#------------------------------------------------------------------------------ #$Date: 2024-04-11 03:53:21 +0300 (Thu, 11 Apr 2024) $ #$Revision: 291173 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/98/7159893.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7159893 loop_ _publ_author_name 'Gerasimova, Tatiana' 'Zagidullin, Almaz' 'Nikolaeva, Anastasiya' 'Fayzullin, Robert R.' 'Saitova, Alya' 'Miluykov, Vasily' 'Grimme, Stefan' 'Katsyuba, Sergey' _publ_section_title ; Structural flexibility of favipiravir and its structural analogues in solutions: experimental and computational insight ; _journal_name_full 'Organic & Biomolecular Chemistry' _journal_paper_doi 10.1039/D4OB00404C _journal_year 2024 _chemical_formula_moiety 'C5 H5 N3 O2, 0.59(H2 O)' _chemical_formula_sum 'C5 H6.18 N3 O2.59' _chemical_formula_weight 149.75 _chemical_melting_point 538 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2ybc' _space_group_name_H-M_alt 'P 1 21/c 1' _atom_sites_solution_hydrogens mixed _audit_creation_method SHELXL-2018/3 _audit_update_record ; 2021-08-23 deposited with the CCDC. 2024-04-09 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 99.9049(16) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 3.62939(6) _cell_length_b 17.4327(3) _cell_length_c 10.06875(17) _cell_measurement_reflns_used 6388 _cell_measurement_temperature 93(2) _cell_measurement_theta_max 76.5090 _cell_measurement_theta_min 2.4150 _cell_volume 627.555(19) _computing_cell_refinement 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_collection 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_molecular_graphics ; WinGX (Farrugia, 2012); ORTEP-3 (Farrugia, 2012); PLATON (Spek, 2009); Olex2 (Dolomanov et al., 2009) ; _computing_publication_material ; WinGX (Farrugia, 2012); PLATON (Spek, 2009) ; _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015)' _diffrn_ambient_temperature 93(2) _diffrn_measured_fraction_theta_full 0.986 _diffrn_measured_fraction_theta_max 0.970 _diffrn_measurement_device_type 'XtaLAB Synergy, single source at home/near' _diffrn_measurement_method '\w scans' _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0167 _diffrn_reflns_av_unetI/netI 0.0080 _diffrn_reflns_Laue_measured_fraction_full 0.986 _diffrn_reflns_Laue_measured_fraction_max 0.970 _diffrn_reflns_limit_h_max 4 _diffrn_reflns_limit_h_min -3 _diffrn_reflns_limit_k_max 21 _diffrn_reflns_limit_k_min -21 _diffrn_reflns_limit_l_max 12 _diffrn_reflns_limit_l_min -12 _diffrn_reflns_number 6721 _diffrn_reflns_point_group_measured_fraction_full 0.986 _diffrn_reflns_point_group_measured_fraction_max 0.970 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 76.564 _diffrn_reflns_theta_min 5.074 _diffrn_source 'microfocus sealed X-ray tube' _exptl_absorpt_coefficient_mu 1.122 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_T_min 0.418 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ; CrysAlisPro 1.171.40.84a (Rigaku Oxford Diffraction, 2020). Numerical absorption correction based on gaussian integration over a multifaceted crystal model. Empirical absorption correction using spherical harmonics, frame scaling and detector area scaling, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.585 _exptl_crystal_description prism _exptl_crystal_F_000 312 _exptl_crystal_recrystallization_method 'from a water solution' _exptl_crystal_size_max 0.381 _exptl_crystal_size_mid 0.223 _exptl_crystal_size_min 0.123 _refine_diff_density_max 0.265 _refine_diff_density_min -0.275 _refine_diff_density_rms 0.067 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.061 _refine_ls_hydrogen_treatment mixed _refine_ls_matrix_type full _refine_ls_number_parameters 130 _refine_ls_number_reflns 1286 _refine_ls_number_restraints 5 _refine_ls_restrained_S_all 1.059 _refine_ls_R_factor_all 0.0383 _refine_ls_R_factor_gt 0.0382 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0644P)^2^+0.2760P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1058 _refine_ls_wR_factor_ref 0.1059 _reflns_Friedel_coverage 0.000 _reflns_number_gt 1278 _reflns_number_total 1286 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ob00404c2.cif _cod_data_source_block mil317 _cod_original_cell_volume 627.555(18) _cod_original_sg_symbol_H-M 'P 21/c' _cod_database_code 7159893 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.675 _shelx_estimated_absorpt_t_max 0.874 _shelx_res_file ; TITL mil317 in P2(1)/c shelx.res created by SHELXL-2018/3 at 12:33:46 on 23-Aug-2021 CELL 1.54184 3.629394 17.432674 10.068752 90.0000 99.9049 90.0000 ZERR 4.00 0.000056 0.000273 0.000169 0.0000 0.0016 0.0000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z SFAC C H N O UNIT 20 24.72 12 10.36 MERG 2 OMIT 0 4 0 OMIT 0 3 1 OMIT 0 0 2 OMIT 0 4 2 SADI 0.01 N1 H1A N1 H1B SADI N1 H1A N1 H1B N3 H3 SUMP 1.0 0 1.0 2 1.0 3 1.0 4 MORE -1 FMAP 2 PLAN 10 SIZE 0.123 0.223 0.381 ACTA HTAB N1 O3 EQIV $1 -x+2, -y+1, -z+1 HTAB N1 O1_$1 EQIV $2 x-1, -y+1/2, z-1/2 HTAB N3 O1_$2 HTAB N3 N2_$2 BOND $H CONF LIST 4 L.S. 30 TEMP -180.15 WGHT 0.064400 0.276000 FVAR 0.88568 0.41397 0.40474 0.18129 O1 4 0.998342 0.397060 0.551272 11.00000 0.02527 0.01584 = 0.02287 -0.00022 -0.00683 -0.00166 H1A 2 0.485389 0.450189 0.296861 11.00000 0.03784 H1B 2 0.738939 0.501184 0.397264 11.00000 0.03077 O3 4 0.232184 0.361745 0.188351 11.00000 0.02609 0.01778 = 0.01982 0.00096 -0.00339 -0.00082 N1 3 0.647924 0.455552 0.372038 11.00000 0.02597 0.01404 = 0.02201 -0.00115 -0.00639 -0.00228 N2 3 0.760428 0.258217 0.465091 11.00000 0.01759 0.01557 = 0.01943 -0.00103 0.00230 -0.00042 N3 3 0.298022 0.233419 0.225147 11.00000 0.01977 0.01693 = 0.01712 -0.00248 0.00041 -0.00271 H3 2 0.144404 0.225266 0.147610 11.00000 0.03033 C1 1 0.770879 0.394316 0.444258 11.00000 0.01686 0.01634 = 0.01969 -0.00138 0.00067 -0.00062 C2 1 0.629920 0.317044 0.390181 11.00000 0.01625 0.01617 = 0.01793 -0.00107 0.00296 -0.00038 C3 1 0.375205 0.308739 0.261398 11.00000 0.01787 0.01718 = 0.01730 -0.00189 0.00296 -0.00193 C4 1 0.431654 0.173138 0.303342 11.00000 0.02286 0.01493 = 0.02318 -0.00328 0.00429 -0.00243 AFIX 43 H4 2 0.366655 0.122245 0.274709 11.00000 -1.20000 AFIX 0 C5 1 0.661033 0.185962 0.423934 11.00000 0.02303 0.01439 = 0.02174 -0.00032 0.00264 -0.00016 AFIX 43 H5 2 0.751908 0.143681 0.479590 11.00000 -1.20000 AFIX 6 PART -1 O11 4 0.388529 0.488096 0.047058 20.50000 0.04533 0.01412 = 0.03410 0.00924 0.00328 0.00404 H11A 2 0.332138 0.440296 0.061687 20.50000 -1.50000 H11B 2 0.295724 0.495979 -0.037798 20.50000 -1.50000 PART -2 O12 4 0.974102 0.504489 0.073635 30.50000 0.04919 0.00642 = 0.02425 0.00440 -0.00354 -0.00072 H12A 2 0.995733 0.455907 0.092595 30.50000 -1.50000 H12B 2 1.088207 0.531131 0.141572 30.50000 -1.50000 PART 3 O13 4 0.724897 0.496497 0.081411 41.00000 0.03035 0.00683 = 0.01708 0.00623 0.00808 0.00728 H13A 2 0.771623 0.456363 0.132855 41.00000 -1.50000 H13B 2 0.617616 0.528595 0.128966 41.00000 -1.50000 PART 0 AFIX 0 HKLF 4 REM mil317 in P2(1)/c REM wR2 = 0.1059, GooF = S = 1.061, Restrained GooF = 1.059 for all data REM R1 = 0.0382 for 1278 Fo > 4sig(Fo) and 0.0383 for all 1286 data REM 130 parameters refined using 5 restraints END WGHT 0.0644 0.2761 REM Highest difference peak 0.265, deepest hole -0.275, 1-sigma level 0.067 Q1 1 0.1709 0.4991 -0.0034 11.00000 0.05 0.26 Q2 1 0.5146 0.3151 0.3277 11.00000 0.05 0.22 Q3 1 1.3333 0.3915 0.5100 11.00000 0.05 0.20 Q4 1 0.8382 0.4946 0.0955 11.00000 0.05 0.20 Q5 1 0.9710 0.4939 0.1000 11.00000 0.05 0.19 Q6 1 0.7380 0.4015 0.5842 11.00000 0.05 0.18 Q7 1 1.1421 0.3929 0.3933 11.00000 0.05 0.17 Q8 1 0.9526 0.4590 0.2792 11.00000 0.05 0.17 Q9 1 1.1174 0.5094 0.3202 11.00000 0.05 0.17 Q10 1 0.5000 0.5000 0.0000 10.50000 0.05 0.16 ; _shelx_res_checksum 50464 _shelx_hkl_file ; 0 0 1 0.06 0.04 0 0 -1 0.08 0.04 0 0 2 71.33 0.74 0 0 -2 71.08 0.82 0 0 3 0.03 0.06 0 0 3 0.14 0.08 0 0 -3 0.09 0.07 0 0 4 158.42 1.62 0 0 4 157.27 1.60 0 0 -5 0.29 0.13 0 0 5 0.07 0.10 0 0 6 560.55 4.35 0 0 7 0.07 0.12 0 0 7 0.05 0.06 0 0 -7 0.20 0.09 0 0 7 0.19 0.09 0 0 -8 238.55 2.10 0 0 8 238.41 4.08 0 0 9 -0.06 0.21 0 0 9 0.39 0.12 0 0 10 21.01 0.53 0 0 -10 20.61 0.54 0 0 10 19.46 0.39 0 0 -10 18.68 0.48 0 0 11 -0.06 0.09 0 0 11 -0.11 0.13 0 0 -11 0.04 0.09 0 0 -12 62.45 0.69 0 0 12 83.90 0.77 0 1 0 0.10 0.02 0 1 0 0.01 0.01 0 1 -2 880.02 4.57 0 -1 2 875.29 4.20 0 1 2 854.93 3.87 0 1 2 889.33 4.30 0 1 -2 856.66 3.88 0 1 -3 65.44 0.95 0 -1 -3 66.73 0.97 0 1 3 67.98 0.84 0 -1 3 65.38 0.88 0 1 -4 901.81 5.66 0 -1 4 972.09 5.52 0 -1 -4 909.73 5.67 0 1 4 971.47 5.59 0 1 4 967.97 5.39 0 -1 4 939.16 5.23 0 1 5 353.16 3.09 0 -1 -5 314.13 3.01 0 -1 5 332.68 2.95 0 -1 5 368.01 2.93 0 -1 -6 19.34 0.72 0 -1 6 21.83 0.77 0 1 -6 19.77 0.74 0 1 6 22.75 0.79 0 1 7 45.01 0.67 0 -1 7 44.23 0.53 0 1 7 46.12 0.79 0 1 7 48.51 1.66 0 1 -7 48.13 0.81 0 -1 8 0.73 0.30 0 -1 8 0.10 0.10 0 1 8 0.64 0.29 0 1 8 0.24 0.11 0 1 -8 0.15 0.10 0 -1 -8 0.32 0.12 0 -1 -9 1.84 0.19 0 -1 9 1.98 0.20 0 -1 9 1.61 0.38 0 1 -9 2.24 0.21 0 1 9 1.60 0.18 0 1 9 1.66 0.38 0 1 -9 2.01 0.20 0 -1 9 1.56 0.13 0 -1 -10 9.09 0.36 0 1 10 9.66 0.28 0 1 -10 9.23 0.34 0 1 10 9.34 0.35 0 -1 10 9.93 0.37 0 1 -10 9.13 0.37 0 1 10 8.91 0.40 0 1 11 195.65 1.67 0 -1 11 194.66 1.68 0 1 11 175.96 1.41 0 -1 -11 172.15 1.47 0 1 -11 183.57 1.50 0 -1 11 174.14 1.40 0 1 12 6.19 0.20 0 1 -12 4.88 0.18 0 -1 12 6.30 0.20 0 -1 -12 4.44 0.17 0 2 0 1768.83 8.07 0 2 0 1793.04 8.11 0 2 0 1767.93 7.88 0 2 -1 656.12 3.39 0 2 1 627.26 3.39 0 -2 2 1021.86 4.74 0 2 2 1048.20 4.80 0 2 -2 1014.18 4.83 0 2 -2 1041.89 5.43 0 2 -3 32.15 0.68 0 2 -3 31.75 0.38 0 -2 3 32.30 0.47 0 2 -4 993.01 6.10 0 -2 -4 1001.91 6.05 0 -2 4 1035.87 5.93 0 -2 4 1019.90 5.42 0 2 4 1062.33 6.13 0 2 -5 286.43 2.87 0 -2 5 306.98 2.84 0 2 5 313.43 2.99 0 -2 -5 305.20 2.92 0 -2 5 289.28 2.38 0 -2 -6 26.28 0.84 0 -2 6 28.99 0.91 0 -2 6 28.68 0.74 0 -2 -7 39.69 0.74 0 2 7 39.02 0.73 0 2 -7 40.78 0.74 0 -2 7 42.35 1.21 0 2 7 37.61 1.16 0 2 7 38.58 0.62 0 2 7 39.15 1.49 0 2 8 2.04 0.19 0 2 8 1.94 0.16 0 2 8 2.55 0.45 0 -2 8 2.15 0.21 0 -2 -8 2.45 0.20 0 2 -8 2.56 0.22 0 2 -9 7.71 0.35 0 -2 9 9.31 0.39 0 -2 9 7.90 0.77 0 -2 -9 7.77 0.34 0 2 9 7.48 0.73 0 2 9 8.64 0.37 0 2 -9 8.97 0.38 0 2 10 8.18 0.33 0 2 -10 8.69 0.36 0 -2 10 7.79 0.32 0 -2 -10 8.16 0.34 0 2 10 8.49 0.38 0 -2 -11 9.73 0.31 0 2 11 9.37 0.28 0 2 -11 9.81 0.31 0 2 11 10.22 0.35 0 2 11 9.67 0.24 0 -2 11 9.30 0.28 0 -2 12 0.05 0.06 0 -2 -12 0.18 0.06 0 2 -12 0.26 0.07 0 2 12 0.11 0.06 0 3 0 0.83 0.08 0 3 0 0.04 0.05 0 3 1 92.14 0.95 0 3 -1 94.98 0.99 0 3 2 104.37 1.17 0 3 -2 101.23 1.13 0 3 -2 103.54 0.91 0 3 3 1223.95 5.89 0 -3 3 1203.43 5.73 0 3 4 467.29 3.66 0 -3 -5 318.67 3.03 0 -3 5 319.61 3.02 0 -3 6 335.65 3.43 0 3 -6 339.40 3.35 0 3 6 338.44 4.21 0 3 7 7.66 0.29 0 3 7 8.21 0.34 0 3 7 8.47 0.58 0 3 -7 9.04 0.35 0 -3 7 8.95 0.57 0 3 7 9.34 0.74 0 3 8 98.02 1.12 0 3 -8 96.82 1.27 0 3 8 98.90 1.27 0 3 8 99.99 2.58 0 3 -8 100.49 1.29 0 -3 -9 7.15 0.33 0 3 -9 7.02 0.34 0 3 9 7.84 0.35 0 -3 9 7.87 0.36 0 -3 9 7.50 0.75 0 3 9 7.66 0.74 0 3 9 7.25 0.37 0 3 -9 7.98 0.37 0 3 -10 21.41 0.54 0 3 10 21.82 0.58 0 -3 10 21.42 0.52 0 3 10 21.11 0.52 0 3 -11 95.17 1.12 0 3 11 92.64 0.81 0 3 -11 92.95 0.97 0 -3 12 43.78 0.51 0 3 -12 36.19 0.47 0 4 0 21.58 0.39 0 4 1 131.65 1.29 0 4 -1 131.25 1.31 0 4 1 130.98 1.24 0 4 2 14.33 0.35 0 4 2 15.91 0.46 0 4 -2 14.97 0.45 0 4 -2 16.50 0.38 0 4 3 80.01 1.21 0 4 3 81.14 0.91 0 4 -3 82.25 0.91 0 4 -4 7.96 0.27 0 4 -4 7.39 0.38 0 4 4 8.28 0.27 0 4 -5 58.56 1.19 0 -4 5 58.29 1.56 0 4 5 61.49 1.54 0 4 6 83.86 1.03 0 4 -6 86.06 1.05 0 4 -6 87.34 1.58 0 -4 6 90.18 1.70 0 4 6 87.24 2.05 0 4 6 86.79 0.94 0 -4 -6 84.99 1.59 0 4 -7 7.68 0.24 0 4 7 8.33 0.34 0 -4 7 8.55 0.58 0 4 7 7.95 0.69 0 4 -7 8.44 0.35 0 4 -7 8.29 0.35 0 4 7 8.08 0.58 0 4 7 7.90 0.30 0 4 8 353.63 2.81 0 4 -8 358.38 2.76 0 4 8 352.85 4.95 0 4 8 345.37 2.49 0 4 8 353.51 2.70 0 4 -8 352.67 2.74 0 4 9 47.43 0.85 0 -4 9 45.54 0.86 0 4 9 45.83 0.75 0 4 9 45.02 0.89 0 4 -9 43.75 0.84 0 4 10 2.54 0.19 0 -4 10 2.26 0.18 0 4 10 2.34 0.21 0 4 -10 2.72 0.21 0 4 -10 2.50 0.23 0 4 11 0.01 0.09 0 4 11 0.08 0.06 0 4 11 0.22 0.07 0 -4 -11 0.14 0.08 0 4 -11 0.08 0.08 0 -4 12 0.19 0.06 0 4 -12 0.35 0.06 0 5 0 5.06 0.22 0 5 1 1525.46 7.81 0 5 1 1531.70 7.86 0 5 -1 1527.87 7.90 0 5 1 1512.19 7.70 0 5 2 132.58 1.31 0 5 -2 132.18 1.52 0 5 2 130.35 1.52 0 5 -3 1034.86 5.66 0 5 -3 1048.01 6.19 0 5 4 0.17 0.14 0 5 -4 0.23 0.12 0 5 -4 0.20 0.08 0 5 4 0.29 0.08 0 5 -5 100.16 1.63 0 5 5 100.19 2.01 0 5 6 7.88 0.28 0 5 6 7.70 0.32 0 5 6 9.17 0.60 0 5 6 7.67 0.31 0 5 6 7.59 0.62 0 5 -6 8.19 0.32 0 5 -6 8.13 0.32 0 5 -6 7.67 0.48 0 5 -6 7.83 0.23 0 -5 6 8.49 0.71 0 5 7 267.38 3.54 0 5 7 256.51 2.20 0 -5 7 253.01 1.71 0 5 7 263.26 2.01 0 5 7 269.58 4.04 0 5 -7 260.70 2.19 0 -5 7 266.25 3.42 0 5 -7 253.28 1.78 0 5 7 258.70 2.14 0 5 -7 250.60 2.17 0 5 -8 244.83 2.23 0 5 8 254.20 2.19 0 5 8 250.20 2.02 0 5 8 249.47 2.26 0 5 -8 251.24 2.22 0 -5 -8 243.84 2.13 0 5 -8 254.24 1.82 0 -5 8 250.89 3.49 0 5 9 456.80 3.32 0 5 9 465.09 3.21 0 -5 9 454.58 3.27 0 5 9 456.26 3.02 0 5 -9 464.14 3.25 0 5 -10 0.26 0.14 0 -5 10 0.12 0.10 0 5 -10 0.32 0.12 0 5 10 0.30 0.13 0 5 10 0.25 0.10 0 5 -11 0.25 0.06 0 -5 -11 0.15 0.07 0 5 -11 -0.02 0.06 0 5 -11 