#------------------------------------------------------------------------------ #$Date: 2024-04-16 03:58:17 +0300 (Tue, 16 Apr 2024) $ #$Revision: 291217 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/98/7159897.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7159897 loop_ _publ_author_name 'Yaragorla, Srinivasarao' 'Khan, Tabassum' 'Chakraborty, Sayonika' _publ_section_title ; Cu(OTf)2/HFIP Catalyzed Regioselective Cycloisomerization of Indole-C3-functionalized Alkynols to Carbazoles ; _journal_name_full 'Organic & Biomolecular Chemistry' _journal_paper_doi 10.1039/D4OB00421C _journal_year 2024 _chemical_formula_moiety 'C37 H27 N' _chemical_formula_sum 'C37 H27 N' _chemical_formula_weight 485.59 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-09-14 _audit_creation_method ; Olex2 1.3-ac4 (compiled 2018.12.18 svn.r3554 for Rigaku Oxford Diffraction, GUI svn.r1) ; _audit_update_record ; 2023-09-14 deposited with the CCDC. 2024-04-15 downloaded from the CCDC. ; _cell_angle_alpha 66.465(4) _cell_angle_beta 77.764(5) _cell_angle_gamma 82.339(5) _cell_formula_units_Z 2 _cell_length_a 9.6614(12) _cell_length_b 12.3016(17) _cell_length_c 12.4047(16) _cell_measurement_reflns_used 7342 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 21.70 _cell_measurement_theta_min 2.57 _cell_volume 1319.0(3) _computing_cell_refinement 'SAINT V8.40B (?, 2016)' _computing_data_reduction 'SAINT V8.40B (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'ShelXT (Sheldrick, 2015)' _diffrn_ambient_temperature 298.0 _diffrn_measured_fraction_theta_full 0.891 _diffrn_measured_fraction_theta_max 0.892 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0938 _diffrn_reflns_av_unetI/netI 0.2231 _diffrn_reflns_Laue_measured_fraction_full 0.891 _diffrn_reflns_Laue_measured_fraction_max 0.892 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 14 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_l_max 14 _diffrn_reflns_limit_l_min -14 _diffrn_reflns_number 20603 _diffrn_reflns_point_group_measured_fraction_full 0.891 _diffrn_reflns_point_group_measured_fraction_max 0.892 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 25.349 _diffrn_reflns_theta_min 1.808 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.070 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6086 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1798 before and 0.1053 after correction. The Ratio of minimum to maximum transmission is 0.8163. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'metallic yellowish yellow' _exptl_crystal_colour_lustre metallic _exptl_crystal_colour_modifier yellowish _exptl_crystal_colour_primary yellow _exptl_crystal_density_diffrn 1.223 _exptl_crystal_description plate _exptl_crystal_F_000 512 _exptl_crystal_size_max 0.231 _exptl_crystal_size_mid 0.141 _exptl_crystal_size_min 0.114 _refine_diff_density_max 0.235 _refine_diff_density_min -0.201 _refine_diff_density_rms 0.057 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 0.970 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 344 _refine_ls_number_reflns 4319 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 0.970 _refine_ls_R_factor_all 0.1829 _refine_ls_R_factor_gt 0.1040 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0752P)^2^] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.2546 _refine_ls_wR_factor_ref 0.2919 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2010 _reflns_number_total 4319 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ob00421c2.cif _cod_data_source_block ysr014_0m _cod_database_code 7159897 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.992 _shelx_estimated_absorpt_t_min 0.984 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C5(H5), C12(H12), C11(H11), C26(H26), C23(H23), C9(H9), C29(H29), C27(H27), C8(H8), C36(H36), C10(H10), C30(H30), C14(H14), C35(H35), C20(H20), C15(H15), C16(H16), C18(H18), C21(H21), C34(H34), C22(H22), C32(H32), C17(H17), C33(H33) 2.b Idealised Me refined as rotating group: C37(H37A,H37B,H37C) ; _shelx_res_file ; TITL ysr014_0m_a.res in P-1 ysr014_0m.res created by SHELXL-2018/3 at 11:04:32 on 14-Sep-2023 REM Old TITL YSR014_0m in P-1 REM SHELXT solution in P-1: R1 0.238, Rweak 0.040, Alpha 0.077 REM 0.000 for 0 systematic absences, Orientation as input REM Formula found by SHELXT: C35 N3 CELL 0.71073 9.6614 12.3016 12.4047 66.465 77.764 82.339 ZERR 2 0.0012 0.0017 0.0016 0.004 0.005 0.005 LATT 1 SFAC C H N UNIT 74 54 2 L.S. 40 PLAN 20 SIZE 0.141 0.114 0.231 TEMP 24.85 BOND list 4 fmap 2 acta SHEL 9999 0.83 REM REM REM WGHT 0.075200 FVAR 0.43943 N1 3 0.108667 0.126959 0.733471 11.00000 0.07089 0.06847 = 0.05637 -0.02279 -0.00025 -0.02090 C2 1 0.177114 0.114834 0.627382 11.00000 0.05133 0.04781 = 0.05167 -0.01622 -0.00681 -0.00848 C5 1 0.313838 0.138638 0.402698 11.00000 0.04809 0.05263 = 0.04656 -0.01775 -0.00408 -0.00704 AFIX 43 H5 2 0.359255 0.145234 0.326505 11.00000 -1.20000 AFIX 0 C25 1 0.357121 0.351304 0.340564 11.00000 0.05700 0.04278 = 0.05302 -0.01756 -0.00566 -0.00664 C6 1 0.267727 0.029019 0.482691 11.00000 0.04276 0.04570 = 0.05267 -0.01474 -0.00842 -0.00852 C1 1 0.200973 0.012873 0.599690 11.00000 0.04461 0.05111 = 0.05210 -0.01181 -0.00861 -0.00954 C4 1 0.296440 0.239566 0.429236 11.00000 0.04897 0.04475 = 0.05023 -0.01170 -0.01147 -0.00677 C7 1 0.291149 -0.070835 0.440719 11.00000 0.05083 0.04947 = 0.05015 -0.01649 -0.01168 -0.00078 C19 1 0.172852 0.312846 0.598455 11.00000 0.04809 0.05239 = 0.06969 -0.02733 -0.01969 0.00128 C12 1 0.425804 -0.099054 0.387447 11.00000 0.06115 0.05098 = 0.06021 -0.01941 -0.01505 -0.00308 AFIX 43 H12 2 0.503470 -0.060568 0.385404 11.00000 -1.20000 AFIX 0 C3 1 0.221921 0.227225 0.543195 11.00000 0.04681 0.04536 = 0.05711 -0.01708 -0.01109 -0.00823 C11 1 0.444714 -0.182856 0.338149 11.00000 0.08306 0.05486 = 0.07093 -0.02207 -0.01995 0.01541 AFIX 43 H11 2 0.534641 -0.200034 0.301686 11.00000 -1.20000 AFIX 0 C26 1 0.455089 0.407033 0.365349 11.00000 0.07110 0.05254 = 0.06121 -0.01230 -0.02464 -0.01351 AFIX 43 H26 2 0.482732 0.373855 0.439781 11.00000 -1.20000 AFIX 0 C24 1 0.102245 0.246709 0.714987 11.00000 0.05324 0.07937 = 0.07043 -0.03884 -0.00654 -0.01260 C31 1 0.527907 0.680823 0.083575 11.00000 0.06980 0.04606 = 0.05205 -0.01566 -0.00708 -0.01107 C13 1 0.166602 -0.108345 0.689239 11.00000 0.05705 0.04999 = 0.05341 -0.01530 -0.01043 -0.01314 C23 1 0.029884 0.299896 0.794426 11.00000 0.08880 0.07814 = 0.07526 -0.04026 -0.00380 -0.01045 AFIX 43 H23 2 -0.019044 0.255373 0.869442 11.00000 -1.20000 AFIX 0 C9 1 0.197569 -0.217223 0.397241 11.00000 0.07967 0.05058 = 0.09257 -0.02888 -0.03230 -0.00098 AFIX 43 H9 2 0.120810 -0.258055 0.401723 11.00000 -1.20000 AFIX 0 C28 1 0.474253 0.565313 0.169895 11.00000 0.05961 0.04417 = 0.05182 -0.01513 -0.00508 -0.00794 C29 1 0.379239 0.506727 0.144942 11.00000 0.08837 0.06431 = 0.05324 -0.00504 -0.02587 -0.02386 AFIX 43 H29 2 0.352019 0.539355 0.070347 11.00000 -1.20000 AFIX 0 C27 1 0.511859 0.510375 0.281731 11.00000 0.06083 0.05474 = 0.06752 -0.02084 -0.01982 -0.01044 AFIX 43 H27 2 0.578164 0.544770 0.301031 11.00000 -1.20000 AFIX 0 C8 1 0.178671 -0.132287 0.445145 11.00000 0.06429 0.04662 = 0.07107 -0.02012 -0.02093 -0.00323 AFIX 43 H8 2 0.088396 -0.115574 0.481388 11.00000 -1.20000 AFIX 0 C36 1 0.444017 0.764978 0.007393 11.00000 0.08724 0.06035 = 0.07605 -0.00059 -0.02540 -0.02464 AFIX 43 H36 2 0.352703 0.746719 0.009975 11.00000 -1.20000 AFIX 0 C10 1 0.330301 -0.241902 0.342543 11.00000 0.12162 0.05097 = 0.07327 -0.02540 -0.03572 0.00441 AFIX 43 H10 2 0.343112 -0.298339 0.308489 11.00000 -1.20000 AFIX 0 C30 1 0.324909 0.402840 0.226752 11.00000 0.08367 0.06005 = 0.06293 -0.01274 -0.02690 -0.02477 AFIX 43 H30 2 0.264118 0.365341 0.205313 11.00000 -1.20000 AFIX 0 C14 1 0.275358 -0.188208 0.732900 11.00000 0.06635 0.06087 = 0.06016 -0.00858 -0.00760 -0.00563 AFIX 43 H14 2 0.368114 -0.164489 0.705826 11.00000 -1.20000 AFIX 0 C35 1 0.491174 0.873861 -0.071345 11.00000 0.11340 0.06132 = 0.07878 -0.00001 -0.03133 -0.01636 AFIX 43 H35 2 0.432355 0.928002 -0.120927 11.00000 -1.20000 AFIX 0 C20 1 0.173050 0.434065 0.562874 11.00000 0.07540 0.05657 = 0.09359 -0.03226 -0.01907 -0.00407 AFIX 43 H20 2 0.216425 0.481048 0.486584 11.00000 -1.20000 AFIX 0 C15 1 0.251602 -0.300339 0.814108 11.00000 0.10504 0.05599 = 0.07329 -0.01201 -0.02178 0.00411 AFIX 43 H15 2 0.327769 -0.351308 0.841822 11.00000 -1.20000 AFIX 0 C16 1 0.119321 -0.338364 0.854787 11.00000 0.14282 0.05630 = 0.07758 -0.00583 -0.02855 -0.02260 AFIX 43 H16 2 0.103723 -0.415327 0.910045 11.00000 -1.20000 AFIX 0 C18 1 0.029757 -0.146715 0.730751 11.00000 0.06072 0.08829 = 0.08974 -0.00984 -0.01250 -0.03282 AFIX 43 H18 2 -0.046847 -0.096023 0.703606 11.00000 -1.20000 AFIX 0 C21 1 0.106126 0.484485 0.644791 11.00000 0.10370 0.07955 = 0.09499 -0.04643 -0.01463 0.00019 AFIX 43 H21 2 0.109595 0.565803 0.623259 11.00000 -1.20000 AFIX 0 C34 1 0.625296 0.902225 -0.076409 11.00000 0.11841 0.06343 = 0.07432 -0.00516 -0.01234 -0.02902 AFIX 43 H34 2 0.658880 0.975310 -0.130060 11.00000 -1.20000 AFIX 0 C22 1 0.035299 0.417973 0.756177 11.00000 0.10212 0.09592 = 0.08984 -0.05319 -0.00194 -0.00208 AFIX 43 H22 2 -0.010215 0.456088 0.806478 11.00000 -1.20000 AFIX 0 C32 1 0.661241 0.712351 0.074531 11.00000 0.07363 0.07077 = 0.08810 -0.00247 -0.01664 -0.01752 AFIX 43 H32 2 0.722115 0.657826 0.121653 11.00000 -1.20000 AFIX 0 C17 1 0.008279 -0.262964 0.814218 11.00000 0.10238 0.10446 = 0.09134 -0.01288 -0.00258 -0.06912 AFIX 43 H17 2 -0.083412 -0.289057 0.842384 11.00000 -1.20000 AFIX 0 C33 1 0.708751 0.822381 -0.002160 11.00000 0.09192 0.07481 = 0.11331 0.00108 -0.01445 -0.03646 AFIX 43 H33 2 0.798741 0.842111 -0.003065 11.00000 -1.20000 AFIX 0 C37 1 0.044763 0.040080 0.843704 11.00000 0.18018 0.11377 = 0.06463 -0.03808 0.03346 -0.05428 AFIX 137 H37A 2 -0.020473 -0.002246 0.828396 11.00000 -1.50000 H37B 2 -0.005221 0.078801 0.895341 11.00000 -1.50000 H37C 2 0.117075 -0.014649 0.881392 11.00000 -1.50000 AFIX 0 HKLF 4 REM ysr014_0m_a.res in P-1 REM wR2 = 0.2919, GooF = S = 0.970, Restrained GooF = 0.970 for all data REM R1 = 0.1040 for 2010 Fo > 4sig(Fo) and 0.1829 for all 4319 data REM 344 parameters refined using 0 restraints END WGHT 0.0752 0.0000 REM Highest difference peak 0.235, deepest hole -0.201, 1-sigma level 0.057 Q1 1 0.3046 -0.2042 0.3604 11.00000 0.05 0.23 Q2 1 -0.0649 0.2755 0.8536 11.00000 0.05 0.23 Q3 1 0.4581 -0.1227 0.2768 11.00000 0.05 0.23 Q4 1 -0.0669 0.1437 0.8999 11.00000 0.05 0.23 Q5 1 0.1678 0.2293 0.6357 11.00000 0.05 0.22 Q6 1 0.0624 -0.1207 0.9327 11.00000 0.05 0.21 Q7 1 0.4359 -0.2165 0.3672 11.00000 0.05 0.20 Q8 1 0.3257 0.4053 0.3767 11.00000 