#------------------------------------------------------------------------------ #$Date: 2024-04-04 18:30:56 +0300 (Thu, 04 Apr 2024) $ #$Revision: 290787 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/98/7159878.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7159878 loop_ _publ_author_name 'Shaikh, Aijaz' 'Sahoo, Satyajit' 'Marder, Seth R.' 'Barlow, Stephen' 'Mohapatra, Swagat K.' _publ_section_title ; Reductive dimerization of benzothiazolium salts. ; _journal_issue 10 _journal_name_full 'Organic & biomolecular chemistry' _journal_page_first 2115 _journal_page_last 2123 _journal_paper_doi 10.1039/d3ob01871g _journal_volume 22 _journal_year 2024 _chemical_formula_sum 'C30 H28 N2 S2' _chemical_formula_weight 480.66 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2019/1 _audit_update_record ; 2023-10-14 deposited with the CCDC. 2024-01-24 downloaded from the CCDC. ; _cell_angle_alpha 72.225(9) _cell_angle_beta 77.082(11) _cell_angle_gamma 88.777(10) _cell_formula_units_Z 4 _cell_length_a 12.016(4) _cell_length_b 14.397(5) _cell_length_c 15.879(6) _cell_measurement_reflns_used 9930 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 26.85 _cell_measurement_theta_min 2.59 _cell_volume 2546.4(16) _computing_cell_refinement 'Bruker SAINT' _computing_data_collection 'Bruker APEX2' _computing_data_reduction 'Bruker SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2019/1 (Sheldrick, 2019)' _computing_structure_solution 'SHELXS-97 (Sheldrick 2008)' _diffrn_ambient_temperature 298(2) _diffrn_measured_fraction_theta_full 0.994 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0614 _diffrn_reflns_av_unetI/netI 0.0378 _diffrn_reflns_Laue_measured_fraction_full 0.994 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_number 78849 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.533 _diffrn_reflns_theta_min 2.248 _exptl_absorpt_coefficient_mu 0.230 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6492 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ; _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.254 _exptl_crystal_description block _exptl_crystal_F_000 1016.0 _exptl_crystal_size_max 0.27 _exptl_crystal_size_mid 0.23 _exptl_crystal_size_min 0.19 _refine_diff_density_max 0.248 _refine_diff_density_min -0.343 _refine_diff_density_rms 0.045 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.253 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 621 _refine_ls_number_reflns 11676 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.253 _refine_ls_R_factor_all 0.0843 _refine_ls_R_factor_gt 0.0497 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.1000P)^2^+0.0270P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1484 _refine_ls_wR_factor_ref 0.1882 _reflns_Friedel_coverage 0.000 _reflns_number_gt 8146 _reflns_number_total 11747 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d3ob01871g2.cif _cod_data_source_block T-MBThiazine _cod_original_cell_volume 2546.3(15) _cod_database_code 7159878 _shelx_shelxl_version_number 2019/1 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_res_file ; TITL TOL6D_0m_a.res in P-1 TOL6D_0m_a.res created by SHELXL-2019/1 at 23:06:23 on 05-Sep-2023 CELL 0.71073 12.0158 14.3968 15.8790 72.225 77.082 88.777 ZERR 42.000 0.0044 0.0045 0.0055 0.009 0.011 0.010 LATT 1 SFAC C H N S UNIT 42 42 42 42 REM Old TITL TOL6D_0m in P-1 REM SHELXT solution in P-1: R1 0.169, Rweak 0.005, Alpha 0.054 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C60 N4 S4 L.S. 10 ACTA BOND FMAP 2 PLAN 20 TEMP 24.850 WGHT 0.100000 0.026950 FVAR 0.91966 S1 4 0.369560 0.722639 0.022416 11.00000 0.03977 0.05154 = 0.05295 -0.01936 -0.01565 0.00068 S2 4 0.026723 0.692387 -0.026756 11.00000 0.03973 0.05424 = 0.06254 -0.01274 -0.01713 -0.00236 S4 4 0.282884 0.678486 0.409319 11.00000 0.04983 0.05846 = 0.05830 -0.02835 -0.00320 -0.00782 S3 4 0.487310 0.930478 0.409658 11.00000 0.06763 0.05843 = 0.07100 -0.02497 -0.02800 -0.00668 N1 3 0.133638 0.777494 0.067952 11.00000 0.04276 0.04115 = 0.04912 -0.01650 -0.00082 -0.00128 N2 3 0.268132 0.749886 -0.119702 11.00000 0.04313 0.04215 = 0.03795 -0.01059 -0.00734 0.00022 N4 3 0.386075 0.851062 0.290319 11.00000 0.06173 0.07205 = 0.04203 -0.01702 -0.01492 -0.01137 N3 3 0.275385 0.842011 0.488501 11.00000 0.05854 0.06300 = 0.04721 -0.02859 -0.01723 0.00877 C7 1 0.139202 0.690077 0.038300 11.00000 0.03751 0.03937 = 0.04517 -0.01355 -0.00752 -0.00202 C22 1 0.256930 0.684414 -0.027101 11.00000 0.03726 0.04236 = 0.03741 -0.01359 -0.00897 -0.00022 C23 1 0.278308 0.579825 -0.029452 11.00000 0.03840 0.03933 = 0.04226 -0.01451 -0.00767 0.00023 C8 1 0.113038 0.598700 0.121310 11.00000 0.03948 0.04303 = 0.04260 -0.01238 -0.00439 0.00024 C24 1 0.236946 0.547263 -0.091215 11.00000 0.04949 0.04504 = 0.04834 -0.01500 -0.01332 0.00241 AFIX 43 H24 2 0.199706 0.589703 -0.131754 11.00000 -1.20000 AFIX 0 C16 1 0.327485 0.843761 0.000133 11.00000 0.04802 0.04890 = 0.04404 -0.01818 -0.01147 -0.00582 C6 1 0.192969 0.822692 -0.145659 11.00000 0.05165 0.04308 = 0.04289 -0.01499 -0.01636 0.00379 C21 1 0.211495 0.858553 0.025298 11.00000 0.04802 0.04390 = 0.04131 -0.01658 -0.01005 -0.00256 C28 1 0.335033 0.515044 0.028264 11.00000 0.05022 0.04828 = 0.05218 -0.01750 -0.01719 0.00563 AFIX 43 H28 2 0.364221 0.535415 0.069608 11.00000 -1.20000 AFIX 0 C15 1 0.382090 0.760042 -0.178487 11.00000 0.04958 0.05898 = 0.04569 -0.01425 