#------------------------------------------------------------------------------ #$Date: 2024-05-05 06:58:46 +0300 (Sun, 05 May 2024) $ #$Revision: 291684 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/98/7159886.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7159886 loop_ _publ_author_name 'Gao, Siyu' 'Sun, Xiang' 'Peng, Sijie' 'Zha, Zhenggen' 'Sun, Qi' 'Wang, Zhiyong' _publ_section_title ; A copper-catalyzed asymmetric Friedel-Crafts hydroxyalkylation of pyrazole-4,5-diones with 5-aminoisoxazoles. ; _journal_issue 17 _journal_name_full 'Organic & biomolecular chemistry' _journal_page_first 3391 _journal_page_last 3395 _journal_paper_doi 10.1039/d4ob00322e _journal_volume 22 _journal_year 2024 _chemical_absolute_configuration ad _chemical_formula_moiety 'C23 H24 N4 O3' _chemical_formula_sum 'C23 H24 N4 O3' _chemical_formula_weight 404.46 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _atom_sites_solution_hydrogens geom _audit_creation_date 2023-09-21 _audit_creation_method ; Olex2 1.3 (compiled 2020.11.12 svn.r5f609507 for OlexSys, GUI svn.r6408) ; _audit_update_record ; 2024-02-28 deposited with the CCDC. 2024-04-08 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 8.99824(7) _cell_length_b 13.13119(9) _cell_length_c 17.79770(13) _cell_measurement_reflns_used 13066 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 72.9810 _cell_measurement_theta_min 4.1590 _cell_volume 2102.93(3) _computing_cell_refinement 'CrysAlisPro 1.171.41.110a (Rigaku OD, 2021)' _computing_data_collection 'CrysAlisPro 1.171.41.110a (Rigaku OD, 2021)' _computing_data_reduction 'CrysAlisPro 1.171.41.110a (Rigaku OD, 2021)' _computing_molecular_graphics 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2013/4 (Sheldrick, 2015)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'CCD plate' _diffrn_detector_area_resol_mean 5.2169 _diffrn_detector_type AtlasS2 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -122.00 -1.00 1.00 2.00 -- -41.76 -19.00 30.00 121 2 \w -87.00 -6.00 1.00 2.00 -- -41.76 125.00-180.00 81 3 \w -116.00 -17.00 1.00 2.00 -- -41.76 -38.00 -60.00 99 4 \w 80.00 178.00 1.00 4.00 -- 106.05 45.00 0.00 98 5 \w 103.00 178.00 1.00 4.00 -- 106.05 77.00 60.00 75 6 \w 30.00 139.00 1.00 4.00 -- 106.05 -77.00-150.00 109 7 \w 97.00 178.00 1.00 4.00 -- 106.05 125.00 -60.00 81 8 \w 103.00 178.00 1.00 4.00 -- 106.05 77.00-160.00 75 9 \w 103.00 178.00 1.00 4.00 -- 106.05 77.00 30.00 75 10 \w 103.00 178.00 1.00 4.00 -- 106.05 77.00 -90.00 75 11 \w -116.00 -17.00 1.00 2.00 -- -41.76 -38.00-180.00 99 12 \w 14.00 115.00 1.00 2.00 -- 41.76 57.00 150.00 101 13 \w 6.00 83.00 1.00 2.00 -- 41.76 -99.00 60.00 77 14 \w 80.00 178.00 1.00 4.00 -- 106.05 45.00 150.00 98 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'SuperNova, Dual, Cu at home/near, AtlasS2' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.1029699000 _diffrn_orient_matrix_UB_12 0.0714421000 _diffrn_orient_matrix_UB_13 0.0447856000 _diffrn_orient_matrix_UB_21 0.0184975000 _diffrn_orient_matrix_UB_22 -0.0680329000 _diffrn_orient_matrix_UB_23 0.0698888000 _diffrn_orient_matrix_UB_31 0.1354975000 _diffrn_orient_matrix_UB_32 0.0635666000 _diffrn_orient_matrix_UB_33 0.0244816000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0284 _diffrn_reflns_av_unetI/netI 0.0172 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -16 _diffrn_reflns_limit_l_max 22 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 15262 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.983 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 72.906 _diffrn_reflns_theta_min 4.184 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'SuperNova (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.701 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.61887 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.41.110a (Rigaku Oxford Diffraction, 2021) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_density_diffrn 1.277 _exptl_crystal_description block _exptl_crystal_F_000 856 _exptl_crystal_size_max 0.22 _exptl_crystal_size_mid 0.19 _exptl_crystal_size_min 0.18 _refine_diff_density_max 0.321 _refine_diff_density_min -0.228 _refine_diff_density_rms 0.059 _refine_ls_abs_structure_details ; Flack x determined using 1699 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons and Flack (2004), Acta Cryst. A60, s61). ; _refine_ls_abs_structure_Flack 0.04(6) _refine_ls_extinction_coef 0.0338(19) _refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc^2^\l^3^/sin(2\q)]^-1/4^ _refine_ls_extinction_method SHELXL _refine_ls_goodness_of_fit_ref 1.079 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 276 _refine_ls_number_reflns 4132 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.079 _refine_ls_R_factor_all 0.0439 _refine_ls_R_factor_gt 0.0434 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0688P)^2^+0.3457P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1143 _refine_ls_wR_factor_ref 0.1151 _reflns_Friedel_coverage 0.732 _reflns_Friedel_fraction_full 1.000 _reflns_Friedel_fraction_max 0.968 _reflns_number_gt 4059 _reflns_number_total 4132 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ob00322e2.cif _cod_data_source_block scd-gsy2023-0706_auto _cod_depositor_comments 'Adding full bibliography for 7159886.cif.' _cod_database_code 7159886 _shelxl_version_number 2013-4 _chemical_oxdiff_formula C20H20N2O2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.884 _shelx_estimated_absorpt_t_min 0.861 _reflns_odcompleteness_completeness 99.91 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 66.97 _olex2_refinement_description ; 1.a Ternary CH refined with riding coordinates: C13(H13) 1.b Secondary CH2 refined with riding coordinates: C16(H16A,H16B) 1.c Aromatic/amide H refined with riding coordinates: N4(H4), C23(H23), C19(H19), C12(H12), C20(H20), C10(H10), C11(H11), C22(H22), C9(H9), C8(H8), C21(H21) 1.d Idealised Me refined as rotating group: C15(H15A,H15B,H15C), C14(H14A,H14B,H14C), C17(H17A,H17B,H17C) 1.e Idealised tetrahedral OH refined as rotating group: O1(H1) ; _shelx_res_file ; TITL scd-gsy2023-0706_auto_a.res in P2(1)2(1)2(1) REM Old TITL SCD-GSY2023-0706_auto in P212121 #19 REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.162, Rweak 0.058, Alpha 0.006, Orientation as input REM Flack x = 0.267 ( 0.090 ) from Parsons' quotients REM Formula found by SHELXT: N1 N3 O3 CELL 1.54184 8.998237 13.131191 17.797704 90 90 90 ZERR 4 0.000067 0.00009 0.000126 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 92 96 16 12 EQIV $1 1-X,-0.5+Y,0.5-Z L.S. 4 0 0 PLAN 9 SIZE 0.18 0.19 0.22 CONF HTAB O1 N3_$1 BOND $H LIST 6 MORE -1 fmap 2 53 acta REM REM REM WGHT 0.068800 0.345700 EXTI 0.033783 FVAR 11.06802 O3 4 0.576964 0.729016 0.160037 11.00000 0.08562 0.03426 = 0.04830 0.01018 -0.00863 -0.00616 O1 4 0.412910 0.451205 0.226565 11.00000 0.07401 0.04079 = 0.05832 0.01242 -0.02812 -0.01712 AFIX 147 H1 2 0.383481 0.398107 0.245712 11.00000 -1.50000 AFIX 0 O2 4 0.309874 0.571047 0.358692 11.00000 0.04996 0.08565 = 0.07634 0.02605 0.00932 0.02458 N2 3 0.633918 0.428719 0.378363 11.00000 0.04656 0.03202 = 0.03805 0.00109 -0.00031 0.00597 N1 3 0.506950 0.479119 0.407076 11.00000 0.04412 0.03672 = 0.04022 0.00355 0.00149 0.00631 N3 3 0.671835 0.752034 0.222275 11.00000 0.06602 0.03265 = 0.05048 0.00197 -0.00180 -0.00431 C4 1 0.556933 0.600483 0.241103 11.00000 0.05120 0.03038 = 0.03909 0.00254 -0.00341 0.00243 C18 1 0.740289 0.672877 0.339987 11.00000 0.04446 0.02727 = 0.04353 -0.00331 -0.00069 -0.00319 N4 3 0.412936 0.606331 0.121690 11.00000 0.12126 0.04915 = 0.06313 0.01732 -0.04313 -0.01935 AFIX 43 H4 2 0.378785 0.545614 0.127170 11.00000 -1.20000 AFIX 0 C13 1 0.761888 0.400148 0.259458 11.00000 0.05967 0.04043 = 0.03973 -0.00006 0.00690 0.00117 AFIX 13 H13 2 0.804629 0.459513 0.234029 11.00000 -1.20000 AFIX 0 C23 1 0.890979 0.652375 0.340223 11.00000 0.04401 0.04845 = 0.05730 -0.00894 0.00596 -0.00139 AFIX 43 H23 2 0.941366 0.643867 0.295033 11.00000 -1.20000 AFIX 0 C6 1 0.655992 0.674536 0.268031 11.00000 0.04617 0.02844 = 0.04210 -0.00149 0.00326 0.00267 C19 1 0.667999 0.688109 0.407783 11.00000 0.04723 0.04523 = 0.05028 -0.00873 0.00323 -0.00229 AFIX 43 H19 2 0.567251 0.703902 0.408136 11.00000 -1.20000 AFIX 0 C5 1 0.509115 0.639475 0.173163 11.00000 0.07038 0.03244 = 0.04563 0.00514 -0.00746 -0.00249 C3 1 0.507601 0.502700 0.277624 11.00000 0.04779 0.03306 = 0.04112 0.00456 -0.00846 -0.00386 C7 1 0.488055 0.483918 0.485995 11.00000 0.04532 0.03432 = 0.04027 -0.00249 0.00379 -0.00448 C12 1 0.570937 0.420337 0.531425 11.00000 0.05762 0.05176 = 0.03985 -0.00690 -0.00243 0.00915 AFIX 43 H12 2 0.640352 0.376240 0.510442 11.00000 -1.20000 AFIX 0 C2 1 0.424467 0.524663 0.351884 11.00000 0.04209 0.04143 = 0.05114 0.01226 -0.00155 0.00157 C20 1 0.744076 0.680061 0.474668 11.00000 0.06806 0.06014 = 0.04350 -0.00988 0.00088 -0.01123 AFIX 43 H20 2 0.694626 0.689939 0.519970 11.00000 -1.20000 AFIX 0 C10 1 0.450546 0.490032 0.640771 11.00000 0.06837 0.07634 = 0.04529 -0.01744 0.00404 -0.00389 AFIX 43 H10 2 0.435852 0.490835 0.692491 11.00000 -1.20000 AFIX 0 C11 1 0.549654 0.422795 0.609210 11.00000 0.07594 0.07860 = 0.03854 -0.00649 -0.00777 0.01357 AFIX 43 H11 2 0.602976 0.378583 0.639863 11.00000 -1.20000 AFIX 0 C22 1 0.966992 0.644489 0.407553 11.00000 0.04499 0.06715 = 0.07847 -0.01168 -0.00976 0.00100 AFIX 43 H22 2 1.068283 0.630408 0.407553 11.00000 -1.20000 AFIX 0 C9 1 0.373643 0.555804 0.595464 11.00000 0.06053 0.05118 = 0.06155 -0.01496 0.01841 -0.00229 AFIX 43 H9 2 0.309740 0.603243 0.616949 11.00000 -1.20000 AFIX 0 C8 1 0.389693 0.552693 0.517931 11.00000 0.05611 0.03982 = 0.05896 0.00206 0.01244 0.00482 AFIX 43 H8 2 0.334836 0.596446 0.487613 11.00000 -1.20000 AFIX 0 C21 1 0.893089 0.657421 0.474354 11.00000 0.06708 0.06105 = 0.05946 -0.00468 -0.02024 -0.00916 AFIX 43 H21 2 0.944091 0.650831 0.519542 11.00000 -1.20000 AFIX 0 C15 1 0.884517 0.354142 0.304403 11.00000 0.09008 0.11424 = 0.06291 0.00886 0.01317 0.05745 AFIX 137 H15A 2 0.910887 0.399291 0.344678 11.00000 -1.50000 H15B 2 0.969390 0.343349 0.272705 11.00000 -1.50000 H15C 2 0.852243 0.290159 0.324768 11.00000 -1.50000 AFIX 0 C16 1 0.360630 0.664106 0.056911 11.00000 0.10476 0.05523 = 0.05147 0.00919 -0.01769 -0.00127 AFIX 23 H16A 2 0.255211 0.651698 0.050133 11.00000 -1.20000 H16B 2 0.373833 0.736214 0.066682 11.00000 -1.20000 AFIX 0 C14 1 0.709572 0.328842 0.197936 11.00000 0.09688 0.13164 = 0.08015 -0.06285 0.02028 -0.01155 AFIX 137 H14A 2 0.673890 0.266757 0.219976 11.00000 -1.50000 H14B 2 0.790852 0.313970 0.164764 11.00000 -1.50000 H14C 2 0.630840 0.360635 0.170102 11.00000 -1.50000 AFIX 0 C17 1 0.437119 0.637987 -0.010626 11.00000 0.25845 0.09762 = 0.08069 0.02008 0.05985 0.03438 AFIX 137 H17A 2 0.393612 0.673922 -0.052131 11.00000 -1.50000 H17B 2 0.429258 0.565985 -0.019088 11.00000 -1.50000 H17C 2 0.539947 0.656481 -0.006095 11.00000 -1.50000 AFIX 0 C1 1 0.636813 0.439625 0.306908 11.00000 0.04969 0.02710 = 0.03695 0.00144 -0.00295 -0.00192 HKLF 4 REM scd-gsy2023-0706_auto_a.res in P2(1)2(1)2(1) REM R1 = 0.0434 for 4059 Fo > 4sig(Fo) and 0.0439 for all 4132 data REM 276 parameters refined using 0 restraints END WGHT 0.0688 0.3457 REM Highest difference peak 0.321, deepest hole -0.228, 1-sigma level 0.059 Q1 1 0.4842 0.6614 0.0351 11.00000 0.05 0.32 Q2 1 0.5054 0.6192 0.1032 11.00000 0.05 0.26 Q3 1 0.6598 0.8255 0.2283 11.00000 0.05 0.20 Q4 1 0.3321 0.6596 -0.0049 11.00000 0.05 0.20 Q5 1 0.7961 0.4920 0.2643 11.00000 0.05 0.20 Q6 1 0.5821 0.5443 0.2602 11.00000 0.05 0.19 Q7 1 0.6537 0.5993 0.2426 11.00000 0.05 0.18 Q8 1 0.7631 0.4896 0.3659 11.00000 0.05 0.17 Q9 1 0.5843 0.6576 0.1551 11.00000 0.05 0.17 ; _shelx_res_checksum 36984 _shelx_hkl_file ; 0 0 -2 280662. 2601.04 1 0 0 2 284508. 2558.44 11 0 0 -3 454.914 50.2823 1 0 0 3 184.333 27.0017 11 0 0 -4 6675.09 217.050 1 0 0 4 6958.62 188.512 11 0 0 -5 534.887 70.3469 1 0 0 5 50.7980 20.9832 11 0 0 -6 131381. 1671.10 1 0 0 6 146778. 1579.71 11 0 0 -7 72.3148 44.6823 1 0 0 7 404.454 65.8292 11 0 0 -8 584373. 6088.07 1 0 0 8 652517. 5900.00 11 0 0 -9 48.0346 55.8543 1 0 0 9 95.2195 41.7237 11 0 0 -10 1667.35 182.693 1 0 0 10 1560.12 143.283 11 0 0 -11 136.800 74.4714 1 0 0 11 5.62988 47.9290 13 0 0 11 105.130 44.0247 11 0 0 -12 19534.2 737.163 1 0 0 12 18532.3 682.474 13 0 0 -13 54.7484 72.4045 1 0 0 13 179.607 70.4835 13 0 0 13-36.6922 63.8935 8 0 0 -14 4927.32 408.460 1 0 0 14 4991.66 379.979 13 0 0 14 5075.42 298.324 8 0 0 -15 196.385 93.1876 1 0 0 15 207.640 82.3483 8 0 0 16 62546.2 1198.81 8 0 0 17 204.688 105.639 8 0 0 18 439.054 101.744 8 0 0 -19 65.4790 61.9550 9 0 0 19 48.9790 54.6248 8 0 0 20 630.148 95.0599 8 0 0 -20 631.224 94.9458 9 0 0 21 7.16553 38.3183 8 0 0 -21-0.93358 39.3165 9 0 0 22 592.354 68.0170 8 0 1 -1 2197.82 72.7907 1 0 -1 1 2211.95 75.5208 3 0 1 -1 2043.29 62.5630 12 0 -1 2 186850. 1730.46 3 0 1 2 189631. 1707.29 11 0 1 -3 52925.8 698.271 1 0 -1 -3 53926.4 693.159 1 0 1 3 53458.4 637.991 11 0 -1 -4 81291.7 998.218 1 0 1 4 80313.4 912.643 11 0 -1 -5 48574.1 753.847 1 0 1 5 48553.5 666.379 11 0 -1 -6 1195.39 113.301 1 0 1 -6 1065.80 108.566 1 0 -1 6 1209.26 95.5885 11 0 -1 7 315.966 56.6232 11 0 1 7 391.525 57.8122 11 0 1 -8 974.591 129.776 1 0 -1 -8 1069.01 133.235 1 0 1 8 1197.37 103.313 11 0 -1 8 1176.54 109.088 11 0 -1 -9 1922.08 184.496 1 0 1 -9 1953.24 182.634 1 0 1 9 2066.28 152.056 11 0 -1 9 2282.51 161.657 11 0 1 -10 3898.31 280.096 1 0 -1 -10 3708.82 279.464 1 0 -1 10 4395.54 237.452 11 0 1 10 4183.26 232.781 11 0 -1 10 3582.57 252.059 13 0 1 -11 15173.3 596.478 1 0 -1 -11 16539.6 634.749 1 0 -1 11 15508.8 479.102 11 0 -1 11 14499.8 548.290 13 0 1 11 14894.3 607.356 13 0 -1 -12 290.970 97.2690 1 0 1 -12 284.237 103.968 1 0 -1 12 320.621 94.7868 13 0 1 12 237.000 76.5016 13 0 -1 -13 7557.69 485.247 1 0 1 -13 7818.14 486.797 1 0 1 13 6698.81 443.739 13 0 -1 13 7271.66 424.469 13 0 -1 13 7346.14 344.319 8 0 1 13 6839.04 334.925 8 0 1 -14 15892.6 737.345 1 0 -1 -14 16082.0 753.597 1 0 1 14 14596.8 679.028 13 0 1 14 14278.9 511.019 8 0 -1 14 14733.1 515.739 8 0 1 -15 10651.5 625.188 1 0 -1 -15 10582.5 632.376 1 0 1 15 9092.21 546.118 13 0 1 15 9309.73 418.853 8 0 -1 15 9562.90 422.063 8 0 -1 16 25272.5 717.417 8 0 1 16 23597.0 689.702 8 0 -1 17 38672.7 899.421 8 0 1 17 35618.2 862.777 8 0 1 -18 222.958 78.2142 9 0 1 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411347. 