 1 3 209.34 6.00 8 1 3 218.87 5.64 8 -1 3 212.73 5.72 8 -1 4 0.77 0.40 8 1 4 -0.12 0.47 8 1 4 -0.34 0.36 8 -1 4 0.76 0.36 8 -1 5 75.80 3.21 8 1 5 74.22 3.22 8 -1 5 71.04 2.81 8 -1 6 32.49 2.08 8 1 6 31.33 2.04 8 -1 6 33.31 1.77 8 -1 7 0.78 0.53 8 1 7 0.53 0.47 8 -1 8 17.55 1.48 8 1 8 20.89 1.60 8 -1 9 1.68 0.51 8 1 9 2.49 0.61 8 -1 10 0.21 0.31 8 1 10 0.31 0.39 8 -1 11 0.00 0.29 8 1 11 0.34 0.29 8 2 -12 13.02 0.88 8 -2 -12 14.27 0.91 8 2 -11 7.76 0.79 8 -2 -11 7.79 0.80 8 2 -10 0.70 0.44 8 -2 -10 0.51 0.37 8 2 -9 20.33 1.48 8 -2 -9 21.92 1.55 8 2 -8 39.80 2.17 8 -2 -8 37.21 2.14 8 2 -7 3.77 0.72 8 -2 -7 4.00 0.80 8 2 -6 10.67 1.14 8 -2 -6 9.98 1.11 8 2 -5 122.47 4.09 8 -2 -5 116.14 4.07 8 -2 -5 124.95 3.94 8 2 -4 51.93 2.44 8 -2 -4 56.10 2.55 8 -2 -4 55.09 2.44 8 2 -3 31.55 1.80 8 -2 -3 30.96 1.80 8 2 -3 35.00 1.89 8 -2 -3 33.26 1.86 8 2 -2 1.24 0.46 8 -2 -2 0.99 0.44 8 2 -2 0.97 0.39 8 -2 -2 0.22 0.36 8 2 -2 1.30 0.52 8 -2 -1 41.04 1.97 8 2 -1 40.24 1.95 8 -2 -1 38.15 2.11 8 2 -1 36.10 2.02 8 2 -1 39.03 1.96 8 -2 -1 36.68 1.96 8 -2 0 62.53 2.49 8 2 0 62.32 2.46 8 -2 0 62.96 2.78 8 2 0 60.01 2.68 8 2 0 61.62 2.50 8 -2 0 62.51 2.64 8 -2 1 74.71 2.73 8 2 1 74.78 2.72 8 -2 1 74.79 3.07 8 2 1 74.22 3.06 8 2 1 75.62 2.81 8 -2 1 74.61 2.92 8 -2 2 11.76 1.01 8 2 2 10.76 0.97 8 -2 2 10.61 1.13 8 2 2 11.47 1.17 8 2 2 12.52 1.07 8 -2 2 10.68 1.07 8 -2 3 32.63 1.69 8 2 3 31.59 1.68 8 -2 3 32.51 1.99 8 2 3 29.63 1.91 8 2 3 33.02 1.73 8 -2 3 31.05 1.82 8 -2 4 7.76 0.99 8 2 4 6.74 0.92 8 -2 4 8.78 0.96 8 -2 5 9.64 1.12 8 2 5 9.53 1.12 8 -2 5 8.08 0.93 8 -2 6 7.98 1.06 8 2 6 8.68 1.12 8 -2 6 7.08 0.85 8 -2 7 0.90 0.48 8 2 7 0.19 0.45 8 -2 7 0.94 0.40 8 -2 8 35.00 2.07 8 2 8 35.77 2.14 8 -2 9 28.71 1.78 8 2 9 34.54 1.95 8 -2 10 5.38 0.71 8 2 10 7.14 0.84 8 -2 11 3.00 0.47 8 2 11 3.43 0.52 8 3 -12 0.29 0.24 8 -3 -12 0.22 0.23 8 3 -11 3.58 0.54 8 -3 -11 4.19 0.60 8 3 -10 1.62 0.47 8 -3 -10 1.16 0.41 8 3 -9 8.60 1.00 8 -3 -9 8.19 0.97 8 3 -8 6.80 0.93 8 -3 -8 6.02 0.88 8 3 -7 57.72 2.66 8 -3 -7 54.21 2.61 8 3 -6 31.16 1.92 8 -3 -6 30.10 1.89 8 3 -5 141.28 4.48 8 -3 -5 144.61 4.55 8 -3 -5 140.69 4.30 8 -3 -4 0.51 0.47 8 3 -4 0.79 0.42 8 -3 -4 0.58 0.35 8 3 -3 1.46 0.60 8 -3 -3 1.66 0.58 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0.57 8 -4 -12 7.53 0.60 8 4 -11 2.81 0.45 8 -4 -11 3.22 0.49 8 4 -10 20.37 1.33 8 -4 -10 19.66 1.30 8 -4 -9 8.20 0.92 8 4 -9 7.47 0.91 8 4 -8 0.14 0.42 8 -4 -8 -0.46 0.42 8 4 -7 9.15 1.03 8 -4 -7 7.63 0.97 8 4 -6 49.13 2.39 8 -4 -6 48.69 2.40 8 4 -5 179.96 5.21 8 -4 -5 186.11 5.32 8 -4 -5 185.63 5.12 8 4 -4 9.96 1.04 8 -4 -4 11.91 1.13 8 -4 -4 9.62 1.01 8 4 -3 22.02 1.47 8 -4 -3 22.23 1.50 -8 -4 3 19.43 2.29 8 -4 -3 24.26 1.58 8 4 -2 1.09 0.54 8 -4 -2 1.24 0.53 8 4 -2 0.45 0.36 8 -4 -2 0.14 0.30 8 -4 -1 57.21 2.36 8 4 -1 57.08 2.36 8 -4 -1 58.78 2.68 8 4 -1 55.04 2.51 8 4 -1 61.37 2.48 8 -4 -1 57.71 2.54 8 4 0 1.09 0.45 8 -4 0 0.57 0.35 8 -4 0 1.07 0.37 8 4 0 1.07 0.40 8 -4 0 1.26 0.47 8 4 0 0.45 0.34 8 -4 1 6.85 0.87 8 -4 1 6.66 0.75 8 4 1 6.39 0.76 8 4 1 8.42 0.85 8 -4 1 7.57 0.94 8 4 1 6.95 0.87 8 -4 2 35.20 1.72 8 4 2 35.51 1.75 8 -4 2 36.24 2.08 8 4 2 32.97 1.96 8 -4 2 33.66 1.95 8 4 3 0.27 0.38 8 -4 3 0.29 0.47 8 -4 4 83.75 3.37 8 4 4 75.35 3.21 8 -4 4 78.91 3.14 8 -4 5 110.52 3.97 8 4 5 102.72 3.86 8 -4 5 101.99 3.66 8 -4 6 17.45 1.51 8 4 6 17.20 1.49 8 -4 6 17.52 1.37 8 -4 7 0.92 0.53 8 4 7 1.25 0.59 8 -4 7 1.52 0.47 8 -4 8 38.76 2.12 8 4 8 40.53 2.19 8 -4 8 38.41 1.83 8 -4 9 0.51 0.40 8 4 9 0.46 0.40 8 -4 10 6.22 0.73 8 4 10 6.68 0.78 8 4 11 0.02 0.29 8 -4 11 0.09 0.23 8 5 -11 0.53 0.29 8 -5 -11 0.01 0.23 8 5 -10 14.21 1.06 8 -5 -10 13.43 1.03 8 5 -9 0.83 0.36 8 -5 -9 1.11 0.41 8 5 -8 17.63 1.34 8 -5 -8 20.09 1.43 8 5 -7 8.02 0.90 8 -5 -7 7.81 0.93 8 5 -6 1.82 0.52 8 -5 -6 2.08 0.53 8 5 -5 35.70 1.97 8 -5 -5 35.33 1.96 8 -5 -5 38.33 1.96 8 5 -4 80.01 3.05 8 -5 -4 82.95 3.07 8 -5 -4 81.68 3.03 8 -5 -3 3.19 0.69 8 5 -3 2.25 0.55 8 -5 -3 2.32 0.49 -8 -5 3 1.68 0.89 8 5 -2 1.10 0.34 8 -5 -2 1.50 0.49 8 -5 -2 0.69 0.35 8 5 -2 0.71 0.34 8 -5 -1 15.75 1.17 8 5 -1 14.84 1.16 8 -5 -1 16.40 1.41 8 5 -1 17.95 1.35 -8 -5 1 16.05 2.10 8 5 -1 18.67 1.32 8 -5 -1 14.81 1.25 8 -5 0 16.55 1.16 8 5 0 16.49 1.18 8 -5 0 16.69 1.40 8 5 0 16.12 1.29 8 5 0 16.36 1.21 8 -5 0 15.52 1.28 8 -5 1 13.05 1.00 8 5 1 10.78 0.95 8 -5 1 13.40 1.23 8 5 1 10.79 1.07 8 -5 1 11.55 1.10 8 -5 2 4.21 0.75 8 -5 2 4.92 0.66 8 5 2 4.01 0.61 8 -5 2 3.93 0.69 8 5 2 2.90 0.60 8 -5 3 63.10 2.83 8 5 3 53.43 2.57 8 -5 3 59.23 2.67 8 5 4 2.39 0.61 8 -5 4 3.16 0.71 8 -5 4 2.82 0.68 8 -5 5 32.87 2.01 8 5 5 30.67 1.97 8 -5 5 32.21 1.94 8 5 6 8.72 1.06 8 -5 6 9.61 1.12 8 -5 6 9.72 1.10 8 -5 7 6.83 0.93 8 5 7 5.43 0.83 8 -5 7 5.88 0.80 8 -5 8 3.94 0.70 