0.09 0.09 0 5 11 0.01 0.09 0 5 11 0.00 0.06 0 5 -12 19.62 0.29 0 6 -1 0.30 0.11 0 6 -1 0.30 0.12 0 6 1 0.24 0.10 0 6 1 0.36 0.11 0 6 -2 529.96 3.85 0 6 2 528.78 3.50 0 6 2 538.62 3.86 0 6 3 325.97 3.05 0 6 -3 329.58 2.90 0 6 -3 329.13 2.61 0 6 -4 491.81 3.34 0 6 -4 452.24 3.79 0 6 4 480.79 4.18 0 6 4 467.51 3.29 0 6 -5 1.67 0.24 0 -6 5 1.20 0.22 0 -6 6 7.89 0.24 0 6 -6 8.55 0.51 0 -6 6 8.33 0.71 0 6 -6 7.42 0.24 0 6 6 8.85 0.62 0 6 -6 8.15 0.33 0 6 -6 8.43 0.34 0 6 6 7.96 0.32 0 6 6 7.95 0.32 0 -6 7 131.84 3.03 0 6 -7 131.35 1.48 0 6 7 136.64 1.37 0 6 7 135.39 1.46 0 6 -7 128.36 1.18 0 -6 7 133.63 1.15 0 -6 7 129.83 1.17 0 6 -7 136.21 1.52 0 6 7 132.32 1.49 0 6 -8 1.42 0.19 0 6 8 1.18 0.18 0 6 -8 1.07 0.19 0 -6 8 1.30 0.28 0 6 -8 1.15 0.13 0 6 8 1.31 0.17 0 6 8 0.97 0.18 0 6 9 301.72 2.39 0 6 -9 300.86 2.59 0 6 -9 299.74 2.42 0 6 9 298.36 2.49 0 6 9 293.75 2.25 0 6 -10 213.21 1.82 0 6 10 224.28 1.92 0 6 -10 223.97 1.95 0 6 10 214.91 1.76 0 6 11 5.78 0.19 0 6 -11 5.64 0.18 0 7 0 1.48 0.19 0 7 0 0.04 0.10 0 7 -1 1268.16 7.26 0 7 1 1287.30 7.15 0 7 -1 1288.47 7.01 0 7 1 1280.38 7.27 0 7 1 1286.87 7.29 0 7 1 1275.98 7.03 0 7 -2 1970.78 10.98 0 7 -2 1933.12 10.41 0 7 -2 1959.02 10.08 0 7 2 1915.00 10.47 0 7 -3 287.41 3.27 0 7 -3 318.89 2.67 0 7 3 298.73 3.06 0 7 -3 306.47 2.94 0 7 3 309.40 2.67 0 7 -4 182.14 2.28 0 7 4 186.80 1.97 0 -7 5 277.04 3.12 0 7 -5 277.84 3.04 0 7 5 297.23 3.54 0 7 -5 284.12 1.78 0 7 5 262.56 2.03 0 7 5 266.00 2.06 0 7 -5 265.12 2.06 0 7 6 2.60 0.20 0 7 6 2.61 0.18 0 7 6 2.50 0.20 0 7 -6 2.80 0.32 0 7 -6 2.52 0.16 0 -7 6 2.70 0.44 0 -7 6 2.84 0.16 0 7 -6 2.31 0.21 0 7 -6 2.58 0.20 0 7 -7 108.11 1.09 0 -7 7 104.47 1.06 0 7 7 106.82 1.29 0 -7 7 109.73 2.82 0 -7 7 112.42 1.07 0 7 -7 106.85 1.32 0 7 7 109.06 1.23 0 7 7 106.66 1.34 0 -7 8 303.26 3.97 0 7 8 312.21 2.37 0 7 8 312.18 2.49 0 7 -8 304.23 4.47 0 7 -8 315.13 2.54 0 7 -8 302.09 2.16 0 7 8 309.83 2.56 0 -7 8 306.62 2.08 0 7 9 2.75 0.23 0 7 -9 3.05 0.23 0 7 -9 2.58 0.24 0 7 -10 17.39 0.43 0 7 -10 16.86 0.44 0 7 -10 18.29 0.49 0 7 10 17.71 0.43 0 7 11 5.97 0.18 0 7 -11 5.45 0.17 0 8 0 229.00 2.47 0 8 0 239.98 2.30 0 8 1 547.44 3.96 0 8 1 557.21 4.16 0 8 -1 539.15 3.94 0 8 1 528.67 3.82 0 8 1 555.27 4.17 0 8 -2 395.08 3.23 0 8 -2 383.50 3.67 0 8 2 393.71 3.23 0 8 -2 390.22 3.42 0 8 2 388.02 3.38 0 8 -3 9.66 0.45 0 8 3 9.15 0.44 0 8 -3 8.58 0.48 0 8 -3 9.27 0.58 0 8 4 472.67 3.76 0 8 -4 462.60 4.13 0 8 4 474.38 4.46 0 8 -4 463.31 4.77 0 8 5 11.43 0.69 0 8 5 11.23 0.37 0 8 -5 11.29 0.60 0 -8 5 11.22 0.29 0 -8 5 11.37 0.62 0 8 -5 11.51 0.30 0 8 -5 11.59 0.76 0 8 -5 12.18 0.39 0 8 5 11.76 0.38 0 8 -5 11.52 0.39 0 -8 6 59.79 0.75 0 8 -6 63.04 0.99 0 8 -6 61.98 1.45 0 8 -6 63.95 1.88 0 8 -6 62.68 0.77 0 8 6 61.23 0.87 0 8 6 61.16 0.94 0 -8 6 59.67 1.94 0 8 6 61.26 0.93 0 8 -6 67.06 0.99 0 -8 6 63.51 1.59 0 8 7 8.28 0.68 0 8 -7 7.57 0.37 0 8 -7 7.69 0.69 0 -8 7 8.21 0.62 0 8 7 7.42 0.33 0 8 -7 7.57 0.35 0 8 -7 6.97 0.27 0 8 7 7.46 0.35 0 -8 7 7.08 0.27 0 -8 7 7.46 0.27 0 -8 7 7.75 0.78 0 8 8 259.11 2.29 0 8 8 258.31 2.12 0 -8 8 256.58 1.88 0 8 -8 257.89 2.33 0 -8 8 256.76 4.54 0 8 -8 253.14 2.23 0 8 8 266.60 2.22 0 -8 9 7.11 0.25 0 8 -9 7.61 0.33 0 8 9 7.70 0.31 0 8 9 7.67 0.32 0 8 -9 7.45 0.35 0 8 -10 36.65 0.60 0 8 -10 38.43 0.66 0 8 10 38.21 0.60 0 8 -11 3.77 0.17 0 8 -11 2.81 0.12 0 9 0 0.09 0.13 0 9 0 0.07 0.14 0 9 1 298.87 2.89 0 9 -1 293.39 2.91 0 9 1 290.10 2.99 0 9 2 304.32 2.97 0 9 -2 290.03 3.28 0 9 -3 130.12 1.98 0 9 3 130.06 2.07 0 9 -3 120.25 1.79 0 9 -3 143.10 2.36 0 9 3 137.47 1.89 0 9 -4 360.47 4.16 0 -9 4 344.48 2.09 0 9 4 353.60 2.43 0 9 -4 362.75 3.64 0 9 -4 364.17 3.37 0 9 4 370.04 3.35 0 9 -4 345.83 2.44 0 9 -5 271.95 1.90 0 9 -5 270.27 3.23 0 -9 5 284.32 1.91 0 9 -5 286.36 2.23 0 9 5 286.34 2.19 0 -9 5 280.95 3.32 0 9 -5 290.76 2.26 0 9 -5 291.35 3.91 0 9 5 289.35 3.67 0 -9 5 276.37 1.88 0 9 6 55.50 0.89 0 9 -6 53.81 1.39 0 9 -6 58.36 0.94 0 -9 6 55.78 1.54 0 9 6 55.67 0.92 0 -9 6 59.72 0.78 0 -9 6 57.35 0.75 0 9 -6 57.05 0.77 0 9 -6 57.59 0.94 0 9 -6 58.89 1.78 0 9 -7 282.36 4.17 0 9 7 289.55 2.28 0 9 -7 284.82 2.43 0 9 -7 276.84 2.35 0 -9 7 275.89 2.05 0 -9 7 279.90 4.72 0 9 7 286.22 2.34 0 -9 7 281.99 3.78 0 9 -8 301.14 2.48 0 -9 8 302.83 2.12 0 9 -8 297.48 2.41 0 9 8 299.35 2.32 0 9 8 301.29 2.39 0 -9 8 281.39 4.77 0 -9 8 279.70 3.82 0 9 9 90.88 1.08 0 9 9 90.19 1.09 0 -9 9 91.22 0.94 0 9 -9 93.31 1.19 0 9 -9 89.92 1.12 0 9 -10 27.17 0.53 0 9 10 26.87 0.48 0 9 10 25.37 0.46 0 9 -10 26.52 0.49 0 9 -11 29.62 0.42 0 10 0 79.29 1.58 0 10 0 77.32 1.46 0 10 1 12.12 0.58 0 10 -1 11.96 0.57 0 10 -1 11.21 0.63 0 10 2 523.37 4.36 0 10 -2 522.36 4.87 0 10 -2 517.63 4.33 0 10 -3 114.37 1.22 0 10 -3 117.68 1.00 0 10 -3 110.11 1.80 0 10 3 115.21 1.18 0 10 3 118.84 1.87 0 10 -3 118.65 2.19 0 10 3 112.89 1.14 0 -10 3 110.08 0.99 0 10 3 109.13 1.00 0 10 3 124.15 2.03 0 10 -4 7.00 0.47 0 10 4 7.58 0.56 0 10 4 7.50 0.47 0 10 -4 7.05 0.24 0 -10 4 6.97 0.24 0 -10 4 7.22 0.23 0 10 -4 7.24 0.31 0 10 -4 7.70 0.60 0 10 4 7.45 0.30 0 10 -5 7.21 0.32 0 10 -5 7.29 0.33 0 10 -5 7.70 0.53 0 10 5 7.07 0.31 0 10 -5 6.85 0.61 0 -10 5 7.16 0.53 0 10 -5 7.05 0.26 0 10 -6 518.35 3.52 0 -10 6 524.14 3.12 0 10 -6 514.98 3.17 0 10 -6 519.80 3.49 0 10 6 520.03 3.46 0 -10 6 537.91 3.20 0 10 -6 538.84 5.83 0 -10 6 522.38 5.18 0 10 -7 338.15 2.40 0 10 -7 330.48 2.66 0 10 -7 342.53 2.66 0 10 7 343.07 2.57 0 10 -7 328.69 4.43 0 -10 7 329.09 4.14 0 -10 7 337.22 5.26 0 10 7 346.66 2.62 0 -10 7 349.99 2.40 0 10 -7 346.97 2.72 0 -10 8 62.23 0.82 0 10 8 58.66 0.91 0 10 -8 58.75 0.96 0 10 -8 60.42 0.96 0 10 8 60.93 0.91 0 10 -9 71.91 0.98 0 10 -9 73.01 0.96 0 10 9 72.80 0.93 0 10 9 73.91 0.93 0 10 10 69.21 0.74 0 10 -10 67.70 0.75 0 10 -10 68.73 0.76 0 10 -11 1.06 0.08 0 11 0 0.13 0.06 0 11 0 -0.01 0.12 0 11 0 0.06 0.14 0 11 1 35.18 1.05 0 11 -1 31.80 0.52 0 11 -1 30.58 0.55 0 11 -1 34.62 1.13 0 11 -1 35.55 1.05 0 11 -1 31.46 0.57 0 11 1 32.16 0.53 0 -11 2 3.48 0.17 0 11 -2 2.96 0.15 0 11 -2 3.84 0.18 0 11 2 3.20 0.18 0 11 -2 3.86 0.42 0 11 -2 3.16 0.19 0 11 2 4.47 0.39 0 11 -2 3.42 0.34 0 11 2 3.25 0.19 0 11 -2 3.59 0.21 0 11 2 3.98 0.19 0 11 3 2.44 0.30 0 11 -3 2.40 0.31 0 11 3 2.41 0.15 0 11 3 3.47 0.22 0 11 -3 2.40 0.15 0 11 -3 3.66 0.44 0 11 3 2.36 0.15 0 11 -3 2.88 0.20 0 11 -3 2.52 0.16 0 11 3 2.39 0.33 0 -11 3 2.57 0.14 0 11 -4 51.71 0.84 0 11 -4 49.95 0.69 0 11 -4 48.66 1.29 0 11 4 53.63 1.35 0 11 4 50.59 0.70 0 11 -4 51.25 1.56 0 11 4 52.16 1.52 0 11 4 52.79 0.83 0 -11 4 47.92 0.64 0 11 -4 51.19 0.70 0 -11 4 52.53 0.72 0 11 -5 11.41 0.42 0 -11 5 11.46 0.68 0 11 -5 11.85 0.78 0 -11 5 12.13 0.33 0 11 5 11.18 0.39 0 11 -6 34.86 0.73 0 -11 6 33.91 1.23 0 11 -6 33.45 1.33 0 -11 6 35.22 0.63 0 11 6 34.43 0.71 0 11 -6 34.86 0.73 0 11 -6 35.70 0.63 0 -11 7 2.66 0.38 0 11 -7 3.17 0.44 0 11 7 3.10 0.23 0 -11 7 2.69 0.49 0 11 7 4.12 0.26 0 -11 7 4.61 0.25 0 11 -7 3.30 0.24 0 11 -7 2.87 0.24 0 -11 8 98.99 1.07 0 11 -8 98.92 1.21 0 11 -8 93.01 1.19 0 11 8 95.19 1.14 0 11 8 95.87 1.15 0 11 9 18.43 0.43 0 11 -9 17.87 0.44 0 11 9 17.42 0.42 0 11 -10 0.87 0.09 0 11 -10 0.72 0.08 0 11 -10 0.68 0.09 0 12 0 71.86 0.85 0 12 0 70.86 0.79 0 12 0 68.59 1.64 0 12 0 67.09 0.87 0 12 0 72.15 1.63 0 12 0 71.74 1.69 0 12 1 0.75 0.20 0 12 -1 0.71 0.09 0 12 1 1.66 0.14 0 12 -1 0.56 0.22 0 12 -1 1.49 0.13 0 12 1 0.50 0.09 0 12 -1 0.44 0.10 0 12 -1 0.47 0.10 0 12 -1 0.59 0.19 0 -12 1 0.50 0.08 0 12 -2 135.26 2.50 0 -12 2 128.10 1.15 0 12 2 125.40 1.08 0 12 -2 130.53 1.13 0 12 2 131.83 1.31 0 12 -2 134.13 1.37 0 12 -2 142.67 2.29 0 12 2 129.96 2.21 0 12 2 124.48 1.21 0 12 -2 124.39 1.20 0 -12 -2 136.66 1.24 0 12 -2 137.16 1.38 0 12 -2 127.50 1.31 0 12 -3 184.60 1.68 0 12 3 189.74 1.72 0 12 -3 180.64 1.52 0 12 -3 191.71 2.74 0 12 -3 191.71 3.11 0 12 -3 192.60 1.75 0 12 3 198.43 2.83 0 -12 3 178.70 1.47 0 12 -3 186.08 1.48 0 12 3 186.21 1.55 0 12 -4 71.39 1.93 0 12 4 64.00 0.83 0 -12 4 64.61 0.84 0 12 -4 67.28 0.99 0 12 -4 63.65 1.56 0 12 -4 67.36 1.01 0 12 -4 61.73 0.82 0 12 4 64.41 1.57 0 12 -4 64.41 0.82 0 12 4 67.46 0.98 0 12 5 7.54 0.34 0 12 -5 7.48 0.65 0 12 -5 6.28 0.32 0 -12 5 6.70 0.53 0 12 -6 16.16 0.95 0 -12 6 15.29 0.83 0 12 6 14.94 0.40 0 12 6 15.67 0.48 0 12 -6 16.41 0.51 0 12 -6 15.74 0.43 0 -12 6 16.14 0.44 0 12 -7 312.85 2.50 0 12 -7 323.74 2.55 0 12 7 316.20 2.44 0 -12 7 327.91 2.32 0 12 8 49.71 0.78 0 12 -8 53.52 0.84 0 12 8 51.45 0.79 0 12 -8 52.28 0.81 0 12 -8 49.66 0.81 0 -12 8 54.64 0.76 0 -12 9 83.67 0.83 0 12 -9 76.19 0.90 0 12 9 80.80 0.88 0 12 -9 78.18 0.88 0 12 10 2.37 0.11 0 12 -10 2.62 0.11 0 12 -10 2.96 0.14 0 12 -10 2.73 0.12 0 13 0 0.50 0.11 0 13 0 0.15 0.16 0 13 0 0.11 0.07 0 13 0 0.56 0.20 0 13 0 0.28 0.09 0 13 -1 154.04 2.56 0 -13 1 149.88 1.29 0 13 -1 157.37 1.42 0 13 1 160.80 2.61 0 13 -1 148.05 1.44 0 13 1 151.24 1.34 0 13 -1 158.55 2.72 0 13 1 150.88 1.44 0 13 1 157.60 1.44 0 13 -1 160.25 2.72 0 13 2 156.88 2.62 0 13 -2 148.59 1.27 0 13 -2 143.46 1.37 0 13 2 144.79 1.38 0 13 -2 150.87 1.52 0 13 -2 148.35 1.52 0 13 -2 159.69 2.63 0 -13 -2 143.92 1.36 0 -13 2 140.78 1.29 0 13 2 144.36 1.44 0 13 -2 155.04 2.79 0 13 -2 144.95 1.45 0 13 -3 19.17 0.43 0 -13 3 17.84 0.43 0 13 -3 19.17 0.46 0 13 -3 18.87 0.50 0 13 -3 20.24 0.92 0 13 3 20.60 0.48 0 13 -3 20.78 0.54 0 13 -3 20.77 1.03 0 13 3 20.59 0.94 0 -13 4 57.00 1.48 0 13 -4 54.20 1.50 0 -13 4 54.57 0.79 0 13 -4 53.90 0.80 0 13 -4 57.79 0.94 0 13 4 57.84 0.92 0 13 -4 56.57 1.73 0 13 4 56.54 1.53 0 13 4 57.04 0.81 0 13 -4 57.26 0.79 0 13 -5 52.12 1.69 0 -13 5 54.18 1.51 0 13 -5 53.70 0.92 0 13 -5 52.73 0.79 0 -13 5 54.42 0.81 0 13 5 55.06 0.90 0 13 -5 53.71 0.91 0 13 -6 57.72 0.94 0 13 6 58.49 0.92 0 13 -6 57.63 0.95 0 13 6 56.19 0.79 0 13 7 7.12 0.31 0 13 -7 6.72 0.31 0 -13 7 6.29 0.28 0 13 -7 6.47 0.31 0 13 -8 6.91 0.28 0 13 -8 6.86 0.29 0 13 8 6.22 0.26 0 -13 8 7.37 0.27 0 13 -8 7.21 0.29 0 13 -9 2.47 0.15 0 13 9 2.30 0.14 0 -13 9 2.33 0.13 0 13 -9 2.46 0.14 0 13 -9 2.35 0.15 0 13 -10 13.25 0.23 0 14 0 863.38 4.60 0 14 0 873.67 4.86 0 14 0 860.85 4.88 0 14 1 465.58 4.94 0 -14 -1 432.73 2.89 0 14 1 431.03 2.74 0 14 -1 475.37 5.00 0 14 -1 449.49 4.96 0 14 -1 425.71 4.84 0 14 1 431.19 2.93 0 14 1 439.82 2.92 0 -14 1 427.54 2.73 0 14 -1 428.52 2.90 0 14 -1 435.68 2.94 0 14 -2 167.60 1.63 0 -14 -2 177.73 1.58 0 14 2 170.57 2.85 0 14 -2 170.59 2.99 0 14 -2 171.59 2.84 0 14 2 167.39 1.62 0 -14 2 164.68 1.46 0 14 -2 171.22 1.70 0 14 2 170.39 1.58 0 14 2 173.22 1.53 0 14 -2 172.08 1.58 0 14 -3 145.34 2.62 0 -14 3 142.06 1.35 0 14 -3 149.49 2.84 0 14 3 152.12 1.46 0 14 -3 144.63 2.82 0 -14 3 141.04 2.26 0 14 -3 143.82 1.51 0 14 -3 144.79 1.55 0 14 3 144.79 2.63 0 14 -3 146.90 1.45 0 14 4 0.05 0.09 0 14 -4 0.13 0.21 0 -14 4 -0.03 0.11 0 14 -4 0.35 0.12 0 14 -4 0.08 0.11 0 14 -4 0.06 0.12 0 -14 4 0.03 0.09 0 -14 5 5.38 0.27 0 -14 5 4.68 0.45 0 14 -5 4.76 0.52 0 14 -5 4.57 0.28 0 14 -5 4.51 0.28 0 14 -6 85.48 1.12 0 14 -6 85.20 1.13 0 -14 7 49.85 0.71 0 14 -7 48.64 0.77 0 14 -7 48.14 0.79 0 14 -8 0.06 0.08 0 -14 8 0.09 0.08 0 14 -8 0.04 0.08 0 14 -8 0.14 0.09 0 14 -9 1.27 0.10 0 14 9 1.16 0.10 0 14 -9 1.39 0.10 0 15 0 0.06 0.17 0 15 0 0.35 0.08 0 15 0 0.47 0.12 0 15 0 0.11 0.10 0 15 1 618.45 3.85 0 15 -1 631.08 6.20 0 15 1 626.60 6.12 0 15 -1 632.47 3.86 0 15 1 620.66 3.64 0 15 1 644.71 3.90 0 15 -1 610.57 6.05 0 -15 -1 642.73 3.85 0 -15 1 615.88 3.65 0 15 -1 622.44 3.87 0 15 -2 510.51 5.51 0 -15 2 503.26 3.18 0 15 -2 514.45 3.33 0 15 2 498.89 3.34 0 15 2 516.08 3.35 0 15 -2 513.44 3.36 0 -15 -2 506.09 3.23 0 15 2 512.93 5.45 0 15 2 521.00 3.21 0 15 -2 518.71 3.46 0 15 3 16.10 0.46 0 15 -3 16.11 0.87 0 15 -3 15.18 0.46 0 15 -3 15.30 0.91 0 15 3 15.24 0.87 0 -15 3 15.22 0.42 0 15 -3 14.66 0.47 0 15 -3 15.66 0.45 0 15 3 16.02 0.44 0 15 4 8.01 0.30 0 -15 4 7.79 0.31 0 15 -4 7.95 0.35 0 15 -4 8.11 0.66 0 15 -4 7.36 0.29 0 15 -4 7.58 0.33 0 15 -5 0.74 0.15 0 15 5 0.79 0.12 0 15 -5 1.06 0.16 0 -15 5 0.74 0.13 0 15 -6 10.26 0.36 0 -15 6 10.99 0.36 0 15 6 10.34 0.35 0 15 -6 10.42 0.38 0 15 6 10.08 0.30 0 15 -7 74.39 0.93 0 15 -7 74.27 0.91 0 15 7 74.55 0.88 0 15 -8 6.46 0.22 0 -15 8 7.11 0.23 0 15 -9 40.74 0.43 0 15 9 31.06 0.38 0 16 0 271.16 3.90 0 -16 0 273.71 2.22 0 16 0 265.41 2.18 0 -16 -1 153.77 1.54 0 16 1 150.51 1.54 0 16 1 144.97 1.34 0 16 1 152.98 2.86 0 16 -1 153.21 2.85 0 16 -1 160.04 1.58 0 -16 1 155.82 1.43 0 16 -1 152.40 1.54 0 16 1 162.00 1.59 0 16 -2 2.90 0.42 0 16 -2 3.32 0.23 0 16 -2 2.87 0.42 0 16 -2 3.07 0.25 0 -16 -2 2.92 0.21 0 16 2 3.41 0.25 0 16 2 3.16 0.21 0 16 -2 3.12 0.24 0 -16 2 2.82 0.21 0 16 2 3.36 0.45 0 16 -3 269.85 2.14 0 16 3 276.79 2.09 0 16 -3 276.24 2.21 0 16 3 281.62 2.17 0 -16 3 268.19 2.08 0 16 -3 272.39 2.26 0 -16 4 0.02 0.10 0 16 -4 0.10 0.11 0 16 4 0.07 0.10 0 16 -5 27.61 0.59 0 -16 5 28.93 0.60 0 16 5 27.46 0.56 0 16 -5 26.46 0.57 0 -16 5 29.39 0.58 0 16 -6 59.69 0.82 0 -16 6 61.82 0.81 0 16 6 59.86 0.79 0 16 7 36.64 0.55 0 16 7 37.98 0.56 0 16 -7 37.31 0.56 0 16 8 1.92 0.11 0 16 -8 1.73 0.10 0 -16 8 1.80 0.11 0 17 0 -0.03 0.11 0 17 0 0.10 0.10 0 -17 0 0.01 0.10 0 17 -1 20.90 0.52 0 -17 1 21.74 0.55 0 17 1 21.07 0.54 0 17 1 21.06 0.53 0 -17 1 21.20 0.47 0 -17 -1 21.84 0.53 0 17 -1 21.26 0.54 0 17 -2 0.79 0.14 0 17 -2 0.42 0.11 0 17 2 0.63 0.13 0 -17 2 0.60 0.11 0 -17 -2 0.37 0.10 0 17 2 0.50 0.10 0 17 -3 