4362.41 1 0 -2 -8 408405. 4379.31 1 0 -2 8 414247. 4123.97 11 0 2 8 423575. 4137.82 11 0 -2 -9 234762. 2878.96 1 0 2 9 233505. 2597.78 11 0 -2 9 232619. 2603.50 11 0 -2 9 237352. 2685.17 13 0 2 -10 33772.4 877.962 1 0 -2 -10 36614.3 937.190 1 0 2 10 35512.0 752.355 11 0 -2 10 34476.5 790.800 13 0 -2 10 35863.9 758.817 11 0 2 -11 69832.2 1405.04 1 0 -2 -11 74929.9 1499.47 1 0 -2 11 73894.9 1310.92 13 0 -2 11 74964.5 1236.01 11 0 2 11 72265.1 1488.54 13 0 2 -12 19365.0 726.985 1 0 -2 -12 20337.8 779.480 1 0 -2 12 20504.2 666.167 13 0 -2 12 20482.9 591.386 11 0 2 12 20622.4 523.373 14 0 2 12 18640.2 737.680 13 0 -2 -13 13995.2 676.823 1 0 2 -13 14147.5 650.326 1 0 2 13 14192.7 444.378 14 0 2 13 13034.0 640.439 13 0 -2 13 13432.1 471.649 8 0 2 13 13270.4 475.441 8 0 2 -14 1673.68 247.853 1 0 -2 -14 1378.85 220.834 1 0 2 14 1504.22 228.736 13 0 2 14 1532.34 170.028 8 0 -2 14 1525.83 163.192 8 0 2 -15 4242.05 390.394 1 0 -2 -15 4825.42 431.361 1 0 2 15 3705.38 357.197 13 0 -2 15 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20187.6 587.593 8 1 -4 -14 9228.44 622.067 1 1 -4 -14 8339.56 321.914 4 -1 4 -14 8552.61 548.646 1 1 4 14 7778.62 542.026 13 -1 -4 14 8704.36 387.153 8 1 4 14 8517.63 398.877 8 -1 4 -14 9399.88 426.455 9 -1 -4 15 86616.8 1427.85 8 1 4 15 86091.8 1456.76 8 -1 4 -15 89946.9 1497.66 9 -1 -4 16 2173.09 199.507 8 1 4 16 1997.61 190.666 8 -1 4 -16 2391.35 216.633 9 -1 -4 17 11839.1 442.847 8 -1 4 -17 11110.1 439.269 9 1 4 17 11109.9 431.853 8 1 4 18 3470.21 222.744 8 -1 -4 18 3330.24 222.859 8 -1 4 -18 3231.60 218.708 9 -1 4 -19 3840.32 233.187 5 -1 -4 19 3641.80 212.386 8 -1 4 -19 3712.59 209.008 9 1 4 19 3740.40 209.549 8 -1 4 -20 1377.49 126.768 5 1 4 20 1206.10 105.205 8 -1 -4 20 1205.77 108.106 8 -1 4 -21 1135.85 96.9440 5 1 -4 -21 1158.32 101.985 9 1 5 -20 528.445 71.2864 5 1 5 -20 549.346 78.0507 9 1 5 -19 2298.91 167.306 5 1 -5 19 2251.56 152.537 8 -1 5 19 2223.78 141.798 8 1 5 -19 2088.57 166.526 9 1 5 -18 2010.19 175.142 5 1 5 -18 1991.80 182.793 9 1 -5 18 1843.49 153.498 8 -1 5 18 1819.15 145.237 8 1 5 -17 2243.40 199.671 5 1 -5 17 2224.69 184.048 8 1 5 -17 1955.20 199.291 9 -1 5 17 2312.17 179.926 8 1 5 -16 21471.2 655.734 5 -1 5 16 22889.1 596.627 14 1 -5 16 21841.8 621.054 8 -1 5 16 21120.5 591.702 8 1 5 -16 22487.2 695.573 9 1 5 -15 2782.29 237.879 5 -1 5 15 2871.46 208.965 14 1 -5 15 2814.77 222.025 8 1 5 -15 2775.89 252.017 9 -1 5 15 2703.56 212.015 8 1 5 -14 1879.96 201.643 5 -1 5 14 1762.65 166.755 14 -1 5 14 1813.32 176.717 8 1 5 -14 1928.03 208.216 9 1 -5 14 2016.63 193.198 8 1 5 -13 38600.9 871.751 4 1 5 -13 38115.5 1118.88 1 1 5 -13 35796.6 1138.74 2 -1 5 13 39302.0 1236.00 13 -1 5 13 41987.7 848.159 14 1 5 -13 39381.3 962.774 9 -1 5 13 38908.6 849.185 8 1 -5 13 41369.1 885.935 8 1 5 -12 26156.0 697.700 4 1 5 -12 26545.9 874.421 1 1 5 -12 24273.0 897.482 2 -1 5 12 27492.4 998.754 13 -1 5 12 29737.9 693.007 14 1 -5 12 28207.1 701.159 8 1 5 -12 26712.1 760.559 9 1 5 -11 3733.93 246.392 4 1 5 -11 3603.30 295.104 1 1 5 -11 3465.45 305.115 2 1 5 -11 3852.75 269.743 9 1 5 -10 6685.20 384.504 1 1 5 -10 6034.45 388.602 2 -1 5 10 6452.81 392.100 11 1 5 -9 115445. 1785.43 1 -1 -5 -9 117204. 1808.36 1 -1 5 9 112295. 1835.18 11 1 5 -8 23840.2 729.199 2 1 5 -8 25251.4 689.504 1 -1 -5 -8 24694.4 679.496 1 1 -5 8 26494.2 693.380 3 -1 5 8 23745.6 719.925 11 1 -5 7 11244.3 419.370 3 1 5 -7 10971.3 461.447 2 -1 -5 -7 11650.3 420.713 1 1 5 -7 11897.4 432.925 1 -1 5 7 10873.2 459.429 11 -1 -5 -6 32855.5 693.242 1 1 5 -6 32594.6 776.938 2 1 5 -6 34335.2 717.904 1 1 -5 6 33704.9 738.271 3 -1 5 6 33497.9 809.941 11 1 -5 5 140887. 1813.11 3 1 5 -5 138454. 1714.75 1 1 5 -5 139729. 1847.99 2 -1 -5 -5 137573. 1987.58 3 -1 5 5 140790. 1913.63 11 -1 -5 -4 28831.1 723.451 3 1 5 -4 29770.3 660.813 2 1 5 -4 30190.3 583.139 1 1 -5 4 28472.5 655.454 3 -1 5 4 28035.6 652.944 12 -1 5 4 30115.0 721.189 11 1 5 -3 72860.3 964.813 1 -1 -5 -3 69761.7 1161.41 3 1 -5 3 69382.0 1116.24 3 1 5 -3 70692.4 1061.44 2 -1 5 3 66890.1 1068.81 12 -1 5 3 73481.4 1196.97 11 1 -5 2 19302.4 522.610 3 -1 -5 -2 20840.4 551.491 3 1 5 -2 20963.7 485.396 2 1 5 -2 20855.1 408.615 1 -1 5 2 19673.5 492.434 12 -1 5 2 21050.7 571.471 11 -1 -5 -1 61202.7 1003.37 3 1 -5 1 64494.9 1061.64 3 1 5 -1 65500.5 936.503 2 1 5 -1 62365.0 790.947 1 -1 5 1 60554.2 949.137 12 1 5 -1 64034.8 750.145 13 -1 -5 0 86492.9 1229.32 3 1 -5 0 92443.8 1331.48 3 1 5 0 94207.4 1188.33 2 1 5 0 91553.1 1012.40 1 -1 5 0 88332.3 1208.01 12 1 5 0 91429.0 1070.05 13 1 5 1 64113.0 922.312 2 -1 -5 1 62450.2 977.927 3 1 -5 -1 63907.8 1074.04 3 1 5 1 64364.0 891.417 13 -1 5 -1 61584.6 943.060 12 1 5 2 20418.8 456.145 2 1 -5 -2 21311.2 592.414 3 -1 -5 2 19610.4 475.955 3 1 5 2 20142.9 463.373 13 1 -5 -3 72373.0 1234.66 3 -1 5 -3 71652.8 1107.95 1 -1 -5 3 70099.2 1048.97 3 1 5 3 70008.2 1059.02 13 1 -5 -4 30868.5 782.135 3 -1 5 -4 28975.9 662.481 1 -1 -5 4 28353.3 595.424 3 -1 5 -4 26597.4 614.304 12 1 5 4 28984.4 659.920 13 1 -5 -5 142778. 2068.88 3 -1 -5 5 137873. 1712.53 3 -1 5 -5 142286. 1873.58 1 1 5 5 141361. 1898.27 13 1 -5 -6 35040.6 938.517 3 -1 5 -6 34243.2 806.587 1 -1 -5 6 33014.5 688.791 3 -1 5 -6 32362.5 769.662 12 1 5 6 34498.9 841.854 13 1 -5 -7 13167.6 551.387 1 1 -5 -7 12951.9 584.599 3 -1 5 -7 11457.3 471.531 1 -1 5 -7 12197.6 475.575 12 1 5 7 11630.2 505.543 13 -1 5 -8 25854.1 761.890 1 1 -5 -8 26432.9 912.631 3 1 5 8 24175.3 792.917 13 -1 5 -8 26529.6 761.710 12 -1 5 -9 116356. 1923.02 1 1 -5 -9 127352. 2156.26 1 -1 5 -9 125123. 1981.02 12 1 5 9 116440. 2049.25 13 1 -5 -10 8255.41 515.204 1 -1 5 -10 7240.69 436.437 1 -1 -5 10 7406.28 394.909 11 1 5 10 6784.53 455.356 13 1 -5 -11 4768.42 405.822 1 1 -5 -11 4413.59 209.626 4 -1 5 -11 4252.97 356.003 1 1 5 11 4178.45 373.777 13 1 5 11 3865.93 223.619 14 -1 -5 11 3913.44 299.272 11 1 -5 -12 27869.6 1051.41 1 -1 5 -12 28008.5 964.037 1 1 -5 -12 26363.9 575.155 4 1 5 12 26072.3 634.782 14 1 5 12 26900.0 997.031 13 -1 -5 12 27695.2 845.985 11 -1 5 -12 29276.6 765.601 9 -1 -5 12 28992.3 691.354 8 1 -5 -13 41761.6 1435.35 3 1 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14 1 6 -16 12725.0 513.068 9 1 6 -15 5054.89 317.924 5 -1 6 15 5001.04 276.520 14 1 6 -15 5048.03 333.304 9 1 6 -14 39714.4 958.422 5 -1 6 14 39936.2 841.671 14 1 6 -14 41988.9 1014.78 9 1 6 -13 12080.0 508.950 5 1 6 -13 12123.7 617.155 1 -1 6 13 11885.1 434.194 14 1 6 -13 12384.2 533.189 9 1 6 -12 23773.6 718.613 5 1 6 -12 23333.4 828.247 1 -1 -6 -12 24463.5 1063.78 3 -1 6 12 26452.8 671.398 14 -1 6 12 25600.0 982.806 13 1 6 -12 24465.3 751.060 9 1 6 -11 4703.31 306.244 5 1 6 -11 4250.69 363.248 2 -1 -6 -11 3854.26 403.580 3 1 6 -11 4042.80 327.859 1 -1 6 11 5372.14 299.998 14 -1 6 11 4138.22 380.881 13 1 6 -11 3903.53 285.116 9 1 6 -10 20727.3 640.743 5 -1 -6 -10 20817.3 896.122 3 1 6 -10 20536.4 781.751 2 1 6 -10 21089.2 716.414 1 1 6 -10 20304.2 649.382 9 1 6 -9 14014.4 612.815 2 -1 -6 -9 13668.7 682.805 3 1 6 -9 13665.1 544.905 1 -1 6 9 14884.8 457.660 14 -1 6 9 13715.6 589.699 11 1 -6 8 39299.8 921.620 3 -1 -6 -8 37723.6 1107.25 3 1 6 -8 38661.6 903.639 1 1 6 -8 37742.1 992.608 2 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43850.7 808.496 12 1 6 0 45903.2 653.104 13 -1 -6 1 96646.6 1402.61 3 1 6 1 97344.3 1273.19 2 1 -6 -1 96109.8 1512.16 3 1 6 1 99569.9 1224.95 13 -1 6 -1 95662.6 1338.60 12 1 -6 -2 152846. 2107.23 3 -1 6 -2 153050. 1930.45 1 -1 6 -2 149519. 1863.15 12 1 6 2 155275. 1804.30 13 1 -6 -3 62294.2 1234.79 3 -1 -6 3 58773.4 1012.19 3 -1 6 -3 60267.6 1052.71 1 1 6 3 60023.4 991.638 13 -1 6 -3 57402.8 988.558 12 -1 6 -4 55515.5 1034.87 1 -1 -6 4 56045.0 973.256 3 -1 6 -4 55540.9 990.028 12 1 6 4 57581.0 1033.96 13 -1 -6 5 121767. 1634.56 3 1 -6 -5 122114. 1983.23 3 -1 6 -5 115296. 1717.51 1 1 6 5 121860. 1760.27 13 -1 6 -5 114919. 1646.42 12 1 -6 -6 37070.8 1042.07 3 -1 -6 6 36178.9 771.288 3 -1 6 -6 35542.8 864.512 1 1 6 6 34784.2 879.183 13 -1 6 -6 35594.4 810.406 12 1 -6 -7 37378.9 1106.17 3 -1 6 -7 34439.2 891.854 1 -1 -6 7 38501.3 832.649 3 -1 6 -7 35928.5 853.165 12 1 6 7 35542.8 952.001 13 -1 6 -8 39714.5 1003.06 1 1 -6 -8 41069.7 1215.81 3 1 6 8 38958.3 1057.02 13 1 -6 -9 14766.7 747.508 3 -1 6 -9 14135.0 599.877 1 1 6 9 13980.2 648.740 13 1 -6 -10 22022.7 962.159 3 -1 6 -10 19846.3 752.799 1 1 -6 -10 20577.3 484.384 4 1 6 10 20748.1 537.081 14 1 6 10 21267.5 843.177 13 1 -6 -11 4569.75 452.477 3 -1 6 -11 4555.53 373.375 1 1 -6 -11 4428.61 222.465 4 1 6 11 4025.90 233.746 14 -1 -6 11 4485.82 330.976 11 1 6 11 4171.85 386.660 13 -1 6 -11 4722.61 292.065 9 1 -6 -12 24528.6 561.775 4 1 -6 -12 26112.1 1128.81 3 -1 6 -12 25874.7 936.757 1 -1 -6 12 24224.0 812.321 11 1 6 12 24259.7 978.956 13 1 6 12 23678.8 608.371 14 -1 6 -12 26657.6 742.426 9 1 -6 -13 12102.2 388.521 4 1 6 13 11614.4 420.827 14 -1 -6 13 11869.4 570.076 11 -1 6 -13 12512.2 504.264 9 1 -6 -14 42797.9 797.418 4 -1 6 -14 41898.2 1016.14 5 -1 6 -14 42964.8 982.011 9 -1 6 -15 5505.77 345.135 5 -1 6 -15 5430.56 323.271 9 -1 6 -16 12552.8 504.810 5 -1 6 -16 12429.9 464.391 9 -1 6 -17 4449.26 284.782 5 -1 6 -18 2840.11 208.394 5 -1 6 -19 322.164 73.8635 5 -1 6 -20 1401.83 110.320 5 1 7 -19 1306.37 107.527 5 1 7 -19 1250.58 104.552 9 1 7 -18 154.965 55.4797 5 1 7 -18 171.825 49.4464 9 1 7 -17 283.493 77.7900 5 1 7 -17 109.477 56.9183 9 1 7 -16 7285.99 359.726 5 -1 7 16 7519.10 313.134 14 1 7 -16 7031.98 362.995 9 1 7 -15 1022.95 146.477 5 -1 7 15 928.042 117.301 14 1 7 -15 1234.75 169.660 9 1 7 -14 4734.25 318.376 5 -1 7 14 4919.83 275.413 14 1 7 -14 5157.14 343.692 9 1 7 -13 90082.6 1585.07 5 -1 7 13 90398.5 1395.53 14 1 7 -13 94929.8 1655.20 9 1 7 -12 73244.4 1411.04 5 -1 -7 -12 75284.7 1976.43 3 1 7 -12 76157.3 1456.76 9 1 7 -11 31132.1 851.257 5 -1 -7 -11 31507.4 1199.46 3 1 7 -11 31052.5 943.918 1 -1 7 11 32915.8 1130.32 13 1 7 -11 31757.1 874.301 9 1 7 -10 6813.32 378.640 5 -1 7 10 7294.88 283.050 6 1 7 -10 7082.12 415.125 1 -1 -7 -10 6584.48 518.177 3 -1 7 10 7453.84 512.862 13 -1 7 10 8382.65 381.825 14 1 7 -10 7374.49 397.090 9 -1 7 9 26199.6 565.197 6 1 7 -9 26175.0 740.538 5 1 7 -9 27128.2 802.580 1 -1 -7 -9 25968.5 997.705 3 -1 7 9 28106.7 668.018 14 -1 7 9 27874.2 963.573 13 1 7 -9 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2 -2 2 3885.28 162.082 3 -2 2 2 4225.35 198.328 11 2 -2 2 4007.26 168.831 13 2 -2 1 218137. 2045.30 2 2 2 -1 224383. 2312.37 2 2 2 -1 225912. 2018.80 1 -2 -2 -1 214720. 2042.43 3 2 -2 1 212684. 2175.45 3 2 2 -1 222152. 2237.98 13 2 2 0 483151. 4785.40 2 -2 -2 0 430524. 4444.97 3 -2 -2 0 476337. 4552.19 12 2 2 0 489023. 4749.66 13 2 -2 -1 212182. 2093.53 3 2 2 1 216904. 2173.31 2 -2 -2 1 224475. 1848.01 12 2 2 1 213699. 2152.91 13 -2 2 -1 220984. 2115.07 11 2 -2 -2 4384.92 148.283 2 2 -2 -2 4162.40 179.413 3 2 2 2 4234.06 193.472 2 -2 -2 2 4356.00 78.4207 12 2 2 2 3903.26 187.179 13 2 2 3 188866. 2058.69 2 2 -2 -3 186306. 2035.61 3 -2 2 -3 187715. 2092.88 1 2 -2 -3 185947. 2128.51 1 -2 2 -3 186223. 2144.10 12 2 2 3 188979. 2108.11 13 -2 2 -4 198827. 2211.18 1 2 -2 -4 198224. 2261.02 1 -2 -2 4 189114. 2120.05 11 -2 2 -4 199611. 2298.81 12 2 2 4 192417. 2200.50 13 2 -2 -5 177033. 2124.58 1 -2 2 -5 172581. 2050.06 1 -2 2 -5 168894. 2142.68 12 -2 -2 5 173898. 