0.00054 -0.00025 AFIX 137 H15A 2 0.376054 0.774018 -0.240362 11.00000 -1.50000 H15B 2 0.420302 0.700330 -0.160935 11.00000 -1.50000 H15C 2 0.425023 0.812473 -0.172911 11.00000 -1.50000 AFIX 0 C51 1 0.400739 0.775948 0.372007 11.00000 0.04966 0.05319 = 0.03926 -0.01817 -0.00685 -0.00838 C36 1 0.180833 0.833077 0.453380 11.00000 0.05449 0.05577 = 0.03993 -0.01404 -0.01026 0.00398 C13 1 0.147648 0.596647 0.200174 11.00000 0.05325 0.05537 = 0.04513 -0.01730 -0.00635 -0.00160 AFIX 43 H13 2 0.184841 0.651522 0.202450 11.00000 -1.20000 AFIX 0 C52 1 0.512735 0.725679 0.354104 11.00000 0.04838 0.06625 = 0.04453 -0.02632 -0.00334 -0.00940 C37 1 0.391447 0.817270 0.454525 11.00000 0.05332 0.05360 = 0.04195 -0.02029 -0.01215 -0.00138 C5 1 0.230993 0.912836 -0.211782 11.00000 0.06985 0.04974 = 0.04645 -0.01093 -0.01446 0.00045 AFIX 43 H5 2 0.308752 0.926994 -0.236756 11.00000 -1.20000 AFIX 0 C31 1 0.171358 0.758255 0.415273 11.00000 0.04904 0.05675 = 0.04174 -0.01493 -0.00787 -0.00422 C38 1 0.436966 0.747307 0.531517 11.00000 0.06319 0.05797 = 0.04307 -0.02364 -0.01695 0.00836 C17 1 0.405528 0.922930 -0.041963 11.00000 0.05359 0.06154 = 0.06116 -0.02074 -0.01456 -0.01492 AFIX 43 H17 2 0.482469 0.912574 -0.060976 11.00000 -1.20000 AFIX 0 C25 1 0.251000 0.451823 -0.092597 11.00000 0.05669 0.04878 = 0.06350 -0.02456 -0.01337 -0.00303 AFIX 43 H25 2 0.221797 0.431167 -0.133777 11.00000 -1.20000 AFIX 0 C26 1 0.306912 0.386794 -0.034790 11.00000 0.04838 0.04286 = 0.06869 -0.01957 -0.00952 0.00119 C9 1 0.056981 0.515077 0.121751 11.00000 0.05127 0.04980 = 0.05174 -0.01270 -0.00800 -0.00557 AFIX 43 H9 2 0.032421 0.514607 0.070334 11.00000 -1.20000 AFIX 0 C27 1 0.349234 0.419848 0.025586 11.00000 0.05429 0.04648 = 0.07066 -0.01448 -0.02040 0.01108 AFIX 43 H27 2 0.387904 0.377625 0.065123 11.00000 -1.20000 AFIX 0 C20 1 0.176362 0.954651 0.010566 11.00000 0.06635 0.04157 = 0.06370 -0.02087 -0.01421 0.00231 AFIX 43 H20 2 0.099484 0.966221 0.027989 11.00000 -1.20000 AFIX 0 C39 1 0.362134 0.681053 0.602970 11.00000 0.06985 0.06722 = 0.04433 -0.02308 -0.01327 0.01167 AFIX 43 H39 2 0.284161 0.681625 0.605060 11.00000 -1.20000 AFIX 0 C57 1 0.609283 0.778786 0.292984 11.00000 0.05506 0.06692 = 0.05144 -0.01817 -0.00462 -0.01109 AFIX 43 H57 2 0.603263 0.843187 0.259033 11.00000 -1.20000 AFIX 0 C50 1 0.360288 0.947691 0.285301 11.00000 0.05412 0.06765 = 0.04970 -0.00093 -0.01354 -0.01055 C1 1 0.075600 0.805124 -0.108159 11.00000 0.05080 0.05130 = 0.05226 -0.01272 -0.02070 0.00597 C55 1 0.726878 0.640036 0.331424 11.00000 0.05536 0.08157 = 0.06795 -0.03451 0.00082 -0.00220 C30 1 0.021195 0.794965 0.116502 11.00000 0.05713 0.05710 = 0.07503 -0.02511 0.01267 0.00168 AFIX 137 H30A 2 0.029729 0.829326 0.158028 11.00000 -1.50000 H30B 2 -0.020169 0.733640 0.149654 11.00000 -1.50000 H30C 2 -0.020092 0.833443 0.073825 11.00000 -1.50000 AFIX 0 C4 1 0.152693 0.980580 -0.239756 11.00000 0.09854 0.05409 = 0.05678 -0.00278 -0.02209 0.01030 AFIX 43 H4 2 0.178597 1.039205 -0.284880 11.00000 -1.20000 AFIX 0 C32 1 0.075200 0.746819 0.384909 11.00000 0.06117 0.07344 = 0.05485 -0.01964 -0.01461 -0.00456 AFIX 43 H32 2 0.071588 0.698230 0.358047 11.00000 -1.20000 AFIX 0 C18 1 0.369363 1.017314 -0.055795 11.00000 0.08148 0.05206 = 0.07303 -0.01462 -0.01871 -0.02305 AFIX 43 H18 2 0.421898 1.070363 -0.082602 11.00000 -1.20000 AFIX 0 C12 1 0.127042 0.513712 0.274813 11.00000 0.06528 0.06961 = 0.04452 -0.00731 -0.01013 0.00323 AFIX 43 H12 2 0.150884 0.513881 0.326600 11.00000 -1.20000 AFIX 0 C11 1 0.071925 0.430456 0.274605 11.00000 0.06277 0.05816 = 0.05564 -0.00050 -0.00172 -0.00028 C10 1 0.036950 0.432814 0.196654 11.00000 0.06442 0.04895 = 0.06658 -0.00719 -0.00759 -0.01258 AFIX 43 H10 2 -0.000707 0.377951 0.194798 11.00000 -1.20000 AFIX 0 C59 1 0.367828 0.815897 0.217762 11.00000 0.07639 0.12334 = 0.04026 -0.02875 -0.01048 -0.02684 AFIX 137 H59A 2 0.287593 0.802267 0.225893 11.00000 -1.50000 H59B 2 0.408033 0.757316 0.219046 11.00000 -1.50000 H59C 2 0.395788 0.864844 0.160343 11.00000 -1.50000 AFIX 0 C56 1 0.713438 0.736353 0.282662 11.00000 0.05166 0.08514 = 0.06335 -0.02013 0.00370 -0.01262 AFIX 43 H56 2 0.776626 0.773208 0.241882 11.00000 -1.20000 AFIX 0 C53 1 0.524903 0.628907 0.400293 11.00000 0.05610 0.05854 = 0.06703 -0.02263 0.00615 -0.00699 AFIX 43 H53 2 0.461183 0.590983 0.439031 11.00000 -1.20000 AFIX 0 C43 1 0.552489 0.744699 0.533001 11.00000 0.06445 0.08049 = 0.06122 -0.02640 -0.02201 0.00750 AFIX 43 H43 2 0.604732 0.788953 0.486726 11.00000 -1.20000 AFIX 0 C35 1 0.089339 0.893622 0.458788 11.00000 0.07801 0.06725 = 0.07022 -0.02767 -0.03096 0.01810 AFIX 43 H35 2 0.093468 0.944809 0.482411 11.00000 -1.20000 AFIX 0 C46 1 0.404039 0.995219 0.336257 11.00000 0.06243 0.05455 = 0.06636 -0.00641 -0.01653 -0.00755 C19 1 0.255855 1.031651 -0.029682 11.00000 0.08164 0.04405 = 0.07988 -0.02025 -0.02275 -0.00456 AFIX 43 H19 2 0.231685 1.095084 -0.039355 11.00000 -1.20000 AFIX 0 C45 1 0.263442 0.897399 0.553541 11.00000 0.08349 0.08408 = 0.06601 -0.04703 -0.02661 0.02144 AFIX 137 H45A 2 0.269037 0.966069 0.521434 11.00000 -1.50000 H45B 2 0.323071 0.881697 0.586230 11.00000 -1.50000 H45C 2 0.190410 0.880656 0.595496 11.00000 -1.50000 AFIX 0 C40 1 0.402616 0.614096 0.671184 11.00000 0.09076 0.07267 = 0.04401 -0.01756 -0.01263 0.01875 AFIX 43 H40 2 0.350719 0.570048 0.717961 11.00000 -1.20000 AFIX 0 C54 1 0.630244 0.587482 0.389892 