0.88 0.14 0 -17 3 0.71 0.12 0 17 -3 0.89 0.13 0 17 3 0.76 0.12 0 -17 3 0.90 0.15 0 17 3 0.81 0.13 0 17 4 139.28 1.30 0 17 -4 139.45 1.43 0 17 -5 16.36 0.41 0 -17 5 17.50 0.44 0 17 5 16.30 0.39 0 17 -5 16.07 0.42 0 -17 5 17.49 0.43 0 17 5 15.01 0.36 0 17 6 15.25 0.35 0 -17 6 14.64 0.36 0 17 6 15.11 0.36 0 -17 6 15.84 0.37 0 17 -6 15.02 0.37 0 17 7 3.28 0.15 0 17 7 3.44 0.15 0 18 0 0.58 0.12 0 -18 0 0.51 0.12 0 18 0 0.55 0.13 0 18 -1 45.40 0.76 0 -18 -1 43.56 0.71 0 18 -1 45.08 0.74 0 18 1 44.43 0.75 0 18 2 41.81 0.71 0 -18 2 41.91 0.74 0 18 -2 41.05 0.69 0 18 -2 39.49 0.69 0 -18 2 41.02 0.63 0 -18 3 26.43 0.51 0 -18 3 27.87 0.59 0 18 -3 26.80 0.54 0 18 4 6.28 0.24 0 18 -4 6.23 0.25 0 -18 4 6.70 0.26 0 18 4 6.72 0.24 0 -18 5 18.95 0.40 0 18 5 17.85 0.38 0 -18 5 18.61 0.42 0 18 5 17.25 0.34 0 18 5 18.17 0.37 0 18 -5 18.76 0.40 0 -18 6 3.40 0.16 0 18 6 3.35 0.15 0 -18 6 3.40 0.15 0 18 6 3.15 0.14 0 18 -6 3.18 0.15 0 18 -7 11.53 0.21 0 -18 7 10.96 0.22 0 18 7 10.88 0.20 0 -19 0 0.21 0.09 0 19 0 0.19 0.09 0 -19 1 44.99 0.72 0 19 -1 43.40 0.68 0 -19 2 0.29 0.08 0 19 -2 0.37 0.09 0 19 2 0.27 0.06 0 -19 3 0.43 0.08 0 19 -3 0.66 0.10 0 19 3 0.38 0.07 0 -19 3 0.68 0.12 0 19 4 40.74 0.55 0 19 4 38.27 0.52 0 19 4 36.47 0.47 0 19 -4 38.88 0.56 0 19 -5 1.51 0.11 0 19 5 1.56 0.11 0 -19 5 1.30 0.11 0 19 5 1.32 0.09 0 19 5 1.25 0.08 0 -19 5 1.44 0.12 0 19 6 10.93 0.20 0 19 -6 11.26 0.22 0 -19 6 10.60 0.22 0 -20 0 73.41 0.80 0 -20 1 66.00 0.77 0 -20 -1 58.54 0.64 0 20 -2 127.90 1.10 0 -20 2 128.76 1.16 0 20 -3 0.25 0.07 0 -20 3 0.17 0.05 0 -20 3 0.24 0.08 0 20 4 0.43 0.06 0 20 4 0.40 0.06 0 -20 4 0.36 0.06 0 20 -4 0.45 0.07 0 -20 5 15.89 0.27 0 20 -5 19.78 0.28 0 -21 0 0.05 0.05 0 -21 2 26.73 0.40 0 21 3 1.23 0.08 0 -21 3 1.14 0.09 1 0 -12 0.38 0.09 1 0 -11 0.03 0.10 1 0 -11 0.08 0.08 1 0 -11 0.08 0.10 1 0 -10 11.03 0.45 -1 0 10 10.48 0.36 1 0 -10 10.99 0.43 1 0 -10 11.51 0.37 1 0 -9 0.51 0.22 -1 0 9 0.06 0.22 -1 0 8 77.31 1.67 1 0 -8 74.77 1.94 -1 0 7 0.13 0.10 1 0 -7 0.14 0.18 -1 0 7 0.31 0.21 1 0 -7 0.00 0.11 -1 0 6 486.44 5.01 1 0 -6 483.86 4.83 1 0 -5 0.03 0.15 1 0 -4 337.97 2.43 1 0 -4 356.14 3.49 1 0 -3 0.22 0.10 -1 0 2 9414.80 41.31 1 0 -1 0.09 0.08 1 0 0 1009.28 5.56 1 0 1 0.39 0.07 1 0 1 0.04 0.07 1 0 2 571.05 3.65 1 0 2 575.33 3.63 1 0 3 0.10 0.11 1 0 3 0.18 0.08 1 0 4 30.04 0.94 1 0 4 28.22 0.50 1 0 7 0.08 0.15 1 0 7 0.25 0.12 1 0 8 172.37 1.55 1 0 8 172.14 1.88 1 0 9 0.03 0.14 1 0 9 0.41 0.11 1 0 10 145.71 1.48 1 0 10 142.04 1.22 1 0 11 0.05 0.05 1 0 11 0.01 0.07 1 1 -12 2.91 0.12 1 1 -12 3.26 0.18 1 1 -11 0.12 0.09 1 1 -11 0.13 0.10 1 -1 -11 0.18 0.08 1 1 -11 0.31 0.12 1 -1 -11 0.35 0.12 1 1 -10 26.97 0.56 -1 -1 10 25.61 0.56 1 1 -10 27.14 0.68 -1 1 10 26.08 0.57 1 1 -10 27.73 0.68 1 1 -9 20.41 1.01 1 -1 -9 20.96 0.51 1 -1 -9 20.20 1.01 1 1 -9 22.15 0.63 -1 -1 9 22.28 1.29 -1 1 9 21.43 1.24 1 -1 -9 21.72 0.62 -1 1 9 19.87 0.52 1 -1 -8 31.23 0.75 -1 -1 8 29.44 1.40 -1 -1 8 27.68 0.42 1 -1 -8 30.12 1.24 1 1 -8 28.07 0.69 -1 1 8 32.12 1.10 1 1 -8 29.96 1.23 -1 -1 8 30.07 0.98 -1 -1 8 27.19 0.91 -1 1 8 31.22 1.45 -1 -1 7 305.55 4.29 -1 1 7 313.96 3.50 -1 -1 7 319.55 3.27 -1 1 7 301.08 4.30 1 -1 -7 297.86 3.95 -1 -1 7 289.33 3.00 1 1 -7 284.38 3.84 -1 -1 6 3.41 0.29 1 1 -6 3.86 0.42 1 -1 -6 4.11 0.44 -1 1 6 3.62 0.44 -1 1 5 49.19 0.83 1 1 -5 52.45 1.36 -1 1 5 47.61 1.29 1 -1 -5 50.70 1.34 1 -1 -4 231.91 1.95 -1 1 4 218.71 2.57 1 1 -4 220.89 1.85 1 1 -4 236.37 2.78 -1 -1 4 244.83 2.72 1 1 -3 1627.32 8.25 -1 -1 3 1624.04 8.90 -1 1 2 9997.49 44.54 1 1 -2 9999.00 44.60 1 1 -2 9998.25 45.09 1 1 -1 295.48 2.30 1 -1 -1 295.15 2.27 1 1 -1 288.58 2.26 1 -1 -1 286.50 2.30 1 1 0 7.08 0.31 1 -1 0 7.46 0.31 1 1 1 16.65 0.30 -1 1 -1 17.56 0.32 1 -1 1 16.82 0.49 1 1 1 16.89 0.24 1 -1 2 1286.49 6.92 1 -1 2 1294.89 6.89 -1 1 -2 1277.39 6.10 1 1 3 28.13 0.57 1 -1 3 27.26 0.60 1 -1 3 29.03 0.80 1 -1 4 517.04 4.44 1 1 4 502.49 2.91 1 1 5 55.08 1.42 1 -1 5 56.91 1.51 1 1 6 107.65 1.33 1 -1 6 105.17 1.21 1 -1 7 0.61 0.24 1 1 7 0.76 0.26 1 1 7 0.68 0.15 1 -1 8 5.96 0.27 1 1 8 5.77 0.34 1 -1 8 5.78 0.60 1 -1 8 5.81 0.34 1 1 8 5.23 0.57 1 1 9 194.77 1.94 1 -1 9 195.56 1.96 1 1 9 196.17 1.64 1 -1 9 195.31 1.62 1 1 10 16.81 0.47 1 -1 10 17.02 0.48 1 1 10 17.63 0.39 1 -1 10 16.73 0.37 1 1 11 6.56 0.18 1 1 11 6.45 0.23 1 -1 11 6.67 0.23 1 -2 -12 0.17 0.08 1 -2 -12 0.24 0.07 1 2 -12 0.16 0.05 1 2 -12 0.16 0.08 1 2 -11 0.34 0.13 -1 2 11 0.23 0.08 1 -2 -11 0.22 0.08 1 2 -11 0.23 0.10 1 2 -11 0.18 0.10 1 -2 -11 0.21 0.12 -1 2 10 0.07 0.09 1 2 -10 0.20 0.14 1 -2 -10 0.14 0.12 -1 -2 10 0.02 0.09 -1 2 9 27.65 1.13 1 2 -9 26.87 1.17 -1 -2 9 26.35 1.38 1 2 -9 28.70 0.72 1 -2 -9 28.70 0.58 -1 2 9 29.03 1.43 1 2 -9 28.34 0.72 -1 2 9 29.30 0.63 -1 -2 8 0.27 0.14 -1 2 8 0.14 0.10 -1 -2 8 0.21 0.23 1 -2 -8 0.19 0.10 1 2 -8 0.13 0.12 1 -2 -8 0.31 0.20 -1 -2 8 0.17 0.06 -1 2 8 0.29 0.17 -1 2 8 0.12 0.07 -1 2 8 0.13 0.23 -1 2 7 34.22 1.40 1 2 -7 33.46 1.23 -1 2 7 38.94 1.21 -1 -2 7 37.68 1.01 1 -2 -7 34.34 1.30 1 2 -7 33.60 0.70 -1 -2 7 34.56 0.99 -1 2 6 728.03 6.55 1 2 -6 739.88 6.28 1 -2 -6 746.08 6.48 -1 2 5 288.80 3.43 -1 2 5 280.58 2.11 1 2 -5 288.20 3.39 -1 -2 5 288.82 3.45 -1 2 4 1.94 0.26 1 2 -4 2.00 0.28 -1 2 4 1.80 0.13 -1 -2 4 2.06 0.26 1 2 -4 2.06 0.17 -1 2 3 2.21 0.24 1 2 -3 2.23 0.18 -1 -2 3 2.09 0.23 1 -2 -3 2.58 0.21 -1 -2 2 502.04 3.19 1 -2 -2 471.19 3.38 1 2 -2 493.85 3.63 1 2 -2 505.03 3.28 1 2 -2 483.30 3.44 1 2 -2 478.57 3.19 1 2 -1 923.27 5.29 -1 -2 1 919.12 4.51 1 -2 -1 932.70 5.41 1 2 -1 933.94 5.22 1 2 0 657.09 3.63 1 2 0 653.49 3.72 1 -2 0 660.64 3.98 -1 2 -1 321.62 2.00 1 2 1 321.91 1.89 1 2 1 317.25 2.57 1 2 1 321.42 2.39 -1 2 -1 315.22 2.14 -1 2 -2 24.14 0.48 1 2 2 23.57 0.55 1 -2 3 1402.19 7.47 1 2 3 1395.61 7.84 1 -2 3 1410.76 8.18 -1 2 -3 1384.52 7.25 1 2 3 1412.11 7.12 -1 2 -4 275.74 2.50 1 -2 4 280.93 2.19 1 2 5 9.63 0.59 1 -2 5 8.69 0.60 1 -2 5 8.85 0.30 1 2 6 13.55 0.80 1 2 6 13.67 0.38 1 2 6 13.27 0.45 1 -2 6 13.70 0.35 1 -2 6 13.81 0.85 1 -2 6 13.23 0.41 1 2 7 0.67 0.23 1 -2 7 0.99 0.13 1 2 7 0.99 0.16 1 -2 7 0.92 0.15 1 -2 8 47.94 0.74 1 -2 8 45.47 1.67 1 -2 8 48.43 0.96 1 2 8 46.31 0.91 1 -2 9 148.42 1.34 -1 2 -9 149.07 1.51 1 2 9 150.39 1.66 1 -2 9 153.00 1.71 1 2 9 154.54 1.42 1 2 9 146.70 1.66 1 -2 10 5.10 0.27 1 2 10 5.37 0.23 1 -2 10 5.09 0.20 1 2 10 5.18 0.27 1 -2 11 10.25 0.28 1 2 11 10.35 0.28 1 2 11 10.14 0.23 1 3 -12 7.12 0.18 1 -3 -12 7.43 0.21 1 -3 -12 9.14 0.27 1 3 -12 8.48 0.25 1 3 -11 41.34 0.62 1 -3 -11 40.25 0.71 1 -3 -11 42.45 0.76 1 3 -11 41.36 0.73 1 3 -11 41.22 0.73 -1 3 10 4.73 0.25 1 -3 -10 4.75 0.23 -1 -3 9 3.54 0.53 1 3 -9 3.29 0.27 -1 3 9 3.08 0.18 -1 3 9 3.91 0.46 -1 -3 9 3.74 0.38 1 3 -9 3.12 0.41 1 -3 -9 3.31 0.21 -1 3 9 3.11 0.22 -1 3 8 142.71 3.09 1 -3 -8 136.69 1.34 1 3 -8 136.80 1.60 -1 3 8 136.48 1.25 1 3 -8 132.93 2.64 -1 -3 8 131.22 1.11 1 3 -8 136.32 1.60 -1 3 8 137.24 1.43 1 -3 -8 139.43 2.77 -1 -3 8 132.57 2.21 -1 3 7 23.58 0.53 -1 3 7 23.67 1.17 -1 -3 7 25.25 0.88 1 3 -7 24.85 0.62 1 -3 -7 23.49 1.10 -1 3 7 24.66 0.46 -1 3 7 27.16 1.03 1 -3 -7 25.51 0.51 1 3 -7 26.39 1.13 -1 3 6 21.21 0.83 -1 -3 6 19.44 0.98 1 3 -6 18.41 0.87 1 -3 -6 18.69 0.92 -1 3 6 19.02 0.95 -1 -3 5 26.44 1.01 1 3 -5 27.81 0.99 -1 3 5 28.45 1.04 -1 3 4 58.83 1.32 -1 -3 4 58.16 1.31 1 3 -4 57.88 0.97 1 3 -4 57.55 1.30 1 -3 -4 57.64 0.99 -1 -3 3 9.46 0.44 1 -3 -3 9.96 0.41 1 3 -3 9.96 0.38 1 3 -2 44.07 0.77 1 3 -2 41.40 0.86 1 3 -2 42.37 0.89 1 -3 -2 42.73 0.86 1 3 -2 42.80 0.76 1 3 -1 12.58 0.41 1 3 -1 12.38 0.47 1 3 -1 12.59 0.41 1 3 -1 12.48 0.43 1 3 0 68.61 0.91 1 3 0 65.62 0.72 -1 3 0 67.24 0.89 1 -3 0 67.29 0.97 1 -3 1 1109.78 5.97 1 3 1 1083.10 5.98 -1 3 -1 1087.37 5.70 1 3 1 1094.69 6.33 -1 3 -1 1111.22 5.91 1 3 1 1100.69 5.53 1 -3 1 1130.56 6.37 -1 3 -2 900.96 5.08 1 -3 2 917.55 5.50 1 3 2 913.51 5.12 1 3 3 12.13 0.50 -1 3 -3 9.39 0.38 1 3 4 57.42 1.27 1 -3 4 55.03 0.92 -1 3 -4 57.23 1.08 1 -3 4 56.27 1.37 1 3 5 5.06 0.44 1 -3 5 5.05 0.24 1 3 5 5.95 0.23 1 3 5 5.15 0.20 -1 3 -5 5.23 0.37 1 -3 5 5.26 0.20 1 -3 5 5.40 0.50 1 3 6 309.21 3.92 1 -3 6 325.01 4.32 1 3 6 316.28 2.22 1 3 6 302.93 2.48 1 -3 6 314.30 2.35 1 -3 6 312.80 2.11 1 3 7 21.70 1.06 1 -3 7 22.91 0.49 1 3 7 23.22 0.62 1 3 7 23.15 0.53 1 -3 7 23.16 0.59 1 -3 8 9.67 0.33 1 3 8 9.74 0.42 1 3 8 10.04 0.43 1 3 9 90.90 1.26 1 -3 9 88.56 0.96 1 -3 9 91.32 1.27 1 3 9 88.28 1.23 1 3 10 51.74 0.80 1 -3 10 49.89 0.60 1 -3 10 51.14 0.82 1 3 11 13.03 0.26 1 -3 11 13.06 0.31 1 3 11 13.19 0.31 1 4 -12 0.29 0.06 1 -4 -12 0.29 0.08 1 4 -12 0.24 0.08 1 -4 -11 42.06 0.71 1 4 -11 41.26 0.71 1 -4 -10 396.80 2.51 1 4 -10 412.81 3.04 1 4 -10 392.05 2.98 -1 -4 10 402.59 2.37 1 -4 -10 405.95 2.99 -1 4 10 412.38 2.72 -1 4 9 37.06 0.70 -1 -4 9 34.72 1.58 1 4 -9 31.37 1.21 1 -4 -9 36.84 0.64 -1 -4 9 32.67 1.12 -1 4 9 35.77 0.60 1 4 -9 36.22 0.81 -1 4 9 35.88 1.33 1 -4 -9 37.94 0.84 1 4 -9 36.08 0.79 -1 4 8 15.63 0.45 -1 -4 8 16.98 0.80 1 4 -8 16.60 0.92 1 4 -8 17.54 0.56 1 -4 -8 16.25 0.42 1 4 -8 17.00 0.55 -1 -4 8 16.41 0.36 -1 4 8 15.69 0.40 -1 -4 7 49.19 1.75 -1 -4 7 46.38 1.25 -1 4 7 44.32 0.73 -1 4 7 44.98 1.61 -1 4 7 45.78 0.66 -1 4 7 49.02 1.44 1 4 -7 46.26 1.49 1 -4 -7 46.63 1.56 1 4 -7 45.48 0.84 -1 4 6 18.46 0.94 -1 -4 6 19.67 1.00 -1 4 6 20.62 0.84 1 4 -6 16.85 0.57 1 4 -6 18.58 0.91 -1 4 5 17.79 0.83 1 4 -5 17.02 0.54 1 4 -5 16.95 0.79 -1 -4 5 18.62 0.87 -1 -4 4 0.41 0.16 1 4 -4 0.44 0.11 1 -4 -4 0.71 0.14 1 4 -3 231.25 2.37 1 -4 -3 230.02 2.27 1 4 -2 202.06 1.81 1 4 -2 200.32 1.87 1 4 -1 568.78 3.89 1 4 -1 580.67 3.81 1 4 -1 579.99 4.01 -1 4 0 432.32 3.02 1 4 0 427.50 2.52 1 4 0 433.85 2.70 -1 4 -1 0.25 0.09 1 -4 1 0.12 0.09 1 4 1 0.06 0.08 -1 4 -2 37.67 0.78 1 4 2 39.16 0.89 1 -4 3 74.08 1.22 -1 4 -3 66.81 1.09 1 4 4 89.93 1.62 -1 4 -4 85.33 1.41 1 -4 4 89.61 1.30 1 -4 5 84.94 0.88 1 4 5 86.19 0.94 -1 4 -5 92.08 1.58 1 4 5 82.96 0.87 1 -4 5 88.90 2.03 1 -4 5 83.40 0.99 1 4 5 86.80 1.79 -1 4 -6 13.05 0.41 1 4 6 12.71 0.76 1 4 6 11.93 0.29 1 -4 6 12.64 0.41 1 -4 6 13.23 0.87 1 -4 6 14.11 0.36 1 4 7 200.98 1.97 1 4 7 205.84 1.78 1 -4 7 200.61 1.64 1 -4 7 204.98 3.72 1 4 7 202.69 1.99 1 -4 7 202.72 1.89 -1 4 -8 2.80 0.16 1 -4 8 2.41 0.18 -1 4 -8 2.35 0.21 1 4 8 2.32 0.23 1 4 8 2.47 0.23 1 -4 9 19.77 0.42 1 4 9 20.57 0.57 -1 4 -9 20.12 0.50 1 -4 9 20.98 0.60 1 4 9 20.18 0.56 1 4 10 54.70 0.82 1 4 10 55.36 0.70 1 4 10 55.38 0.82 1 -4 10 54.49 0.84 1 -4 11 60.09 0.67 1 4 11 61.04 0.58 1 4 11 59.08 0.65 1 5 -12 27.08 0.39 1 5 -12 23.91 0.39 1 5 -12 27.21 0.35 1 5 -12 32.84 0.45 1 -5 -12 31.38 0.45 1 5 -11 302.13 2.01 1 -5 -11 303.23 2.16 1 5 -11 304.83 2.20 1 5 -10 2.83 0.25 1 5 -10 3.57 0.26 1 -5 -10 2.54 0.16 -1 -5 10 3.48 0.17 1 5 -10 3.03 0.25 1 -5 -9 7.53 0.28 -1 -5 9 7.71 0.56 -1 5 9 7.90 0.29 1 5 -9 9.14 0.42 1 5 -9 9.11 0.42 -1 5 9 8.80 0.70 -1 5 9 8.10 0.33 1 5 -8 0.45 0.14 -1 -5 8 0.30 0.15 -1 -5 8 0.19 0.08 1 5 -8 0.20 0.18 1 -5 -8 0.31 0.10 -1 5 8 0.46 0.10 1 -5 -8 0.46 0.22 -1 5 8 0.35 0.11 -1 5 8 0.35 0.21 1 5 -8 0.33 0.13 -1 5 7 5.41 0.26 1 -5 -7 5.69 0.25 -1 -5 7 4.66 0.42 -1 -5 7 5.40 0.61 1 5 -7 4.95 0.51 1 -5 -7 4.03 0.50 -1 5 7 5.50 0.24 -1 -5 6 20.98 1.06 1 5 -6 22.78 1.00 -1 5 6 18.70 0.44 1 -5 -6 20.98 0.48 1 -5 -6 19.81 0.42 1 5 -6 20.65 0.52 -1 -5 5 81.29 1.86 1 -5 -5 77.96 1.26 1 5 -5 81.38 1.78 1 5 -5 79.98 1.74 1 5 -5 75.48 1.06 1 5 -4 0.49 0.14 -1 -5 4 0.85 0.20 1 5 -4 0.48 0.20 1 5 -3 146.74 1.48 1 5 -3 155.93 2.18 1 5 -2 44.30 0.97 1 5 -1 80.79 1.28 1 5 -1 84.32 1.35 1 5 0 548.38 3.41 -1 5 0 540.15 3.80 1 5 0 546.19 3.76 1 5 0 550.53 3.26 -1 5 -1 760.19 4.84 1 -5 1 771.56 4.56 1 5 1 804.93 5.23 -1 5 -1 798.86 4.99 -1 5 -2 29.18 0.74 1 5 2 30.65 0.84 1 -5 2 29.19 0.73 1 5 3 3.57 0.30 -1 5 -3 3.36 0.27 1 -5 3 3.27 0.28 1 -5 3 4.25 0.33 -1 5 -4 32.36 0.89 1 -5 5 352.46 4.33 1 5 5 355.28 2.31 1 -5 5 354.11 2.23 1 5 5 350.07 2.18 1 5 5 361.22 2.26 -1 5 -5 343.78 3.44 1 5 5 364.62 2.37 1 5 5 352.42 2.12 1 -5 5 352.17 2.44 1 5 5 356.13 2.54 -1 5 -5 359.40 2.46 -1 5 -6 621.10 3.76 1 -5 6 618.36 6.45 1 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2.24 -1 6 7 79.06 1.90 1 -6 -7 70.91 2.01 -1 6 7 71.45 0.90 1 6 -7 72.73 1.87 1 -6 -7 71.03 0.88 -1 -6 7 72.03 0.79 -1 6 7 69.37 0.96 -1 6 6 141.48 1.36 1 -6 -6 146.99 1.28 1 6 -6 145.25 1.53 1 6 -6 143.88 2.55 1 -6 -6 150.12 1.45 1 6 -5 603.35 5.36 -1 -6 5 619.00 5.70 1 6 -4 32.37 0.93 1 6 -4 31.61 1.03 1 6 -3 6.33 0.41 1 6 -3 6.58 0.46 1 6 -1 49.21 1.03 1 6 -1 45.96 0.97 1 6 0 1119.95 6.07 1 -6 0 1111.69 6.28 1 6 0 1156.42 6.30 1 6 0 1175.74 6.63 -1 6 0 1119.92 6.75 1 -6 1 160.69 1.62 -1 6 -1 162.03 1.96 1 -6 2 38.52 0.87 1 6 2 38.61 0.98 -1 6 -2 38.61 0.92 1 -6 3 156.88 2.06 1 6 3 157.09 2.10 -1 6 -3 154.61 2.03 1 -6 4 3.54 0.35 1 6 4 2.64 0.19 -1 6 -4 3.01 0.29 1 -6 4 3.18 0.29 1 -6 5 22.78 1.08 1 -6 5 20.19 0.43 1 6 5 20.60 0.41 1 6 5 21.11 0.46 1 -6 5 21.38 0.42 -1 6 -5 19.24 0.75 1 -6 5 20.53 0.48 -1 6 -5 20.11 0.48 1 6 5 21.36 0.39 1 6 5 20.77 0.46 1 6 5 21.10 0.52 1 -6 6 347.24 2.54 1 -6 6 346.49 2.34 1 6 6 348.82 2.47 1 -6 6 349.29 4.86 1 -6 6 341.95 2.28 1 6 6 350.85 2.68 1 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1375.97 9.22 1 7 -3 0.76 0.23 1 7 -3 0.46 0.16 1 7 -2 1.31 0.22 1 7 -1 452.19 3.67 1 7 -1 462.21 3.85 1 7 -1 451.71 4.07 1 -7 0 32.86 0.72 1 7 0 33.16 0.77 -1 7 0 35.30 0.91 1 7 0 