1992.92 11 2 -2 -6 38447.7 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548.040 14 2 11 -2 20063.3 639.757 9 2 -11 2 20701.9 561.260 10 2 11 -1 11620.5 452.166 6 -2 11 1 11482.7 401.802 6 2 11 -1 11427.2 455.472 5 -2 11 1 12147.3 418.790 14 2 -11 1 12389.8 416.420 10 -2 11 0 39518.5 788.778 6 2 11 0 38436.1 867.045 5 -2 11 0 43475.3 839.253 5 2 11 0 41753.9 890.119 6 -2 11 -1 11578.1 395.392 6 2 11 1 11517.4 439.833 5 -2 11 -1 11916.3 428.296 5 2 11 1 12259.1 456.600 6 -2 11 -2 19411.6 565.374 5 -2 11 -2 18849.6 500.242 6 2 11 2 19640.1 579.911 6 2 11 2 19798.0 574.233 5 2 11 3 24555.7 642.936 5 -2 11 -3 23691.6 644.982 5 2 11 3 23545.1 629.540 6 2 11 4 14703.0 482.224 6 -2 11 -4 14620.9 507.048 5 2 11 5 10109.4 388.844 6 -2 11 -5 10306.2 431.717 5 2 -11 -6 4978.72 265.812 4 2 11 6 5035.43 265.487 6 -2 11 -6 5111.59 310.752 5 2 -11 -7 28110.9 659.097 4 2 11 7 26843.5 625.526 6 -2 11 -7 26602.1 740.064 5 2 -11 -8 115.413 57.1184 4 2 11 8 25.8972 45.6159 6 -2 11 -8 44.8897 61.7344 5 2 -11 -9 12373.8 410.090 4 -2 11 -9 12344.8 495.534 5 2 11 9 11956.3 366.270 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341.885 97.5575 9 2 -12 8 401.660 90.8716 10 2 12 -7 9494.33 363.480 6 2 12 -7 9421.50 430.185 5 -2 12 7 10836.7 403.861 14 2 -12 7 9508.21 382.204 10 2 12 -7 9490.56 433.653 9 -2 12 6 2039.76 166.941 6 2 12 -6 2092.27 179.622 6 2 12 -6 1798.78 188.915 5 -2 12 6 2286.26 182.953 14 2 -12 6 2065.37 178.942 10 2 12 -6 2228.38 212.640 9 -2 12 5 8989.22 344.894 6 2 12 -5 7865.14 393.404 5 2 12 -5 9370.84 388.736 6 -2 12 5 8932.90 356.761 14 2 12 -5 9119.01 427.771 9 2 -12 5 9200.30 376.326 10 -2 12 4 9432.96 357.084 6 2 12 -4 8444.61 408.039 5 2 12 -4 9185.49 392.641 6 -2 12 4 9735.74 371.874 14 2 -12 4 9439.91 382.238 10 2 12 -4 9488.23 440.239 9 2 12 -3 26938.8 740.207 5 -2 12 3 28218.5 647.843 6 2 12 -3 28113.5 719.923 6 -2 12 3 29321.9 673.018 14 2 -12 3 30404.5 700.256 10 -2 12 2 25713.1 614.317 6 2 12 -2 25548.6 687.258 6 2 -12 2 26962.4 646.739 10 2 12 -1 3334.02 241.518 6 -2 12 1 2984.99 200.927 6 2 12 0 4502.99 277.419 5 -2 12 0 4287.49 236.362 6 2 12 0 4946.07 289.645 6 2 12 1 2972.55 224.486 5 -2 12 -1 3083.72 199.681 6 -2 12 -1 2665.15 194.116 5 2 12 2 26106.3 666.422 5 2 12 2 25439.7 659.375 6 -2 12 -2 25265.2 570.491 6 -2 12 -2 25141.8 639.299 5 -2 12 -3 28362.3 695.576 5 2 12 3 28527.0 693.483 6 2 12 4 9312.54 371.826 6 -2 12 -4 9550.19 394.688 5 2 -12 -5 8875.22 350.785 4 -2 12 -5 8641.71 382.273 5 2 12 5 8976.63 356.354 6 2 -12 -6 2088.93 168.154 4 -2 12 -6 1969.28 184.671 5 2 12 6 2040.01 164.747 6 2 -12 -7 10151.0 368.423 4 -2 12 -7 8993.15 393.843 5 2 12 7 9536.64 341.336 6 2 -12 -8 418.351 89.5586 4 -2 12 -8 309.259 86.5024 5 2 12 8 432.752 80.2434 6 2 -12 -9 8378.50 318.139 4 2 12 9 8646.85 287.462 6 -2 12 -9 7960.55 363.212 5 2 -12 -10 1227.69 119.301 4 2 12 10 1259.43 102.253 6 -2 12 -10 1134.99 136.953 5 2 -12 -11 1223.02 110.337 4 -2 12 -11 1216.10 134.629 5 2 -12 -12 1529.78 113.949 4 -2 12 -12 1716.11 147.525 5 2 -12 -13 14057.4 322.419 4 -2 12 -13 15145.3 399.848 5 2 13 -12 1244.90 99.5170 5 2 -13 12 1343.20 95.3435 10 2 13 -11 1131.32 108.611 5 -2 13 11 1244.12 88.4006 14 2 -13 11 1199.43 103.019 10 2 13 -10 3712.82 212.086 5 -2 13 10 3871.67 171.294 14 2 -13 10 3797.33 195.856 10 2 13 -9 3608.12 223.136 5 -2 13 9 3869.04 183.475 14 2 -13 9 3508.60 200.605 10 2 13 -8 7926.89 349.449 5 2 -13 8 7764.43 313.794 10 2 13 -7 2466.11 203.023 5 2 13 -7 2582.55 164.276 6 -2 13 7 3016.90 188.194 14 2 -13 7 2495.09 181.785 10 2 13 -6 5646.19 310.950 5 2 13 -6 5855.95 268.107 6 -2 -13 -6 5658.48 229.245 4 2 -13 6 5842.86 283.402 10 -2 13 5 10093.6 343.814 6 2 13 -5 9859.66 414.477 5 2 13 -5 10007.4 374.067 6 2 -13 5 10034.0 375.307 10 2 13 -4 8709.10 390.796 5 -2 13 4 7927.51 306.764 6 2 13 -4 8075.14 346.704 6 2 -13 4 8251.89 338.279 10 2 13 -3 3334.15 239.483 5 -2 13 3 3055.41 193.002 6 2 13 -3 3605.19 236.024 6 2 -13 3 3217.83 206.426 10 -2 13 2 3959.33 217.386 6 2 13 -2 4141.99 263.821 5 2 13 -2 4433.72 264.934 6 2 -13 2 4324.06 231.440 10 -2 13 1 14904.4 429.954 6 2 13 -1 16516.5 531.319 5 2 13 -1 16336.7 515.848 6 2 13 0 22324.8 598.144 6 2 13 0 21401.0 601.189 5 -2 13 -1 14308.4 404.401 6 2 13 1 15394.2 492.383 6 -2 13 -2 3991.62 198.071 6 -2 13 -2 4096.53 227.903 5 2 13 2 4299.64 252.230 6 -2 13 -3 3394.15 211.830 5 2 13 3 3522.12 222.487 6 2 -13 -4 8316.73 329.622 4 2 13 4 8792.54 342.475 6 -2 13 -4 7613.01 324.744 5 2 -13 -5 9756.12 355.889 4 2 13 5 10350.5 359.763 6 -2 13 -5 9391.98 363.100 5 2 -13 -6 5875.84 267.272 4 -2 13 -6 5395.25 273.369 5 2 13 6 5896.15 258.961 6 2 -13 -7 2689.25 174.076 4 -2 13 -7 2342.84 177.316 5 2 13 7 2532.13 161.487 6 2 -13 -8 8095.57 295.555 4 -2 13 -8 7555.57 316.026 5 2 13 8 8545.77 276.551 6 2 -13 -9 3874.22 193.200 4 2 13 9 3758.20 165.997 6 -2 13 -9 3362.96 201.742 5 2 -13 -10 3814.23 178.009 4 -2 13 -10 3413.10 193.078 5 2 -13 -11 1225.63 94.1520 4 -2 13 -11 1098.92 102.232 5 2 14 -10 437.313 62.4632 5 2 -14 10 469.818 60.2769 10 2 14 -9 3702.20 185.975 5 2 -14 9 3659.31 174.722 10 2 14 -8 5966.00 252.977 5 2 -14 8 6152.70 239.121 10 2 14 -7 118.840 54.2779 5 2 -14 7 166.811 54.3423 10 2 14 -6 8998.53 345.675 5 2 14 -6 9593.35 289.878 6 2 -14 6 9033.33 311.485 10 -2 -14 -5 822.366 80.7396 4 2 14 -5 1109.16 126.488 5 2 14 -5 971.271 103.034 6 2 -14 5 931.345 103.084 10 2 14 -4 3440.75 195.605 6 2 14 -4 3724.36 226.951 5 2 -14 4 3588.30 193.570 10 2 14 -3 3242.12 197.041 6 2 14 -3 3581.61 227.281 5 2 -14 3 3564.30 187.520 10 2 14 -2 7035.78 320.217 5 2 14 -2 6666.98 290.006 6 -2 14 2 6312.64 250.275 6 2 14 -1 3923.17 224.754 6 -2 14 1 3775.28 190.794 6 -2 14 0 25739.0 521.920 6 2 14 0 27507.5 624.133 6 -2 14 -1 3903.61 183.178 6 2 14 1 4001.75 223.241 6 2 -14 -2 7062.10 282.309 4 2 14 2 6940.05 290.771 6 2 -14 -3 3388.29 197.338 4 2 14 3 3544.07 203.421 6 2 -14 -4 3687.62 198.732 4 2 14 4 3807.03 202.334 6 -2 14 -4 3582.68 188.679 5 2 -14 -5 975.570 103.583 4 -2 14 -5 943.568 98.4713 5 2 14 5 953.094 99.8636 6 2 -14 -6 8941.73 296.206 4 2 14 6 9116.39 286.396 6 -2 14 -6 8426.32 288.599 5 2 -14 -7 208.604 56.6383 4 2 14 7 194.757 51.8791 6 -2 14 -7 152.937 50.4028 5 2 -14 -8 6058.17 220.592 4 -2 14 -8 5561.34 215.914 5 2 14 8 6203.92 199.635 6 2 -14 -9 3784.83 162.300 4 2 -14 -10 411.137 50.3377 4 2 15 -7 97.8291 38.3741 5 2 15 -6 5094.23 209.917 5 2 15 -5 888.947 96.6832 5 -2 -15 -4 2358.84 122.338 4 2 15 -4 2603.76 162.381 5 2 15 -4 2546.10 135.662 6 -2 -15 -3 6160.49 213.718 4 2 15 -3 7011.04 243.215 6 2 15 -2 2943.50 164.456 6 2 -15 1 2629.45 150.354 4 2 15 -1 2689.66 158.841 6 2 -15 0 8941.08 282.660 4 2 15 0 8777.92 290.736 6 2 -15 -1 2700.17 154.672 4 2 15 1 2583.40 155.594 6 2 -15 -2 2998.34 160.963 4 2 15 2 3258.82 171.080 6 2 -15 -3 6508.48 236.281 4 2 15 3 6932.31 242.902 6 2 -15 -4 2439.64 139.736 4 2 15 4 2694.42 145.377 6 2 -15 -5 759.988 76.8355 4 2 15 5 792.245 79.3892 6 2 -15 -6 4554.57 175.974 4 2 15 6 5178.13 176.545 6 2 -15 -7 89.0165 33.3868 4 -3 0 0-3.75297 28.0494 12 -3 0 0 33.3147 20.3616 11 3 0 1 175936. 1916.12 2 3 0 -1 162884. 1917.25 2 3 0 -1 158762. 1503.40 3 -3 0 1 178069. 1871.93 11 3 0 1 181158. 2007.32 13 -3 0 -1 185365. 1772.45 11 -3 0 1 178670. 1851.39 12 -3 0 -1 187492. 1968.03 12 3 0 -2 160921. 1914.19 2 3 0 2 161104. 1847.64 2 3 0 -2 162145. 1543.21 3 -3 0 -2 170782. 1955.03 12 -3 0 2 166188. 1779.58 12 -3 0 2 159268. 1854.59 11 -3 0 -2 162396. 1658.25 11 3 0 2 167580. 1963.28 13 3 0 -3 13267.2 266.901 3 3 0 -3 13545.3 384.754 1 3 0 3 12323.1 358.170 2 3 0 -3 12009.6 388.119 2 -3 0 -3 12896.1 351.203 1 -3 0 3 13635.8 333.154 12 -3 0 3 13538.7 392.857 11 -3 0 -3 14475.8 439.967 12 3 0 3 13114.0 411.961 13 -3 0 -3 13920.1 260.749 11 3 0 -4 24493.1 599.267 2 3 0 -4 27200.9 599.556 1 -3 0 -4 25278.0 543.507 1 -3 0 4 27488.6 617.558 11 -3 0 4 27697.3 517.240 12 -3 0 -4 28640.2 678.002 12 3 0 4 27530.6 635.838 13 -3 0 -5 26593.6 587.626 1 3 0 -5 27402.4 639.598 1 -3 0 5 27037.7 641.816 11 -3 0 -5 27458.9 693.883 12 -3 0 5 28144.1 541.898 12 3 0 5 26574.7 645.457 13 -3 0 -6 1291.06 130.808 1 -3 0 6 1506.95 151.757 11 3 0 6 1396.38 147.235 13 -3 0 -7 81253.7 1280.22 1 3 0 -7 77764.5 1327.16 1 -3 0 7 80281.4 1329.23 11 3 0 -8 214769. 2795.15 1 -3 0 8 218430. 2748.74 11 3 0 8 215072. 2774.90 13 -3 0 -9 5401.92 327.794 1 3 0 -9 4860.82 333.543 1 -3 0 9 5201.86 323.882 11 3 0 9 4528.80 314.525 13 3 0 -10 18081.9 690.782 1 -3 0 10 18462.6 652.735 11 3 0 10 16845.8 644.577 13 3 0 -11 147.023 74.9148 1 -3 0 -11 237.601 94.8049 1 3 0 11 300.872 109.188 13 -3 0 11 265.864 87.2121 11 3 0 11 194.931 78.5842 8 3 0 -12 723.692 108.320 4 -3 0 -12 975.308 178.572 1 3 0 -12 694.479 166.657 1 3 0 12 684.479 130.078 13 -3 0 12 754.375 151.993 11 3 0 12 801.516 124.860 8 3 0 -13 85928.7 1341.97 4 3 0 -13 89213.9 1923.29 1 -3 0 -13 94727.6 1818.52 1 -3 0 -13 88548.4 1974.72 12 -3 0 13 85708.2 1716.19 11 3 0 13 80272.4 1699.77 13 3 0 13 89476.5 1507.95 8 3 0 -14 45058.2 912.063 4 3 0 -14 46891.5 1387.58 1 -3 0 -14 48779.2 1289.26 1 3 0 14 43332.4 1213.55 13 -3 0 14 44590.6 1201.09 11 3 0 14 46413.7 1042.36 8 3 0 -15 9274.14 383.546 4 -3 0 15 9734.64 423.353 8 3 0 15 9349.82 441.293 8 3 0 -16 4460.00 259.367 4 3 0 -16 4703.11 301.994 9 -3 0 16 4684.17 287.482 8 3 0 16 4207.03 288.319 8 3 0 -17 854.775 112.513 4 -3 0 17 811.752 123.592 8 3 0 -17 951.002 138.379 9 3 0 17 708.599 120.538 8 3 0 -18 993.173 112.138 4 3 0 -18 1248.01 150.793 9 3 0 18 1119.59 139.038 8 -3 0 18 978.087 128.582 8 3 0 -19 1683.14 131.464 4 3 0 -19 1918.55 165.148 9 3 0 19 1740.75 160.313 8 -3 0 19 1940.04 162.226 8 -3 0 20 1250.68 116.496 8 3 0 -20 1300.25 125.031 9 3 0 20 1162.36 116.169 8 3 0 -21 442.330 62.0879 9 3 0 21 531.058 70.2856 8 -3 0 21 542.009 67.4447 8 3 -1 21 245.045 45.8790 8 3 1 -21 241.859 49.6349 9 -3 1 21 247.976 48.0315 8 -3 1 20 5570.36 237.290 8 3 1 -20 5430.14 250.817 9 3 -1 20 5219.10 235.298 8 3 1 -19 1086.42 103.889 4 3 -1 19 1146.18 127.908 8 -3 1 19 1219.70 127.437 8 3 1 -19 1022.20 127.712 9 3 1 -18 182.347 55.8982 4 3 1 -18 334.341 83.2503 9 3 -1 18 204.623 68.0045 8 -3 1 18 260.536 74.3380 8 3 1 -17 2627.01 198.011 4 3 1 -17 2746.95 225.692 9 -3 1 17 2703.04 214.270 8 3 -1 17 2603.28 220.628 8 3 1 -16 1297.45 148.620 4 3 1 -16 1323.12 166.410 9 3 -1 16 1063.46 142.806 8 -3 1 16 1109.88 140.224 8 3 1 -15 4834.95 278.593 4 3 1 -15 5061.98 317.036 9 -3 1 15 4908.30 299.058 8 3 -1 15 5079.89 321.413 8 3 1 -14 26444.3 687.160 4 3 1 -14 26761.2 1004.98 1 3 1 -14 26291.6 992.570 2 -3 1 14 25967.3 920.412 11 -3 1 14 29919.5 646.634 14 3 1 -14 26700.9 753.019 9 3 -1 14 27543.5 773.436 8 3 1 -13 29317.2 718.722 4 -3 -1 -13 31840.8 992.986 1 3 1 -13 28667.8 1012.13 1 3 1 -13 26443.9 975.254 2 -3 1 13 32757.3 674.995 14 -3 1 13 28484.4 945.588 11 3 -1 13 30005.1 800.885 8 3 1 -12 5078.34 276.825 4 3 1 -12 4594.51 374.029 1 -3 -1 -12 5793.28 392.877 1 -3 1 12 5730.83 262.257 14 -3 1 12 5451.76 396.557 11 3 -1 12 4729.74 353.046 13 3 -1 12 5306.20 315.455 8 3 1 -11 14872.3 465.202 4 -3 -1 -11 16210.2 625.174 1 3 1 -11 13159.4 608.455 1 -3 1 11 14097.5 607.370 11 3 -1 11 12731.8 561.191 13 3 -1 11 14786.1 510.027 8 3 1 -10 22872.1 765.838 1 3 -1 10 23101.9 731.738 13 -3 1 10 23876.6 768.147 11 3 1 -9 18588.0 648.522 1 -3 1 9 18846.5 652.985 11 3 -1 9 17702.4 607.635 13 3 1 -8 49894.2 1046.23 1 -3 1 8 50331.2 1077.82 11 3 -1 8 47545.3 1011.55 13 -3 -1 -7 11823.9 407.661 1 3 1 -7 11809.3 446.279 1 3 1 -7 10935.4 460.311 2 -3 1 7 11797.7 465.216 11 3 -1 7 11714.2 443.841 13 3 1 -6 2484.28 211.937 2 -3 -1 -6 2777.40 179.529 1 3 1 -6 2692.26 195.103 1 -3 1 6 3055.92 190.229 12 -3 1 6 2695.97 207.527 11 3 -1 6 2669.84 197.877 13 3 1 -5 39922.3 866.130 2 -3 -1 -5 41637.5 732.575 1 -3 1 5 42059.8 860.177 11 3 -1 5 42039.8 828.936 13 -3 1 5 42624.2 751.851 12 -3 -1 -4 49614.0 761.968 1 3 1 -4 47919.6 812.882 1 -3 1 4 49834.1 798.435 12 -3 1 4 50218.3 910.136 11 3 -1 4 50142.2 888.002 13 3 1 -3 65661.0 1087.48 2 3 1 -3 68626.2 975.047 1 -3 -1 -3 67124.9 902.576 1 -3 -1 -3 73181.1 1094.06 12 -3 1 3 68980.9 984.577 12 3 -1 3 72034.3 1087.37 13 -3 1 3 73715.8 1100.91 11 -3 -1 -3 68034.9 681.746 11 3 -1 2 40994.1 672.572 2 -3 -1 -2 39838.2 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9750.36 445.786 5 -3 8 9 9494.03 389.618 14 3 -8 9 9244.66 382.105 10 3 8 -9 9684.30 483.211 9 3 8 -8 6908.18 350.415 6 3 8 -8 6653.69 361.802 5 3 -8 8 6793.58 429.428 3 -3 8 8 6415.56 313.610 14 3 -8 8 6601.03 319.662 10 3 8 -8 6547.58 385.702 9 3 8 -7 3147.67 235.790 6 3 8 -7 2913.30 233.799 5 3 -8 7 3023.23 282.352 3 -3 8 7 3093.52 208.741 14 3 8 -7 3092.80 259.945 9 3 -8 7 3161.87 217.226 10 -3 8 6 38738.9 724.880 6 3 8 -6 35631.1 845.812 5 3 8 -6 37195.4 847.385 6 3 8 -6 35409.2 1082.94 2 3 -8 6 34792.3 972.947 3 -3 8 6 35669.1 761.008 14 3 8 -6 35372.0 892.273 9 3 8 -5 3123.54 229.242 5 3 8 -5 2643.86 211.062 6 3 8 -5 3084.26 296.332 2 3 -8 5 2566.68 254.016 3 -3 8 5 2559.76 264.135 12 -3 8 5 2668.90 189.555 14 3 8 -5 2546.98 218.507 9 -3 8 4 9800.55 337.001 6 3 8 -4 9503.44 389.136 5 3 8 -4 9712.20 399.840 6 3 8 -4 11349.0 544.712 2 3 -8 4 9135.58 481.617 3 -3 8 4 9593.66 360.989 14 -3 8 4 9454.35 497.128 12 3 8 -4 9616.14 414.576 9 3 -8 4 10064.2 370.469 10 -3 8 3 10255.9 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6129.40 392.600 1 3 8 3 10024.4 363.172 5 3 8 3 9882.30 364.275 6 -3 8 -3 9556.19 500.305 12 -3 8 -3 9307.29 376.647 14 3 -8 -3 9776.46 543.056 3 -3 8 -3 9242.70 489.368 1 3 8 4 10016.7 364.357 6 -3 8 -4 9245.85 383.460 14 -3 8 -4 8990.69 496.328 12 3 -8 -4 9796.18 563.251 3 -3 8 -4 9032.50 485.679 1 3 8 5 2610.09 182.049 6 -3 8 -5 2495.19 263.217 12 3 -8 -5 2509.75 170.382 4 3 -8 -5 2481.09 298.716 3 -3 8 -5 2361.43 257.448 1 -3 8 -6 37900.4 834.353 5 3 8 6 36591.0 729.935 6 -3 8 -6 36886.0 1088.84 12 3 8 6 37233.9 1039.21 13 3 -8 -6 36222.7 724.918 4 3 -8 -6 37267.3 1219.12 3 -3 8 -6 34855.0 1037.21 1 -3 8 -7 3177.67 234.467 5 3 8 7 3415.27 200.140 6 -3 -8 7 3059.67 284.987 11 3 8 7 3311.40 311.295 13 3 -8 -7 3116.61 361.483 3 -3 8 -7 3069.20 311.076 1 3 -8 -7 3039.63 198.192 4 -3 8 -8 6782.83 358.484 5 -3 -8 8 7595.19 458.405 11 3 8 8 6498.17 457.516 13 -3 8 -8 6857.75 469.294 1 3 -8 -8 6716.39 299.834 4 3 -8 -8 7210.34 559.072 3 -3 8 -9 10159.6 450.580 5 -3 -8 9 10186.1 548.869 11 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928.813 9 3 9 -11 770.860 132.749 5 -3 9 11 852.096 153.507 14 3 9 -11 682.644 146.184 9 3 -9 11 747.673 113.757 10 3 9 -10 9659.46 388.205 6 3 9 -10 8837.80 423.876 5 -3 9 10 9605.43 404.286 14 3 -9 10 8403.15 363.623 10 3 9 -10 8990.18 464.968 9 3 9 -9 25527.6 680.292 6 3 9 -9 24296.8 723.380 5 -3 9 9 23788.5 641.720 14 3 -9 9 22664.5 621.339 10 3 9 -9 24404.8 777.597 9 3 9 -8 4241.35 273.579 6 3 9 -8 4228.65 293.963 5 -3 9 8 4021.62 248.568 14 3 9 -8 4080.56 307.856 9 3 -9 8 3911.61 250.888 10 3 9 -7 4912.74 313.316 5 3 9 -7 4840.15 296.163 6 3 -9 7 4672.49 353.217 3 -3 9 7 4452.92 261.140 14 3 -9 7 5168.72 283.677 10 3 9 -7 4704.49 324.328 9 -3 9 6 2664.39 185.916 6 3 9 -6 2120.81 204.285 5 3 9 -6 2198.32 202.927 6 3 -9 6 2088.30 242.949 3 -3 9 6 2150.01 179.272 14 3 -9 6 2238.31 186.111 10 3 9 -6 2278.32 220.376 9 -3 9 5 4015.48 224.880 6 3 9 -5 3465.46 256.819 5 3 9 -5 3747.46 259.617 6 3 -9 5 3591.46 319.511 3 -3 9 5 3467.92 226.823 14 3 -9 5 3852.80 238.525 10 3 9 -5 3592.67 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4 -3 9 -7 4686.45 389.515 1 3 -9 -7 4792.00 457.242 3 3 -9 -8 4181.75 241.536 4 3 9 8 4138.01 217.704 6 -3 9 -8 4033.29 276.129 5 3 -9 -9 25632.3 626.504 4 -3 9 -9 24936.2 725.838 5 3 -9 -10 9485.15 365.564 4 -3 9 -10 9597.10 443.901 5 3 -9 -11 988.702 137.041 4 -3 9 -11 779.065 146.783 5 3 -9 -12 37950.0 762.941 4 -3 9 -12 36223.0 891.627 5 3 -9 -13 6333.63 283.442 4 -3 9 -13 6358.33 343.164 5 3 -9 -14 886.495 104.501 4 -3 9 -14 1031.06 136.925 5 3 -9 -15 300.294 55.4921 4 -3 9 -15 420.282 83.0630 5 3 -9 -16 6202.24 222.486 4 -3 9 -16 6483.53 265.324 5 3 10 -16 1628.12 116.333 9 3 10 -15 104.972 41.0437 5 -3 10 15-15.2770 35.6136 14 3 -10 15-5.48120 26.5928 10 3 10 -15 16.7173 40.1191 9 3 10 -14 8257.13 301.451 5 -3 10 14 8743.92 291.549 14 3 -10 14 7851.49 258.910 10 3 10 -14 8368.73 348.568 9 3 10 -13 10903.4 385.478 5 3 -10 13 10095.4 330.414 10 3 10 -13 10592.0 428.409 9 3 10 -12 1346.02 148.731 5 -3 10 12 1421.36 138.574 14 3 -10 12 1289.54 130.737 10 3 10 -12 1277.17 160.800 9 3 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7 158246. 