11.00000 0.06297 0.06536 = 0.07367 -0.02712 0.00426 0.00147 AFIX 43 H54 2 0.636055 0.522744 0.423063 11.00000 -1.20000 AFIX 0 C33 1 -0.015357 0.805668 0.393495 11.00000 0.06993 0.08493 = 0.07664 -0.02402 -0.03414 0.00719 AFIX 43 H33 2 -0.081004 0.795637 0.374923 11.00000 -1.20000 AFIX 0 C2 1 -0.000149 0.876422 -0.136219 11.00000 0.06263 0.07565 = 0.07256 -0.01470 -0.02536 0.01850 AFIX 43 H2 2 -0.077855 0.865055 -0.109632 11.00000 -1.20000 AFIX 0 C41 1 0.515931 0.610366 0.672293 11.00000 0.09849 0.08539 = 0.05477 -0.02927 -0.03052 0.03619 C34 1 -0.007212 0.879556 0.429987 11.00000 0.07352 0.08891 = 0.08501 -0.02841 -0.03504 0.02780 AFIX 43 H34 2 -0.067465 0.920569 0.435341 11.00000 -1.20000 AFIX 0 C3 1 0.038162 0.963131 -0.202471 11.00000 0.09061 0.06854 = 0.07940 -0.00758 -0.03335 0.02831 AFIX 43 H3 2 -0.013295 1.009541 -0.221795 11.00000 -1.20000 AFIX 0 C42 1 0.590733 0.677540 0.601995 11.00000 0.07573 0.09995 = 0.07284 -0.03872 -0.03462 0.02712 AFIX 43 H42 2 0.668345 0.677395 0.601261 11.00000 -1.20000 AFIX 0 C60 1 0.381456 1.091841 0.331002 11.00000 0.07688 0.06096 = 0.09963 -0.01203 -0.01641 -0.00391 AFIX 43 H60 2 0.407963 1.120406 0.368495 11.00000 -1.20000 AFIX 0 C29 1 0.321102 0.283499 -0.038777 11.00000 0.08823 0.04517 = 0.12346 -0.03448 -0.03231 0.00897 AFIX 137 H29A 2 0.250564 0.258060 -0.043916 11.00000 -1.50000 H29B 2 0.341371 0.243415 0.015597 11.00000 -1.50000 H29C 2 0.380380 0.283442 -0.090542 11.00000 -1.50000 AFIX 0 C58 1 0.840374 0.593465 0.323981 11.00000 0.05928 0.10197 = 0.10921 -0.03679 0.00036 0.00735 AFIX 137 H58A 2 0.837804 0.538391 0.377071 11.00000 -1.50000 H58B 2 0.899203 0.640165 0.319090 11.00000 -1.50000 H58C 2 0.856581 0.572103 0.271030 11.00000 -1.50000 AFIX 0 C49 1 0.294500 1.002499 0.226395 11.00000 0.07203 0.09751 = 0.07145 0.00749 -0.02960 -0.01647 AFIX 43 H49 2 0.262146 0.973388 0.192076 11.00000 -1.20000 AFIX 0 C14 1 0.049406 0.339419 0.356835 11.00000 0.12221 0.08233 = 0.08097 0.01842 -0.01055 -0.01403 AFIX 137 H14A 2 -0.009108 0.298163 0.352093 11.00000 -1.50000 H14B 2 0.024780 0.357849 0.411061 11.00000 -1.50000 H14C 2 0.118317 0.304722 0.359310 11.00000 -1.50000 AFIX 0 C44 1 0.558619 0.535942 0.746432 11.00000 0.13516 0.13130 = 0.07913 -0.01801 -0.04793 0.05837 AFIX 137 H44A 2 0.571822 0.476539 0.730987 11.00000 -1.50000 H44B 2 0.502477 0.523134 0.802654 11.00000 -1.50000 H44C 2 0.628737 0.560770 0.752859 11.00000 -1.50000 AFIX 0 C48 1 0.277863 1.099478 0.219429 11.00000 0.08361 0.09788 = 0.11482 0.02646 -0.03517 0.00373 AFIX 43 H48 2 0.236421 1.135159 0.178461 11.00000 -1.20000 AFIX 0 C47 1 0.320298 1.145219 0.270814 11.00000 0.08489 0.06890 = 0.13705 0.00348 -0.02687 0.00513 AFIX 43 H47 2 0.307918 1.210647 0.264981 11.00000 -1.20000 AFIX 0 HKLF 4 REM TOL6D_0m_a.res in P-1 REM wR2 = 0.1882, GooF = S = 1.253, Restrained GooF = 1.253 for all data REM R1 = 0.0497 for 8146 Fo > 4sig(Fo) and 0.0843 for all 11676 data REM 621 parameters refined using 0 restraints END WGHT 0.0609 1.0529 REM Highest difference peak 0.248, deepest hole -0.343, 1-sigma level 0.045 Q1 1 0.0965 0.3436 0.4075 11.00000 0.05 0.25 Q2 1 0.2946 0.2444 -0.0818 11.00000 0.05 0.23 Q3 1 0.6231 0.7116 0.4586 11.00000 0.05 0.22 Q4 1 0.1999 0.6711 0.0175 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183.68 19.80 0 11 -3 161.78 17.80 0 11 -3 224.58 19.00 0 -11 3 171.58 18.60 0 -11 3 208.48 18.30 0 -11 3 215.78 24.70 -1 11 -3 -4.60 7.20 -1 11 -3 -5.90 5.00 1 -11 3 -2.20 6.50 1 -11 3 -12.40 3.70 1 -11 3 1.70 8.90 -2 11 -3 404.76 31.30 -2 11 -3 433.06 29.90 2 -11 3 381.06 34.80 2 -11 3 403.86 29.40 -3 11 -3 90.89 13.90 -3 11 -3 82.89 14.70 3 -11 3 84.19 14.90 3 -11 3 79.69 17.40 -4 11 -3 -0.60 2.70 -4 11 -3 1.40 2.70 -4 11 -3 0.00 6.50 -4 11 -3 -0.30 5.70 4 -11 3 5.30 3.10 4 -11 3 2.40 4.20 4 -11 3 7.40 7.80 -5 11 -3 10.70 6.60 -5 11 -3 15.80 4.50 -5 11 -3 -1.40 4.80 -5 11 -3 1.90 7.20 -5 11 -3 12.00 8.10 5 -11 3 4.60 4.10 5 -11 3 7.20 4.80 5 -11 3 -1.20 8.00 5 -11 3 3.20 4.50 -6 11 -3 124.19 13.80 -6 11 -3 83.09 12.40 -6 11 -3 114.29 17.60 -6 11 -3 114.59 18.40 6 -11 3 93.79 13.30 6 -11 3 102.89 18.00 6 -11 3 129.39 11.90 6 -11 3 104.59 11.60 -7 11 -3 43.40 10.30 -7 11 -3 57.59 13.20 -7 11 -3 54.99 9.10 7 -11 3 48.60 9.10 7 -11 3 53.09 11.10 7 -11 3 50.79 8.90 7 -11 3 61.19 14.30 -8 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6 19 -6.60 4.90 4 6 19 -3.70 3.40 4 6 19 8.30 9.00 4 6 19 -11.10 8.10 5 6 19 34.20 11.80 5 6 19 39.10 14.80 5 6 19 24.70 8.90 -6 -6 -19 38.90 15.20 6 6 19 24.00 12.50 6 6 19 44.90 18.50 -7 -6 -19 37.10 17.30 7 6 19 -2.10 14.40 7 6 19 39.70 15.40 -8 -6 -19 0.90 8.40 8 6 19 22.20 13.70 8 6 19 6.00 11.60 -9 -6 -19 -21.50 10.40 9 6 19 -3.60 12.60 9 6 19 5.30 7.70 9 6 19 -23.80 11.70 2 -7 -19 2.60 12.80 2 -7 -19 -10.70 10.30 2 -7 -19 -4.70 7.40 -2 7 19 -1.90 11.00 1 -7 -19 4.20 10.90 1 -7 -19 16.40 8.30 1 -7 -19 1.80 14.60 -1 7 19 1.10 13.30 -1 7 19 -9.70 9.60 0 -7 -19 41.40 11.10 0 -7 -19 3.10 10.40 0 -7 -19 12.10 13.10 0 7 19 22.00 15.80 0 7 19 39.00 15.20 -1 -7 -19 5.60 8.00 -1 -7 -19 14.00 11.90 1 7 19 -11.40 8.60 -2 -7 -19 34.90 10.60 -2 -7 -19 7.50 9.40 -2 -7 -19 33.70 13.10 2 7 19 19.10 11.40 2 7 19 24.70 13.40 -3 -7 -19 -6.40 7.40 -3 -7 -19 11.30 10.90 -3 -7 -19 1.70 11.00 3 7 19 9.80 9.60 3 7 19 -9.40 8.90 3 7 19 -6.60 2.70 3 7 19 -7.60 5.10 -4 -7 -19 -3.30 8.40 4 7 19 14.60 11.50 4 7 19 19.20 11.20 -5 -7 -19 0.60 10.10 5 7 19 33.80 12.10 5 7 