8 5 8 3.05 0.65 8 -5 8 3.53 0.62 8 -5 9 16.68 1.20 8 5 9 14.75 1.21 8 -5 9 15.02 1.01 8 -5 10 7.58 0.74 8 5 10 7.75 0.79 8 5 11 1.28 0.31 8 6 -12 24.83 1.08 8 6 -11 -0.10 0.23 8 -6 -11 0.04 0.20 8 6 -10 6.82 0.72 8 -6 -10 8.54 0.77 8 6 -9 1.20 0.40 8 -6 -9 1.31 0.41 8 6 -8 0.35 0.37 8 -6 -8 0.33 0.33 8 6 -7 -0.42 0.58 8 -6 -7 0.45 0.43 8 6 -6 148.66 4.49 8 -6 -6 143.63 4.39 8 6 -5 58.76 2.55 8 -6 -5 57.39 2.49 8 -6 -5 58.81 2.47 8 6 -4 77.22 2.94 8 -6 -4 76.35 2.88 8 -6 -4 78.06 2.94 8 6 -3 258.84 6.41 8 -6 -3 256.89 6.32 8 -6 -3 263.14 6.54 8 6 -2 35.70 1.75 8 -6 -2 34.43 1.76 8 6 -2 38.03 1.87 -8 -6 2 40.09 3.49 8 -6 -2 38.03 2.02 8 -6 -1 3.22 0.65 8 -6 -1 4.01 0.58 8 6 -1 3.61 0.55 8 6 -1 4.19 0.68 8 -6 0 2.64 0.57 8 -6 0 3.45 0.54 8 6 0 2.64 0.53 8 -6 0 3.03 0.67 8 6 0 2.61 0.53 8 -6 1 27.48 1.45 8 6 1 27.12 1.50 8 -6 1 29.56 1.83 8 6 1 26.53 1.65 8 -6 1 26.11 1.71 8 6 2 17.39 1.19 8 -6 2 16.77 1.39 8 6 2 16.41 1.33 8 -6 2 15.84 1.37 8 -6 3 32.17 1.96 8 6 3 27.72 1.78 8 -6 3 30.37 1.88 8 -6 4 17.50 1.43 8 6 4 16.75 1.40 8 -6 4 15.91 1.38 8 -6 5 16.34 1.40 8 6 5 17.68 1.45 8 -6 5 17.70 1.43 8 -6 6 48.04 2.37 8 -6 6 49.50 2.46 8 6 6 43.94 2.31 8 -6 7 0.44 0.41 8 6 7 0.17 0.38 8 -6 7 0.05 0.39 8 -6 8 13.69 1.15 8 6 8 11.23 1.08 8 -6 8 12.72 1.07 8 6 9 1.79 0.49 8 -6 9 1.99 0.46 8 -6 9 1.96 0.48 8 6 10 0.75 0.32 8 -6 10 0.76 0.26 8 6 11 0.11 0.20 8 7 -11 12.13 0.75 8 7 -10 1.17 0.34 8 -7 -10 1.23 0.29 8 7 -9 2.78 0.48 8 -7 -9 2.87 0.48 8 7 -8 0.27 0.34 8 -7 -8 0.86 0.35 8 7 -7 -0.38 0.50 8 -7 -7 -0.57 0.49 8 7 -6 108.03 3.58 8 -7 -6 104.97 3.46 8 -7 -5 0.41 0.40 8 7 -5 1.15 0.50 8 -7 -5 0.73 0.41 8 7 -4 179.27 4.95 8 -7 -4 176.01 4.80 8 -7 -4 178.74 4.93 8 7 -3 2.13 0.57 8 -7 -3 2.38 0.63 8 -7 -3 1.27 0.44 8 7 -3 1.89 0.55 8 7 -2 304.89 7.16 8 -7 -2 319.24 7.12 8 7 -2 313.91 7.25 8 -7 -2 314.68 7.56 8 7 -1 5.64 0.67 8 -7 -1 7.25 0.90 8 -7 -1 7.64 0.77 8 7 -1 5.72 0.71 8 -7 0 11.36 0.91 8 7 0 10.32 0.94 8 -7 0 12.58 1.21 8 -7 0 11.32 1.10 8 -7 1 5.89 0.83 8 -7 1 6.63 0.68 8 7 1 6.46 0.72 8 -7 1 5.53 0.84 8 7 1 4.60 0.72 8 7 2 31.67 1.64 8 -7 2 34.72 2.01 8 7 2 32.62 1.84 8 -7 2 34.97 2.00 8 -7 3 13.96 1.29 8 7 3 13.33 1.20 8 -7 3 12.65 1.28 8 -7 4 106.87 3.81 8 7 4 97.77 3.58 8 -7 4 105.00 3.79 8 7 5 4.13 0.73 8 -7 5 5.43 0.93 8 -7 5 5.72 0.85 8 -7 6 77.73 3.09 8 -7 6 78.52 3.12 8 7 6 73.67 3.01 8 7 7 0.58 0.34 8 -7 7 0.83 0.47 8 -7 7 0.59 0.32 8 7 8 1.21 0.45 8 -7 8 1.22 0.44 8 -7 8 1.10 0.41 8 7 9 6.13 0.73 8 -7 9 6.32 0.66 8 -7 9 7.09 0.71 8 7 10 3.60 0.50 8 -7 10 3.48 0.43 8 8 -11 2.07 0.38 8 8 -10 7.39 0.72 8 8 -10 6.90 0.62 8 8 -9 0.10 0.26 8 8 -8 4.64 0.61 8 8 -7 2.17 0.44 8 -8 -7 2.57 0.47 8 8 -6 4.90 0.69 8 8 -5 413.04 9.06 8 -8 -5 408.77 8.94 8 8 -4 136.89 4.23 8 8 -4 132.96 4.01 8 -8 -4 135.17 4.06 8 8 -3 136.65 4.19 8 8 -3 146.10 4.17 8 -8 -3 139.25 4.22 8 8 -2 94.37 3.21 8 8 -2 101.44 3.25 8 -8 -2 94.82 3.39 8 8 -1 2.56 0.46 8 -8 -1 3.59 0.64 8 8 -1 3.29 0.60 8 8 0 158.36 4.29 8 -8 0 156.55 4.77 8 -8 1 6.14 0.87 8 8 1 6.62 0.74 8 -8 1 6.27 0.88 8 -8 2 7.35 0.96 8 -8 2 6.12 0.84 8 -8 3 285.68 7.11 8 8 3 268.26 6.80 8 -8 3 278.30 7.14 8 -8 4 76.60 3.05 8 8 4 67.68 2.79 8 -8 4 68.74 2.99 8 -8 5 70.44 2.96 8 -8 5 72.44 2.92 8 8 5 64.64 2.73 8 8 6 2.55 0.56 8 -8 6 2.18 0.61 8 -8 6 2.24 0.56 8 -8 7 15.52 1.25 8 -8 7 16.82 1.22 8 8 7 14.92 1.19 8 8 8 0.45 0.35 8 -8 8 0.36 0.36 8 8 9 0.13 0.24 8 -8 9 0.05 0.26 8 8 10 0.17 0.20 8 -8 10 0.14 0.19 8 9 -11 0.08 0.19 8 9 -10 0.77 0.27 8 9 -9 2.05 0.48 8 9 -8 2.38 0.51 8 9 -8 3.71 0.52 8 9 -7 0.64 0.44 8 9 -7 0.02 0.29 8 9 -6 126.10 4.02 8 9 -6 116.08 3.59 8 -9 -5 5.50 0.74 8 9 -5 5.24 0.85 8 9 -5 6.78 0.82 8 -9 -4 1.40 0.43 8 9 -4 1.83 0.54 8 9 -4 1.45 0.48 8 9 -3 122.35 3.90 8 9 -3 128.75 3.77 8 -9 -3 121.61 3.83 8 9 -2 25.45 1.53 8 9 -2 28.70 1.54 8 -9 -2 26.65 1.64 8 9 -1 68.14 2.59 8 9 -1 76.15 2.63 8 -9 -1 70.37 2.85 8 9 0 54.26 2.18 8 9 0 62.54 2.30 8 -9 0 57.12 2.58 8 -9 1 0.03 0.39 8 -9 2 27.49 1.70 8 -9 2 26.11 1.74 8 -9 3 52.58 2.41 8 -9 3 49.70 2.48 8 -9 4 7.55 0.97 8 -9 4 8.86 0.98 8 -9 5 64.77 2.87 8 -9 5 71.20 2.78 8 -9 6 21.19 1.51 8 9 6 22.21 1.42 8 9 7 0.20 0.27 8 -9 7 0.54 0.41 8 9 8 3.81 0.53 8 -9 8 4.13 0.63 8 9 9 0.41 0.24 8 -9 9 0.13 0.23 8 10 -10 7.60 0.68 8 10 -9 0.36 0.31 8 10 -8 2.11 0.49 8 10 -7 0.44 0.36 8 10 -6 0.67 0.42 8 10 -5 6.84 0.88 8 -10 -5 7.18 0.76 8 -10 -4 0.26 0.30 8 10 -4 0.56 0.41 8 10 -3 60.09 2.52 8 -10 -3 56.53 2.36 8 10 -2 250.43 6.25 8 -10 -2 257.16 6.35 8 10 -1 113.68 3.53 8 -10 -1 114.29 3.77 8 10 0 29.37 1.56 8 10 0 30.64 1.52 8 -10 0 30.32 1.80 8 10 1 10.06 0.87 8 -10 1 9.78 1.05 8 -10 2 9.75 1.08 8 -10 3 21.13 1.54 8 -10 4 2.93 0.67 8 -10 5 1.05 0.58 8 -10 6 5.41 0.77 8 -10 7 -0.05 0.34 8 -10 8 0.17 0.29 8 -10 9 1.94 0.38 