#------------------------------------------------------------------------------ #$Date: 2024-04-11 03:52:55 +0300 (Thu, 11 Apr 2024) $ #$Revision: 291172 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/98/7159892.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7159892 loop_ _publ_author_name 'Keerthana, Pari' 'Nawaz Khan, Fazlur-Rahman' _publ_section_title ; Copper catalyzed dehydrogenative cyclization, alkenylation towards dihydroquinolinones ; _journal_name_full 'Organic & Biomolecular Chemistry' _journal_paper_doi 10.1039/D4OB00134F _journal_year 2024 _chemical_formula_moiety 'C34 H29 Cl N2 O' _chemical_formula_sum 'C34 H29 Cl N2 O' _chemical_formula_weight 517.04 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2023-05-23 deposited with the CCDC. 2024-04-08 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 103.345(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 13.6720(11) _cell_length_b 11.8313(9) _cell_length_c 17.7342(12) _cell_measurement_reflns_used 6323 _cell_measurement_temperature 300(2) _cell_measurement_theta_max 21.23 _cell_measurement_theta_min 2.30 _cell_volume 2791.2(4) _computing_cell_refinement 'Bruker APEX4/SAINT' _computing_data_collection 'Bruker APEX4' _computing_data_reduction 'Bruker APEX4/SAINT' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2018)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_temperature 300(2) _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker D8 QUEST diffractometer with PHOTON II detector' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0661 _diffrn_reflns_av_unetI/netI 0.0516 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 16 _diffrn_reflns_limit_h_min -16 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 21 _diffrn_reflns_limit_l_min -21 _diffrn_reflns_number 32805 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.701 _diffrn_reflns_theta_min 2.087 _diffrn_source 'i-mu-s microfocus source' _exptl_absorpt_coefficient_mu 0.166 _exptl_absorpt_correction_T_max 0.7453 _exptl_absorpt_correction_T_min 0.6650 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS (BRUKER)' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.230 _exptl_crystal_description block _exptl_crystal_F_000 1088 _exptl_crystal_size_max 0.193 _exptl_crystal_size_mid 0.140 _exptl_crystal_size_min 0.100 _refine_diff_density_max 0.221 _refine_diff_density_min -0.394 _refine_diff_density_rms 0.043 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.030 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 347 _refine_ls_number_reflns 5305 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.030 _refine_ls_R_factor_all 0.1192 _refine_ls_R_factor_gt 0.0549 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0511P)^2^+1.4451P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1147 _refine_ls_wR_factor_ref 0.1524 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2950 _reflns_number_total 5305 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ob00134f2.cif _cod_data_source_block SCDMPT_090523_0m_a _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 7159892 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.969 _shelx_estimated_absorpt_t_max 0.984 _shelx_res_file ; TITL SCDMPT_090523_0m_a.res in P2(1)/c SCDMPT_090523_0m_a.res created by SHELXL-2018/3 at 11:44:54 on 18-May-2023 REM Old TITL SCDMPT_090523_0m in P2(1)/c REM SHELXT solution in P2(1)/c: R1 0.239, Rweak 0.021, Alpha 0.034 REM 0.335 for 275 systematic absences, Orientation as input REM Formula found by SHELXT: C34 Cl N2 O CELL 0.71073 13.6720 11.8313 17.7342 90.000 103.345 90.000 ZERR 4.000 0.0011 0.0009 0.0012 0.000 0.003 0.000 LATT 1 SYMM -X, 1/2+Y, 1/2-Z SFAC C H CL N O UNIT 136 116 4 8 4 ACTA TEMP 26.850 SIZE 0.10 0.14 0.193 L.S. 10 BOND $H HTAB CONF LIST 4 FMAP 2 PLAN 20 WGHT 0.051100 1.445100 FVAR 0.45546 CL1 3 0.481028 1.080112 0.247652 11.00000 0.09164 0.13865 = 0.07766 0.03728 0.02745 -0.02762 O1 5 0.056833 0.723954 0.722894 11.00000 0.09365 0.08459 = 0.12279 -0.03462 0.06857 -0.02549 N1 4 0.531366 0.705292 0.470004 11.00000 0.05161 0.06561 = 0.06899 -0.00645 0.01832 0.00126 N2 4 0.263113 0.630320 0.549194 11.00000 0.05943 0.04477 = 0.04851 -0.00120 0.01773 -0.00584 C1 1 0.431925 0.866155 0.409759 11.00000 0.04597 0.05883 = 0.04041 -0.00671 0.01111 -0.01316 C2 1 0.513255 0.791109 0.417066 11.00000 0.04755 0.06545 = 0.05139 -0.01373 0.01503 -0.00969 C3 1 0.581615 0.806373 0.368552 11.00000 0.05127 0.08884 = 0.06852 -0.02059 0.02530 -0.00858 AFIX 43 H3 2 0.634780 0.756146 0.371943 11.00000 -1.20000 AFIX 0 C4 1 0.570335 0.893665 0.317084 11.00000 0.06349 0.10760 = 0.05961 -0.01286 0.02791 -0.02458 AFIX 43 H4 2 0.615701 0.903050 0.285751 11.00000 -1.20000 AFIX 0 C5 1 0.490866 0.968407 0.311686 11.00000 0.05958 0.09694 = 0.04766 0.00219 0.01792 -0.02641 C6 1 0.422419 0.956426 0.356210 11.00000 0.05109 0.07203 = 0.05037 0.00105 0.01292 -0.01221 AFIX 43 H6 2 0.369612 1.007478 0.351385 11.00000 -1.20000 AFIX 0 C7 1 0.361107 0.846320 0.456540 11.00000 0.04227 0.04769 = 0.04150 -0.00723 0.01092 -0.00972 C8 1 0.378228 0.756690 0.507054 11.00000 0.04570 0.04630 = 0.04295 -0.00475 0.01087 -0.00398 C9 1 0.467012 0.689181 0.514172 11.00000 0.05540 0.05587 = 0.05854 -0.00189 0.01552 -0.00075 C10 1 0.270654 0.919588 0.448842 11.00000 0.04837 0.04701 = 0.04304 0.00181 0.01611 -0.00421 C11 1 0.279705 1.029823 0.474547 11.00000 0.07028 0.04861 = 0.06253 0.00049 0.01636 -0.00600 AFIX 43 H11 2 0.343107 1.059964 0.494983 11.00000 -1.20000 AFIX 0 C12 1 0.195335 1.095865 0.470189 11.00000 0.10307 0.04242 = 0.08453 0.00625 0.03401 0.00723 AFIX 43 H12 2 0.201985 1.169595 0.488856 11.00000 -1.20000 AFIX 0 C13 1 0.101801 1.052958 0.438401 11.00000 0.07485 0.07769 = 0.10601 0.01924 0.02932 0.02602 AFIX 43 H13 2 0.045062 1.097826 0.434832 11.00000 -1.20000 AFIX 0 C14 1 0.092060 0.943918 0.411914 11.00000 0.05187 0.07827 = 0.11541 0.00048 0.01434 0.00526 AFIX 43 H14 2 0.028641 0.914886 0.390054 11.00000 -1.20000 AFIX 0 C15 1 0.175763 0.877209 0.417538 11.00000 0.04797 0.06077 = 0.07515 -0.00422 0.01490 -0.00329 AFIX 43 H15 2 0.168470 0.802864 0.400114 11.00000 -1.20000 AFIX 0 C16 1 0.307428 0.731795 0.557435 11.00000 0.04905 0.04491 = 0.04219 0.00030 0.01338 -0.00180 C17 1 0.197152 0.608015 0.592935 11.00000 0.05371 0.04636 = 0.04632 0.00158 0.01349 -0.00644 C18 1 0.172635 0.684878 0.645539 11.00000 0.05041 0.04523 = 0.04445 0.00181 0.01485 -0.00309 C19 1 0.223635 0.789281 0.656603 11.00000 0.05051 0.04332 = 0.04173 0.00129 0.01054 0.00103 C20 1 0.290732 0.810640 0.610741 11.00000 0.05407 0.04417 = 0.04723 -0.00186 0.01497 -0.00750 AFIX 43 H20 2 0.325172 0.879026 0.615785 11.00000 -1.20000 AFIX 0 C21 1 0.492054 0.599353 0.574728 11.00000 0.07431 0.07939 = 0.09031 0.02062 0.02353 0.02041 AFIX 137 H21A 2 0.492381 0.631289 0.624549 11.00000 -1.50000 H21B 2 0.557211 0.568712 0.575205 11.00000 -1.50000 H21C 2 0.442667 0.540317 0.563357 11.00000 -1.50000 AFIX 0 C22 1 0.150074 0.492171 0.580653 11.00000 0.07722 0.05348 = 0.06054 -0.00397 0.02121 -0.01772 AFIX 23 H22A 2 0.200437 0.438860 0.572305 11.00000 -1.20000 H22B 2 0.096718 0.493658 0.533892 11.00000 -1.20000 AFIX 0 C23 1 0.106984 0.449592 0.646960 11.00000 0.05928 0.05041 = 0.05859 0.00296 0.01905 -0.00855 C24 1 0.041349 0.542057 0.667150 11.00000 0.06177 0.06653 = 0.08666 0.00063 0.02849 -0.01353 AFIX 23 H24A 2 -0.017263 0.549747 0.624589 11.00000 -1.20000 H24B 2 0.017926 0.518262 0.712288 11.00000 -1.20000 AFIX 0 C25 1 0.089355 0.656217 0.683665 11.00000 0.05347 0.06022 = 0.06391 -0.00120 0.02165 -0.00430 C26 1 0.213880 0.878010 0.713701 11.00000 0.04568 0.04147 = 0.04768 0.00064 0.01545 -0.00213 C27 1 0.181542 0.984988 0.689346 11.00000 0.05989 0.05001 = 0.05440 0.00741 0.01436 0.00800 AFIX 43 H27 2 0.158988 0.999674 0.636672 11.00000 -1.20000 AFIX 0 C28 1 0.182253 1.070644 0.742294 11.00000 0.06265 0.04348 = 0.07543 0.00166 0.02232 0.00806 AFIX 43 H28 2 0.158516 1.141798 0.724667 11.00000 -1.20000 AFIX 0 C29 1 0.217343 1.053087 0.820676 11.00000 0.05065 0.05323 = 0.06326 -0.01253 0.02075 -0.00401 C30 1 0.249366 0.946704 0.844625 11.00000 0.06751 0.06063 = 0.04761 -0.00299 0.01230 0.00165 AFIX 43 H30 2 0.272629 0.932577 0.897311 11.00000 -1.20000 AFIX 0 C31 1 0.247980 0.860072 0.792615 11.00000 0.06708 0.04673 = 0.05239 0.00532 0.01479 0.00632 AFIX 43 H31 2 0.270207 0.788599 0.810656 11.00000 -1.20000 AFIX 0 C32 1 0.191467 0.422493 0.717134 11.00000 0.08772 0.07305 = 0.07938 0.01454 0.00604 -0.00152 AFIX 137 H32A 2 0.163263 0.398471 0.759295 11.00000 -1.50000 H32B 2 0.231767 0.488761 0.732176 11.00000 -1.50000 H32C 2 0.232594 0.363176 0.704141 11.00000 -1.50000 AFIX 0 C33 1 0.044699 0.342817 0.621935 11.00000 0.09193 0.06020 = 0.09543 0.00198 0.03093 -0.02535 AFIX 137 H33A 2 0.018060 0.315900 0.664190 11.00000 -1.50000 H33B 2 0.086611 0.285589 0.607387 11.00000 -1.50000 H33C 2 -0.009632 0.360004 0.578535 11.00000 -1.50000 AFIX 0 C34 1 0.220126 1.149081 0.877115 11.00000 0.08279 0.07242 = 0.09462 -0.03119 0.02971 -0.00669 AFIX 137 H34A 2 0.231610 1.119539 0.928835 11.00000 -1.50000 H34B 2 0.157125 1.188625 0.864904 11.00000 -1.50000 H34C 2 0.273414 1.200169 0.873526 11.00000 -1.50000 AFIX 0 HKLF 4 REM SCDMPT_090523_0m_a.res in