19 7.00 10.40 5 7 19 13.60 8.30 -6 -7 -19 -3.30 11.30 6 7 19 -7.60 6.80 6 7 19 -0.30 9.70 6 7 19 -7.60 6.60 -7 -7 -19 13.60 12.60 7 7 19 8.20 14.90 7 7 19 6.70 9.30 -8 -7 -19 8.70 9.20 8 7 19 -14.30 7.70 8 7 19 0.50 10.40 8 7 19 13.00 10.10 2 -8 -19 19.40 15.60 2 -8 -19 -1.40 12.10 2 -8 -19 14.00 7.90 -2 8 19 -0.90 13.90 -2 8 19 -11.90 9.50 1 -8 -19 -10.30 11.70 1 -8 -19 12.60 12.40 1 -8 -19 -1.30 7.20 -1 8 19 -2.10 14.00 -1 8 19 -4.70 9.90 0 -8 -19 11.40 9.10 0 -8 -19 -1.10 12.20 0 -8 -19 7.70 9.60 0 8 19 -13.90 8.90 0 8 19 3.70 12.00 -1 -8 -19 -9.00 9.90 -1 -8 -19 24.00 14.50 -1 -8 -19 6.70 7.50 1 8 19 26.20 12.00 1 8 19 -8.40 11.40 -2 -8 -19 8.80 11.50 -2 -8 -19 -15.00 9.20 2 8 19 -5.10 5.30 2 8 19 -12.50 7.80 2 8 19 5.40 7.70 -3 -8 -19 -0.20 7.10 -3 -8 -19 10.00 10.90 3 8 19 2.70 6.30 3 8 19 -0.50 8.90 3 8 19 -12.70 7.50 -4 -8 -19 3.20 8.90 4 8 19 -8.00 7.30 4 8 19 6.40 7.90 4 8 19 -4.80 7.60 5 8 19 -2.10 7.50 5 8 19 0.40 6.70 5 8 19 13.50 11.30 -6 -8 -19 -13.30 11.10 6 8 19 11.50 12.90 6 8 19 -4.10 7.80 6 8 19 -12.20 6.10 -7 -8 -19 10.20 8.30 7 8 19 10.90 8.50 7 8 19 1.10 9.00 7 8 19 8.30 12.90 -8 -8 -19 -11.80 10.90 -8 -8 -19 -4.00 7.50 8 8 19 -7.60 9.20 8 8 19 -21.00 6.50 8 8 19 -14.70 8.80 1 -9 -19 19.40 12.20 1 -9 -19 13.70 7.30 1 -9 -19 0.30 13.80 -1 9 19 13.70 11.30 -1 9 19 16.30 13.90 0 -9 -19 29.20 9.80 0 -9 -19 21.90 13.70 0 -9 -19 1.90 13.70 0 9 19 23.60 16.70 0 9 19 22.10 13.30 -1 -9 -19 8.60 7.30 -1 -9 -19 2.80 9.70 1 9 19 -10.70 8.40 1 9 19 15.70 13.60 -2 -9 -19 -15.00 11.40 -2 -9 -19 -6.60 11.00 2 9 19 -11.00 7.10 2 9 19 -4.50 12.40 2 9 19 -13.80 5.20 -3 -9 -19 6.80 9.20 -3 -9 -19 -5.70 12.20 3 9 19 2.40 13.30 3 9 19 12.70 7.50 3 9 19 4.10 6.70 -4 -9 -19 -8.90 10.40 4 9 19 -8.00 6.50 4 9 19 6.80 14.10 4 9 19 5.30 8.40 -5 -9 -19 -19.60 9.90 5 9 19 -14.40 6.60 5 9 19 -24.00 10.50 5 9 19 -13.40 6.80 -6 -9 -19 11.50 10.00 6 9 19 0.00 7.80 6 9 19 8.70 9.40 6 9 19 8.90 14.60 -7 -9 -19 15.10 10.90 7 9 19 -17.10 9.00 7 9 19 -4.60 8.70 7 9 19 -11.10 7.90 -8 -9 -19 12.20 13.90 -8 -9 -19 46.30 13.00 8 9 19 16.20 9.20 8 9 19 17.10 11.40 8 9 19 55.09 19.40 1 -10 -19 -4.60 8.20 1 -10 -19 18.00 7.90 1 -10 -19 5.40 10.90 -1 10 19 -7.00 10.00 -1 10 19 -1.20 9.20 0 -10 -19 3.00 6.20 0 -10 -19 5.50 12.00 0 -10 -19 14.00 10.80 0 10 19 0.50 9.90 0 10 19 -11.70 9.80 -1 -10 -19 -6.20 9.60 -1 -10 -19 -7.90 7.10 -1 -10 -19 -13.50 6.50 1 10 19 -5.80 2.60 1 10 19 -6.80 7.70 1 10 19 -10.30 8.20 -2 -10 -19 -9.60 12.30 -2 -10 -19 -2.20 9.10 2 10 19 -2.00 8.30 2 10 19 1.40 9.30 2 10 19 3.20 8.20 -3 -10 -19 15.70 11.80 -3 -10 -19 7.20 14.00 3 10 19 34.30 16.30 3 10 19 4.80 7.00 3 10 19 17.20 8.80 -4 -10 -19 -8.20 6.00 -4 -10 -19 -13.30 7.90 4 10 19 -13.70 6.00 4 10 19 -22.60 10.60 4 10 19 -1.00 6.60 -5 -10 -19 16.00 10.40 5 10 19 16.50 7.30 5 10 19 -1.40 7.60 5 10 19 19.50 13.00 -6 -10 -19 38.90 16.00 6 10 19 30.60 8.20 6 10 19 24.30 13.00 6 10 19 26.50 12.30 -7 -10 -19 107.09 22.00 -7 -10 -19 113.89 18.40 7 10 19 90.19 18.00 7 10 19 157.28 27.80 0 -11 -19 3.30 13.20 0 -11 -19 6.00 6.40 0 -11 -19 18.10 13.90 0 11 19 -7.90 4.50 0 11 19 0.10 10.20 -1 -11 -19 -5.70 8.80 -1 -11 -19 11.40 13.70 1 11 19 -3.80 13.70 1 11 19 2.60 8.50 -2 -11 -19 1.30 14.20 -2 -11 -19 12.10 12.30 2 11 19 19.40 9.30 2 11 19 -4.50 14.70 2 11 19 15.00 7.90 -3 -11 -19 -23.20 10.80 -3 -11 -19 14.70 12.90 3 11 19 -9.10 6.40 3 11 19 -7.90 6.00 3 11 19 -6.10 14.30 -4 -11 -19 2.90 12.90 -4 -11 -19 25.20 13.40 4 11 19 4.50 7.90 4 11 19 -2.80 5.50 4 11 19 -2.40 13.80 -5 -11 -19 13.70 13.50 5 11 19 6.50 8.30 5 11 19 16.00 15.10 -6 -11 -19 12.10 13.40 6 11 19 29.30 15.70 6 11 19 6.70 9.40 -2 -12 -19 -4.20 7.40 -2 -12 -19 -18.00 7.20 2 12 19 17.60 13.70 2 12 19 -7.20 8.60 -3 -12 -19 17.80 11.20 -3 -12 -19 12.80 13.60 3 12 19 24.60 10.80 3 12 19 11.60 11.80 -4 -12 -19 15.30 10.60 -4 -12 -19 9.50 11.60 4 12 19 3.10 10.10 4 12 19 -3.20 9.40 -2 -2 -20 -5.20 9.20 -2 -2 -20 -4.90 12.10 2 2 20 -5.30 13.60 2 2 20 -10.90 10.80 -3 -2 -20 -18.20 7.30 -3 -2 -20 -0.90 10.40 3 2 20 -8.40 12.00 3 2 20 23.00 14.70 -4 -2 -20 -15.80 8.50 -4 -2 -20 -3.00 6.80 -4 -2 -20 1.00 13.10 4 2 20 9.60 14.90 4 2 20 7.10 12.70 -5 -2 -20 -0.70 10.50 -5 -2 -20 21.40 15.00 5 2 20 27.10 16.00 5 2 20 9.20 14.90 -1 -3 -20 -23.70 11.40 -1 -3 -20 -3.30 8.00 -1 -3 -20 -8.50 10.00 1 3 20 -2.20 13.20 1 3 20 4.40 12.80 -2 -3 -20 13.20 14.70 -2 -3 -20 -3.50 10.10 -2 -3 -20 4.90 8.80 2 3 20 -12.70 12.20 2 3 20 -8.20 13.00 -3 -3 -20 -11.30 8.70 -3 -3 -20 -25.20 10.20 -3 -3 -20 1.30 9.90 3 3 20 -15.00 11.10 3 3 20 -12.30 11.80 -4 -3 -20 0.60 9.60 -4 -3 -20 7.90 13.40 -4 -3 -20 -4.20 9.80 4 3 20 1.90 13.10 4 3 20 -5.90 12.10 -5 -3 -20 69.69 20.20 -5 -3 -20 59.19 13.20 5 3 20 62.39 7.90 5 3 20 56.19 20.10 5 3 20 63.19 20.40 -6 -3 -20 14.60 15.50 -6 -3 -20 24.70 12.70 6 3 20 35.20 16.80 6 3 20 18.80 15.50 0 -4 -20 22.40 13.10 0 -4 -20 12.40 11.50 0 -4 -20 11.40 9.60 0 4 20 17.90 12.80 -1 -4 -20 3.60 10.30 -1 -4 -20 -5.50 11.20 -1 -4 -20 0.00 7.90 1 4 20 -4.60 11.50 1 4 20 6.40 8.80 -2 -4 -20 2.20 9.90 -2 -4 -20 -8.20 10.00 -2 -4 -20 2.90 6.70 2 4 20 -10.00 9.10 2 4 20 -24.30 11.80 -3 -4 -20 17.10 13.30 -3 -4 -20 5.00 8.10 -3 -4 -20 -9.20 9.40 3 4 20 8.40 11.30 3 4 20 17.80 14.20 -4 -4 -20 155.28 26.60 -4 -4 -20 113.39 19.80 -4 -4 -20 127.39 20.90 4 4 20 140.19 24.20 4 4 20 122.49 24.30 -5 -4 -20 4.40 10.90 -5 -4 -20 -6.00 9.40 5 4 20 -3.70 13.50 5 4 20 2.60 8.00 5 4 20 -0.10 5.30 -6 -4 -20 39.10 12.60 -6 -4 -20 31.20 14.60 6 4 20 33.70 17.90 6 4 20 30.10 8.80 6 4 20 24.80 13.80 -7 -4 -20 11.30 12.90 -7 -4 -20 -5.90 5.60 0 -5 -20 -7.40 7.20 0 -5 -20 -17.40 9.80 0 -5 -20 4.50 9.10 0 5 20 3.20 12.30 0 5 20 -15.40 8.30 -1 -5 -20 -5.50 6.60 -1 -5 -20 3.80 9.70 -1 -5 -20 11.80 12.50 1 5 20 19.40 12.80 1 5 20 -16.70 9.20 -2 -5 -20 2.40 10.40 -2 -5 -20 15.80 9.60 -2 -5 -20 31.90 13.80 2 5 20 -4.40 11.90 2 5 20 31.10 13.10 -3 -5 -20 9.00 9.10 -3 -5 -20 24.50 13.70 -3 -5 -20 33.90 15.50 3 5 20 35.80 15.40 3 5 20 21.30 12.80 -4 -5 -20 16.30 12.50 -4 -5 -20 2.80 10.20 -4 -5 -20 10.20 9.40 4 5 20 -13.00 6.80 4 5 20 -4.50 11.70 4 5 20 -1.30 4.90 -5 -5 -20 141.79 21.60 -5 -5 -20 160.58 27.10 5 5 20 191.18 29.60 5 5 20 150.18 15.30 5 5 20 147.09 25.80 -6 -5 -20 8.50 12.70 6 5 20 3.40 7.10 6 5 20 -7.60 12.00 6 5 20 31.50 19.40 -7 -5 -20 -15.10 11.80 7 5 20 -8.40 11.90 7 5 20 -6.10 6.80 7 5 20 -6.00 15.30 0 -6 -20 16.40 12.70 0 -6 -20 23.60 11.20 0 -6 -20 38.10 11.60 0 6 20 22.70 12.90 0 6 20 32.30 14.70 -1 -6 -20 10.10 9.00 -1 -6 -20 4.60 10.30 -1 -6 -20 -5.70 7.80 1 6 20 11.30 11.80 1 6 20 13.50 12.30 -2 -6 -20 -4.60 9.90 -2 -6 -20 4.60 9.00 -2 -6 -20 -1.60 7.90 2 6 20 -24.40 9.10 2 6 20 -6.70 7.80 -3 -6 -20 -0.80 10.40 -3 -6 -20 2.20 8.10 -3 -6 -20 -5.90 10.30 3 6 20 -6.40 4.10 3 6 20 -4.50 10.20 3 6 20 -10.20 7.60 -4 -6 -20 71.89 15.30 -4 -6 -20 67.59 16.90 -4 -6 -20 79.29 19.00 4 6 20 66.89 10.50 4 6 20 79.99 20.80 4 6 20 87.89 19.10 -5 -6 -20 10.20 11.70 5 6 20 3.70 9.50 5 6 20 -1.20 5.90 5 6 20 0.20 10.10 -6 -6 -20 -1.30 12.90 6 6 20 21.90 15.60 6 6 20 -4.90 7.50 6 6 20 -8.00 9.10 -7 -6 -20 -5.10 12.40 7 6 20 -3.50 9.30 7 6 20 15.90 14.90 7 6 20 -7.20 9.60 0 -7 -20 -6.70 11.60 0 -7 -20 10.10 10.90 0 -7 -20 3.50 8.20 0 7 20 13.80 12.10 0 7 20 7.70 9.80 -1 -7 -20 4.30 10.10 -1 -7 -20 9.70 8.90 1 7 20 1.60 10.00 1 7 20 4.20 9.70 -2 -7 -20 29.80 12.50 -2 -7 -20 35.00 15.10 2 7 20 41.10 15.80 2 7 20 49.50 15.10 -3 -7 -20 8.20 11.00 -3 -7 -20 -4.50 10.20 -3 -7 -20 14.60 8.60 3 7 20 22.60 13.40 3 7 20 0.80 6.00 3 7 20 7.20 9.70 -4 -7 -20 9.70 9.10 -4 -7 -20 7.60 7.30 -4 -7 -20 13.20 11.70 4 7 20 -6.10 9.00 4 7 20 9.30 7.50 4 7 20 7.20 6.80 -5 -7 -20 7.70 9.80 5 7 20 3.20 6.60 5 7 20 4.30 11.40 5 7 20 9.00 11.60 -6 -7 -20 7.20 14.40 6 7 20 -6.90 14.60 6 7 20 -3.60 7.40 6 7 20 -10.50 9.10 -1 -8 -20 21.40 15.30 -1 -8 -20 60.29 12.30 -1 -8 -20 43.70 16.30 1 8 20 50.39 13.70 1 8 20 48.70 15.00 -2 -8 -20 -16.70 10.50 -2 -8 -20 28.80 14.80 -2 -8 -20 -9.10 7.30 2 8 20 15.60 12.00 2 8 20 4.80 11.00 -3 -8 -20 -9.60 8.20 -3 -8 -20 -1.60 8.20 3 8 20 -17.10 8.30 3 8 20 6.70 11.20 -4 -8 -20 -13.90 11.50 -4 -8 -20 -7.20 8.00 4 8 20 1.50 9.50 4 8 20 1.20 7.30 -5 -8 -20 -6.10 11.70 5 8 20 11.80 15.10 5 8 20 -12.90 8.70 5 8 20 -0.40 8.00 -6 -8 -20 -20.20 10.80 6 8 20 -5.70 8.10 6 8 20 -11.00 9.10 6 8 20 -11.70 13.80 -1 -9 -20 -16.70 11.40 -1 -9 -20 -15.10 10.90 -1 -9 -20 -5.00 6.80 1 9 20 -26.50 11.50 -2 -9 -20 -5.40 8.00 -2 -9 -20 -22.20 10.70 -2 -9 -20 -7.10 12.30 2 9 20 -7.30 9.90 2 9 20 -8.00 12.60 -3 -9 -20 -12.00 11.70 -3 -9 -20 -29.00 10.60 3 9 20 -15.70 6.70 3 9 20 16.00 15.40 3 9 20 -1.70 9.00 -4 -9 -20 16.10 14.70 -4 -9 -20 25.00 12.50 4 9 20 11.70 10.70 4 9 20 16.20 8.90 4 9 20 17.50 17.00 -5 -9 -20 16.90 13.70 5 9 20 -12.90 13.00 5 9 20 -12.80 6.50 5 9 20 -3.80 8.70 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 11441 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group S1 S 0.36956(4) 0.72264(4) 0.02242(4) 0.04647(15) Uani 1 1 d . . . . . S2 S 0.02672(5) 0.69239(4) -0.02676(4) 0.05241(16) Uani 1 1 d . . . . . S4 S 0.28288(5) 0.67849(4) 0.40932(4) 0.05449(17) Uani 1 1 d . . . . . S3 S 0.48731(6) 0.93048(4) 0.40966(5) 0.06236(19) Uani 1 1 d . . . . . N1 N 0.13364(14) 0.77749(11) 0.06795(12) 0.0453(4) Uani 1 1 d . . . . . N2 N 0.26813(14) 0.74989(11) -0.11970(11) 0.0418(4) Uani 1 1 d . . . . . N4 N 0.38607(18) 0.85106(15) 0.29032(12) 0.0580(5) Uani 1 1 d . . . . . N3 N 0.27538(17) 0.84201(13) 0.48850(12) 0.0528(5) Uani 1 1 d . . . . . C7 C 0.13920(17) 0.69008(13) 0.03830(14) 0.0408(4) Uani 1 1 d . . . . . C22 C 0.25693(16) 0.68441(13) -0.02710(13) 0.0386(4) Uani 1 1 d . . . . . C23 C 0.27831(16) 0.57982(13) -0.02945(13) 0.0398(4) Uani 1 1 d . . . . . C8 C 0.11304(17) 0.59870(14) 0.12131(13) 0.0427(4) Uani 1 1 d . . . . . C24 C 0.23695(19) 0.54726(14) -0.09122(14) 0.0471(5) Uani 1 1 d . . . . . H24 H 0.199706 0.589703 -0.131754 0.057 Uiso 1 1 calc R U . . . C16 C 0.32748(18) 0.84376(14) 0.00013(14) 0.0458(5) Uani 1 1 d . . . . . C6 C 0.19297(18) 0.82269(14) -0.14566(14) 0.0446(5) Uani 1 1 d . . . . . C21 C 0.21150(18) 0.85855(14) 0.02530(13) 0.0436(4) Uani 1 1 d . . . . . C28 C 0.33503(19) 0.51504(15) 0.02826(15) 0.0489(5) Uani 1 1 d . . . . . H28 H 0.364221 0.535415 0.069608 0.059 Uiso 1 1 calc R U . . . C15 C 0.38209(19) 0.76004(17) -0.17849(15) 0.0537(5) Uani 1 1 d . . . . . H15A H 0.376054 0.774018 -0.240362 0.081 Uiso 1 1 calc R U . . . H15B H 0.420302 0.700330 -0.160935 0.081 Uiso 1 1 calc R U . . . H15C H 0.425023 0.812473 -0.172911 0.081 Uiso 1 1 calc R U . . . C51 C 0.40074(19) 0.77595(15) 0.37201(14) 0.0468(5) Uani 1 1 d . . . . . C36 C 0.1808(2) 0.83308(16) 0.45338(14) 0.0503(5) Uani 1 1 d . . . . . C13 C 0.1476(2) 0.59665(16) 0.20017(14) 0.0516(5) Uani 1 1 d . . . . . H13 H 0.184841 0.651522 0.202450 0.062 Uiso 1 1 calc R U . . . C52 C 0.51273(19) 0.72568(17) 