8 11 -10 4.97 0.50 8 11 -9 15.30 1.00 8 11 -8 4.23 0.63 8 11 -7 37.95 1.89 8 11 -6 4.83 0.75 8 11 -5 2.13 0.56 8 11 -4 12.04 1.10 8 -11 -4 10.78 0.92 8 11 -3 4.75 0.69 8 -11 -3 3.89 0.61 8 11 -2 21.80 1.44 8 -11 -2 21.03 1.40 8 11 -1 96.67 3.20 8 -11 -1 95.59 3.33 8 11 0 78.72 2.74 8 -11 0 79.84 3.03 8 11 1 44.57 1.89 8 -11 1 43.09 2.17 8 -11 2 0.53 0.38 8 -11 3 11.37 1.12 8 -11 4 7.07 0.89 8 -11 5 47.58 2.28 8 -11 6 5.10 0.74 8 -11 7 2.54 0.54 8 -11 8 14.45 1.03 8 -11 9 1.33 0.32 8 12 -9 2.12 0.39 8 12 -8 8.79 0.81 8 12 -7 20.23 1.32 8 12 -6 6.41 0.80 8 12 -5 10.85 1.04 8 12 -4 0.66 0.45 8 12 -3 27.48 1.63 8 -12 -3 24.76 1.39 8 12 -2 56.80 2.38 8 -12 -2 54.41 2.23 8 12 -1 138.07 4.03 8 -12 -1 137.84 4.08 8 12 0 54.77 2.20 8 -12 0 53.67 2.36 8 12 1 4.98 0.63 8 -12 1 4.13 0.64 8 12 2 -0.01 0.29 8 -12 2 -0.08 0.44 8 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6 2.31 0.41 9 -12 7 8.29 0.65 9 13 -7 21.86 1.05 9 13 -6 3.72 0.48 9 13 -5 2.27 0.41 9 13 -4 35.62 1.57 9 13 -3 -0.22 0.26 9 13 -2 25.86 1.30 9 -13 -2 26.37 1.28 9 13 -1 26.68 1.30 9 -13 -1 29.56 1.41 9 13 0 2.49 0.40 9 -13 0 2.75 0.50 9 -13 1 4.48 0.59 9 -13 2 30.62 1.53 9 -13 3 18.79 1.17 9 -13 4 0.39 0.26 9 -13 5 -0.42 0.31 9 -13 6 5.50 0.55 9 14 -6 -0.16 0.24 9 14 -5 27.12 1.25 9 14 -4 3.47 0.48 9 14 -3 31.80 1.41 9 14 -2 3.48 0.48 9 14 -1 1.52 0.34 9 -14 -1 1.52 0.36 9 14 0 9.09 0.68 9 -14 0 9.89 0.77 9 -14 1 9.42 0.78 9 -14 2 5.45 0.61 9 -14 3 18.09 1.07 9 -14 4 3.77 0.49 9 -14 5 -0.13 0.25 9 15 -5 7.14 0.57 9 15 -4 6.89 0.59 9 15 -3 0.98 0.30 9 15 -2 0.22 0.20 9 15 -1 8.21 0.65 9 -15 0 7.08 0.59 9 15 0 6.55 0.54 9 -15 1 0.53 0.25 9 -15 2 0.66 0.26 9 -15 3 12.30 0.78 9 -15 4 0.37 0.18 9 16 -3 1.21 0.27 9 16 -2 2.99 0.38 9 16 -1 9.73 0.64 10 0 -9 0.23 0.22 10 0 -8 9.15 0.81 10 0 -7 0.37 0.32 10 0 -6 26.90 1.56 10 0 -5 -0.05 0.33 10 0 -4 1.99 0.61 10 0 -3 0.19 0.49 10 0 -2 26.87 1.55 10 0 -2 26.67 1.60 10 0 -1 0.26 0.40 10 0 -1 0.07 0.34 10 0 0 109.40 3.42 10 0 0 113.74 3.62 10 0 1 -0.04 0.35 10 0 1 0.35 0.39 10 0 1 0.21 0.43 10 0 2 13.51 1.24 10 0 2 13.83 1.09 10 0 3 0.53 0.38 10 0 3 -0.06 0.42 10 0 4 63.17 2.71 10 0 4 64.37 2.29 10 0 5 0.32 0.42 10 0 6 -0.52 0.43 10 0 7 0.12 0.36 10 0 8 1.89 0.44 10 1 -9 7.41 0.65 10 -1 -9 8.46 0.68 10 1 -8 0.43 0.31 10 -1 -8 0.95 0.35 10 1 -7 9.81 0.90 10 -1 -7 9.98 0.91 10 -1 -6 0.81 0.37 10 1 -6 0.94 0.41 10 -1 -5 9.96 0.97 10 1 -5 9.55 0.97 10 -1 -4 3.03 0.61 10 1 -4 2.88 0.61 10 -1 -3 6.45 0.87 10 -1 -3 5.38 0.78 10 1 -3 4.99 0.74 10 1 -2 8.06 0.92 10 -1 -2 7.80 0.83 10 1 -2 8.12 0.87 10 -1 -2 9.73 1.00 10 -1 -1 72.92 2.66 10 1 -1 70.85 2.65 10 1 -1 74.61 2.80 10 -1 -1 71.21 2.78 10 1 0 4.94 0.74 10 -1 0 3.92 0.71 10 -1 0 4.78 0.72 10 1 0 4.47 0.69 10 -1 1 21.93 1.35 10 1 1 22.01 1.35 10 -1 1 22.48 1.60 10 1 1 19.59 1.52 10 1 1 21.59 1.39 10 -1 1 24.30 1.51 10 -1 2 20.13 1.52 10 1 2 20.25 1.50 10 1 2 23.79 1.40 10 -1 2 21.65 1.39 10 -1 3 20.35 1.51 10 1 3 17.32 1.39 10 1 3 19.63 1.22 10 -1 3 17.92 1.23 10 -1 4 35.55 1.99 10 1 4 34.54 1.95 10 -1 4 34.36 1.65 10 -1 5 15.66 1.26 10 1 5 17.16 1.30 10 -1 6 7.29 0.82 10 1 6 8.45 0.90 10 -1 7 18.34 1.23 10 1 7 19.46 1.27 10 -1 8 -0.13 0.28 10 1 8 -0.10 0.29 10 -2 -9 1.19 0.31 10 2 -9 0.63 0.26 10 2 -8 0.69 0.31 10 -2 -8 1.19 0.35 10 2 -7 5.20 0.67 10 -2 -7 5.47 0.67 10 -2 -6 1.90 0.50 10 2 -6 1.14 0.39 10 -2 -5 17.21 1.21 10 2 -5 15.16 1.16 10 -2 -4 5.61 0.77 10 2 -4 5.09 0.72 10 -2 -3 0.44 0.48 10 -2 -3 0.40 0.39 10 2 -3 0.03 0.33 10 -2 -2 6.04 0.80 10 -2 -2 6.26 0.75 10 2 -2 5.35 0.72 10 2 -1 1.08 0.49 10 -2 -1 0.23 0.41 10 -2 -1 0.68 0.46 10 2 -1 0.04 0.35 10 -2 0 24.70 1.45 10 2 0 22.50 1.39 10 2 0 24.56 1.50 10 -2 0 26.22 1.61 10 -2 1 14.12 1.07 10 2 1 13.32 1.07 10 -2 1 13.32 1.24 10 2 1 14.34 1.29 10 2 1 13.97 1.10 10 -2 1 14.94 1.21 10 -2 2 52.32 2.52 10 2 2 55.76 2.54 10 2 2 57.43 2.24 10 -2 2 55.00 2.33 10 -2 3 33.54 1.94 10 2 3 36.82 2.00 10 -2 3 36.00 1.79 10 -2 4 0.34 0.31 10 -2 4 0.39 0.46 10 2 4 -0.04 0.38 10 -2 5 -0.46 0.32 10 -2 5 0.01 0.37 10 2 5 0.20 0.35 10 -2 6 0.58 0.37 10 2 6 0.27 0.39 10 -2 7 0.33 0.34 10 2 7 0.73 0.41 10 -2 8 9.06 0.77 10 2 8 9.16 0.78 10 -3 -9 2.65 0.38 10 3 -9 2.17 0.37 10 3 -8 0.23 0.23 10 -3 -8 0.57 0.26 10 3 -8 0.33 0.23 10 3 -7 20.68 1.10 10 -3 -7 21.79 1.24 10 3 -7 22.49 1.29 10 -3 -6 0.14 0.28 10 3 -6 0.70 0.38 10 -3 -5 1.29 0.42 10 3 -5 1.17 0.45 10 -3 -4 0.81 0.41 10 3 -4 0.65 0.42 10 -3 -3 14.77 1.13 10 3 -3 13.69 1.10 10 -3 -3 14.78 1.21 10 -3 -2 19.57 1.28 10 3 -2 18.55 1.25 10 -3 -2 20.52 1.41 10 -3 -1 41.60 1.89 10 3 -1 37.93 1.80 10 -3 -1 42.10 2.05 10 -3 0 7.81 0.82 10 3 0 6.90 0.78 10 3 0 9.21 0.89 10 -3 0 7.91 0.91 10 -3 1 7.15 0.87 10 -3 1 7.25 0.78 10 3 1 6.80 0.76 10 3 1 8.00 0.83 10 -3 1 7.97 0.97 10 3 1 