0.05 0.20 Q9 1 0.2747 0.2021 0.6560 11.00000 0.05 0.19 Q10 1 0.3859 0.3004 0.1868 11.00000 0.05 0.19 Q11 1 0.3475 -0.1243 0.2761 11.00000 0.05 0.19 Q12 1 -0.1160 0.3053 0.9324 11.00000 0.05 0.19 Q13 1 0.4701 0.3434 0.3433 11.00000 0.05 0.19 Q14 1 0.0004 0.2583 0.9791 11.00000 0.05 0.18 Q15 1 0.0840 -0.2039 0.3608 11.00000 0.05 0.18 Q16 1 0.1012 0.1049 0.6231 11.00000 0.05 0.18 Q17 1 0.2094 -0.2412 0.5957 11.00000 0.05 0.17 Q18 1 0.2040 0.4742 0.4530 11.00000 0.05 0.17 Q19 1 0.2173 0.4768 0.4075 11.00000 0.05 0.17 Q20 1 0.6740 -0.1269 0.2724 11.00000 0.05 0.16 ; _shelx_res_checksum 23650 _shelx_hkl_file ; 1 0 0 43.40 18.50 -1 0 0 47.20 18.50 -1 0 0 45.30 18.50 -1 0 0 44.40 18.50 -1 0 0 43.60 18.50 -1 0 0 42.80 18.50 1 0 0 42.30 18.50 1 0 0 42.80 18.50 -2 0 0 5.80 2.60 2 0 0 7.40 2.60 2 0 0 5.20 2.50 2 0 0 7.40 2.60 2 0 0 10.70 2.70 -2 0 0 4.80 2.60 -2 0 0 4.50 2.50 -2 0 0 7.20 2.60 2 0 0 7.30 2.80 -3 0 0 8.70 4.00 -3 0 0 12.90 4.30 3 0 0 9.20 4.00 -3 0 0 8.20 4.10 -3 0 0 9.20 4.00 -3 0 0 7.60 4.10 3 0 0 13.10 4.50 3 0 0 10.90 4.30 3 0 0 10.80 4.20 3 0 0 10.20 4.00 -4 0 0 64.79 24.30 -4 0 0 53.09 24.20 4 0 0 51.99 24.30 -4 0 0 56.29 24.20 4 0 0 63.09 24.50 4 0 0 58.99 24.20 -4 0 0 56.59 24.20 4 0 0 59.69 24.30 -5 0 0 21.90 9.60 5 0 0 23.40 9.70 -5 0 0 23.70 10.00 -5 0 0 23.30 9.80 5 0 0 25.60 9.70 5 0 0 24.20 9.70 -5 0 0 22.10 9.70 -5 0 0 20.60 9.70 -6 0 0 87.39 35.40 -6 0 0 85.89 35.30 6 0 0 85.29 35.30 6 0 0 83.19 35.30 -6 0 0 78.79 35.40 -6 0 0 81.59 35.30 -6 0 0 91.59 35.50 -7 0 0 1.70 1.70 -7 0 0 -0.40 2.40 7 0 0 1.50 1.10 -7 0 0 0.80 1.00 7 0 0 1.40 1.20 -7 0 0 0.70 1.30 -7 0 0 -1.60 2.80 -8 0 0 10.30 6.00 8 0 0 11.40 5.10 -8 0 0 11.50 5.20 -8 0 0 5.20 5.70 -8 0 0 16.60 5.60 -8 0 0 11.60 5.10 -9 0 0 8.90 3.50 -9 0 0 7.70 3.90 -9 0 0 -0.40 1.70 -9 0 0 4.60 2.70 -9 0 0 2.40 2.20 -10 0 0 2.00 3.90 -10 0 0 3.30 1.80 -10 0 0 0.10 2.60 -10 0 0 7.20 4.60 -11 0 0 5.80 3.30 -11 0 0 3.70 4.40 -11 0 0 2.20 2.30 -11 0 0 8.00 5.50 -12 0 0 0.20 4.90 -12 0 0 0.30 3.60 -12 0 0 -0.30 2.10 0 -1 0 129.89 58.09 0 1 0 147.19 58.09 2 -1 0 310.27 129.39 2 -1 0 293.57 129.29 -2 -1 0 313.37 129.29 -2 -1 0 350.06 129.39 -2 -1 0 308.17 129.39 -2 -1 0 302.77 129.39 2 -1 0 303.17 129.29 2 -1 0 320.07 129.39 2 -1 0 267.47 129.39 -2 -1 0 323.47 129.39 -2 -1 0 316.47 129.39 2 -1 0 293.57 129.29 2 -1 0 303.17 129.39 -2 1 0 316.67 129.39 2 1 0 317.67 129.39 2 1 0 275.37 129.39 2 1 0 320.37 129.39 -2 1 0 283.57 129.39 2 1 0 320.07 129.39 2 1 0 312.17 129.29 -2 1 0 303.37 129.29 -2 1 0 313.67 129.29 2 1 0 308.47 129.39 -2 1 0 318.57 129.39 3 -1 0 1.70 3.30 -3 -1 0 5.50 3.00 -3 -1 0 8.20 2.90 -3 -1 0 5.90 2.90 -3 -1 0 11.30 3.10 3 -1 0 1.70 3.40 -3 1 0 3.40 3.20 3 1 0 7.00 2.90 3 1 0 7.80 2.90 3 1 0 8.60 3.10 3 1 0 6.80 3.40 3 1 0 8.50 3.00 3 1 0 6.50 2.90 3 1 0 4.50 3.00 -4 -1 0 46.50 22.60 -4 -1 0 59.79 22.60 -4 -1 0 56.09 22.70 -4 -1 0 43.40 22.70 4 1 0 54.79 22.80 4 1 0 52.89 22.70 4 1 0 54.29 22.60 4 1 0 56.79 22.90 4 1 0 52.99 22.60 4 1 0 65.89 22.60 -5 -1 0 89.39 34.60 -5 -1 0 80.19 34.70 -5 -1 0 80.29 34.60 -5 -1 0 81.39 34.60 -5 -1 0 75.19 34.60 5 1 0 89.49 34.60 5 1 0 76.99 34.80 5 1 0 79.99 34.60 5 1 0 82.89 34.50 -6 -1 0 11.60 3.40 6 -1 0 6.10 2.70 -6 -1 0 4.30 3.30 -6 -1 0 6.40 3.00 -6 -1 0 8.80 2.70 -6 -1 0 2.20 2.80 6 -1 0 8.80 3.10 -6 1 0 4.10 2.80 -6 1 0 5.80 3.10 -6 1 0 2.60 2.70 -6 1 0 5.20 3.90 -6 1 0 5.80 3.30 6 1 0 10.40 3.30 6 1 0 7.50 2.70 7 -1 0 15.70 7.50 7 -1 0 19.10 7.60 -7 -1 0 8.10 7.80 -7 1 0 20.20 7.40 -7 1 0 19.00 7.70 -7 1 0 24.40 7.50 -7 1 0 21.40 8.00 7 1 0 8.50 7.60 -7 1 0 19.40 7.90 8 -1 0 24.20 10.20 -8 1 0 30.80 10.70 -8 1 0 21.30 10.60 -8 1 0 24.70 10.50 -8 1 0 26.30 10.10 -8 1 0 18.30 10.20 -9 -1 0 3.80 3.20 -9 -1 0 1.50 1.50 -9 -1 0 3.00 2.10 -9 -1 0 4.40 3.60 -9 -1 0 1.10 2.80 -9 1 0 4.00 2.10 -9 1 0 -2.00 3.20 -9 1 0 1.60 4.20 -9 1 0 3.80 3.00 -9 1 0 0.90 1.50 -10 -1 0 3.60 2.50 -10 -1 0 2.40 1.60 -10 -1 0 -0.90 3.80 -10 1 0 -1.80 3.40 -10 1 0 1.00 1.40 -10 1 0 1.40 2.40 -11 -1 0 0.60 4.10 -11 -1 0 3.10 3.10 -11 -1 0 -1.60 1.80 -11 1 0 0.60 5.10 -11 1 0 1.90 2.90 -11 1 0 4.40 4.00 -11 1 0 2.20 1.80 -12 -1 0 1.40 2.20 -12 -1 0 2.00 4.70 -12 -1 0 3.30 4.00 -12 1 0 -0.50 2.10 -12 1 0 -2.10 6.00 -12 1 0 -3.10 3.40 -12 1 0 0.40 5.10 0 -2 0 412.06 181.68 0 -2 0 445.96 181.68 0 2 0 423.26 181.68 0 2 0 451.25 181.68 1 -2 0 169.98 74.29 1 -2 0 178.08 74.29 1 -2 0 174.28 74.29 1 -2 0 178.48 74.29 1 -2 0 177.28 74.29 1 -2 0 183.78 74.29 -1 2 0 194.48 74.29 -1 2 0 175.98 74.29 -1 2 0 159.48 74.29 -1 2 0 165.48 74.29 -1 2 0 175.68 74.29 -1 2 0 190.48 74.29 5 -2 0 6.50 2.50 5 -2 0 4.70 2.80 5 -2 0 4.50 2.90 5 -2 0 4.80 2.50 -5 2 0 3.30 2.70 5 2 0 21.30 4.10 -5 2 0 5.30 3.00 -5 2 0 7.40 2.60 -5 2 0 1.50 3.30 -5 2 0 5.30 2.50 5 2 0 19.10 3.60 -6 -2 0 1.70 1.20 -6 -2 0 0.00 2.40 -6 -2 0 1.80 1.40 6 -2 0 2.90 2.30 6 -2 0 1.90 1.50 -6 -2 0 -0.10 1.70 6 2 0 1.90 1.20 -6 2 0 4.10 1.40 6 2 0 1.70 2.70 -6 2 0 4.70 2.60 -6 2 0 4.30 1.20 -6 2 0 4.50 3.40 -6 2 0 3.10 1.60 7 -2 0 53.59 21.60 7 -2 0 49.20 21.50 7 -2 0 45.20 21.30 -7 2 0 49.99 21.70 -7 2 0 56.79 21.40 -7 2 0 42.30 21.30 -7 2 0 55.59 21.20 -7 2 0 48.00 21.60 -8 -2 0 11.00 4.70 -8 -2 0 12.50 5.20 -8 -2 0 7.80 4.90 -8 -2 0 12.00 5.30 8 -2 0 2.30 5.30 -8 2 0 1.30 5.90 -8 2 0 1.90 5.50 8 2 0 15.30 4.70 -9 -2 0 3.60 3.20 -9 -2 0 4.90 2.30 -9 -2 0 1.90 2.80 -9 -2 0 2.70 3.70 -9 2 0 6.00 2.20 -9 2 0 1.20 3.90 -9 2 0 5.00 3.30 -9 2 0 3.60 2.60 -9 2 0 11.40 5.10 -10 -2 0 0.60 2.50 -10 -2 0 0.10 1.60 -10 2 0 0.30 1.40 -10 2 0 0.70 2.20 -10 2 0 -0.70 5.20 -11 -2 0 -0.20 3.20 -11 -2 0 3.20 4.10 -11 -2 0 2.90 1.90 -11 2 0 -2.90 4.30 -11 2 0 -1.00 4.10 -11 2 0 -3.40 5.50 -12 -2 0 0.00 3.90 -12 -2 0 0.10 2.20 -12 -2 0 0.20 4.70 -12 2 0 -5.40 6.00 12 2 0 3.40 3.70 -12 2 0 1.70 3.40 -12 2 0 -0.30 5.00 0 -3 0 335.17 144.29 0 -3 0 347.67 144.29 0 3 0 357.46 144.29 0 3 0 335.27 144.29 2 -3 0 59.89 25.30 2 -3 0 58.09 25.30 2 -3 0 62.69 25.40 2 -3 0 60.19 25.20 2 -3 0 63.49 25.30 2 -3 0 59.79 25.30 -2 3 0 58.79 25.30 -2 3 0 58.19 25.30 -2 3 0 65.19 25.20 -2 3 0 59.29 25.30 -2 3 0 55.79 25.20 -2 3 0 60.69 25.30 3 -3 0 76.89 28.90 3 -3 0 70.49 28.70 3 -3 0 63.09 28.70 3 -3 0 65.19 28.70 3 -3 0 65.29 28.70 3 -3 0 65.29 28.90 3 -3 0 60.39 28.80 -3 3 0 74.39 28.70 -3 3 0 71.49 28.70 -3 3 0 71.59 28.70 4 -3 0 2.30 1.10 4 -3 0 3.40 1.50 4 -3 0 1.60 1.80 4 -3 0 0.80 1.20 -4 -3 0 -0.70 1.50 4 -3 0 2.90 1.30 -4 -3 0 1.20 0.80 -4 -3 0 1.50 1.10 -4 -3 0 0.90 1.10 -4 -3 0 1.60 0.90 4 -3 0 1.80 0.80 -4 -3 0 0.90 1.30 4 3 0 1.90 1.00 4 3 0 1.90 3.10 -4 3 0 0.90 1.90 -4 3 0 1.70 1.10 4 3 0 1.50 1.50 -4 3 0 0.30 0.90 -4 3 0 1.30 1.70 4 3 0 4.40 2.40 4 3 0 1.50 0.90 -5 -3 0 6.40 1.80 -5 -3 0 6.30 1.40 -5 -3 0 4.20 1.10 5 -3 0 1.70 1.20 5 -3 0 1.80 1.70 5 -3 0 -0.10 2.30 5 -3 0 1.30 1.70 5 -3 0 0.40 1.40 -5 3 0 -0.70 1.30 -5 3 0 1.90 1.50 5 3 0 10.40 2.50 -5 3 0 -0.30 2.70 5 3 0 4.20 3.00 -5 3 0 -1.30 2.00 -6 -3 0 5.80 3.20 -6 -3 0 7.40 3.00 6 -3 0 5.50 3.30 6 -3 0 5.60 3.90 -6 -3 0 11.00 3.50 -6 -3 0 8.80 3.20 6 -3 0 6.10 3.40 6 -3 0 7.40 3.20 6 3 0 8.30 4.40 -6 3 0 3.90 3.10 6 3 0 7.20 3.20 6 3 0 9.20 3.00 -6 3 0 5.80 3.40 -6 3 0 5.20 3.80 -6 3 0 3.50 4.40 7 -3 0 -1.30 3.50 -7 -3 0 5.90 1.90 -7 -3 0 8.40 2.80 -7 -3 0 5.80 2.40 -7 -3 0 5.60 2.20 7 -3 0 1.60 3.30 -7 3 0 -0.40 3.20 -7 3 0 -1.50 2.50 -7 3 0 0.00 3.70 -7 3 0 1.90 2.10 7 3 0 7.20 2.30 -8 -3 0 0.90 1.90 -8 -3 0 2.50 1.40 -8 -3 0 3.50 2.30 -8 -3 0 1.40 2.70 8 -3 0 0.70 3.40 -8 3 0 0.10 3.60 -8 3 0 -3.30 3.10 -8 3 0 0.90 2.40 8 3 0 3.70 2.00 8 3 0 2.00 1.50 -8 3 0 1.20 1.80 -9 -3 0 4.80 2.40 -9 -3 0 4.70 2.50 -9 3 0 0.10 5.00 -9 3 0 0.30 2.60 9 3 0 0.90 2.20 -9 3 0 0.10 2.10 -10 -3 0 3.30 3.20 -10 -3 0 3.30 3.00 -10 -3 0 2.40 2.00 -10 3 0 1.50 3.50 10 3 0 4.80 2.90 -10 3 0 1.30 2.50 -10 3 0 2.40 5.40 -11 -3 0 0.20 3.70 -11 -3 0 5.90 3.40 -11 -3 0 3.50 2.10 -11 3 0 -0.50 6.00 11 3 0 1.00 3.00 -11 3 0 -1.30 2.70 -11 3 0 -0.90 4.40 -12 -3 0 3.30 2.30 -12 -3 0 -2.20 4.10 -12 -3 0 2.40 4.40 12 3 0 -1.00 3.50 0 -4 0 2.50 1.50 0 -4 0 1.10 0.70 0 -4 0 1.40 1.20 0 4 0 2.60 2.00 0 4 0 0.90 0.60 0 4 0 0.70 0.50 1 -4 0 4.70 1.90 1 -4 0 4.40 2.10 1 -4 0 1.40 2.40 1 -4 0 6.80 2.40 1 -4 0 3.20 1.90 -1 4 0 3.00 1.90 -1 4 0 3.50 2.60 1 4 0 14.00 2.90 -1 4 0 4.70 1.90 -1 4 0 5.40 2.10 -1 4 0 7.30 2.00 2 -4 0 49.40 19.60 2 -4 0 37.30 19.60 2 -4 0 49.40 19.50 2 -4 0 44.60 19.50 2 -4 0 39.90 19.70 2 -4 0 45.40 19.50 -2 4 0 43.80 19.70 -2 4 0 49.60 19.50 -2 4 0 48.70 19.60 -2 4 0 42.20 19.60 3 -4 0 60.99 26.60 3 -4 0 65.99 26.70 3 -4 0 64.39 26.60 3 -4 0 66.29 26.60 3 -4 0 61.49 26.70 3 -4 0 64.09 26.60 -3 4 0 48.20 26.70 -3 4 0 65.99 26.70 -3 4 0 62.99 26.60 -3 4 0 54.99 26.70 -3 4 0 68.19 26.60 -5 -4 0 0.70 1.50 -5 -4 0 0.50 1.20 5 -4 0 0.50 0.70 5 -4 0 -0.10 2.40 5 -4 0 0.70 1.40 -5 -4 0 1.20 0.70 -5 -4 0 -0.80 0.90 -5 -4 0 -0.30 0.90 -5 4 0 0.10 1.80 -5 4 0 0.10 2.00 5 4 0 0.80 0.80 5 4 0 1.00 1.00 5 4 0 -0.60 1.70 -5 4 0 1.10 1.30 7 -4 0 -2.20 4.60 -7 -4 0 15.60 3.70 -7 -4 0 15.00 3.80 -7 4 0 1.30 3.40 -7 4 0 0.50 4.10 -7 4 0 -0.80 4.80 -8 -4 0 10.90 2.30 8 -4 0 1.50 1.70 -8 -4 0 8.40 2.50 8 -4 0 0.70 4.20 -8 4 0 -0.20 4.30 -8 4 0 1.40 3.60 -8 4 0 0.00 2.40 -8 4 0 -1.90 1.80 -9 -4 0 3.90 2.40 -9 -4 0 5.90 3.30 -9 -4 0 6.40 3.40 9 4 0 2.60 2.90 -9 4 0 0.90 5.50 -9 4 0 4.90 3.60 -9 4 0 7.50 2.80 -10 -4 0 6.50 4.40 -10 -4 0 5.20 4.00 -10 -4 0 11.70 3.20 -10 4 0 6.00 6.10 -10 4 0 0.10 3.40 10 4 0 10.10 3.80 -10 4 0 2.30 4.50 -11 -4 0 -0.10 3.50 -11 -4 0 -2.80 3.50 -11 -4 0 -0.10 2.00 11 4 0 -0.40 2.90 -11 4 0 3.20 4.30 -11 4 0 -2.00 2.60 -11 4 0 -2.60 6.00 0 -5 0 213.78 85.79 0 -5 0 226.48 85.89 0 5 0 230.28 85.89 0 5 0 189.58 85.79 0 5 0 168.08 85.79 1 -5 0 1.20 0.60 1 -5 0 -0.20 1.60 1 -5 0 0.70 2.10 1 -5 0 0.60 0.90 1 -5 0 0.40 1.80 -1 5 0 0.30 1.00 -1 5 0 3.40 2.50 -1 5 0 0.00 0.90 -1 5 0 0.50 0.40 -1 5 0 0.70 0.60 1 5 0 15.60 3.00 3 -5 0 3.80 1.80 3 -5 0 2.20 2.80 3 -5 0 4.10 1.70 -3 -5 0 13.50 2.90 -3 5 0 5.30 2.80 -3 5 0 3.60 1.90 -3 5 0 1.30 2.30 -3 5 0 3.70 2.70 -3 5 0 3.60 1.90 4 -5 0 29.90 11.50 4 -5 0 28.30 11.80 4 -5 0 26.80 11.60 -4 5 0 24.40 11.50 -4 5 0 29.20 11.60 -4 5 0 26.30 11.70 -4 5 0 17.10 11.80 -4 5 0 31.20 11.80 5 -5 0 11.40 3.90 -5 -5 0 14.10 4.40 5 -5 0 6.30 4.50 5 -5 0 8.40 3.60 -5 5 0 8.60 3.80 -5 5 0 2.40 4.20 -5 5 0 4.40 4.50 -6 5 0 -1.20 3.70 -6 5 0 2.60 2.80 7 -5 0 0.50 4.10 -7 -5 0 0.90 2.20 -7 -5 0 3.90 2.50 -7 -5 0 4.20 1.80 7 5 0 4.80 2.10 -7 5 0 1.50 3.20 -7 5 0 2.50 2.60 -7 5 0 -4.60 4.20 7 5 0 6.40 2.10 -7 5 0 1.70 2.00 -8 -5 0 15.90 5.40 8 -5 0 -2.80 6.70 -8 -5 0 13.50 4.90 -8 -5 0 9.70 5.20 8 5 0 8.70 5.10 -8 5 0 -1.60 6.50 8 5 0 12.80 5.10 -9 -5 0 5.20 3.00 -9 -5 0 6.60 2.20 -9 -5 0 3.00 3.00 9 5 0 4.80 2.50 -9 5 0 3.70 6.00 9 5 0 3.60 2.70 -9 5 0 2.90 2.50 -9 5 0 1.30 3.30 -10 -5 0 3.20 2.90 -10 -5 0 0.20 1.80 -10 -5 0 1.70 3.30 -10 5 0 0.10 3.70 -10 5 0 -0.30 2.40 -10 5 0 -5.20 6.00 10 5 0 1.90 2.50 -11 -5 0 4.00 2.00 -11 -5 0 2.30 4.00 -11 -5 0 -3.50 3.50 11 5 0 1.80 3.00 -11 5 0 0.40 2.70 -11 5 0 0.70 6.80 -11 5 0 -2.80 4.30 0 -6 0 15.60 6.20 0 6 0 15.70 6.30 0 6 0 19.10 6.40 0 6 0 11.60 6.20 -1 -6 0 1.00 0.70 1 -6 0 -0.70 2.40 -1 -6 0 -0.70 2.00 1 -6 0 3.00 2.80 1 -6 0 1.30 0.80 -1 -6 0 0.50 1.60 1 6 0 1.30 1.00 1 6 0 1.00 0.70 -1 6 0 1.10 1.50 -1 6 0 -0.90 3.50 -1 6 0 -0.70 1.00 -1 6 0 -0.10 0.70 1 6 0 0.90 0.50 2 -6 0 5.40 2.60 -2 -6 0 1.40 2.50 -2 -6 0 -0.60 1.40 2 -6 0 8.30 1.40 2 6 0 1.10 1.30 2 6 0 1.00 1.40 -2 6 0 9.50 1.60 -2 6 0 7.90 3.50 2 6 0 -0.10 1.50 -2 6 0 6.00 1.60 -2 6 0 3.60 1.40 3 -6 0 22.30 9.30 3 -6 0 25.00 9.70 3 -6 0 21.30 9.30 -3 6 0 32.60 10.00 -3 6 0 22.20 9.70 -3 6 0 21.40 9.40 -3 6 0 18.90 9.50 -3 6 0 23.80 9.40 -3 6 0 21.00 9.20 4 -6 0 0.50 0.90 -4 -6 0 -0.80 1.60 -4 -6 0 0.80 2.40 4 -6 0 -0.30 2.70 -4 -6 0 -0.70 1.00 4 -6 0 -0.10 0.80 -4 6 0 0.80 1.90 4 6 0 -0.30 0.90 -4 6 0 -2.10 2.50 -4 6 0 -0.20 0.90 4 6 0 -0.30 1.10 -4 6 0 -0.50 3.30 5 -6 0 7.50 2.60 5 -6 0 4.80 4.10 5 -6 0 5.40 2.70 -5 6 0 3.60 3.30 -5 6 0 7.90 2.90 -5 6 0 -0.70 3.70 -5 6 0 4.10 2.60 -6 -6 0 8.50 2.10 -6 -6 0 5.50 2.40 -6 -6 0 9.80 3.50 6 -6 0 -1.70 4.10 -6 6 0 1.90 3.50 6 6 0 6.70 2.40 6 6 0 3.90 2.30 -6 6 0 0.50 2.60 -6 6 0 -1.40 4.10 -7 -6 0 2.20 2.00 7 -6 0 8.20 4.90 -7 -6 0 6.50 3.70 -7 -6 0 2.00 2.40 7 6 0 2.40 2.30 -7 6 0 7.10 5.40 -7 6 0 10.40 2.90 7 6 0 3.80 2.40 -8 -6 0 7.90 2.50 8 -6 0 -7.00 7.70 -8 -6 0 4.00 1.50 8 6 0 1.70 2.10 -8 6 0 2.60 1.70 8 6 0 -0.10 2.00 -8 6 0 3.80 5.20 -8 6 0 0.90 2.70 -9 -6 0 14.20 3.10 -9 6 0 -0.50 6.30 9 6 0 9.60 3.50 -9 6 0 1.30 4.00 9 6 0 6.60 3.40 -9 6 0 0.60 3.20 -10 -6 0 0.60 1.70 -10 -6 0 -0.80 3.10 -10 6 0 1.10 6.40 -10 6 0 -0.10 4.10 10 6 0 -2.90 2.50 -10 6 0 0.30 2.30 -11 -6 0 -0.70 3.70 -11 -6 0 -1.30 2.00 11 6 0 -0.90 3.20 0 -7 0 41.00 14.70 0 7 0 30.60 14.80 0 7 0 28.90 14.70 0 7 0 44.60 14.80 0 7 0 41.00 15.10 1 -7 0 26.30 13.80 -1 -7 0 31.60 13.50 1 -7 0 40.30 14.00 -1 -7 0 19.20 13.70 1 -7 0 30.50 13.40 -1 -7 0 39.90 13.60 -1 7 0 27.60 13.50 -1 7 0 37.30 13.70 -1 7 0 31.40 13.60 -1 7 0 32.50 13.40 1 7 0 24.90 13.50 1 7 0 35.20 13.40 1 7 0 38.40 13.50 -2 -7 0 2.40 4.20 -2 -7 0 2.90 3.40 2 -7 0 10.40 3.40 2 -7 0 6.30 4.30 -2 7 0 8.70 3.30 -2 7 0 5.70 3.50 -2 7 0 8.40 3.40 -2 7 0 12.30 3.60 3 -7 0 1.70 3.00 -3 -7 0 -0.40 1.10 3 -7 0 2.90 1.10 -3 -7 0 -3.50 2.70 -3 7 0 3.00 1.30 3 7 0 0.40 1.10 3 7 0 1.20 0.90 -3 7 0 6.00 4.20 -3 7 0 1.00 3.10 -3 7 0 1.00 1.30 3 7 0 1.30 1.30 4 -7 0 1.10 5.20 -4 -7 0 31.40 5.30 -4 7 0 -1.90 5.20 5 -7 0 -0.80 3.60 -5 -7 0 2.60 3.00 -5 -7 0 -0.40 1.30 -5 7 0 -0.10 1.50 -5 7 0 0.80 1.10 -5 7 0 5.30 3.60 5 7 0 -1.50 1.40 5 7 0 0.10 1.20 -6 -7 0 19.00 5.80 6 -7 0 13.80 7.10 -6 -7 0 8.70 6.40 -6 7 0 23.30 6.20 -6 7 0 11.00 7.20 6 7 0 7.70 5.80 -6 7 0 15.00 5.70 6 7 0 8.40 5.70 7 -7 0 5.90 5.20 -7 -7 0 0.50 3.50 -7 -7 0 3.80 2.20 -7 -7 0 3.20 1.60 7 7 0 3.00 2.20 -7 7 0 7.80 5.00 -7 7 0 3.00 2.60 7 7 0 1.10 1.90 -8 -7 0 11.50 3.60 -8 7 0 -3.80 7.30 -8 7 0 -0.50 3.90 8 7 0 10.80 3.50 8 7 0 7.90 3.40 -9 -7 0 0.40 1.60 -9 -7 0 3.50 2.90 -9 7 0 3.00 7.10 -9 7 0 3.60 3.60 9 7 0 0.90 2.30 9 7 0 0.50 2.50 -10 -7 0 0.80 1.90 -10 -7 0 -2.00 3.20 -10 7 0 0.20 4.30 -10 7 0 -3.10 7.40 10 7 0 3.70 2.80 -11 -7 0 2.50 4.30 -11 -7 0 -1.20 2.20 11 7 0 3.10 3.20 0 -8 0 56.49 20.00 0 8 0 41.10 20.00 0 8 0 45.40 19.90 -1 -8 0 2.60 5.10 -1 -8 0 11.30 4.90 -1 -8 0 11.00 4.40 1 -8 0 9.40 5.40 1 8 0 11.80 4.40 -1 8 0 18.30 4.60 1 8 0 6.40 4.50 1 8 0 8.40 4.30 -2 -8 0 1.80 3.20 2 -8 0 6.50 3.50 -2 -8 0 1.00 1.50 -2 8 0 4.80 1.60 -2 8 0 7.20 2.30 -2 8 0 3.60 1.20 2 8 0 1.60 1.30 2 8 0 1.40 1.70 -2 8 0 2.30 1.80 2 8 0 0.90 1.40 3 -8 0 -2.50 3.30 -3 -8 0 -2.00 2.90 3 -8 0 -2.40 1.40 -3 -8 0 0.50 1.20 -3 8 0 -0.60 1.40 3 8 0 1.10 1.50 3 8 0 1.00 0.80 -3 8 0 -2.30 3.40 -3 8 0 -0.20 1.30 3 8 0 0.10 0.90 -3 8 0 -0.10 0.60 -4 -8 0 19.30 5.30 4 -8 0 15.80 6.50 -4 -8 0 19.90 6.20 -4 8 0 10.90 5.10 4 8 0 15.80 5.40 -4 8 0 9.60 5.30 -4 8 0 12.80 6.80 -4 8 0 8.70 5.40 5 -8 0 1.90 4.30 -5 -8 0 7.00 3.60 -5 -8 0 -2.00 1.50 5 8 0 0.80 1.00 -5 8 0 -1.50 1.30 -5 8 0 2.50 4.10 5 8 0 1.50 1.20 5 8 0 1.50 1.70 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23.90 6.90 4 9 0 16.50 6.80 4 9 0 16.60 6.60 -5 -9 0 4.30 4.10 -5 -9 0 0.50 1.80 5 -9 0 5.60 4.90 -5 9 0 18.10 5.30 5 9 0 2.20 1.40 5 9 0 0.80 1.60 5 9 0 1.90 2.20 -6 -9 0 4.00 5.50 -6 -9 0 12.30 4.00 6 -9 0 6.10 6.30 6 9 0 12.10 3.60 -6 9 0 2.10 6.50 -6 9 0 1.60 4.10 6 9 0 7.60 4.10 6 9 0 9.90 3.80 -7 -9 0 3.50 2.60 7 -9 0 1.10 6.40 -7 -9 0 -1.30 4.70 7 9 0 0.50 1.90 -7 9 0 -1.60 5.90 7 9 0 -0.20 2.70 7 9 0 2.40 2.20 -7 9 0 6.30 3.10 -8 -9 0 1.70 4.60 -8 -9 0 0.80 2.90 -8 -9 0 0.90 2.50 8 9 0 1.40 2.80 8 9 0 -0.20 1.80 8 9 0 -0.30 2.00 -8 9 0 -0.50 3.20 -8 9 0 -0.50 6.60 -9 -9 0 2.10 3.50 -9 -9 0 3.80 2.00 9 9 0 2.20 3.50 -9 9 0 11.40 8.40 9 9 0 0.00 2.50 -9 9 0 1.80 4.20 9 9 0 4.40 2.20 -10 -9 0 1.20 2.10 -10 -9 0 -0.60 4.00 10 9 0 3.00 2.80 10 9 0 -0.50 2.40 0 -10 0 10.00 5.50 0 -10 0 9.40 3.40 0 10 0 5.90 3.30 0 10 0 12.80 3.90 0 10 0 6.50 3.50 1 -10 0 -0.60 7.00 -1 -10 0 29.30 7.20 2 -10 0 -3.60 4.30 -2 -10 0 6.70 4.20 -2 -10 0 -1.50 1.30 2 10 0 1.10 