0.35410(14) 0.0519(5) Uani 1 1 d . . . . . C37 C 0.39145(19) 0.81727(15) 0.45452(14) 0.0481(5) Uani 1 1 d . . . . . C5 C 0.2310(2) 0.91284(16) -0.21178(15) 0.0560(6) Uani 1 1 d . . . . . H5 H 0.308752 0.926994 -0.236756 0.067 Uiso 1 1 calc R U . . . C31 C 0.17136(19) 0.75825(16) 0.41527(14) 0.0495(5) Uani 1 1 d . . . . . C38 C 0.4370(2) 0.74731(16) 0.53152(15) 0.0522(5) Uani 1 1 d . . . . . C17 C 0.4055(2) 0.92293(17) -0.04196(17) 0.0578(6) Uani 1 1 d . . . . . H17 H 0.482469 0.912574 -0.060976 0.069 Uiso 1 1 calc R U . . . C25 C 0.2510(2) 0.45182(16) -0.09260(17) 0.0546(5) Uani 1 1 d . . . . . H25 H 0.221797 0.431167 -0.133777 0.066 Uiso 1 1 calc R U . . . C26 C 0.30691(19) 0.38679(15) -0.03479(17) 0.0534(5) Uani 1 1 d . . . . . C9 C 0.0570(2) 0.51508(15) 0.12175(16) 0.0521(5) Uani 1 1 d . . . . . H9 H 0.032421 0.514607 0.070334 0.063 Uiso 1 1 calc R U . . . C27 C 0.3492(2) 0.41985(16) 0.02559(18) 0.0571(6) Uani 1 1 d . . . . . H27 H 0.387904 0.377625 0.065123 0.069 Uiso 1 1 calc R U . . . C20 C 0.1764(2) 0.95465(15) 0.01057(16) 0.0562(6) Uani 1 1 d . . . . . H20 H 0.099484 0.966221 0.027989 0.067 Uiso 1 1 calc R U . . . C39 C 0.3621(2) 0.68105(18) 0.60297(15) 0.0592(6) Uani 1 1 d . . . . . H39 H 0.284161 0.681625 0.605060 0.071 Uiso 1 1 calc R U . . . C57 C 0.6093(2) 0.77879(19) 0.29298(16) 0.0588(6) Uani 1 1 d . . . . . H57 H 0.603263 0.843187 0.259033 0.071 Uiso 1 1 calc R U . . . C50 C 0.3603(2) 0.94769(18) 0.28530(16) 0.0606(6) Uani 1 1 d . . . . . C1 C 0.07560(19) 0.80512(16) -0.10816(15) 0.0508(5) Uani 1 1 d . . . . . C55 C 0.7269(2) 0.6400(2) 0.33142(19) 0.0680(7) Uani 1 1 d . . . . . C30 C 0.0212(2) 0.79496(18) 0.11650(19) 0.0666(7) Uani 1 1 d . . . . . H30A H 0.029729 0.829326 0.158028 0.100 Uiso 1 1 calc R U . . . H30B H -0.020169 0.733640 0.149654 0.100 Uiso 1 1 calc R U . . . H30C H -0.020092 0.833443 0.073825 0.100 Uiso 1 1 calc R U . . . C4 C 0.1527(3) 0.98058(19) -0.23976(18) 0.0725(7) Uani 1 1 d . . . . . H4 H 0.178597 1.039205 -0.284880 0.087 Uiso 1 1 calc R U . . . C32 C 0.0752(2) 0.74682(19) 0.38491(17) 0.0628(6) Uani 1 1 d . . . . . H32 H 0.071588 0.698230 0.358047 0.075 Uiso 1 1 calc R U . . . C18 C 0.3694(3) 1.01731(18) -0.05580(19) 0.0693(7) Uani 1 1 d . . . . . H18 H 0.421898 1.070363 -0.082602 0.083 Uiso 1 1 calc R U . . . C12 C 0.1270(2) 0.51371(18) 0.27481(16) 0.0626(6) Uani 1 1 d . . . . . H12 H 0.150884 0.513881 0.326600 0.075 Uiso 1 1 calc R U . . . C11 C 0.0719(2) 0.43046(18) 0.27460(17) 0.0647(7) Uani 1 1 d . . . . . C10 C 0.0369(2) 0.43281(17) 0.19665(18) 0.0634(6) Uani 1 1 d . . . . . H10 H -0.000707 0.377951 0.194798 0.076 Uiso 1 1 calc R U . . . C59 C 0.3678(3) 0.8159(2) 0.21776(16) 0.0792(9) Uani 1 1 d . . . . . H59A H 0.287593 0.802267 0.225893 0.119 Uiso 1 1 calc R U . . . H59B H 0.408033 0.757316 0.219046 0.119 Uiso 1 1 calc R U . . . H59C H 0.395788 0.864844 0.160343 0.119 Uiso 1 1 calc R U . . . C56 C 0.7134(2) 0.7364(2) 0.28266(19) 0.0699(7) Uani 1 1 d . . . . . H56 H 0.776626 0.773208 0.241882 0.084 Uiso 1 1 calc R U . . . C53 C 0.5249(2) 0.62891(17) 0.40029(18) 0.0630(6) Uani 1 1 d . . . . . H53 H 0.461183 0.590983 0.439031 0.076 Uiso 1 1 calc R U . . . C43 C 0.5525(2) 0.7447(2) 0.53300(18) 0.0665(7) Uani 1 1 d . . . . . H43 H 0.604732 0.788953 0.486726 0.080 Uiso 1 1 calc R U . . . C35 C 0.0893(2) 0.89362(19) 0.45879(19) 0.0682(7) Uani 1 1 d . . . . . H35 H 0.093468 0.944809 0.482411 0.082 Uiso 1 1 calc R U . . . C46 C 0.4040(2) 0.99522(18) 0.33626(18) 0.0635(6) Uani 1 1 d . . . . . C19 C 0.2559(3) 1.03165(17) -0.02968(19) 0.0674(7) Uani 1 1 d . . . . . H19 H 0.231685 1.095084 -0.039355 0.081 Uiso 1 1 calc R U . . . C45 C 0.2634(3) 0.8974(2) 0.55354(18) 0.0710(7) Uani 1 1 d . . . . . H45A H 0.269037 0.966069 0.521434 0.107 Uiso 1 1 calc R U . . . H45B H 0.323071 0.881697 0.586230 0.107 Uiso 1 1 calc R U . . . H45C H 0.190410 0.880656 0.595496 0.107 Uiso 1 1 calc R U . . . C40 C 0.4026(3) 0.6141(2) 0.67118(17) 0.0699(7) Uani 1 1 d . . . . . H40 H 0.350719 0.570048 0.717961 0.084 Uiso 1 1 calc R U . . . C54 C 0.6302(2) 0.5875(2) 0.38989(19) 0.0693(7) Uani 1 1 d . . . . . H54 H 0.636055 0.522744 0.423063 0.083 Uiso 1 1 calc R U . . . C33 C -0.0154(3) 0.8057(2) 0.3935(2) 0.0745(7) Uani 1 1 d . . . . . H33 H -0.081004 0.795637 0.374923 0.089 Uiso 1 1 calc R U . . . C2 C -0.0001(2) 0.8764(2) -0.13622(19) 0.0708(7) Uani 1 1 d . . . . . H2 H -0.077855 0.865055 -0.109632 0.085 Uiso 1 1 calc R U . . . C41 C 0.5159(3) 0.6104(2) 0.67229(19) 0.0761(8) Uani 1 1 d . . . . . C34 C -0.0072(3) 0.8796(2) 0.4300(2) 0.0797(8) Uani 1 1 d . . . . . H34 H -0.067465 0.920569 0.435341 0.096 Uiso 1 1 calc R U . . . C3 C 0.0382(3) 0.9631(2) -0.2025(2) 0.0811(9) Uani 1 1 d . . . . . H3 H -0.013295 1.009541 -0.221795 0.097 Uiso 1 1 calc R U . . . C42 C 0.5907(3) 0.6775(2) 0.6020(2) 0.0775(8) Uani 1 1 d . . . . . H42 H 0.668345 0.677395 0.601261 0.093 Uiso 1 1 calc R U . . . C60 C 0.3815(3) 1.0918(2) 0.3310(2) 0.0826(9) Uani 1 1 d . . . . . H60 H 0.407963 1.120406 0.368495 0.099 Uiso 1 1 calc R U . . . C29 C 0.3211(3) 0.28350(17) -0.0388(2) 0.0824(9) Uani 1 1 d . . . . . H29A H 0.250564 0.258060 -0.043916 0.124 Uiso 1 1 calc R U . . . H29B H 0.341371 0.243415 0.015597 0.124 Uiso 1 1 calc R U . . . H29C H 0.380380 0.283442 -0.090542 0.124 Uiso 1 1 calc R U . . . C58 C 0.8404(3) 0.5935(2) 0.3240(3) 0.0925(10) Uani 1 1 d . . . . . H58A H 0.837804 0.538391 0.377071 0.139 