6.90 0.88 10 -3 2 35.85 1.99 10 3 2 35.51 1.99 10 -3 2 36.50 1.86 10 -3 3 30.06 1.80 10 3 3 31.91 1.86 10 -3 3 30.61 1.67 10 -3 4 4.75 0.64 10 -3 4 5.68 0.81 10 3 4 4.70 0.71 10 -3 5 9.65 0.97 10 3 5 10.53 1.02 10 -3 5 10.31 0.86 10 -3 6 10.29 0.96 10 3 6 11.53 1.00 10 -3 6 9.67 0.74 10 -3 7 7.92 0.77 10 3 7 8.90 0.84 10 -3 8 -0.14 0.25 10 3 8 0.16 0.27 10 -4 -9 0.86 0.25 10 4 -9 0.66 0.22 10 4 -8 13.62 0.84 10 -4 -8 16.68 0.95 10 4 -8 14.79 0.95 10 4 -7 1.55 0.34 10 -4 -7 1.84 0.44 10 4 -7 1.92 0.46 10 4 -6 17.53 1.03 10 -4 -6 18.88 1.19 10 4 -6 17.17 1.16 10 -4 -5 3.78 0.59 10 4 -5 3.87 0.60 10 -4 -4 2.72 0.62 10 -4 -4 3.16 0.61 10 4 -4 3.19 0.58 10 -4 -3 62.99 2.40 10 4 -3 62.71 2.41 10 -4 -3 64.35 2.55 10 -4 -2 3.69 0.66 10 -4 -2 4.08 0.60 10 4 -2 3.62 0.58 10 -4 -1 0.94 0.51 10 -4 -1 0.09 0.31 10 4 -1 0.21 0.33 10 -4 0 12.15 0.95 10 4 0 10.99 0.93 10 -4 0 12.39 1.12 10 4 1 13.57 1.01 10 4 1 13.13 1.15 10 -4 1 15.53 1.21 10 -4 2 2.61 0.58 10 -4 2 2.48 0.66 10 4 2 2.60 0.59 10 -4 3 9.26 1.03 10 4 3 9.20 0.98 10 -4 3 10.15 0.99 10 -4 4 8.16 0.86 10 -4 4 6.90 0.86 10 4 4 6.54 0.82 10 -4 5 0.67 0.35 10 -4 5 0.54 0.39 10 4 5 0.38 0.32 10 -4 6 0.57 0.28 10 -4 6 0.22 0.32 10 4 6 0.42 0.31 10 -4 7 0.34 0.26 10 4 7 0.12 0.28 10 -4 8 22.93 1.13 10 4 8 23.00 1.16 10 5 -9 10.11 0.64 10 5 -8 1.90 0.35 10 -5 -8 2.13 0.34 10 5 -8 2.41 0.40 10 5 -7 3.09 0.44 10 -5 -7 3.30 0.45 10 5 -7 3.17 0.49 10 5 -6 5.38 0.59 10 -5 -6 4.57 0.57 10 5 -6 4.88 0.62 10 -5 -5 26.84 1.39 10 5 -5 26.66 1.45 10 -5 -4 0.65 0.44 10 -5 -4 1.20 0.43 10 5 -4 1.14 0.41 10 -5 -3 1.41 0.53 10 -5 -3 1.12 0.36 10 5 -3 0.77 0.37 10 -5 -2 2.30 0.56 10 -5 -2 2.58 0.48 10 5 -2 2.10 0.46 10 -5 -1 15.99 1.07 10 5 -1 13.81 1.03 10 -5 -1 17.15 1.28 10 -5 0 7.99 0.77 10 5 0 6.98 0.73 10 -5 0 8.65 0.97 10 -5 1 1.56 0.53 10 5 1 1.53 0.48 10 -5 2 7.17 0.85 10 5 2 7.35 0.85 10 -5 2 7.62 0.93 10 -5 3 0.26 0.37 10 -5 3 0.17 0.36 10 5 3 0.23 0.33 10 -5 4 12.96 1.11 10 5 4 12.94 1.07 10 -5 4 12.45 1.02 10 -5 5 11.12 0.99 10 5 5 11.31 0.99 10 -5 5 11.72 0.94 10 -5 6 2.17 0.41 10 -5 6 1.59 0.42 10 5 6 2.04 0.46 10 -5 7 0.25 0.21 10 -5 7 -0.50 0.34 10 5 7 -0.02 0.22 10 6 -8 0.14 0.20 10 6 -8 0.07 0.19 10 6 -7 0.87 0.29 10 -6 -7 0.63 0.25 10 6 -7 0.75 0.29 10 6 -6 17.48 1.03 10 -6 -6 20.46 1.09 10 6 -6 18.02 1.09 10 6 -5 4.46 0.54 10 6 -5 5.30 0.64 10 -6 -5 5.16 0.59 10 -6 -4 7.18 0.79 10 -6 -4 6.33 0.66 10 6 -4 6.09 0.69 10 -6 -3 41.53 1.73 10 6 -3 40.03 1.78 10 -6 -3 41.01 1.92 10 -6 -2 2.50 0.59 10 -6 -2 2.30 0.44 10 6 -2 2.08 0.42 10 -6 -1 10.33 0.82 10 6 -1 9.37 0.84 10 -6 -1 10.75 1.04 10 6 0 28.00 1.45 10 -6 0 33.56 1.77 10 -6 1 14.41 1.17 10 -6 2 3.96 0.69 10 6 2 4.40 0.64 10 -6 3 9.72 0.98 10 6 3 10.31 0.95 10 -6 3 9.68 0.95 10 -6 4 27.45 1.58 10 6 4 27.23 1.50 10 -6 4 26.16 1.50 10 -6 5 2.60 0.48 10 -6 5 2.66 0.51 10 6 5 2.57 0.48 10 -6 6 0.37 0.28 10 -6 6 -0.20 0.27 10 6 6 0.36 0.24 10 -6 7 0.47 0.23 10 -6 7 -0.02 0.23 10 6 7 -0.01 0.23 10 7 -8 0.02 0.20 10 7 -7 4.42 0.49 10 7 -7 3.80 0.45 10 7 -6 1.23 0.32 10 7 -6 1.06 0.31 10 7 -5 3.92 0.50 10 -7 -5 4.86 0.52 10 7 -5 4.50 0.55 10 -7 -4 101.12 2.78 10 7 -4 91.40 2.86 10 -7 -4 95.95 3.03 10 -7 -3 5.35 0.72 10 -7 -3 5.11 0.56 10 7 -3 4.33 0.57 10 -7 -2 4.40 0.66 10 -7 -2 5.84 0.60 10 7 -2 5.19 0.63 10 -7 -1 4.76 0.74 10 -7 -1 5.51 0.60 10 7 -1 4.59 0.60 10 -7 0 8.85 0.93 10 -7 1 6.53 0.81 10 -7 2 1.41 0.44 10 -7 3 1.84 0.49 10 7 3 1.95 0.44 10 -7 4 1.53 0.45 10 7 4 1.31 0.39 10 -7 5 19.55 1.21 10 7 5 19.73 1.14 10 -7 5 20.66 1.22 10 -7 6 3.04 0.46 10 -7 6 2.51 0.44 10 7 6 1.66 0.34 10 -7 7 2.01 0.33 10 8 -7 12.94 0.79 10 8 -7 13.34 0.73 10 8 -6 9.84 0.73 10 8 -6 9.48 0.69 10 8 -5 1.67 0.35 10 8 -5 1.45 0.34 10 -8 -4 0.81 0.41 10 8 -4 0.30 0.28 10 8 -4 0.83 0.34 10 8 -3 8.22 0.73 10 -8 -3 9.00 0.86 10 8 -2 48.01 1.84 10 -8 -2 49.11 2.06 10 -8 -1 0.38 0.37 10 8 -1 0.35 0.33 10 -8 0 69.39 2.59 10 -8 1 17.94 1.26 10 -8 2 0.92 0.40 10 -8 3 9.28 0.88 10 -8 4 3.23 0.52 10 -8 5 2.50 0.47 10 -8 6 5.71 0.58 10 9 -7 1.47 0.30 10 9 -6 1.55 0.31 10 9 -5 5.56 0.54 10 9 -5 5.38 0.51 10 9 -4 0.29 0.25 10 9 -4 1.00 0.32 10 9 -3 21.50 1.10 10 -9 -3 21.18 1.23 10 9 -2 75.93 2.35 10 -9 -2 75.22 2.57 10 -9 -1 1.92 0.51 10 -9 0 27.34 1.50 10 -9 1 12.31 1.01 10 -9 2 17.65 1.19 10 -9 3 1.38 0.42 10 -9 4 -0.47 0.35 10 -9 5 11.77 0.88 10 -9 6 1.41 0.32 10 10 -6 1.61 0.29 10 10 -5 23.24 1.09 10 10 -4 5.17 0.52 10 -10 -3 4.54 0.60 10 -10 -2 0.70 0.34 10 -10 -1 3.75 0.58 10 -10 0 3.22 0.54 10 -10 1 0.92 0.38 10 -10 2 0.54 0.36 10 -10 3 1.12 0.35 10 -10 4 10.64 0.84 10 -10 5 0.36 0.26 10 -10 6 1.62 0.33 10 11 -5 0.42 0.19 10 11 -4 15.49 0.85 10 -11 -3 5.04 0.55 10 -11 -2 15.03 0.95 10 -11 -1 51.74 1.92 10 -11 0 4.99 0.59 10 -11 1 0.13 0.27 10 -11 2 1.27 0.36 