P2(1)/c REM wR2 = 0.152438, GooF = S = 1.02969, Restrained GooF = 1.02969 for all data REM R1 = 0.054854 for 2950 Fo > 4sig(Fo) and 0.119242 for all 5305 data REM 347 parameters refined using 0 restraints END WGHT 0.0511 1.4452 REM No hydrogen bonds found for HTAB generation REM Highest difference peak 0.221, deepest hole -0.394, 1-sigma level 0.043 Q1 1 0.4723 1.1429 0.2881 11.00000 0.05 0.22 Q2 1 0.2088 1.2402 0.8384 11.00000 0.05 0.17 Q3 1 -0.0006 0.5423 0.5765 11.00000 0.05 0.17 Q4 1 -0.0151 0.3494 0.6708 11.00000 0.05 0.16 Q5 1 -0.0367 0.5562 0.6937 11.00000 0.05 0.15 Q6 1 0.5268 1.0245 0.2631 11.00000 0.05 0.14 Q7 1 0.4286 0.5582 0.5993 11.00000 0.05 0.14 Q8 1 0.3739 1.1246 0.3634 11.00000 0.05 0.14 Q9 1 0.6016 0.9167 0.2109 11.00000 0.05 0.14 Q10 1 0.4400 0.8987 0.6295 11.00000 0.05 0.14 Q11 1 0.4256 0.7283 0.6946 11.00000 0.05 0.14 Q12 1 0.1235 0.2806 0.6119 11.00000 0.05 0.13 Q13 1 0.5786 0.6780 0.6465 11.00000 0.05 0.13 Q14 1 0.3002 1.1584 0.9443 11.00000 0.05 0.13 Q15 1 0.1501 0.7612 0.4491 11.00000 0.05 0.13 Q16 1 0.2670 0.4979 0.5394 11.00000 0.05 0.13 Q17 1 0.6329 0.9380 0.3956 11.00000 0.05 0.13 Q18 1 0.1607 0.9091 0.9336 11.00000 0.05 0.13 Q19 1 0.4843 0.6260 0.7098 11.00000 0.05 0.13 Q20 1 0.2447 0.6627 0.7488 11.00000 0.05 0.12 ; _shelx_res_checksum 65305 _shelx_hkl_file ; -2 0 0 223.08 7.90 2 0 0 216.78 7.90 2 0 0 228.68 7.90 -2 0 0 222.98 8.10 -2 0 0 225.18 8.00 3 0 0 9999.00 231.08 4 0 0 4423.46 96.09 5 0 0 2.00 1.30 -5 0 0 1.30 1.20 -5 0 0 2.30 2.00 -5 0 0 0.90 1.50 5 0 0 -0.40 1.00 5 0 0 0.50 1.20 6 0 0 3.70 2.20 -6 0 0 3.50 1.70 -6 0 0 9.10 2.90 -6 0 0 3.00 2.00 6 0 0 9.50 3.30 6 0 0 5.20 2.70 -7 0 0 602.94 23.60 -7 0 0 607.84 24.70 7 0 0 610.84 23.70 -7 0 0 610.04 24.40 7 0 0 652.73 25.10 7 0 0 620.44 24.00 -8 0 0 62.39 8.90 -8 0 0 42.40 7.00 8 0 0 46.80 7.70 8 0 0 42.60 6.90 8 0 0 55.99 8.00 -8 0 0 44.00 7.80 -9 0 0 171.48 13.20 9 0 0 188.38 14.20 -9 0 0 168.38 13.90 9 0 0 197.78 14.10 9 0 0 196.78 13.60 -9 0 0 161.48 12.60 -10 0 0 112.29 12.10 10 0 0 117.49 11.50 -10 0 0 131.09 12.20 10 0 0 120.99 12.00 -10 0 0 104.19 11.30 10 0 0 110.29 11.10 -11 0 0 49.20 10.10 11 0 0 52.99 9.40 -11 0 0 30.00 9.10 11 0 0 42.20 9.00 11 0 0 31.00 6.90 12 0 0 5.70 5.00 -12 0 0 1.30 3.00 13 0 0 45.70 10.00 -13 0 0 59.09 12.30 -14 0 0 2.10 5.00 15 0 0 22.10 7.30 -15 0 0 33.50 10.20 -16 0 0 7.30 3.80 16 0 0 4.80 5.70 0 1 0 -0.20 0.20 -1 -1 0 3039.20 74.59 1 1 0 3031.60 74.49 -2 -1 0 13.60 1.90 2 -1 0 18.20 2.80 -2 -1 0 15.10 2.30 2 -1 0 17.10 2.70 -2 -1 0 15.60 2.40 2 -1 0 15.70 2.30 -2 1 0 20.50 2.80 -2 1 0 16.90 2.40 -2 1 0 17.60 2.40 2 1 0 13.40 2.40 2 1 0 12.00 2.00 2 1 0 11.10 1.90 -3 -1 0 537.75 16.20 -3 -1 0 542.55 16.60 -3 -1 0 534.15 16.80 3 -1 0 572.74 16.70 3 -1 0 526.45 16.80 -3 1 0 525.75 17.00 -3 1 0 517.95 16.40 -3 1 0 505.25 16.60 3 1 0 540.55 16.60 3 1 0 523.75 16.40 3 1 0 539.95 16.40 4 -1 0 930.41 26.70 -4 -1 0 941.01 26.30 -4 -1 0 926.01 26.80 4 -1 0 944.01 27.40 4 -1 0 908.11 26.10 -4 -1 0 940.81 26.50 4 1 0 866.21 25.80 4 1 0 916.71 26.30 4 1 0 937.11 26.40 -4 1 0 909.41 27.00 -4 1 0 901.01 26.00 -4 1 0 928.91 27.00 5 -1 0 1.00 1.30 -5 -1 0 0.30 1.10 5 -1 0 -0.40 1.10 5 -1 0 3.10 1.70 -5 -1 0 0.50 1.20 -5 -1 0 1.70 1.30 -5 1 0 1.90 2.00 -5 1 0 -0.20 1.00 -5 1 0 -0.10 1.30 5 1 0 0.60 1.30 5 1 0 1.60 1.40 6 -1 0 86.59 7.60 -6 -1 0 80.19 7.50 6 -1 0 67.99 6.80 6 -1 0 89.39 8.10 -6 -1 0 69.39 6.90 -6 -1 0 75.49 7.10 -6 1 0 79.39 7.20 6 1 0 82.59 7.20 -6 1 0 69.49 7.00 6 1 0 83.19 7.40 6 1 0 77.49 7.10 -6 1 0 77.69 7.40 -7 -1 0 65.59 8.60 -7 -1 0 66.19 7.00 7 -1 0 57.19 7.80 7 -1 0 66.09 7.10 7 -1 0 61.09 8.30 -7 -1 0 64.89 7.10 7 1 0 61.29 8.30 -7 1 0 67.39 7.60 -7 1 0 64.99 8.80 7 1 0 55.29 7.50 -7 1 0 56.59 7.80 7 1 0 73.89 7.40 8 -1 0 72.09 9.70 -8 -1 0 65.79 9.20 8 -1 0 66.89 9.40 -8 -1 0 49.99 7.90 -8 -1 0 55.39 8.20 8 -1 0 62.89 8.70 -8 1 0 73.39 9.90 8 1 0 69.99 7.90 8 1 0 51.39 7.90 -8 1 0 67.89 9.20 8 1 0 62.09 8.80 -8 1 0 61.89 9.20 9 -1 0 14.10 4.80 -9 -1 0 9.10 3.70 9 -1 0 15.70 5.50 -9 -1 0 14.60 4.70 9 -1 0 16.00 5.30 -9 -1 0 16.90 5.10 9 1 0 26.90 6.10 -9 1 0 21.60 5.50 -9 1 0 7.10 3.70 9 1 0 16.10 5.10 -9 1 0 14.50 5.00 9 1 0 16.30 5.30 -10 -1 0 34.40 7.60 -10 -1 0 29.00 6.30 10 -1 0 23.50 6.20 10 -1 0 23.10 6.10 -10 -1 0 25.50 7.30 10 -1 0 28.20 7.00 10 1 0 28.90 7.00 10 1 0 27.10 6.20 -10 1 0 29.60 7.80 10 1 0 19.20 5.90 -10 1 0 21.90 6.70 11 -1 0 29.70 7.50 -11 -1 0 27.80 8.90 11 -1 0 28.70 7.00 11 -1 0 18.40 5.90 -11 -1 0 21.70 6.90 -11 1 0 27.00 7.30 11 1 0 21.70 6.70 11 1 0 27.90 7.00 11 1 0 20.90 6.90 12 -1 0 17.60 6.40 -12 -1 0 18.10 6.50 12 1 0 8.90 5.40 -12 1 0 20.80 6.70 -13 -1 0 7.10 5.60 13 -1 0 11.90 5.20 13 1 0 3.80 5.60 -13 1 0 -3.00 2.70 -14 -1 0 43.40 10.10 14 -1 0 41.00 9.90 14 1 0 23.30 7.80 -14 1 0 41.80 10.50 15 -1 0 4.00 6.40 -15 -1 0 24.10 8.70 15 1 0 2.60 2.70 -15 1 0 12.20 5.80 -16 -1 0 10.30 4.50 16 -1 0 4.50 5.60 16 1 0 7.30 6.30 -16 1 0 4.50 3.60 0 -2 0 1062.49 26.20 0 -2 0 1059.59 23.80 0 2 0 1072.19 26.40 0 2 0 1098.39 26.30 0 2 0 1090.19 23.90 1 -2 0 697.33 17.40 -1 -2 0 715.53 18.70 1 -2 0 647.74 18.10 -1 -2 0 665.33 16.00 1 -2 0 706.03 19.20 -1 -2 0 653.43 18.30 -1 2 0 689.13 19.10 1 2 0 689.43 18.50 -1 2 0 644.54 17.90 1 2 0 669.63 18.50 1 2 0 670.53 16.10 -1 2 0 693.53 17.40 2 -2 0 97.49 5.70 -2 -2 0 92.59 5.70 2 -2 0 88.09 5.70 2 -2 0 93.59 5.50 -2 -2 0 89.99 5.50 2 -2 0 102.19 6.30 -2 -2 0 105.59 4.90 -2 2 0 95.19 5.60 2 2 0 99.59 4.80 -2 2 0 90.29 5.40 2 2 0 93.59 5.60 2 2 0 99.49 5.80 3 -2 0 1397.46 37.80 -3 -2 0 1632.34 39.00 3 -2 0 1582.94 39.30 -3 -2 0 1585.14 39.10 3 -2 0 1599.74 39.10 -3 -2 0 1559.84 37.00 -3 2 0 1548.05 38.60 3 2 0 1551.74 37.10 3 2 0 1596.54 38.70 3 2 0 1567.54 38.70 -3 2 0 1539.95 38.80 -3 2 0 1564.54 39.30 -4 -2 0 15.50 3.40 4 -2 0 19.00 3.70 4 -2 0 14.50 3.40 -4 -2 0 13.60 3.10 4 -2 0 17.40 3.70 -4 -2 0 17.10 3.30 -4 2 0 12.90 2.80 -4 2 0 18.90 3.70 4 2 0 17.10 3.50 -4 2 0 12.10 3.00 4 2 0 12.30 3.00 4 2 0 14.50 2.90 5 -2 0 5.30 2.20 -5 -2 0 5.40 2.50 -5 -2 0 5.70 2.50 5 -2 0 5.90 2.70 -5 -2 0 3.60 1.80 5 -2 0 2.40 1.80 -5 2 0 4.50 2.40 5 2 0 3.70 1.80 5 2 0 0.60 1.20 5 2 0 4.20 2.20 -5 2 0 3.20 1.90 -5 2 0 7.10 2.70 6 -2 0 3.60 2.40 -6 -2 0 5.70 2.60 -6 -2 0 5.40 2.50 6 -2 0 3.90 2.10 6 -2 0 2.30 1.70 -6 -2 0 4.10 2.40 -6 2 0 3.20 2.00 6 2 0 6.60 2.80 -6 2 0 1.50 2.10 6 2 0 3.40 2.30 -6 2 0 4.10 2.20 6 2 0 2.60 2.20 -7 -2 0 9.20 3.70 7 -2 0 8.50 2.80 7 -2 0 7.40 3.40 -7 -2 0 6.70 3.30 7 -2 0 5.20 2.70 -7 -2 0 7.90 3.30 7 2 0 10.50 3.50 -7 2 0 11.90 4.00 7 2 0 7.70 2.80 -7 2 0 7.20 2.90 -7 2 0 4.90 3.20 7 2 0 7.80 3.60 -8 -2 0 37.20 7.40 8 -2 0 28.40 6.80 -8 -2 0 30.20 6.50 -8 -2 0 36.00 6.60 8 -2 0 24.10 5.20 8 -2 0 25.30 5.70 8 2 0 18.10 4.80 -8 2 0 22.50 5.50 8 2 0 35.70 6.90 -8 2 0 31.80 7.10 -8 2 0 21.40 5.70 8 2 0 22.10 5.30 -9 -2 0 4.90 2.60 9 -2 0 -1.90 1.90 9 -2 0 -1.00 2.30 9 -2 0 -2.90 1.20 -9 -2 0 3.90 3.00 -9 -2 0 3.00 2.20 9 2 0 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0 376.06 10.80 -1 -3 0 389.16 13.80 -1 -3 0 378.76 13.70 -1 3 0 386.06 13.50 1 3 0 358.46 13.60 1 3 0 378.66 13.70 -1 3 0 366.86 11.80 -1 3 0 371.96 14.20 1 3 0 369.36 10.80 2 -3 0 189.58 9.80 -2 -3 0 192.78 9.40 -2 -3 0 180.28 9.10 2 -3 0 206.98 9.50 2 -3 0 192.68 8.60 -2 3 0 196.38 9.30 2 3 0 173.48 9.10 2 3 0 184.98 7.20 2 3 0 188.68 7.30 -2 3 0 171.68 9.50 2 3 0 173.08 8.90 -2 3 0 180.78 8.50 3 -3 0 95.59 7.10 -3 -3 0 91.69 5.40 3 -3 0 90.29 7.00 3 -3 0 95.59 6.60 -3 -3 0 71.29 6.00 3 -3 0 94.09 6.60 -3 -3 0 102.99 7.00 3 3 0 90.09 6.60 -3 3 0 83.09 6.40 3 3 0 80.29 6.30 -3 3 0 89.39 6.40 3 3 0 95.09 5.40 3 3 0 91.69 5.50 4 -3 0 23.30 4.60 4 -3 0 32.20 5.10 -4 -3 0 24.50 4.60 -4 -3 0 20.70 4.10 -4 -3 0 22.30 3.60 4 -3 0 20.50 4.00 -4 3 0 21.90 4.00 -4 3 0 23.70 4.20 4 3 0 19.90 4.10 4 3 0 16.60 3.10 4 3 0 20.90 4.20 -4 3 0 20.60 4.30 5 -3 0 189.08 11.50 -5 -3 0 167.38 9.50 5 -3 0 168.58 10.70 -5 -3 0 160.98 10.50 -5 -3 0 195.48 11.60 5 -3 0 173.58 10.60 5 3 0 167.18 9.70 -5 3 0 174.58 11.00 5 3 0 170.68 10.60 -5 3 0 163.38 10.80 5 3 0 168.68 10.70 -5 3 0 176.08 10.70 6 -3 0 26.70 5.60 -6 -3 0 28.60 5.40 6 -3 0 33.60 5.80 -6 -3 0 34.30 6.10 6 -3 0 19.00 4.40 -6 -3 0 32.30 5.20 -6 3 0 15.40 4.00 -6 3 0 31.20 5.90 6 3 0 42.90 6.70 6 3 0 24.80 4.70 6 3 0 25.20 5.00 -6 3 0 25.80 5.40 -7 -3 0 144.19 10.30 7 -3 0 141.39 11.40 -7 -3 0 160.68 12.00 7 -3 0 166.08 11.60 -7 -3 0 141.59 11.10 7 -3 0 155.08 11.70 7 3 0 149.79 11.20 -7 3 0 159.08 12.10 -7 3 0 136.49 10.90 -7 3 0 143.89 11.70 7 3 0 145.59 11.10 7 3 0 168.68 11.30 -8 -3 0 66.09 9.40 8 -3 0 56.79 8.60 -8 -3 0 66.79 9.00 -8 -3 0 66.29 9.70 8 -3 0 60.19 9.10 8 -3 0 38.20 7.20 8 3 0 56.29 8.40 8 3 0 57.09 8.50 -8 3 0 59.19 9.10 -8 3 0 64.79 9.50 8 3 0 59.59 8.70 -8 3 0 54.89 8.70 9 -3 0 4.30 2.90 9 -3 0 9.80 3.70 -9 -3 0 9.30 4.20 -9 -3 0 18.20 6.30 -9 -3 0 13.30 5.30 9 -3 0 19.80 5.60 -9 3 0 13.10 4.80 9 3 0 14.50 4.60 -9 3 0 9.00 4.30 9 3 0 9.60 3.80 -9 3 0 17.40 5.70 9 3 0 9.40 4.00 10 -3 0 0.70 1.40 -10 -3 0 1.20 3.00 -10 -3 0 0.80 2.70 -10 -3 0 0.60 2.90 10 -3 0 0.90 3.50 10 3 0 0.90 2.80 10 3 0 -1.70 2.60 -10 3 0 -1.00 3.20 -10 3 0 -0.70 2.70 -10 3 0 4.80 4.60 10 3 0 0.60 3.60 -11 -3 0 65.89 10.70 11 -3 0 96.39 14.30 11 -3 0 74.89 11.70 -11 -3 0 101.39 