Uiso 1 1 calc R U . . . H58B H 0.899203 0.640165 0.319090 0.139 Uiso 1 1 calc R U . . . H58C H 0.856581 0.572103 0.271030 0.139 Uiso 1 1 calc R U . . . C49 C 0.2945(3) 1.0025(2) 0.2264(2) 0.0856(9) Uani 1 1 d . . . . . H49 H 0.262146 0.973388 0.192076 0.103 Uiso 1 1 calc R U . . . C14 C 0.0494(4) 0.3394(2) 0.3568(2) 0.1070(12) Uani 1 1 d . . . . . H14A H -0.009108 0.298163 0.352093 0.161 Uiso 1 1 calc R U . . . H14B H 0.024780 0.357849 0.411061 0.161 Uiso 1 1 calc R U . . . H14C H 0.118317 0.304722 0.359310 0.161 Uiso 1 1 calc R U . . . C44 C 0.5586(4) 0.5359(3) 0.7464(2) 0.1154(14) Uani 1 1 d . . . . . H44A H 0.571822 0.476539 0.730987 0.173 Uiso 1 1 calc R U . . . H44B H 0.502477 0.523134 0.802654 0.173 Uiso 1 1 calc R U . . . H44C H 0.628737 0.560770 0.752859 0.173 Uiso 1 1 calc R U . . . C48 C 0.2779(3) 1.0995(3) 0.2194(3) 0.1104(14) Uani 1 1 d . . . . . H48 H 0.236421 1.135159 0.178461 0.132 Uiso 1 1 calc R U . . . C47 C 0.3203(3) 1.1452(3) 0.2708(3) 0.1048(12) Uani 1 1 d . . . . . H47 H 0.307918 1.210647 0.264981 0.126 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 S1 0.0398(3) 0.0515(3) 0.0529(3) -0.0194(2) -0.0157(2) 0.0007(2) S2 0.0397(3) 0.0542(3) 0.0625(4) -0.0127(3) -0.0171(2) -0.0024(2) S4 0.0498(3) 0.0585(3) 0.0583(3) -0.0284(3) -0.0032(3) -0.0078(2) S3 0.0676(4) 0.0584(3) 0.0710(4) -0.0250(3) -0.0280(3) -0.0067(3) N1 0.0428(10) 0.0412(8) 0.0491(10) -0.0165(7) -0.0008(8) -0.0013(7) N2 0.0431(9) 0.0421(8) 0.0379(8) -0.0106(7) -0.0073(7) 0.0002(7) N4 0.0617(12) 0.0720(12) 0.0420(10) -0.0170(9) -0.0149(9) -0.0114(10) N3 0.0585(12) 0.0630(11) 0.0472(10) -0.0286(9) -0.0172(9) 0.0088(9) C7 0.0375(10) 0.0394(9) 0.0452(11) -0.0135(8) -0.0075(8) -0.0020(7) C22 0.0373(10) 0.0424(10) 0.0374(10) -0.0136(8) -0.0090(8) -0.0002(8) C23 0.0384(10) 0.0393(9) 0.0423(10) -0.0145(8) -0.0077(8) 0.0002(8) C8 0.0395(11) 0.0430(10) 0.0426(11) -0.0124(8) -0.0044(8) 0.0002(8) C24 0.0495(12) 0.0450(11) 0.0483(11) -0.0150(9) -0.0133(9) 0.0024(9) C16 0.0480(12) 0.0489(11) 0.0440(11) -0.0182(9) -0.0115(9) -0.0058(9) C6 0.0516(12) 0.0431(10) 0.0429(11) -0.0150(8) -0.0164(9) 0.0038(9) C21 0.0480(12) 0.0439(10) 0.0413(10) -0.0166(8) -0.0100(9) -0.0026(8) C28 0.0502(12) 0.0483(11) 0.0522(12) -0.0175(9) -0.0172(10) 0.0056(9) C15 0.0496(13) 0.0590(13) 0.0457(12) -0.0142(10) 0.0005(10) -0.0003(10) C51 0.0497(12) 0.0532(11) 0.0393(11) -0.0182(9) -0.0068(9) -0.0084(9) C36 0.0545(13) 0.0558(12) 0.0399(11) -0.0140(9) -0.0103(9) 0.0040(10) C13 0.0532(13) 0.0554(12) 0.0451(12) -0.0173(9) -0.0064(10) -0.0016(10) C52 0.0484(12) 0.0662(14) 0.0445(11) -0.0263(10) -0.0033(9) -0.0094(10) C37 0.0533(13) 0.0536(12) 0.0420(11) -0.0203(9) -0.0121(9) -0.0014(9) C5 0.0699(16) 0.0497(12) 0.0465(12) -0.0109(10) -0.0145(11) 0.0005(10) C31 0.0490(12) 0.0567(12) 0.0417(11) -0.0149(9) -0.0079(9) -0.0042(9) C38 0.0632(14) 0.0580(12) 0.0431(11) -0.0236(10) -0.0170(10) 0.0084(10) C17 0.0536(14) 0.0615(14) 0.0612(14) -0.0207(11) -0.0146(11) -0.0149(10) C25 0.0567(14) 0.0488(12) 0.0635(14) -0.0246(10) -0.0134(11) -0.0030(10) C26 0.0484(13) 0.0429(11) 0.0687(14) -0.0196(10) -0.0095(11) 0.0012(9) C9 0.0513(13) 0.0498(11) 0.0517(12) -0.0127(10) -0.0080(10) -0.0056(9) C27 0.0543(14) 0.0465(11) 0.0707(15) -0.0145(11) -0.0204(12) 0.0111(10) C20 0.0664(15) 0.0416(11) 0.0637(14) -0.0209(10) -0.0142(12) 0.0023(10) C39 0.0698(16) 0.0672(14) 0.0443(12) -0.0231(11) -0.0133(11) 0.0117(12) C57 0.0551(14) 0.0669(14) 0.0514(13) -0.0182(11) -0.0046(11) -0.0111(11) C50 0.0541(14) 0.0676(15) 0.0497(13) -0.0009(11) -0.0135(11) -0.0105(11) C1 0.0508(13) 0.0513(12) 0.0523(12) -0.0127(10) -0.0207(10) 0.0060(9) C55 0.0554(15) 0.0816(18) 0.0679(16) -0.0345(14) 0.0008(12) -0.0022(13) C30 0.0571(15) 0.0571(13) 0.0750(17) -0.0251(12) 0.0127(12) 0.0017(11) C4 0.099(2) 0.0541(14) 0.0568(15) -0.0028(11) -0.0221(15) 0.0103(14) C32 0.0612(15) 0.0734(16) 0.0549(14) -0.0196(12) -0.0146(12) -0.0046(12) C18 0.081(2) 0.0521(13) 0.0730(17) -0.0146(12) -0.0187(14) -0.0231(12) C12 0.0653(16) 0.0696(15) 0.0445(12) -0.0073(11) -0.0101(11) 0.0032(12) C11 0.0628(16) 0.0582(14) 0.0556(14) -0.0005(11) -0.0017(12) -0.0003(11) C10 0.0644(16) 0.0490(12) 0.0666(16) -0.0072(11) -0.0076(12) -0.0126(11) C59 0.0764(19) 0.123(2) 0.0403(13) -0.0287(14) -0.0105(12) -0.0268(17) C56 0.0517(15) 0.0851(18) 0.0633(16) -0.0201(14) 0.0037(12) -0.0126(13) C53 0.0561(15) 0.0585(14) 0.0670(15) -0.0226(12) 0.0062(12) -0.0070(11) C43 0.0645(16) 0.0805(17) 0.0612(15) -0.0264(13) -0.0220(12) 0.0075(13) C35 0.0780(18) 0.0673(15) 0.0702(16) -0.0277(13) -0.0310(14) 0.0181(13) C46 0.0624(15) 0.0545(13) 0.0664(15) -0.0064(11) -0.0165(12) -0.0075(11) C19 0.0816(19) 0.0440(12) 0.0799(18) -0.0202(12) -0.0228(15) -0.0046(12) C45 0.0835(19) 0.0841(17) 0.0660(16) -0.0470(14) -0.0266(14) 0.0214(15) C40 0.091(2) 0.0727(16) 0.0440(13) -0.0176(12) -0.0126(13) 0.0187(14) C54 0.0630(16) 0.0654(15) 0.0737(17) -0.0271(13) 0.0043(13) 0.0015(12) C33 0.0699(18) 0.0849(18) 0.0766(18) -0.0240(15) -0.0341(15) 0.0072(14) C2 0.0626(16) 0.0757(17) 0.0726(17) -0.0147(14) -0.0254(14) 0.0185(13) C41 0.098(2) 0.0854(19) 0.0548(15) -0.0293(14) -0.0305(15) 0.0362(17) C34 0.0735(19) 0.089(2) 0.085(2) -0.0284(16) -0.0350(16) 0.0278(15) C3 0.091(2) 0.0685(17) 0.0794(19) -0.0076(14) -0.0333(17) 0.0283(15) C42 0.0757(19) 0.100(2) 0.0728(18) -0.0387(17) -0.0346(16) 0.0271(16) C60 0.077(2) 0.0610(16) 0.100(2) -0.0120(15) -0.0164(17) -0.0039(14) C29 