10 -11 3 2.07 0.42 10 -11 4 2.17 0.39 10 -11 5 4.16 0.46 10 12 -4 0.44 0.20 10 -12 -2 3.82 0.48 10 -12 -1 0.56 0.30 10 -12 0 0.94 0.35 10 -12 1 16.49 0.98 10 -12 2 0.85 0.27 10 -12 3 24.14 1.17 10 -12 4 0.62 0.25 10 -13 -1 1.30 0.30 10 -13 0 3.68 0.45 10 -13 1 3.20 0.43 10 -13 2 0.61 0.28 10 -13 3 5.26 0.49 11 0 -7 13.75 0.82 11 0 -6 -0.39 0.27 11 0 -5 8.02 0.73 11 0 -4 0.27 0.34 11 0 -3 22.38 1.25 11 0 -2 0.32 0.32 11 0 -1 2.44 0.49 11 0 0 1.11 0.42 11 0 1 1.56 0.44 11 0 2 -0.07 0.23 11 0 3 0.05 0.32 11 0 4 0.07 0.37 11 0 5 22.71 1.29 11 0 6 -0.61 0.33 11 -1 -7 0.00 0.21 11 1 -7 0.24 0.27 11 -1 -6 7.48 0.65 11 1 -6 7.47 0.66 11 -1 -5 0.19 0.24 11 1 -5 -0.30 0.31 11 -1 -4 53.03 1.97 11 1 -4 51.51 1.97 11 -1 -3 1.35 0.39 11 1 -3 0.59 0.35 11 -1 -2 1.23 0.41 11 1 -2 1.41 0.38 11 -1 -1 9.54 0.83 11 1 -1 9.76 0.82 11 -1 -1 8.92 0.87 11 -1 0 19.36 1.20 11 -1 1 0.46 0.31 11 1 2 1.60 0.36 11 -1 2 1.54 0.39 11 -1 3 0.61 0.28 11 -1 3 0.56 0.36 11 1 3 0.37 0.41 11 -1 4 29.11 1.54 11 1 4 31.43 1.58 11 -1 5 4.64 0.58 11 1 5 4.62 0.59 11 -1 6 4.58 0.54 11 1 6 3.97 0.52 11 -2 -7 -0.19 0.20 11 2 -7 0.08 0.21 11 -2 -6 0.03 0.21 11 2 -6 0.53 0.27 11 -2 -5 7.20 0.66 11 2 -5 7.18 0.69 11 -2 -4 0.37 0.26 11 2 -4 0.45 0.32 11 -2 -3 10.58 0.84 11 2 -3 9.74 0.81 11 -2 -2 1.26 0.37 11 2 -2 1.57 0.42 11 -2 -1 0.49 0.43 11 -2 -1 0.86 0.37 11 2 -1 0.37 0.32 11 -2 0 11.05 0.93 11 -2 1 1.22 0.39 11 -2 2 2.09 0.43 11 2 3 23.49 1.39 11 -2 3 23.83 1.22 11 -2 4 4.99 0.51 11 -2 4 5.46 0.69 11 2 4 4.77 0.62 11 -2 5 11.41 0.89 11 2 5 12.57 0.92 11 -2 6 1.60 0.35 11 2 6 0.98 0.31 11 -3 -7 0.07 0.15 11 3 -7 -0.16 0.21 11 -3 -6 5.44 0.52 11 3 -6 5.10 0.53 11 -3 -5 15.58 0.93 11 3 -5 16.63 0.99 11 -3 -4 0.07 0.23 11 3 -4 0.31 0.28 11 -3 -3 0.30 0.28 11 3 -3 0.09 0.27 11 -3 -2 0.73 0.42 11 -3 -2 0.72 0.34 11 3 -2 0.71 0.34 11 -3 -1 15.20 0.99 11 3 -1 15.21 0.99 11 -3 -1 15.53 1.09 11 -3 0 14.01 1.06 11 -3 1 6.77 0.73 11 -3 2 23.33 1.28 11 -3 3 9.14 0.76 11 3 4 9.09 0.81 11 -3 4 8.24 0.66 11 -3 5 31.38 1.47 11 3 5 30.03 1.41 11 3 6 5.67 0.56 11 4 -7 2.52 0.33 11 -4 -6 0.16 0.20 11 4 -6 0.44 0.22 11 -4 -5 0.08 0.21 11 4 -5 -0.23 0.24 11 -4 -4 5.58 0.57 11 4 -4 6.11 0.63 11 -4 -3 17.17 0.99 11 4 -3 16.95 1.02 11 -4 -2 1.78 0.50 11 -4 -2 1.72 0.36 11 4 -2 2.16 0.44 11 4 -1 39.62 1.62 11 -4 -1 41.71 1.82 11 -4 0 9.58 0.87 11 -4 1 2.35 0.48 11 -4 2 0.19 0.36 11 -4 3 4.24 0.54 11 4 4 18.44 1.11 11 -4 4 17.75 0.98 11 4 5 39.68 1.57 11 5 -6 6.08 0.52 11 -5 -5 9.76 0.65 11 5 -5 10.78 0.74 11 -5 -4 4.89 0.49 11 5 -4 5.49 0.56 11 -5 -3 8.22 0.65 11 5 -3 8.75 0.72 11 -5 -2 5.44 0.66 11 -5 -2 4.60 0.52 11 5 -2 4.57 0.55 11 -5 -1 17.66 1.16 11 -5 0 10.70 0.91 11 -5 1 5.14 0.64 11 -5 2 1.70 0.44 11 -5 3 2.91 0.47 11 -5 4 0.18 0.26 11 6 -6 0.87 0.22 11 6 -5 19.72 0.95 11 -6 -4 7.67 0.56 11 6 -4 7.26 0.61 11 -6 -3 3.59 0.41 11 6 -3 3.93 0.48 11 -6 -2 0.61 0.39 11 6 -2 0.16 0.25 11 -6 -1 41.36 1.76 11 -6 0 3.86 0.57 11 -6 1 9.93 0.85 11 -6 2 3.14 0.52 11 -6 3 5.62 0.60 11 -6 4 1.59 0.34 11 7 -5 9.22 0.59 11 7 -4 18.60 0.91 11 7 -3 0.89 0.29 11 -7 -2 14.35 0.97 11 -7 -1 4.09 0.57 11 -7 0 3.34 0.54 11 -7 1 49.57 1.90 11 -7 2 2.51 0.47 11 -7 3 0.96 0.33 11 -7 4 3.93 0.48 11 -8 -2 9.28 0.75 11 -8 -1 0.78 0.34 11 -8 0 1.42 0.38 11 -8 1 -0.25 0.28 11 -8 2 28.96 1.32 11 -8 3 2.21 0.40 11 -8 4 4.61 0.47 11 -9 -2 4.27 0.50 11 -9 -1 23.01 1.13 11 -9 0 2.68 0.42 11 -9 1 0.72 0.29 11 -9 2 0.52 0.27 11 -9 3 0.69 0.30 11 -10 -1 12.57 0.78 11 -10 0 5.82 0.54 11 -10 1 6.55 0.56 11 -10 2 8.88 0.63 12 0 -4 4.47 0.42 12 1 -4 2.06 0.30 0 0 0 0.00 0.00 TITL 161109 in P2(1)/n REM P2(1)/n (#14 in standard setting) CELL 1.54184 10.003737 20.270585 13.212217 90.0000 92.2306 90.0000 ZERR 4.00 0.000088 0.000190 0.000127 0.0000 0.0008 0.0000 LATT 1 SYMM -x+1/2, y+1/2,-z+1/2 SFAC C H N O UNIT 124.00 132.00 4.00 12.00 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2014/5 (Sheldrick, 2014)' ; _shelx_hkl_checksum 77913 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.34539(13) 0.48870(7) 0.55842(10) 0.0611(4) Uani 1 1 d . . . . . O2 O 0.38401(15) 0.72243(7) 0.46195(12) 0.0697(4) Uani 1 1 d . . . . . N1 N 0.13751(15) 0.53165(7) 0.58460(11) 0.0535(4) Uani 1 1 d . . . . . C9 C 0.30828(15) 0.56896(7) 0.35465(12) 0.0407(4) Uani 1 1 d . . . . . C22 C 0.35059(16) 0.50210(8) 0.32916(13) 0.0438(4) Uani 1 1 d . . . . . H22 H 0.3958 0.4772 0.3786 0.053 Uiso 1 1 calc R U . . . C18 C 0.24146(16) 0.60673(8) 0.27322(12) 0.0429(4) Uani 1 1 d . . . . . H18 H 0.2192 0.6504 0.2862 0.051 Uiso 1 1 calc R U . . . C10 C 0.39460(15) 0.60744(8) 0.43172(11) 0.0414(4) Uani 1 1 d . . . . . H10 H 0.4692 0.5817 0.4614 0.050 Uiso 1 1 calc R U . . . C2 C 0.26141(15) 0.58606(8) 0.46648(12) 0.0424(4) Uani 1 1 d . . . . . C3 C 