2571.41 11 4 4 -6 5395.92 402.543 2 4 -4 6 5831.19 303.807 3 -4 4 6 5181.22 330.715 12 -4 4 6 6068.56 419.898 11 4 4 -5 14377.3 621.418 2 4 -4 5 14354.8 459.760 3 -4 4 5 14145.1 535.100 12 -4 4 5 15801.9 655.496 11 4 4 -4 6179.78 385.463 2 4 -4 4 6290.62 293.446 3 -4 4 4 7160.63 414.266 11 -4 4 4 6215.73 338.839 12 4 4 -3 9149.48 453.009 2 4 -4 3 9588.27 360.965 3 -4 -4 -3 10304.4 388.852 12 -4 4 3 9113.06 412.439 12 -4 4 3 9727.70 474.830 11 4 4 -2 220550. 2842.47 2 4 -4 2 230950. 2541.81 3 -4 4 2 225062. 2853.69 11 4 4 -1 88384.1 1528.58 2 4 -4 1 96331.2 1359.59 3 -4 4 1 87813.6 1476.81 12 -4 -4 -1 87905.3 1170.95 11 -4 4 1 94890.2 1549.77 11 4 4 0 28217.3 773.352 2 4 -4 0 30306.4 676.128 3 -4 4 0 29232.4 777.784 12 -4 -4 0 28807.0 600.777 11 4 4 0 30709.6 748.180 13 -4 4 0 30230.2 777.949 11 4 4 1 87419.2 1499.72 2 4 -4 -1 95545.7 1400.31 3 -4 -4 1 92746.0 1328.28 11 -4 4 -1 89605.0 1536.51 12 4 4 1 95002.8 1515.52 13 -4 4 -1 97086.9 1514.45 11 4 -4 -2 227494. 2644.02 3 -4 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11057.6 596.091 13 -4 4 -9 10812.3 625.310 12 4 4 9 11444.3 433.104 8 4 -4 -10 8719.14 338.397 4 -4 4 -10 9131.00 533.465 1 4 -4 -10 9600.16 545.674 3 4 4 10 8652.50 547.631 13 -4 4 -10 8173.14 561.394 12 -4 -4 10 8718.94 487.251 11 4 4 10 7974.18 375.166 8 4 -4 -11 5518.18 274.597 4 -4 4 -11 5454.66 420.562 1 -4 -4 11 5032.93 384.773 11 4 4 11 4901.42 427.943 13 -4 4 -11 5095.13 457.960 12 4 4 11 5089.80 308.542 8 4 -4 -12 30159.2 699.025 4 -4 4 -12 32204.6 1073.93 1 -4 -4 12 30403.4 977.878 11 4 -4 -13 7136.34 329.975 4 4 4 13 6753.71 367.218 8 4 -4 -14 7127.63 324.369 4 4 4 14 6732.13 361.793 8 4 -4 -15 5419.29 281.474 4 4 4 15 5312.16 312.331 8 -4 -4 15 5723.74 301.284 8 4 -4 -16 177.965 60.4039 4 -4 -4 16 273.173 75.0564 8 4 4 16 185.009 57.1105 8 4 -4 -17 1330.88 130.428 4 4 4 17 1234.27 131.208 8 -4 -4 17 1355.16 128.334 8 4 -4 -17 1559.81 140.146 9 4 -4 -18 607.164 82.0109 4 -4 4 -18 792.937 103.497 5 4 -4 -18 680.320 87.1737 9 4 4 18 622.184 82.1731 8 -4 -4 18 656.333 84.9440 8 4 -4 -19 539.445 68.5719 4 -4 4 -19 522.820 71.6978 5 -4 -4 19 462.445 61.4398 8 4 5 -19 1748.38 126.094 9 4 5 -18 16.7825 46.3880 9 -4 5 17 4498.08 211.417 8 4 -5 17 4070.16 211.786 8 4 5 -17 4530.89 265.660 9 -4 5 16 2021.40 147.493 14 -4 5 16 1917.56 148.395 8 4 -5 16 1873.46 159.660 8 4 5 -16 2170.75 199.898 9 4 5 -15 1379.72 154.856 4 -4 5 15 1318.14 129.771 14 -4 5 15 1645.45 151.498 8 4 -5 15 1332.99 145.681 8 4 5 -15 1366.86 165.773 9 4 5 -14 3917.33 267.343 4 -4 5 14 4458.60 247.406 14 -4 5 14 4153.63 245.057 8 4 -5 14 4328.87 272.988 8 4 5 -14 4325.65 304.149 9 4 5 -13 5042.17 316.872 4 -4 5 13 5930.01 305.966 14 4 -5 13 5313.70 306.001 8 4 5 -13 5156.67 336.829 9 4 5 -12 13658.9 533.268 4 4 5 -12 13513.3 478.209 6 4 -5 12 12768.4 415.578 10 4 -5 12 13825.6 505.078 8 4 5 -12 13585.3 556.308 9 4 5 -11 14757.0 553.699 4 4 5 -11 15948.7 530.617 6 4 5 -11 14906.8 830.320 2 -4 5 11 16726.2 522.914 14 -4 5 11 15276.2 784.819 11 4 -5 11 14787.4 462.312 10 4 -5 11 15893.8 535.713 8 4 5 -11 14622.6 579.120 9 4 5 -10 5777.85 316.304 6 4 5 -10 5356.68 322.727 4 4 5 -10 5396.94 486.549 2 -4 5 10 5351.62 279.852 14 -4 5 10 5280.07 454.161 11 4 -5 10 5347.28 275.068 10 4 -5 10 5593.61 307.753 8 4 5 -10 4969.16 329.658 9 4 5 -9 12985.1 476.927 6 4 5 -9 12004.5 481.521 4 4 5 -9 12019.4 706.380 2 -4 5 9 11841.0 671.885 11 -4 5 9 12907.7 426.810 14 4 -5 9 12359.5 450.982 8 4 -5 9 12554.9 428.235 10 4 5 -9 12027.7 507.515 9 4 5 -8 5440.12 304.116 6 4 5 -8 5462.92 313.491 4 4 5 -8 5285.59 445.472 2 -4 5 8 5560.62 447.675 11 -4 5 8 5503.61 267.706 14 4 -5 8 5157.09 266.906 10 4 5 -8 4867.77 307.502 9 4 5 -7 9150.62 390.310 6 4 5 -7 8746.16 379.953 4 4 5 -7 8562.79 546.306 2 -4 5 7 8793.37 466.833 12 -4 5 7 9327.57 344.917 14 -4 5 7 9350.96 565.158 11 4 -5 7 9333.56 355.891 10 4 5 -7 8391.55 391.408 9 4 5 -6 5409.87 414.743 2 4 -5 6 5288.16 306.522 3 -4 5 6 5600.39 422.029 11 -4 5 6 5091.00 344.967 12 4 5 -5 31989.3 991.764 2 4 -5 5 31801.8 767.305 3 -4 5 5 31088.7 862.408 12 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198.033 10 4 6 -13 3634.75 286.262 9 4 6 -12 8562.01 424.185 4 4 6 -12 9506.57 392.693 6 4 -6 12 8487.32 340.943 10 4 6 -12 8572.71 445.658 9 4 6 -11 24186.0 672.473 6 4 6 -11 22659.4 714.050 4 4 -6 11 22544.0 595.314 10 4 6 -11 24200.5 765.528 9 4 6 -10 27368.9 726.709 6 4 6 -10 25529.5 749.633 4 4 6 -10 26254.0 1094.31 2 -4 6 10 28355.0 684.126 14 -4 6 10 25665.8 1050.04 11 4 -6 10 25592.3 644.426 10 4 6 -10 25708.6 788.462 9 4 6 -9 35063.1 837.007 6 4 6 -9 32122.9 839.340 4 4 6 -9 33600.1 1221.51 2 -4 6 9 34779.8 758.146 14 -4 6 9 31380.7 1155.71 11 4 -6 9 33836.8 757.141 10 4 6 -9 34818.8 911.416 9 4 6 -8 5702.01 329.712 4 4 6 -8 5970.49 329.576 6 4 6 -8 5837.90 477.679 2 -4 6 8 6169.54 297.854 14 -4 6 8 5904.78 486.008 11 4 -6 8 5809.97 292.775 10 4 6 -8 5646.49 348.141 9 4 6 -7 2023.80 187.021 4 4 6 -7 2357.46 202.673 6 4 6 -7 2847.94 327.544 2 4 -6 7 2593.95 236.689 3 -4 6 7 2552.45 186.880 14 -4 6 7 2098.28 280.188 11 4 -6 7 2409.17 187.705 10 4 6 -7 2209.85 208.792 9 4 6 -6 13890.0 486.491 4 4 6 -6 14836.6 511.811 6 4 6 -6 14139.9 704.262 2 -4 6 6 15093.1 457.562 14 -4 6 6 14258.3 614.464 12 -4 6 6 14514.5 724.795 11 4 -6 6 15014.7 465.100 10 4 6 -6 13424.1 506.545 9 4 6 -5 6048.21 311.834 6 4 6 -5 5933.54 430.042 2 4 -6 5 5342.70 324.996 3 -4 6 5 5433.45 366.367 12 -4 6 5 5806.60 272.904 14 -4 6 5 5984.14 445.861 11 4 -6 5 6454.83 289.126 10 4 6 -5 5235.33 296.896 9 4 6 -4 24875.2 857.997 2 4 -6 4 24491.4 708.714 3 -4 6 4 24530.8 783.241 12 -4 6 4 26215.9 923.110 11 4 6 -3 17324.3 681.615 2 4 -6 3 17374.4 590.158 3 -4 6 3 17112.0 640.489 12 -4 6 3 19285.1 761.571 11 4 6 -2 14140.0 600.034 2 4 -6 2 13868.8 527.722 3 -4 6 2 12784.7 549.390 12 -4 6 2 14419.2 643.628 11 4 -6 1 124381. 1876.78 3 -4 6 1 120514. 1937.51 12 -4 6 1 127310. 2084.66 11 4 -6 0 134975. 1974.40 3 -4 -6 0 135411. 1784.09 11 -4 6 0 129556. 2038.81 12 4 -6 -1 122109. 1901.13 3 -4 6 -1 121034. 1985.77 12 4 6 1 121021. 1827.28 13 4 6 2 12245.7 531.379 2 4 -6 -2 13912.5 568.466 3 -4 -6 2 15640.3 537.465 11 -4 6 -2 12804.5 573.249 12 4 6 2 14720.8 555.502 13 4 6 3 15901.9 603.816 2 4 -6 -3 17803.3 644.485 3 -4 6 -3 16653.8 657.724 1 -4 -6 3 19148.5 626.952 11 -4 6 -3 17047.1 679.884 12 4 6 3 17575.7 634.218 13 4 -6 -4 24482.9 784.380 3 -4 6 -4 24730.6 820.246 1 -4 6 -4 24473.0 849.799 12 4 6 4 25094.8 792.195 13 4 -6 -5 5383.09 236.869 4 4 -6 -5 5475.76 376.647 3 -4 6 -5 5834.52 393.176 1 -4 -6 5 6346.67 378.281 11 -4 6 -5 5544.79 404.793 12 4 6 5 5431.85 377.777 13 4 6 5 5434.48 268.425 7 -4 -6 6 15505.2 617.671 11 -4 6 -6 13456.6 658.705 12 4 6 6 13725.7 620.841 13 4 -6 -6 14738.9 413.856 4 4 -6 -6 13950.6 635.337 3 -4 6 -6 14534.9 651.926 1 -4 -6 7 2446.44 254.036 11 -4 6 -7 2180.21 274.652 12 4 6 7 2223.89 260.346 13 -4 6 -7 2408.24 266.374 1 4 -6 -7 2412.57 169.707 4 4 -6 -7 2483.58 274.772 3 -4 -6 8 6306.34 418.656 11 -4 6 -8 5649.24 449.305 12 4 6 8 5651.11 431.892 13 -4 6 -8 6213.65 449.386 1 4 -6 -8 6028.91 273.907 4 4 -6 -8 6243.66 461.856 3 -4 -6 9 36731.3 1064.41 11 -4 6 -9 31916.4 1134.07 12 4 6 9 32403.7 1100.32 13 -4 6 -9 36803.9 1140.36 1 4 -6 -9 34540.6 718.084 4 4 -6 -9 35846.4 1184.27 3 -4 6 -10 28256.9 744.758 5 -4 6 -10 25764.1 1033.54 12 -4 -6 10 29322.3 970.841 11 4 6 10 25056.7 992.550 13 4 -6 -10 26513.1 630.960 4 -4 6 -10 29500.7 1034.19 1 4 -6 -10 26073.7 1042.35 3 4 -6 -11 24315.7 613.137 4 -4 6 -11 25262.8 718.460 5 4 -6 -12 9200.42 367.069 4 -4 6 -12 9581.15 436.202 5 4 -6 -13 3680.76 230.412 4 -4 6 -13 3962.04 274.909 5 4 -6 -14 960.149 119.913 4 -4 6 -14 1003.43 137.949 5 -4 6 -15 4155.27 264.020 5 4 -6 -15 3952.11 229.332 4 4 -6 -16 3539.40 205.757 4 -4 6 -16 3602.02 230.206 5 -4 6 -17 2712.37 179.495 5 4 -6 -17 2833.53 169.992 4 -4 6 -18 2179.76 137.605 5 4 -6 -18 2211.16 131.093 4 4 7 -18 1420.96 112.192 9 4 7 -17 607.628 89.7689 9 -4 7 16 409.454 66.3055 14 4 7 -16 431.057 92.1000 9 -4 7 15 3549.35 201.686 14 4 7 -15 3961.54 265.088 9 -4 7 14 10111.9 366.274 14 4 -7 14 9290.39 311.635 10 4 7 -14 9953.53 447.379 9 -4 7 13 6241.12 316.914 14 4 -7 13 5023.88 246.056 10 4 7 -13 5667.19 349.818 9 4 7 -12 19551.9 559.907 6 4 7 -12 18814.6 668.896 9 4 7 -11 16785.2 545.516 6 4 -7 11 16094.8 497.958 10 4 7 -11 15937.3 623.631 9 4 7 -10 13279.7 497.022 6 -4 7 10 13079.9 465.521 14 4 -7 10 12184.7 440.301 10 4 7 -10 11893.2 536.697 9 4 7 -9 32135.7 810.227 6 4 7 -9 31016.3 1184.56 2 -4 7 9 30677.3 727.121 14 -4 7 9 28634.1 1130.12 11 4 -7 9 29546.0 714.169 10 4 7 -9 30483.4 870.651 9 4 7 -8 45021.0 980.693 6 4 7 -8 41473.4 1356.84 2 -4 7 8 44369.5 884.181 14 -4 7 8 41109.0 1359.41 11 4 -7 8 43480.2 891.043 10 4 7 -8 43374.2 1042.46 9 4 7 -7 6995.79 339.655 5 4 7 -7 6712.37 355.274 6 4 7 -7 6578.01 509.865 2 4 -7 7 6617.99 405.430 3 -4 7 7 7041.14 322.535 14 -4 7 7 6801.07 532.784 11 4 -7 7 6620.86 319.066 10 4 7 -7 6769.98 377.336 9 4 7 -6 5078.70 285.113 5 4 7 -6 5508.58 312.878 6 4 7 -6 5394.65 436.802 2 4 -7 6 5008.76 342.283 3 -4 7 6 4868.78 378.119 12 -4 7 6 5396.69 276.117 14 -4 7 6 5497.37 461.076 11 4 -7 6 5641.44 290.592 10 4 7 -6 5033.08 318.478 9 4 7 -5 23550.2 619.738 5 4 7 -5 24655.9 684.470 6 4 7 -5 22894.6 884.475 2 4 -7 5 23451.6 751.692 3 -4 7 5 23664.9 821.624 12 -4 7 5 24535.4 613.613 14 -4 7 5 25082.8 986.981 11 4 -7 5 26303.1 630.964 10 4 7 -5 23610.8 682.468 9 4 7 -4 13756.5 490.339 6 4 7 -4 12574.8 625.657 2 4 -7 4 13636.2 563.975 3 -4 7 4 13158.5 436.515 14 -4 7 4 13497.8 603.721 12 -4 7 4 15067.2 740.089 11 4 -7 4 15561.1 465.689 10 4 7 -4 13189.7 481.829 9 4 7 -3 3111.77 219.899 6 4 7 -3 3455.05 313.553 2 4 -7 3 3101.13 267.197 3 -4 7 3 2794.30 269.333 12 -4 7 3 3083.32 203.666 14 -4 7 3 3198.05 333.909 11 4 -7 3 3152.44 201.468 10 4 7 -3 3156.27 223.142 9 4 7 -2 1836.86 165.885 6 4 7 -2 1980.74 232.884 2 4 -7 2 1799.70 203.937 3 -4 7 2 1979.99 226.088 12 -4 7 2 1939.45 161.302 14 4 7 -2 1761.66 163.602 9 4 -7 2 2110.40 159.339 10 4 7 -1 20424.8 567.286 6 4 7 -1 19743.6 720.779 2 4 -7 1 20772.4 712.286 3 -4 7 1 19484.3 725.199 12 -4 7 1 21353.6 562.917 14 4 7 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24905.5 558.248 4 4 -7 -5 23843.6 856.176 3 -4 7 -5 22366.7 820.849 1 -4 -7 6 5677.49 383.271 11 -4 7 -6 4911.40 406.047 12 4 7 6 5125.50 386.562 13 4 -7 -6 5437.83 253.243 4 4 -7 -6 5100.42 403.981 3 -4 7 -6 5188.13 394.814 1 -4 -7 7 7363.00 450.426 11 -4 7 -7 6685.53 489.091 12 4 7 7 6518.99 452.128 13 -4 7 -7 6322.18 449.615 1 4 -7 -7 7034.15 294.355 4 4 -7 -7 6977.55 492.471 3 -4 7 -8 40575.5 1275.73 12 4 7 8 40419.1 1215.86 13 -4 7 -8 44043.6 1261.57 1 4 -7 -8 42695.9 814.248 4 4 -7 -8 42186.5 1297.63 3 -4 7 -9 29343.1 1097.70 12 4 -7 -9 30651.5 680.399 4 4 -7 -9 29468.1 1102.20 3 -4 7 -9 31721.5 1072.44 1 4 -7 -10 12660.8 429.781 4 -4 7 -10 13546.1 505.778 5 4 -7 -11 17328.4 509.357 4 -4 7 -11 16376.8 571.383 5 4 -7 -12 19773.8 550.246 4 -4 7 -12 19574.2 624.819 5 4 -7 -13 5693.83 281.543 4 -4 7 -13 5967.46 332.688 5 4 -7 -14 9779.77 361.545 4 -4 7 -14 10075.1 414.227 5 -4 7 -15 3729.81 236.741 5 4 -7 -15 3895.45 217.421 4 4 -7 -16 557.685 85.7825 4 -4 7 -16 474.931 85.1359 5 4 -7 -17 570.846 73.1396 4 -4 7 -17 651.560 81.7389 5 4 8 -17 1714.39 127.066 9 -4 8 16 727.640 78.6096 14 4 8 -16 801.606 104.148 9 -4 8 15 556.044 78.7550 14 4 8 -15 647.094 105.855 9 -4 8 14 2038.55 162.446 14 4 -8 14 1705.19 126.758 10 4 8 -14 1896.14 183.844 9 -4 8 13 378.355 86.5612 14 4 8 -13 319.232 91.7862 9 4 -8 13 155.028 42.6450 10 4 8 -12 1088.74 159.117 9 4 -8 12 958.076 114.834 10 4 8 -11 1908.36 178.722 5 4 8 -11 2007.99 182.192 6 -4 8 11 2161.08 196.842 14 4 -8 11 1743.18 157.997 10 4 8 -11 1750.29 201.333 9 4 8 -10 21564.1 627.084 5 4 8 -10 21911.7 640.765 6 -4 8 10 22861.6 622.311 14 4 8 -10 20972.6 718.242 9 4 8 -9 8967.64 401.269 5 4 8 -9 9711.50 429.316 6 -4 8 9 9112.71 385.115 14 4 -8 9 8522.80 369.819 10 4 8 -9 8640.70 458.036 9 4 8 -8 1961.67 190.235 5 4 8 -8 2258.25 213.143 6 -4 8 8 1779.81 168.224 14 4 -8 8 1868.92 180.439 10 4 8 -8 1678.42 199.458 9 4 8 -7 12093.9 466.863 5 4 8 -7 12679.2 504.161 6 4 8 -7 12506.6 700.537 2 4 -8 7 11831.1 567.897 3 -4 8 7 11984.3 437.963 14 4 -8 7 12890.1 457.745 10 4 8 -7 11427.3 510.888 9 4 8 -6 22163.8 638.461 5 4 8 -6 22262.6 673.389 6 4 8 -6 22027.2 911.882 2 4 -8 6 21952.5 766.811 3 -4 8 6 22124.4 598.887 14 4 -8 6 23624.0 625.419 10 4 8 -6 21723.3 696.685 9 4 8 -5 2776.34 212.596 5 4 8 -5 2871.43 234.285 6 4 8 -5 2807.55 307.395 2 4 -8 5 2755.93 266.801 3 -4 8 5 2884.72 300.224 12 -4 8 5 2696.17 199.796 14 4 -8 5 3097.14 217.006 10 4 8 -5 2452.63 221.091 9 4 8 -4 3094.93 221.311 5 4 8 -4 3334.54 246.938 6 4 8 -4 3301.88 325.306 2 4 -8 4 3199.61 288.457 3 -4 8 4 3437.03 314.047 12 -4 8 4 3402.77 225.314 14 4 -8 4 3657.63 229.863 10 4 8 -4 3154.59 239.832 9 4 8 -3 23701.1 622.428 5 4 8 -3 25012.7 685.446 6 4 8 -3 22841.8 842.265 2 4 -8 3 24593.1 817.878 3 -4 8 3 24484.0 862.781 12 -4 8 3 24872.8 630.100 14 4 -8 3 25911.1 624.756 10 4 8 -3 24348.1 684.085 9 4 8 -2 37557.3 794.571 5 4 8 -2 37480.9 848.229 6 4 8 -2 36078.5 1053.00 2 4 -8 2 38067.5 1041.88 3 -4 8 2 37925.1 1080.99 12 -4 8 2 37192.0 802.068 14 4 -8 2 40575.1 787.921 10 4 8 -2 37206.8 850.870 9 4 8 -1 8477.44 347.755 5 4 8 -1 9274.31 389.956 6 4 8 -1 8024.64 470.305 2 4 -8 1 9455.31 510.580 3 -4 8 1 9001.32 506.107 12 -4 8 1 9258.31 374.796 14 4 -8 1 9309.69 346.934 10 4 8 -1 8790.42 386.057 9 4 8 0 97454.5 1422.84 5 4 8 0 98712.8 1488.08 6 4 8 0 93828.8 1786.82 2 4 -8 0 102177. 