33.92 0.73 1 7 0 36.42 0.89 -1 7 -1 294.65 2.85 -1 7 -1 290.70 2.93 1 -7 1 287.99 2.25 1 7 2 939.67 6.38 -1 7 -2 915.60 6.06 1 -7 3 134.71 1.95 -1 7 -3 141.31 2.05 1 -7 4 25.07 0.91 1 7 4 23.26 0.50 1 7 4 23.78 0.53 1 7 4 24.03 0.42 -1 7 -4 24.74 0.87 1 -7 4 24.63 0.83 1 7 4 24.31 0.44 1 7 4 23.96 0.41 1 7 4 25.34 0.50 -1 7 -4 24.28 0.50 1 -7 4 24.56 0.44 1 7 5 0.15 0.09 -1 7 -5 0.18 0.09 -1 7 -5 0.42 0.16 1 7 5 0.16 0.09 1 7 5 0.10 0.08 1 7 5 0.23 0.09 1 -7 5 0.19 0.08 1 -7 5 0.20 0.09 1 7 6 8.09 0.36 1 -7 6 7.53 0.72 -1 7 -6 8.71 0.31 -1 7 -6 7.88 0.33 1 7 6 7.94 0.32 1 -7 6 7.55 0.33 1 7 7 80.89 1.16 1 7 7 80.87 1.05 1 7 7 82.95 1.20 1 -7 7 79.95 2.37 -1 7 -7 81.98 1.11 1 -7 7 81.01 0.94 1 -7 7 79.46 0.96 -1 7 -7 81.32 0.90 1 -7 7 80.11 1.10 1 7 8 314.52 2.53 -1 7 -8 319.30 2.14 -1 7 -8 331.49 2.44 1 7 8 329.59 2.62 1 7 8 317.67 2.35 1 7 9 16.11 0.46 -1 7 -9 16.80 0.42 -1 7 -9 16.04 0.35 1 7 9 17.15 0.48 1 7 10 18.74 0.37 1 -7 10 17.90 0.43 1 7 10 18.41 0.41 1 7 11 8.52 0.17 1 -7 11 8.59 0.21 1 8 -11 3.90 0.18 1 -8 -11 3.70 0.16 1 8 -11 3.79 0.18 -1 8 10 34.47 0.52 1 8 -10 36.54 0.66 1 8 -10 35.63 0.67 1 8 -9 138.50 1.52 -1 8 9 146.37 1.34 -1 -8 9 134.56 1.18 1 8 -9 148.11 1.60 -1 -8 8 15.68 1.07 1 8 -8 16.85 0.54 -1 -8 8 16.60 0.86 -1 8 8 17.69 0.46 -1 -8 8 17.08 0.40 1 8 -8 14.91 0.85 -1 8 8 19.25 1.07 -1 -8 7 85.94 2.43 1 -8 -7 82.06 0.95 1 8 -7 87.79 1.25 1 8 -7 87.99 2.10 -1 8 7 88.65 1.07 1 -8 -7 94.03 1.17 1 8 -6 392.52 4.54 1 8 -6 377.44 2.86 1 8 -6 393.51 2.87 -1 8 6 402.94 4.45 1 -8 -6 369.32 2.42 1 8 -6 377.88 2.82 -1 -8 6 379.61 5.00 1 8 -5 1.22 0.23 1 8 -5 1.10 0.14 1 -8 -5 1.16 0.12 1 -8 -5 1.09 0.21 1 8 -5 1.33 0.29 1 8 -5 1.27 0.15 1 8 -5 1.08 0.15 -1 8 5 1.49 0.28 1 8 -4 303.79 3.60 -1 8 4 309.61 3.30 1 8 -3 709.39 5.69 1 8 -2 2.47 0.30 1 8 -2 2.63 0.32 1 8 -1 9.52 0.56 1 8 -1 9.31 0.52 1 8 -1 8.61 0.46 1 8 0 1299.30 7.70 1 8 0 1273.28 7.33 -1 8 0 1303.19 8.03 1 8 0 1277.58 7.21 1 -8 1 5.54 0.30 -1 8 -1 5.66 0.42 1 8 1 5.93 0.45 -1 8 -1 5.74 0.41 1 -8 2 1.24 0.18 -1 8 -2 0.83 0.19 -1 8 -2 1.53 0.26 1 -8 3 464.29 4.09 1 -8 3 496.58 4.64 1 8 3 476.74 3.01 -1 8 -3 502.06 4.37 1 8 3 513.82 4.51 1 -8 3 489.81 2.91 1 8 4 68.83 0.92 -1 8 -4 69.20 0.88 1 -8 4 66.80 0.85 -1 8 -4 75.64 1.62 1 8 4 71.82 1.51 1 8 4 72.40 0.90 1 8 4 69.74 0.85 -1 8 -4 72.51 0.92 1 8 4 68.05 0.78 1 8 4 67.83 0.78 1 8 4 69.08 0.80 1 -8 4 72.55 0.86 1 8 4 72.00 0.97 1 -8 4 68.94 1.49 1 -8 4 68.30 1.53 1 8 5 214.07 1.89 -1 8 -5 213.56 1.76 1 -8 5 217.96 1.82 1 8 5 222.27 1.81 1 8 5 210.47 1.65 -1 8 -5 213.37 1.82 -1 8 -5 218.70 2.95 1 8 5 216.62 1.77 1 -8 5 214.01 1.75 1 8 6 985.77 5.60 -1 8 -6 954.47 5.31 1 -8 6 992.09 5.33 1 8 6 989.56 5.29 -1 8 -6 987.26 5.45 1 8 6 968.58 5.34 1 -8 6 980.62 5.45 1 -8 6 961.79 8.97 1 8 7 77.81 1.13 -1 8 -7 75.79 0.97 1 -8 7 75.60 2.32 1 8 7 75.05 1.01 -1 8 -7 77.76 1.06 1 8 7 79.81 1.16 -1 8 -7 78.38 0.90 1 -8 7 77.10 0.96 1 -8 7 76.96 1.06 1 8 8 46.71 0.84 -1 8 -8 47.34 0.78 -1 8 -8 45.23 0.65 1 8 8 45.58 0.84 1 8 8 44.21 0.73 -1 8 -9 32.89 0.57 1 8 9 32.40 0.63 1 8 10 15.54 0.31 1 8 10 15.26 0.34 1 -8 10 15.36 0.37 1 9 -11 126.38 1.02 1 9 -11 117.03 0.97 1 9 -10 78.58 0.92 1 9 -10 79.64 0.97 -1 -9 9 6.99 0.25 -1 -9 9 7.07 0.26 -1 9 9 7.55 0.29 1 9 -9 7.31 0.33 1 9 -8 231.14 2.10 1 9 -8 227.10 3.95 -1 -9 7 60.61 2.05 1 9 -7 59.03 1.72 1 9 -7 60.75 0.99 -1 -9 7 60.58 0.76 -1 9 7 62.59 0.91 1 -9 -7 62.15 0.97 1 9 -6 33.19 0.69 -1 -9 6 31.65 1.40 1 9 -6 34.98 1.31 -1 9 6 32.62 0.59 -1 -9 6 32.17 0.52 1 9 -6 32.66 0.72 -1 9 5 129.44 1.87 -1 9 5 155.45 2.55 1 9 -5 149.27 2.64 1 9 -5 141.57 1.42 -1 9 5 140.83 1.31 1 -9 -5 130.71 2.20 1 9 -5 124.64 2.18 1 9 -5 141.65 1.48 1 -9 -4 2.13 0.32 1 9 -4 1.55 0.31 1 9 -4 0.64 0.21 1 9 -4 0.77 0.11 1 9 -4 0.68 0.24 1 9 -4 0.65 0.12 1 9 -4 1.41 0.14 -1 9 4 0.92 0.23 1 9 -3 63.60 1.63 -1 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1.06 0.15 -1 -15 6 0.90 0.12 1 15 -6 0.93 0.12 1 15 -6 0.90 0.12 1 -15 -6 1.45 0.17 1 15 -5 157.95 1.54 -1 -15 5 160.34 1.39 1 15 -5 157.62 1.57 -1 -15 4 27.15 0.52 -1 15 4 27.16 0.54 1 15 -4 27.53 0.56 1 15 -3 0.88 0.15 1 15 -3 0.85 0.15 -1 -15 3 1.28 0.13 1 15 -3 0.98 0.25 1 15 -3 1.14 0.28 1 -15 -3 0.86 0.29 -1 15 3 1.23 0.28 1 15 -3 0.77 0.13 1 -15 -3 1.15 0.16 1 15 -3 0.99 0.29 1 15 -3 1.04 0.13 -1 15 3 1.24 0.15 1 15 -2 488.76 3.22 1 15 -2 495.87 3.05 -1 -15 2 479.77 2.86 -1 15 2 517.24 3.41 1 15 -2 481.98 3.04 1 15 -2 458.13 4.77 1 15 -2 479.24 5.04 -1 15 2 532.91 5.33 1 -15 -2 488.86 3.35 1 15 -2 496.54 3.08 -1 15 2 477.56 3.11 1 15 -2 483.64 5.60 1 -15 -1 678.77 3.96 1 15 -1 643.52 3.78 -1 15 1 691.52 4.19 1 15 -1 648.71 6.74 1 -15 -1 664.78 4.18 1 15 -1 669.89 3.89 1 15 -1 651.02 3.68 1 -15 0 318.34 2.42 1 15 0 318.97 2.32 1 15 0 309.26 2.22 -1 15 0 346.86 2.57 -1 15 0 321.57 2.33 1 15 0 319.01 2.06 -1 15 0 341.09 4.15 1 -15 0 327.12 2.58 1 -15 1 110.29 1.27 -1 15 -1 104.49 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20.98 0.81 2 1 -1 20.82 0.69 2 1 -1 21.86 0.80 2 -1 -1 21.72 0.84 2 1 0 8.95 0.37 2 1 0 8.63 0.33 2 1 1 171.84 2.31 2 -1 1 175.65 2.43 2 1 2 437.41 3.92 2 -1 2 437.51 4.06 2 1 3 5.77 0.21 2 -1 3 5.62 0.21 2 1 3 5.84 0.40 2 -1 3 6.52 0.24 2 -1 3 7.18 0.46 2 1 3 5.91 0.22 2 1 3 7.20 0.28 2 1 3 5.78 0.24 2 1 4 120.57 1.05 2 -1 4 115.67 1.03 2 -1 4 117.25 1.72 2 -1 4 119.09 1.17 2 1 4 116.64 1.15 2 1 4 121.49 1.16 2 -1 4 119.46 1.11 2 1 4 118.17 1.34 2 -1 4 118.83 1.28 2 1 4 117.68 1.24 2 1 4 119.75 1.66 2 1 5 28.23 0.56 2 1 5 29.30 0.55 2 -1 5 29.07 0.51 2 1 5 27.64 0.66 2 1 5 26.94 0.45 2 -1 5 28.62 0.63 2 1 5 28.69 0.62 2 -1 5 27.31 0.44 2 1 6 5.88 0.28 2 -1 6 5.92 0.34 2 1 6 6.17 0.34 2 1 6 5.54 0.19 2 -1 6 6.69 0.33 2 -1 7 39.80 0.70 2 1 7 38.01 0.80 2 -1 7 38.53 0.83 2 1 7 37.19 0.72 2 1 8 106.46 1.14 2 -1 8 108.37 1.33 2 1 8 107.32 1.30 2 -1 8 110.01 1.15 2 1 9 6.32 0.24 2 -1 9 6.06 0.27 2 1 9 6.04 0.26 2 -1 9 6.43 0.24 2 1 10 23.37 0.38 2 2 -12 3.28 0.12 2 -2 -12 3.81 0.15 2 2 -12 3.60 0.14 2 -2 -12 3.48 0.15 2 2 -11 0.13 0.09 2 -2 -11 0.11 0.09 2 2 -11 0.21 0.09 2 -2 -11 0.29 0.11 2 -2 -11 0.23 0.09 2 2 -10 46.24 0.73 2 2 -10 47.60 0.83 2 2 -9 79.66 1.05 2 -2 -9 84.51 1.07 2 2 -9 83.19 1.22 2 2 -9 78.92 1.16 2 -2 -8 61.29 0.91 2 2 -8 60.51 1.05 2 -2 -8 59.11 1.07 2 -2 -8 56.31 1.65 2 2 -8 55.25 1.83 2 -2 -8 56.13 1.93 2 2 -8 52.53 0.77 2 -2 -8 54.10 0.81 2 2 -8 57.51 0.98 2 2 -7 76.97 1.00 2 -2 -7 77.18 1.00 2 -2 -7 79.41 1.97 2 2 -7 71.72 1.66 2 2 -7 78.72 2.18 2 -2 -7 81.11 2.30 2 2 -7 73.55 0.93 2 2 -7 74.76 1.11 2 -2 -7 78.23 1.03 2 2 -6 10.20 0.32 2 -2 -6 10.17 0.37 2 -2 -6 10.73 0.82 2 -2 -6 11.96 0.75 2 2 -5 133.85 1.88 2 -2 -5 135.85 1.28 2 2 -5 128.23 1.22 2 -2 -5 133.67 2.40 2 2 -5 130.41 2.18 2 2 -5 148.02 2.76 2 -2 -5 131.47 1.36 2 -2 -5 140.87 2.08 2 2 -5 136.82 1.29 2 -2 -5 138.86 1.38 2 2 -5 129.82 1.24 2 2 -4 372.62 3.80 2 -2 -4 375.23 2.41 2 2 -4 389.25 3.62 2 2 -4 398.48 4.39 2 -2 -4 374.73 2.55 2 2 -4 374.95 2.47 2 2 -4 375.47 2.49 2 -2 -4 377.49 2.55 2 -2 -4 394.49 3.84 2 -2 -3 343.07 3.61 2 -2 -3 342.83 3.70 2 2 -3 341.29 3.54 2 2 -3 340.02 3.37 2 -2 -2 7.07 0.50 2 -2 -2 8.27 0.54 2 2 -2 7.86 0.51 2 2 -2 7.42 0.47 2 2 -2 6.68 0.45 2 -2 -1 315.77 3.43 2 2 -1 313.46 2.88 2 -2 -1 318.63 3.38 2 2 -1 309.84 2.90 2 2 0 372.99 2.70 2 2 0 385.02 2.80 2 -2 1 475.54 4.40 2 2 1 477.91 4.11 2 2 2 51.45 1.18 2 -2 2 52.10 1.30 2 2 3 5.40 0.20 2 2 3 5.47 0.38 2 -2 3 5.41 0.21 2 -2 3 5.04 0.22 2 2 3 4.77 0.20 2 -2 3 5.70 0.42 2 2 3 4.99 0.24 2 2 3 4.80 0.21 2 -2 4 41.79 0.57 2 -2 4 40.96 1.03 2 -2 4 42.40 0.66 2 2 4 40.77 0.63 2 2 4 42.64 0.66 2 -2 4 42.49 0.60 2 2 4 43.04 0.76 2 2 4 41.31 0.93 2 -2 4 43.06 0.74 2 2 4 42.38 0.70 2 2 4 42.40 0.58 2 2 5 16.19 0.42 2 2 5 18.08 0.44 2 -2 5 16.87 0.37 2 2 5 16.56 0.51 2 2 5 17.00 0.36 2 -2 5 17.45 0.50 2 2 5 17.27 0.48 2 -2 5 16.82 0.34 2 -2 6 14.07 0.42 2 2 6 13.33 0.40 2 2 6 14.20 0.39 2 -2 6 14.14 0.52 2 2 6 13.74 0.48 2 2 6 13.09 0.30 2 -2 6 13.82 0.47 2 2 6 12.80 0.42 2 -2 7 476.70 3.03 2 -2 7 471.41 3.43 2 -2 8 10.03 0.34 2 -2 8 9.48 0.39 2 2 8 9.54 0.37 2 2 8 8.99 0.32 2 2 9 1.40 0.15 2 2 9 1.69 0.15 2 -2 9 1.43 0.15 2 -2 9 1.57 0.14 2 -2 9 1.64 0.14 2 2 10 0.04 0.05 2 2 10 0.06 0.05 2 3 -12 44.81 0.48 2 -3 -12 43.66 0.50 2 3 -11 39.64 0.57 2 -3 -11 40.96 0.68 2 3 -11 38.83 0.62 2 -3 -11 38.59 0.53 2 -3 -11 38.91 0.64 2 3 -10 6.09 0.31 -2 -3 10 6.13 0.19 2 3 -10 6.24 0.30 2 -3 -9 6.84 0.31 -2 -3 9 6.76 0.22 2 3 -9 6.66 0.34 2 3 -8 105.93 1.23 2 -3 -8 104.90 1.23 2 3 -8 97.89 1.37 2 -3 -8 101.99 2.30 2 3 -8 102.22 2.48 2 -3 -8 102.68 2.66 2 -3 -8 99.92 1.17 -2 3 8 109.15 2.25 2 3 -8 100.56 1.32 2 -3 -7 27.22 0.60 2 3 -7 30.56 0.72 2 -3 -7 30.06 1.43 2 3 -7 29.05 0.58 2 -3 -7 31.17 0.65 2 3 -7 27.43 0.54 2 3 -7 29.93 0.67 2 -3 -6 18.10 0.47 2 3 -6 17.66 0.44 2 -3 -6 18.32 1.07 2 3 -6 17.73 0.79 2 3 -6 17.90 0.43 2 -3 -6 18.16 0.50 2 3 -6 18.47 0.50 2 3 -5 32.28 1.26 2 -3 -5 30.76 0.61 2 3 -5 28.63 0.54 2 -3 -5 30.94 1.00 2 3 -5 30.88 0.59 2 -3 -5 31.39 0.62 2 3 -5 28.42 0.83 2 3 -5 28.53 0.54 2 3 -5 29.41 0.57 2 3 -4 10.06 0.54 2 -3 -4 11.51 0.63 2 -3 -4 9.83 0.31 2 3 -4 10.50 0.67 2 -3 -4 11.04 0.36 2 3 -4 9.69 0.33 2 -3 -4 10.06 0.64 2 -3 -4 10.43 0.35 2 3 -4 9.49 0.31 2 3 -3 3.18 0.32 2 -3 -3 2.59 0.32 2 3 -3 2.78 0.33 2 3 -3 3.37 0.35 2 -3 -2 338.02 3.68 2 -3 -2 345.26 3.65 2 3 -2 348.84 3.41 2 3 -2 344.86 3.52 2 3 -1 38.30 1.05 2 -3 -1 37.05 1.14 2 3 -1 36.55 0.90 2 3 0 101.47 1.31 2 -3 0 109.85 1.88 2 3 1 51.53 1.21 2 -3 1 51.61 1.34 2 3 2 27.67 0.86 2 -3 2 28.50 0.98 2 -3 2 28.51 0.50 2 -3 2 26.41 0.47 2 3 3 27.38 0.46 2 -3 3 27.41 0.53 2 -3 3 26.87 0.47 2 -3 3 26.07 0.49 2 3 3 26.76 0.41 2 3 3 25.40 0.53 2 -3 3 26.53 0.95 2 3 3 27.24 0.82 2 3 3 25.78 0.49 2 -3 4 121.54 1.07 2 3 4 126.65 1.03 2 -3 4 120.96 1.89 2 3 4 127.24 1.23 2 3 4 126.97 1.37 2 -3 4 127.68 1.36 2 3 4 127.36 1.09 2 3 4 123.96 1.25 2 -3 5 18.67 0.46 2 3 5 18.06 0.45 2 3 5 18.60 0.45 2 3 5 18.99 0.54 2 3 5 18.97 0.38 2 -3 5 18.86 0.53 2 3 5 18.91 0.48 2 -3 6 20.24 0.50 2 3 6 19.66 0.48 2 3 6 20.24 0.58 2 3 6 19.57 0.38 2 3 6 19.77 0.51 2 -3 7 23.52 0.54 2 3 7 22.11 0.52 2 -3 7 23.14 0.65 2 3 7 21.73 0.59 2 3 7 22.48 0.53 2 3 8 7.12 0.28 2 -3 8 7.72 0.35 2 3 8 7.55 0.33 2 3 9 85.06 0.97 2 -3 9 86.65 1.01 2 3 10 0.13 0.06 2 3 10 0.02 0.05 2 4 -11 0.47 0.10 2 -4 -11 0.28 0.10 2 4 -11 0.37 0.09 2 -4 -11 0.26 0.10 2 4 -10 6.74 0.31 2 -4 -10 6.83 0.33 -2 -4 10 6.64 0.20 2 4 -10 7.33 0.31 -2 -4 9 11.19 0.29 2 -4 -9 11.25 0.37 2 4 -9 11.05 0.43 2 -4 -9 9.95 0.31 2 4 -9 10.72 0.41 2 -4 -8 8.81 0.35 -2 4 8 10.17 0.71 2 -4 -8 9.25 0.82 2 4 -8 8.69 0.74 2 -4 -8 9.53 0.36 2 4 -8 8.19 0.30 2 4 -8 8.98 0.39 2 4 -7 0.50 0.13 2 4 -7 0.50 0.11 2 -4 -7 0.83 0.31 2 4 -7 0.38 0.13 2 -4 -7 0.53 0.13 2 4 -6 0.40 0.11 2 -4 -6 0.51 0.13 2 4 -6 0.55 0.11 2 4 -6 0.49 0.12 2 4 -6 0.83 0.26 2 -4 -6 0.51 0.26 2 -4 -6 0.50 0.11 2 4 -6 0.39 0.11 2 4 -6 0.38 0.10 2 -4 -6 0.48 0.12 2 4 -6 0.50 0.17 2 4 -5 122.70 1.31 2 4 -5 125.73 2.08 2 -4 -5 127.72 1.34 2 4 -5 126.17 1.29 2 -4 -5 126.27 1.36 2 -4 -5 125.55 2.11 2 4 -5 121.62 1.25 2 4 -4 23.00 0.49 2 -4 -4 24.19 1.00 2 -4 -4 24.69 0.94 2 4 -4 25.43 0.90 2 4 -4 23.41 0.40 2 4 -4 23.64 0.99 2 -4 -4 24.10 0.55 2 4 -4 23.60 0.51 2 -4 -4 22.79 0.53 2 4 -4 22.86 0.79 2 4 -3 127.87 1.96 2 -4 -3 134.71 2.27 2 4 -3 130.76 2.04 2 -4 -3 132.74 2.24 2 4 -3 132.75 2.26 2 4 -3 130.00 1.21 2 4 -3 125.28 1.22 2 4 -3 131.62 1.24 2 -4 -2 337.33 3.76 2 4 -2 339.40 3.36 2 -4 -2 348.16 3.71 2 4 -2 340.70 3.45 2 4 -1 16.20 0.67 2 4 -1 15.04 0.60 2 -4 0 141.70 2.16 2 4 0 135.93 1.63 2 4 1 29.20 0.90 2 -4 2 3.12 0.19 2 -4 2 3.54 0.19 2 -4 2 3.19 0.18 2 4 2 3.32 0.15 2 -4 2 2.92 0.35 2 4 2 2.79 0.29 2 -4 3 121.19 2.12 2 -4 3 118.65 1.22 2 -4 3 118.77 1.10 2 4 3 114.96 0.96 2 4 3 117.20 1.00 2 4 3 113.08 1.20 2 4 3 119.82 1.05 2 -4 4 132.34 1.13 2 -4 4 131.99 1.31 2 4 4 137.37 1.29 2 4 4 137.11 1.12 2 4 4 135.47 1.43 2 4 4 133.81 1.15 2 -4 5 46.77 0.75 2 4 5 44.89 0.61 2 4 5 45.79 0.72 2 4 5 45.44 0.84 2 4 5 44.74 0.61 2 4 5 43.96 0.73 2 -4 6 87.96 1.07 2 4 6 83.03 1.02 2 4 6 86.51 1.20 2 4 6 87.05 0.88 2 4 6 81.37 1.05 2 4 7 11.92 0.38 2 -4 7 13.46 0.41 2 4 7 13.05 0.39 2 -4 7 13.05 0.49 2 4 7 12.16 0.44 2 -4 7 13.20 0.45 2 4 8 42.06 0.66 -2 4 -8 42.53 0.51 2 4 8 44.58 0.68 2 -4 8 46.58 0.84 2 4 8 45.24 0.77 2 -4 9 8.87 0.31 2 4 9 9.08 0.29 2 4 10 43.31 0.42 2 4 10 38.02 0.43 2 5 -11 39.78 0.58 2 -5 -11 39.82 0.62 2 5 -10 0.27 0.11 2 -5 -10 0.40 0.11 2 5 -10 0.23 0.11 2 5 -9 0.53 0.14 2 5 -9 1.04 0.15 2 5 -9 0.44 0.13 -2 -5 9 1.30 0.12 2 -5 -9 0.41 0.12 2 -5 -9 0.39 0.09 2 5 -8 24.94 0.53 -2 5 8 26.26 1.15 2 5 -8 24.50 0.64 2 -5 -8 23.68 1.29 2 5 -8 22.24 0.56 2 5 -8 22.67 1.14 2 -5 -8 24.85 0.58 2 5 -8 25.23 0.63 -2 5 7 6.34 0.58 2 -5 -7 5.17 0.27 2 5 -7 5.24 0.26 2 -5 -7 6.39 0.69 2 5 -7 5.92 0.62 2 -5 -7 5.90 0.30 2 5 -7 6.01 0.31 2 -5 -6 2.99 0.21 2 5 -6 2.96 0.20 2 5 -6 2.99 0.43 2 -5 -6 2.93 0.49 2 -5 -6 2.42 0.20 2 5 -6 2.83 0.20 2 -5 -6 2.54 0.21 2 5 -6 2.73 0.21 2 5 -5 0.52 0.11 2 5 -5 0.20 0.14 2 5 -5 0.04 0.17 2 -5 -5 0.09 0.10 2 5 -5 0.20 0.10 2 -5 -5 0.15 0.10 2 5 -5 0.19 0.10 2 5 -4 1.08 0.13 2 5 -4 1.31 0.10 2 -5 -4 1.06 0.27 2 5 -4 1.01 0.26 2 5 -4 1.05 0.26 2 -5 -4 1.13 0.15 2 5 -4 0.99 0.13 2 -5 -4 0.97 0.14 2 -5 -4 1.07 0.24 2 -5 -3 0.08 0.08 2 5 -3 0.05 0.07 2 