0.13607(16) 0.62353(8) 0.48278(13) 0.0470(4) Uani 1 1 d . . . . . C11 C 0.42999(16) 0.67835(8) 0.41231(13) 0.0471(4) Uani 1 1 d . . . . . C19 C 0.21055(16) 0.58262(8) 0.18201(12) 0.0460(4) Uani 1 1 d . . . . . C1 C 0.25833(17) 0.52912(8) 0.54013(13) 0.0473(4) Uani 1 1 d . . . . . C21 C 0.32697(17) 0.47538(8) 0.23782(13) 0.0479(4) Uani 1 1 d . . . . . C12 C 0.52399(17) 0.69142(9) 0.33012(13) 0.0508(4) Uani 1 1 d . . . . . C4 C 0.06319(18) 0.58666(9) 0.55105(14) 0.0522(4) Uani 1 1 d . . . . . C8 C 0.0809(2) 0.68107(10) 0.44441(16) 0.0615(5) Uani 1 1 d . . . . . H8 H 0.1293 0.7076 0.4016 0.074 Uiso 1 1 calc R U . . . C23 C 0.1432(2) 0.62431(10) 0.09828(14) 0.0585(5) Uani 1 1 d . . . . . C27 C 0.3833(2) 0.40800(9) 0.20801(17) 0.0631(5) Uani 1 1 d . . . . . C20 C 0.2455(2) 0.51305(11) 0.16154(15) 0.0690(6) Uani 1 1 d . U . . . C13 C 0.5796(2) 0.64096(11) 0.27468(17) 0.0696(6) Uani 1 1 d . . . . . H13 H 0.5600 0.5973 0.2895 0.084 Uiso 1 1 calc R U . . . C5 C -0.0643(2) 0.60438(11) 0.57738(19) 0.0719(6) Uani 1 1 d . . . . . H5 H -0.1118 0.5791 0.6224 0.086 Uiso 1 1 calc R U . . . C17 C 0.5543(2) 0.75672(11) 0.30750(19) 0.0708(6) Uani 1 1 d . . . . . H17 H 0.5174 0.7909 0.3442 0.085 Uiso 1 1 calc R U . . . C31 C 0.0999(2) 0.48654(12) 0.66429(17) 0.0732(6) Uani 1 1 d . . . . . H31A H 0.1595 0.4494 0.6661 0.110 Uiso 1 1 calc R U . . . H31B H 0.0099 0.4716 0.6510 0.110 Uiso 1 1 calc R U . . . H31C H 0.1056 0.5089 0.7284 0.110 Uiso 1 1 calc R U . . . O3 O 0.2120(4) 0.48809(12) 0.08152(18) 0.1590(13) Uani 1 1 d . U . . . C7 C -0.0475(2) 0.69916(12) 0.4702(2) 0.0810(7) Uani 1 1 d . . . . . H7 H -0.0855 0.7376 0.4435 0.097 Uiso 1 1 calc R U . . . C6 C -0.1186(2) 0.66086(13) 0.5346(2) 0.0868(8) Uani 1 1 d . . . . . H6 H -0.2051 0.6732 0.5497 0.104 Uiso 1 1 calc R U . . . C16 C 0.6394(3) 0.77054(15) 0.2304(2) 0.0983(9) Uani 1 1 d . . . . . H16 H 0.6594 0.8141 0.2153 0.118 Uiso 1 1 calc R U . . . C28 C 0.2705(3) 0.35913(12) 0.1827(2) 0.0932(8) Uani 1 1 d . . . . . H28A H 0.2120 0.3566 0.2384 0.140 Uiso 1 1 calc R U . . . H28B H 0.3079 0.3164 0.1705 0.140 Uiso 1 1 calc R U . . . H28C H 0.2210 0.3737 0.1231 0.140 Uiso 1 1 calc R U . . . C15 C 0.6945(3) 0.72052(18) 0.1760(2) 0.1043(10) Uani 1 1 d . . . . . H15 H 0.7523 0.7303 0.1246 0.125 Uiso 1 1 calc R U . . . C30 C 0.4666(3) 0.37767(12) 0.2953(3) 0.0973(9) Uani 1 1 d . . . . . H30A H 0.5424 0.4054 0.3112 0.146 Uiso 1 1 calc R U . . . H30B H 0.4970 0.3347 0.2760 0.146 Uiso 1 1 calc R U . . . H30C H 0.4129 0.3738 0.3537 0.146 Uiso 1 1 calc R U . . . C14 C 0.6643(3) 0.65555(16) 0.1973(2) 0.0933(8) Uani 1 1 d . . . . . H14 H 0.7008 0.6217 0.1597 0.112 Uiso 1 1 calc R U . . . C24 C 0.0048(3) 0.59822(16) 0.0718(3) 0.1130(12) Uani 1 1 d . . . . . H24A H 0.0111 0.5534 0.0492 0.170 Uiso 1 1 calc R U . . . H24B H -0.0360 0.6247 0.0188 0.170 Uiso 1 1 calc R U . . . H24C H -0.0487 0.6001 0.1305 0.170 Uiso 1 1 calc R U . . . C26 C 0.1248(4) 0.69498(12) 0.1322(2) 0.1060(11) Uani 1 1 d . . . . . H26A H 0.0668 0.6960 0.1884 0.159 Uiso 1 1 calc R U . . . H26B H 0.0857 0.7204 0.0773 0.159 Uiso 1 1 calc R U . . . H26C H 0.2101 0.7134 0.1525 0.159 Uiso 1 1 calc R U . . . C29 C 0.4705(5) 0.41688(16) 0.1173(3) 0.1400(17) Uani 1 1 d . . . . . H29A H 0.4173 0.4339 0.0612 0.210 Uiso 1 1 calc R U . . . H29B H 0.5078 0.3751 0.0992 0.210 Uiso 1 1 calc R U . . . H29C H 0.5415 0.4473 0.1343 0.210 Uiso 1 1 calc R U . . . C25 C 0.2314(4) 0.6258(3) 0.0071(2) 0.154(2) Uani 1 1 d . . . . . H25A H 0.3217 0.6359 0.0290 0.231 Uiso 1 1 calc R U . . . H25B H 0.1992 0.6589 -0.0397 0.231 Uiso 1 1 calc R U . . . H25C H 0.2290 0.5835 -0.0256 0.231 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0555(7) 0.0618(8) 0.0662(8) 0.0197(6) 0.0040(6) 0.0065(6) O2 0.0793(9) 0.0496(7) 0.0816(9) -0.0197(7) 0.0217(7) -0.0125(6) N1 0.0550(8) 0.0522(8) 0.0542(8) 0.0040(6) 0.0149(6) -0.0065(6) C9 0.0407(8) 0.0376(8) 0.0439(8) -0.0013(6) 0.0040(6) 0.0000(6) C22 0.0424(8) 0.0366(8) 0.0526(9) 0.0014(6) 0.0046(6) 0.0014(6) C18 0.0424(8) 0.0356(7) 0.0508(9) -0.0006(6) 0.0021(6) 0.0010(6) C10 0.0390(8) 0.0427(8) 0.0424(8) -0.0004(6) 0.0028(6) -0.0013(6) C2 0.0420(8) 0.0400(8) 0.0454(8) -0.0012(6) 0.0051(6) -0.0025(6) C3 0.0458(8) 0.0429(8) 0.0527(9) -0.0063(7) 0.0084(7) -0.0017(7) C11 0.0436(8) 0.0458(9) 0.0518(9) -0.0024(7) 0.0001(7) -0.0060(7) C19 0.0447(8) 0.0459(9) 0.0474(8) 0.0012(7) 0.0036(7) -0.0015(7) C1 0.0471(9) 0.0473(9) 0.0477(9) 0.0020(7) 0.0036(7) -0.0040(7) C21 0.0499(9) 0.0393(8) 0.0552(9) -0.0041(7) 0.0108(7) 0.0000(7) C12 0.0436(8) 0.0532(10) 0.0556(9) 0.0094(8) 0.0004(7) -0.0054(7) C4 0.0497(9) 0.0501(9) 0.0575(10) -0.0076(8) 0.0130(7) -0.0049(7) C8 0.0617(11) 0.0479(10) 0.0759(12) 0.0007(9) 0.0162(9) 0.0090(8) C23 0.0627(11) 0.0619(11) 