1.40 2 10 0 0.60 2.00 -2 10 0 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12 14 -0.40 2.00 1 12 14 0.90 3.10 1 12 14 1.40 2.90 -2 -12 -14 -1.80 3.80 2 12 14 0.90 2.00 2 12 14 0.90 2.90 2 12 14 1.60 3.30 -3 -12 -14 2.30 3.80 -3 -12 -14 1.20 2.40 3 12 14 0.40 2.80 3 12 14 0.30 3.30 3 12 14 3.10 2.00 -4 -12 -14 0.30 2.30 -4 -12 -14 -2.90 3.40 4 12 14 -0.80 1.70 4 12 14 -0.10 3.40 4 12 14 2.20 2.30 -5 -12 -14 0.30 3.20 -5 -12 -14 -1.10 2.40 5 12 14 0.20 2.30 5 12 14 3.20 3.30 5 12 14 -0.30 1.90 1 1 15 4.10 5.30 1 1 15 1.50 4.80 -2 -1 -15 0.70 3.00 -2 -1 -15 0.80 3.90 2 1 15 0.00 4.60 2 1 15 3.40 4.50 -3 -1 -15 -0.80 2.90 -3 -1 -15 0.30 4.10 3 1 15 1.70 4.40 3 1 15 -3.40 4.20 -4 -1 -15 -0.80 4.40 4 1 15 -2.50 4.10 0 -2 -15 6.00 4.80 0 2 15 7.00 6.20 0 2 15 15.00 5.80 -1 -2 -15 3.90 3.00 1 2 15 1.70 4.40 1 2 15 -3.40 4.00 -2 -2 -15 1.40 2.80 2 2 15 -1.70 3.80 2 2 15 2.30 4.20 -3 -2 -15 -1.90 3.60 3 2 15 -2.40 3.80 3 2 15 2.00 3.70 -4 -2 -15 0.70 4.20 -4 -2 -15 5.30 2.90 4 2 15 2.40 3.70 4 2 15 -1.00 4.00 -5 -2 -15 -2.30 4.20 -5 -2 -15 -0.50 2.60 5 2 15 0.30 3.60 5 2 15 -0.20 3.80 1 -3 -15 0.80 3.10 -1 3 15 1.30 4.90 -1 3 15 2.80 4.20 0 -3 -15 0.20 3.30 0 3 15 10.90 4.90 0 3 15 4.60 4.20 -1 -3 -15 -0.40 2.80 1 3 15 0.30 3.60 1 3 15 5.50 4.00 -2 -3 -15 2.00 2.70 2 3 15 -0.30 3.80 2 3 15 -1.50 3.30 -3 -3 -15 -2.30 2.50 3 3 15 2.30 3.70 3 3 15 0.80 3.30 -4 -3 -15 -0.10 3.60 4 3 15 -0.40 3.20 4 3 15 1.60 3.50 -5 -3 -15 3.90 2.60 -5 -3 -15 -1.30 3.90 5 3 15 -2.10 3.40 5 3 15 0.30 3.20 -6 -3 -15 1.70 2.60 -6 -3 -15 1.00 4.20 6 3 15 -1.20 3.40 6 3 15 1.10 3.50 1 -4 -15 5.00 3.20 -1 4 15 -1.30 3.80 -1 4 15 4.10 4.80 0 -4 -15 -1.30 2.90 0 4 15 -3.00 3.30 0 4 15 -0.80 4.10 -1 -4 -15 -3.00 2.60 1 4 15 -0.10 3.60 1 4 15 0.60 3.20 -2 -4 -15 0.70 2.60 2 4 15 -0.60 2.90 2 4 15 0.90 3.60 -3 -4 -15 1.70 2.40 3 4 15 -1.80 2.90 3 4 15 -0.10 3.50 -4 -4 -15 3.10 2.90 -4 -4 -15 6.40 3.90 4 4 15 5.60 3.70 4 4 15 1.50 3.30 -5 -4 -15 3.60 3.70 5 4 15 1.20 2.90 5 4 15 -2.60 3.20 -6 -4 -15 -1.80 2.40 -6 -4 -15 1.70 3.90 6 4 15 -1.00 3.30 6 4 15 1.80 3.00 1 -5 -15 0.50 3.00 -1 5 15 6.20 4.40 -1 5 15 -0.90 3.40 0 -5 -15 -1.20 2.90 0 5 15 2.80 3.00 0 5 15 1.20 4.00 -1 -5 -15 2.50 2.70 1 5 15 -1.90 2.80 1 5 15 -1.40 3.40 -2 -5 -15 0.20 2.50 2 5 15 -0.10 3.40 2 5 15 -0.10 2.80 -3 -5 -15 1.10 2.50 3 5 15 -0.70 2.80 3 5 15 2.30 3.30 -4 -5 -15 -0.20 2.30 4 5 15 -0.20 2.70 4 5 15 -0.50 1.70 4 5 15 0.60 3.20 -5 -5 -15 3.30 3.60 -5 -5 -15 1.10 2.30 -5 -5 -15 1.30 1.70 5 5 15 2.40 3.20 5 5 15 0.30 1.80 5 5 15 -0.40 2.70 -6 -5 -15 0.10 1.80 -6 -5 -15 3.40 3.80 6 5 15 -0.70 2.80 6 5 15 1.40 1.90 6 5 15 -1.10 3.20 -2 6 15 1.90 5.10 1 -6 -15 1.60 3.20 -1 6 15 5.30 4.10 -1 6 15 -2.80 3.10 -1 6 15 3.00 4.70 0 -6 -15 8.50 3.80 0 6 15 4.50 6.30 0 6 15 3.60 4.30 0 6 15 3.60 3.60 -1 -6 -15 -0.90 2.60 1 6 15 -0.20 2.80 1 6 15 0.70 3.40 -2 -6 -15 0.30 2.60 2 6 15 3.30 3.30 2 6 15 -1.50 1.70 2 6 15 3.50 2.80 -3 -6 -15 -1.20 2.40 3 6 15 1.50 3.10 3 6 15 -1.60 2.60 -4 -6 -15 -0.70 2.40 -4 -6 -15 -2.40 1.60 4 6 15 -1.80 2.60 4 6 15 1.60 1.70 4 6 15 -1.80 2.90 -5 -6 -15 1.10 1.70 -5 -6 -15 0.50 2.20 5 6 15 -0.10 2.60 5 6 15 -3.20 1.70 5 6 15 2.90 2.90 -6 -6 -15 0.30 2.30 -6 -6 -15 0.00 1.90 -6 -6 -15 0.60 3.80 6 6 15 -1.80 1.80 6 6 15 1.30 2.70 6 6 15 -1.00 3.20 -7 -6 -15 4.40 4.20 7 6 15 2.90 3.70 1 -7 -15 0.50 3.40 -1 7 15 -1.60 3.90 -1 7 15 -0.10 4.30 -1 7 15 1.20 3.10 0 -7 -15 0.10 3.10 0 7 15 1.40 2.90 0 7 15 -2.00 3.60 0 7 15 3.30 3.80 -1 -7 -15 1.40 2.90 1 7 15 -5.00 2.60 1 7 15 -1.60 1.80 1 7 15 -2.10 3.30 -2 -7 -15 1.30 2.80 2 7 15 1.90 2.80 2 7 15 2.50 3.20 2 7 15 2.00 1.90 -3 -7 -15 0.00 2.60 3 7 15 -2.60 2.90 3 7 15 1.40 2.60 3 7 15 2.70 1.80 -4 -7 -15 -0.40 2.50 -4 -7 -15 -0.50 1.70 4 7 15 -0.50 2.60 4 7 15 0.70 1.80 4 7 15 -1.60 3.00 -5 -7 -15 3.80 2.30 -5 -7 -15 1.70 2.70 5 7 15 2.00 3.30 5 7 15 4.00 3.00 -6 -7 -15 1.50 2.10 -6 -7 -15 3.90 3.60 -6 -7 -15 -0.90 2.40 6 7 15 0.90 2.70 6 7 15 4.10 3.40 -7 -7 -15 -3.70 3.70 1 -8 -15 -2.00 3.30 -1 8 15 -1.60 3.80 -1 8 15 1.50 3.00 0 -8 -15 4.40 3.50 0 8 15 -0.20 2.90 0 8 15 -2.20 3.50 0 8 15 0.60 2.00 -1 -8 -15 0.80 3.00 1 8 15 1.10 2.00 1 8 15 1.10 3.40 1 8 15 2.70 3.00 -2 -8 -15 -0.90 2.80 2 8 15 4.50 1.90 2 8 15 0.40 2.80 2 8 15 -0.60 3.00 -3 -8 -15 2.80 2.80 3 8 15 2.40 2.70 3 8 15 0.40 1.90 3 8 15 0.50 3.00 -4 -8 -15 -2.80 1.90 -4 -8 -15 -0.60 2.50 4 8 15 -2.70 1.60 4 8 15 3.80 3.10 4 8 15 0.50 2.60 -5 -8 -15 0.80 2.10 -5 -8 -15 -0.80 2.50 5 8 15 2.50 2.70 5 8 15 4.20 3.30 5 8 15 2.80 2.00 -6 -8 -15 0.40 2.10 -6 -8 -15 1.20 2.40 -6 -8 -15 -2.50 3.60 6 8 15 0.80 3.30 6 8 15 -1.10 2.70 6 8 15 -1.50 1.90 1 -9 -15 2.90 3.90 -1 9 15 4.30 4.00 -1 9 15 1.50 3.30 0 -9 -15 1.70 3.40 0 9 15 1.10 3.00 0 9 15 1.20 3.60 0 9 15 0.70 2.10 -1 -9 -15 -0.20 3.40 1 9 15 2.00 2.00 1 9 15 0.10 2.80 1 9 15 2.60 3.30 -2 -9 -15 -4.90 3.00 2 9 15 1.80 2.90 2 9 15 3.70 2.00 2 9 15 0.40 2.70 -3 -9 -15 0.70 3.00 3 9 15 -0.10 2.70 3 9 15 2.00 2.90 3 9 15 -0.60 1.70 -4 -9 -15 -0.30 2.10 -4 -9 -15 2.00 2.90 4 9 15 0.10 3.20 4 9 15 2.00 2.80 4 9 15 3.10 2.00 -5 -9 -15 1.20 2.10 -5 -9 -15 0.20 2.60 5 9 15 -0.70 2.70 5 9 15 -0.10 1.80 5 9 15 -0.60 3.20 -6 -9 -15 -0.40 2.30 -6 -9 -15 3.70 2.60 6 9 15 0.00 1.90 6 9 15 1.10 3.30 6 9 15 0.70 2.80 0 -10 -15 2.90 4.00 0 10 15 -1.30 3.00 0 10 15 -0.70 2.20 0 10 15 1.60 3.70 -1 -10 -15 -1.40 3.50 1 10 