1868.01 3 -4 8 0 98423.5 1871.41 12 -4 8 0 100265. 1487.90 14 4 -8 0 103432. 1396.65 10 4 8 0 100008. 1501.25 9 4 8 1 9197.29 354.914 5 4 8 1 9319.47 377.578 6 4 8 1 8455.99 472.054 2 4 -8 -1 9174.02 513.032 3 -4 8 -1 9434.35 527.070 12 -4 8 -1 8592.81 372.280 14 4 -8 -1 9850.28 343.875 10 4 8 2 39561.1 787.399 5 4 8 2 38061.0 795.283 6 -4 -8 2 39557.3 979.448 11 -4 8 -2 37625.3 1088.52 12 -4 8 -2 37576.0 837.619 14 4 8 2 36661.8 1012.12 2 4 -8 -2 38420.5 1106.09 3 -4 8 -2 37080.9 1087.14 1 4 8 3 24971.5 614.228 6 -4 -8 3 26484.2 809.621 11 -4 8 -3 23811.2 868.270 12 -4 8 -3 23597.2 656.359 14 4 -8 -3 24479.8 552.912 4 4 -8 -3 25210.7 910.371 3 -4 8 -3 23264.1 853.749 1 4 8 4 3210.53 208.478 6 -4 -8 4 3638.16 299.299 11 -4 8 -4 3401.28 330.409 12 -4 8 -4 3188.77 230.091 14 4 -8 -4 3561.81 202.968 4 4 -8 -4 3613.36 347.137 3 -4 8 -4 2927.37 297.428 1 4 8 5 2801.37 192.070 6 -4 -8 5 2966.53 276.872 11 -4 8 -5 3080.11 322.487 12 4 -8 -5 2863.47 186.972 4 4 -8 -5 2477.08 292.123 3 -4 8 -5 2917.35 304.016 1 4 8 6 22102.2 545.778 6 -4 -8 6 22595.1 800.213 11 -4 8 -6 21542.7 881.413 12 4 -8 -6 22469.6 553.136 4 4 -8 -6 20183.1 848.382 3 -4 8 -6 21931.8 849.002 1 -4 8 -7 12161.3 675.943 12 -4 -8 7 12891.1 606.784 11 4 8 7 11173.0 600.000 13 4 -8 -7 12318.9 408.092 4 -4 8 -7 12252.8 640.615 1 4 -8 -7 11153.0 650.451 3 4 -8 -8 1631.08 152.187 4 4 -8 -9 9055.89 359.119 4 -4 8 -10 21272.4 633.109 5 4 -8 -10 21977.9 573.390 4 -4 8 -11 2055.81 195.847 5 4 -8 -11 1962.78 171.761 4 -4 8 -12 1053.51 139.289 5 4 -8 -12 1241.57 132.162 4 -4 8 -13 304.951 81.0186 5 4 -8 -13 324.764 71.5109 4 -4 8 -14 1824.28 164.595 5 4 -8 -14 1975.55 152.768 4 -4 8 -15 575.921 89.3006 5 4 -8 -15 609.900 89.1809 4 4 -8 -16 799.301 93.5369 4 -4 8 -16 645.784 81.3555 5 -4 8 -16 666.132 77.9933 14 4 -8 -17 1579.88 102.361 4 -4 9 16-1.60187 28.2122 14 4 9 -16 40.3127 31.0386 9 -4 9 15 1088.48 98.9254 14 4 -9 15 1123.94 83.0939 10 4 9 -15 1111.81 121.147 9 -4 9 14 10956.9 340.055 14 4 -9 14 9861.97 294.205 10 4 9 -14 10777.1 408.227 9 -4 9 13 1521.34 142.352 14 4 -9 13 1283.26 111.830 10 4 9 -13 1531.08 166.056 9 4 9 -12 412.087 86.2021 5 -4 9 12 287.078 83.5146 14 4 9 -12 317.426 96.1916 9 4 -9 12 229.821 54.8946 10 4 9 -11 3637.39 234.041 5 4 9 -11 3536.54 222.648 6 4 -9 11 3412.75 215.124 10 4 9 -11 3229.17 265.033 9 4 9 -10 4087.23 259.987 5 4 9 -10 4701.80 277.383 6 -4 9 10 4393.06 264.847 14 4 -9 10 3837.87 239.877 10 4 9 -10 4299.49 311.999 9 4 9 -9 1106.10 146.735 5 4 9 -9 1453.11 171.891 6 -4 9 9 1221.17 147.550 14 4 9 -9 1065.63 154.384 9 4 -9 9 1337.44 150.041 10 4 9 -8 9594.26 420.842 5 4 9 -8 10314.5 443.667 6 -4 9 8 9666.82 396.162 14 4 -9 8 9339.95 388.827 10 4 9 -8 8999.64 459.691 9 4 9 -7 22261.1 656.409 5 4 9 -7 23479.8 696.630 6 -4 9 7 21808.4 607.072 14 4 -9 7 23017.4 626.390 10 4 9 -7 22106.8 727.532 9 4 9 -6 1884.69 188.374 5 4 9 -6 2018.71 204.175 6 -4 9 6 2019.03 180.435 14 4 -9 6 2150.70 186.685 10 4 9 -6 1844.94 201.190 9 4 9 -5 5694.28 317.296 5 4 9 -5 6099.50 348.761 6 4 -9 5 5703.86 396.894 3 -4 9 5 5426.77 290.559 14 4 -9 5 6282.50 315.502 10 4 9 -5 5347.39 337.872 9 4 9 -4 17834.6 563.702 5 4 9 -4 18410.3 605.478 6 4 -9 4 18213.4 726.178 3 -4 9 4 19180.5 791.890 12 -4 9 4 17846.3 541.083 14 4 -9 4 19449.5 555.140 10 4 9 -4 17664.7 612.756 9 4 9 -3 13401.6 478.882 5 4 9 -3 14373.9 525.358 6 4 -9 3 13296.6 625.391 3 -4 9 3 13872.3 664.236 12 -4 9 3 13747.7 470.188 14 4 -9 3 14928.7 475.283 10 4 9 -3 13430.9 519.731 9 4 9 -2 8694.18 373.410 5 4 9 -2 8862.49 407.455 6 4 -9 2 8901.29 515.209 3 -4 9 2 9160.46 540.538 12 -4 9 2 9122.47 380.831 14 4 -9 2 9504.92 372.306 10 4 9 -2 10592.6 443.949 9 4 9 -1 77173.0 1256.36 5 4 9 -1 73801.0 1298.12 6 4 -9 1 78534.5 1649.81 3 -4 9 1 76253.8 1668.75 12 -4 9 1 76739.4 1266.96 14 4 -9 1 80702.9 1217.87 10 4 9 -1 74627.2 1313.32 9 4 9 0 391.532 93.0781 5 4 9 0 862.866 133.960 6 4 -9 0 464.075 142.024 3 -4 9 0 210.319 108.333 12 -4 9 0 621.963 120.194 14 4 -9 0 568.411 101.324 10 4 9 1 75879.5 1225.37 5 4 9 1 76916.6 1271.19 6 -4 9 -1 76411.3 1663.60 12 -4 9 -1 75186.1 1280.41 14 4 -9 -1 77198.8 1680.72 3 -4 9 -1 74723.5 1659.44 1 4 9 2 9291.89 373.140 5 4 9 2 8932.54 378.360 6 -4 9 -2 8761.44 533.529 12 -4 9 -2 8776.96 390.907 14 4 -9 -2 9020.37 546.696 3 -4 9 -2 8671.79 523.477 1 4 9 3 14152.3 468.263 6 -4 9 -3 13454.6 668.488 12 -4 -9 3 14159.1 598.082 11 -4 9 -3 13124.3 490.625 14 4 -9 -3 13824.5 418.427 4 4 -9 -3 14012.2 702.044 3 -4 9 -3 12510.3 635.055 1 4 9 4 17960.2 523.433 6 -4 9 -4 18026.7 787.307 12 -4 -9 4 17940.9 687.647 11 -4 9 -4 17171.3 571.670 14 4 -9 -4 18233.9 491.138 4 4 -9 -4 18533.6 823.235 3 -4 9 -4 16798.6 733.978 1 4 9 5 5556.47 277.584 6 -4 -9 5 5712.88 393.205 11 -4 9 -5 5452.07 320.693 14 4 -9 -5 5815.66 273.486 4 4 -9 -5 5707.35 467.215 3 -4 9 -5 5262.46 408.152 1 4 9 6 1899.82 159.450 6 -4 9 -6 1536.28 169.859 14 4 -9 -6 1970.42 165.090 4 4 9 7 22525.8 538.304 6 4 -9 -7 23149.2 577.174 4 -4 9 -8 9311.07 430.600 14 4 -9 -8 9619.86 364.190 4 4 -9 -9 1307.45 144.414 4 4 -9 -10 4632.55 250.618 4 -4 9 -11 3334.33 227.306 5 4 -9 -11 3859.37 230.499 4 -4 9 -12 303.735 69.2570 5 4 -9 -12 386.582 78.9702 4 -4 9 -13 1457.03 140.699 5 -4 9 -13 1570.53 150.202 14 4 -9 -13 1418.76 131.764 4 -4 9 -14 10296.3 344.516 5 -4 9 -14 11036.4 354.966 14 4 -9 -14 10807.8 339.727 4 4 -9 -15 1236.30 107.614 4 -4 9 -15 1027.24 94.6693 5 4 -9 -16 41.6829 34.1712 4 -4 10 15 1033.09 83.8210 14 4 10 -15 925.579 93.5312 9 -4 10 14 290.679 56.7581 14 4 10 -14 246.469 63.6609 9 4 -10 14 311.746 51.6080 10 -4 10 13 9532.03 313.315 14 4 -10 13 8389.82 276.044 10 4 10 -13 9072.83 362.296 9 4 10 -12 198.444 53.7844 5 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1575.15 146.278 6 6 -8 11 1471.63 130.053 10 6 8 -11 1563.30 158.784 9 6 8 -10 1120.84 133.844 6 -6 8 10 1067.66 127.716 14 6 8 -10 1095.13 137.098 9 6 -8 10 1069.30 119.754 10 6 8 -9 1127.30 144.842 6 -6 8 9 1250.58 143.445 14 6 8 -9 1197.84 149.607 9 6 -8 9 950.956 118.692 10 6 8 -8 3514.14 254.770 6 -6 8 8 3671.04 233.763 14 6 -8 8 3457.26 228.987 10 6 8 -8 3526.08 262.178 9 6 8 -7 1905.42 197.793 6 -6 8 7 1769.22 168.073 14 6 -8 7 1435.06 154.703 10 6 8 -7 1760.66 190.743 9 6 8 -6 1315.76 162.994 6 -6 8 6 1429.04 157.518 14 6 -8 6 1533.59 160.692 10 6 8 -6 1348.16 162.367 9 6 8 -5 3678.72 268.912 6 -6 8 5 3872.32 249.873 14 6 -8 5 3829.01 249.529 10 6 8 -5 3781.85 267.474 9 6 8 -4 25592.6 736.324 6 -6 8 4 27750.4 696.081 14 6 -8 4 26824.6 670.500 10 6 8 -4 25905.9 716.700 9 6 8 -3 12321.8 494.321 6 -6 8 3 12739.1 467.015 14 6 8 -3 13386.7 472.161 7 6 -8 3 12035.3 432.143 10 6 8 -3 12168.9 470.453 9 6 -8 2 6114.18 269.685 7 6 8 -2 6398.86 348.286 6 -6 8 2 6358.94 331.987 14 6 8 -2 6748.05 338.685 7 6 -8 2 6447.96 310.930 10 6 8 -2 6665.59 339.378 9 6 -8 1 4440.98 239.258 7 6 8 -1 4640.06 288.388 6 -6 8 1 4695.60 286.919 14 6 8 -1 4292.22 275.980 7 6 -8 1 4320.01 249.895 10 6 -8 0 3859.53 230.691 7 6 8 0 3862.74 257.187 6 -6 8 0 3782.91 260.046 14 6 8 0 4261.32 280.844 7 6 -8 0 4022.83 238.484 10 6 8 1 4325.13 266.488 6 -6 8 -1 4347.95 279.161 14 6 8 1 4315.84 283.923 7 6 -8 -1 4348.29 241.944 10 6 8 2 6334.87 309.027 6 -6 8 -2 6470.13 346.099 14 6 -8 -2 6627.87 292.001 10 6 8 3 11738.6 410.866 6 -6 8 -3 11624.0 471.370 14 6 -8 -3 12920.9 384.269 4 6 8 4 25573.3 599.464 6 -6 8 -4 24398.9 706.709 14 -6 8 -5 3445.99 255.172 14 6 -8 -5 3940.67 215.527 4 -6 8 -6 1152.80 146.616 14 6 -8 -6 1239.13 125.645 4 -6 8 -7 1443.97 169.855 14 6 -8 -7 1774.51 148.705 4 -6 8 -8 3167.99 242.977 14 6 -8 -8 3541.32 210.915 4 -6 8 -9 963.125 132.588 14 6 -8 -9 1170.44 124.915 4 6 -8 -10 937.088 112.846 7 -6 8 -10 839.529 122.455 14 6 -8 -10 924.763 109.025 4 6 -8 -11 1463.17 128.797 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4400.24 259.603 7 7 2 -6 4391.90 419.722 2 -7 2 6 4024.50 379.141 11 7 -2 6 4487.63 263.588 10 7 2 -5 1401.80 242.996 2 7 2 -5 1350.97 149.038 7 7 -2 5 1244.47 121.141 7 -7 2 5 1211.97 201.391 11 7 -2 5 1496.83 152.417 10 7 -2 4 10715.6 372.024 7 7 2 -4 11766.9 437.872 7 7 2 -4 11610.9 648.271 2 -7 2 4 10730.1 587.222 11 7 -2 4 11702.3 425.146 10 7 2 -3 5595.57 304.063 7 7 -2 3 4776.19 248.603 7 7 2 -3 5972.44 321.789 6 7 2 -3 5301.26 428.871 2 -7 2 3 5469.49 399.962 11 7 -2 3 5226.66 281.421 10 7 2 -2 3037.64 223.624 7 7 -2 2 2911.31 199.818 7 7 2 -2 3118.06 225.702 6 7 2 -2 2685.08 297.479 2 -7 2 2 2718.98 268.065 12 7 -2 2 3280.75 219.328 10 7 2 -1 6565.87 312.158 6 7 2 -1 6609.83 332.099 7 7 -2 1 6789.24 312.717 7 7 2 -1 7153.65 476.358 2 -7 2 1 6040.49 396.411 12 7 -2 1 6552.82 305.883 10 7 2 0 261.712 75.6972 7 7 -2 0 341.251 77.9968 7 7 2 0 269.783 86.3711 2 -7 2 0 190.894 78.4114 12 7 -2 0 224.869 57.3401 10 7 -2 -1 6551.20 317.161 7 7 2 1 6589.15 450.670 2 -7 2 -1 6466.18 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5531.64 244.852 10 7 10 -1 1883.10 159.842 6 -7 10 1 1753.48 159.106 14 7 -10 1 1758.07 135.682 10 7 -10 0 10287.7 313.117 7 7 10 0 10865.8 376.319 6 -7 10 0 10008.3 370.510 14 7 -10 0 9834.23 314.176 10 7 -10 -1 1968.10 141.139 7 7 10 1 1940.85 150.212 6 -7 10 -1 1780.34 158.242 14 7 -10 -2 5809.18 247.069 7 7 10 2 5879.19 250.047 6 -7 10 -2 5808.13 280.008 14 7 10 3 554.727 73.9395 6 7 -10 -3 572.458 85.0083 7 -7 10 -3 428.655 80.5401 14 7 -10 -4 3723.65 198.431 7 -7 10 -4 3833.29 223.823 14 7 -10 -5 2062.17 148.980 7 -7 10 -5 2195.42 169.154 14 7 -10 -6 3347.14 183.797 7 -7 10 -6 3566.05 210.201 14 7 -10 -6 3468.22 157.384 4 7 -10 -7 4682.98 208.170 7 -7 10 -7 4656.73 230.587 14 7 -10 -7 4532.03 179.388 4 7 -10 -8 151.894 47.3904 7 -7 10 -8 187.171 58.8410 14 7 -10 -8 127.122 34.8414 4 7 -10 -9 1372.74 91.7306 4 7 -10 -9 1168.26 94.0726 7 -7 10 -9 1332.69 111.130 14 7 -10 -10 17.6455 27.0659 7 -7 10 -10 11.3333 26.3600 14 7 11 -8 1609.18 105.025 6 7 -11 8 1615.35 99.4251 10 7 11 -7 2482.41 142.187 6 -7 11 7 2520.94 144.092 14 7 -11 7 2330.25 127.938 10 7 11 -6 1321.08 113.552 6 -7 11 6 1381.16 110.494 14 7 -11 6 1149.92 96.8284 10 7 11 -5 296.588 61.2996 6 -7 11 5 381.658 67.1666 14 7 -11 5 418.033 62.2200 10 7 11 -4 127.807 49.9180 6 -7 11 4 107.315 41.3992 14 7 -11 4 212.273 48.4048 10 7 11 -3 876.848 104.179 6 -7 11 3 921.579 103.765 14 7 -11 3 788.398 86.0275 10 7 11 -2 3225.91 190.738 6 -7 11 2 3274.98 186.897 14 7 -11 2 2667.19 147.936 10 7 11 -1 538.261 82.9033 6 -7 11 1 620.868 88.9293 14 7 -11 1 536.539 67.6982 10 7 11 0 1307.98 116.856 6 -7 11 0 1279.61 123.373 14 7 11 1 636.725 81.4847 6 7 -11 -1 573.216 68.0439 7 -7 11 -1 494.102 84.6549 14 7 -11 -2 3057.07 156.060 7 7 11 2 3302.00 168.179 6 -7 11 -2 2998.75 183.501 14 7 -11 -3 826.246 84.4950 7 7 11 3 1003.25 85.2391 6 -7 11 -3 819.138 97.0772 14 7 -11 -4 180.780 42.7649 7 -7 11 -4 179.217 47.3538 14 7 -11 -5 384.494 63.4028 7 -7 11 -5 295.935 57.3958 14 7 -11 -6 1345.16 103.197 7 -7 11 -6 1204.31 104.134 14 7 -11 -7 2439.90 131.086 7 -7 11 -7 2359.28 139.167 14 7 -11 -8 1615.24 100.867 7 -7 11 -8 1630.71 105.525 14 7 12 -5 3755.44 161.001 6 -7 12 5 3904.00 165.724 14 7 12 -4 1553.20 107.595 6 -7 12 4 1444.14 103.283 14 7 12 -3 5.28460 31.6347 6 -7 12 3 4.59398 36.9433 14 7 12 -2 2939.65 155.662 6 -7 12 2 2756.65 147.921 14 7 12 -1 3219.25 161.033 6 -7 12 1 3100.48 160.186 14 7 12 0 2875.83 147.054 6 -7 12 0 2753.39 151.763 14 7 12 1 3373.20 150.477 6 -7 12 -1 3135.48 162.193 14 -7 12 -2 2786.25 150.187 14 -7 12 -3 20.4129 32.1158 14 -7 12 -4 1398.24 100.805 14 8 0 0 16169.2 532.973 7 8 0 0 15054.9 487.869 10 8 0 1 4045.85 259.702 7 8 0 -1 4032.02 268.556 7 8 0 -1 4151.86 250.889 10 8 0 1 3958.85 247.346 10 8 0 -2 4374.85 278.588 7 8 0 2 3875.86 243.401 10 8 0 2 3627.23 240.302 7 8 0 -3 4701.41 289.486 7 8 0 3 4237.47 253.779 7 8 0 3 4408.64 258.675 10 8 0 -4 5936.34 317.081 7 8 0 4 5092.26 280.707 10 8 0 4 5034.51 272.071 7 8 0 5 84.1947 47.1586 7 8 0 -5 85.3343 57.4994 7 8 0 5 78.8088 53.3665 10 8 0 -6 1386.44 156.178 7 8 0 6 1345.28 138.470 10 8 0 6 1182.47 124.274 7 8 0 7 74.6789 43.9031 7 8 0 -7 54.5493 48.3774 7 8 0 7 3.26913 46.8674 10 8 0 -8 472.229 87.7446 7 8 0 8 559.381 85.7752 10 8 0 -9 156.559 64.8126 4 8 0 -9 210.206 66.4181 7 8 0 -10 10939.7 387.084 4 8 0 -11-50.3632 57.2915 4 8 0 -12 3231.89 204.623 6 8 0 -12 3018.91 186.461 4 8 0 -13 115.042 43.1215 4 8 0 -13 33.0402 46.2174 6 8 0 -14 2744.15 157.490 6 8 0 -14 2759.12 152.712 4 8 0 -15 90.9590 30.8367 6 -8 0 15 132.340 42.0962 8 -8 1 15 6539.86 219.372 8 8 1 -14 593.387 74.3629 4 8 1 -14 522.826 73.5825 6 8 1 -13 2396.74 164.108 6 8 1 -13 2450.06 156.615 4 8 1 -12 2434.70 180.184 6 8 1 -12 2340.22 164.887 4 8 1 -11 2627.37 183.672 4 8 1 -11 2550.19 195.212 6 8 1 -10 8741.08 379.602 6 8 1 -10 8659.00 342.733 4 8 1 -9 2946.61 227.440 6 8 1 -9 3016.89 203.581 4 8 1 -9 2973.35 186.131 7 8 -1 9 2805.66 182.641 10 8 -1 8 5235.60 262.458 10 8 1 -8 5750.43 276.345 7 8 1 -7 5648.78 286.690 7 8 -1 7 5363.75 275.688 10 8 1 -6 7944.42 353.470 7 8 -1 6 8109.33 348.724 10 8 -1 6 7873.81 310.496 7 8 1 -5 4546.95 272.423 7 8 -1 5 4246.96 257.016 10 8 -1 5 3871.91 224.801 7 8 1 -4 4378.36 272.171 7 8 1 -4 4392.55 279.126 6 8 -1 4 4374.95 260.646 10 8 -1 4 