0.0504(9) 0.0060(8) -0.0041(8) 0.0047(9) C27 0.0700(12) 0.0462(10) 0.0742(12) -0.0124(9) 0.0172(10) 0.0079(9) C20 0.0939(15) 0.0571(11) 0.0550(10) -0.0153(9) -0.0112(10) 0.0133(10) C13 0.0655(12) 0.0686(12) 0.0764(13) 0.0116(11) 0.0246(10) 0.0012(10) C5 0.0599(12) 0.0703(13) 0.0877(15) -0.0088(11) 0.0306(11) -0.0033(10) C17 0.0677(12) 0.0600(12) 0.0848(14) 0.0179(11) 0.0040(10) -0.0102(10) C31 0.0807(14) 0.0752(14) 0.0650(12) 0.0160(11) 0.0207(10) -0.0145(11) O3 0.266(3) 0.0989(15) 0.1043(15) -0.0527(12) -0.0918(19) 0.0661(18) C7 0.0726(14) 0.0645(13) 0.1073(18) 0.0015(12) 0.0232(13) 0.0247(11) C6 0.0593(12) 0.0851(16) 0.118(2) -0.0099(15) 0.0313(13) 0.0163(12) C16 0.0908(18) 0.0898(18) 0.116(2) 0.0503(17) 0.0204(16) -0.0119(15) C28 0.108(2) 0.0553(13) 0.116(2) -0.0331(13) -0.0017(16) -0.0008(13) C15 0.0853(17) 0.133(3) 0.0973(19) 0.0540(19) 0.0358(15) 0.0043(17) C30 0.0995(19) 0.0554(13) 0.135(2) -0.0217(14) -0.0168(17) 0.0300(13) C14 0.0836(16) 0.109(2) 0.0906(17) 0.0209(15) 0.0407(14) 0.0119(15) C24 0.097(2) 0.103(2) 0.133(3) 0.0218(19) -0.062(2) -0.0137(17) C26 0.149(3) 0.0618(14) 0.103(2) 0.0166(13) -0.0535(19) 0.0148(16) C29 0.185(4) 0.088(2) 0.155(3) -0.022(2) 0.113(3) 0.019(2) C25 0.156(3) 0.228(5) 0.0804(19) 0.074(3) 0.046(2) 0.088(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 N1 C4 111.17(14) . . ? C1 N1 C31 123.08(17) . . ? C4 N1 C31 125.43(16) . . ? C18 C9 C22 116.37(13) . . ? C18 C9 C10 117.05(13) . . ? C22 C9 C10 117.80(13) . . ? C18 C9 C2 115.01(13) . . ? C22 C9 C2 120.63(13) . . ? C10 C9 C2 56.81(9) . . ? C21 C22 C9 122.76(15) . . ? C21 C22 H22 118.6 . . ? C9 C22 H22 118.6 . . ? C19 C18 C9 124.05(15) . . ? C19 C18 H18 118.0 . . ? C9 C18 H18 118.0 . . ? C2 C10 C11 123.31(14) . . ? C2 C10 C9 64.35(10) . . ? C11 C10 C9 120.40(13) . . ? C2 C10 H10 113.4 . . ? C11 C10 H10 113.4 . . ? C9 C10 H10 113.4 . . ? C3 C2 C10 131.64(14) . . ? C3 C2 C1 104.96(13) . . ? C10 C2 C1 117.48(14) . . ? C3 C2 C9 121.41(13) . . ? C10 C2 C9 58.84(10) . . ? C1 C2 C9 116.22(13) . . ? C8 C3 C4 118.58(16) . . ? C8 C3 C2 134.88(16) . . ? C4 C3 C2 106.50(15) . . ? O2 C11 C12 121.92(16) . . ? O2 C11 C10 121.08(15) . . ? C12 C11 C10 117.01(14) . . ? C18 C19 C20 117.96(16) . . ? C18 C19 C23 122.34(16) . . ? C20 C19 C23 119.69(15) . . ? O1 C1 N1 125.48(16) . . ? O1 C1 C2 127.72(15) . . ? N1 C1 C2 106.80(14) . . ? C22 C21 C20 118.59(15) . . ? C22 C21 C27 122.61(17) . . ? C20 C21 C27 118.78(16) . . ? C13 C12 C17 119.50(19) . . ? C13 C12 C11 122.14(16) . . ? C17 C12 C11 118.35(18) . . ? C5 C4 C3 122.20(19) . . ? C5 C4 N1 127.58(18) . . ? C3 C4 N1 110.21(15) . . ? C3 C8 C7 119.5(2) . . ? C3 C8 H8 120.2 . . ? C7 C8 H8 120.2 . . ? C24 C23 C26 106.2(2) . . ? C24 C23 C25 112.2(3) . . ? C26 C23 C25 107.3(3) . . ? C24 C23 C19 110.42(18) . . ? C26 C23 C19 111.34(16) . . ? C25 C23 C19 109.32(19) . . ? C29 C27 C30 109.3(3) . . ? C29 C27 C28 110.2(3) . . ? C30 C27 C28 106.3(2) . . ? C29 C27 C21 108.95(19) . . ? C30 C27 C21 111.10(17) . . ? C28 C27 C21 110.95(17) . . ? O3 C20 C19 120.0(2) . . ? O3 C20 C21 120.4(2) . . ? C19 C20 C21 119.60(16) . . ? C14 C13 C12 120.1(2) . . ? C14 C13 H13 119.9 . . ? C12 C13 H13 119.9 . . ? C6 C5 C4 117.7(2) . . ? C6 C5 H5 121.1 . . ? C4 C5 H5 121.1 . . ? C16 C17 C12 119.8(2) . . ? C16 C17 H17 120.1 . . ? C12 C17 H17 120.1 . . ? N1 C31 H31A 109.5 . . ? N1 C31 H31B 109.5 . . ? H31A C31 H31B 109.5 . . ? N1 C31 H31C 109.5 . . ? H31A C31 H31C 109.5 . . ? H31B C31 H31C 109.5 . . ? C6 C7 C8 120.6(2) . . ? C6 C7 H7 119.7 . . ? C8 C7 H7 119.7 . . ? C7 C6 C5 121.2(2) . . ? C7 C6 H6 119.4 . . ? C5 C6 H6 119.4 . . ? C15 C16 C17 120.6(2) . . ? C15 C16 H16 119.7 . . ? C17 C16 H16 119.7 . . ? C27 C28 H28A 109.5 . . ? C27 C28 H28B 109.5 . . ? H28A C28 H28B 109.5 . . ? C27 C28 H28C 109.5 . . ? H28A C28 H28C 109.5 . . ? H28B C28 H28C 109.5 . . ? C16 C15 C14 120.1(2) . . ? C16 C15 H15 119.9 . . ? C14 C15 H15 119.9 . . ? C27 C30 H30A 109.5 . . ? C27 C30 H30B 109.5 . . ? H30A C30 H30B 109.5 . . ? C27 C30 H30C 109.5 . . ? H30A C30 H30C 109.5 . . ? H30B C30 H30C 109.5 . . ? C15 C14 C13 119.9(3) . . ? C15 C14 H14 120.0 . . ? C13 C14 H14 120.0 . . ? C23 C24 H24A 109.5 . . ? C23 C24 H24B 109.5 . . ? H24A C24 H24B 109.5 . . ? C23 C24 H24C 109.5 . . ? H24A C24 H24C 109.5 . . ? H24B C24 H24C 109.5 . . ? C23 C26 H26A 109.5 . . ? C23 C26 H26B 109.5 . . ? H26A C26 H26B 109.5 . . ? C23 C26 H26C 109.5 . . ? H26A C26 H26C 109.5 . . ? H26B C26 H26C 109.5 . . ? C27 C29 H29A 109.5 . . ? C27 C29 H29B 109.5 . . ? H29A C29 H29B 109.5 . . ? C27 C29 H29C 109.5 . . ? H29A C29 H29C 109.5 . . ? H29B C29 H29C 109.5 . . ? C23 C25 H25A 109.5 . . ? C23 C25 H25B 109.5 . . ? H25A C25 H25B 109.5 . . ? C23 C25 H25C 109.5 . . ? H25A C25 H25C 109.5 . . ? H25B C25 