0.088(2) 0.0452(13) 0.123(3) -0.0345(15) -0.0323(19) 0.0090(13) C58 0.0593(18) 0.102(2) 0.109(3) -0.037(2) 0.0004(17) 0.0073(16) C49 0.0720(19) 0.098(2) 0.0714(19) 0.0075(16) -0.0296(15) -0.0165(16) C14 0.122(3) 0.082(2) 0.081(2) 0.0184(17) -0.011(2) -0.014(2) C44 0.135(3) 0.131(3) 0.079(2) -0.018(2) -0.048(2) 0.058(3) C48 0.084(2) 0.098(3) 0.115(3) 0.026(2) -0.035(2) 0.004(2) C47 0.085(2) 0.069(2) 0.137(3) 0.003(2) -0.027(2) 0.0051(17) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C16 S1 C22 93.56(9) . . ? C1 S2 C7 94.89(10) . . ? C31 S4 C51 95.36(10) . . ? C46 S3 C37 94.60(11) . . ? C21 N1 C30 117.10(17) . . ? C21 N1 C7 123.10(16) . . ? C30 N1 C7 115.25(17) . . ? C6 N2 C22 124.39(16) . . ? C6 N2 C15 117.10(17) . . ? C22 N2 C15 115.29(16) . . ? C50 N4 C59 117.6(2) . . ? C50 N4 C51 124.85(18) . . ? C59 N4 C51 115.6(2) . . ? C36 N3 C37 125.71(17) . . ? C36 N3 C45 117.76(19) . . ? C37 N3 C45 115.50(19) . . ? N1 C7 C8 109.68(16) . . ? N1 C7 C22 112.78(15) . . ? C8 C7 C22 111.22(15) . . ? N1 C7 S2 109.35(13) . . ? C8 C7 S2 107.08(13) . . ? C22 C7 S2 106.51(13) . . ? N2 C22 C23 109.53(15) . . ? N2 C22 C7 113.30(15) . . ? C23 C22 C7 111.55(15) . . ? N2 C22 S1 108.44(13) . . ? C23 C22 S1 107.91(13) . . ? C7 C22 S1 105.87(13) . . ? C28 C23 C24 117.96(18) . . ? C28 C23 C22 123.09(17) . . ? C24 C23 C22 118.95(17) . . ? C9 C8 C13 117.43(19) . . ? C9 C8 C7 122.61(19) . . ? C13 C8 C7 119.95(18) . . ? C25 C24 C23 120.3(2) . . ? C17 C16 C21 120.3(2) . . ? C17 C16 S1 122.08(18) . . ? C21 C16 S1 117.65(15) . . ? N2 C6 C1 119.77(18) . . ? N2 C6 C5 121.9(2) . . ? C1 C6 C5 118.3(2) . . ? C16 C21 C20 118.61(19) . . ? C16 C21 N1 119.49(17) . . ? C20 C21 N1 121.8(2) . . ? C23 C28 C27 121.1(2) . . ? N4 C51 C52 111.20(17) . . ? N4 C51 C37 112.07(17) . . ? C52 C51 C37 111.29(17) . . ? N4 C51 S4 109.77(15) . . ? C52 C51 S4 106.58(14) . . ? C37 C51 S4 105.62(14) . . ? C35 C36 N3 122.1(2) . . ? C35 C36 C31 116.9(2) . . ? N3 C36 C31 120.9(2) . . ? C12 C13 C8 120.5(2) . . ? C53 C52 C57 117.6(2) . . ? C53 C52 C51 122.2(2) . . ? C57 C52 C51 120.1(2) . . ? N3 C37 C38 110.41(17) . . ? N3 C37 C51 112.35(17) . . ? C38 C37 C51 111.92(17) . . ? N3 C37 S3 109.25(14) . . ? C38 C37 S3 106.97(15) . . ? C51 C37 S3 105.65(14) . . ? C4 C5 C6 120.0(2) . . ? C32 C31 C36 120.6(2) . . ? C32 C31 S4 120.80(18) . . ? C36 C31 S4 118.61(17) . . ? C39 C38 C43 117.3(2) . . ? C39 C38 C37 119.8(2) . . ? C43 C38 C37 122.9(2) . . ? C18 C17 C16 120.3(2) . . ? C26 C25 C24 121.9(2) . . ? C25 C26 C27 117.6(2) . . ? C25 C26 C29 120.3(2) . . ? C27 C26 C29 122.1(2) . . ? C10 C9 C8 121.5(2) . . ? C26 C27 C28 121.2(2) . . ? C19 C20 C21 119.8(2) . . ? C38 C39 C40 120.5(3) . . ? C56 C57 C52 120.5(2) . . ? C46 C50 N4 120.7(2) . . ? C46 C50 C49 117.0(3) . . ? N4 C50 C49 122.3(3) . . ? C2 C1 C6 119.9(2) . . ? C2 C1 S2 121.3(2) . . ? C6 C1 S2 118.79(16) . . ? C54 C55 C56 117.0(3) . . ? C54 C55 C58 120.0(3) . . ? C56 C55 C58 123.0(3) . . ? C3 C4 C5 121.4(2) . . ? C33 C32 C31 121.4(2) . . ? C19 C18 C17 119.3(2) . . ? C11 C12 C13 121.8(2) . . ? C10 C11 C12 117.7(2) . . ? C10 C11 C14 120.7(3) . . ? C12 C11 C14 121.6(3) . . ? C9 C10 C11 121.1(2) . . ? C57 C56 C55 122.0(2) . . ? C54 C53 C52 121.2(2) . . ? C42 C43 C38 121.1(3) . . ? C34 C35 C36 121.6(3) . . ? C60 C46 C50 121.7(3) . . ? C60 C46 S3 119.6(2) . . ? C50 C46 S3 118.65(19) . . ? C18 C19 C20 121.6(2) . . ? C41 C40 C39 122.4(3) . . ? C55 C54 C53 121.6(3) . . ? C34 C33 C32 118.8(3) . . ? C3 C2 C1 121.0(3) . . ? C40 C41 C42 117.3(3) . . ? C40 C41 C44 121.7(3) . . ? C42 C41 C44 121.1(3) . . ? C33 C34 C35 120.7(3) . . ? C4 C3 C2 119.3(3) . . ? C41 C42 C43 121.4(3) . . ? C47 C60 C46 120.4(3) . . ? C48 C49 C50 120.1(3) . . ? C47 C48 C49 122.4(3) . . ? C48 C47 C60 118.3(3) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag S1 C16 1.757(2) . ? S1 C22 1.877(2) . ? S2 C1 1.752(2) . ? S2 C7 1.870(2) . ? S4 C31 1.751(2) . ? S4 C51 1.878(2) . ? S3 C46 1.745(3) . ? S3 C37 1.869(2) . ? N1 C21 1.406(2) . ? N1 C30 1.456(3) . ? N1 C7 1.468(2) . ? N2 C6 1.395(3) . ? N2 C22 1.463(2) . ? N2 C15 1.457(3) . ? N4 C50 1.401(3) . ? N4 C59 1.451(3) . ? N4 C51 1.456(3) . ? N3 C36 1.397(3) . ? N3 C37 1.457(3) . ? N3 C45 1.468(3) . ? C7 C8 1.530(3) . ? C7 C22 1.574(3) . ? C22 C23 1.532(3) . ? C23 C28 1.380(3) . ? C23 C24 1.392(3) . ? C8 C9 1.389(3) . ? C8 C13 1.397(3) . ? C24 C25 1.387(3) . ? C16 C17 1.388(3) . ? C16 C21 1.392(3) . ? C6 C1 1.398(3) . ? C6 C5 1.405(3) . ? C21 C20 1.403(3) . ? C28 C27 1.390(3) . ? C51 C52 1.526(3) . ? C51 C37 1.578(3) . ? C36 C35 1.392(3) . ? C36 C31 1.405(3) . ? C13 C12 1.382(3) . ? C52 C53 1.384(3) . ? C52 C57 1.398(3) . ? C37 C38 1.527(3) . ? C5 C4 1.385(4) . ? C31 C32 1.378(3) . ? C38 C39 1.388(3) . ? C38 C43 1.393(4) . ? C17 C18 1.385(4) . ? C25 C26 1.376(3) . ? C26 C27 1.382(3) . ? C26 C29 1.512(3) . ? C9 C10 1.378(3) . ? C20 C19 1.375(3) . ? C39 C40 1.385(3) . ? C57 C56 1.380(4) . ? C50 C46 1.394(4) . ? C50 C49 1.406(4) . ? C1 C2 1.394(3) . ? C55 C54 1.382(4) . ? C55 C56 1.393(4) . ? C55 C58 1.504(4) . ? C4 C3 1.366(4) . ? C32 C33 1.373(4) . ? C18 C19 1.365(4) . ? C12 C11 1.383(4) . ? C11 C10 1.384(4) . ? C11 C14 1.519(3) . ? C53 C54 1.385(4) . ? C43 C42 1.380(4) . ? C35 C34 1.378(4) . ? C46 C60 1.392(4) . ? C40 C41 1.365(4) . ? C33 C34 1.372(4) . ? C2 C3 1.372(4) . ? C41 C42 1.385(4) . ? C41 C44 1.508(4) . ? C60 C47 1.373(5) . ? C49 C48 1.380(5) . ? C48 C47 1.374(6) . ?