15 0.60 2.90 1 10 15 -0.10 3.20 1 10 15 1.10 2.10 -2 -10 -15 -1.20 3.50 2 10 15 -0.40 2.90 2 10 15 4.40 3.20 2 10 15 -1.30 1.90 -3 -10 -15 2.60 3.20 3 10 15 -0.20 3.20 3 10 15 -0.50 2.80 3 10 15 -0.80 1.80 -4 -10 -15 -0.70 2.30 -4 -10 -15 -0.70 3.00 4 10 15 2.50 2.80 4 10 15 0.20 1.90 4 10 15 3.10 3.20 -5 -10 -15 0.30 2.40 -5 -10 -15 -1.00 2.90 5 10 15 -2.80 3.20 5 10 15 2.30 2.90 5 10 15 2.20 1.90 -2 -11 -15 -0.30 3.70 2 11 15 -0.50 2.20 2 11 15 4.20 3.30 2 11 15 5.80 3.20 -3 -11 -15 -1.90 3.40 3 11 15 0.70 3.20 3 11 15 -1.70 3.20 3 11 15 1.10 2.10 -4 -11 -15 0.50 3.30 -4 -11 -15 1.80 2.50 4 11 15 -0.40 3.30 4 11 15 0.30 2.00 4 11 15 -0.80 3.10 -2 -5 -16 0.90 2.90 2 5 16 3.90 4.20 2 5 16 -0.30 3.50 -3 -5 -16 -1.30 2.80 3 5 16 1.80 3.90 3 5 16 1.60 3.30 -2 -6 -16 -1.80 3.00 2 6 16 0.70 4.00 2 6 16 -0.30 3.30 -3 -6 -16 -0.10 2.80 3 6 16 -2.00 3.20 3 6 16 -2.00 3.70 -4 -6 -16 1.00 2.80 4 6 16 -1.10 1.90 4 6 16 0.30 3.10 4 6 16 1.20 3.70 -2 -7 -16 -1.70 3.00 2 7 16 -3.00 3.80 2 7 16 -0.50 3.30 2 7 16 -0.40 2.00 -3 -7 -16 0.80 2.90 3 7 16 -1.00 2.00 3 7 16 0.10 3.70 3 7 16 0.20 3.10 4 7 16 1.00 3.10 4 7 16 -2.20 1.90 4 7 16 3.00 3.60 3 8 16 -0.70 3.30 3 8 16 2.90 2.30 3 8 16 5.90 3.80 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 54472 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N1 N 0.1087(4) 0.1270(4) 0.7335(4) 0.0656(11) Uani 1 1 d . . . . . C2 C 0.1771(4) 0.1148(4) 0.6274(4) 0.0510(10) Uani 1 1 d . . . . . C5 C 0.3138(4) 0.1386(4) 0.4027(4) 0.0497(10) Uani 1 1 d . . . . . H5 H 0.359255 0.145234 0.326505 0.060 Uiso 1 1 calc R . . . . C25 C 0.3571(4) 0.3513(4) 0.3406(4) 0.0514(10) Uani 1 1 d . . . . . C6 C 0.2677(4) 0.0290(4) 0.4827(4) 0.0477(10) Uani 1 1 d . . . . . C1 C 0.2010(4) 0.0129(4) 0.5997(4) 0.0511(10) Uani 1 1 d . . . . . C4 C 0.2964(4) 0.2396(4) 0.4292(4) 0.0492(10) Uani 1 1 d . . . . . C7 C 0.2911(4) -0.0708(4) 0.4407(4) 0.0507(10) Uani 1 1 d . . . . . C19 C 0.1729(4) 0.3128(4) 0.5985(4) 0.0543(11) Uani 1 1 d . . . . . C12 C 0.4258(5) -0.0991(4) 0.3874(4) 0.0573(11) Uani 1 1 d . . . . . H12 H 0.503470 -0.060568 0.385404 0.069 Uiso 1 1 calc R . . . . C3 C 0.2219(4) 0.2272(4) 0.5432(4) 0.0497(10) Uani 1 1 d . . . . . C11 C 0.4447(6) -0.1829(4) 0.3381(5) 0.0711(14) Uani 1 1 d . . . . . H11 H 0.534641 -0.200034 0.301686 0.085 Uiso 1 1 calc R . . . . C26 C 0.4551(5) 0.4070(4) 0.3653(4) 0.0616(12) Uani 1 1 d . . . . . H26 H 0.482732 0.373855 0.439781 0.074 Uiso 1 1 calc R . . . . C24 C 0.1022(4) 0.2467(5) 0.7150(5) 0.0642(13) Uani 1 1 d . . . . . C31 C 0.5279(5) 0.6808(4) 0.0836(4) 0.0568(11) Uani 1 1 d . . . . . C13 C 0.1666(4) -0.1083(4) 0.6892(4) 0.0538(11) Uani 1 1 d . . . . . C23 C 0.0299(6) 0.2999(5) 0.7944(5) 0.0783(15) Uani 1 1 d . . . . . H23 H -0.019044 0.255373 0.869442 0.094 Uiso 1 1 calc R . . . . C9 C 0.1976(6) -0.2172(4) 0.3972(5) 0.0713(14) Uani 1 1 d . . . . . H9 H 0.120810 -0.258055 0.401723 0.086 Uiso 1 1 calc R . . . . C28 C 0.4743(4) 0.5653(4) 0.1699(4) 0.0531(10) Uani 1 1 d . . . . . C29 C 0.3792(5) 0.5067(5) 0.1449(4) 0.0701(14) Uani 1 1 d . . . . . H29 H 0.352019 0.539355 0.070347 0.084 Uiso 1 1 calc R . . . . C27 C 0.5119(4) 0.5104(4) 0.2817(4) 0.0598(12) Uani 1 1 d . . . . . H27 H 0.578164 0.544770 0.301031 0.072 Uiso 1 1 calc R . . . . C8 C 0.1787(5) -0.1323(4) 0.4451(4) 0.0600(12) Uani 1 1 d . . . . . H8 H 0.088396 -0.115574 0.481388 0.072 Uiso 1 1 calc R . . . . C36 C 0.4440(6) 0.7650(5) 0.0074(5) 0.0789(15) Uani 1 1 d . . . . . H36 H 0.352703 0.746719 0.009975 0.095 Uiso 1 1 calc R . . . . C10 C 0.3303(7) -0.2419(5) 0.3425(5) 0.0793(16) Uani 1 1 d . . . . . H10 H 0.343112 -0.298339 0.308489 0.095 Uiso 1 1 calc R . . . . C30 C 0.3249(5) 0.4028(4) 0.2268(4) 0.0680(13) Uani 1 1 d . . . . . H30 H 0.264118 0.365341 0.205313 0.082 Uiso 1 1 calc R . . . . C14 C 0.2754(5) -0.1882(5) 0.7329(4) 0.0675(12) Uani 1 1 d . . . . . H14 H 0.368114 -0.164489 0.705826 0.081 Uiso 1 1 calc R . . . . C35 C 0.4912(7) 0.8739(5) -0.0713(6) 0.0897(17) Uani 1 1 d . . . . . H35 H 0.432355 0.928002 -0.120927 0.108 Uiso 1 1 calc R . . . . C20 C 0.1730(5) 0.4341(5) 0.5629(5) 0.0733(14) Uani 1 1 d . . . . . H20 H 0.216425 0.481048 0.486584 0.088 Uiso 1 1 calc R . . . . C15 C 0.2516(7) -0.3003(5) 0.8141(5) 0.0821(15) Uani 1 1 d . . . . . H15 H 0.327769 -0.351308 0.841822 0.098 Uiso 1 1 calc R . . . . C16 C 0.1193(9) -0.3384(6) 0.8548(6) 0.0954(19) Uani 1 1 d . . . . . H16 H 0.103723 -0.415327 0.910045 0.115 Uiso 1 1 calc R . . . . C18 C 0.0298(5) -0.1467(5) 0.7308(5) 0.0846(17) Uani 1 1 d . . . . . H18 H -0.046847 -0.096023 0.703606 0.102 Uiso 1 1 calc R . . . . C21 C 0.1061(6) 0.4845(6) 0.6448(6) 0.0895(17) Uani 1 1 d . . . . . H21 H 0.109595 0.565803 0.623259 0.107 Uiso 1 1 calc R . . . . C34 C 0.6253(7) 0.9022(6) -0.0764(6) 0.0905(17) Uani 1 1 d . . . . . H34 H 0.658880 0.975310 -0.130060 0.109 Uiso 1 1 calc R . . . . C22 C 0.0353(7) 0.4180(6) 0.7562(6) 0.0930(18) Uani 1 1 d . . . . . H22 H -0.010215 0.456088 0.806478 0.112 Uiso 1 1 calc R . . . . C32 C 0.6612(6) 0.7124(5) 0.0745(5) 0.0848(16) Uani 1 1 d . . . . . H32 H 0.722115 0.657826 0.121653 0.102 Uiso 1 1 calc R . . . . C17 C 0.0083(7) -0.2630(6) 0.8142(6) 0.103(2) Uani 1 1 d . . . . . H17 H -0.083412 -0.289057 0.842384 0.124 Uiso 1 1 calc R . . . . C33 C 0.7088(7) 0.8224(6) -0.0022(7) 0.103(2) Uani 1 1 d . . . . . H33 H 0.798741 0.842111 -0.003065 0.123 Uiso 1 1 calc R . . . . C37 C 0.0448(9) 0.0401(7) 0.8437(6) 0.122(3) Uani 1 1 d . . . . . H37A H -0.020473 -0.002246 0.828396 0.184 Uiso 1 1 calc GR . . . . H37B H -0.005221 0.078801 0.895341 0.184 Uiso 1 1 calc GR . . . . H37C H 0.117075 -0.014649 0.881392 0.184 Uiso 1 1 calc GR . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N1 0.071(2) 0.068(3) 0.056(2) -0.023(2) -0.0002(18) -0.021(2) C2 0.051(2) 0.048(2) 0.052(3) -0.016(2) -0.0068(19) -0.0085(19) C5 0.048(2) 0.053(3) 0.047(2) -0.018(2) -0.0041(18) -0.0070(19) C25 0.057(2) 0.043(2) 0.053(3) -0.018(2) -0.0057(19) -0.0066(19) C6 0.043(2) 0.046(2) 0.053(3) -0.015(2) -0.0084(18) -0.0085(18) C1 0.045(2) 0.051(3) 0.052(3) -0.012(2) -0.0086(18) -0.0095(18) C4 0.049(2) 0.045(2) 0.050(3) -0.012(2) -0.0115(18) -0.0068(18) C7 0.051(2) 0.049(3) 0.050(2) -0.016(2) -0.0117(19) -0.0008(19) C19 0.048(2) 0.052(3) 0.070(3) -0.027(2) -0.020(2) 0.0013(19) C12 0.061(3) 0.051(3) 0.060(3) -0.019(2) -0.015(2) -0.003(2) C3 0.047(2) 0.045(2) 0.057(3) -0.017(2) -0.0111(19) -0.0082(18) C11 0.083(3) 0.055(3) 0.071(3) -0.022(3) -0.020(3) 0.015(3) C26 0.071(3) 0.053(3) 0.061(3) -0.012(2) -0.025(2) -0.014(2) C24 0.053(2) 0.079(4) 0.070(3) -0.039(3) -0.007(2) -0.013(2) C31 0.070(3) 0.046(3) 0.052(3) -0.016(2) -0.007(2) -0.011(2) C13 0.057(3) 0.050(3) 0.053(3) -0.015(2) -0.010(2) -0.013(2) C23 0.089(4) 0.078(4) 0.075(4) -0.040(3) -0.004(3) -0.010(3) C9 0.080(3) 0.051(3) 0.093(4) -0.029(3) -0.032(3) -0.001(2) C28 0.060(2) 0.044(2) 0.052(3) -0.015(2) -0.0051(19) -0.0079(19) C29 0.088(3) 0.064(3) 0.053(3) -0.005(3) -0.026(2) -0.024(3) C27 0.061(3) 0.055(3) 0.068(3) -0.021(3) -0.020(2) -0.010(2) C8 0.064(3) 0.047(3) 0.071(3) -0.020(2) -0.021(2) -0.003(2) C36 0.087(3) 0.060(3) 0.076(4) -0.001(3) -0.025(3) -0.025(3) C10 0.122(5) 0.051(3) 0.073(4) -0.025(3) -0.036(3) 0.004(3) C30 0.084(3) 0.060(3) 0.063(3) -0.013(3) -0.027(2) -0.025(2) C14 0.066(3) 0.061(3) 0.060(3) -0.009(3) -0.008(2) -0.006(2) C35 0.113(5) 0.061(3) 0.079(4) 0.000(3) -0.031(3) -0.016(3) C20 0.075(3) 0.057(3) 0.094(4) -0.032(3) -0.019(3) -0.004(2) C15 0.105(4) 0.056(3) 0.073(4) -0.012(3) -0.022(3) 0.004(3) C16 0.143(6) 0.056(3) 0.078(4) -0.006(3) -0.029(4) -0.023(4) C18 0.061(3) 0.088(4) 0.090(4) -0.010(4) -0.012(3) -0.033(3) C21 0.104(4) 0.080(4) 0.095(5) -0.046(4) -0.015(4) 0.000(3) C34 0.118(5) 0.063(4) 0.074(4) -0.005(3) -0.012(3) -0.029(4) C22 0.102(4) 0.096(5) 0.090(5) -0.053(4) -0.002(3) -0.002(4) C32 0.074(3) 0.071(4) 0.088(4) -0.002(3) -0.017(3) -0.018(3) C17 0.102(5) 0.104(5) 0.091(5) -0.013(4) -0.003(4) -0.069(4) C33 0.092(4) 0.075(4) 0.113(5) 0.001(4) -0.014(4) -0.036(3) C37 0.180(7) 0.114(6) 0.065(4) -0.038(4) 0.033(4) -0.054(5) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C2 N1 C37 130.1(4) . . ? C24 N1 C2 108.1(4) . . ? C24 N1 C37 121.8(4) . . ? N1 C2 C1 129.3(4) . . ? N1 C2 C3 108.8(3) . . ? C1 C2 C3 122.0(4) . . ? C6 C5 C4 123.9(4) . . ? C26 C25 C4 121.6(4) . . ? C30 C25 C4 121.9(3) . . ? C30 C25 C26 116.5(4) . . ? C5 C6 C1 120.7(4) . . ? C5 C6 C7 117.9(4) . . ? C1 C6 C7 121.4(4) . . ? C2 C1 C13 123.2(4) . . ? C6 C1 C2 116.4(4) . . ? C6 C1 C13 120.2(4) . . ? C5 C4 C25 120.1(4) . . ? C5 C4 C3 116.3(4) . . ? C3 C4 C25 123.5(3) . . ? C12 C7 C6 120.7(3) . . ? C8 C7 C6 121.0(4) . . ? C8 C7 C12 118.1(4) . . ? C24 C19 C3 105.6(4) . . ? C20 C19 C3 136.1(5) . . ? C20 C19 C24 118.2(4) . . ? C11 C12 C7 120.7(4) . . ? C2 C3 C19 107.4(4) . . ? C4 C3 C2 120.5(4) . . ? C4 C3 C19 132.1(4) . . ? C12 C11 C10 120.1(5) . . ? C27 C26 C25 121.0(4) . . ? N1 C24 C19 110.0(4) . . ? N1 C24 C23 126.9(5) . . ? C23 C24 C19 122.9(5) . . ? C36 C31 C28 121.7(4) . . ? C32 C31 C28 122.3(5) . . ? C32 C31 C36 116.0(5) . . ? C14 C13 C1 119.2(4) . . ? C14 C13 C18 117.4(5) . . ? C18 C13 C1 123.4(4) . . ? C22 C23 C24 116.5(6) . . ? C8 C9 C10 119.8(4) . . ? C29 C28 C31 121.9(4) . . ? C27 C28 C31 122.2(3) . . ? C27 C28 C29 115.8(4) . . ? C30 C29 C28 121.8(4) . . ? C26 C27 C28 122.5(4) . . ? C9 C8 C7 121.4(5) . . ? C35 C36 C31 122.4(5) . . ? C9 C10 C11 120.0(4) . . ? C29 C30 C25 122.2(4) . . ? C15 C14 C13 122.3(5) . . ? C34 C35 C36 119.6(6) . . ? C19 C20 C21 118.0(5) . . ? C16 C15 C14 120.7(6) . . ? C15 C16 C17 119.3(6) . . ? C13 C18 C17 119.1(6) . . ? C22 C21 C20 122.3(6) . . ? C33 C34 C35 119.2(6) . . ? C23 C22 C21 122.0(5) . . ? C31 C32 C33 122.2(6) . . ? C16 C17 C18 121.2(5) . . ? C34 C33 C32 120.6(6) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N1 C2 1.397(5) . ? N1 C24 1.392(6) . ? N1 C37 1.430(8) . ? C2 C1 1.406(6) . ? C2 C3 1.416(6) . ? C5 C6 1.380(6) . ? C5 C4 1.388(5) . ? C25 C4 1.475(6) . ? C25 C26 1.387(5) . ? C25 C30 1.382(6) . ? C6 C1 1.403(6) . ? C6 C7 1.489(6) . ? C1 C13 1.490(6) . ? C4 C3 1.402(6) . ? C7 C12 1.396(6) . ? C7 C8 1.384(6) . ? C19 C3 1.452(6) . ? C19 C24 1.417(7) . ? C19 C20 1.376(7) . ? C12 C11 1.370(6) . ? C11 C10 1.382(8) . ? C26 C27 1.373(7) . ? C24 C23 1.410(7) . ? C31 C28 1.477(6) . ? C31 C36 1.393(7) . ? C31 C32 1.364(7) . ? C13 C14 1.380(7) . ? C13 C18 1.386(6) . ? C23 C22 1.341(9) . ? C9 C8 1.370(6) . ? C9 C10 1.374(8) . ? C28 C29 1.390(6) . ? C28 C27 1.383(6) . ? C29 C30 1.362(7) . ? C36 C35 1.373(8) . ? C14 C15 1.359(7) . ? C35 C34 1.369(8) . ? C20 C21 1.398(7) . ? C15 C16 1.343(9) . ? C16 C17 1.362(9) . ? C18 C17 1.402(9) . ? C21 C22 1.376(10) . ? C34 C33 1.358(9) . ? C32 C33 1.378(8) . ?