5 -3 0.06 0.12 2 5 -3 0.02 0.13 2 5 -3 0.33 0.16 2 5 -3 0.09 0.06 2 5 -3 0.09 0.08 2 -5 -2 192.03 2.70 2 5 -2 188.73 2.55 2 -5 -2 185.33 2.78 2 5 -2 194.86 2.45 2 5 -1 65.27 1.31 2 -5 -1 64.71 1.60 2 -5 -1 64.28 1.47 2 5 -1 66.78 1.39 2 -5 0 0.21 0.14 2 5 0 0.48 0.17 2 5 0 0.12 0.09 2 5 1 74.95 0.77 2 -5 1 72.98 0.94 2 -5 1 74.26 0.92 2 5 1 76.13 0.78 2 5 1 72.17 0.86 2 -5 1 77.10 1.77 2 5 1 74.04 0.76 2 5 1 75.87 1.50 2 -5 2 31.29 0.60 2 -5 2 33.49 0.57 2 -5 2 33.39 1.15 2 5 2 32.12 0.46 2 5 2 32.20 0.47 2 5 2 32.50 0.48 2 5 2 31.62 0.51 2 5 2 33.27 0.50 2 -5 3 38.69 1.20 2 -5 3 35.73 0.66 2 5 3 35.73 0.49 2 -5 3 37.83 0.59 2 5 3 36.48 0.53 2 5 3 36.47 0.54 2 5 3 36.20 0.64 2 5 3 37.41 0.54 2 -5 4 98.96 1.14 2 -5 4 95.29 0.93 2 -5 4 97.91 1.10 2 5 4 95.61 0.94 2 5 4 96.84 1.08 2 5 4 96.28 1.17 2 5 4 97.92 0.96 2 5 5 257.18 2.02 2 -5 5 269.69 2.05 2 -5 5 278.27 2.11 2 5 5 273.28 1.87 2 5 5 269.42 2.03 2 5 5 271.34 2.27 2 5 5 264.79 1.83 2 -5 5 276.57 2.29 2 -5 6 78.13 1.01 2 5 6 74.63 0.83 2 5 6 77.75 1.12 2 -5 6 76.48 1.12 2 5 7 8.46 0.31 2 5 7 7.95 0.30 2 5 7 8.54 0.36 2 -5 7 8.84 0.37 2 5 8 106.83 1.07 2 -5 8 110.12 1.30 2 5 8 107.91 1.21 2 5 9 3.18 0.16 2 5 9 3.42 0.18 2 -6 -11 4.46 0.21 2 6 -11 4.13 0.18 2 -6 -11 4.76 0.21 2 6 -10 1.31 0.14 2 6 -10 1.46 0.15 2 6 -9 22.31 0.51 2 -6 -9 22.30 0.50 2 6 -9 21.45 0.57 -2 -6 9 20.29 0.39 2 6 -9 20.29 0.44 2 -6 -9 20.00 0.44 2 6 -9 21.46 0.55 2 6 -8 0.99 0.14 2 6 -8 0.96 0.17 2 6 -8 0.59 0.13 2 -6 -8 0.74 0.14 2 6 -8 0.90 0.17 2 -6 -7 262.45 2.06 2 6 -7 253.69 2.05 2 6 -7 260.99 2.27 2 -6 -7 262.85 4.39 2 6 -7 253.69 3.94 2 6 -7 261.02 2.04 2 -6 -7 258.54 2.18 2 6 -7 253.89 2.18 2 -6 -6 65.88 0.91 2 6 -6 62.85 0.98 2 -6 -6 63.71 0.94 2 6 -6 65.21 0.94 2 6 -6 65.63 0.94 2 -6 -6 64.20 0.99 2 6 -6 62.68 0.94 2 6 -5 12.45 0.28 2 6 -5 12.78 0.40 2 6 -5 12.61 0.40 2 -6 -5 13.09 0.42 2 6 -5 14.28 0.85 2 6 -5 13.21 0.41 2 -6 -5 13.11 0.44 2 6 -5 13.48 0.40 2 -6 -5 12.58 0.70 2 6 -4 54.97 0.64 2 -6 -4 56.15 0.81 2 -6 -4 55.14 0.79 2 6 -4 57.67 1.59 2 6 -4 54.23 0.82 2 -6 -4 56.78 1.60 2 6 -4 54.87 0.82 2 6 -4 56.21 0.72 2 6 -3 36.85 0.64 2 -6 -3 40.07 0.68 2 -6 -3 37.43 1.23 2 -6 -3 38.59 0.60 2 6 -3 40.15 1.25 2 -6 -3 36.11 0.68 2 -6 -3 38.34 1.28 2 6 -3 37.57 0.66 2 6 -3 38.15 0.53 2 -6 -3 39.65 0.73 2 6 -3 37.67 0.58 2 -6 -2 62.14 0.87 2 6 -2 63.46 0.84 2 6 -2 62.14 0.70 2 -6 -2 63.23 1.54 2 -6 -2 63.33 0.86 2 6 -2 60.36 1.22 2 6 -2 63.67 1.47 2 -6 -2 62.08 0.90 2 6 -2 62.82 0.81 2 6 -2 62.67 1.35 2 -6 -2 62.68 0.89 2 6 -2 61.84 0.74 2 6 -1 484.17 2.71 2 -6 -1 470.45 3.01 2 -6 -1 485.17 4.48 2 6 -1 481.50 4.12 2 -6 -1 484.91 3.11 2 6 -1 480.21 2.86 2 6 -1 477.49 2.97 2 6 -1 480.47 4.20 2 6 -1 477.14 2.81 2 -6 0 51.87 0.78 2 6 0 51.85 0.63 2 -6 0 55.96 1.35 2 6 0 52.19 1.08 2 -6 0 55.22 0.82 2 6 0 51.57 0.63 2 6 0 51.10 0.68 2 6 0 53.70 0.65 2 6 0 49.49 0.71 2 6 0 48.80 1.21 2 6 0 51.16 0.60 2 -6 1 47.08 0.77 2 6 1 47.43 0.59 2 6 1 48.09 0.60 2 -6 1 49.09 0.76 2 6 1 47.00 0.70 2 -6 1 49.18 0.76 2 6 1 48.24 0.61 2 6 1 49.00 0.67 2 -6 1 49.41 1.46 2 6 1 49.80 0.61 2 -6 2 7.88 0.32 2 -6 2 7.36 0.29 2 -6 2 7.18 0.27 2 6 2 6.74 0.28 2 -6 2 8.14 0.59 2 6 2 6.71 0.21 2 6 2 7.27 0.22 2 -6 2 7.37 0.29 2 6 2 6.44 0.22 2 6 2 6.50 0.24 2 6 2 6.74 0.23 2 6 3 61.97 0.68 2 -6 3 62.78 0.92 2 -6 3 62.99 1.60 2 6 3 62.38 0.70 2 6 3 63.17 0.74 2 6 3 63.34 0.78 2 6 3 61.60 0.86 2 -6 3 65.26 0.80 2 -6 4 476.47 3.17 2 -6 4 477.10 2.77 2 6 4 485.44 2.83 2 6 4 477.59 2.85 2 6 4 472.41 3.18 2 6 4 487.69 2.81 2 -6 5 202.93 1.75 2 6 5 200.96 1.56 2 6 5 205.48 1.69 2 6 5 203.12 1.90 2 6 5 203.76 1.55 2 -6 5 208.54 1.93 2 6 6 38.73 0.68 2 6 6 39.70 0.60 2 6 6 40.84 0.79 2 6 7 0.13 0.10 2 6 7 0.36 0.12 2 -6 7 0.10 0.13 -2 6 -8 15.16 0.30 2 6 8 15.35 0.37 2 -6 8 15.95 0.47 2 6 8 15.14 0.42 2 6 9 39.07 0.49 2 6 9 39.04 0.55 2 7 -11 4.78 0.17 2 -7 -11 4.75 0.20 2 7 -10 1.08 0.13 -2 -7 10 0.87 0.09 2 7 -10 0.91 0.12 2 7 -9 12.52 0.38 2 7 -9 11.93 0.34 2 -7 -9 12.99 0.35 2 7 -9 12.68 0.41 2 7 -8 203.18 1.73 2 7 -8 203.10 1.95 2 -7 -8 206.96 1.82 2 7 -8 205.23 1.88 2 -7 -7 16.26 0.46 2 7 -7 16.23 0.47 2 7 -7 16.17 0.51 2 -7 -7 16.08 1.09 2 7 -7 14.20 0.40 2 7 -7 16.24 0.98 2 7 -7 16.36 0.35 2 7 -7 16.62 0.46 2 -7 -7 16.09 0.49 2 7 -7 16.02 0.49 2 -7 -6 93.19 1.12 -2 7 6 93.37 2.10 2 7 -6 89.68 1.18 2 7 -6 95.59 1.18 2 -7 -6 90.14 1.14 2 7 -6 94.22 1.16 2 -7 -6 87.39 1.21 2 7 -6 85.70 1.12 2 7 -5 57.95 0.89 2 7 -5 56.47 0.86 2 -7 -5 52.66 1.49 2 7 -5 61.34 1.78 2 -7 -5 60.14 0.93 2 7 -5 57.77 0.88 2 7 -5 53.40 0.71 2 7 -5 55.68 0.83 2 7 -4 2.86 0.15 2 7 -4 2.77 0.20 2 -7 -4 2.69 0.38 2 -7 -4 2.71 0.19 2 -7 -4 2.42 0.35 2 7 -4 2.50 0.20 2 7 -4 2.49 0.20 2 -7 -4 3.04 0.23 2 7 -4 2.76 0.16 2 7 -3 15.83 0.34 2 7 -3 15.33 0.43 2 -7 -3 16.16 0.44 2 -7 -3 15.77 0.38 2 7 -3 15.54 0.75 2 7 -3 15.95 0.82 2 -7 -3 15.53 0.46 2 7 -3 17.10 0.45 2 -7 -3 16.39 0.49 2 7 -3 15.29 0.36 2 -7 -2 457.31 3.00 2 7 -2 446.18 2.89 2 7 -2 449.06 2.60 2 7 -2 434.93 4.88 2 -7 -2 448.59 2.97 2 -7 -2 451.54 4.51 2 7 -2 424.22 3.69 2 7 -2 456.11 4.39 2 7 -2 453.63 2.67 2 -7 -2 458.06 3.07 2 7 -2 445.88 2.67 2 -7 -1 10.02 0.36 2 7 -1 10.78 0.28 2 7 -1 11.79 0.75 2 -7 -1 12.31 0.39 2 7 -1 11.75 0.60 2 -7 -1 11.74 0.64 2 7 -1 11.58 0.36 2 7 -1 11.36 0.34 2 7 -1 11.45 0.30 2 7 -1 11.21 0.35 2 -7 -1 13.19 0.81 2 -7 -1 10.78 0.37 2 7 -1 10.73 0.25 2 -7 0 192.99 1.76 2 7 0 204.59 3.21 2 7 0 202.48 1.46 2 -7 0 211.70 2.71 2 7 0 193.49 1.59 2 7 0 205.43 1.48 2 -7 0 196.32 1.77 2 7 0 208.78 1.62 2 7 0 208.02 1.67 2 -7 0 202.92 1.77 2 7 0 203.92 1.41 2 7 0 204.48 1.51 2 -7 1 46.18 0.79 2 7 1 47.42 0.61 2 -7 1 47.79 0.77 2 7 1 47.61 0.73 2 7 1 48.66 0.62 2 -7 1 49.70 0.80 2 7 1 46.69 0.62 2 7 1 46.45 0.68 2 7 1 46.64 0.69 2 7 1 46.07 0.60 2 7 1 46.50 0.60 2 7 2 5.54 0.20 2 -7 2 6.32 0.30 2 -7 2 5.76 0.27 2 -7 2 5.80 0.25 2 7 2 5.47 0.26 2 7 2 5.87 0.21 2 -7 2 6.01 0.54 2 7 2 5.90 0.22 2 -7 2 5.74 0.27 2 7 2 5.80 0.20 2 7 2 5.84 0.24 2 7 2 5.98 0.22 2 7 3 118.38 1.03 2 -7 3 123.39 1.38 2 -7 3 125.40 1.19 2 7 3 121.07 1.08 2 -7 3 123.87 2.34 2 7 3 123.80 1.12 2 -7 3 122.66 1.28 2 7 3 121.19 1.22 2 7 3 125.79 1.20 2 7 3 120.94 1.27 2 -7 4 886.44 5.10 2 7 4 879.36 4.66 2 7 4 881.02 4.73 2 7 4 889.47 5.04 2 7 4 897.29 4.64 2 -7 5 107.51 1.25 2 7 5 110.36 1.09 2 7 5 105.75 1.05 2 7 5 113.30 1.11 2 7 5 112.82 1.33 2 -7 5 114.79 1.38 2 -7 6 412.95 2.70 2 7 6 410.58 2.96 2 -7 6 419.79 3.01 2 7 7 0.26 0.09 2 7 7 0.30 0.11 2 -7 7 0.34 0.13 -2 7 -8 44.78 0.53 2 7 8 43.23 0.60 2 -7 8 45.96 0.79 2 7 8 44.58 0.68 2 7 9 0.75 0.09 2 7 9 0.77 0.09 2 8 -11 53.41 0.55 2 8 -11 52.23 0.51 2 -8 -11 52.90 0.60 2 8 -10 20.42 0.39 2 8 -10 20.10 0.42 2 8 -9 89.51 1.00 2 8 -9 88.56 0.97 -2 -8 9 91.35 0.86 2 8 -9 89.21 1.07 2 8 -8 34.22 0.65 2 -8 -8 32.96 0.66 2 8 -8 34.51 0.69 2 8 -7 21.91 0.55 -2 8 7 22.68 1.07 2 -8 -7 22.15 1.27 2 8 -7 21.62 1.10 2 8 -7 20.65 0.51 2 -8 -7 20.83 0.56 2 8 -7 21.20 0.55 2 8 -6 271.32 2.23 -2 8 6 276.48 3.73 2 -8 -6 268.82 2.17 2 8 -6 260.68 1.79 2 8 -6 263.29 2.16 2 -8 -6 258.28 2.31 2 8 -6 253.15 2.12 2 8 -5 182.81 3.17 2 -8 -5 184.90 1.78 2 8 -5 180.83 1.44 2 8 -5 184.11 1.74 2 8 -5 177.36 1.62 2 8 -4 3.85 0.18 2 8 -4 3.74 0.23 2 -8 -4 3.62 0.23 2 -8 -4 3.74 0.45 2 8 -4 4.06 0.44 2 8 -4 3.50 0.43 2 -8 -4 3.77 0.25 2 -8 -4 3.62 0.43 2 8 -4 3.59 0.19 2 8 -4 3.70 0.24 2 8 -4 3.68 0.23 2 8 -4 3.28 0.19 2 8 -3 168.63 1.33 2 -8 -3 167.62 1.61 2 -8 -3 167.45 2.73 2 8 -3 162.05 2.46 2 8 -3 170.29 2.76 2 -8 -3 163.82 1.65 2 8 -3 170.24 3.00 2 8 -3 171.18 1.37 2 8 -3 170.49 1.56 2 8 -3 164.75 1.57 2 8 -3 167.12 1.38 2 -8 -3 171.29 1.76 2 8 -3 161.82 1.32 2 -8 -2 381.80 2.76 2 8 -2 386.52 2.38 2 -8 -2 387.87 2.80 2 -8 -2 393.87 4.19 2 8 -2 409.69 4.81 2 8 -2 396.31 4.18 2 -8 -2 390.54 2.87 2 8 -2 389.87 2.42 2 8 -2 397.02 2.43 2 -8 -2 403.31 2.89 2 8 -2 398.41 2.68 2 -8 -2 413.28 4.86 2 8 -1 0.10 0.09 2 -8 -1 0.15 0.10 2 -8 -1 0.12 0.09 2 8 -1 0.07 0.05 2 -8 -1 0.18 0.16 2 8 -1 0.13 0.07 2 8 -1 0.06 0.12 2 8 -1 0.10 0.19 2 -8 -1 0.04 0.17 2 8 -1 0.14 0.09 2 8 -1 0.04 0.06 2 8 -1 0.29 0.08 2 8 -1 0.10 0.09 2 -8 -1 0.04 0.08 2 8 0 345.56 2.13 2 -8 0 326.30 2.50 2 8 0 331.97 2.33 2 -8 0 331.89 2.52 2 -8 0 346.79 3.53 2 8 0 335.30 2.14 2 -8 0 326.99 2.53 2 8 0 335.46 2.31 2 8 0 328.87 2.33 2 8 0 349.48 4.42 2 -8 0 335.80 2.41 2 8 0 334.20 2.04 2 8 0 332.11 2.17 2 8 1 267.20 1.82 2 -8 1 270.57 2.17 2 8 1 264.28 2.07 2 8 1 271.12 1.84 2 -8 1 278.16 2.23 2 8 1 280.14 3.90 2 8 1 280.52 2.03 2 8 1 267.83 1.99 2 8 1 266.63 1.83 2 8 1 271.59 1.79 2 8 2 20.60 0.40 2 -8 2 19.26 0.53 2 -8 2 19.59 0.50 2 -8 2 20.11 0.52 2 8 2 20.26 0.51 2 8 2 20.43 0.41 2 8 2 20.03 0.41 2 8 2 21.05 0.46 2 8 2 20.49 0.47 2 8 2 20.18 0.40 2 -8 2 20.31 0.99 2 8 2 19.36 0.44 2 8 2 21.59 0.41 2 -8 3 463.24 3.28 2 -8 3 482.72 2.95 2 -8 3 470.05 5.01 2 8 3 479.31 2.86 2 -8 3 471.44 3.13 2 8 3 481.10 2.98 2 8 3 499.10 3.04 2 -8 3 483.92 3.10 2 8 3 470.81 3.06 2 8 3 476.35 2.83 2 -8 4 329.73 2.59 2 8 4 339.47 2.26 2 8 4 341.56 2.38 2 8 4 345.07 2.35 2 8 4 332.88 2.25 2 8 4 342.36 2.54 2 -8 5 150.75 1.53 2 8 5 153.41 1.35 2 8 5 150.24 1.33 2 8 5 155.76 1.36 2 8 5 153.02 1.58 2 -8 5 155.93 1.63 2 -8 6 21.13 0.49 2 8 6 21.47 0.54 2 -8 6 21.99 0.57 2 8 7 44.76 0.65 -2 8 -7 45.67 0.60 2 8 7 46.70 0.75 -2 8 -8 18.69 0.33 2 8 8 17.77 0.35 2 -8 8 18.51 0.47 2 8 8 18.18 0.40 2 8 9 0.75 0.07 2 8 9 0.92 0.08 2 9 -10 78.03 0.81 2 9 -10 75.34 0.74 2 9 -9 0.24 0.10 2 9 -9 0.11 0.08 2 -9 -9 0.11 0.07 2 9 -8 9.93 0.35 -2 -9 8 10.56 0.29 2 9 -8 9.64 0.25 2 -9 -8 10.21 0.36 2 9 -8 10.07 0.36 2 9 -7 15.76 0.36 2 9 -7 16.22 0.45 2 -9 -7 15.54 0.49 2 9 -7 16.39 0.47 2 9 -6 76.39 1.08 -2 9 6 82.67 2.03 2 9 -6 67.97 1.98 2 -9 -6 75.37 1.04 2 9 -6 72.73 0.80 2 9 -6 73.97 0.86 2 9 -6 74.85 1.04 2 -9 -6 76.84 1.17 2 9 -6 70.91 0.99 2 9 -5 60.17 0.95 2 -9 -5 56.77 0.86 2 9 -5 53.64 1.69 2 9 -5 60.15 1.78 2 -9 -5 56.63 0.94 2 9 -5 57.60 0.73 2 9 -5 58.55 0.76 2 9 -5 59.53 0.94 2 -9 -5 60.71 1.04 2 9 -5 56.61 0.84 2 -9 -4 0.78 0.24 2 -9 -4 0.53 0.12 2 9 -4 0.72 0.22 2 9 -4 0.69 0.24 2 -9 -4 0.62 0.14 2 -9 -4 0.69 0.23 2 9 -4 0.46 0.15 2 9 -4 1.08 0.12 2 9 -4 0.60 0.14 2 9 -3 27.97 0.61 2 -9 -3 26.55 0.62 2 -9 -3 31.23 1.16 2 9 -3 25.98 0.95 2 9 -3 28.39 1.13 2 9 -3 26.71 0.49 2 -9 -3 27.28 0.65 2 9 -3 28.74 1.26 2 9 -3 28.83 0.60 2 9 -3 29.75 0.51 2 9 -3 26.35 0.61 2 -9 -3 28.51 1.24 2 -9 -3 28.92 0.70 2 9 -2 8.09 0.26 2 -9 -2 7.56 0.67 2 -9 -2 7.97 0.34 2 9 -2 7.31 0.30 2 -9 -2 8.27 0.58 2 9 -2 7.32 0.26 2 9 -2 8.46 0.58 2 -9 -2 8.03 0.36 2 -9 -2 7.97 0.35 2 9 -2 7.37 0.32 2 -9 -2 8.25 0.37 2 9 -1 17.98 0.39 2 -9 -1 16.70 0.49 2 9 -1 17.51 0.46 2 -9 -1 18.79 1.03 2 -9 -1 17.43 0.51 2 9 -1 16.32 0.42 2 9 -1 18.17 0.79 2 9 -1 17.75 0.39 2 9 -1 17.87 0.40 2 9 -1 17.32 0.46 2 9 -1 15.50 0.32 2 -9 -1 18.55 0.53 2 9 -1 17.98 0.41 2 -9 0 0.52 0.13 2 -9 0 0.32 0.12 2 9 0 0.33 0.07 2 9 0 0.25 0.09 2 9 0 0.32 0.09 2 -9 0 0.35 0.13 2 -9 0 0.49 0.24 2 9 0 0.27 0.08 2 9 0 0.33 0.11 2 9 0 0.30 0.09 2 9 0 0.34 0.10 2 -9 0 0.89 0.13 2 9 0 0.73 0.11 2 -9 1 36.59 0.73 2 9 1 34.25 0.66 2 9 1 35.77 0.57 2 9 1 37.12 1.42 2 -9 1 36.32 0.74 2 9 1 35.14 0.58 2 9 1 35.58 0.64 2 9 1 33.08 0.61 2 9 1 34.65 0.56 2 -9 1 34.84 1.39 2 9 1 35.68 0.54 2 -9 2 303.80 2.47 2 -9 2 298.68 2.36 2 9 2 303.68 2.07 2 9 2 302.35 2.35 2 9 2 304.63 2.05 2 -9 2 300.16 2.42 2 9 2 300.96 2.12 2 9 2 297.22 2.03 2 9 2 297.25 2.13 2 -9 3 123.21 1.46 2 -9 3 126.52 1.21 2 -9 3 122.39 1.31 2 -9 3 116.57 2.40 2 9 3 122.38 1.17 2 -9 3 117.37 1.34 2 9 3 121.61 1.22 2 9 3 127.11 1.28 2 9 3 121.26 1.17 2 9 3 122.16 1.29 2 -9 4 80.06 1.13 2 9 4 80.73 0.93 2 9 4 80.67 0.97 2 9 4 81.83 0.99 2 9 4 79.24 1.05 2 -9 5 32.09 0.67 2 9 5 32.89 0.58 2 9 5 32.60 0.57 2 9 5 32.92 0.67 2 -9 5 33.56 0.71 2 -9 6 7.19 0.29 2 9 6 7.10 0.30 2 -9 6 7.62 0.33 -2 9 -7 3.21 0.16 2 9 7 3.03 0.16 2 9 7 3.31 0.20 2 -9 7 3.42 0.21 -2 9 -8 77.39 0.70 2 9 8 77.57 0.81 2 10 -10 20.33 0.34 -2 -10 10 18.85 0.28 2 10 -9 17.49 0.41 2 10 -9 17.86 0.37 2 10 -9 17.71 0.39 2 -10 -9 16.88 0.35 2 10 -8 4.56 0.24 -2 -10 8 4.76 0.19 2 -10 -8 4.40 0.24 2 10 -8 4.11 0.18 2 10 -7 20.39 0.53 -2 -10 7 20.99 0.41 2 10 -7 19.64 0.37 2 10 -7 19.84 0.49 2 -10 -7 20.60 0.56 2 10 -6 11.98 0.42 2 10 -6 9.88 0.74 2 10 -6 10.29 0.28 2 -10 -6 10.28 0.37 2 10 -6 11.22 0.31 2 10 -6 11.41 0.40 2 -10 -6 9.68 0.42 2 10 -5 50.14 0.87 -2 10 5 52.02 1.56 2 -10 -5 46.71 0.78 2 -10 -5 45.34 1.51 2 10 -5 43.21 1.46 2 10 -5 46.55 1.58 2 10 -5 46.85 0.65 2 -10 -5 48.03 0.86 2 10 -5 47.74 0.67 2 10 -5 48.55 0.86 2 -10 -5 47.75 0.95 2 10 -4 2.08 0.16 -2 10 4 2.18 0.33 2 -10 -4 1.93 0.34 2 10 -4 2.26 0.33 2 10 -4 2.56 0.39 2 10 -4 2.18 0.15 2 -10 -4 2.27 0.21 2 10 -4 2.12 0.15 2 10 -4 1.76 0.21 2 -10 -4 2.24 0.19 2 10 -4 2.31 0.20 2 10 -3 23.50 0.57 -2 10 3 23.96 0.93 2 -10 -3 23.12 0.60 2 -10 -3 24.39 1.04 2 10 -3 23.56 0.91 2 10 -3 25.78 1.10 2 10 -3 24.15 0.48 2 -10 -3 23.89 0.62 2 10 -3 24.98 0.58 2 10 -3 24.51 0.59 2 10 -3 26.09 1.25 2 -10 -3 26.79 0.69 2 -10 -3 21.64 1.12 2 -10 -2 1.83 0.19 2 10 -2 2.16 0.18 2 -10 -2 1.97 0.38 2 -10 -2 2.06 0.20 2 -10 -2 2.12 0.31 2 10 -2 1.82 0.15 2 10 -2 1.96 0.15 2 -10 -2 2.04 0.20 2 10 -2 2.30 0.16 2 10 -2 2.45 0.20 2 -10 -2 2.12 0.22 2 10 -1 0.40 0.10 2 10 -1 0.45 0.12 2 -10 -1 0.35 0.12 2 -10 -1 0.37 0.13 2 10 -1 0.26 0.07 -2 10 1 0.59 0.11 2 10 -1 0.24 0.09 2 -10 -1 0.37 0.24 2 10 -1 0.60 0.10 2 10 -1 0.36 0.10 2 10 -1 0.26 0.12 2 -10 -1 0.28 0.12 2 -10 0 286.90 2.40 2 -10 0 283.60 2.40 2 -10 0 285.73 4.29 -2 10 0 278.74 2.05 2 10 0 283.30 2.21 2 -10 0 292.47 2.43 2 10 0 289.79 1.98 2 10 0 297.61 2.20 2 10 0 288.72 2.22 2 10 0 274.39 1.87 2 10 0 287.29 2.03 2 -10 0 293.51 2.31 2 -10 1 1.79 0.20 2 -10 1 1.15 0.16 2 -10 1 0.86 0.28 2 10 1 2.15 0.18 2 10 1 1.34 0.13 2 10 1 1.02 0.12 2 10 1 1.62 0.34 2 -10 1 1.08 0.16 2 10 1 0.96 0.12 2 10 1 1.08 0.14 2 10 1 1.06 0.12 2 10 1 0.84 0.12 2 10 1 0.90 0.11 2 10 2 0.22 0.09 2 10 2 0.15 0.10 2 10 2 0.42 0.10 2 10 2 0.32 0.10 2 -10 2 0.15 0.12 2 10 2 0.16 0.10 2 -10 2 0.24 0.11 2 -10 3 230.89 2.13 2 -10 3 235.94 1.77 2 -10 3 235.14 1.97 2 10 3 236.29 1.78 2 -10 3 231.43 2.04 2 10 3 236.47 1.80 2 10 3 240.71 1.92 2 10 3 233.26 1.77 2 10 3 228.17 1.89 2 -10 4 116.47 1.40 2 10 4 114.05 1.16 2 -10 4 111.43 1.24 2 10 4 115.56 1.18 2 10 4 118.81 1.22 2 10 4 116.35 1.27 2 -10 5 5.00 0.28 2 10 5 5.28 0.24 2 10 5 4.69 0.22 2 10 5 5.04 0.26 2 -10 5 5.29 0.29 2 -10 6 34.42 0.62 -2 10 -6 34.52 0.54 2 10 6 33.78 0.63 2 -10 6 34.48 0.66 -2 10 -7 69.58 0.73 2 10 7 70.70 0.84 2 -10 7 72.32 0.87 -2 10 -8 4.88 0.15 2 -10 8 4.87 0.22 2 10 8 4.87 0.18 2 11 -10 29.05 0.35 -2 -11 10 26.50 0.31 2 11 -9 31.40 0.50 2 11 -9 29.63 0.43 2 11 -9 30.72 0.49 2 11 -9 31.74 0.49 -2 -11 9 30.53 0.43 2 -11 -9 30.27 0.42 2 11 -8 0.20 0.06 2 11 -8 0.44 0.10 2 11 -8 0.22 0.10 -2 -11 8 0.34 0.09 2 -11 -8 0.14 0.09 2 11 -7 14.21 0.41 -2 -11 7 14.93 0.34 -2 11 7 14.34 0.34 2 11 -7 14.88 0.44 2 11 -7 15.25 0.42 2 11 -7 14.47 0.35 2 11 -6 14.62 0.42 2 11 -6 14.33 0.31 2 -11 -6 15.31 0.44 2 11 -6 15.56 0.34 2 11 -6 15.01 0.46 2 -11 -6 15.20 0.52 -2 -11 6 14.67 0.34 2 11 -6 15.09 0.39 2 11 -5 1.73 0.16 2 -11 -5 2.35 0.19 2 -11 -5 1.75 0.33 2 11 -5 1.95 0.14 2 11 -5 1.63 0.30 2 11 -5 1.95 0.35 2 -11 -5 2.34 0.21 2 11 -5 1.98 0.20 2 -11 -5 1.89 0.22 2 11 -5 1.91 0.17 2 11 -4 14.08 0.39 2 11 -4 14.71 0.47 -2 11 4 14.38 0.79 2 -11 -4 15.50 0.85 2 11 -4 13.14 0.74 2 11 -4 15.11 0.37 2 11 -4 14.37 0.86 2 -11 -4 15.25 0.50 2 11 -4 15.42 0.37 2 11 -4 15.06 0.47 2 11 -4 15.50 0.49 2 -11 -4 15.61 0.47 2 11 -4 15.70 0.42 2 11 -3 53.69 0.87 2 -11 -3 57.59 0.96 2 -11 -3 53.21 1.53 2 11 -3 56.32 0.75 2 11 -3 55.74 1.62 2 -11 -3 58.93 1.00 2 11 -3 56.27 1.88 2 11 -3 56.92 0.75 2 11 -3 58.17 0.90 2 11 -3 55.56 0.93 2 -11 -3 58.23 1.06 2 11 -3 58.51 0.82 2 -11 -3 55.20 1.85 2 -11 -2 31.30 0.69 2 11 -2 32.48 0.65 2 -11 -2 33.30 0.74 2 -11 -2 30.55 1.39 2 11 -2 30.73 0.58 2 11 -2 32.62 0.56 2 -11 -2 32.93 0.75 2 11 -2 32.86 0.55 2 11 -2 32.78 0.70 2 -11 -1 186.11 1.84 2 11 -1 194.49 1.72 2 -11 -1 187.17 1.92 -2 11 1 186.95 1.65 2 11 -1 182.38 1.65 2 11 -1 191.66 1.54 2 -11 -1 188.83 3.54 2 -11 -1 186.68 1.91 2 11 -1 190.85 3.52 2 11 -1 187.96 1.51 2 11 -1 195.91 1.73 2 11 -1 189.13 1.77 2 11 -1 180.74 1.57 2 11 0 0.42 0.10 2 -11 0 0.44 0.24 2 -11 0 0.40 0.13 -2 11 0 0.58 0.10 2 11 0 0.40 0.11 2 11 0 0.52 0.11 2 11 0 0.38 0.08 2 -11 0 0.50 0.15 2 -11 0 0.57 0.15 2 11 0 0.45 0.12 2 11 0 0.46 0.09 2 -11 0 0.39 0.11 2 -11 1 16.86 1.02 2 -11 1 16.89 0.52 -2 11 -1 16.66 0.42 2 -11 1 17.25 0.53 2 11 1 17.27 0.42 2 11 1 16.65 0.49 2 11 1 16.44 0.40 2 11 1 17.81 1.04 2 -11 1 16.64 0.53 2 11 1 16.20 0.38 2 11 1 16.76 0.46 2 11 1 16.85 0.42 2 11 1 15.72 0.44 2 11 1 16.16 0.39 2 -11 2 44.16 0.81 -2 11 -2 44.22 0.69 2 11 2 44.90 0.81 2 11 2 46.70 0.69 2 -11 2 42.61 0.84 2 11 2 43.46 0.65 2 11 2 46.80 0.77 2 11 2 44.63 0.67 2 11 2 44.51 0.70 2 -11 3 102.30 1.32 2 -11 3 100.75 1.20 2 -11 3 98.73 1.25 2 11 3 101.44 1.05 2 11 3 104.20 1.18 2 11 3 100.69 1.15 2 -11 4 3.44 0.25 2 11 4 3.34 0.20 2 -11 4 3.28 0.21 2 11 4 3.27 0.20 2 11 4 3.19 0.20 2 -11 5 129.06 1.38 2 11 5 132.30 1.22 2 11 5 123.97 1.20 2 11 5 127.88 1.30 2 -11 5 127.30 1.36 -2 11 -6 65.04 0.74 2 -11 6 65.68 0.88 -2 11 -7 7.73 0.22 2 11 7 7.73 0.25 -2 11 -8 22.44 0.30 2 -11 8 22.24 0.40 2 11 8 21.47 0.32 2 12 -9 6.83 0.20 2 12 -9 6.66 0.21 -2 -12 9 7.24 0.19 -2 -12 9 6.99 0.18 2 12 -8 1.94 0.14 2 12 -8 1.84 0.14 2 12 -8 2.10 0.16 2 12 -8 1.76 0.10 2 -12 -8 1.90 0.15 2 12 -7 9.62 0.32 2 12 -7 9.52 0.32 2 12 -7 9.80 0.35 -2 -12 7 10.05 0.27 -2 12 7 9.43 0.27 2 12 -7 9.55 0.32 2 -12 -7 10.15 0.37 2 12 -7 9.58 0.27 2 12 -6 0.42 0.10 2 12 -6 0.36 0.11 2 12 -6 0.36 0.10 2 12 -6 0.48 0.14 -2 -12 6 0.49 0.09 2 -12 -6 0.34 0.10 2 12 -6 0.37 0.13 2 -12 -6 0.30 0.14 2 12 -5 49.49 0.75 2 12 -5 51.64 0.78 2 -12 -5 56.43 0.85 -2 12 5 52.65 0.70 -2 -12 5 53.27 0.64 2 12 -5 54.83 0.68 2 -12 -5 55.15 0.89 2 12 -5 54.75 0.66 2 12 -5 55.44 0.91 2 -12 -5 57.44 1.05 2 12 -5 56.60 0.79 2 12 -4 44.95 0.80 2 -12 -4 45.49 0.82 2 12 -4 44.90 0.64 2 -12 -4 45.69 0.86 2 12 -4 45.48 0.63 2 12 -4 46.17 0.80 2 12 -4 47.16 0.85 2 12 -4 45.60 0.73 2 12 -3 55.33 0.88 2 -12 -3 56.09 0.96 2 12 -3 56.18 0.74 2 -12 -3 56.82 0.99 2 12 -3 55.29 1.89 2 12 -3 57.14 0.73 2 12 -3 58.97 0.91 2 12 -3 57.94 0.95 2 -12 -3 59.92 1.07 2 12 -3 57.72 0.82 2 -12 -3 53.21 1.82 2 -12 -2 10.22 0.40 2 12 -2 10.39 0.37 2 -12 -2 9.59 0.79 2 -12 -2 10.44 0.42 2 12 -2 10.01 0.33 2 12 -2 10.88 0.33 2 -12 -2 10.69 0.44 2 12 -2 10.86 0.31 2 12 -2 10.67 0.39 2 12 -2 10.65 0.41 2 -12 -2 10.96 0.45 2 -12 -1 12.99 0.45 2 12 -1 13.09 0.40 2 -12 -1 13.05 0.47 -2 12 1 12.16 0.39 2 12 -1 12.26 0.40 2 12 -1 12.72 0.36 2 -12 -1 12.36 0.91 2 -12 -1 12.69 0.47 2 12 -1 12.23 0.90 2 12 -1 12.54 0.34 2 12 -1 12.87 0.41 2 12 -1 12.38 0.43 2 12 -1 11.91 0.37 2 -12 -1 12.97 0.47 2 -12 0 3.46 0.26 -2 12 0 4.15 0.23 2 12 0 3.37 0.20 2 -12 0 3.38 0.50 2 12 0 3.05 0.22 2 12 0 3.55 0.20 2 12 0 3.63 0.22 2 12 0 3.20 0.22 2 -12 0 3.58 0.24 2 -12 1 5.61 0.62 2 -12 1 6.36 0.33 2 -12 1 6.04 0.32 2 12 1 6.50 0.27 -2 12 -1 6.46 0.27 2 12 1 6.20 0.31 2 12 1 6.18 0.25 2 12 1 6.34 0.65 2 -12 1 5.69 0.33 2 12 1 6.09 0.22 2 12 1 5.83 0.28 2 12 1 5.73 0.27 2 12 2 91.91 1.19 2 -12 2 90.86 1.25 -2 12 -2 90.94 1.03 2 -12 2 90.25 1.19 2 12 2 93.75 1.01 2 -12 2 91.00 1.24 2 12 2 90.91 0.93 -2 12 -3 0.58 0.10 2 -12 3 0.54 0.12 -2 12 -3 0.48 0.09 2 -12 3 0.80 0.15 2 12 3 0.66 0.13 2 12 3 0.61 0.11 2 -12 4 1.84 0.19 2 -12 4 1.53 0.16 2 12 4 2.20 0.18 2 12 4 1.84 0.16 2 -12 4 1.62 0.17 2 12 5 184.28 1.56 2 -12 5 184.73 1.61 2 -12 6 36.02 0.59 -2 12 -6 33.46 0.49 2 12 6 34.95 0.56 2 -12 6 34.50 0.57 -2 12 -7 3.75 0.15 2 13 -9 0.07 0.05 2 -13 -9 0.08 0.06 -2 -13 9 0.17 0.05 2 13 -8 11.79 0.28 -2 -13 8 12.07 0.27 -2 -13 8 12.59 0.26 2 -13 -8 12.04 0.31 2 13 -7 17.79 0.39 2 13 -7 18.40 0.44 -2 13 7 17.47 0.34 2 13 -7 17.32 0.40 2 13 -7 16.44 0.33 2 -13 -7 17.02 0.45 -2 -13 6 228.29 1.52 2 13 -6 230.80 1.86 2 -13 -6 233.46 2.05 2 13 -5 205.01 1.66 2 13 -5 209.69 1.84 2 -13 -5 208.14 1.75 -2 13 5 204.74 1.55 -2 -13 5 206.47 1.43 2 13 -5 200.37 1.47 2 -13 -5 218.05 1.86 2 13 -5 201.75 1.41 2 13 -5 218.31 1.91 2 -13 -5 212.21 2.08 2 13 -5 216.02 1.66 2 13 -4 159.71 1.42 2 13 -4 171.12 1.63 2 -13 -4 168.59 1.65 -2 13 4 165.51 1.44 -2 -13 4 163.96 1.21 2 13 -4 169.89 1.37 2 -13 -4 166.17 1.71 2 13 -4 167.11 1.29 2 13 -4 168.80 1.68 2 13 -4 173.98 1.49 2 13 -3 35.41 0.69 2 -13 -3 35.72 0.75 2 13 -3 36.03 0.59 2 -13 -3 36.01 0.77 2 13 -3 33.53 1.45 2 13 -3 35.37 0.55 2 13 -3 36.28 0.73 2 -13 -3 33.14 1.42 2 13 -3 35.14 0.63 2 -13 -3 37.69 0.83 2 -13 -2 17.92 1.07 2 -13 -2 18.93 0.53 2 13 -2 21.91 0.53 2 -13 -2 20.13 0.58 2 13 -2 20.55 0.46 2 13 -2 18.64 0.45 2 -13 -2 19.17 0.58 2 13 -2 20.53 0.43 2 13 -2 21.06 0.54 2 13 -2 21.14 0.56 2 13 -2 20.11 0.48 2 -13 -2 19.41 0.59 2 13 -1 64.13 0.89 2 -13 -1 63.27 1.04 -2 13 1 62.83 0.91 2 -13 -1 57.66 1.93 2 13 -1 65.70 0.85 2 13 -1 61.92 0.91 2 13 -1 63.72 0.79 2 -13 -1 65.74 1.07 2 13 -1 64.94 0.94 2 13 -1 62.00 0.96 2 -13 -1 60.70 1.01 2 -13 0 26.55 0.65 2 -13 0 24.42 1.25 2 13 0 28.21 0.55 -2 13 0 25.85 0.56 2 13 0 25.36 0.59 2 13 0 27.12 0.51 2 13 0 25.92 0.54 2 13 0 27.03 0.60 2 13 0 26.81 0.60 2 -13 0 25.63 0.60 2 -13 1 1.63 0.35 2 -13 1 0.78 0.16 2 -13 1 2.03 0.20 -2 13 -1 1.21 0.14 2 13 1 0.52 0.13 2 13 1 0.80 0.12 2 13 1 0.63 0.26 2 -13 1 0.65 0.14 2 13 1 1.44 0.16 2 -13 2 140.27 1.57 -2 13 -2 142.66 1.30 2 -13 2 142.74 1.51 2 -13 2 138.64 1.29 -2 13 -2 140.48 1.33 2 13 2 142.86 1.51 2 -13 2 142.50 1.58 2 13 2 143.27 1.42 -2 13 -3 138.38 1.17 2 -13 3 137.27 1.38 2 13 3 139.43 1.28 -2 13 -3 138.83 1.21 2 -13 3 134.19 1.45 2 13 3 137.68 1.36 2 -13 4 28.77 0.63 -2 13 -4 27.96 0.47 -2 13 -4 27.09 0.47 2 -13 4 27.23 0.56 2 13 4 28.43 0.54 2 -13 4 27.44 0.56 -2 13 -5 73.28 0.77 2 -13 5 71.97 0.86 2 -13 6 34.74 0.50 -2 13 -7 21.78 0.32 -2 -14 8 1.58 0.10 2 14 -8 1.63 0.12 2 -14 -8 1.74 0.11 2 14 -7 76.17 0.86 -2 -14 7 80.39 0.77 -2 14 7 74.61 0.70 2 14 -7 72.82 0.66 2 14 -7 73.92 0.79 2 -14 -7 81.32 0.92 -2 -14 6 183.12 1.35 -2 -14 6 182.71 1.26 2 14 -6 175.78 1.35 2 14 -6 175.37 1.52 2 -14 -6 181.57 1.67 2 14 -5 3.07 0.21 2 -14 -5 1.98 0.17 -2 -14 5 3.06 0.15 -2 14 5 2.87 0.16 2 -14 -5 2.18 0.18 2 14 -5 3.05 0.23 2 14 -5 2.99 0.19 2 -14 -5 2.56 0.24 2 14 -4 20.26 0.50 2 -14 -4 20.91 0.53 -2 14 4 21.07 0.45 -2 -14 4 19.79 0.33 2 14 -4 20.74 0.41 2 -14 -4 21.33 0.55 2 14 -4 19.22 0.36 2 14 -4 20.28 0.53 2 14 -4 21.40 0.47 2 14 -3 43.59 0.74 -2 14 3 43.67 0.69 2 -14 -3 42.76 0.80 2 14 -3 45.00 0.65 2 -14 -3 45.01 0.84 2 14 -3 42.40 0.58 2 14 -3 44.54 0.78 2 14 -3 44.70 0.71 2 -14 -3 47.33 0.90 2 -14 -2 250.20 2.10 2 14 -2 259.11 2.03 -2 14 2 261.97 1.98 2 -14 -2 259.22 2.26 2 14 -2 261.56 1.91 2 14 -2 246.64 1.91 2 14 -2 255.93 1.77 2 14 -2 266.01 2.08 2 14 -2 261.97 1.99 2 14 -2 252.81 2.15 2 -14 -2 258.15 2.29 -2 14 1 3.17 0.21 2 -14 -1 3.35 0.25 2 14 -1 2.91 0.20 2 14 -1 3.23 0.18 2 -14 -1 3.37 0.27 2 14 -1 3.00 0.22 2 -14 -1 3.56 0.25 2 -14 0 7.60 0.35 -2 14 0 7.83 0.30 -2 14 0 7.80 0.31 2 14 0 7.95 0.33 2 14 0 8.01 0.28 2 14 0 7.48 0.32 2 14 0 7.77 0.32 2 -14 0 8.93 0.35 2 -14 1 16.35 0.50 -2 14 -1 14.38 0.31 -2 14 -1 15.23 0.40 2 -14 1 15.03 0.48 -2 14 -1 16.80 0.43 2 14 1 15.29 0.46 2 14 1 16.21 0.39 2 -14 1 15.40 0.50 2 14 1 15.04 0.41 2 -14 2 0.84 0.17 -2 14 -2 0.90 0.10 2 -14 2 0.16 0.11 -2 14 -2 0.41 0.10 -2 14 -2 0.95 0.12 2 14 2 0.23 0.12 2 -14 2 0.26 0.14 2 14 2 0.65 0.13 2 14 2 0.16 0.10 -2 14 -3 101.99 0.95 2 -14 3 102.78 1.12 -2 14 -3 101.63 0.97 -2 14 -3 98.27 1.01 2 14 3 101.84 1.03 2 -14 3 103.42 1.20 2 14 3 99.17 1.08 2 -14 4 9.11 0.35 -2 14 -4 9.12 0.26 2 14 4 9.62 0.29 -2 14 -4 8.29 0.25 2 14 4 8.80 0.29 2 -14 4 8.56 0.29 2 -14 5 62.05 0.81 -2 14 -5 60.53 0.65 2 14 5 55.30 0.66 2 -14 5 55.66 0.66 2 15 -8 0.41 0.06 -2 -15 8 0.18 0.05 -2 -15 7 88.67 0.75 2 -15 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3 4.10 0.20 3 -3 3 4.66 0.26 3 3 3 4.60 0.22 3 -3 4 95.15 0.93 3 -3 4 96.49 1.07 3 3 4 94.26 1.05 3 3 4 93.84 0.95 3 3 5 115.60 0.99 3 -3 5 117.57 1.26 3 3 6 0.29 0.09 3 4 -10 28.20 0.37 3 4 -10 24.95 0.32 3 -4 -9 1.46 0.14 3 4 -9 1.04 0.08 3 4 -8 0.10 0.08 3 -4 -8 0.11 0.09 3 4 -8 0.28 0.08 3 4 -7 5.02 0.24 3 -4 -7 4.66 0.27 3 -4 -7 4.66 0.26 3 4 -7 4.65 0.24 3 4 -6 0.24 0.10 3 4 -6 0.19 0.07 3 -4 -6 0.19 0.08 3 -4 -6 0.38 0.14 3 4 -6 0.19 0.11 3 4 -5 15.96 0.37 3 -4 -5 15.38 0.95 3 -4 -5 14.36 0.80 3 -4 -5 16.20 1.02 3 4 -5 14.49 0.84 3 4 -5 16.00 0.44 3 -4 -4 15.62 0.43 3 4 -4 14.82 0.38 3 -4 -4 15.03 0.94 3 -4 -4 14.79 0.41 3 -4 -4 14.34 0.93 3 -4 -4 14.29 0.49 3 4 -4 13.44 0.77 3 -4 -4 13.56 0.82 3 -4 -4 14.55 0.48 3 4 -4 14.38 0.74 3 4 -4 15.02 0.44 3 4 -3 1.07 0.11 3 -4 -3 1.01 0.28 3 4 -3 0.75 0.22 3 -4 -3 1.15 0.31 3 -4 -3 0.90 0.14 3 4 -3 0.75 0.12 3 -4 -3 0.71 0.23 3 4 -3 0.73 0.12 3 -4 -3 0.69 0.14 3 -4 -3 1.21 0.16 3 4 -3 0.79 0.14 3 4 -2 9.19 0.28 3 -4 -2 8.46 0.68 3 -4 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0.23 0.04 -3 -5 9 35.44 0.42 3 -5 -9 34.01 0.49 3 5 -8 2.42 0.16 3 5 -8 2.43 0.14 3 -5 -8 2.25 0.17 3 5 -7 28.06 0.52 3 -5 -7 28.97 0.64 3 -5 -7 30.01 0.63 3 5 -7 27.25 0.51 3 5 -6 4.71 0.18 3 5 -6 4.30 0.21 3 -5 -6 5.26 0.23 3 -5 -6 4.60 0.21 3 -5 -6 5.13 0.30 3 5 -6 4.94 0.24 3 5 -5 0.82 0.10 3 -5 -5 0.40 0.11 3 -5 -5 0.76 0.22 3 5 -5 0.38 0.19 3 -5 -5 0.28 0.14 3 -5 -5 0.37 0.18 3 5 -5 0.34 0.11 3 -5 -4 0.35 0.23 3 -5 -4 0.60 0.13 3 -5 -4 0.35 0.11 3 -5 -4 0.31 0.22 3 5 -4 0.38 0.19 3 -5 -4 0.41 0.16 3 5 -4 0.35 0.10 3 -5 -4 0.52 0.15 3 5 -4 0.38 0.12 3 5 -3 0.33 0.07 3 -5 -3 0.47 0.23 3 -5 -3 0.40 0.24 3 -5 -3 0.34 0.13 3 -5 -3 0.30 0.11 3 -5 -3 0.34 0.21 3 5 -3 0.30 0.10 3 5 -3 0.27 0.10 3 -5 -3 0.38 0.14 3 -5 -3 0.30 0.11 3 5 -3 0.36 0.12 3 -5 -2 46.17 0.80 3 5 -2 44.64 0.69 3 -5 -2 42.95 1.50 3 -5 -2 44.85 0.80 3 -5 -2 44.83 0.85 3 5 -2 44.53 0.68 3 -5 -2 42.53 0.78 3 -5 -2 42.24 1.54 3 5 -2 41.43 1.32 3 -5 -2 44.30 0.72 3 5 -2 45.19 0.76 3 5 -2 45.39 0.62 3 -5 -1 71.35 1.04 3 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3 6 -6 11.02 0.33 3 6 -5 4.56 0.20 3 -6 -5 4.98 0.25 3 -6 -5 4.78 0.29 3 6 -5 4.98 0.25 3 6 -5 4.35 0.22 3 6 -4 93.81 0.98 3 -6 -4 93.73 1.16 3 -6 -4 89.29 2.26 3 -6 -4 90.77 1.04 3 -6 -4 87.31 2.37 3 -6 -4 97.58 1.30 3 6 -4 80.54 1.87 3 -6 -4 85.17 2.11 3 -6 -4 92.42 1.26 3 6 -4 91.75 1.07 3 6 -3 151.84 1.33 3 -6 -3 154.80 1.56 3 -6 -3 146.32 2.86 3 -6 -3 153.12 1.50 3 -6 -3 136.80 2.93 3 -6 -3 151.20 1.62 3 -6 -3 138.14 2.82 3 -6 -3 151.77 1.44 3 6 -3 146.16 1.43 3 6 -2 77.76 0.92 3 -6 -2 78.16 1.08 3 -6 -2 79.10 1.07 3 -6 -2 76.17 1.16 3 6 -2 77.02 0.91 3 -6 -2 75.38 1.06 3 -6 -2 75.57 0.94 3 -6 -2 78.37 2.14 3 6 -2 76.25 0.81 3 6 -1 0.84 0.11 3 -6 -1 1.10 0.16 3 6 -1 0.80 0.12 3 6 -1 0.87 0.13 3 -6 -1 0.88 0.13 3 -6 -1 0.91 0.12 3 6 -1 0.84 0.11 3 6 0 4.19 0.21 3 -6 0 4.29 0.27 3 6 0 4.86 0.22 3 -6 0 4.12 0.27 3 6 0 3.80 0.20 3 6 0 4.12 0.31 3 6 0 3.50 0.17 3 -6 0 4.24 0.51 3 6 0 3.91 0.20 3 6 1 184.32 1.48 3 -6 1 190.24 1.68 3 6 1 184.05 1.43 3 -6 1 189.40 1.74 3 6 1 187.77 1.46 3 6 1 174.84 1.48 3 -6 1 172.31 3.12 3 6 1 189.06 1.50 3 -6 2 0.93 0.15 3 6 2 0.80 0.10 3 -6 2 1.40 0.20 3 -6 2 0.91 0.13 3 6 2 1.05 0.12 3 6 2 0.49 0.10 3 6 2 0.78 0.13 3 -6 3 1.75 0.14 3 -6 3 1.74 0.19 3 6 3 1.76 0.13 3 6 3 2.07 0.19 3 -6 3 1.74 0.19 3 -6 4 301.92 1.87 3 -6 4 299.04 2.22 3 6 4 303.74 2.13 3 6 4 304.74 1.99 3 -6 4 306.62 2.34 3 -6 5 0.81 0.11 3 6 5 1.08 0.11 3 -6 5 0.87 0.14 3 -6 6 34.11 0.56 3 7 -9 19.73 0.31 3 -7 -9 18.80 0.38 -3 -7 9 20.13 0.29 3 7 -9 18.29 0.28 3 -7 -9 18.48 0.32 3 -7 -8 15.30 0.42 3 7 -8 14.41 0.27 3 -7 -8 15.16 0.38 3 7 -8 14.39 0.30 3 7 -7 33.37 0.50 3 7 -7 33.69 0.53 3 -7 -7 33.13 0.65 3 -7 -6 13.28 0.36 3 7 -6 13.72 0.35 3 7 -6 13.59 0.36 3 -7 -6 13.66 0.46 3 7 -6 12.55 0.32 3 7 -5 16.61 0.36 3 -7 -5 16.11 0.45 3 -7 -5 17.20 0.52 3 7 -5 17.65 0.42 3 7 -5 16.88 0.41 3 7 -5 16.15 0.40 3 7 -4 292.86 2.01 3 -7 -4 283.19 4.08 3 -7 -4 288.30 2.08 3 -7 -4 282.85 4.45 3 -7 -4 298.06 2.50 3 7 -4 302.26 2.11 3 7 -4 300.02 2.11 3 -7 -4 296.96 2.46 3 -7 -4 299.39 2.18 3 7 -4 291.84 2.12 3 7 -3 40.94 0.64 3 -7 -3 40.91 0.72 3 -7 -3 41.31 0.80 3 -7 -3 39.76 0.66 3 -7 -2 2.07 0.39 3 7 -2 2.45 0.18 3 -7 -2 2.29 0.22 3 -7 -2 2.41 0.38 3 -7 -2 2.37 0.21 3 -7 -2 2.92 0.25 3 7 -2 2.36 0.18 3 7 -2 2.26 0.17 3 -7 -2 2.62 0.22 3 7 -2 2.24 0.14 3 -7 -2 2.21 0.16 3 -7 -1 54.64 0.90 3 -7 -1 53.47 0.95 3 7 -1 52.92 0.74 3 7 -1 54.20 0.75 3 7 -1 55.84 0.87 3 -7 -1 51.22 0.80 3 7 -1 53.47 0.68 3 7 -1 51.63 0.72 3 7 0 11.17 0.33 3 -7 0 11.35 0.40 3 -7 0 11.17 0.41 3 7 0 10.98 0.32 3 -7 0 11.44 0.43 3 7 0 10.65 0.32 3 7 0 10.29 0.42 3 7 0 10.29 0.29 3 7 0 10.87 0.31 3 -7 0 10.48 0.79 3 7 1 126.76 1.16 3 -7 1 125.86 1.31 3 -7 1 128.41 1.46 3 7 1 122.24 1.12 3 -7 1 126.77 1.40 3 7 1 124.90 1.16 3 7 1 123.90 1.23 3 7 1 126.79 1.16 3 7 2 1003.36 5.10 3 -7 2 1017.52 5.33 3 7 2 991.64 5.04 3 -7 2 1010.04 5.38 3 7 2 1023.28 5.14 3 7 2 1009.45 5.41 3 7 2 1014.11 5.16 3 -7 3 41.03 0.59 3 -7 3 42.89 0.78 3 7 3 41.63 0.58 3 7 3 41.09 0.61 3 -7 3 41.61 0.77 3 -7 4 25.36 0.54 3 7 4 23.64 0.48 3 7 4 25.56 0.46 3 -7 4 24.44 0.57 3 -7 5 2.29 0.15 3 -8 -9 24.13 0.40 3 -8 -9 23.58 0.33 3 8 -9 22.81 0.31 3 -8 -8 44.26 0.69 -3 -8 8 43.26 0.49 3 8 -8 44.15 0.51 3 8 -7 2.10 0.13 3 8 -7 1.98 0.14 3 -8 -7 1.72 0.17 3 -8 -6 2.06 0.16 3 8 -6 2.15 0.15 3 8 -6 2.11 0.16 3 -8 -6 1.79 0.19 3 -8 -5 60.51 0.98 3 8 -5 59.65 0.76 3 8 -5 58.01 0.77 3 8 -4 0.86 0.13 3 -8 -4 0.80 0.12 3 -8 -4 1.44 0.21 3 8 -4 0.94 0.15 3 8 -4 1.11 0.15 3 -8 -4 1.27 0.19 3 -8 -4 0.81 0.13 3 8 -3 5.31 0.23 3 -8 -3 5.32 0.26 3 -8 -3 5.64 0.33 3 8 -3 4.76 0.23 3 8 -3 4.92 0.24 3 -8 -3 5.34 0.30 3 -8 -3 4.73 0.22 3 -8 -3 4.44 0.52 3 -8 -2 81.88 2.23 3 8 -2 87.19 0.97 3 -8 -2 88.41 1.17 3 -8 -2 88.23 1.12 3 -8 -2 87.12 1.25 3 -8 -2 82.51 1.11 3 8 -2 93.05 1.22 3 8 -2 85.04 0.82 3 8 -2 87.07 0.99 3 8 -1 0.36 0.10 3 8 -1 0.34 0.09 3 -8 -1 0.39 0.14 3 8 -1 0.45 0.12 3 8 -1 0.35 0.11 3 -8 -1 0.30 0.15 3 -8 -1 0.20 0.10 3 8 0 83.56 0.94 3 -8 0 87.30 1.12 3 -8 0 85.95 1.16 3 8 0 85.20 0.93 3 -8 0 86.32 1.20 3 8 0 84.31 0.94 3 8 0 85.80 1.08 3 8 0 82.12 0.88 3 8 0 85.40 0.88 3 8 1 190.16 1.49 3 -8 1 193.13 1.68 3 8 1 188.51 1.48 3 -8 1 190.45 1.84 3 8 1 192.93 1.50 3 8 1 186.90 1.62 3 8 1 193.03 1.62 3 8 1 192.22 1.48 3 -8 2 53.65 0.75 3 8 2 53.80 0.70 3 -8 2 53.26 0.79 3 8 2 54.71 0.79 3 -8 3 94.83 1.17 3 8 3 93.79 0.91 3 8 3 93.35 1.03 3 8 3 95.72 0.96 3 -8 4 95.71 1.08 3 -8 5 5.63 0.22 -3 8 -6 39.65 0.44 3 -9 -8 64.50 0.80 -3 -9 8 64.90 0.59 3 9 -8 63.68 0.57 3 9 -8 63.49 0.64 3 9 -7 70.31 0.68 3 -9 -7 70.66 0.91 3 -9 -6 1.34 0.13 3 -9 -6 1.22 0.17 3 -9 -5 2.75 0.23 3 9 -5 2.72 0.17 3 -9 -5 2.41 0.16 3 -9 -4 32.18 0.52 3 -9 -4 34.95 0.75 3 9 -4 35.31 0.59 3 9 -4 35.96 0.59 3 9 -4 35.30 0.74 3 -9 -4 33.95 0.73 3 -9 -4 33.09 0.55 3 9 -3 0.40 0.11 3 -9 -3 0.08 0.09 3 9 -3 0.20 0.10 3 9 -3 0.12 0.10 3 -9 -3 0.23 0.11 3 9 -2 168.35 1.42 3 -9 -2 166.66 1.58 3 9 -2 169.26 1.71 3 -9 -2 159.83 1.60 3 9 -2 158.89 1.20 3 9 -2 160.64 1.42 3 -9 -1 110.41 1.29 3 9 -1 108.93 1.09 3 -9 -1 110.80 1.41 3 9 -1 117.42 1.30 3 -9 -1 104.36 1.16 3 9 -1 100.43 0.95 3 9 -1 105.80 1.06 3 -9 0 32.40 0.68 3 9 0 30.84 0.54 3 -9 0 31.04 0.70 3 9 0 31.62 0.54 3 9 0 29.63 0.57 3 9 0 34.00 0.68 3 9 0 29.83 0.51 3 9 0 33.27 0.52 3 -9 1 70.65 0.93 3 9 1 72.77 0.83 3 -9 1 72.09 1.05 3 -9 1 72.71 1.03 3 9 1 72.62 0.84 3 9 1 70.65 0.88 3 9 1 72.50 0.94 3 9 1 73.93 0.82 3 -9 2 220.56 1.67 3 9 2 224.73 1.64 3 -9 2 216.75 1.79 3 9 2 230.70 1.74 3 9 2 228.58 1.71 3 9 2 229.28 1.66 3 9 3 79.09 0.82 3 9 3 78.32 0.88 3 9 3 80.56 0.85 3 -9 4 0.82 0.13 3 9 4 0.45 0.08 3 -9 5 73.98 0.78 3 -9 5 75.97 0.87 -3 9 -6 0.79 0.07 3 -10 -8 14.26 0.33 -3 -10 8 13.90 0.23 3 -10 -8 13.46 0.29 3 10 -8 13.30 0.25 -3 -10 7 0.47 0.07 3 10 -7 0.29 0.06 3 10 -7 0.40 0.07 3 -10 -7 0.40 0.11 3 10 -7 0.42 0.09 3 -10 -7 0.23 0.06 3 -10 -6 1.54 0.14 3 10 -6 1.47 0.11 3 10 -6 1.54 0.12 3 -10 -6 1.39 0.16 3 -10 -6 1.35 0.11 3 10 -6 1.61 0.14 3 10 -5 0.32 0.09 3 -10 -5 0.22 0.12 3 10 -5 0.31 0.09 3 -10 -5 0.46 0.14 3 10 -4 1.03 0.13 3 -10 -4 0.97 0.16 3 10 -4 1.06 0.13 3 10 -4 0.94 0.17 3 -10 -4 0.87 0.15 3 10 -4 0.86 0.13 3 -10 -3 5.54 0.24 3 10 -3 6.07 0.25 3 -10 -3 6.27 0.34 3 10 -3 5.73 0.24 3 10 -3 5.80 0.32 3 -10 -3 5.63 0.29 3 10 -3 5.84 0.25 3 -10 -2 52.78 0.81 3 10 -2 53.87 0.73 3 10 -2 54.81 0.91 3 -10 -2 51.30 0.83 3 10 -2 52.57 0.73 3 -10 -1 0.69 0.14 3 -10 -1 0.55 0.13 3 10 -1 0.63 0.11 3 10 -1 0.64 0.11 3 -10 -1 0.68 0.16 3 10 -1 0.65 0.09 3 10 -1 0.74 0.11 3 -10 -1 0.52 0.11 3 10 0 72.81 0.84 3 -10 0 71.37 1.00 3 -10 0 72.43 1.08 3 10 0 71.16 0.83 3 10 0 69.80 0.84 3 10 0 66.01 0.78 3 10 0 76.22 1.00 3 10 0 72.21 0.79 3 -10 1 164.89 1.46 3 10 1 166.68 1.35 3 -10 1 163.65 1.61 3 10 1 170.58 1.37 3 -10 1 158.15 1.59 3 10 1 159.17 1.36 3 10 1 174.14 1.51 3 10 1 160.78 1.31 3 -10 2 2.84 0.16 3 10 2 2.96 0.17 3 10 2 3.00 0.18 3 10 2 3.28 0.25 3 10 2 3.11 0.18 3 10 3 67.32 0.73 3 10 3 65.99 0.75 3 -10 3 65.28 0.90 3 -10 4 47.75 0.68 3 -10 4 47.54 0.71 -3 10 -5 35.44 0.43 3 -10 5 34.83 0.48 3 -10 5 34.12 0.52 -3 10 -6 66.01 0.52 3 -11 -8 10.57 0.23 3 11 -8 11.53 0.20 3 -11 -7 1.72 0.10 -3 -11 7 2.21 0.10 3 11 -7 1.65 0.08 3 11 -7 2.00 0.10 3 -11 -7 1.85 0.14 3 11 -7 2.01 0.12 3 -11 -6 35.75 0.54 -3 -11 6 36.51 0.44 3 11 -6 36.64 0.46 3 11 -6 36.74 0.47 3 11 -6 36.56 0.53 3 11 -5 0.77 0.10 3 11 -5 0.83 0.10 3 11 -5 0.69 0.11 3 11 -4 15.57 0.36 3 -11 -4 15.74 0.47 3 11 -4 15.70 0.35 3 11 -4 15.69 0.47 3 -11 -4 14.58 0.45 3 -11 -3 9.51 0.28 3 11 -3 10.88 0.31 3 -11 -3 10.67 0.42 3 11 -3 13.16 0.33 3 11 -3 10.62 0.40 3 -11 -3 9.08 0.35 3 11 -3 14.14 0.37 3 -11 -2 9.03 0.31 3 11 -2 9.18 0.29 3 11 -2 9.12 0.37 3 -11 -2 8.69 0.33 3 11 -2 8.92 0.29 3 -11 -1 14.22 0.42 3 -11 -1 13.81 0.40 3 11 -1 13.60 0.36 3 -11 -1 14.36 0.48 3 11 -1 14.11 0.35 3 11 -1 13.10 0.31 3 11 -1 14.37 0.50 3 11 -1 13.22 0.35 3 -11 0 1.53 0.16 3 11 0 2.05 0.16 3 -11 0 1.56 0.17 3 -11 0 1.64 0.19 3 11 0 1.31 0.12 3 11 0 1.78 0.29 3 -11 1 0.73 0.11 3 -11 1 0.78 0.14 3 11 1 0.69 0.11 3 -11 1 1.04 0.15 3 11 1 0.89 0.11 3 11 1 0.73 0.23 3 -11 2 4.84 0.19 3 -11 2 4.64 0.25 3 11 2 5.27 0.21 3 11 2 4.70 0.19 3 11 2 5.25 0.28 3 11 3 19.35 0.36 3 -11 3 19.64 0.46 3 -11 4 37.62 0.56 3 -11 4 37.72 0.58 3 -11 5 0.52 0.07 3 -11 5 0.20 0.07 -3 -12 7 82.93 0.61 3 -12 -7 81.64 0.80 3 12 -7 80.97 0.68 3 -12 -6 29.25 0.45 -3 -12 6 29.19 0.35 3 12 -6 29.25 0.37 3 12 -6 30.55 0.37 3 12 -6 30.54 0.44 -3 -12 5 19.16 0.29 3 12 -5 20.05 0.35 3 -12 -5 20.55 0.47 3 12 -5 19.89 0.34 3 -12 -5 18.81 0.45 3 12 -5 20.15 0.39 -3 -12 4 1.24 0.08 3 12 -4 1.56 0.13 3 -12 -4 1.43 0.16 3 12 -4 1.44 0.12 3 12 -4 1.37 0.17 3 -12 -4 1.51 0.16 3 12 -3 75.18 0.82 3 -12 -3 73.96 1.03 3 12 -3 71.95 0.77 3 12 -3 73.73 1.00 3 12 -3 72.18 0.83 3 -12 -2 0.64 0.10 3 12 -2 0.77 0.12 3 12 -2 0.77 0.11 3 12 -2 0.74 0.11 3 12 -2 0.70 0.14 3 -12 -2 0.79 0.12 3 -12 -1 6.52 0.28 3 -12 -1 6.28 0.26 3 -12 -1 6.27 0.31 3 12 -1 5.90 0.22 3 12 -1 5.79 0.22 3 12 -1 6.99 0.39 3 -12 0 1.40 0.15 3 -12 0 1.15 0.14 3 -12 0 1.13 0.16 3 -12 1 49.16 0.65 3 -12 1 51.20 0.75 3 -12 1 50.94 0.77 3 -12 2 7.88 0.29 3 12 2 8.48 0.25 3 12 2 8.11 0.30 -3 12 -3 240.45 1.46 3 12 3 242.53 1.54 3 -12 3 238.62 1.74 -3 12 -4 5.72 0.16 3 -12 4 5.52 0.20 -3 12 -5 3.43 0.10 3 -12 5 3.37 0.12 3 13 -7 11.48 0.19 3 -13 -7 9.97 0.22 3 -13 -6 4.63 0.16 3 13 -6 4.30 0.11 3 13 -6 4.88 0.17 3 -13 -5 21.54 0.41 3 13 -5 22.08 0.34 3 -13 -5 22.25 0.43 3 13 -5 22.00 0.32 3 13 -5 22.61 0.39 3 -13 -5 21.63 0.45 3 13 -4 18.14 0.34 3 -13 -4 18.46 0.44 3 13 -4 17.59 0.32 3 -13 -4 18.13 0.42 3 13 -3 4.41 0.19 3 -13 -3 4.07 0.24 3 13 -3 4.41 0.18 3 13 -3 4.61 0.20 3 13 -3 4.07 0.23 3 -13 -3 3.79 0.20 3 13 -2 11.57 0.30 3 13 -2 10.93 0.28 3 13 -2 11.01 0.29 3 13 -2 10.43 0.34 3 -13 -1 15.98 0.39 3 -13 -1 15.44 0.36 3 13 -1 16.43 0.34 3 -13 -1 16.48 0.46 3 -13 0 126.78 1.14 3 -13 0 127.47 1.16 3 13 0 133.03 1.08 3 -13 0 128.46 1.30 3 13 0 132.50 1.22 -3 13 -1 6.15 0.21 3 -13 1 6.20 0.24 3 -13 1 6.03 0.25 3 13 1 6.49 0.31 3 -13 2 11.64 0.31 3 13 2 11.89 0.27 3 -13 2 11.43 0.32 -3 13 -3 16.50 0.26 3 -13 3 16.36 0.34 3 13 3 17.17 0.30 3 -13 3 16.29 0.35 -3 13 -4 14.26 0.21 3 -13 4 15.40 0.28 3 -14 -6 112.02 0.77 3 -14 -5 51.82 0.58 3 14 -5 51.25 0.44 -3 14 4 65.45 0.66 3 -14 -4 69.04 0.76 3 -14 -4 76.33 0.83 3 14 -4 73.30 0.62 3 -14 -4 67.83 0.76 -3 14 3 50.15 0.60 3 -14 -3 50.86 0.72 3 14 -3 51.25 0.55 3 -14 -2 1.14 0.12 3 14 -2 1.38 0.11 3 -14 -2 1.36 0.15 -3 14 1 18.48 0.37 3 -14 -1 18.09 0.33 3 -14 -1 18.91 0.45 3 -14 0 104.27 0.92 -3 14 0 113.81 0.96 3 -14 0 109.39 0.95 3 14 0 113.25 0.92 3 -14 0 109.44 1.10 3 14 0 107.42 1.01 -3 14 -1 47.79 0.55 3 -14 1 50.07 0.60 3 14 1 52.58 0.57 3 -14 1 49.37 0.64 3 14 1 50.62 0.62 -3 14 -2 1.08 0.07 3 -14 2 1.09 0.10 3 -14 2 1.22 0.11 3 -14 3 7.72 0.20 3 -14 3 8.31 0.21 3 -15 -5 24.40 0.34 3 -15 -4 76.07 0.69 -3 15 4 67.82 0.60 3 15 -4 72.53 0.53 3 -15 -4 71.29 0.67 -3 15 3 9.41 0.22 3 15 -3 9.11 0.19 3 15 -2 24.03 0.33 3 -15 -2 22.55 0.44 -3 15 1 8.19 0.22 3 15 -1 8.55 0.20 -3 15 0 25.44 0.37 3 15 0 25.30 0.35 -3 15 -1 34.12 0.41 3 -15 1 35.83 0.42 3 15 1 40.06 0.44 3 -15 1 35.14 0.46 3 -15 1 38.66 0.49 3 -15 2 45.81 0.47 3 -15 2 51.29 0.51 -3 16 3 115.45 0.79 3 -16 -3 123.81 0.91 3 -16 -2 0.12 0.04 3 16 -2 0.18 0.04 3 -16 -2 0.14 0.06 -3 16 1 1.78 0.10 3 16 -1 1.87 0.08 -3 16 0 17.19 0.26 3 16 0 17.11 0.24 3 -16 0 17.43 0.28 4 0 -7 0.03 0.05 4 0 -6 32.87 0.51 4 0 -5 0.04 0.05 4 0 -5 0.05 0.09 4 0 -4 10.61 0.27 4 0 -4 9.75 0.21 4 0 -3 0.19 0.07 4 0 -3 0.39 0.08 4 0 -2 149.90 1.17 4 0 -2 149.82 1.25 4 0 -1 0.07 0.07 4 0 0 17.00 0.35 4 0 0 17.34 0.35 4 0 1 0.02 0.06 4 0 1 0.01 0.07 4 0 1 0.02 0.05 4 0 2 14.22 0.28 4 0 2 14.32 0.28 4 0 3 0.10 0.05 4 1 -7 30.39 0.38 4 -1 -7 32.63 0.44 4 1 -6 0.38 0.08 4 -1 -6 0.44 0.10 4 1 -5 3.34 0.14 4 -1 -5 3.33 0.14 4 -1 -5 3.41 0.19 4 1 -4 89.98 0.83 4 -1 -4 91.78 0.86 4 -1 -3 58.00 0.64 4 1 -3 58.83 0.68 4 1 -3 54.30 0.62 4 1 -3 55.65 0.59 4 -1 -2 52.44 0.64 4 1 -2 54.12 0.67 4 -1 -2 54.44 0.70 4 1 -2 51.68 0.60 4 -1 -1 7.84 0.25 4 1 -1 7.65 0.23 4 -1 0 3.39 0.17 4 1 0 3.34 0.16 4 -1 0 3.47 0.17 4 1 0 3.66 0.17 4 1 1 1.65 0.11 4 -1 1 1.42 0.10 4 1 1 1.54 0.13 4 -1 1 1.89 0.12 4 1 1 1.52 0.11 4 1 2 47.52 0.54 4 -1 2 49.07 0.53 4 1 3 68.08 0.57 4 -1 3 67.16 0.56 4 2 -7 2.86 0.12 4 -2 -7 2.60 0.13 4 -2 -6 137.60 1.14 4 2 -5 8.68 0.21 4 -2 -5 7.64 0.21 4 2 -5 8.38 0.23 4 2 -5 8.35 0.22 4 -2 -5 8.09 0.27 4 -2 -4 0.40 0.07 4 2 -4 0.47 0.09 4 2 -4 0.54 0.08 4 2 -4 0.44 0.09 4 -2 -4 0.47 0.09 4 -2 -3 9.97 0.26 4 2 -3 9.90 0.27 4 -2 -3 10.66 0.30 4 2 -3 9.81 0.25 4 2 -3 9.56 0.22 4 -2 -2 22.12 0.41 4 2 -2 22.51 0.41 4 2 -2 22.98 0.37 4 -2 -1 7.63 0.24 4 2 -1 7.96 0.23 4 -2 0 1.61 0.13 4 2 0 1.60 0.12 4 -2 0 1.84 0.13 4 2 0 1.58 0.12 4 2 1 24.13 0.36 4 -2 1 24.61 0.38 4 2 1 24.11 0.42 4 2 1 24.94 0.39 4 2 2 0.40 0.08 4 -2 2 0.48 0.07 4 2 3 0.08 0.05 4 -2 3 0.04 0.04 4 2 3 0.14 0.05 4 3 -7 6.64 0.16 4 3 -7 6.46 0.16 4 -3 -7 6.55 0.19 4 3 -6 5.47 0.17 4 -3 -6 5.28 0.20 4 3 -5 16.23 0.28 4 -3 -5 16.19 0.29 4 3 -5 16.53 0.31 4 -3 -5 16.43 0.36 4 3 -4 15.29 0.30 4 -3 -4 15.44 0.33 4 3 -4 15.52 0.32 4 3 -4 14.60 0.29 4 -3 -3 1.14 0.11 4 3 -3 1.27 0.11 4 -3 -3 1.00 0.12 4 3 -3 1.05 0.10 4 3 -3 1.04 0.09 4 3 -3 0.97 0.08 4 -3 -2 3.03 0.16 4 3 -2 3.29 0.16 4 -3 -2 3.36 0.19 4 3 -2 2.68 0.13 4 3 -2 3.03 0.13 4 -3 -1 1.10 0.11 4 3 -1 0.16 0.07 4 -3 0 14.04 0.32 4 3 0 13.55 0.29 4 -3 0 13.91 0.33 4 3 0 13.59 0.29 4 3 1 27.81 0.38 4 -3 1 28.08 0.41 4 3 1 27.26 0.45 4 3 2 50.67 0.57 4 3 2 50.08 0.52 4 -3 2 50.78 0.53 4 3 3 64.90 0.57 4 -3 3 63.42 0.51 4 4 -7 8.50 0.17 4 4 -7 8.12 0.17 4 -4 -7 8.37 0.19 4 4 -6 2.50 0.12 4 4 -6 2.88 0.12 4 -4 -6 2.52 0.13 4 4 -5 0.06 0.06 4 -4 -5 0.16 0.06 4 -4 -5 0.07 0.07 4 -4 -5 0.04 0.07 4 -4 -4 0.16 0.06 4 4 -4 0.03 