4110.25 237.167 7 8 1 -3 5356.13 305.756 7 8 1 -3 5249.57 298.641 6 8 -1 3 4776.46 275.304 10 8 -1 3 4821.35 267.301 7 8 1 -2 8548.01 388.419 7 8 1 -2 8122.76 361.399 6 8 -1 2 7776.51 349.663 7 8 -1 2 7396.18 341.463 10 8 1 -1 30849.2 768.304 7 8 -1 1 29131.7 716.075 7 8 -1 1 28506.5 694.139 10 8 -1 0 2375.63 201.153 7 8 -1 0 2101.53 184.125 10 8 1 0 1921.58 191.756 7 8 -1 -1 29178.6 740.921 7 8 -1 -1 29642.1 699.437 10 8 1 1 29164.6 738.650 7 8 -1 -2 8346.74 382.575 7 8 1 2 7612.27 344.529 10 8 -1 -2 7780.44 343.215 10 8 1 2 7734.76 359.560 7 8 -1 -3 5324.72 303.854 7 8 1 3 4824.99 271.831 10 8 1 3 4708.68 272.179 7 8 -1 -4 4649.81 280.656 7 8 1 4 3868.00 240.423 10 8 1 4 4139.18 247.542 7 8 -1 -5 4668.78 277.673 7 8 1 5 4035.67 242.529 10 8 1 5 4020.84 236.345 7 8 -1 -6 7868.85 353.077 7 8 1 6 7473.23 323.945 10 8 1 6 7364.46 315.811 7 8 -1 -7 5505.90 289.570 7 8 1 7 5052.99 250.737 7 8 -1 -8 5701.76 282.520 7 8 -1 -9 2720.15 190.608 7 8 -1 -9 3108.72 202.079 4 8 -1 -10 7993.47 300.920 7 8 -1 -10 8266.73 329.479 4 8 -1 -11 2760.73 183.005 4 8 -1 -12 2321.33 160.156 4 8 -1 -13 2554.58 170.658 6 8 -1 -13 2438.84 154.087 4 8 -1 -14 520.525 71.3899 4 8 -1 -14 528.951 74.7237 6 8 -1 -15 5708.69 197.631 6 -8 -1 15 6165.52 212.622 8 8 2 -14 1896.62 128.153 6 8 2 -13 800.762 89.1334 4 8 2 -13 835.239 97.8087 6 8 2 -12 5317.98 259.422 6 8 2 -12 5265.43 245.707 4 8 2 -11 1237.46 136.393 6 8 2 -11 1234.86 124.736 4 8 2 -10 20978.7 589.327 6 8 2 -10 19688.2 530.758 4 8 -2 10 19748.4 463.851 10 8 2 -9 507.655 85.9070 4 8 2 -9 423.201 102.618 6 8 -2 9 475.308 86.3116 10 8 2 -8 9.55349 46.4040 7 8 2 -8 68.3315 70.2416 6 8 -2 8 118.424 63.3863 10 8 2 -7 22391.6 663.545 6 8 -2 7 22685.6 597.021 10 8 2 -7 22953.6 592.815 7 8 2 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157.704 7 8 -2 -6 11241.5 424.194 7 8 2 6 9832.03 372.078 7 8 -2 -7 22974.2 603.309 7 8 2 7 20699.3 534.447 7 8 2 8 130.999 55.6862 7 8 -2 -8 139.352 66.2290 7 8 -2 -9 515.337 88.6308 4 8 -2 -9 568.681 91.1133 7 8 -2 -10 18413.3 470.634 7 8 -2 -10 19278.3 505.733 4 8 -2 -11 1352.58 129.322 4 8 -2 -12 5222.53 236.644 4 8 -2 -13 779.230 89.9375 4 8 -2 -14 1884.89 130.547 6 8 -2 -14 1719.57 117.961 4 8 3 -14 1034.30 90.5152 6 -8 3 14 1256.43 97.8399 8 8 3 -13 2997.43 173.178 6 8 3 -12 201.101 62.0769 6 8 3 -11 2520.17 187.504 6 8 3 -10 5589.77 268.246 4 8 3 -10 5861.15 298.265 6 8 -3 10 5521.97 238.230 10 8 3 -9 1470.26 161.564 6 8 3 -9 1517.51 141.846 4 8 -3 9 1623.32 142.403 10 8 3 -8 18757.5 584.563 6 8 -3 8 18932.8 524.066 10 8 3 -7 1686.39 186.721 6 8 -3 7 1694.78 167.685 10 8 3 -7 1805.70 159.453 7 8 3 -6 15121.9 536.841 6 8 -3 6 14673.6 481.648 10 8 3 -6 14393.5 469.885 7 8 3 -5 3464.90 256.427 6 8 3 -5 3421.93 234.661 7 8 -3 5 3472.77 236.062 10 8 -3 5 3154.61 194.778 7 8 3 -4 4533.29 287.281 6 8 -3 4 4222.13 232.395 7 8 3 -4 4493.46 273.462 7 8 -3 4 4696.83 270.525 10 8 -3 3 26383.9 630.174 7 8 3 -3 28318.3 733.951 6 8 3 -3 29308.2 739.872 7 8 -3 3 27403.2 682.271 10 8 -3 2 7574.20 332.722 7 8 3 -2 8013.29 364.520 6 8 3 -2 7864.30 376.904 7 8 -3 2 7928.06 350.896 10 8 -3 1 3348.17 227.869 7 8 3 -1 3439.34 228.900 6 8 3 -1 3895.32 266.439 7 8 -3 1 3656.27 237.828 10 8 -3 0 2818.88 210.086 7 8 -3 0 2405.71 189.541 10 8 3 0 2503.92 209.596 7 8 -3 -1 3288.17 234.585 7 8 -3 -1 3693.05 231.590 10 8 3 1 3653.34 257.825 7 8 -3 -2 7786.55 363.717 7 -8 3 -2 8361.69 346.730 14 8 -3 -2 7929.99 340.040 10 8 3 2 8249.28 380.759 7 8 -3 -3 29070.5 730.535 7 -8 3 -3 29159.8 691.960 14 8 -3 -3 28542.5 666.624 10 8 3 3 28184.1 717.666 7 8 -3 -4 4380.97 274.780 7 -8 3 -4 4564.85 262.203 14 8 3 4 4348.09 261.639 7 8 -3 -4 4250.59 239.743 10 8 -3 -5 3114.89 223.873 7 -8 3 -5 3145.71 222.925 14 8 3 5 3836.09 240.861 7 8 -3 -6 15090.9 493.531 7 -8 3 -6 14881.3 499.621 14 8 3 6 14016.7 452.834 7 8 -3 -7 1735.26 164.678 7 8 3 7 1608.55 150.669 7 8 -3 -8 18028.8 510.857 7 8 3 8 18462.1 478.292 7 8 -3 -9 1493.69 144.044 7 8 -3 -9 1387.28 130.551 4 8 -3 -10 5278.69 241.877 7 8 -3 -10 5390.39 251.259 4 8 -3 -11 2466.01 164.580 4 8 -3 -11 2546.10 153.197 7 8 -3 -12 143.359 47.2154 4 8 -3 -13 2822.64 156.535 4 8 -3 -14 1000.30 85.5832 4 -8 3 -14 1045.53 89.8000 14 -8 -3 14 1095.12 94.6547 8 8 4 -13 5959.86 231.615 6 8 4 -12 450.259 71.6633 6 8 4 -11 1750.98 150.562 6 8 -4 11 1790.36 118.046 10 8 4 -10 7820.14 339.605 6 8 -4 10 8318.08 292.418 10 8 4 -9 15103.9 498.298 6 8 -4 9 14394.1 426.049 10 8 4 -8 1314.38 150.012 6 8 -4 8 1305.97 135.847 10 8 4 -7 1066.44 143.839 6 8 4 -7 1048.14 118.980 7 8 -4 7 1259.28 140.010 10 8 4 -6 13435.0 503.728 6 8 -4 6 13133.4 451.771 10 8 4 -6 14359.8 455.264 7 8 4 -5 11012.9 453.128 6 8 -4 5 10187.7 398.876 10 8 4 -5 11015.0 410.566 7 8 -4 4 6456.31 281.031 7 8 4 -4 6999.64 357.870 6 8 -4 4 6450.24 318.525 10 8 4 -4 6767.61 331.812 7 8 -4 3 12414.9 407.769 7 8 4 -3 12869.3 481.325 6 8 -4 3 12489.8 447.323 10 8 4 -3 13314.2 479.435 7 8 -4 2 8430.89 347.145 7 8 4 -2 9020.97 393.013 6 8 -4 2 8851.00 370.305 10 8 4 -2 9259.27 406.440 7 8 -4 1 34733.0 768.174 7 8 4 -1 35093.7 788.130 6 8 -4 1 35467.3 777.818 10 8 4 -1 37078.2 859.895 7 8 -4 0 1039.33 138.407 7 8 4 0 977.335 119.204 6 8 4 0 983.482 148.094 7 -8 4 0 1049.74 124.354 14 8 -4 0 1075.02 136.030 10 8 -4 -1 37270.3 823.317 7 -8 4 -1 37859.4 796.115 14 8 -4 -1 36738.5 779.004 10 8 4 1 37788.2 870.055 7 8 -4 -2 8640.41 380.176 7 -8 4 -2 9118.83 373.597 14 8 4 2 9071.51 402.128 7 8 -4 -2 9153.15 358.121 10 8 -4 -3 12907.5 472.223 7 -8 4 -3 13668.8 469.483 14 8 -4 -3 13066.9 427.258 10 8 4 3 13333.2 482.784 7 8 -4 -4 6987.93 340.692 7 -8 4 -4 6944.52 332.501 14 8 -4 -4 6656.20 295.701 10 8 4 4 7021.41 337.613 7 8 -4 -5 11187.5 424.809 7 -8 4 -5 10554.6 419.372 14 8 4 5 10247.8 397.814 7 8 -4 -6 14483.8 478.215 7 -8 4 -6 14308.9 493.709 14 8 4 6 13109.1 441.867 7 8 -4 -7 1140.05 130.603 7 -8 4 -7 1095.86 139.327 14 8 4 7 1063.87 128.033 7 8 -4 -8 1051.63 115.796 7 -8 4 -8 1250.71 142.907 14 8 -4 -9 13690.4 413.773 7 8 -4 -9 14688.7 414.988 4 8 -4 -10 7585.90 287.914 7 8 -4 -10 8087.57 296.324 4 8 -4 -11 1685.63 122.530 7 8 -4 -11 1704.24 128.898 4 8 -4 -12 528.622 74.2598 4 8 -4 -13 5575.32 207.591 4 -8 4 -13 5610.50 229.224 14 -8 4 -14 124.365 37.5417 14 8 5 -13 281.998 50.8067 6 8 5 -12 31.4677 37.0473 6 8 5 -11 762.771 97.6835 6 8 -5 11 801.862 79.7895 10 8 5 -10 56.1785 54.9949 6 8 -5 10 171.467 51.7423 10 8 5 -9 821.423 117.558 6 8 -5 9 889.015 106.835 10 8 5 -8 2671.36 207.254 6 8 -5 8 2678.61 186.319 10 8 5 -7 13222.4 485.847 6 8 -5 7 13430.4 439.771 10 8 5 -6 580.282 92.9456 7 8 5 -6 500.546 102.193 6 8 -5 6 545.225 104.041 10 8 5 -5 97.5657 47.9964 7 8 5 -5-26.9815 73.8557 6 -8 5 5 47.0803 42.7625 14 8 -5 5 31.1064 63.3599 10 8 5 -4 1022.86 132.995 7 8 5 -4 923.533 131.013 6 -8 5 4 914.355 107.657 14 8 -5 4 850.322 113.452 10 8 -5 3 3861.50 218.789 7 8 5 -3 4577.23 282.249 6 -8 5 3 4645.74 246.003 14 8 5 -3 4344.84 267.657 7 8 -5 3 4502.64 260.233 10 8 -5 2 9106.11 347.487 7 8 5 -2 8806.76 384.404 6 -8 5 2 9588.65 362.960 14 8 5 -2 9243.11 401.523 7 8 -5 2 9384.31 376.025 10 8 5 -1 756.052 115.112 6 8 5 -1 686.130 120.361 7 8 -5 1 746.898 110.632 7 -8 5 1 643.836 105.937 14 8 -5 1 679.824 113.222 10 8 5 0 760.633 103.944 6 8 5 0 863.457 132.934 7 8 -5 0 706.746 111.330 7 -8 5 0 849.676 120.767 14 8 -5 0 834.196 114.926 10 8 5 1 717.126 131.538 7 8 -5 -1 619.483 105.979 7 -8 5 -1 758.265 116.602 14 8 -5 -1 661.019 105.797 10 8 -5 -2 9552.98 390.272 7 -8 5 -2 9522.52 384.442 14 8 -5 -2 8909.03 348.365 10 8 5 2 8939.05 396.089 7 8 -5 -3 4412.89 267.780 7 -8 5 -3 4623.05 271.722 14 8 -5 -3 4262.44 232.010 10 8 5 3 4513.07 274.886 7 8 5 4 994.285 130.479 7 8 -5 -4 777.642 115.335 7 -8 5 -4 916.795 124.230 14 8 -5 -4 793.317 99.8353 10 8 5 5 68.5111 60.9288 7 8 -5 -5 28.3988 62.2614 7 -8 5 -5-119.141 83.5016 14 8 5 6 592.606 101.314 7 8 -5 -6 609.601 103.372 7 -8 5 -6 545.734 92.9620 14 8 -5 -7 12363.4 418.528 7 -8 5 -7 12701.3 457.757 14 8 -5 -8 2519.17 178.686 7 -8 5 -8 2538.07 199.261 14 8 -5 -9 703.793 93.8690 7 -8 5 -9 732.912 108.636 14 8 -5 -9 758.314 87.9991 4 8 -5 -10 129.612 45.7766 7 -8 5 -10 114.696 44.5587 14 8 -5 -10 211.461 53.3801 4 8 -5 -11 738.469 80.5442 7 -8 5 -11 703.702 92.4110 14 8 -5 -11 664.626 76.5653 4 8 -5 -12 53.2282 30.8172 7 -8 5 -12 5.04416 39.8622 14 8 -5 -12-17.8019 34.1566 4 -8 5 -13 189.883 44.1842 14 8 -5 -13 239.387 44.8421 4 8 6 -12 2236.49 135.419 6 8 6 -11 2469.20 159.568 6 8 -6 11 2344.43 125.893 10 8 6 -10 530.324 83.8531 6 8 -6 10 567.847 75.2008 10 8 6 -9 365.312 82.6015 6 8 -6 9 284.421 68.9421 10 8 6 -8 4145.05 251.114 6 8 -6 8 3789.06 212.543 10 8 6 -7 6275.39 321.817 6 -8 6 7 6475.42 260.968 14 8 -6 7 6703.55 296.442 10 8 6 -6 2959.30 229.922 6 -8 6 6 3094.50 184.365 14 8 -6 6 2982.05 205.897 10 8 6 -5 9112.39 398.910 6 -8 6 5 9067.79 329.265 14 8 -6 5 8848.67 358.083 10 8 6 -5 8491.70 330.814 7 8 6 -4 6033.15 324.236 6 -8 6 4 6049.31 275.565 14 8 -6 4 5798.16 288.423 10 8 6 -4 5691.94 282.854 7 8 -6 3 14935.5 415.032 7 8 6 -3 15107.9 513.400 6 -8 6 3 14940.3 451.960 14 8 -6 3 15395.1 474.894 10 8 6 -3 14885.6 484.387 7 8 -6 2 3758.85 212.170 7 8 6 -2 3504.34 241.257 6 -8 6 2 3906.88 231.125 14 8 -6 2 3374.80 217.465 10 8 6 -2 3673.84 244.891 7 8 -6 1 6987.56 302.216 7 8 6 -1 6710.01 320.192 6 -8 6 1 7607.05 329.582 14 8 -6 1 6803.08 306.901 10 8 6 -1 6855.11 342.589 7 8 -6 0 37298.7 772.507 7 8 6 0 36221.3 767.922 6 -8 6 0 39145.5 808.272 14 8 -6 0 36967.8 761.927 10 8 6 0 39430.9 864.196 7 8 -6 -1 7049.19 321.384 7 -8 6 -1 7609.67 339.895 14 8 -6 -1 7038.75 302.911 10 8 6 1 7389.27 359.109 7 8 -6 -2 3442.26 228.031 7 -8 6 -2 3753.79 243.028 14 8 -6 -2 3490.00 209.071 10 8 6 2 3822.63 258.988 7 8 -6 -3 14870.7 483.334 7 -8 6 -3 15552.7 499.882 14 8 -6 -3 13963.8 416.437 10 8 6 3 15431.3 513.995 7 8 -6 -4 5917.02 298.965 7 -8 6 -4 5680.87 298.038 14 8 -6 -4 5658.71 248.521 10 8 6 4 6260.59 316.066 7 8 -6 -5 9037.91 365.417 7 -8 6 -5 8481.09 367.411 14 8 6 5 9482.63 373.616 7 8 -6 -6 2860.58 199.282 7 -8 6 -6 2892.62 215.146 14 8 -6 -7 5904.86 276.158 7 -8 6 -7 5940.55 299.057 14 8 -6 -8 3553.35 205.107 7 -8 6 -8 3681.79 229.918 14 8 -6 -9 313.415 61.6325 7 -8 6 -9 273.220 67.9863 14 8 -6 -9 295.489 55.6727 4 8 -6 -10 517.537 71.5878 7 8 -6 -10 657.191 76.3750 4 -8 6 -10 601.149 85.5021 14 8 -6 -11 2309.56 130.130 7 8 -6 -11 2272.12 129.157 4 -8 6 -11 2420.45 158.673 14 8 -6 -12 2087.48 113.908 4 -8 6 -12 2108.70 134.796 14 8 7 -11 718.221 80.3864 6 8 -7 11 657.408 63.4828 10 8 7 -10 93.4763 48.9620 6 8 -7 10 72.9349 35.1227 10 8 7 -9 1928.68 152.132 6 8 -7 9 2028.07 140.092 10 8 7 -8 475.341 89.0477 6 -8 7 8 512.042 77.2812 14 8 -7 8 542.368 83.5446 10 8 7 -7 6689.56 312.907 6 -8 7 7 6550.88 257.748 14 8 -7 7 6480.73 277.925 10 -8 7 6 610.966 84.3835 14 8 -7 6 537.872 86.6568 10 8 7 -5 2095.57 184.699 6 -8 7 5 2081.67 156.348 14 8 7 -5 2065.60 146.753 7 8 -7 5 1891.92 155.688 10 8 7 -4 162.207 66.9533 6 8 7 -4 236.592 72.2414 7 -8 7 4 228.366 66.8863 14 8 -7 4 161.848 59.3553 10 8 7 -3 1299.50 151.966 6 -8 7 3 1239.37 130.051 14 8 7 -3 1187.54 131.271 7 8 -7 3 1058.03 118.843 10 8 7 -2 137.959 71.1218 6 8 7 -2 180.177 74.4200 7 8 -7 2 165.358 55.7046 7 -8 7 2 156.453 65.5721 14 8 -7 2 32.7449 52.6769 10 8 -7 1 941.576 109.839 7 8 7 -1 755.133 109.951 6 8 7 -1 705.031 112.197 7 -8 7 1 852.263 116.309 14 8 -7 1 771.906 100.081 10 8 -7 0 2465.43 176.804 7 8 7 0 2419.19 178.352 6 -8 7 0 2435.73 187.671 14 8 -7 0 2077.59 162.810 10 8 7 0 2290.56 196.957 7 8 7 1 768.040 97.2629 6 8 7 1 901.739 125.130 7 8 -7 -1 894.392 112.578 7 -8 7 -1 732.973 107.114 14 8 -7 -1 750.808 99.6394 10 8 7 2 109.510 58.6472 7 8 -7 -2 146.052 56.0672 7 -8 7 -2 221.349 71.6448 14 8 -7 -2 172.037 54.4137 10 8 -7 -3 1261.35 135.677 7 -8 7 -3 1135.84 131.506 14 8 -7 -3 1080.55 106.385 10 8 -7 -4 152.684 69.8619 7 -8 7 -4 130.132 58.9747 14 8 -7 -5 2036.07 165.595 7 -8 7 -5 2115.53 176.509 14 8 -7 -6 560.393 94.1868 7 -8 7 -6 570.374 96.8771 14 8 -7 -7 5884.68 261.239 7 -8 7 -7 6034.47 286.386 14 8 -7 -8 336.007 64.6566 7 -8 7 -8 401.813 79.6369 14 8 -7 -9 1918.16 134.220 7 8 -7 -9 2058.69 122.444 4 -8 7 -9 2091.07 157.721 14 8 -7 -10 30.0078 32.3393 7 -8 7 -10 79.9240 44.3647 14 8 -7 -10 50.2483 30.1406 4 8 -7 -11 551.167 59.8480 7 -8 7 -11 729.896 81.3776 14 -8 7 -12 364.913 52.5174 14 8 8 -10 4027.61 179.566 6 8 -8 10 3938.31 154.078 10 8 8 -9 7025.72 261.881 6 8 -8 9 6883.96 233.054 10 8 8 -8 648.082 93.4842 6 -8 8 8 527.785 72.4642 14 8 -8 8 478.538 72.3907 10 8 8 -7 304.993 71.1069 6 -8 8 7 293.572 56.2497 14 8 -8 7 299.162 64.2687 10 8 8 -6 2992.96 198.443 6 -8 8 6 2929.68 169.077 14 8 -8 6 2646.48 168.705 10 8 8 -5 657.046 105.623 6 -8 8 5 668.532 84.8572 14 8 -8 5 625.688 88.7764 10 8 8 -4 458.657 93.2333 6 -8 8 4 554.454 85.6863 14 8 -8 4 369.889 69.2909 10 8 8 -3 1452.15 146.554 6 -8 8 3 1470.99 134.431 14 8 -8 3 1232.88 118.002 10 8 8 -2 285.925 80.8986 6 -8 8 2 153.819 52.5675 14 8 -8 2 136.684 50.8446 10 8 -8 1 8453.61 291.538 7 8 8 -1 8979.13 341.879 6 -8 8 1 8609.96 334.882 14 8 -8 1 8053.37 301.815 10 8 8 0 337.158 72.6942 6 8 -8 0 436.219 77.4610 7 -8 8 0 372.091 82.4808 14 8 -8 0 310.451 64.7613 10 8 -8 -1 8578.49 314.274 7 8 8 1 8537.46 303.305 6 -8 8 -1 7984.15 327.713 14 8 -8 -1 7711.84 285.371 10 8 -8 -2 198.773 57.5774 7 -8 8 -2 218.279 68.4966 14 8 -8 -2 205.400 50.4851 10 8 -8 -3 1505.09 135.354 7 -8 8 -3 1361.26 138.937 14 8 -8 -4 373.353 74.1271 7 -8 8 -4 450.208 82.5640 14 8 -8 -5 649.373 90.9097 7 -8 8 -5 566.922 91.1058 14 8 -8 -6 2738.21 171.723 7 -8 8 -6 2670.34 181.707 14 8 -8 -7 270.530 60.1308 7 -8 8 -7 299.842 67.9905 14 8 -8 -8 436.936 68.5390 7 -8 8 -8 391.168 76.0074 14 8 -8 -9 6605.10 228.230 7 -8 8 -9 6601.01 251.971 14 8 -8 -10 3579.61 152.033 7 -8 