14.20 -11 3 0 99.49 14.50 11 3 0 99.09 13.60 11 3 0 81.59 12.10 12 -3 0 42.00 9.00 -12 -3 0 45.60 9.90 -12 3 0 36.30 9.00 12 3 0 21.90 6.90 -13 -3 0 10.20 5.80 13 -3 0 5.40 4.50 13 3 0 11.50 5.40 -13 3 0 11.80 5.90 14 -3 0 6.40 5.90 -14 -3 0 16.10 6.50 14 3 0 14.00 6.70 -14 3 0 11.10 5.50 15 -3 0 0.60 6.40 -15 -3 0 4.30 5.80 -15 3 0 4.00 6.30 15 3 0 2.50 5.10 0 -4 0 475.45 14.10 0 -4 0 490.05 17.60 0 4 0 455.35 17.50 0 4 0 477.15 17.50 0 4 0 487.95 14.00 -1 -4 0 51.09 3.50 -1 -4 0 57.29 5.40 1 -4 0 41.50 4.60 1 -4 0 49.40 4.00 -1 -4 0 54.29 5.20 -1 4 0 51.69 5.00 -1 4 0 52.19 5.40 1 4 0 44.30 6.10 -1 4 0 50.29 4.00 1 4 0 43.10 3.20 1 4 0 41.50 5.50 2 -4 0 372.16 15.70 -2 -4 0 348.77 14.80 -2 -4 0 355.96 11.40 2 -4 0 347.17 13.20 -2 -4 0 376.66 15.20 2 -4 0 378.76 15.00 -2 4 0 349.37 13.30 2 4 0 350.86 11.60 2 4 0 357.26 11.60 2 4 0 346.97 14.70 -2 4 0 358.76 14.70 -2 4 0 363.96 15.90 2 4 0 349.37 15.00 3 -4 0 348.87 15.90 3 -4 0 378.76 15.70 -3 -4 0 390.16 16.20 -3 -4 0 385.96 16.30 3 -4 0 380.66 15.10 3 -4 0 394.46 17.10 -3 4 0 375.96 15.90 3 4 0 357.06 12.80 3 4 0 384.76 16.40 3 4 0 388.46 13.00 -3 4 0 388.46 15.20 3 4 0 387.76 16.20 -4 -4 0 398.46 17.40 4 -4 0 394.96 17.50 -4 -4 0 394.86 16.90 4 -4 0 372.56 16.40 4 -4 0 387.76 17.80 4 -4 0 359.86 16.00 4 4 0 392.96 17.10 -4 4 0 368.46 16.30 4 4 0 400.06 17.00 -4 4 0 377.76 16.70 4 4 0 373.66 13.90 4 4 0 408.86 14.60 -5 -4 0 302.27 15.30 5 -4 0 291.77 16.20 -5 -4 0 273.17 15.00 -5 -4 0 277.97 12.70 5 -4 0 297.17 15.00 5 -4 0 310.97 16.00 5 -4 0 295.97 15.00 -5 4 0 299.87 15.30 5 4 0 279.37 14.80 5 4 0 311.27 15.40 -5 4 0 285.27 14.80 5 4 0 279.47 12.90 -6 -4 0 27.80 5.90 6 -4 0 27.90 6.00 6 -4 0 27.70 6.20 -6 -4 0 34.30 5.50 6 -4 0 27.30 6.30 -6 -4 0 30.60 6.40 6 -4 0 38.30 6.50 -6 4 0 25.90 6.00 6 4 0 37.30 5.80 -6 4 0 25.90 5.80 6 4 0 29.70 5.80 -6 4 0 44.40 7.10 6 4 0 23.30 5.10 7 -4 0 21.80 5.10 -7 -4 0 19.40 5.20 7 -4 0 22.90 5.60 7 -4 0 24.20 6.10 -7 -4 0 9.40 3.60 -7 -4 0 19.70 4.30 -7 4 0 10.80 4.10 7 4 0 21.10 5.10 -7 4 0 20.20 5.30 -7 4 0 15.40 4.50 7 4 0 19.90 5.00 7 4 0 22.80 5.10 -8 -4 0 6.10 3.50 -8 -4 0 -0.30 2.10 8 -4 0 13.50 5.00 -8 -4 0 7.90 4.20 8 -4 0 6.20 3.60 8 -4 0 4.90 3.10 -8 4 0 -0.70 2.10 8 4 0 5.40 2.80 -8 4 0 8.90 4.30 -8 4 0 9.70 4.10 8 4 0 -0.70 2.50 9 -4 0 48.50 9.00 9 -4 0 51.59 9.50 -9 -4 0 45.60 8.50 9 -4 0 35.70 7.30 -9 -4 0 29.80 7.40 -9 -4 0 52.39 8.50 -9 4 0 42.90 8.80 9 4 0 54.29 8.50 -9 4 0 65.99 10.90 -9 4 0 46.30 8.50 9 4 0 40.30 7.30 9 4 0 34.60 7.50 10 -4 0 -2.50 2.00 -10 -4 0 0.20 5.40 10 -4 0 3.10 3.80 10 -4 0 -2.70 1.50 -10 -4 0 -1.50 3.30 -10 -4 0 -1.90 2.30 10 4 0 2.10 3.40 -10 4 0 0.40 3.40 10 4 0 5.20 3.90 11 -4 0 21.60 7.30 -11 -4 0 31.00 7.20 -11 -4 0 23.40 7.70 11 -4 0 15.10 6.10 11 4 0 25.40 6.90 11 4 0 34.60 8.30 -11 4 0 27.60 8.10 -12 -4 0 3.50 5.20 12 -4 0 3.80 3.50 12 4 0 8.40 5.20 -12 4 0 4.10 4.10 -13 -4 0 34.20 9.50 -13 4 0 42.30 9.70 13 4 0 41.70 10.10 14 -4 0 -1.70 3.50 -14 -4 0 11.50 6.30 -14 4 0 11.20 5.20 14 4 0 -6.10 5.00 15 -4 0 0.60 3.90 -15 -4 0 2.10 4.90 15 4 0 5.10 6.30 -15 4 0 6.00 5.90 0 -5 0 0.90 1.70 0 -5 0 0.90 0.80 0 5 0 0.40 1.50 0 5 0 0.70 1.40 0 5 0 1.60 1.00 0 5 0 0.60 1.40 1 -5 0 411.16 14.40 -1 -5 0 417.86 13.40 1 -5 0 420.66 17.80 -1 -5 0 410.46 17.30 -1 -5 0 403.46 17.40 -1 5 0 438.06 18.70 1 5 0 415.16 17.90 1 5 0 422.46 13.20 -1 5 0 401.26 17.10 -1 5 0 421.16 14.50 1 5 0 410.66 17.50 -1 5 0 416.76 17.80 2 -5 0 145.19 8.30 -2 -5 0 138.19 9.60 2 -5 0 143.89 9.50 -2 -5 0 137.39 9.50 -2 -5 0 142.29 6.80 2 -5 0 131.29 9.60 2 5 0 133.29 9.50 -2 5 0 138.69 9.20 2 5 0 144.69 10.10 -2 5 0 146.99 8.40 -2 5 0 124.49 9.70 2 5 0 136.59 6.80 3 -5 0 85.19 6.80 3 -5 0 88.59 7.50 -3 -5 0 89.29 7.90 -3 -5 0 82.09 7.60 3 -5 0 77.29 7.80 -3 5 0 70.89 7.10 -3 5 0 81.49 6.80 3 5 0 80.29 7.40 3 5 0 86.59 7.80 -3 5 0 96.29 8.90 3 5 0 77.69 5.30 3 5 0 72.59 5.20 4 -5 0 288.37 16.00 -4 -5 0 283.77 15.40 -4 -5 0 300.97 15.60 4 -5 0 287.57 14.40 4 -5 0 316.97 15.60 4 -5 0 304.07 16.00 -4 5 0 319.47 15.80 -4 5 0 314.27 15.00 4 5 0 311.77 12.70 4 5 0 301.77 15.90 4 5 0 306.57 12.40 4 5 0 311.77 15.80 -5 -5 0 103.99 9.30 5 -5 0 80.39 7.90 5 -5 0 98.09 8.40 -5 -5 0 103.49 9.40 5 -5 0 81.99 8.40 5 -5 0 84.19 8.80 5 5 0 96.99 6.90 5 5 0 80.89 8.00 5 5 0 98.69 9.10 -5 5 0 89.19 8.60 -5 5 0 80.69 7.90 5 5 0 96.89 7.20 6 -5 0 91.69 8.80 -6 -5 0 82.69 8.80 6 -5 0 109.49 9.70 6 -5 0 90.59 9.40 -6 -5 0 109.89 9.80 6 -5 0 122.99 11.10 6 5 0 95.59 7.80 6 5 0 95.79 9.10 6 5 0 92.19 7.50 6 5 0 87.39 8.90 -6 5 0 98.69 9.10 -6 5 0 90.69 9.10 -7 -5 0 -1.10 1.80 -7 -5 0 2.70 1.80 -7 -5 0 4.30 2.60 7 -5 0 0.40 2.60 7 -5 0 0.50 2.80 7 -5 0 -0.10 2.90 7 -5 0 2.70 2.60 -7 5 0 -1.40 2.10 7 5 0 1.50 2.20 7 5 0 -1.10 1.30 -7 5 0 3.70 2.50 7 5 0 -1.00 2.20 -8 -5 0 145.09 13.10 8 -5 0 153.48 12.70 -8 -5 0 150.28 12.90 8 -5 0 157.38 14.50 8 -5 0 155.08 13.00 8 -5 0 127.49 11.60 -8 -5 0 132.69 10.50 -8 5 0 173.28 14.00 8 5 0 165.78 13.40 8 5 0 117.69 10.20 8 5 0 149.39 12.80 -8 5 0 142.09 12.60 -8 5 0 149.49 12.80 9 -5 0 -0.30 3.00 -9 -5 0 -2.00 2.40 9 -5 0 -4.70 2.60 -9 -5 0 1.20 4.30 9 -5 0 -0.80 4.10 9 -5 0 2.40 3.10 -9 -5 0 3.30 3.80 9 5 0 -2.30 2.40 -9 5 0 0.30 2.60 -9 5 0 -1.60 3.70 9 5 0 -1.60 2.20 -9 5 0 -3.40 3.40 9 5 0 -0.40 2.50 10 -5 0 49.10 9.50 -10 -5 0 52.69 8.70 -10 -5 0 54.59 10.90 -10 -5 0 52.99 10.40 10 -5 0 58.29 10.40 10 5 0 49.40 8.70 10 5 0 45.10 9.30 -10 5 0 45.60 9.10 -11 -5 0 5.40 4.50 -11 -5 0 6.60 4.80 11 -5 0 2.40 3.60 11 -5 0 1.50 5.80 -11 5 0 8.20 4.60 11 5 0 2.50 4.30 -12 -5 0 41.90 10.20 12 -5 0 42.30 9.60 -12 5 0 39.20 10.00 12 5 0 27.40 8.00 13 -5 0 -1.10 4.70 -13 -5 0 6.50 5.00 -13 5 0 4.00 5.50 13 5 0 7.20 5.70 -14 -5 0 6.70 5.40 14 -5 0 -4.10 3.70 -14 5 0 4.90 4.10 14 5 0 -7.10 4.20 -15 -5 0 5.10 6.50 15 -5 0 8.60 7.00 -15 5 0 2.00 4.70 15 5 0 2.30 4.50 0 -6 0 139.39 10.30 0 -6 0 162.98 8.10 0 6 0 145.69 7.60 0 6 0 118.09 9.80 0 6 0 136.09 10.50 0 6 0 144.89 10.50 -1 -6 0 103.19 8.80 1 -6 0 108.89 9.20 -1 -6 0 106.49 6.20 1 -6 0 95.99 6.50 -1 -6 0 96.89 8.70 1 6 0 86.89 8.30 -1 6 0 106.29 9.00 -1 6 0 103.39 8.80 -1 6 0 103.19 6.80 -1 6 0 97.39 9.20 1 6 0 99.69 8.80 1 6 0 101.19 6.10 -2 -6 0 7.10 3.00 -2 -6 0 8.80 3.50 2 -6 0 9.10 2.80 2 -6 0 6.70 2.90 -2 -6 0 6.50 2.00 2 6 0 3.40 2.00 -2 6 0 4.90 2.70 2 6 0 5.50 1.90 2 6 0 9.60 3.40 -2 6 0 7.30 3.10 -2 6 0 7.20 2.40 -3 -6 0 33.50 5.70 -3 -6 0 44.20 7.00 3 -6 0 53.99 5.70 3 -6 0 62.29 8.70 3 -6 0 53.79 7.60 3 6 0 62.59 8.40 -3 6 0 46.60 7.10 3 6 0 51.39 7.90 3 6 0 57.99 4.80 -3 6 0 57.39 8.80 3 6 0 49.30 4.50 -3 6 0 50.69 5.70 4 -6 0 93.09 9.20 4 -6 0 74.29 7.70 -4 -6 0 91.79 8.80 -4 -6 0 72.69 7.90 4 -6 0 95.79 8.10 4 -6 0 81.19 8.90 -4 6 0 69.39 9.00 4 6 0 83.39 6.20 -4 6 0 79.99 7.60 4 6 0 94.99 6.60 4 6 0 73.19 8.00 4 6 0 98.69 9.20 5 -6 0 3.00 2.60 -5 -6 0 0.00 1.80 -5 -6 0 2.80 2.80 5 -6 0 0.00 2.80 5 -6 0 2.70 2.20 5 -6 0 3.00 2.40 5 6 0 0.60 2.20 5 6 0 1.50 1.90 5 6 0 2.20 2.00 -5 6 0 3.40 2.60 5 6 0 1.30 1.80 -5 6 0 1.10 2.20 6 -6 0 17.80 4.90 6 -6 0 17.00 5.10 6 -6 0 11.40 4.60 -6 -6 0 18.30 5.40 -6 -6 0 20.40 5.50 6 -6 0 23.50 5.30 -6 6 0 10.00 4.00 6 6 0 21.20 4.60 6 6 0 23.10 5.80 6 6 0 21.60 5.50 -6 6 0 27.10 6.40 6 6 0 14.80 4.00 -7 -6 0 48.60 8.80 7 -6 0 53.59 8.90 7 -6 0 48.30 8.60 7 -6 0 50.09 8.30 -7 -6 0 63.59 10.10 7 -6 0 44.40 9.00 7 6 0 45.40 7.10 7 6 0 50.19 9.10 -7 6 0 48.10 8.70 -7 6 0 44.10 7.90 7 6 0 62.29 9.20 7 6 0 49.00 6.90 -8 -6 0 -4.90 2.90 8 -6 0 -2.30 2.30 8 -6 0 4.50 4.00 8 -6 0 1.60 2.80 -8 -6 0 0.80 1.80 8 -6 0 1.10 4.00 8 6 0 1.80 2.80 8 6 0 -2.60 2.20 -8 6 0 1.10 4.50 8 6 0 -1.10 2.30 -8 6 0 -4.70 2.70 9 -6 0 -3.80 4.00 -9 -6 0 -2.60 3.30 -9 -6 0 4.40 3.00 -9 -6 0 2.10 4.70 9 -6 0 3.40 3.20 9 -6 0 2.70 3.20 9 6 0 1.10 2.30 9 6 0 1.50 3.10 9 6 0 4.60 3.70 10 -6 0 40.20 8.80 -10 -6 0 44.60 8.10 10 -6 0 49.40 10.40 10 -6 0 33.40 9.10 -10 -6 0 39.80 9.30 10 6 0 50.29 10.30 10 6 0 54.19 8.90 10 6 0 54.69 8.80 11 -6 0 4.20 3.70 -11 -6 0 4.30 5.00 11 -6 0 -0.40 4.30 11 6 0 0.20 4.00 12 -6 0 1.40 5.30 12 -6 0 6.80 7.60 12 6 0 3.50 4.20 13 -6 0 7.20 4.60 13 -6 0 9.50 6.60 -13 -6 0 6.20 6.00 -13 6 0 4.90 6.30 13 6 0 10.40 6.40 -14 -6 0 14.90 7.60 14 -6 0 -11.40 5.20 14 -6 0 0.20 3.50 14 6 0 -10.20 5.70 -14 6 0 -0.20 5.60 0 -7 0 -1.40 1.30 0 7 0 -0.70 2.40 0 7 0 1.60 1.40 0 7 0 4.90 2.70 0 7 0 1.50 2.30 -1 -7 0 76.69 5.70 1 -7 0 53.09 8.00 1 -7 0 75.69 6.20 -1 -7 0 79.79 8.60 1 7 0 80.39 5.80 -1 7 0 97.49 7.10 1 7 0 80.99 8.40 -1 7 0 85.79 8.80 1 7 0 91.99 9.40 -1 7 0 75.69 10.20 -1 7 0 86.79 8.90 2 -7 0 4.30 2.30 -2 -7 0 6.60 2.50 -2 -7 0 4.30 3.40 2 -7 0 2.00 2.40 -2 -7 0 4.00 1.40 2 7 0 2.60 2.30 -2 7 0 1.80 3.00 2 7 0 1.60 1.70 2 7 0 -0.80 1.80 -2 7 0 3.40 2.50 -2 7 0 7.90 3.80 -2 7 0 4.30 2.40 3 -7 0 65.59 6.70 3 -7 0 42.90 7.60 -3 -7 0 51.69 8.30 -3 -7 0 64.79 8.90 -3 7 0 45.20 7.70 3 7 0 61.39 5.20 -3 7 0 61.49 6.50 3 7 0 56.09 8.90 -3 7 0 49.10 8.50 3 7 0 47.70 4.70 3 7 0 56.59 8.50 4 -7 0 21.70 5.80 4 -7 0 34.10 6.20 4 -7 0 26.40 6.00 -4 -7 0 27.70 6.50 -4 -7 0 33.10 6.80 4 -7 0 30.90 6.00 -4 7 0 29.50 7.00 4 7 0 39.50 7.50 4 7 0 27.40 4.30 4 7 0 46.50 8.10 -4 7 0 33.40 7.00 4 7 0 33.20 5.00 5 -7 0 -1.00 1.80 5 -7 0 6.00 3.20 -5 -7 0 0.20 2.10 5 -7 0 3.10 3.30 -5 -7 0 3.70 3.50 5 -7 0 6.80 