0.07 4 4 -4 0.03 0.06 4 4 -4 0.06 0.06 4 -4 -4 0.08 0.07 4 -4 -3 0.25 0.07 4 4 -3 0.13 0.07 4 4 -3 0.04 0.06 4 4 -3 0.06 0.06 4 4 -2 5.94 0.20 4 4 -2 5.55 0.18 4 -4 -2 6.08 0.24 4 4 -2 5.76 0.17 4 -4 -1 4.17 0.19 4 4 -1 3.97 0.15 4 -4 0 22.69 0.40 4 4 0 22.55 0.37 4 -4 0 23.09 0.42 4 4 0 22.19 0.43 4 4 0 23.28 0.37 4 -4 1 29.97 0.43 4 4 1 29.01 0.38 4 -4 1 30.31 0.47 4 -4 1 29.22 0.42 4 4 1 28.40 0.45 4 4 1 29.76 0.40 4 4 2 5.07 0.17 4 4 2 5.06 0.16 4 -4 2 5.19 0.16 4 5 -7 0.45 0.05 4 5 -7 0.38 0.05 4 5 -6 24.95 0.34 4 5 -6 24.30 0.33 4 -5 -6 22.76 0.34 4 5 -6 23.23 0.33 4 -5 -5 31.86 0.35 4 -5 -5 34.58 0.42 4 5 -5 35.99 0.44 4 -5 -5 37.69 0.52 4 -5 -5 33.71 0.46 4 5 -5 35.42 0.43 4 5 -4 34.63 0.44 4 -5 -4 32.50 0.44 4 -5 -4 35.43 0.50 4 5 -4 33.42 0.45 4 5 -4 32.77 0.43 4 -5 -4 32.68 0.49 4 5 -3 1.28 0.10 4 -5 -3 1.24 0.11 4 5 -3 1.15 0.10 4 5 -3 1.21 0.10 4 -5 -2 0.59 0.09 4 5 -2 0.60 0.09 4 5 -2 0.64 0.08 4 -5 -2 0.64 0.10 4 5 -2 0.51 0.07 4 5 -2 0.63 0.07 4 -5 -1 53.53 0.64 4 5 -1 53.63 0.61 4 5 -1 53.13 0.54 4 5 0 45.22 0.52 4 -5 0 45.45 0.59 4 5 0 44.61 0.50 4 -5 1 40.34 0.49 4 -5 1 39.36 0.54 4 5 1 40.34 0.53 4 5 1 41.18 0.47 4 5 2 58.02 0.58 4 5 2 60.09 0.56 4 -6 -6 53.55 0.57 4 6 -6 52.56 0.50 4 -6 -5 6.18 0.15 4 -6 -5 6.56 0.17 4 -6 -4 1.79 0.11 4 -6 -4 1.96 0.12 4 6 -4 2.08 0.12 4 6 -4 1.81 0.11 4 -6 -3 12.35 0.29 4 6 -3 12.48 0.27 4 -6 -3 13.18 0.31 4 6 -3 12.09 0.25 4 6 -2 8.08 0.22 4 -6 -2 7.30 0.23 4 6 -2 7.38 0.20 4 6 -2 6.71 0.19 4 -6 -2 8.04 0.26 4 6 -2 7.19 0.16 4 6 -1 88.04 0.78 4 -6 -1 87.20 0.83 4 -6 -1 87.46 0.87 4 6 -1 85.10 0.84 4 -6 0 195.94 1.43 4 -6 0 195.87 1.38 4 6 0 196.97 1.24 4 -6 1 52.39 0.54 4 -6 1 53.12 0.61 4 6 1 53.66 0.53 4 -6 2 64.50 0.60 4 6 2 64.31 0.60 4 7 -6 15.36 0.23 4 7 -6 13.08 0.21 4 -7 -5 7.67 0.15 4 -7 -5 7.56 0.16 4 7 -5 9.17 0.20 4 7 -5 9.80 0.20 4 7 -5 9.09 0.19 4 7 -4 34.95 0.43 4 -7 -4 34.17 0.45 4 7 -4 34.70 0.42 4 -7 -3 11.02 0.26 4 7 -3 10.48 0.23 4 -7 -3 10.71 0.27 4 7 -3 10.23 0.23 4 -7 -2 54.99 0.62 4 7 -2 52.67 0.54 4 7 -2 51.56 0.59 4 -7 -2 54.55 0.65 4 -7 -1 20.08 0.36 4 -7 -1 19.46 0.37 4 7 -1 18.94 0.34 4 -7 0 128.99 0.98 4 7 0 130.11 1.00 4 7 0 128.62 0.89 4 -7 1 3.04 0.12 4 7 1 3.03 0.13 4 7 1 3.16 0.12 4 -7 2 69.20 0.60 4 -8 -5 5.22 0.15 4 8 -5 5.63 0.14 4 -8 -4 1.18 0.08 4 -8 -4 0.97 0.08 4 8 -4 1.20 0.08 4 -8 -3 40.27 0.49 4 8 -3 40.26 0.45 4 -8 -3 40.79 0.51 4 -8 -2 23.87 0.38 4 8 -2 23.37 0.33 4 8 -2 22.70 0.32 4 -8 -2 23.13 0.39 4 8 -1 0.24 0.05 4 8 -1 0.15 0.06 4 -8 0 403.71 2.23 4 8 0 402.95 2.19 4 -8 1 6.96 0.16 4 8 1 7.10 0.17 4 9 -5 0.13 0.04 4 -9 -4 78.28 0.60 4 9 -4 82.16 0.61 4 -9 -3 9.51 0.21 4 9 -3 9.00 0.19 4 9 -3 9.61 0.19 4 -9 -3 8.80 0.21 4 -9 -2 7.76 0.20 4 9 -2 7.90 0.18 4 -9 -2 8.22 0.21 4 9 -1 146.04 0.92 4 -9 -1 147.57 1.04 4 -9 0 9.68 0.19 4 -9 0 9.84 0.21 4 -9 0 9.24 0.20 4 9 0 8.95 0.18 4 -9 1 17.69 0.26 4 -10 -3 1.94 0.09 4 10 -3 1.81 0.08 4 -10 -3 1.71 0.08 4 10 -2 17.96 0.24 4 -10 -2 17.85 0.28 4 10 -1 4.48 0.11 4 -10 -1 4.64 0.14 0 0 0 0.00 0.00 _chemical_formula_moiety 'C5 H5 N3 O2, 0.59(H2 O)' _exptl_crystal_description prism _exptl_crystal_colour orange _cell_measurement_reflns_used 6388 _cell_measurement_theta_min 2.4150 _cell_measurement_theta_max 76.5090 _exptl_absorpt_correction_T_min 0.418 _exptl_absorpt_correction_T_max 1.000 _exptl_absorpt_correction_type gaussian _exptl_absorpt_process_details ) CrysAlisPro 1.171.40.84a (Rigaku Oxford Diffraction, 2020). Numerical absorption correction based on gaussian integration over a multifaceted crystal model. Empirical absorption correction using spherical harmonics, frame scaling and detector area scaling, implemented in SCALE3 ABSPACK scaling algorithm. ) loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist 0 9 4 0.0806 2 -5 3 0.1689 0 -11 1 0.0634 0 11 -1 0.0654 -2 -4 3 0.1584 0 -11 0 0.0634 2 0 -5 0.1528 0 -10 3 0.0667 2 -3 -1 0.1799 1 10 -1 0.1068 0 -4 6 0.0716 -2 6 3 0.1483 -2 0 4 0.1547 0 11 -1 0.0613 -2 -2 -1 0.1745 2 1 -4 0.1510 -2 5 2 0.1570 0 -11 1 0.0731 -1 -5 -5 0.0898 0 -7 5 0.0668 -2 -2 3 0.1640 -1 -10 2 0.1167 0 9 4 0.0776 0 11 1 0.0601 0 11 0 0.0519 1 9 -3 0.1124 2 -4 -4 0.1436 0 4 6 0.0805 2 2 3 0.1994 0 -11 -1 0.0733 -1 10 -2 0.0768 2 -7 -3 0.1366 -2 0 5 0.1477 0 -11 -1 0.0759 0 11 -2 0.0619 -1 -3 6 0.1314 1 9 -4 0.1148 0 -6 5 0.0771 -2 -3 -3 0.1450 2 3 -5 0.1553 -1 3 -5 0.1036 -1 4 -5 0.0975 0 11 -1 0.0632 -1 -6 6 0.0932 0 1 6 0.0820 2 4 1 0.1949 0 -11 -1 0.0781 -1 -3 -5 0.0933 2 -5 0 0.1816 1 -10 -2 0.0997 -1 9 0 0.1081 _diffrn_orient_matrix_UB_11 0.1449192000 _diffrn_orient_matrix_UB_12 -0.0794025000 _diffrn_orient_matrix_UB_13 0.0521446000 _diffrn_orient_matrix_UB_21 0.1896222000 _diffrn_orient_matrix_UB_22 -0.0101422000 _diffrn_orient_matrix_UB_23 -0.1244912000 _diffrn_orient_matrix_UB_31 0.3585340000 _diffrn_orient_matrix_UB_32 0.0375210000 _diffrn_orient_matrix_UB_33 0.0768839000 _chemical_absolute_configuration . _diffrn_radiation_probe x-ray _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54184 _diffrn_source 'microfocus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray source' _diffrn_measurement_device 'four-circle diffractometer' _diffrn_radiation_monochromator 'multilayer optics' _diffrn_detector HyPix _diffrn_measurement_device_type 'XtaLAB Synergy, single source at home/near' _diffrn_measurement_method '\w scans' _diffrn_measurement_details ) List of Runs (angles in degrees, time in seconds, distance to detector was 34 mm): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -24.00 64.00 0.50 0.40 -- 47.45 -81.00 51.00 176 2 \w 38.00 82.00 0.50 1.59 -- 105.86 -81.00 51.00 88 3 \w 41.00 71.00 0.50 1.59 -- 105.86 -61.00 90.00 60 4 \w 42.00 80.00 0.50 1.59 -- 105.86 -77.00 90.00 76 5 \w 33.00 112.00 0.50 1.59 -- 105.86-125.00 90.00 158 6 \w 34.00 104.00 0.50 1.59 -- 105.86 -94.00 120.00 140 7 \w 34.00 66.00 0.50 1.59 -- 105.86 -61.00 0.00 64 8 \w 92.00 134.00 0.50 1.59 -- 105.86 15.00 -60.00 84 9 \w 151.00 178.00 0.50 1.59 -- 105.86 30.00 -60.00 54 10 \w 150.00 178.00 0.50 1.59 -- 105.86 15.00 -60.00 56 11 \w 102.00 141.00 0.50 1.59 -- 105.86 30.00 -60.00 78 12 \w 90.00 177.00 0.50 1.59 -- 105.86 61.00-150.00 174 13 \w 99.00 177.00 0.50 1.59 -- 105.86 45.00-180.00 156 14 \w 93.00 176.00 0.50 1.59 -- 105.86 30.00 -30.00 166 15 \w 94.00 120.00 0.50 1.59 -- 105.86 61.00 120.00 52 16 \w 106.00 131.00 0.50 1.59 -- 105.86 81.00 174.00 50 17 \w 98.00 175.00 0.50 1.59 -- 105.86 45.00 150.00 154 18 \w 75.00 101.00 0.50 0.40 -- 47.45 125.00 90.00 52 19 \w -3.00 25.00 0.50 0.40 -- -47.45 37.00 -30.00 56 20 \w -38.00 -11.00 0.50 0.40 -- -47.45 37.00 -30.00 54 21 \w -71.00 -46.00 0.50 1.59 -- -105.86 61.00 -30.00 50 22 \w -64.00 -35.00 0.50 1.59 -- -105.86 61.00 30.00 58 23 \w -61.00 -36.00 0.50 1.59 -- -105.86 125.00 30.00 50 24 \w -106.00 -34.00 0.50 1.59 -- -105.86 77.00 -30.00 144 25 \w -68.00 -34.00 0.50 1.59 -- -105.86 61.00-180.00 68 26 \w -105.00 -43.00 0.50 1.59 -- -105.86 77.00-120.00 124 27 \w -111.00 -85.00 0.50 1.59 -- -105.86 125.00 30.00 52 28 \w -55.00 17.00 0.50 0.40 -- -47.45 81.00 174.00 144 29 \w -4.00 40.00 0.50 0.40 -- 47.45 -37.00 90.00 88 30 \w -19.00 26.00 0.50 0.40 -- 47.45 -19.00 120.00 90 31 \w -21.00 4.00 0.50 0.40 -- 47.45 -19.00 150.00 50 32 \w -27.00 18.00 0.50 0.40 -- 47.45 -19.00 60.00 90 33 \w 60.00 85.00 0.50 1.59 -- 105.86-125.00-120.00 50 34 \w 72.00 105.00 0.50 1.59 -- 105.86 -77.00-120.00 66 35 \w 34.00 70.00 0.50 1.59 -- 105.86 -61.00-150.00 72 36 \w -119.00 -82.00 0.50 0.40 -- -47.45-125.00 -60.00 74 37 \w -147.00-103.00 0.50 1.59 -- -105.86 -81.00 51.00 88 38 \w -108.00 -83.00 0.50 1.59 -- -105.86 -77.00 0.00 50 39 \w -120.00 -74.00 0.50 0.40 -- -47.45-125.00 120.00 92 40 \w -163.00-137.00 0.50 1.59 -- -105.86 -77.00 0.00 52 41 \w -176.00-140.00 0.50 1.59 -- -105.86 -15.00 -60.00 72 ) _computing_data_collection 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_cell_refinement 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_data_reduction 'CrysAlisPro 1.171.40.84a (Rigaku OD, 2020)' _computing_structure_solution 'SHELXT-2018/2 (Sheldrick, 2015)' _computing_structure_refinement 'SHELXL-2018/3 (Sheldrick, 2015)' _computing_molecular_graphics ) WinGX (Farrugia, 2012); ORTEP-3 (Farrugia, 2012); PLATON (Spek, 2009); Olex2 (Dolomanov et al., 2009) ) _computing_publication_material ) WinGX (Farrugia, 2012); PLATON (Spek, 2009) ) _refine_special_details ) Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ) CELL 1.54184 3.629394 17.432674 10.068752 90.0000 99.9049 90.0000 ZERR 4.00 0.000056 0.000273 0.000169 0.0000 0.0016 0.0000 LATT 1 SYMM - X, 1/2 + Y, 1/2 - Z ; _shelx_hkl_checksum 35483 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.9983(3) 0.39706(5) 0.55127(9) 0.0226(3) Uani 1 1 d . . . . . H1A H 0.485(5) 0.4502(12) 0.2969(15) 0.038(5) Uiso 1 1 d D . . . . H1B H 0.739(5) 0.5012(8) 0.3973(18) 0.031(4) Uiso 1 1 d D . . . . O3 O 0.2322(3) 0.36174(5) 0.18835(9) 0.0221(3) Uani 1 1 d . . . . . N1 N 0.6479(3) 0.45555(6) 0.37204(11) 0.0219(3) Uani 1 1 d D . . . . N2 N 0.7604(3) 0.25822(6) 0.46509(10) 0.0176(3) Uani 1 1 d . . . . . N3 N 0.2980(3) 0.23342(6) 0.22515(10) 0.0183(3) Uani 1 1 d D . . . . H3 H 0.144(5) 0.2253(10) 0.1476(17) 0.030(4) Uiso 1 1 d D . . . . C1 C 0.7709(3) 0.39432(7) 0.44426(12) 0.0179(3) Uani 1 1 d . . . . . C2 C 0.6299(3) 0.31704(7) 0.39018(12) 0.0168(3) Uani 1 1 d . . . . . C3 C 0.3752(3) 0.30874(7) 0.26140(12) 0.0175(3) Uani 1 1 d . . . . . C4 C 0.4317(4) 0.17314(7) 0.30334(13) 0.0203(3) Uani 1 1 d . . . . . H4 H 0.366655 0.122245 0.274709 0.024 Uiso 1 1 calc R U . . . C5 C 0.6610(4) 0.18596(7) 0.42393(13) 0.0199(3) Uani 1 1 d . . . . . H5 H 0.751908 0.143681 0.479590 0.024 Uiso 1 1 calc R U . . . O11 O 0.3885(11) 0.4881(3) 0.0471(5) 0.0316(12) Uani 0.2070(14) 1 d G . P A -1 H11A H 0.332138 0.440296 0.061687 0.047 Uiso 0.2070(14) 1 d G U P A -1 H11B H 0.295724 0.495979 -0.037798 0.047 Uiso 0.2070(14) 1 d G U P A -1 O12 O 0.9741(11) 0.5045(2) 0.0736(4) 0.0278(12) Uani 0.2024(15) 1 d G . P B -2 H12A H 0.995733 0.455907 0.092595 0.042 Uiso 0.2024(15) 1 d G U P B -2 H12B H 1.088207 0.531131 0.141572 0.042 Uiso 0.2024(15) 1 d G U P B -2 O13 O 0.7249(11) 0.4965(2) 0.0814(3) 0.0176(12) Uani 0.181(3) 1 d G . P C 3 H13A H 0.771623 0.456363 0.132855 0.026 Uiso 0.181(3) 1 d G U P C 3 H13B H 0.617616 0.528595 0.128966 0.026 Uiso 0.181(3) 1 d G U P C 3 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0253(5) 0.0158(5) 0.0229(5) -0.0002(3) -0.0068(4) -0.0017(3) O3 0.0261(5) 0.0178(5) 0.0198(5) 0.0010(3) -0.0034(4) -0.0008(3) N1 0.0260(6) 0.0140(5) 0.0220(6) -0.0012(4) -0.0064(4) -0.0023(4) N2 0.0176(5) 0.0156(5) 0.0194(5) -0.0010(4) 0.0023(4) -0.0004(4) N3 0.0198(5) 0.0169(5) 0.0171(5) -0.0025(4) 0.0004(4) -0.0027(4) C1 0.0169(6) 0.0163(6) 0.0197(6) -0.0014(4) 0.0007(5) -0.0006(4) C2 0.0162(6) 0.0162(6) 0.0179(6) -0.0011(4) 0.0030(5) -0.0004(4) C3 0.0179(6) 0.0172(6) 0.0173(6) -0.0019(4) 0.0030(5) -0.0019(4) C4 0.0229(6) 0.0149(6) 0.0232(6) -0.0033(5) 0.0043(5) -0.0024(5) C5 0.0230(6) 0.0144(6) 0.0217(6) -0.0003(4) 0.0026(5) -0.0002(4) O11 0.045(3) 0.014(2) 0.034(3) 0.0092(19) 0.003(2) 0.0040(19) O12 0.049(3) 0.006(2) 0.024(2) 0.0044(16) -0.004(2) -0.001(2) O13 0.030(3) 0.007(2) 0.017(2) 0.0062(16) 0.008(2) 0.0073(19) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C1 N1 H1A 119.9(13) . . ? C1 N1 H1B 119.6(12) . . ? H1A N1 H1B 120.4(18) . . ? C2 N2 C5 119.98(11) . . ? C4 N3 C3 123.36(11) . . ? C4 N3 H3 119.7(12) . . ? C3 N3 H3 116.9(12) . . ? O1 C1 N1 123.82(11) . . ? O1 C1 C2 118.79(11) . . ? N1 C1 C2 117.38(11) . . ? N2 C2 C3 122.83(11) . . ? N2 C2 C1 115.07(11) . . ? C3 C2 C1 122.07(11) . . ? O3 C3 N3 120.54(11) . . ? O3 C3 C2 126.05(11) . . ? N3 C3 C2 113.40(11) . . ? N3 C4 C5 119.52(11) . . ? N3 C4 H4 120.2 . . ? C5 C4 H4 120.2 . . ? N2 C5 C4 120.85(12) . . ? N2 C5 H5 119.6 . . ? C4 C5 H5 119.6 . . ? H11A O11 H11B 104.6 . . ? H12A O12 H12B 109.6 . . ? H13A O13 H13B 104.4 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.2405(15) . ? O3 C3 1.2381(15) . ? N1 C1 1.3251(16) . ? N1 H1A 0.881(13) . ? N1 H1B 0.882(13) . ? N2 C2 1.3123(16) . ? N2 C5 1.3554(16) . ? N3 C4 1.3521(16) . ? N3 C3 1.3786(16) . ? N3 H3 0.889(15) . ? C1 C2 1.5089(16) . ? C2 C3 1.4644(17) . ? C4 C5 1.3673(18) . ? C4 H4 0.9500 . ? C5 H5 0.9500 . ? O11 H11A 0.8765 . ? O11 H11B 0.8737 . ? O12 H12A 0.8687 . ? O12 H12B 0.8705 . ? O13 H13A 0.8697 . ? O13 H13B 0.8707 . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A _geom_hbond_publ_flag N1 H1A O3 0.881(13) 2.017(17) 2.7224(14) 136.2(18) . yes N1 H1B O1 0.882(13) 2.038(13) 2.9163(14) 173.7(16) 3_766 yes N3 H3 O1 0.889(15) 2.365(17) 2.9609(14) 124.5(15) 4_465 yes N3 H3 N2 0.889(15) 2.126(16) 2.9878(15) 162.9(16) 4_465 yes loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag C5 N2 C2 C3 0.20(18) . . . . ? C5 N2 C2 C1 -177.99(10) . . . . ? O1 C1 C2 N2 1.18(17) . . . . ? N1 C1 C2 N2 179.83(11) . . . . ? O1 C1 C2 C3 -177.02(11) . . . . ? N1 C1 C2 C3 1.63(18) . . . . ? C4 N3 C3 O3 -176.90(11) . . . . ? C4 N3 C3 C2 2.60(17) . . . . ? N2 C2 C3 O3 177.35(11) . . . . ? C1 C2 C3 O3 -4.6(2) . . . . ? N2 C2 C3 N3 -2.13(17) . . . . ? C1 C2 C3 N3 175.94(10) . . . . ? C3 N3 C4 C5 -1.21(19) . . . . ? C2 N2 C5 C4 1.43(18) . . . . ? N3 C4 C5 N2 -0.98(19) . . . . ?