8 -10 3823.76 176.737 14 8 9 -9 781.460 75.4428 6 8 -9 9 727.707 68.2372 10 8 9 -8 2019.56 131.601 6 8 -9 8 2114.38 121.347 10 8 9 -7 9.52002 35.1376 6 -8 9 7 57.6024 40.2510 14 8 -9 7 62.3429 33.2059 10 8 9 -6 6663.12 266.959 6 -8 9 6 6703.48 241.479 14 8 -9 6 5996.34 231.140 10 8 9 -5 340.539 75.8916 6 -8 9 5 307.310 60.8414 14 8 -9 5 271.915 59.3327 10 8 9 -4 2628.25 176.625 6 -8 9 4 2370.34 154.488 14 8 -9 4 2169.24 144.471 10 8 9 -3 2214.01 163.459 6 -8 9 3 2134.46 150.267 14 8 -9 3 1790.53 132.739 10 8 9 -2-14.5463 39.8155 6 -8 9 2 41.0456 38.0882 14 8 -9 2-2.03895 33.3907 10 8 9 -1 2532.92 165.078 6 -8 9 1 2481.65 169.391 14 8 -9 1 2484.76 152.353 10 8 9 0 254.766 57.7264 6 8 -9 0 225.653 50.9343 7 -8 9 0 222.710 63.1834 14 8 -9 0 257.035 56.4486 10 8 -9 -1 2644.68 155.729 7 8 9 1 2721.17 155.903 6 -8 9 -1 2480.74 172.466 14 8 -9 -1 2492.31 142.008 10 8 -9 -2-8.75093 45.0400 7 -8 9 -2-2.00077 42.6206 14 8 -9 -3 2024.05 141.991 7 -8 9 -3 1913.42 148.480 14 8 -9 -4 2208.83 146.888 7 -8 9 -4 2138.64 153.743 14 8 -9 -5 215.396 51.3368 7 -8 9 -5 262.944 59.3164 14 8 -9 -6 6337.45 236.849 7 -8 9 -6 6074.18 248.476 14 8 -9 -7 12.6337 35.3053 7 -8 9 -7 52.5908 43.8771 14 8 -9 -8 1940.53 117.698 7 -8 9 -8 1990.18 131.108 14 8 -9 -9 630.146 61.5410 7 -8 9 -9 779.753 75.1882 14 8 10 -7 8958.91 251.315 6 8 -10 7 7946.29 217.849 10 8 10 -6 1487.91 109.678 6 -8 10 6 1460.62 101.215 14 8 -10 6 1354.48 94.1953 10 8 10 -5 934.372 92.3480 6 -8 10 5 905.646 85.1036 14 8 -10 5 825.601 77.8040 10 8 10 -4 1806.64 129.306 6 -8 10 4 1914.46 124.415 14 8 -10 4 1868.07 116.784 10 8 10 -3 91.7930 41.6240 6 -8 10 3 115.473 39.9232 14 8 -10 3 109.925 38.4415 10 8 10 -2 579.482 78.1521 6 -8 10 2 616.041 79.7102 14 8 -10 2 553.206 66.4004 10 8 10 -1 1008.53 94.2548 6 -8 10 1 954.506 97.8367 14 8 -10 1 938.525 82.1463 10 8 10 0 3112.19 157.837 6 -8 10 0 3029.72 170.305 14 8 -10 -1 1010.43 83.4694 7 8 10 1 1088.38 88.9823 6 -8 10 -1 881.124 95.6229 14 8 -10 -2 488.942 63.7284 7 -8 10 -2 587.680 78.8271 14 8 -10 -3 104.923 39.5504 7 -8 10 -3 126.523 41.9004 14 8 -10 -4 1830.96 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521.548 7 9 -1 -3 6301.11 319.970 7 9 1 3 6356.07 307.253 7 9 -1 -4 7997.63 353.978 7 9 -1 -4 8634.86 353.786 6 9 1 4 8076.33 334.634 7 9 -1 -5 1056.91 130.382 7 9 1 5 911.552 109.845 7 9 -1 -5 1015.67 125.721 6 9 -1 -6 1537.53 147.305 7 9 -1 -6 1857.48 168.181 6 9 1 6 1596.72 134.216 7 9 -1 -7 1679.90 146.601 7 9 1 7 1741.41 130.959 7 9 -1 -8 3719.93 227.139 6 9 -1 -8 3493.59 195.762 7 9 -1 -9 4181.72 230.257 6 9 -1 -9 3969.20 193.725 7 9 -1 -10 398.411 75.4621 6 9 -1 -11 2329.35 152.097 6 9 -1 -12 2345.04 140.035 6 9 2 -12 1063.80 95.4551 6 9 2 -11 1712.50 130.032 6 9 2 -10 706.594 92.8092 6 9 2 -9 743.362 101.309 6 9 -2 9 693.937 75.3965 10 9 2 -8 1853.25 161.952 6 9 -2 8 1633.04 128.053 10 9 2 -8 1473.25 119.863 7 9 2 -7 2621.87 199.021 6 9 -2 7 2351.39 166.643 10 9 2 -7 2273.83 159.894 7 9 2 -6 5957.29 300.743 6 9 -2 6 5976.72 275.406 10 9 2 -6 5404.47 263.982 7 9 2 -5 1444.26 152.306 6 9 -2 5 1382.47 138.940 10 9 -2 5 1364.33 123.513 7 9 2 -5 1321.95 140.104 7 9 2 -4 233.368 70.5836 7 9 -2 4 165.449 53.1305 7 9 2 -4 218.780 69.7225 6 9 -2 4 184.754 65.8518 10 9 2 -3 440.661 93.0464 7 9 2 -3 502.931 99.0869 6 9 -2 3 395.462 75.8237 7 9 -2 3 571.600 108.498 10 9 2 -2 4699.73 250.040 6 9 2 -2 4676.45 279.581 7 9 -2 2 4325.03 244.811 7 9 -2 2 4293.36 252.295 10 9 -2 1 11639.9 422.938 7 9 -2 1 11988.7 417.828 10 9 2 -1 12619.1 466.836 7 9 2 0 1114.50 156.008 7 9 -2 0 1016.10 138.447 7 9 -2 0 1163.94 137.825 10 9 -2 -1 12003.9 440.976 7 9 2 1 12303.7 454.584 7 9 -2 -2 4731.76 276.875 7 9 2 2 4999.96 283.414 7 9 2 3 448.960 91.4932 7 9 -2 -3 379.502 80.7346 7 9 2 4 112.836 49.8668 7 9 -2 -4 180.091 68.3173 7 9 -2 -5 1373.85 144.991 7 9 2 5 1485.43 140.545 7 9 -2 -6 5479.03 272.517 7 9 2 6 5396.58 247.849 7 9 -2 -7 2285.59 171.405 7 9 2 7 2387.75 157.022 7 9 -2 -8 1580.87 132.163 7 9 -2 -9 737.957 91.4079 7 9 -2 -10 772.796 99.9119 6 9 -2 -10 607.628 69.8137 7 9 -2 -11 1477.50 119.082 6 9 -2 -12 1080.00 94.8692 6 9 3 -12 3498.42 160.473 6 9 3 -11 3513.10 180.180 6 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1368.81 140.408 10 9 -4 2 1045.71 117.701 7 9 4 -2 1035.48 132.004 7 9 4 -2 1348.62 135.533 6 9 -4 2 1158.44 131.216 10 9 -4 1 5545.92 269.605 7 9 -4 1 5052.43 261.345 10 9 4 -1 5425.98 294.008 7 9 -4 0 4236.50 243.730 7 9 -4 0 3548.34 216.526 10 9 4 0 3909.88 255.030 7 9 -4 -1 5582.44 285.052 7 9 -4 -1 5148.55 255.421 10 9 4 1 5525.62 297.536 7 9 -4 -2 1157.11 133.696 7 9 -4 -2 1033.19 115.175 10 9 4 2 1274.30 148.171 7 9 -4 -3 1393.91 146.116 7 9 4 3 1421.67 152.197 7 9 -4 -4 2217.34 182.275 7 -9 4 -4 2299.79 164.059 14 9 4 4 2276.50 180.977 7 9 -4 -5 3299.65 216.134 7 -9 4 -5 3455.62 201.922 14 9 4 5 3463.83 209.426 7 9 -4 -6 1334.55 129.030 7 -9 4 -6 1334.20 126.572 14 9 4 6 1480.18 130.577 7 9 -4 -7 1883.66 148.065 7 -9 4 -7 1940.63 147.067 14 9 -4 -8 406.957 71.3529 7 -9 4 -8 481.304 77.6198 14 9 -4 -9 1303.27 106.731 7 -9 4 -9 1318.62 112.026 14 9 -4 -10 1018.03 84.0633 7 -9 4 -10 1021.07 92.4809 14 9 5 -11 1308.44 95.5713 6 9 5 -10 66.3237 36.9665 6 9 5 -9 496.889 76.3917 6 9 -5 9 435.259 60.5523 10 9 5 -8 1342.80 127.278 6 9 -5 8 1270.35 106.629 10 9 5 -7 309.274 68.4493 6 9 -5 7 257.325 58.7762 10 9 5 -6 814.897 109.198 6 9 5 -6 821.978 86.7524 7 9 -5 6 858.888 100.955 10 9 5 -5 943.612 119.491 6 9 5 -5 842.175 97.9307 7 9 -5 5 876.895 109.008 10 9 5 -4 4361.74 244.088 6 9 -5 4 4073.85 222.134 10 9 5 -4 4053.78 219.091 7 9 5 -3 1289.46 136.264 6 9 -5 3 1069.08 121.177 10 9 -5 3 1149.90 111.221 7 9 5 -3 1112.05 127.350 7 9 5 -2 521.595 89.3966 6 9 5 -2 358.249 79.5289 7 9 -5 2 297.533 64.4853 7 9 -5 2 425.298 86.4536 10 9 -5 1 7175.16 291.109 7 9 5 -1 7628.83 295.244 6 9 -5 1 6696.26 288.910 10 9 5 -1 7000.41 324.100 7 9 5 0 470.129 100.035 7 9 -5 0 480.553 91.4422 7 9 -5 0 384.315 87.6914 10 9 -5 -1 7433.77 313.838 7 -9 5 -1 7097.75 276.986 14 9 -5 -1 6349.61 269.717 10 9 5 1 7144.86 329.177 7 9 5 2 453.280 90.1554 7 9 -5 -2 446.179 89.4932 7 -9 5 -2 453.412 83.1048 14 9 -5 -2 378.152 72.8381 10 9 -5 -3 1043.36 123.427 7 9 5 3 1117.28 130.161 7 -9 5 -3 1096.27 114.818 14 9 -5 -4 4287.43 238.861 7 -9 5 -4 4149.09 219.306 14 9 5 4 4390.80 240.727 7 9 -5 -5 917.648 112.005 7 -9 5 -5 1014.48 113.100 14 9 5 5 918.510 112.282 7 9 -5 -6 786.543 100.266 7 -9 5 -6 881.717 101.493 14 9 -5 -7 269.663 59.2826 7 -9 5 -7 317.544 66.7534 14 9 -5 -8 1158.92 103.129 7 -9 5 -8 1254.20 112.940 14 9 -5 -9 466.744 64.9632 7 -9 5 -9 475.427 69.1813 14 9 -5 -10 59.3928 26.2311 7 -9 5 -10 92.7138 36.8160 14 9 6 -10 965.560 83.7442 6 9 6 -9 475.647 66.9519 6 9 -6 9 461.578 57.4972 10 9 6 -8 1105.42 107.964 6 9 -6 8 1001.26 88.1478 10 9 6 -7 3355.71 190.468 6 9 -6 7 2973.45 165.167 10 9 6 -6 1444.89 131.868 6 9 -6 6 1272.06 114.766 10 9 6 -5 2672.94 180.205 6 9 -6 5 2647.36 166.077 10 9 6 -5 2636.07 151.708 7 9 6 -4 640.313 95.7998 6 9 6 -4 565.443 85.0760 7 9 -6 4 693.540 95.3513 10 9 6 -3 3157.74 195.960 6 9 -6 3 2793.54 176.832 10 9 6 -3 2987.58 186.139 7 9 6 -2 546.779 84.3624 6 9 6 -2 527.577 91.3306 7 9 -6 2 529.557 75.1403 7 -9 6 2 558.586 75.3497 14 9 -6 2 488.738 85.0243 10 9 -6 1 3888.49 199.347 7 9 6 -1 3986.03 202.418 6 -9 6 1 3963.12 195.113 14 9 -6 1 3996.02 208.336 10 9 6 -1 3897.08 227.418 7 9 -6 0 1332.11 122.826 7 -9 6 0 1351.00 117.746 14 9 -6 0 1350.19 121.049 10 9 6 0 1340.65 139.351 7 9 -6 -1 4225.21 221.448 7 -9 6 -1 3920.08 204.780 14 9 -6 -1 3658.81 191.797 10 9 6 1 4126.27 240.217 7 9 6 2 487.768 91.6033 7 9 -6 -2 391.819 73.5165 7 -9 6 -2 516.102 82.5710 14 9 -6 -2 447.667 71.5521 10 9 -6 -3 2985.16 186.340 7 -9 6 -3 2972.28 181.009 14 9 6 3 3258.24 207.431 7 9 -6 -4 564.027 89.2201 7 -9 6 -4 690.371 93.9620 14 9 -6 -5 2606.22 168.871 7 -9 6 -5 2751.75 173.160 14 9 -6 -6 1229.17 112.890 7 -9 6 -6 1344.98 119.636 14 9 -6 -7 2854.92 160.959 7 -9 6 -7 3169.62 174.113 14 9 -6 -8 844.126 86.0712 7 -9 6 -8 990.090 96.3330 14 9 -6 -9 432.433 55.3016 7 -9 6 -9 474.306 66.5874 14 9 7 -8 3472.88 165.764 6 9 -7 8 2961.25 138.090 10 9 7 -7 2667.79 156.273 6 9 -7 7 2656.59 139.969 10 9 7 -6 2117.71 145.315 6 9 -7 6 1971.23 128.986 10 9 7 -5 1970.08 144.155 6 9 -7 5 1877.90 130.215 10 9 7 -4 129.813 54.9587 6 -9 7 4 95.5044 35.8881 14 9 -7 4 96.6446 43.2976 10 9 7 -3 2618.86 168.110 6 -9 7 3 2639.09 147.391 14 9 -7 3 2267.25 148.241 10 9 7 -2 2484.27 157.711 6 -9 7 2 2636.95 151.008 14 9 -7 2 2411.09 150.871 10 9 -7 1 1087.20 99.3251 7 9 7 -1 1252.55 108.466 6 -9 7 1 1099.48 102.854 14 9 -7 1 1023.72 100.689 10 9 -7 0 719.327 83.7538 7 -9 7 0 698.080 86.0660 14 9 -7 0 682.931 82.2882 10 9 -7 -1 1047.87 101.707 7 -9 7 -1 1106.01 107.600 14 9 -7 -1 1005.81 93.4346 10 9 -7 -2 2532.73 159.283 7 -9 7 -2 2652.92 162.323 14 9 -7 -3 2544.04 159.130 7 -9 7 -3 2645.83 162.182 14 9 -7 -4 107.617 43.1821 7 -9 7 -4 98.9552 43.9364 14 9 -7 -5 1759.10 127.569 7 -9 7 -5 1828.80 130.281 14 9 -7 -6 2071.64 134.094 7 -9 7 -6 2179.32 139.016 14 9 -7 -7 2632.97 141.962 7 -9 7 -7 2661.56 146.307 14 9 -7 -8 3045.45 140.975 7 -9 7 -8 3197.91 150.268 14 9 8 -7 1020.74 84.0714 6 9 -8 7 901.959 71.9260 10 9 8 -6 186.502 40.4310 6 9 -8 6 143.258 35.2388 10 9 8 -5 879.232 88.6240 6 9 -8 5 814.586 77.5489 10 9 8 -4 651.688 76.9862 6 -9 8 4 624.909 62.8724 14 9 -8 4 617.551 70.4719 10 9 8 -3 1538.31 114.977 6 -9 8 3 1532.87 103.658 14 9 -8 3 1470.26 108.414 10 9 8 -2 5370.37 208.925 6 -9 8 2 5347.34 202.653 14 9 -8 2 4738.79 193.464 10 9 8 -1 1342.08 98.5293 6 -9 8 1 1260.10 102.569 14 9 -8 1 1166.27 95.3867 10 9 -8 0 1076.90 87.3358 7 -9 8 0 1176.04 101.368 14 9 -8 0 1029.13 86.5121 10 9 -8 -1 1254.42 97.4842 7 -9 8 -1 1272.32 105.565 14 9 -8 -1 1186.15 88.5626 10 9 -8 -2 5106.80 200.663 7 -9 8 -2 5073.34 208.299 14 9 -8 -3 1489.04 108.944 7 -9 8 -3 1562.62 114.809 14 9 -8 -4 565.728 66.9357 7 -9 8 -4 599.268 73.4472 14 9 -8 -5 845.762 80.8769 7 -9 8 -5 836.525 80.6113 14 9 -8 -6 208.758 43.6679 7 -9 8 -6 174.513 42.3963 14 9 -8 -7 814.137 71.9014 7 9 -9 3 182.449 36.2104 10 -9 9 2 1913.35 107.595 14 9 -9 2 1757.23 98.0552 10 -9 9 1 166.460 40.3818 14 -9 9 0 4275.89 169.906 14 -9 9 -1 166.838 41.9669 14 -9 9 -2 2001.06 117.062 14 -9 9 -3 214.620 41.6097 14 10 0 0-72.8569 65.0493 7 10 0 1 704.150 98.2082 7 10 0 -1 662.452 94.3147 7 10 0 -2 1173.17 123.769 7 10 0 2 1412.18 129.924 7 10 0 -3 9229.93 338.820 7 10 0 3 9419.92 323.155 7 10 0 4 11.9698 35.5769 7 10 0 -4-6.09077 42.5235 7 10 0 5-2.25519 39.7342 7 10 0 -5 8.07931 45.5607 7 10 0 -5-7.65782 31.4950 6 10 0 -6 5562.71 224.995 6 10 0 6 5098.14 186.351 7 10 0 -6 4958.10 215.164 7 10 0 -7 1860.41 127.919 6 10 0 -7 1695.87 114.296 7 10 0 -8 135.375 35.1627 7 10 0 -8 114.619 37.5544 6 10 0 -9 2400.09 129.295 6 10 1 -9 143.058 35.3728 6 10 1 -8 3.09031 27.6402 6 10 1 -7 184.889 41.8358 7 10 1 -7 183.336 46.7611 6 10 1 -6 2353.68 148.715 6 10 1 -6 1936.36 131.407 7 10 1 -5 2650.21 157.723 6 10 1 -5 2445.18 156.700 7 10 -1 5 2407.27 136.606 7 10 -1 4 466.444 72.0280 7 10 1 -4 498.821 80.4250 7 10 -1 3 1364.36 120.277 7 10 1 -3 1354.93 130.994 7 10 1 -2 1582.10 144.543 7 10 -1 2 1675.91 137.255 7 10 1 -1 4198.24 232.364 7 10 -1 1 4185.85 225.139 7 10 -1 0 5375.22 260.325 7 10 1 0 5647.17 269.202 7 10 1 1 4492.99 236.864 7 10 -1 -1 4438.25 238.203 7 10 1 2 1575.07 139.103 7 10 -1 -2 1704.51 147.066 7 10 -1 -3 1192.79 125.453 7 10 1 3 1369.49 125.928 7 10 1 4 472.322 73.9649 7 10 -1 -4 457.571 81.3460 7 10 1 5 2223.38 138.823 7 10 -1 -5 2297.99 155.736 7 10 -1 -6 2337.97 140.794 6 10 -1 -6 2284.22 146.768 7 10 1 6 2104.84 123.485 7 10 -1 -7 128.845 31.2038 7 10 -1 -7 151.737 47.8831 6 10 -1 -8 13.5346 23.8736 7 10 -1 -8-15.4070 33.3974 6 10 -1 -9 140.084 37.4082 6 10 2 -9 12.6150 24.9484 6 10 2 -8 1140.36 95.8689 6 10 2 -7 1006.04 95.8615 6 10 2 -7 1058.24 84.3171 7 10 2 -6 633.958 77.1102 6 10 2 -6 574.875 71.8730 7 10 2 -5 8135.58 276.136 6 10 2 -5 7350.31 268.582 7 10 -2 4 2479.95 142.876 7 10 2 -4 2330.63 158.473 7 10 2 -3 3497.64 201.764 7 10 -2 3 3511.57 181.098 7 10 2 -2 614.771 90.7621 7 10 -2 2 530.149 81.7019 7 10 2 -1 226.991 63.2106 7 10 -2 1 227.935 62.7279 7 10 2 0 7449.49 311.098 7 10 -2 0 7538.83 299.580 7 10 2 1 280.515 77.3042 7 10 -2 -1 169.098 64.9921 7 10 2 2 553.248 87.6032 7 10 -2 -2 570.418 91.9346 7 10 -2 -3 3626.21 208.490 7 10 2 3 3610.69 202.206 7 10 -2 -4 2464.69 168.531 7 10 2 4 2557.68 160.307 7 10 -2 -5 7478.56 277.932 7 10 2 5 7722.57 261.838 7 10 -2 -6 632.594 79.9386 7 10 -2 -6 620.405 74.5974 6 10 2 6 682.727 76.9735 7 10 -2 -7 1024.93 88.8148 6 10 -2 -7 998.509 91.8909 7 10 -2 -8 1096.15 85.8161 6 10 -2 -8 936.693 76.6699 7 10 3 -8 1329.89 97.7835 6 10 3 -7 2387.51 138.772 6 10 3 -6 282.572 55.5998 6 10 3 -6 289.956 52.7839 7 10 3 -5 152.073 52.1252 6 10 3 -5 137.964 43.6559 7 10 3 -4 348.412 60.5871 6 10 3 -4 284.647 57.6135 7 10 -3 4 279.566 48.5359 7 10 -3 3 1978.63 129.269 7 10 3 -3 2183.79 154.980 7 10 3 -2 4416.43 226.739 7 10 -3 2 4288.42 202.471 7 10 -3 1 8491.74 300.229 7 10 3 -1 8716.99 325.577 7 10 3 0 185.640 72.7967 7 10 -3 0 115.237 58.8898 7 10 -3 -1 8704.17 317.356 7 10 3 1 8705.32 327.772 7 10 -3 -2 4312.98 221.617 7 10 3 2 4656.59 232.083 7 10 3 3 2315.06 160.675 7 10 -3 -3 2159.30 158.023 7 10 3 4 398.086 74.5392 7 10 -3 -4 359.858 71.8973 7 10 3 5 161.986 49.5613 7 10 -3 -5 127.244 48.6348 7 10 -3 -6 248.937 54.9436 7 10 -3 -7 2099.19 124.524 7 10 -3 -8 1285.50 87.3982 7 10 4 -7 770.480 76.5111 6 10 4 -6 6596.59 227.727 6 10 4 -5 849.049 86.2615 6 10 4 -5 769.470 77.8616 7 10 4 -4 4419.04 186.628 6 10 4 -4 4170.92 190.208 7 10 4 -3 2349.59 151.611 7 10 -4 3 2518.69 132.261 7 10 4 -2 173.237 58.4936 7 10 -4 2 117.354 41.0545 7 10 4 -1 2369.13 161.046 7 10 -4 1 2433.66 149.721 7 10 -4 0 2426.22 154.019 7 10 4 0 2566.41 169.363 7 10 -4 -1 2395.82 157.407 7 10 4 1 2571.19 170.850 7 10 4 2 201.260 65.7666 7 10 -4 -2 224.210 60.6499 7 10 4 3 2773.42 169.056 7 10 -4 -3 2653.80 163.964 7 10 -4 -4 4497.41 208.580 7 10 4 4 4646.83 207.337 7 10 -4 -5 841.669 89.8293 7 10 -4 -6 6193.03 222.177 7 10 -4 -7 640.366 69.6226 7 10 -5 5 628.991 69.0661 10 10 5 -4 185.726 44.6237 7 10 -5 4 271.092 52.8070 10 10 5 -3 5936.57 221.053 7 10 5 -2 1961.45 134.963 7 10 -5 2 2064.56 116.916 7 10 5 -1 839.976 93.6704 7 10 -5 1 858.616 83.3555 7 10 5 0 455.423 71.6434 7 10 -5 0 322.116 57.2364 7 10 5 1 858.047 98.8079 7 10 -5 -1 837.303 90.1740 7 10 5 2 2183.15 148.413 7 10 -5 -2 2046.53 136.373 7 10 -5 -3 6216.25 235.883 7 10 -5 -4 224.144 51.5622 7 10 -5 -5 715.853 75.4741 7 10 -5 -6 76.0497 31.0819 7 10 -6 0 1879.92 108.887 7 10 -6 -1 645.203 71.1778 7 10 -6 -2 1242.09 95.0900 7 10 -6 -3 1916.55 117.899 7 10 -6 -4 964.519 84.9250 7 10 -6 -5 298.078 48.0471 7 11 0 0 6.45124 27.9126 7 11 0 1 1533.66 103.989 7 11 0 -1 1652.88 111.131 7 11 0 2 1925.62 109.666 7 11 0 -2 1821.43 114.632 7 11 0 -3 946.141 79.5560 7 11 1 -3 1801.87 106.629 7 11 1 -2 557.612 65.2196 7 11 1 -1 1880.22 117.327 7 11 -1 1 1973.76 112.491 7 11 1 0 627.782 72.4333 7 11 -1 0 607.830 67.9503 7 11 -1 -1 1880.03 116.656 7 11 1 1 1942.24 116.663 7 11 -1 -2 577.403 65.7239 7 11 1 2 628.133 66.3154 7 11 -1 -3 1854.90 109.550 7 11 2 -2 677.865 67.2058 7 11 2 -1 1416.78 97.6712 7 11 2 0 152.383 40.1144 7 11 -2 0 70.0611 24.8926 7 11 -2 -1 1372.39 94.3454 7 11 2 1 1483.82 98.7867 7 11 -2 -2 674.542 68.9647 7 0 0 0 0.00 0.00 0 TITL SCD-GSY2023-0706_auto in P2(1)2(1)2(1) REM P2(1)2(1)2(1) (#19 in standard setting) CELL 1.54184 8.998237 13.131191 17.797704 90.0000 90.0000 90.0000 ZERR 5.00 0.000067 0.000090 0.000126 0.0000 0.0000 0.0000 LATT -1 SYMM -x+1/2,-y, z+1/2 SYMM -x, y+1/2,-z+1/2 SYMM x+1/2,-y+1/2,-z SFAC C H N O UNIT 100.00 100.00 10.00 10.00 TREF HKLF 4 END ; _shelx_hkl_checksum 81794 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.470 _oxdiff_exptl_absorpt_empirical_full_min 0.674 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O3 O 0.5770(3) 0.72902(13) 0.16004(10) 0.0561(5) Uani 1 1 d . . . . . O1 O 0.4129(2) 0.45121(13) 0.22656(11) 0.0577(5) Uani 1 1 d . . . . . H1 H 0.3835 0.3981 0.2457 0.087 Uiso 1 1 calc R U . . . O2 O 0.3099(2) 0.57105(19) 0.35869(13) 0.0707(6) Uani 1 1 d . . . . . N2 N 0.6339(2) 0.42872(13) 0.37836(10) 0.0389(4) Uani 1 1 d . . . . . N1 N 0.5069(2) 0.47912(14) 0.40708(11) 0.0404(4) Uani 1 1 d . . . . . N3 N 0.6718(3) 0.75203(15) 0.22228(12) 0.0497(5) Uani 1 1 d . . . . . C4 C 0.5569(3) 0.60048(16) 0.24110(12) 0.0402(5) Uani 1 1 d . . . . . C18 C 0.7403(2) 0.67288(15) 0.33999(13) 0.0384(5) Uani 1 1 d . . . . . N4 N 0.4129(4) 0.6063(2) 0.12169(15) 0.0778(9) Uani 1 1 d . . . . . H4 H 0.3788 0.5456 0.1272 0.093 Uiso 1 1 calc R U . . . C13 C 0.7619(3) 0.40015(18) 0.25946(13) 0.0466(5) Uani 1 1 d . . . . . H13 H 0.8046 0.4595 0.2340 0.056 Uiso 1 1 calc R U . . . C23 C 0.8910(3) 0.6524(2) 0.34022(15) 0.0499(6) Uani 1 1 d . . . . . H23 H 0.9414 0.6439 0.2950 0.060 Uiso 1 1 calc R U . . . C6 C 0.6560(3) 0.67454(16) 0.26803(12) 0.0389(5) Uani 1 1 d . . . . . C19 C 0.6680(3) 0.68811(19) 0.40778(14) 0.0476(5) Uani 1 1 d . . . . . H19 H 0.5673 0.7039 0.4081 0.057 Uiso 1 1 calc R U . . . C5 C 0.5091(3) 0.63948(18) 0.17316(14) 0.0495(6) Uani 1 1 d . . . . . C3 C 0.5076(3) 0.50270(16) 0.27762(13) 0.0407(5) Uani 1 1 d . . . . . C7 C 0.4881(3) 0.48392(17) 0.48599(13) 0.0400(5) Uani 1 1 d . . . . . C12 C 0.5709(3) 0.4203(2) 0.53142(14) 0.0497(6) Uani 1 1 d . . . . . H12 H 0.6404 0.3762 0.5104 0.060 Uiso 1 1 calc R U . . . C2 C 0.4245(3) 0.52466(19) 0.35188(14) 0.0449(5) Uani 1 1 d . . . . . C20 C 0.7441(3) 0.6801(2) 0.47467(15) 0.0572(7) Uani 1 1 d . . . . . H20 H 0.6946 0.6899 0.5200 0.069 Uiso 1 1 calc R U . . . C10 C 0.4505(4) 0.4900(3) 0.64077(16) 0.0633(7) Uani 1 1 d . . . . . H10 H 0.4359 0.4908 0.6925 0.076 Uiso 1 1 calc R U . . . C11 C 0.5497(4) 0.4228(3) 0.60921(14) 0.0644(8) Uani 1 1 d . . . . . H11 H 0.6030 0.3786 0.6399 0.077 Uiso 1 1 calc R U . . . C22 C 0.9670(3) 0.6445(2) 0.40755(19) 0.0635(7) Uani 1 1 d . . . . . H22 H 1.0683 0.6304 0.4076 0.076 Uiso 1 1 calc R U . . . C9 C 0.3736(3) 0.5558(2) 0.59546(17) 0.0578(7) Uani 1 1 d . . . . . H9 H 0.3097 0.6032 0.6169 0.069 Uiso 1 1 calc R U . . . C8 C 0.3897(3) 0.55269(19) 0.51793(16) 0.0516(6) Uani 1 1 d . . . . . H8 H 0.3348 0.5964 0.4876 0.062 Uiso 1 1 calc R U . . . C21 C 0.8931(3) 0.6574(2) 0.47435(18) 0.0625(7) Uani 1 1 d . . . . . H21 H 0.9441 0.6508 0.5195 0.075 Uiso 1 1 calc R U . . . C15 C 0.8845(5) 0.3541(4) 0.30440(19) 0.0891(13) Uani 1 1 d . . . . . H15A H 0.9109 0.3993 0.3447 0.134 Uiso 1 1 calc R U . . . H15B H 0.9694 0.3433 0.2727 0.134 Uiso 1 1 calc R U . . . H15C H 0.8522 0.2902 0.3248 0.134 Uiso 1 1 calc R U . . . C16 C 0.3606(5) 0.6641(2) 0.05691(16) 0.0705(9) Uani 1 1 d . . . . . H16A H 0.2552 0.6517 0.0501 0.085 Uiso 1 1 calc R U . . . H16B H 0.3738 0.7362 0.0667 0.085 Uiso 1 1 calc R U . . . C14 C 0.7096(5) 0.3288(4) 0.1979(2) 0.1029(16) Uani 1 1 d . . . . . H14A H 0.6739 0.2668 0.2200 0.154 Uiso 1 1 calc R U . . . H14B H 0.7909 0.3140 0.1648 0.154 Uiso 1 1 calc R U . . . H14C H 0.6308 0.3606 0.1701 0.154 Uiso 1 1 calc R U . . . C17 C 0.4371(10) 0.6380(5) -0.0106(3) 0.146(3) Uani 1 1 d . . . . . H17A H 0.3936 0.6739 -0.0521 0.218 Uiso 1 1 calc R U . . . H17B H 0.4293 0.5660 -0.0191 0.218 Uiso 1 1 calc R U . . . H17C H 0.5399 0.6565 -0.0061 0.218 Uiso 1 1 calc R U . . . C1 C 0.6368(3) 0.43962(15) 0.30691(12) 0.0379(5) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O3 0.0856(13) 0.0343(8) 0.0483(9) 0.0102(7) -0.0086(9) -0.0062(8) O1 0.0740(12) 0.0408(9) 0.0583(10) 0.0124(8) -0.0281(9) -0.0171(8) O2 0.0500(10) 0.0857(15) 0.0763(13) 0.0260(12) 0.0093(10) 0.0246(10) N2 0.0466(10) 0.0320(8) 0.0381(9) 0.0011(7) -0.0003(8) 0.0060(7) N1 0.0441(9) 0.0367(8) 0.0402(9) 0.0035(7) 0.0015(8) 0.0063(8) N3 0.0660(13) 0.0327(9) 0.0505(11) 0.0020(8) -0.0018(10) -0.0043(9) C4 0.0512(11) 0.0304(10) 0.0391(10) 0.0025(8) -0.0034(9) 0.0024(9) C18 0.0445(11) 0.0273(9) 0.0435(11) -0.0033(8) -0.0007(9) -0.0032(8) N4 0.121(2) 0.0492(13) 0.0631(15) 0.0173(11) -0.0431(16) -0.0194(14) C13 0.0597(14) 0.0404(11) 0.0397(11) -0.0001(9) 0.0069(10) 0.0012(10) C23 0.0440(12) 0.0484(13) 0.0573(13) -0.0089(11) 0.0060(11) -0.0014(10) C6 0.0462(11) 0.0284(9) 0.0421(10) -0.0015(8) 0.0033(9) 0.0027(8) C19 0.0472(12) 0.0452(12) 0.0503(12) -0.0087(11) 0.0032(11) -0.0023(10) C5 0.0704(16) 0.0324(11) 0.0456(12) 0.0051(9) -0.0075(11) -0.0025(10) C3 0.0478(11) 0.0331(10) 0.0411(11) 0.0046(8) -0.0085(9) -0.0039(9) C7 0.0453(11) 0.0343(10) 0.0403(11) -0.0025(8) 0.0038(9) -0.0045(9) C12 0.0576(14) 0.0518(14) 0.0399(11) -0.0069(10) -0.0024(11) 0.0091(11) C2 0.0421(11) 0.0414(11) 0.0511(12) 0.0123(10) -0.0016(10) 0.0016(9) C20 0.0681(17) 0.0601(15) 0.0435(12) -0.0099(11) 0.0009(12) -0.0112(13) C10 0.0684(16) 0.0763(19) 0.0453(13) -0.0174(13) 0.0040(13) -0.0039(15) C11 0.0759(18) 0.0786(19) 0.0385(12) -0.0065(12) -0.0078(12) 0.0136(16) C22 0.0450(13) 0.0671(17) 0.0785(18) -0.0117(15) -0.0098(13) 0.0010(12) C9 0.0605(15) 0.0512(14) 0.0615(15) -0.0150(12) 0.0184(13) -0.0023(12) C8 0.0561(14) 0.0398(12) 0.0590(14) 0.0021(11) 0.0124(12) 0.0048(11) C21 0.0671(18) 0.0610(16) 0.0595(15) -0.0047(13) -0.0202(14) -0.0092(14) C15 0.090(2) 0.114(3) 0.0629(18) 0.0089(19) 0.0132(18) 0.057(2) C16 0.105(2) 0.0552(16) 0.0515(14) 0.0092(13) -0.0177(16) -0.0013(17) C14 0.097(3) 0.132(4) 0.080(2) -0.063(3) 0.020(2) -0.012(3) C17 0.258(8) 0.098(3) 0.081(3) 0.020(3) 0.060(4) 0.034(5) C1 0.0497(12) 0.0271(9) 0.0369(10) 0.0014(7) -0.0029(9) -0.0019(9) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C5 O3 N3 108.72(17) . . ? C3 O1 H1 109.5 . . ? C1 N2 N1 108.83(18) . . ? N2 N1 C7 118.40(17) . . ? C2 N1 N2 112.51(18) . . ? C2 N1 C7 128.8(2) . . ? C6 N3 O3 104.60(18) . . ? C6 C4 C3 129.1(2) . . ? C5 C4 C6 103.9(2) . . ? C5 C4 C3 127.0(2) . . ? C23 C18 C6 120.3(2) . . ? C23 C18 C19 119.1(2) . . ? C19 C18 C6 120.5(2) . . ? C5 N4 H4 117.2 . . ? C5 N4 C16 125.7(3) . . ? C16 N4 H4 117.2 . . ? C15 C13 H13 106.2 . . ? C15 C13 C14 111.5(3) . . ? C15 C13 C1 113.2(2) . . ? C14 C13 H13 106.2 . . ? C1 C13 H13 106.2 . . ? C1 C13 C14 112.8(3) . . ? C18 C23 H23 119.9 . . ? C18 C23 C22 120.1(2) . . ? C22 C23 H23 119.9 . . ? N3 C6 C4 113.2(2) . . ? N3 C6 C18 119.4(2) . . ? C4 C6 C18 127.39(19) . . ? C18 C19 H19 119.7 . . ? C20 C19 C18 120.6(2) . . ? C20 C19 H19 119.7 . . ? O3 C5 C4 109.5(2) . . ? N4 C5 O3 117.4(2) . . ? N4 C5 C4 133.0(2) . . ? O1 C3 C4 107.89(17) . . ? O1 C3 C2 110.3(2) . . ? O1 C3 C1 114.82(18) . . ? C4 C3 C2 110.64(18) . . ? C4 C3 C1 112.78(19) . . ? C1 C3 C2 100.29(17) . . ? C12 C7 N1 119.3(2) . . ? C12 C7 C8 119.9(2) . . ? C8 C7 N1 120.8(2) . . ? C7 C12 H12 120.3 . . ? C7 C12 C11 119.5(2) . . ? C11 C12 H12 120.3 . . ? O2 C2 N1 127.8(2) . . ? O2 C2 C3 126.5(2) . . ? N1 C2 C3 105.64(19) . . ? C19 C20 H20 120.1 . . ? C21 C20 C19 119.9(3) . . ? C21 C20 H20 120.1 . . ? C11 C10 H10 120.3 . . ? C9 C10 H10 120.3 . . ? C9 C10 C11 119.5(3) . . ? C12 C11 H11 119.7 . . ? C10 C11 C12 120.5(3) . . ? C10 C11 H11 119.7 . . ? C23 C22 H22 120.0 . . ? C21 C22 C23 120.1(2) . . ? C21 C22 H22 120.0 . . ? C10 C9 H9 119.5 . . ? C10 C9 C8 121.0(3) . . ? C8 C9 H9 119.5 . . ? C7 C8 C9 119.5(3) . . ? C7 C8 H8 120.2 . . ? C9 C8 H8 120.2 . . ? C20 C21 H21 119.9 . . ? C22 C21 C20 120.2(3) . . ? C22 C21 H21 119.9 . . ? C13 C15 H15A 109.5 . . ? C13 C15 H15B 109.5 . . ? C13 C15 H15C 109.5 . . ? H15A C15 H15B 109.5 . . ? H15A C15 H15C 109.5 . . ? H15B C15 H15C 109.5 . . ? N4 C16 H16A 109.1 . . ? N4 C16 H16B 109.1 . . ? H16A C16 H16B 107.8 . . ? C17 C16 N4 112.7(4) . . ? C17 C16 H16A 109.1 . . ? C17 C16 H16B 109.1 . . ? C13 C14 H14A 109.5 . . ? C13 C14 H14B 109.5 . . ? C13 C14 H14C 109.5 . . ? H14A C14 H14B 109.5 . . ? H14A C14 H14C 109.5 . . ? H14B C14 H14C 109.5 . . ? C16 C17 H17A 109.5 . . ? C16 C17 H17B 109.5 . . ? C16 C17 H17C 109.5 . . ? H17A C17 H17B 109.5 . . ? H17A C17 H17C 109.5 . . ? H17B C17 H17C 109.5 . . ? N2 C1 C13 122.4(2) . . ? N2 C1 C3 112.7(2) . . ? C13 C1 C3 124.71(19) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O3 N3 1.431(3) . ? O3 C5 1.345(3) . ? O1 H1 0.8200 . ? O1 C3 1.417(3) . ? O2 C2 1.204(3) . ? N2 N1 1.416(3) . ? N2 C1 1.280(3) . ? N1 C7 1.416(3) . ? N1 C2 1.369(3) . ? N3 C6 1.311(3) . ? C4 C6 1.403(3) . ? C4 C5 1.382(3) . ? C4 C3 1.506(3) . ? C18 C23 1.382(3) . ? C18 C6 1.489(3) . ? C18 C19 1.385(3) . ? N4 H4 0.8600 . ? N4 C5 1.333(3) . ? N4 C16 1.458(3) . ? C13 H13 0.9800 . ? C13 C15 1.491(4) . ? C13 C14 1.516(4) . ? C13 C1 1.500(3) . ? C23 H23 0.9300 . ? C23 C22 1.384(4) . ? C19 H19 0.9300 . ? C19 C20 1.377(4) . ? C3 C2 1.546(3) . ? C3 C1 1.520(3) . ? C7 C12 1.381(4) . ? C7 C8 1.386(3) . ? C12 H12 0.9300 . ? C12 C11 1.398(3) . ? C20 H20 0.9300 . ? C20 C21 1.373(5) . ? C10 H10 0.9300 . ? C10 C11 1.375(5) . ? C10 C9 1.369(5) . ? C11 H11 0.9300 . ? C22 H22 0.9300 . ? C22 C21 1.373(5) . ? C9 H9 0.9300 . ? C9 C8 1.388(4) . ? C8 H8 0.9300 . ? C21 H21 0.9300 . ? C15 H15A 0.9600 . ? C15 H15B 0.9600 . ? C15 H15C 0.9600 . ? C16 H16A 0.9700 . ? C16 H16B 0.9700 . ? C16 C17 1.427(6) . ? C14 H14A 0.9600 . ? C14 H14B 0.9600 . ? C14 H14C 0.9600 . ? C17 H17A 0.9600 . ? C17 H17B 0.9600 . ? C17 H17C 0.9600 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A O1 H1 N3 0.82 2.06 2.872(3) 169.7 3_645 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O3 N3 C6 C4 0.0(3) . . . . ? O3 N3 C6 C18 179.93(19) . . . . ? O1 C3 C2 O2 -56.6(3) . . . . ? O1 C3 C2 N1 122.4(2) . . . . ? O1 C3 C1 N2 -119.3(2) . . . . ? O1 C3 C1 C13 65.1(3) . . . . ? N2 N1 C7 C12 -15.4(3) . . . . ? N2 N1 C7 C8 163.4(2) . . . . ? N2 N1 C2 O2 178.4(3) . . . . ? N2 N1 C2 C3 -0.6(2) . . . . ? N1 N2 C1 C13 176.55(19) . . . . ? N1 N2 C1 C3 0.8(2) . . . . ? N1 C7 C12 C11 -178.2(3) . . . . ? N1 C7 C8 C9 -179.9(2) . . . . ? N3 O3 C5 C4 -1.2(3) . . . . ? N3 O3 C5 N4 178.5(3) . . . . ? C4 C3 C2 O2 62.7(3) . . . . ? C4 C3 C2 N1 -118.3(2) . . . . ? C4 C3 C1 N2 116.6(2) . . . . ? C4 C3 C1 C13 -59.0(3) . . . . ? C18 C23 C22 C21 -0.3(4) . . . . ? C18 C19 C20 C21 0.4(4) . . . . ? C23 C18 C6 N3 -74.5(3) . . . . ? C23 C18 C6 C4 105.4(3) . . . . ? C23 C18 C19 C20 -1.9(4) . . . . ? C23 C22 C21 C20 -1.2(5) . . . . ? C6 C4 C5 O3 1.1(3) . . . . ? C6 C4 C5 N4 -178.5(3) . . . . ? C6 C4 C3 O1 -176.9(2) . . . . ? C6 C4 C3 C2 62.4(3) . . . . ? C6 C4 C3 C1 -49.0(3) . . . . ? C6 C18 C23 C22 -175.9(2) . . . . ? C6 C18 C19 C20 175.8(2) . . . . ? C19 C18 C23 C22 1.8(4) . . . . ? C19 C18 C6 N3 107.9(3) . . . . ? C19 C18 C6 C4 -72.2(3) . . . . ? C19 C20 C21 C22 1.1(5) . . . . ? C5 O3 N3 C6 0.7(3) . . . . ? C5 C4 C6 N3 -0.7(3) . . . . ? C5 C4 C6 C18 179.4(2) . . . . ? C5 C4 C3 O1 5.7(3) . . . . ? C5 C4 C3 C2 -115.0(3) . . . . ? C5 C4 C3 C1 133.5(3) . . . . ? C5 N4 C16 C17 99.2(5) . . . . ? C3 C4 C6 N3 -178.6(2) . . . . ? C3 C4 C6 C18 1.5(4) . . . . ? C3 C4 C5 O3 179.1(2) . . . . ? C3 C4 C5 N4 -0.5(5) . . . . ? C7 N1 C2 O2 -7.5(4) . . . . ? C7 N1 C2 C3 173.5(2) . . . . ? C7 C12 C11 C10 -2.0(5) . . . . ? C12 C7 C8 C9 -1.1(4) . . . . ? C2 N1 C7 C12 170.7(2) . . . . ? C2 N1 C7 C8 -10.4(4) . . . . ? C2 C3 C1 N2 -1.1(2) . . . . ? C2 C3 C1 C13 -176.7(2) . . . . ? C10 C9 C8 C7 -1.8(4) . . . . ? C11 C10 C9 C8 2.7(5) . . . . ? C9 C10 C11 C12 -0.8(5) . . . . ? C8 C7 C12 C11 2.9(4) . . . . ? C15 C13 C1 N2 -3.9(4) . . . . ? C15 C13 C1 C3 171.4(3) . . . . ? C16 N4 C5 O3 -8.1(5) . . . . ? C16 N4 C5 C4 171.5(3) . . . . ? C14 C13 C1 N2 124.0(3) . . . . ? C14 C13 C1 C3 -60.8(4) . . . . ? C1 N2 N1 C7 -174.9(2) . . . . ? C1 N2 N1 C2 -0.1(3) . . . . ? C1 C3 C2 O2 -178.1(3) . . . . ? C1 C3 C2 N1 1.0(2) . . . . ?