3.10 5 7 0 4.90 2.20 -5 7 0 2.70 2.70 -5 7 0 1.40 2.70 5 7 0 0.70 2.50 5 7 0 3.20 2.00 5 7 0 1.70 2.60 6 -7 0 17.60 5.90 6 -7 0 21.80 6.10 -6 -7 0 15.30 5.50 -6 -7 0 27.80 6.80 6 -7 0 11.80 4.10 6 -7 0 15.10 4.30 6 7 0 14.80 4.00 6 7 0 15.60 5.20 6 7 0 18.50 4.20 -6 7 0 10.80 4.80 6 7 0 19.30 5.60 -6 7 0 17.60 5.50 -7 -7 0 37.70 8.10 7 -7 0 17.40 6.20 -7 -7 0 28.10 6.90 7 -7 0 27.90 7.70 7 -7 0 31.10 7.30 7 -7 0 17.90 5.20 -7 7 0 30.00 7.10 -7 7 0 22.30 6.70 7 7 0 28.30 7.20 7 7 0 32.70 6.40 7 7 0 26.70 5.50 7 7 0 27.90 8.30 8 -7 0 7.70 3.90 8 -7 0 -2.20 5.20 -8 -7 0 3.60 5.00 8 -7 0 3.10 4.20 8 7 0 5.00 4.10 8 7 0 0.50 2.50 8 7 0 -2.80 2.40 -8 7 0 2.50 3.80 -9 -7 0 0.30 3.30 9 -7 0 -5.40 4.00 9 -7 0 -2.90 4.80 9 -7 0 4.90 4.40 9 7 0 6.70 4.10 9 7 0 1.40 3.50 10 -7 0 2.30 5.60 10 -7 0 6.10 3.40 -10 -7 0 4.20 4.60 10 7 0 7.10 4.60 11 -7 0 0.70 5.40 -11 -7 0 -1.10 2.20 11 -7 0 -0.20 2.60 11 7 0 4.60 4.40 12 -7 0 2.20 3.40 12 -7 0 3.50 6.30 -12 -7 0 6.20 4.60 12 7 0 -5.30 4.40 -13 -7 0 0.40 5.40 13 -7 0 1.70 6.90 13 -7 0 10.50 6.10 13 7 0 1.00 6.10 14 -7 0 -12.70 9.00 14 -7 0 -0.70 4.50 -14 -7 0 2.80 4.00 0 -8 0 64.59 5.80 0 -8 0 88.99 9.60 0 8 0 70.79 6.00 0 8 0 74.39 10.20 0 8 0 73.59 10.60 0 8 0 66.09 9.80 -1 -8 0 -0.30 2.60 1 -8 0 6.70 2.50 -1 -8 0 2.30 1.80 1 -8 0 0.40 2.10 -1 8 0 3.90 2.60 1 8 0 0.00 2.50 -1 8 0 -0.40 2.30 1 8 0 1.90 2.40 -1 8 0 1.70 2.70 1 8 0 3.20 2.00 -1 8 0 3.80 2.90 1 8 0 -0.30 2.60 -2 -8 0 108.89 7.00 -2 -8 0 105.29 10.50 2 -8 0 87.79 9.70 -2 -8 0 116.89 10.90 2 -8 0 111.39 8.40 -2 8 0 105.89 11.40 2 8 0 112.09 10.80 2 8 0 115.69 11.00 -2 8 0 102.19 8.40 -2 8 0 104.69 10.80 -2 8 0 94.69 10.10 2 8 0 114.19 7.30 -3 -8 0 89.99 9.60 3 -8 0 80.29 11.40 3 -8 0 67.09 6.90 -3 -8 0 79.69 10.80 -3 8 0 53.49 9.20 3 8 0 66.29 10.40 3 8 0 68.09 5.80 3 8 0 63.29 5.50 -3 8 0 75.19 7.60 3 8 0 69.49 10.30 -3 8 0 79.79 11.00 -4 -8 0 25.10 6.30 4 -8 0 13.20 4.90 -4 -8 0 23.20 6.10 4 -8 0 15.20 5.00 4 -8 0 26.20 5.60 -4 8 0 25.70 5.80 -4 8 0 19.80 6.20 4 8 0 23.50 6.40 -4 8 0 11.90 6.10 4 8 0 21.90 4.30 4 8 0 34.10 7.50 4 8 0 26.00 4.40 -5 -8 0 107.29 11.60 5 -8 0 115.59 11.30 5 -8 0 119.79 10.40 5 -8 0 133.89 12.80 5 -8 0 122.99 12.20 -5 -8 0 128.39 12.30 5 8 0 149.79 13.80 -5 8 0 123.39 12.60 5 8 0 118.99 11.80 5 8 0 129.09 8.80 -5 8 0 119.09 10.70 5 8 0 117.29 8.60 -6 -8 0 1.30 4.90 6 -8 0 1.80 3.90 -6 -8 0 2.00 3.50 6 -8 0 0.80 3.10 6 -8 0 -2.20 2.10 6 -8 0 -2.80 2.50 6 8 0 5.00 3.00 -6 8 0 -1.80 3.50 -6 8 0 -1.00 2.00 6 8 0 -3.20 2.00 6 8 0 0.60 3.40 -7 -8 0 10.90 7.30 7 -8 0 0.70 2.60 7 -8 0 0.70 4.80 7 -8 0 5.60 3.90 -7 -8 0 0.10 2.50 7 8 0 4.00 3.30 -7 8 0 0.30 3.90 7 8 0 10.70 5.00 8 -8 0 1.60 2.70 -8 -8 0 4.10 3.70 8 -8 0 1.60 5.80 -8 -8 0 4.50 6.30 8 -8 0 5.70 5.00 8 8 0 3.70 3.70 8 8 0 -3.40 2.90 -9 -8 0 -2.60 3.00 9 -8 0 -0.90 2.80 9 -8 0 -3.60 4.80 9 8 0 -3.80 3.30 9 8 0 -2.50 2.30 10 -8 0 15.10 6.10 10 -8 0 -0.80 5.20 -10 -8 0 11.10 6.00 10 8 0 10.90 5.20 11 -8 0 12.70 5.90 -11 -8 0 -0.70 2.60 11 -8 0 -2.10 6.20 12 -8 0 -9.10 4.90 -12 -8 0 -3.20 4.00 12 -8 0 -1.00 2.60 -13 -8 0 -1.50 4.70 13 -8 0 -14.20 6.20 13 -8 0 -1.50 2.80 0 -9 0 -1.90 1.40 0 -9 0 -3.60 1.30 0 9 0 0.40 2.20 0 9 0 -2.20 2.50 0 9 0 -0.60 4.30 0 9 0 2.80 3.20 1 -9 0 47.70 6.50 1 -9 0 39.90 8.20 -1 -9 0 51.19 9.20 -1 -9 0 53.09 5.20 1 9 0 45.40 8.50 -1 9 0 44.30 8.60 1 9 0 43.30 8.70 -1 9 0 38.50 8.10 1 9 0 37.60 8.00 -1 9 0 53.59 10.00 1 9 0 41.80 5.60 -1 9 0 52.39 6.90 2 -9 0 16.10 3.90 2 -9 0 14.10 4.80 -2 -9 0 15.90 3.50 -2 -9 0 14.30 5.50 -2 9 0 30.70 6.90 2 9 0 7.20 3.70 2 9 0 12.70 3.30 -2 9 0 12.90 5.30 -2 9 0 9.00 3.70 -2 9 0 13.70 5.50 2 9 0 17.30 5.70 3 -9 0 67.59 7.40 -3 -9 0 39.90 8.20 -3 -9 0 51.69 9.10 3 -9 0 43.80 8.70 -3 9 0 52.39 10.00 3 9 0 59.69 5.90 3 9 0 62.39 10.40 -3 9 0 86.19 12.40 3 9 0 55.49 10.20 3 9 0 62.99 6.00 -3 9 0 68.89 8.90 -3 9 0 51.99 10.30 4 -9 0 87.89 12.60 -4 -9 0 109.39 11.80 -4 -9 0 95.79 12.60 4 -9 0 105.29 9.80 4 9 0 92.39 7.40 -4 9 0 93.59 9.50 -4 9 0 62.59 12.00 4 9 0 91.69 7.60 4 9 0 118.99 12.30 -4 9 0 77.49 13.80 -5 -9 0 -0.70 2.80 -5 -9 0 4.20 3.40 5 -9 0 0.70 2.80 5 -9 0 -1.30 3.90 5 -9 0 -2.00 2.70 5 9 0 2.40 2.70 5 9 0 4.30 2.80 -5 9 0 -5.90 2.30 6 -9 0 10.80 4.20 6 -9 0 29.40 8.60 -6 -9 0 15.60 6.10 6 -9 0 20.70 6.90 -6 -9 0 26.60 7.80 -6 9 0 23.80 6.70 6 9 0 14.50 4.30 6 9 0 22.90 7.20 -7 -9 0 -4.80 5.20 7 -9 0 10.90 5.80 -7 -9 0 2.70 4.10 7 -9 0 7.80 3.90 7 9 0 21.80 6.70 -7 9 0 4.50 5.10 7 9 0 11.00 4.30 -8 -9 0 9.70 5.40 8 -9 0 1.00 3.60 8 -9 0 13.00 5.80 8 9 0 2.30 3.60 9 -9 0 -6.00 3.70 -9 -9 0 5.80 4.00 9 -9 0 3.50 3.90 10 -9 0 11.90 5.20 10 -9 0 -7.60 4.50 11 -9 0 1.00 2.80 11 -9 0 -5.80 6.80 -11 -9 0 -7.00 3.40 12 -9 0 -0.70 3.90 12 -9 0 -6.40 5.70 -12 -9 0 -0.40 4.40 0 -10 0 5.70 3.30 0 -10 0 9.20 3.00 0 10 0 15.30 5.50 -1 -10 0 53.19 5.50 -1 -10 0 50.49 10.00 1 -10 0 47.90 9.70 1 -10 0 39.80 6.10 -1 10 0 63.29 11.00 1 10 0 44.80 9.00 -2 -10 0 2.00 1.70 2 -10 0 -2.10 2.50 2 -10 0 -2.10 1.90 -2 -10 0 0.30 3.20 2 10 0 1.20 2.90 -2 10 0 -1.70 5.40 -2 10 0 2.90 3.10 3 -10 0 128.69 10.60 -3 -10 0 133.49 13.70 3 -10 0 160.68 14.70 -3 10 0 148.79 15.00 -3 10 0 119.89 15.50 3 10 0 139.09 13.70 3 10 0 134.89 8.90 -4 -10 0 25.90 7.50 4 -10 0 20.70 5.80 4 -10 0 23.50 6.60 -4 -10 0 20.30 6.70 -4 10 0 24.10 7.30 4 10 0 17.70 6.50 -4 10 0 13.40 6.10 -5 -10 0 0.10 3.50 5 -10 0 3.10 3.70 5 -10 0 0.30 3.20 -5 -10 0 -5.30 4.60 5 10 0 1.60 3.60 -5 10 0 -7.70 5.90 -6 -10 0 73.09 12.70 6 -10 0 91.29 12.00 6 -10 0 86.59 13.70 6 10 0 96.29 14.50 -7 -10 0 5.40 4.00 7 -10 0 7.70 5.30 7 -10 0 8.50 4.20 7 10 0 1.70 3.60 8 -10 0 24.10 7.00 -8 -10 0 26.70 7.10 8 -10 0 26.10 8.80 9 -10 0 6.60 4.00 -9 -10 0 16.00 6.50 9 -10 0 0.60 4.80 10 -10 0 4.30 5.90 -10 -10 0 8.60 6.50 10 -10 0 1.30 4.30 11 -10 0 6.60 5.20 -11 -10 0 2.10 4.20 11 -10 0 6.40 6.30 0 -11 0 1.50 3.00 0 11 0 -0.60 2.90 -1 -11 0 15.10 5.50 1 -11 0 18.80 4.70 1 -11 0 20.60 6.50 1 11 0 17.90 7.30 -1 11 0 11.20 5.80 -2 -11 0 72.09 11.80 2 -11 0 76.69 12.50 2 -11 0 82.09 8.50 2 11 0 100.89 14.80 -2 11 0 78.29 13.30 -3 -11 0 28.40 8.20 3 -11 0 32.80 8.80 3 -11 0 28.40 6.40 -3 11 0 18.60 7.60 3 11 0 23.00 7.10 -4 -11 0 42.50 9.20 4 -11 0 39.10 9.50 -4 11 0 46.30 9.90 4 11 0 57.29 11.40 -5 -11 0 -6.30 3.20 5 -11 0 -4.50 3.80 5 -11 0 -2.00 2.60 -5 11 0 -1.70 3.70 5 11 0 0.40 3.70 -6 -11 0 19.60 7.10 6 -11 0 23.40 6.30 6 -11 0 36.40 9.10 7 -11 0 28.10 8.80 -7 -11 0 31.00 8.90 7 -11 0 19.60 6.80 -8 -11 0 4.50 3.40 8 -11 0 3.40 4.40 8 -11 0 -3.30 3.80 9 -11 0 17.30 8.10 -9 -11 0 14.70 6.30 9 -11 0 8.80 5.70 -10 -11 0 4.50 5.90 10 -11 0 10.90 5.50 10 -11 0 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6.00 -5 -3 -4 71.89 6.20 5 3 4 51.49 7.40 -5 3 -4 70.49 7.70 -5 3 -4 63.29 5.80 -5 3 -4 81.19 8.00 5 3 4 81.19 6.50 5 3 4 66.49 7.00 6 -3 4 18.10 4.10 6 -3 4 15.20 4.90 -6 -3 -4 12.40 3.80 -6 -3 -4 6.90 3.50 6 -3 4 21.70 5.60 -6 -3 -4 13.20 3.70 6 3 4 17.00 4.10 6 3 4 11.20 3.90 -6 3 -4 10.70 4.00 -6 3 -4 11.60 4.20 6 3 4 11.20 4.20 -6 3 -4 11.30 3.30 -7 -3 -4 229.78 15.30 -7 -3 -4 259.17 15.50 7 -3 4 251.27 16.40 7 -3 4 258.87 13.60 -7 -3 -4 260.07 14.40 7 3 4 242.98 14.10 -7 3 -4 279.57 14.80 -7 3 -4 246.48 16.30 7 3 4 264.77 16.30 -7 3 -4 240.58 16.00 7 3 4 264.77 15.10 8 -3 4 31.60 7.30 8 -3 4 31.40 5.70 -8 -3 -4 45.10 8.00 -8 -3 -4 39.00 6.70 8 -3 4 32.20 7.20 -8 -3 -4 33.20 7.20 -8 3 -4 37.00 6.70 -8 3 -4 51.19 9.10 -8 3 -4 36.50 7.60 8 3 4 41.90 7.10 8 3 4 39.60 7.00 8 3 4 34.00 7.40 9 -3 4 4.60 3.90 -9 -3 -4 2.90 3.20 -9 -3 -4 -1.90 2.60 9 -3 4 -3.40 3.00 9 3 4 -1.90 2.60 9 3 4 5.60 3.30 -9 3 -4 -0.10 4.40 9 3 4 3.00 2.50 10 -3 4 48.20 8.70 -10 -3 -4 63.09 10.40 -10 -3 -4 50.99 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243.68 11.00 1 4 -4 253.87 12.60 0 -4 4 1.10 0.90 0 -4 -4 1.30 1.30 0 -4 -4 4.20 2.20 0 -4 4 -0.30 1.40 0 -4 4 3.20 1.90 0 4 -4 -0.30 1.30 0 4 -4 -0.30 1.30 0 4 -4 0.90 1.50 0 4 4 2.30 1.60 0 4 4 0.50 1.80 0 4 -4 1.80 1.30 -1 -4 -4 93.09 6.70 1 -4 4 78.09 6.90 -1 -4 -4 83.09 7.20 1 -4 4 79.59 5.30 1 -4 4 90.69 7.40 1 4 4 95.89 6.80 -1 4 -4 77.89 6.80 -1 4 -4 85.69 6.00 1 4 4 78.49 7.40 -1 4 -4 88.29 7.50 2 -4 4 332.87 15.70 -2 -4 -4 325.77 9.00 2 -4 4 325.87 12.30 2 -4 4 339.47 15.60 -2 -4 -4 343.87 14.50 -2 -4 -4 336.57 15.60 -2 4 -4 309.97 15.20 -2 4 -4 307.27 14.80 2 4 4 320.77 14.30 2 4 4 343.67 9.00 -2 4 -4 317.27 12.90 2 4 4 313.37 15.50 3 -4 4 5.90 2.70 -3 -4 -4 10.20 3.20 3 -4 4 6.70 2.40 3 -4 4 6.10 2.40 3 -4 4 11.00 3.80 -3 -4 -4 11.60 3.50 -3 -4 -4 10.50 1.90 3 4 4 10.00 1.90 -3 4 -4 8.30 3.20 3 4 4 5.80 2.90 -3 4 -4 9.40 3.10 3 4 4 7.30 2.40 4 -4 4 111.09 9.40 4 -4 4 107.39 7.50 -4 -4 -4 95.89 8.20 4 -4 4 91.19 6.80 -4 -4 -4 101.89 8.50 -4 -4 -4 96.89 6.10 4 -4 4 86.49 8.70 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1.00 4.30 13 -7 -5 7.50 4.00 13 -7 -5 3.60 5.50 13 7 -5 0.60 5.30 12 -7 -5 79.49 15.10 -12 -7 5 98.39 16.30 12 -7 -5 134.59 14.70 12 7 -5 101.39 14.90 11 -7 -5 3.60 4.30 -11 -7 5 7.40 5.20 11 -7 -5 5.30 4.00 11 7 -5 4.10 4.60 -10 -7 5 -0.40 3.50 10 -7 -5 7.70 4.10 10 -7 -5 0.30 4.50 10 7 -5 -3.30 2.80 9 -7 -5 0.00 4.30 -9 -7 5 -3.80 2.90 9 -7 -5 6.20 4.00 9 7 -5 0.00 3.30 9 7 -5 2.70 4.90 -9 7 5 6.70 5.00 8 -7 -5 66.89 13.30 8 -7 -5 76.49 10.70 -8 -7 5 82.49 