H25C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.213(2) . ? O2 C11 1.210(2) . ? N1 C1 1.365(2) . ? N1 C4 1.402(2) . ? N1 C31 1.455(2) . ? C9 C18 1.461(2) . ? C9 C22 1.463(2) . ? C9 C10 1.524(2) . ? C9 C2 1.605(2) . ? C22 C21 1.335(2) . ? C22 H22 0.9300 . ? C18 C19 1.326(2) . ? C18 H18 0.9300 . ? C10 C2 1.490(2) . ? C10 C11 1.505(2) . ? C10 H10 0.9800 . ? C2 C3 1.489(2) . ? C2 C1 1.511(2) . ? C3 C8 1.378(3) . ? C3 C4 1.398(2) . ? C11 C12 1.488(2) . ? C19 C20 1.480(3) . ? C19 C23 1.528(2) . ? C21 C20 1.483(3) . ? C21 C27 1.535(2) . ? C12 C13 1.387(3) . ? C12 C17 1.393(3) . ? C4 C5 1.382(3) . ? C8 C7 1.391(3) . ? C8 H8 0.9300 . ? C23 C24 1.510(3) . ? C23 C26 1.515(3) . ? C23 C25 1.521(4) . ? C27 C29 1.520(4) . ? C27 C30 1.526(4) . ? C27 C28 1.529(3) . ? C20 O3 1.208(3) . ? C13 C14 1.385(3) . ? C13 H13 0.9300 . ? C5 C6 1.379(4) . ? C5 H5 0.9300 . ? C17 C16 1.381(4) . ? C17 H17 0.9300 . ? C31 H31A 0.9600 . ? C31 H31B 0.9600 . ? C31 H31C 0.9600 . ? C7 C6 1.371(4) . ? C7 H7 0.9300 . ? C6 H6 0.9300 . ? C16 C15 1.371(5) . ? C16 H16 0.9300 . ? C28 H28A 0.9600 . ? C28 H28B 0.9600 . ? C28 H28C 0.9600 . ? C15 C14 1.383(4) . ? C15 H15 0.9300 . ? C30 H30A 0.9600 . ? C30 H30B 0.9600 . ? C30 H30C 0.9600 . ? C14 H14 0.9300 . ? C24 H24A 0.9600 . ? C24 H24B 0.9600 . ? C24 H24C 0.9600 . ? C26 H26A 0.9600 . ? C26 H26B 0.9600 . ? C26 H26C 0.9600 . ? C29 H29A 0.9600 . ? C29 H29B 0.9600 . ? C29 H29C 0.9600 . ? C25 H25A 0.9600 . ? C25 H25B 0.9600 . ? C25 H25C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C18 C9 C22 C21 -1.9(2) . . . . ? C10 C9 C22 C21 -148.58(16) . . . . ? C2 C9 C22 C21 145.44(16) . . . . ? C22 C9 C18 C19 4.4(2) . . . . ? C10 C9 C18 C19 151.32(16) . . . . ? C2 C9 C18 C19 -144.78(16) . . . . ? C18 C9 C10 C2 103.49(15) . . . . ? C22 C9 C10 C2 -110.08(15) . . . . ? C18 C9 C10 C11 -11.6(2) . . . . ? C22 C9 C10 C11 134.79(16) . . . . ? C2 C9 C10 C11 -115.13(16) . . . . ? C11 C10 C2 C3 4.8(3) . . . . ? C9 C10 C2 C3 -106.10(19) . . . . ? C11 C10 C2 C1 -143.63(15) . . . . ? C9 C10 C2 C1 105.51(15) . . . . ? C11 C10 C2 C9 110.86(17) . . . . ? C18 C9 C2 C3 15.6(2) . . . . ? C22 C9 C2 C3 -132.19(16) . . . . ? C10 C9 C2 C3 122.72(17) . . . . ? C18 C9 C2 C10 -107.13(15) . . . . ? C22 C9 C2 C10 105.10(16) . . . . ? C18 C9 C2 C1 145.21(14) . . . . ? C22 C9 C2 C1 -2.6(2) . . . . ? C10 C9 C2 C1 -107.65(15) . . . . ? C10 C2 C3 C8 25.4(3) . . . . ? C1 C2 C3 C8 176.6(2) . . . . ? C9 C2 C3 C8 -49.0(3) . . . . ? C10 C2 C3 C4 -157.14(17) . . . . ? C1 C2 C3 C4 -5.91(17) . . . . ? C9 C2 C3 C4 128.43(15) . . . . ? C2 C10 C11 O2 33.2(2) . . . . ? C9 C10 C11 O2 110.74(19) . . . . ? C2 C10 C11 C12 -147.12(15) . . . . ? C9 C10 C11 C12 -69.54(19) . . . . ? C9 C18 C19 C20 0.2(3) . . . . ? C9 C18 C19 C23 -178.72(15) . . . . ? C4 N1 C1 O1 176.44(17) . . . . ? C31 N1 C1 O1 2.6(3) . . . . ? C4 N1 C1 C2 -2.91(19) . . . . ? C31 N1 C1 C2 -176.72(17) . . . . ? C3 C2 C1 O1 -173.93(17) . . . . ? C10 C2 C1 O1 -17.8(3) . . . . ? C9 C2 C1 O1 48.9(2) . . . . ? C3 C2 C1 N1 5.40(18) . . . . ? C10 C2 C1 N1 161.47(14) . . . . ? C9 C2 C1 N1 -131.73(14) . . . . ? C9 C22 C21 C20 -4.8(3) . . . . ? C9 C22 C21 C27 173.81(15) . . . . ? O2 C11 C12 C13 178.35(19) . . . . ? C10 C11 C12 C13 -1.4(3) . . . . ? O2 C11 C12 C17 -2.9(3) . . . . ? C10 C11 C12 C17 177.36(16) . . . . ? C8 C3 C4 C5 3.1(3) . . . . ? C2 C3 C4 C5 -174.83(18) . . . . ? C8 C3 C4 N1 -177.60(17) . . . . ? C2 C3 C4 N1 4.44(19) . . . . ? C1 N1 C4 C5 178.3(2) . . . . ? C31 N1 C4 C5 -8.1(3) . . . . ? C1 N1 C4 C3 -1.0(2) . . . . ? C31 N1 C4 C3 172.67(18) . . . . ? C4 C3 C8 C7 -3.3(3) . . . . ? C2 C3 C8 C7 174.0(2) . . . . ? C18 C19 C23 C24 -114.8(2) . . . . ? C20 C19 C23 C24 66.2(3) . . . . ? C18 C19 C23 C26 2.9(3) . . . . ? C20 C19 C23 C26 -176.0(2) . . . . ? C18 C19 C23 C25 121.3(3) . . . . ? C20 C19 C23 C25 -57.7(3) . . . . ? C22 C21 C27 C29 -120.3(3) . . . . ? C20 C21 C27 C29 58.3(3) . . . . ? C22 C21 C27 C30 0.1(3) . . . . ? C20 C21 C27 C30 178.7(2) . . . . ? C22 C21 C27 C28 118.2(2) . . . . ? C20 C21 C27 C28 -63.2(3) . . . . ? C18 C19 C20 O3 175.6(3) . . . . ? C23 C19 C20 O3 -5.4(4) . . . . ? C18 C19 C20 C21 -7.2(3) . . . . ? C23 C19 C20 C21 171.79(18) . . . . ? C22 C21 C20 O3 -173.3(3) . . . . ? C27 C21 C20 O3 8.0(4) . . . . ? C22 C21 C20 C19 9.5(3) . . . . ? C27 C21 C20 C19 -169.17(18) . . . . ? C17 C12 C13 C14 -0.2(3) . . . . ? C11 C12 C13 C14 178.5(2) . . . . ? C3 C4 C5 C6 -0.6(3) . . . . ? N1 C4 C5 C6 -179.8(2) . . . . ? C13 C12 C17 C16 -0.1(3) . . . . ? C11 C12 C17 C16 -178.9(2) . . . . ? C3 C8 C7 C6 1.1(4) . . . . ? C8 C7 C6 C5 1.5(4) . . . . ? C4 C5 C6 C7 -1.7(4) . . . . ? C12 C17 C16 C15 -0.1(4) . . . . ? C17 C16 C15 C14 0.6(5) . . . . ? C16 C15 C14 C13 -0.9(5) . . . . ? C12 C13 C14 C15 0.7(4) . . . . ?