13.10 8 7 -5 106.29 10.90 -8 7 5 75.19 10.80 8 7 -5 73.09 11.20 7 -7 -5 11.70 4.40 -7 -7 5 8.80 4.30 -7 -7 5 7.40 4.90 7 -7 -5 14.50 6.00 7 -7 -5 4.40 3.90 7 7 -5 7.30 4.00 -7 7 5 8.10 4.00 7 7 -5 7.20 4.00 7 7 -5 12.30 4.80 7 7 -5 9.20 4.00 -7 7 5 10.50 4.40 6 -7 -5 5.00 3.20 -6 -7 5 6.30 4.50 6 -7 -5 0.30 3.10 6 -7 -5 0.00 2.30 -6 -7 5 4.10 3.30 6 7 -5 5.40 3.00 -6 7 5 2.30 3.50 6 7 -5 4.10 3.10 6 7 -5 5.90 2.90 6 7 -5 5.80 3.40 -6 7 5 8.50 3.50 5 -7 -5 178.38 15.90 5 -7 -5 221.78 12.30 -5 -7 5 192.78 14.00 -5 -7 5 168.08 13.40 5 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33.90 7.90 1 7 -5 27.50 5.60 1 7 -5 39.20 7.10 0 -7 5 208.98 13.50 0 -7 5 217.58 12.40 0 -7 -5 185.08 14.30 0 7 5 187.58 15.20 0 7 -5 218.38 15.00 0 7 -5 196.88 12.90 0 7 -5 201.88 12.90 0 7 5 200.88 12.90 0 7 -5 214.28 14.60 -1 -7 -5 8.40 3.90 -1 -7 -5 7.40 2.90 1 -7 5 3.60 2.50 1 -7 5 4.60 3.20 1 -7 5 2.60 2.70 -1 7 -5 5.90 4.00 -1 7 -5 7.30 3.60 -1 7 -5 7.50 3.50 -1 7 -5 7.90 3.20 1 7 5 1.30 2.50 1 7 5 8.20 3.30 -2 -7 -5 10.80 3.90 2 -7 5 15.50 4.30 -2 -7 -5 16.40 4.50 2 -7 5 8.70 3.80 2 -7 5 4.80 3.10 -2 7 -5 8.00 4.40 2 7 5 10.00 4.00 2 7 5 9.50 3.30 -2 7 -5 14.60 4.60 -2 7 -5 7.60 3.50 -3 -7 -5 21.50 4.10 3 -7 5 28.00 6.20 3 -7 5 21.80 5.50 -3 -7 -5 23.80 6.20 3 -7 5 33.30 6.00 -3 7 -5 21.90 5.70 3 7 5 21.60 5.60 3 7 5 30.80 7.40 -3 7 -5 20.80 5.90 -3 7 -5 19.20 5.50 -4 -7 -5 6.00 3.40 4 -7 5 10.10 3.20 4 -7 5 1.70 2.60 -4 -7 -5 6.10 2.80 4 -7 5 6.10 3.00 4 -7 5 5.40 3.30 -4 7 -5 5.70 4.50 4 7 5 6.10 1.10 4 7 5 5.30 1.00 4 7 5 3.70 2.40 -4 7 -5 0.00 3.40 4 7 5 3.20 2.30 5 -7 5 135.19 13.10 5 -7 5 127.39 10.40 5 -7 5 140.39 11.10 -5 -7 -5 157.48 13.60 5 -7 5 130.99 12.20 -5 -7 -5 119.89 11.70 5 7 5 152.28 13.00 5 7 5 136.89 6.70 -5 7 -5 116.19 12.70 -5 7 -5 114.69 11.70 5 7 5 126.19 6.60 5 7 5 136.19 12.90 6 -7 5 52.89 10.00 6 -7 5 43.60 7.70 6 -7 5 43.60 8.80 -6 -7 -5 47.20 9.10 -6 -7 -5 42.90 8.50 6 -7 5 58.59 8.10 6 7 5 55.49 5.40 -6 7 -5 52.39 9.60 6 7 5 64.29 10.20 7 -7 5 27.60 7.90 -7 -7 -5 26.00 7.50 7 -7 5 14.80 5.60 -7 -7 -5 23.80 7.10 7 -7 5 26.70 7.80 7 7 5 16.60 5.40 7 7 5 16.30 4.10 -7 7 -5 13.40 6.60 -8 -7 -5 9.70 4.50 8 -7 5 5.90 4.80 8 -7 5 11.60 4.80 8 -7 5 11.10 5.40 8 7 5 11.40 5.20 9 -7 5 6.40 4.40 -9 -7 -5 3.20 4.00 9 -7 5 4.30 6.20 9 7 5 1.50 3.00 -10 -7 -5 -1.20 3.20 10 -7 5 -2.60 3.00 10 7 5 -1.80 2.80 -11 -7 -5 15.60 5.30 12 -7 5 3.30 4.50 -12 -7 -5 3.30 2.80 -13 -8 5 5.90 3.60 13 -8 -5 -11.00 6.60 13 -8 -5 2.30 4.60 13 8 -5 -5.10 4.10 12 -8 -5 4.30 4.70 -12 -8 5 2.70 5.60 12 -8 -5 2.40 4.30 12 8 -5 -2.40 4.60 11 -8 -5 2.50 6.40 11 -8 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39.00 8.40 -2 8 -5 43.30 8.00 -2 8 -5 39.90 7.60 -2 8 -5 48.60 9.40 2 8 5 34.10 7.20 -2 8 -5 42.20 8.40 3 -8 5 2.20 3.60 -3 -8 -5 -0.10 3.80 3 -8 5 14.10 5.30 -3 -8 -5 5.00 4.40 3 -8 5 14.80 4.90 3 8 5 7.70 5.30 -3 8 -5 8.50 4.50 -3 8 -5 3.30 3.50 3 8 5 7.60 4.30 -3 8 -5 5.60 3.50 4 -8 5 27.10 6.90 -4 -8 -5 30.30 7.00 -4 -8 -5 29.40 7.10 4 -8 5 15.50 5.30 4 -8 5 27.00 6.30 4 -8 5 19.70 6.10 -4 8 -5 22.00 6.80 4 8 5 20.40 6.20 -4 8 -5 20.60 6.60 5 -8 5 44.00 8.60 5 -8 5 19.60 6.00 5 -8 5 24.70 6.80 -5 -8 -5 19.50 6.80 -5 -8 -5 31.10 8.20 5 -8 5 27.00 6.50 -5 8 -5 23.10 7.10 5 8 5 40.30 8.30 -6 -8 -5 6.00 4.50 6 -8 5 16.60 5.40 6 -8 5 6.90 3.90 6 -8 5 8.50 4.70 6 8 5 15.10 5.80 -6 8 -5 -0.90 8.70 7 -8 5 3.30 3.90 7 -8 5 0.00 2.50 7 -8 5 -0.10 4.40 -7 -8 -5 0.70 3.10 7 8 5 0.00 4.10 8 -8 5 2.00 4.30 -8 -8 -5 -3.80 3.20 8 -8 5 0.70 3.20 8 8 5 -3.10 4.10 -9 -8 -5 4.20 4.60 9 -8 5 -0.70 3.60 9 8 5 -4.30 3.10 10 -8 5 3.70 4.00 -10 -8 -5 10.70 5.80 10 8 5 5.20 5.00 -11 -8 -5 19.40 6.10 11 -8 5 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3 -9 57.69 7.40 -1 3 -9 48.80 7.50 -2 -3 -9 3.20 2.20 -2 -3 -9 0.10 1.40 -2 -3 -9 0.00 1.40 2 -3 9 3.80 2.70 2 -3 9 1.50 1.40 2 3 9 -1.00 1.40 -2 3 -9 -1.30 2.00 -2 3 -9 -1.80 1.60 2 3 9 0.50 2.30 2 3 9 2.10 1.90 3 -3 9 11.00 4.10 -3 -3 -9 12.40 3.40 -3 -3 -9 10.80 3.30 3 -3 9 10.90 3.60 -3 3 -9 9.60 3.50 3 3 9 9.40 3.40 -3 3 -9 12.20 3.90 3 3 9 12.20 3.30 3 3 9 12.40 3.60 4 -3 9 -0.30 2.00 -4 -3 -9 0.30 1.40 -4 -3 -9 0.30 2.10 -4 -3 -9 2.80 2.60 4 -3 9 0.90 2.40 -4 3 -9 -0.20 1.80 4 3 9 0.50 1.80 4 3 9 3.00 2.20 4 3 9 0.60 3.10 -4 3 -9 0.80 2.30 -5 -3 -9 29.50 5.90 5 -3 9 35.40 7.50 5 -3 9 19.40 5.40 -5 -3 -9 22.50 5.20 -5 -3 -9 26.20 5.50 5 3 9 25.80 5.60 -5 3 -9 23.80 6.10 -5 3 -9 35.10 7.90 5 3 9 30.10 6.50 5 3 9 31.20 6.50 -6 -3 -9 -0.90 1.70 6 -3 9 3.70 2.20 -6 -3 -9 -0.10 3.00 6 -3 9 -0.40 1.60 6 -3 9 -3.80 2.00 -6 -3 -9 3.80 2.20 6 -3 9 1.90 1.50 6 3 9 -1.80 3.00 6 3 9 3.00 2.20 -6 3 -9 3.00 3.20 6 3 9 0.70 2.30 7 -3 9 58.19 10.30 7 -3 9 59.09 10.80 -7 -3 -9 69.19 9.70 -7 -3 -9 78.59 8.80 7 3 9 88.69 11.80 7 3 9 88.09 12.20 7 3 9 61.79 9.00 -7 3 -9 72.49 11.40 8 -3 9 17.20 6.30 -8 -3 -9 15.70 6.10 8 -3 9 18.40 6.80 -8 -3 -9 22.50 6.10 8 3 9 13.70 5.60 8 3 9 17.40 6.20 9 -3 9 44.60 10.50 9 -3 9 47.10 9.80 -9 -3 -9 48.70 9.00 9 3 9 49.70 8.90 9 3 9 43.50 9.70 10 -3 9 1.30 4.10 10 -3 9 -9.10 3.00 -10 -3 -9 -1.50 3.50 10 3 9 -2.50 3.00 10 3 9 0.50 3.90 11 -3 9 11.40 4.60 11 3 9 2.00 5.10 11 3 9 -1.60 5.20 12 -3 9 10.00 4.90 12 3 9 -4.90 5.30 15 -4 -9 9.80 6.70 -15 -4 9 -2.90 4.40 15 4 -9 -2.10 5.30 -15 4 9 -6.40 3.30 14 -4 -9 6.40 5.40 -14 -4 9 4.40 4.70 14 4 -9 2.40 4.60 -14 4 9 -1.40 3.80 -13 -4 9 3.10 6.30 13 -4 -9 26.20 8.30 13 4 -9 10.80 6.80 -13 4 9 8.40 5.50 -12 -4 9 13.60 7.10 12 -4 -9 14.90 6.40 -12 4 9 4.20 4.90 12 4 -9 4.80 5.20 -11 -4 9 10.10 5.00 -10 -4 9 1.80 4.40 10 -4 -9 1.40 2.10 10 -4 -9 4.40 4.60 10 4 -9 0.40 2.50 -10 4 9 4.60 3.60 9 -4 -9 72.29 11.10 -9 -4 9 72.29 11.80 -9 4 9 54.49 9.30 -9 4 9 73.99 7.90 9 4 -9 63.29 11.00 -9 4 9 75.19 13.00 9 4 -9 46.60 8.90 -8 -4 9 193.28 13.50 8 -4 -9 173.48 16.50 8 -4 -9 192.68 18.30 8 -4 -9 172.18 13.80 -8 -4 9 175.58 15.20 8 4 -9 199.68 14.60 8 4 -9 176.18 15.00 -8 4 9 201.78 17.60 -8 4 9 195.78 11.40 -8 4 9 181.78 13.70 8 4 -9 195.78 12.30 8 4 -9 192.78 15.40 7 -4 -9 65.19 9.60 -7 -4 9 61.09 9.70 7 -4 -9 50.49 10.50 7 -4 -9 46.30 9.10 7 -4 -9 57.59 8.30 -7 -4 9 68.99 7.40 7 4 -9 52.19 8.90 7 4 -9 58.99 10.00 7 4 -9 51.79 7.00 7 4 -9 64.09 9.30 -7 4 9 50.09 8.20 7 4 -9 54.89 7.40 -7 4 9 60.19 5.70 -6 -4 9 13.90 4.60 -6 -4 9 10.90 3.60 6 -4 -9 17.70 6.40 6 -4 -9 12.10 3.70 -6 -4 9 5.40 2.80 6 -4 -9 16.20 3.70 6 -4 -9 7.60 2.70 6 4 -9 13.20 3.70 6 4 -9 4.00 3.80 6 4 -9 14.60 4.10 6 4 -9 14.70 3.80 -6 4 9 7.30 2.20 6 4 -9 11.50 3.60 5 -4 -9 159.38 13.90 5 -4 -9 172.98 11.20 -5 -4 9 163.18 12.70 5 -4 -9 151.68 13.80 5 -4 -9 175.78 11.20 -5 -4 9 146.59 10.70 -5 -4 9 205.58 13.30 5 4 -9 140.09 10.60 5 4 -9 174.48 10.40 -5 4 9 153.48 7.90 5 4 -9 151.78 12.50 5 4 -9 164.98 10.00 -4 -4 9 140.39 11.70 4 -4 -9 137.19 9.50 4 -4 -9 144.09 13.10 -4 -4 9 138.29 10.30 4 -4 -9 145.99 13.00 4 -4 -9 137.69 9.50 -4 -4 9 131.39 9.70 4 4 -9 146.89 9.30 -4 4 9 126.79 6.80 4 4 -9 129.79 9.50 4 4 -9 142.89 11.70 4 4 -9 141.99 9.40 -3 -4 9 351.36 16.00 -3 -4 9 354.86 19.10 3 -4 -9 349.67 20.10 3 -4 -9 334.07 19.30 3 -4 -9 376.36 15.40 3 -4 -9 372.86 15.30 3 4 -9 368.26 15.60 -3 4 9 349.57 12.50 3 4 -9 340.87 18.50 3 4 -9 336.17 15.40 3 4 -9 365.86 15.20 -2 -4 9 -1.40 1.30 2 -4 -9 0.00 1.50 -2 -4 9 -0.50 1.60 2 -4 -9 -0.40 2.10 -2 -4 9 0.40 2.30 2 -4 -9 -1.10 1.10 2 -4 -9 -4.00 1.30 -2 4 9 0.30 0.70 2 4 -9 -0.70 1.40 2 4 -9 0.10 2.00 2 4 -9 0.50 1.30 2 4 -9 -2.40 1.10 1 -4 -9 9.10 3.90 -1 -4 9 8.10 3.60 1 -4 -9 11.90 2.80 1 -4 -9 9.50 2.40 -1 -4 9 8.00 2.90 -1 -4 9 5.20 2.10 1 4 -9 7.50 1.90 1 4 -9 4.50 3.20 -1 4 9 5.20 2.00 1 4 -9 3.60 2.10 -1 4 9 11.80 2.70 1 4 -9 7.20 2.80 -1 4 9 11.80 4.20 0 -4 -9 340.27 17.60 0 -4 9 329.17 11.10 0 -4 -9 316.37 11.60 0 -4 9 327.07 18.20 0 -4 9 294.77 15.70 0 -4 -9 306.27 12.10 0 4 -9 320.57 10.70 0 4 9 337.17 13.90 0 4 9 314.47 12.30 0 4 -9 306.87 15.60 0 4 -9 316.87 17.60 0 4 -9 302.57 15.70 0 4 9 323.17 18.30 1 -4 9 92.89 9.50 -1 -4 -9 86.19 6.40 1 -4 9 79.59 3.20 -1 -4 -9 81.19 8.20 -1 -4 -9 101.39 6.40 1 -4 9 84.39 8.40 -1 4 -9 78.09 7.80 1 4 9 102.99 7.70 1 4 9 89.59 9.20 -1 4 -9 97.89 9.60 1 4 9 89.69 6.20 2 -4 9 3.20 2.20 -2 -4 -9 5.10 1.80 2 -4 9 0.80 2.70 -2 -4 -9 3.00 1.80 -2 -4 -9 4.50 3.00 2 4 9 3.50 3.70 2 4 9 2.20 2.00 -2 4 -9 4.90 3.20 2 4 9 2.70 2.10 -2 4 -9 2.00 2.40 3 -4 9 -1.50 1.60 3 -4 9 -1.30 1.50 -3 -4 -9 1.40 1.70 -3 -4 -9 0.10 1.50 -3 -4 -9 5.00 2.90 3 4 9 -0.20 1.60 3 4 9 -0.40 2.50 -3 4 -9 -5.90 2.40 3 4 9 0.80 2.00 -4 -4 -9 4.00 2.10 4 -4 9 2.20 2.30 4 -4 9 -1.90 1.90 -4 -4 -9 -1.00 1.80 -4 -4 -9 -1.10 2.00 4 4 9 -2.30 2.70 4 4 9 0.50 1.70 4 4 9 2.30 2.40 -4 4 -9 -2.10 2.60 -4 4 -9 1.10 2.00 -5 -4 -9 4.30 2.80 5 -4 9 -1.70 2.40 5 -4 9 5.90 3.20 -5 -4 -9 -2.30 1.70 -5 -4 -9 0.40 2.60 5 4 9 0.00 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15.70 7.10 12 5 -9 8.40 5.60 11 -5 -9 11.30 6.10 11 -5 -9 9.80 4.80 -11 -5 9 8.50 5.40 -11 5 9 1.60 4.10 11 5 -9 5.80 5.00 10 -5 -9 87.79 12.30 -10 -5 9 88.99 13.80 10 -5 -9 92.79 16.30 10 5 -9 134.99 14.00 -10 5 9 103.49 15.90 9 -5 -9 2.90 3.50 -9 -5 9 6.80 5.70 9 -5 -9 -1.40 4.10 9 5 -9 -4.70 3.30 -9 5 9 -1.70 2.40 -9 5 9 5.00 4.30 8 -5 -9 22.40 6.00 -8 -5 9 21.20 6.50 8 -5 -9 5.40 4.20 -8 5 9 13.90 4.90 8 5 -9 14.00 5.80 8 5 -9 18.20 5.70 8 5 -9 28.60 7.40 -8 5 9 27.40 5.80 7 -5 -9 9.90 3.90 7 -5 -9 7.60 6.20 -7 -5 9 7.00 3.80 7 -5 -9 6.10 4.40 7 5 -9 9.10 3.80 7 5 -9 5.70 3.20 -7 5 9 4.20 3.00 7 5 -9 -0.20 2.30 7 5 -9 1.30 3.10 7 5 -9 16.20 5.20 -7 5 9 6.00 3.40 6 -5 -9 1.50 1.80 6 -5 -9 2.40 3.00 -6 -5 9 5.50 3.50 -6 -5 9 11.10 4.40 6 -5 -9 1.30 3.90 6 -5 -9 1.80 2.00 6 5 -9 4.50 2.50 6 5 -9 6.10 3.30 6 5 -9 0.50 2.20 -6 5 9 2.90 1.90 6 5 -9 0.50 2.80 5 -5 -9 6.80 2.90 5 -5 -9 3.90 3.90 -5 -5 9 7.80 3.90 -5 -5 9 7.20 2.80 5 -5 -9 9.60 3.50 5 -5 -9 1.40 2.80 -5 5 9 4.60 2.40 5 5 -9 13.90 4.40 5 5 -9 12.30 4.20 5 5 -9 6.60 3.10 5 5 -9 7.80 3.10 4 -5 -9 4.50 3.90 -4 -5 9 5.20 2.90 4 -5 -9 8.10 3.10 -4 -5 9 7.20 3.50 4 -5 -9 9.70 4.80 4 -5 -9 5.90 2.40 4 5 -9 16.40 5.20 -4 5 9 3.50 1.80 4 5 -9 7.50 2.90 4 5 -9 5.90 2.70 4 5 -9 5.50 2.20 -4 5 9 2.90 1.80 -3 -5 9 26.10 5.50 3 -5 -9 31.90 4.70 3 -5 -9 24.50 6.50 3 -5 -9 19.90 5.70 3 -5 -9 28.10 4.50 -3 -5 9 22.00 5.70 3 5 -9 18.70 4.10 3 5 -9 26.20 5.90 3 5 -9 17.70 4.50 -3 5 9 17.10 3.30 3 5 -9 21.00 4.50 2 -5 -9 100.29 10.30 -2 -5 9 98.49 9.80 2 -5 -9 102.09 6.50 -2 -5 9 97.09 7.60 2 -5 -9 90.19 6.30 2 -5 -9 82.19 9.30 -2 5 9 104.49 7.20 2 5 -9 87.79 8.00 2 5 -9 69.69 9.90 2 5 -9 93.69 7.10 -2 5 9 102.29 11.00 2 5 -9 91.79 8.20 1 -5 -9 5.10 1.80 -1 -5 9 3.50 2.60 1 -5 -9 11.40 2.50 -1 -5 9 3.90 2.10 1 -5 -9 1.20 2.10 -1 -5 9 5.70 2.60 1 5 -9 3.40 2.80 1 5 -9 4.00 3.00 1 5 -9 3.80 1.70 -1 5 9 2.50 1.90 -1 5 9 5.80 4.00 1 5 -9 3.10 2.00 0 -5 9 -0.50 2.30 0 -5 9 3.00 2.60 0 -5 9 2.50 1.70 0 -5 -9 3.70 1.60 0 -5 -9 2.10 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6.80 3.90 2 6 -10 16.90 4.30 2 6 -10 8.40 3.00 2 6 -10 20.40 5.40 2 6 -10 23.00 5.50 -2 6 10 17.40 3.90 -2 6 10 15.50 6.70 -1 -6 10 85.79 12.80 -1 -6 10 86.19 11.00 1 -6 -10 84.29 5.20 1 -6 -10 85.89 11.90 -1 -6 10 73.49 6.80 1 -6 -10 83.49 5.20 -1 6 10 71.69 7.00 -1 6 10 92.09 12.90 1 6 -10 76.39 11.60 1 6 -10 99.69 9.60 1 6 -10 70.79 6.60 1 6 -10 95.19 9.20 0 -6 10 76.69 10.70 0 -6 -10 79.89 4.60 0 -6 -10 97.39 10.80 0 -6 10 77.09 11.40 0 -6 -10 73.89 4.40 0 -6 10 62.49 5.40 0 6 10 77.29 7.50 0 6 10 54.89 10.10 0 6 -10 63.19 9.80 0 6 -10 88.79 9.40 0 6 -10 81.39 10.70 0 6 -10 73.49 6.20 1 -6 10 7.50 3.30 1 -6 10 2.80 1.50 -1 -6 -10 1.70 1.20 -1 -6 -10 4.20 2.30 -1 -6 -10 1.30 1.00 -1 -6 -10 1.30 2.90 1 -6 10 4.40 2.30 1 6 10 9.10 2.90 -1 6 -10 4.30 3.00 -1 6 -10 2.80 3.50 1 6 10 -1.00 3.70 -1 6 -10 -0.90 3.00 -1 6 -10 5.10 1.90 2 -6 10 36.10 3.20 -2 -6 -10 47.40 8.50 2 -6 10 29.90 7.30 2 -6 10 22.10 6.30 2 6 10 24.90 7.20 2 6 10 29.80 3.10 -2 6 -10 25.80 6.50 2 6 10 27.30 5.90 3 -6 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4.40 9 -7 -10 -3.60 2.90 -9 -7 10 -0.90 3.80 9 7 -10 1.90 2.20 8 -7 -10 5.30 3.60 8 -7 -10 9.60 5.80 -8 -7 10 10.10 6.20 8 7 -10 5.90 4.70 -7 -7 10 64.79 11.20 -7 -7 10 70.39 11.20 7 -7 -10 51.89 11.50 7 -7 -10 52.29 8.30 7 7 -10 41.60 8.20 7 7 -10 54.59 10.70 -6 -7 10 179.68 15.10 6 -7 -10 180.08 12.30 6 -7 -10 228.48 20.10 -6 -7 10 187.18 15.30 -6 7 10 178.18 12.00 6 7 -10 191.68 14.10 5 -7 -10 75.09 13.10 -5 -7 10 72.19 10.50 -5 -7 10 96.99 10.90 5 -7 -10 69.39 7.10 -5 7 10 76.89 7.60 5 7 -10 77.59 8.70 -5 7 10 68.69 7.60 4 -7 -10 24.60 4.50 -4 -7 10 20.60 6.70 -4 -7 10 22.80 5.70 4 -7 -10 22.40 7.20 -4 7 10 17.10 4.40 4 7 -10 31.10 8.50 4 7 -10 25.60 5.60 -4 7 10 15.10 4.60 -3 -7 10 10.20 5.20 3 -7 -10 12.70 5.80 -3 -7 10 14.60 4.60 3 -7 -10 11.60 2.70 -3 7 10 13.20 4.30 3 7 -10 11.00 5.10 3 7 -10 8.50 3.90 -2 -7 10 7.00 3.50 2 -7 -10 8.40 4.50 2 -7 -10 6.40 1.80 -2 -7 10 7.30 3.50 2 7 -10 2.30 3.00 -2 7 10 13.00 3.80 2 7 -10 4.40 4.10 -2 7 10 3.80 3.80 2 7 -10 13.60 5.70 -1 -7 10 -2.40 2.20 1 -7 -10 3.40 3.40 -1 -7 10 -4.90 1.90 1 7 -10 -4.60 3.60 -1 7 10 0.00 2.40 1 7 -10 -2.40 2.50 1 7 -10 -4.20 2.90 -1 7 10 4.70 4.40 0 -7 10 28.40 7.20 0 -7 -10 30.00 7.70 0 -7 10 26.60 4.90 0 -7 10 22.70 6.40 0 7 10 24.10 5.30 0 7 10 21.90 6.10 0 7 -10 27.00 6.20 1 -7 10 29.80 7.90 1 -7 10 18.70 3.60 1 -7 10 13.70 5.30 -1 -7 -10 22.70 6.70 -1 7 -10 22.00 6.30 1 7 10 11.50 4.30 1 7 10 10.30 6.20 -2 -7 -10 3.80 2.90 2 -7 10 9.50 3.70 2 -7 10 -1.50 2.10 2 7 10 2.20 5.50 2 7 10 12.30 4.40 3 -7 10 -3.20 2.60 3 -7 10 -0.50 2.00 -3 -7 -10 4.60 3.10 3 7 10 -1.60 1.40 -4 -7 -10 79.69 11.40 4 -7 10 91.69 14.10 4 -7 10 102.89 14.10 4 7 10 96.09 12.60 -5 -7 -10 34.40 8.10 5 -7 10 31.40 7.90 5 -7 10 25.30 7.00 5 7 10 23.00 7.10 -6 -7 -10 15.20 5.90 6 -7 10 19.40 6.40 6 -7 10 20.00 7.30 6 7 10 25.50 7.20 7 -7 10 -1.20 4.40 7 -7 10 4.30 5.40 -7 -7 -10 -2.80 3.40 7 7 10 5.60 4.30 8 -7 10 3.10 4.30 8 -7 10 1.60 4.00 -8 -7 -10 2.80 3.80 8 7 10 0.80 4.50 9 -7 10 10.90 6.20 -9 -7 -10 13.10 6.80 9 7 10 -0.20 4.40 10 -7 10 5.80 5.60 -10 -7 -10 3.80 4.70 10 7 10 6.00 7.90 13 -8 -10 9.50 5.00 -13 -8 10 17.80 6.90 13 -8 -10 5.70 8.40 13 8 -10 14.30 7.90 -12 -8 10 6.80 5.70 12 -8 -10 8.20 4.50 12 -8 -10 22.10 9.00 12 8 -10 16.40 8.30 11 -8 -10 -2.20 4.10 11 -8 -10 1.90 3.90 -11 -8 10 0.10 3.00 11 8 -10 -3.00 3.60 10 -8 -10 7.40 4.50 -10 -8 10 15.50 5.50 10 -8 -10 10.20 6.40 10 8 -10 12.50 7.30 9 -8 -10 1.60 3.10 9 -8 -10 11.00 5.60 -9 -8 10 -9.50 3.80 9 8 -10 3.90 4.50 8 -8 -10 7.80 4.00 -8 -8 10 3.50 5.50 8 -8 -10 9.00 5.90 8 8 -10 7.10 5.70 7 -8 -10 14.90 4.60 -7 -8 10 16.00 5.90 -7 -8 10 16.50 6.20 7 -8 -10 41.20 11.00 7 8 -10 17.70 6.90 6 -8 -10 20.20 7.80 6 -8 -10 28.40 5.90 -6 -8 10 34.60 7.80 -6 -8 10 22.80 7.00 6 8 -10 35.20 8.30 -6 8 10 30.30 6.40 5 -8 -10 39.40 9.60 -5 -8 10 46.30 8.90 -5 -8 10 39.60 8.50 5 8 -10 25.70 7.30 -5 8 10 35.80 6.70 -4 -8 10 1.00 3.30 -4 -8 10 2.00 3.20 4 -8 -10 7.00 4.30 4 8 -10 -3.00 2.60 -4 8 10 4.50 2.50 3 -8 -10 80.09 12.90 -3 -8 10 75.09 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2 -19 1.00 5.40 6 -2 -19 2.50 3.00 -6 -2 19 3.70 4.50 6 -2 -19 7.00 5.90 5 -2 -19 33.20 8.80 -5 -2 19 31.30 8.50 -4 -2 19 8.00 5.00 4 -2 -19 2.50 4.30 -4 2 19 5.70 1.70 -4 2 19 2.90 5.70 -3 -2 19 -2.30 4.30 -3 -2 19 -4.40 1.30 -3 2 19 0.90 5.00 -3 2 19 -1.20 1.90 -2 -2 19 1.00 4.30 -2 -2 19 12.90 4.30 -2 2 19 11.50 5.50 -1 -2 19 -4.90 3.40 -1 -2 19 -6.20 2.80 -1 2 19 1.80 3.10 -1 2 19 4.50 5.00 0 -2 19 12.60 5.50 0 2 19 12.90 5.90 1 -2 19 0.70 2.90 1 -2 19 0.20 5.20 1 2 19 5.20 3.80 1 2 19 -2.00 6.20 2 -2 19 -3.90 3.10 2 -2 19 18.90 6.20 2 2 19 0.20 5.60 2 2 19 4.20 3.90 3 -2 19 7.40 7.30 3 -2 19 -5.80 4.00 3 2 19 3.80 4.30 4 -2 19 4.10 4.60 4 -2 19 -1.10 4.00 4 2 19 -5.20 3.40 10 -3 -19 2.30 4.50 10 -3 -19 -1.20 4.40 10 3 -19 -2.60 5.70 9 -3 -19 -0.10 4.50 9 -3 -19 -5.70 4.60 9 3 -19 -6.70 5.10 8 -3 -19 -4.50 4.20 8 3 -19 7.50 5.70 7 -3 -19 13.30 5.50 -7 -3 19 -0.70 3.20 7 -3 -19 1.60 4.20 7 3 -19 -3.30 4.40 6 -3 -19 -2.00 2.30 6 -3 -19 -1.30 3.20 5 -3 -19 4.90 3.50 5 -3 -19 14.10 8.20 -5 -3 19 -2.60 4.30 4 -3 -19 2.60 3.70 -4 -3 19 0.20 3.30 -4 3 19 2.20 1.50 -3 -3 19 1.60 2.70 -3 -3 19 -0.70 4.30 -3 3 19 5.10 2.20 -3 3 19 3.90 5.30 -2 -3 19 7.80 3.40 -2 -3 19 7.80 5.50 -2 3 19 -3.90 4.30 -2 3 19 2.50 1.90 -1 -3 19 10.20 4.30 -1 -3 19 6.70 5.00 0 -3 19 -2.90 2.50 0 -3 19 -2.50 4.30 0 3 19 -0.10 3.50 1 -3 19 0.70 4.20 1 -3 19 3.60 4.40 1 3 19 0.30 3.40 2 -3 19 0.70 3.60 2 -3 19 0.20 4.20 2 3 19 2.10 3.50 3 -3 19 -3.90 3.10 3 -3 19 3.90 6.70 3 3 19 -3.10 3.40 9 -4 -19 7.00 6.50 9 -4 -19 8.20 5.10 9 4 -19 -5.20 5.40 8 -4 -19 23.20 8.60 8 -4 -19 41.30 9.80 8 4 -19 22.40 7.20 -7 -4 19 -1.60 4.60 7 -4 -19 -0.10 4.90 7 -4 -19 -8.00 4.70 6 -4 -19 1.00 5.80 -6 -4 19 -9.00 3.40 -5 -4 19 5.10 6.10 5 -4 -19 3.60 5.70 -4 -4 19 8.40 2.60 -4 4 19 0.50 1.60 -3 -4 19 4.20 3.10 -3 4 19 5.40 2.50 -2 -4 19 0.30 2.90 -2 4 19 -4.70 2.10 -1 -4 19 -3.90 3.50 -1 -4 19 4.80 4.20 -1 4 19 4.10 2.90 0 -4 19 6.50 6.10 0 -4 19 4.90 3.90 0 4 19 3.10 3.40 1 -4 19 -1.60 2.50 1 -4 19 -2.40 5.40 1 4 19 3.60 3.80 2 -4 19 -4.50 3.60 2 -4 19 -6.30 4.80 2 4 19 1.80 3.60 -8 -5 19 5.20 5.00 8 -5 -19 17.30 7.00 8 5 -19 3.20 6.90 -7 -5 19 -1.20 4.50 7 -5 -19 8.60 6.40 6 -5 -19 6.10 6.70 -6 -5 19 4.90 4.60 5 -5 -19 0.40 5.50 -5 -5 19 -1.20 3.50 -5 5 19 0.00 1.00 -5 5 19 0.80 1.10 -4 -5 19 2.70 5.90 4 -5 -19 8.00 5.40 -4 5 19 2.30 2.20 -3 -5 19 5.60 5.10 -2 -5 19 6.30 4.20 -2 -5 19 -0.40 4.60 -2 5 19 -1.00 2.60 -1 -5 19 2.80 6.80 -1 -5 19 1.00 4.30 -1 5 19 -5.50 2.50 0 -5 19 -2.00 3.60 0 -5 19 -3.20 3.10 0 5 19 -1.10 3.10 1 -5 19 4.00 4.30 1 -5 19 19.70 7.60 1 5 19 5.10 4.70 -7 -6 19 6.30 5.20 7 -6 -19 19.70 7.20 6 -6 -19 -1.00 4.80 -6 -6 19 4.20 5.20 -6 6 19 0.40 0.90 -5 -6 19 -0.60 4.20 5 -6 -19 2.90 5.80 -5 6 19 -2.80 1.90 4 -6 -19 9.90 5.70 -4 -6 19 5.30 4.70 -4 6 19 0.40 2.60 -3 -6 19 3.60 5.30 -3 6 19 9.30 3.10 -2 -6 19 -3.50 3.80 -2 6 19 3.60 2.90 -1 -6 19 7.60 6.80 -1 -6 19 -6.70 2.70 -1 6 19 -0.40 4.10 0 -6 19 10.60 4.90 0 -6 19 0.50 4.80 0 6 19 1.50 4.20 9 0 -20 -4.80 4.30 8 0 -20 16.00 7.90 7 0 -20 6.30 3.10 6 0 -20 -4.80 3.40 -6 0 20 0.00 4.40 -5 0 20 1.00 5.80 -4 0 20 8.70 3.40 -4 0 20 23.30 7.40 -3 0 20 -1.60 5.00 -3 0 20 0.70 1.60 -2 0 20 79.69 7.80 -2 0 20 50.19 11.80 -1 0 20 -3.10 4.70 -1 0 20 -1.50 3.10 0 0 20 21.10 8.70 0 0 20 29.10 7.10 1 0 20 13.10 5.70 1 0 20 10.70 7.10 2 0 20 2.00 4.70 2 0 20 6.50 4.40 9 -1 -20 -1.90 3.60 9 1 -20 0.00 4.50 8 -1 -20 -1.00 3.30 8 1 -20 9.30 6.00 7 -1 -20 6.40 3.40 7 1 -20 -1.20 5.00 -6 -1 20 -4.60 3.50 6 -1 -20 3.60 4.50 6 1 -20 -1.80 3.60 5 -1 -20 11.30 5.70 -5 -1 20 5.20 5.20 -5 1 20 4.60 5.50 -4 -1 20 7.70 2.30 -4 -1 20 19.20 7.30 -4 1 20 10.80 2.40 -3 -1 20 6.60 3.80 -3 -1 20 7.40 3.30 -3 1 20 9.00 3.80 -3 1 20 8.30 6.50 -2 -1 20 6.60 5.20 -2 -1 20 3.70 3.40 -2 1 20 8.70 5.20 -2 1 20 16.30 3.90 -1 -1 20 115.89 16.70 -1 -1 20 112.19 11.20 -1 1 20 117.19 10.50 -1 1 20 85.89 13.40 0 -1 20 27.90 8.30 0 -1 20 29.80 6.80 0 1 20 19.30 8.10 0 1 20 27.60 6.00 1 -1 20 3.30 3.70 1 -1 20 3.40 3.70 1 1 20 8.30 5.00 1 1 20 1.20 6.70 2 -1 20 -1.00 4.40 2 -1 20 8.10 5.30 2 1 20 3.60 4.50 2 1 20 -1.60 5.90 9 -2 -20 -6.90 4.10 9 -2 -20 -3.00 3.70 9 2 -20 2.00 4.20 8 -2 -20 2.80 4.30 8 2 -20 1.70 4.60 -7 -2 20 1.30 5.20 7 -2 -20 -3.20 3.30 7 2 -20 -1.30 4.30 6 -2 -20 -6.40 3.20 -6 -2 20 3.20 6.50 -5 -2 20 1.10 3.10 5 -2 -20 4.40 4.40 4 -2 -20 -3.80 2.50 -4 -2 20 -0.40 3.80 -4 2 20 0.80 4.80 -4 2 20 1.00 1.20 -3 -2 20 -1.90 2.80 -3 -2 20 -4.50 5.00 -3 2 20 -3.90 4.60 -3 2 20 1.40 2.50 -2 -2 20 9.60 6.20 -2 -2 20 22.10 5.50 -2 2 20 25.40 5.30 -2 2 20 19.90 8.20 -1 -2 20 21.40 5.70 -1 -2 20 32.20 10.00 -1 2 20 26.90 5.80 -1 2 20 32.10 8.90 0 -2 20 4.30 4.70 0 -2 20 2.20 3.80 0 2 20 0.50 3.30 1 -2 20 1.00 4.30 1 -2 20 2.50 6.00 1 2 20 0.40 3.70 2 -2 20 11.90 7.20 2 2 20 8.20 5.30 8 -3 -20 20.80 9.30 8 -3 -20 5.60 5.40 8 3 -20 13.90 6.00 -7 -3 20 21.30 8.10 7 -3 -20 6.90 5.20 7 3 -20 17.40 7.90 -6 -3 20 2.10 4.50 6 -3 -20 3.90 4.70 -5 -3 20 2.40 4.10 5 -3 -20 8.20 4.90 -4 -3 20 8.50 6.30 -3 -3 20 1.50 3.20 -3 -3 20 -8.90 3.10 -3 3 20 0.70 2.50 -2 -3 20 13.70 6.20 -2 -3 20 10.00 4.00 -2 3 20 11.00 3.60 -1 -3 20 -1.00 3.00 -1 -3 20 1.70 6.60 -1 3 20 8.10 3.60 0 -3 20 4.00 3.20 0 -3 20 -1.80 3.50 0 3 20 2.00 3.40 1 -3 20 8.00 6.90 1 -3 20 -3.90 3.50 1 3 20 -0.10 4.00 -7 -4 20 -2.20 5.10 7 -4 -20 10.90 6.50 -6 -4 20 6.20 4.90 -5 -4 20 6.80 6.40 -4 4 20 -1.80 1.40 -3 -4 20 -1.20 4.70 -3 4 20 -4.00 2.10 -2 -4 20 -0.30 3.40 -2 4 20 2.70 3.00 -1 -4 20 1.60 3.90 -1 -4 20 3.00 3.90 -1 4 20 -3.00 2.60 0 -4 20 11.00 6.00 0 -4 20 -4.30 3.30 0 4 20 0.70 3.50 6 -5 -20 1.00 5.20 -6 -5 20 5.20 6.50 -5 -5 20 9.80 6.60 -4 -5 20 -1.50 5.60 -4 5 20 -2.00 2.00 -3 -5 20 1.90 5.70 -3 5 20 1.80 3.00 -2 -5 20 11.20 6.00 -2 -5 20 13.40 6.90 -2 5 20 9.80 4.40 -1 -5 20 -5.70 5.20 7 0 -21 -0.90 4.30 6 0 -21 -1.10 3.50 -5 0 21 -6.40 4.30 -4 0 21 2.90 6.20 -4 0 21 0.50 2.00 -3 0 21 0.20 2.50 -3 0 21 2.70 5.90 -2 0 21 5.60 5.60 -2 0 21 4.10 2.40 -1 0 21 -3.50 3.80 0 0 21 -6.10 3.60 0 0 21 5.30 5.20 7 -1 -21 2.80 4.70 7 1 -21 1.50 4.40 6 -1 -21 8.30 4.60 -6 -1 21 2.70 6.60 6 1 -21 14.10 7.70 -5 -1 21 -3.80 5.00 5 -1 -21 -3.60 4.40 -5 1 21 -6.00 4.60 -4 -1 21 5.20 7.10 -4 1 21 -1.50 2.10 -4 1 21 -11.90 4.10 -3 -1 21 -2.00 4.00 -3 -1 21 7.20 3.70 -3 1 21 5.80 2.70 -3 1 21 0.70 4.20 -2 -1 21 10.10 3.40 -2 -1 21 9.50 7.40 -2 1 21 11.40 3.40 -2 1 21 3.60 5.70 -1 -1 21 0.70 4.90 -1 -1 21 1.50 3.90 -1 1 21 -7.60 2.70 -1 1 21 -2.80 6.80 6 -2 -21 -8.70 4.10 -6 -2 21 -0.80 4.10 -5 -2 21 -2.90 4.60 5 -2 -21 7.30 3.70 4 -2 -21 -0.70 2.90 -4 -2 21 -7.60 4.40 -4 2 21 -0.20 5.50 -4 2 21 -1.30 1.80 -3 -2 21 21.30 5.70 -3 -2 21 28.10 9.90 -3 2 21 14.20 4.50 -3 2 21 20.90 8.30 -2 -2 21 15.60 5.40 -2 -2 21 12.80 8.70 -2 2 21 5.00 3.60 -1 -2 21 -4.50 3.20 -1 -2 21 5.30 5.80 -1 2 21 1.20 3.30 -5 -3 21 0.10 3.00 -4 -3 21 -1.40 5.30 -4 3 21 -0.20 1.50 -3 -3 21 -5.00 2.80 -3 -3 21 2.60 5.30 -3 3 21 -2.10 2.80 -2 -3 21 23.20 8.30 -2 -3 21 3.40 3.60 -2 3 21 7.00 4.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 55368 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Cl1 Cl 0.48103(7) 1.08011(10) 0.24765(5) 0.1014(4) Uani 1 1 d . . . . . O1 O 0.05683(18) 0.7240(2) 0.72289(15) 0.0933(8) Uani 1 1 d . . . . . N1 N 0.53137(17) 0.7053(2) 0.47000(14) 0.0614(7) Uani 1 1 d . . . . . N2 N 0.26311(17) 0.63032(18) 0.54919(12) 0.0500(6) Uani 1 1 d . . . . . C1 C 0.4319(2) 0.8662(2) 0.40976(14) 0.0482(7) Uani 1 1 d . . . . . C2 C 0.5133(2) 0.7911(3) 0.41707(16) 0.0542(7) Uani 1 1 d . . . . . C3 C 0.5816(2) 0.8064(3) 0.36855(18) 0.0677(9) Uani 1 1 d . . . . . H3 H 0.634780 0.756146 0.371943 0.081 Uiso 1 1 calc R U . . . C4 C 0.5703(3) 0.8937(3) 0.31708(18) 0.0747(10) Uani 1 1 d . . . . . H4 H 0.615701 0.903050 0.285751 0.090 Uiso 1 1 calc R U . . . C5 C 0.4909(2) 0.9684(3) 0.31169(16) 0.0672(9) Uani 1 1 d . . . . . C6 C 0.4224(2) 0.9564(3) 0.35621(15) 0.0576(8) Uani 1 1 d . . . . . H6 H 0.369612 1.007478 0.351385 0.069 Uiso 1 1 calc R U . . . C7 C 0.36111(19) 0.8463(2) 0.45654(14) 0.0436(6) Uani 1 1 d . . . . . C8 C 0.37823(19) 0.7567(2) 0.50705(14) 0.0449(6) Uani 1 1 d . . . . . C9 C 0.4670(2) 0.6892(2) 0.51417(16) 0.0562(7) Uani 1 1 d . . . . . C10 C 0.27065(19) 0.9196(2) 0.44884(14) 0.0452(6) Uani 1 1 d . . . . . C11 C 0.2797(2) 1.0298(2) 0.47455(16) 0.0603(8) Uani 1 1 d . . . . . H11 H 0.343107 1.059964 0.494983 0.072 Uiso 1 1 calc R U . . . C12 C 0.1953(3) 1.0959(3) 0.47019(19) 0.0747(10) Uani 1 1 d . . . . . H12 H 0.201985 1.169595 0.488856 0.090 Uiso 1 1 calc R U . . . C13 C 0.1018(3) 1.0530(3) 0.4384(2) 0.0848(11) Uani 1 1 d . . . . . H13 H 0.045062 1.097826 0.434832 0.102 Uiso 1 1 calc R U . . . C14 C 0.0921(3) 0.9439(3) 0.4119(2) 0.0827(10) Uani 1 1 d . . . . . H14 H 0.028641 0.914886 0.390054 0.099 Uiso 1 1 calc R U . . . C15 C 0.1758(2) 0.8772(3) 0.41754(17) 0.0612(8) Uani 1 1 d . . . . . H15 H 0.168470 0.802864 0.400114 0.073 Uiso 1 1 calc R U . . . C16 C 0.30743(19) 0.7318(2) 0.55744(14) 0.0449(6) Uani 1 1 d . . . . . C17 C 0.1972(2) 0.6080(2) 0.59294(15) 0.0485(7) Uani 1 1 d . . . . . C18 C 0.17264(19) 0.6849(2) 0.64554(14) 0.0461(7) Uani 1 1 d . . . . . C19 C 0.22364(19) 0.7893(2) 0.65660(14) 0.0452(6) Uani 1 1 d . . . . . C20 C 0.2907(2) 0.8106(2) 0.61074(14) 0.0480(7) Uani 1 1 d . . . . . H20 H 0.325172 0.879026 0.615785 0.058 Uiso 1 1 calc R U . . . C21 C 0.4921(2) 0.5994(3) 0.57473(19) 0.0806(10) Uani 1 1 d . . . . . H21A H 0.492381 0.631289 0.624549 0.121 Uiso 1 1 calc R U . . . H21B H 0.557211 0.568712 0.575205 0.121 Uiso 1 1 calc R U . . . H21C H 0.442667 0.540317 0.563357 0.121 Uiso 1 1 calc R U . . . C22 C 0.1501(2) 0.4922(2) 0.58065(16) 0.0629(8) Uani 1 1 d . . . . . H22A H 0.200437 0.438860 0.572305 0.075 Uiso 1 1 calc R U . . . H22B H 0.096718 0.493658 0.533892 0.075 Uiso 1 1 calc R U . . . C23 C 0.1070(2) 0.4496(2) 0.64696(16) 0.0552(7) Uani 1 1 d . . . . . C24 C 0.0413(2) 0.5421(3) 0.66715(19) 0.0698(9) Uani 1 1 d . . . . . H24A H -0.017263 0.549747 0.624589 0.084 Uiso 1 1 calc R U . . . H24B H 0.017926 0.518262 0.712288 0.084 Uiso 1 1 calc R U . . . C25 C 0.0894(2) 0.6562(3) 0.68366(17) 0.0579(8) Uani 1 1 d . . . . . C26 C 0.21388(19) 0.8780(2) 0.71370(14) 0.0442(6) Uani 1 1 d . . . . . C27 C 0.1815(2) 0.9850(2) 0.68935(16) 0.0546(7) Uani 1 1 d . . . . . H27 H 0.158988 0.999674 0.636672 0.065 Uiso 1 1 calc R U . . . C28 C 0.1823(2) 1.0706(2) 0.74229(18) 0.0595(8) Uani 1 1 d . . . . . H28 H 0.158516 1.141798 0.724667 0.071 Uiso 1 1 calc R U . . . C29 C 0.2173(2) 1.0531(2) 0.82068(17) 0.0545(7) Uani 1 1 d . . . . . C30 C 0.2494(2) 0.9467(2) 0.84463(16) 0.0587(8) Uani 1 1 d . . . . . H30 H 0.272629 0.932577 0.897311 0.070 Uiso 1 1 calc R U . . . C31 C 0.2480(2) 0.8601(2) 0.79261(15) 0.0552(7) Uani 1 1 d . . . . . H31 H 0.270207 0.788599 0.810656 0.066 Uiso 1 1 calc R U . . . C32 C 0.1915(3) 0.4225(3) 0.71713(19) 0.0822(10) Uani 1 1 d . . . . . H32A H 0.163263 0.398471 0.759295 0.123 Uiso 1 1 calc R U . . . H32B H 0.231767 0.488761 0.732176 0.123 Uiso 1 1 calc R U . . . H32C H 0.232594 0.363176 0.704141 0.123 Uiso 1 1 calc R U . . . C33 C 0.0447(3) 0.3428(3) 0.6219(2) 0.0810(10) Uani 1 1 d . . . . . H33A H 0.018060 0.315900 0.664190 0.122 Uiso 1 1 calc R U . . . H33B H 0.086611 0.285589 0.607387 0.122 Uiso 1 1 calc R U . . . H33C H -0.009632 0.360004 0.578535 0.122 Uiso 1 1 calc R U . . . C34 C 0.2201(3) 1.1491(3) 0.8771(2) 0.0818(10) Uani 1 1 d . . . . . H34A H 0.231610 1.119539 0.928835 0.123 Uiso 1 1 calc R U . . . H34B H 0.157125 1.188625 0.864904 0.123 Uiso 1 1 calc R U . . . H34C H 0.273414 1.200169 0.873526 0.123 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Cl1 0.0916(7) 0.1387(9) 0.0777(6) 0.0373(6) 0.0274(5) -0.0276(6) O1 0.0937(18) 0.0846(17) 0.123(2) -0.0346(15) 0.0686(16) -0.0255(14) N1 0.0516(15) 0.0656(17) 0.0690(16) -0.0064(14) 0.0183(13) 0.0013(13) N2 0.0594(15) 0.0448(14) 0.0485(13) -0.0012(10) 0.0177(11) -0.0058(11) C1 0.0460(16) 0.0588(18) 0.0404(15) -0.0067(13) 0.0111(13) -0.0132(14) C2 0.0476(17) 0.065(2) 0.0514(17) -0.0137(15) 0.0150(14) -0.0097(15) C3 0.0513(19) 0.089(2) 0.069(2) -0.0206(19) 0.0253(16) -0.0086(17) C4 0.063(2) 0.108(3) 0.060(2) -0.013(2) 0.0279(17) -0.025(2) C5 0.060(2) 0.097(2) 0.0477(17) 0.0022(16) 0.0179(15) -0.0264(19) C6 0.0511(17) 0.072(2) 0.0504(16) 0.0011(15) 0.0129(14) -0.0122(15) C7 0.0423(15) 0.0477(16) 0.0415(14) -0.0072(12) 0.0109(12) -0.0097(12) C8 0.0457(16) 0.0463(16) 0.0430(14) -0.0047(13) 0.0109(12) -0.0040(13) C9 0.0554(19) 0.0559(18) 0.0585(18) -0.0019(14) 0.0155(15) -0.0007(15) C10 0.0484(17) 0.0470(17) 0.0430(14) 0.0018(12) 0.0161(12) -0.0042(13) C11 0.070(2) 0.0486(18) 0.0625(18) 0.0005(15) 0.0164(16) -0.0060(16) C12 0.103(3) 0.0424(18) 0.085(2) 0.0062(16) 0.034(2) 0.007(2) C13 0.075(3) 0.078(3) 0.106(3) 0.019(2) 0.029(2) 0.026(2) C14 0.052(2) 0.078(3) 0.115(3) 0.000(2) 0.0143(19) 0.0053(19) C15 0.0480(19) 0.0608(19) 0.075(2) -0.0042(16) 0.0149(16) -0.0033(15) C16 0.0491(16) 0.0449(16) 0.0422(14) 0.0003(12) 0.0134(12) -0.0018(13) C17 0.0537(17) 0.0464(16) 0.0463(15) 0.0016(13) 0.0135(13) -0.0064(13) C18 0.0504(16) 0.0452(16) 0.0444(15) 0.0018(12) 0.0149(13) -0.0031(13) C19 0.0505(16) 0.0433(16) 0.0417(14) 0.0013(12) 0.0105(12) 0.0010(13) C20 0.0541(17) 0.0442(16) 0.0472(15) -0.0019(12) 0.0150(13) -0.0075(13) C21 0.074(2) 0.079(2) 0.090(2) 0.021(2) 0.0235(19) 0.0204(19) C22 0.077(2) 0.0535(18) 0.0605(18) -0.0040(15) 0.0212(16) -0.0177(16) C23 0.0593(18) 0.0504(18) 0.0586(18) 0.0030(14) 0.0191(15) -0.0086(14) C24 0.062(2) 0.067(2) 0.087(2) 0.0006(17) 0.0285(18) -0.0135(17) C25 0.0535(18) 0.0602(19) 0.0639(19) -0.0012(15) 0.0216(15) -0.0043(15) C26 0.0457(16) 0.0415(16) 0.0477(15) 0.0006(12) 0.0154(12) -0.0021(12) C27 0.0599(18) 0.0500(18) 0.0544(16) 0.0074(14) 0.0144(14) 0.0080(14) C28 0.0626(19) 0.0435(17) 0.075(2) 0.0017(15) 0.0223(16) 0.0081(14) C29 0.0507(17) 0.0532(19) 0.0633(19) -0.0125(15) 0.0207(14) -0.0040(14) C30 0.068(2) 0.061(2) 0.0476(17) -0.0030(15) 0.0123(14) 0.0017(16) C31 0.067(2) 0.0467(17) 0.0524(17) 0.0053(14) 0.0148(15) 0.0063(14) C32 0.088(3) 0.073(2) 0.079(2) 0.0145(19) 0.006(2) -0.0015(19) C33 0.092(3) 0.060(2) 0.095(3) 0.0020(18) 0.031(2) -0.0254(19) C34 0.083(2) 0.072(2) 0.095(3) -0.031(2) 0.030(2) -0.0067(19) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C9 N1 C2 118.4(2) . . ? C16 N2 C17 117.4(2) . . ? C2 C1 C6 119.1(2) . . ? C2 C1 C7 118.0(2) . . ? C6 C1 C7 122.9(3) . . ? N1 C2 C1 123.2(2) . . ? N1 C2 C3 118.1(3) . . ? C1 C2 C3 118.8(3) . . ? C4 C3 C2 120.9(3) . . ? C4 C3 H3 119.6 . . ? C2 C3 H3 119.6 . . ? C3 C4 C5 119.7(3) . . ? C3 C4 H4 120.2 . . ? C5 C4 H4 120.2 . . ? C6 C5 C4 121.7(3) . . ? C6 C5 Cl1 120.0(3) . . ? C4 C5 Cl1 118.3(2) . . ? C5 C6 C1 119.9(3) . . ? C5 C6 H6 120.1 . . ? C1 C6 H6 120.1 . . ? C8 C7 C1 117.9(2) . . ? C8 C7 C10 121.5(2) . . ? C1 C7 C10 120.6(2) . . ? C7 C8 C9 120.1(2) . . ? C7 C8 C16 120.5(2) . . ? C9 C8 C16 119.4(2) . . ? N1 C9 C8 122.3(3) . . ? N1 C9 C21 117.1(3) . . ? C8 C9 C21 120.6(3) . . ? C11 C10 C15 118.7(3) . . ? C11 C10 C7 120.7(2) . . ? C15 C10 C7 120.5(2) . . ? C10 C11 C12 120.5(3) . . ? C10 C11 H11 119.8 . . ? C12 C11 H11 119.8 . . ? C13 C12 C11 120.1(3) . . ? C13 C12 H12 119.9 . . ? C11 C12 H12 119.9 . . ? C14 C13 C12 119.9(3) . . ? C14 C13 H13 120.1 . . ? C12 C13 H13 120.1 . . ? C13 C14 C15 120.2(3) . . ? C13 C14 H14 119.9 . . ? C15 C14 H14 119.9 . . ? C14 C15 C10 120.6(3) . . ? C14 C15 H15 119.7 . . ? C10 C15 H15 119.7 . . ? N2 C16 C20 122.5(2) . . ? N2 C16 C8 116.9(2) . . ? C20 C16 C8 120.6(2) . . ? N2 C17 C18 123.6(2) . . ? N2 C17 C22 114.6(2) . . ? C18 C17 C22 121.8(2) . . ? C17 C18 C19 118.4(2) . . ? C17 C18 C25 118.7(2) . . ? C19 C18 C25 122.8(2) . . ? C20 C19 C18 116.9(2) . . ? C20 C19 C26 116.6(2) . . ? C18 C19 C26 126.5(2) . . ? C19 C20 C16 121.0(2) . . ? C19 C20 H20 119.5 . . ? C16 C20 H20 119.5 . . ? C9 C21 H21A 109.5 . . ? C9 C21 H21B 109.5 . . ? H21A C21 H21B 109.5 . . ? C9 C21 H21C 109.5 . . ? H21A C21 H21C 109.5 . . ? H21B C21 H21C 109.5 . . ? C17 C22 C23 114.8(2) . . ? C17 C22 H22A 108.6 . . ? C23 C22 H22A 108.6 . . ? C17 C22 H22B 108.6 . . ? C23 C22 H22B 108.6 . . ? H22A C22 H22B 107.6 . . ? C24 C23 C22 107.6(2) . . ? C24 C23 C32 109.8(3) . . ? C22 C23 C32 110.2(3) . . ? C24 C23 C33 110.2(2) . . ? C22 C23 C33 109.8(2) . . ? C32 C23 C33 109.2(3) . . ? C25 C24 C23 116.2(2) . . ? C25 C24 H24A 108.2 . . ? C23 C24 H24A 108.2 . . ? C25 C24 H24B 108.2 . . ? C23 C24 H24B 108.2 . . ? H24A C24 H24B 107.4 . . ? O1 C25 C18 122.0(3) . . ? O1 C25 C24 120.4(3) . . ? C18 C25 C24 117.5(3) . . ? C27 C26 C31 117.8(2) . . ? C27 C26 C19 120.6(2) . . ? C31 C26 C19 121.2(2) . . ? C26 C27 C28 120.7(3) . . ? C26 C27 H27 119.7 . . ? C28 C27 H27 119.7 . . ? C29 C28 C27 121.5(3) . . ? C29 C28 H28 119.3 . . ? C27 C28 H28 119.3 . . ? C30 C29 C28 117.7(3) . . ? C30 C29 C34 122.0(3) . . ? C28 C29 C34 120.4(3) . . ? C29 C30 C31 121.6(3) . . ? C29 C30 H30 119.2 . . ? C31 C30 H30 119.2 . . ? C30 C31 C26 120.8(3) . . ? C30 C31 H31 119.6 . . ? C26 C31 H31 119.6 . . ? C23 C32 H32A 109.5 . . ? C23 C32 H32B 109.5 . . ? H32A C32 H32B 109.5 . . ? C23 C32 H32C 109.5 . . ? H32A C32 H32C 109.5 . . ? H32B C32 H32C 109.5 . . ? C23 C33 H33A 109.5 . . ? C23 C33 H33B 109.5 . . ? H33A C33 H33B 109.5 . . ? C23 C33 H33C 109.5 . . ? H33A C33 H33C 109.5 . . ? H33B C33 H33C 109.5 . . ? C29 C34 H34A 109.5 . . ? C29 C34 H34B 109.5 . . ? H34A C34 H34B 109.5 . . ? C29 C34 H34C 109.5 . . ? H34A C34 H34C 109.5 . . ? H34B C34 H34C 109.5 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Cl1 C5 1.727(3) . ? O1 C25 1.211(3) . ? N1 C9 1.320(3) . ? N1 C2 1.366(4) . ? N2 C16 1.338(3) . ? N2 C17 1.344(3) . ? C1 C2 1.405(4) . ? C1 C6 1.415(4) . ? C1 C7 1.432(3) . ? C2 C3 1.420(4) . ? C3 C4 1.363(4) . ? C3 H3 0.9300 . ? C4 C5 1.387(5) . ? C4 H4 0.9300 . ? C5 C6 1.364(4) . ? C6 H6 0.9300 . ? C7 C8 1.373(3) . ? C7 C10 1.490(4) . ? C8 C9 1.434(4) . ? C8 C16 1.490(3) . ? C9 C21 1.493(4) . ? C10 C11 1.378(4) . ? C10 C15 1.382(4) . ? C11 C12 1.381(4) . ? C11 H11 0.9300 . ? C12 C13 1.370(5) . ? C12 H12 0.9300 . ? C13 C14 1.369(5) . ? C13 H13 0.9300 . ? C14 C15 1.375(4) . ? C14 H14 0.9300 . ? C15 H15 0.9300 . ? C16 C20 1.384(3) . ? C17 C18 1.398(3) . ? C17 C22 1.508(4) . ? C18 C19 1.410(4) . ? C18 C25 1.491(4) . ? C19 C20 1.382(3) . ? C19 C26 1.486(3) . ? C20 H20 0.9300 . ? C21 H21A 0.9600 . ? C21 H21B 0.9600 . ? C21 H21C 0.9600 . ? C22 C23 1.518(4) . ? C22 H22A 0.9700 . ? C22 H22B 0.9700 . ? C23 C24 1.509(4) . ? C23 C32 1.524(4) . ? C23 C33 1.531(4) . ? C24 C25 1.501(4) . ? C24 H24A 0.9700 . ? C24 H24B 0.9700 . ? C26 C27 1.377(4) . ? C26 C31 1.386(4) . ? C27 C28 1.380(4) . ? C27 H27 0.9300 . ? C28 C29 1.378(4) . ? C28 H28 0.9300 . ? C29 C30 1.368(4) . ? C29 C34 1.508(4) . ? C30 C31 1.376(4) . ? C30 H30 0.9300 . ? C31 H31 0.9300 . ? C32 H32A 0.9600 . ? C32 H32B 0.9600 . ? C32 H32C 0.9600 . ? C33 H33A 0.9600 . ? C33 H33B 0.9600 . ? C33 H33C 0.9600 . ? C34 H34A 0.9600 . ? C34 H34B 0.9600 . ? C34 H34C 0.9600 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C9 N1 C2 C1 2.9(4) . . . . ? C9 N1 C2 C3 -178.6(2) . . . . ? C6 C1 C2 N1 176.5(2) . . . . ? C7 C1 C2 N1 -4.5(4) . . . . ? C6 C1 C2 C3 -2.0(4) . . . . ? C7 C1 C2 C3 177.1(2) . . . . ? N1 C2 C3 C4 -176.9(3) . . . . ? C1 C2 C3 C4 1.6(4) . . . . ? C2 C3 C4 C5 -0.3(5) . . . . ? C3 C4 C5 C6 -0.7(5) . . . . ? C3 C4 C5 Cl1 178.3(2) . . . . ? C4 C5 C6 C1 0.3(4) . . . . ? Cl1 C5 C6 C1 -178.7(2) . . . . ? C2 C1 C6 C5 1.1(4) . . . . ? C7 C1 C6 C5 -177.9(2) . . . . ? C2 C1 C7 C8 1.5(3) . . . . ? C6 C1 C7 C8 -179.5(2) . . . . ? C2 C1 C7 C10 -177.1(2) . . . . ? C6 C1 C7 C10 1.9(4) . . . . ? C1 C7 C8 C9 2.6(4) . . . . ? C10 C7 C8 C9 -178.8(2) . . . . ? C1 C7 C8 C16 179.9(2) . . . . ? C10 C7 C8 C16 -1.5(4) . . . . ? C2 N1 C9 C8 1.5(4) . . . . ? C2 N1 C9 C21 -176.4(3) . . . . ? C7 C8 C9 N1 -4.4(4) . . . . ? C16 C8 C9 N1 178.4(2) . . . . ? C7 C8 C9 C21 173.5(3) . . . . ? C16 C8 C9 C21 -3.8(4) . . . . ? C8 C7 C10 C11 110.8(3) . . . . ? C1 C7 C10 C11 -70.7(3) . . . . ? C8 C7 C10 C15 -67.6(3) . . . . ? C1 C7 C10 C15 111.0(3) . . . . ? C15 C10 C11 C12 1.0(4) . . . . ? C7 C10 C11 C12 -177.3(3) . . . . ? C10 C11 C12 C13 -1.6(5) . . . . ? C11 C12 C13 C14 0.9(5) . . . . ? C12 C13 C14 C15 0.4(5) . . . . ? C13 C14 C15 C10 -0.9(5) . . . . ? C11 C10 C15 C14 0.2(4) . . . . ? C7 C10 C15 C14 178.6(3) . . . . ? C17 N2 C16 C20 2.7(4) . . . . ? C17 N2 C16 C8 -178.3(2) . . . . ? C7 C8 C16 N2 120.3(3) . . . . ? C9 C8 C16 N2 -62.4(3) . . . . ? C7 C8 C16 C20 -60.7(3) . . . . ? C9 C8 C16 C20 116.6(3) . . . . ? C16 N2 C17 C18 0.3(4) . . . . ? C16 N2 C17 C22 180.0(2) . . . . ? N2 C17 C18 C19 -3.6(4) . . . . ? C22 C17 C18 C19 176.8(2) . . . . ? N2 C17 C18 C25 172.6(2) . . . . ? C22 C17 C18 C25 -7.0(4) . . . . ? C17 C18 C19 C20 3.7(4) . . . . ? C25 C18 C19 C20 -172.3(2) . . . . ? C17 C18 C19 C26 -175.2(2) . . . . ? C25 C18 C19 C26 8.9(4) . . . . ? C18 C19 C20 C16 -0.9(4) . . . . ? C26 C19 C20 C16 178.0(2) . . . . ? N2 C16 C20 C19 -2.4(4) . . . . ? C8 C16 C20 C19 178.6(2) . . . . ? N2 C17 C22 C23 158.8(2) . . . . ? C18 C17 C22 C23 -21.5(4) . . . . ? C17 C22 C23 C24 49.5(3) . . . . ? C17 C22 C23 C32 -70.1(3) . . . . ? C17 C22 C23 C33 169.5(3) . . . . ? C22 C23 C24 C25 -53.3(3) . . . . ? C32 C23 C24 C25 66.7(3) . . . . ? C33 C23 C24 C25 -173.0(3) . . . . ? C17 C18 C25 O1 -171.5(3) . . . . ? C19 C18 C25 O1 4.4(4) . . . . ? C17 C18 C25 C24 4.1(4) . . . . ? C19 C18 C25 C24 -179.9(3) . . . . ? C23 C24 C25 O1 -156.5(3) . . . . ? C23 C24 C25 C18 27.8(4) . . . . ? C20 C19 C26 C27 61.1(3) . . . . ? C18 C19 C26 C27 -120.1(3) . . . . ? C20 C19 C26 C31 -111.1(3) . . . . ? C18 C19 C26 C31 67.7(4) . . . . ? C31 C26 C27 C28 -0.7(4) . . . . ? C19 C26 C27 C28 -173.3(3) . . . . ? C26 C27 C28 C29 1.6(4) . . . . ? C27 C28 C29 C30 -1.6(4) . . . . ? C27 C28 C29 C34 178.2(3) . . . . ? C28 C29 C30 C31 0.8(4) . . . . ? C34 C29 C30 C31 -179.0(3) . . . . ? C29 C30 C31 C26 0.0(4) . . . . ? C27 C26 C31 C30 -0.1(4) . . . . ? C19 C26 C31 C30 172.4(3) . . . . ?