#------------------------------------------------------------------------------ #$Date: 2024-07-05 20:58:16 +0300 (Fri, 05 Jul 2024) $ #$Revision: 293262 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/98/7159898.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7159898 loop_ _publ_author_name 'Yaragorla, Srinivasarao' 'Khan, Tabassum' 'Chakroborty, Sayonika' _publ_section_title ; Cu(OTf)2/HFIP catalyzed regioselective cycloisomerization of indole-C3-functionalized alkynols to carbazoles. ; _journal_issue 18 _journal_name_full 'Organic & biomolecular chemistry' _journal_page_first 3622 _journal_page_last 3629 _journal_paper_doi 10.1039/d4ob00421c _journal_volume 22 _journal_year 2024 _chemical_formula_moiety 'C35 H28 N2' _chemical_formula_sum 'C35 H28 N2' _chemical_formula_weight 476.59 _space_group_crystal_system monoclinic _space_group_IT_number 14 _space_group_name_Hall '-P 2yn' _space_group_name_H-M_alt 'P 1 21/n 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary iterative _audit_creation_date 2023-09-14 _audit_creation_method ; Olex2 1.3-ac4 (compiled 2018.12.18 svn.r3554 for Rigaku Oxford Diffraction, GUI svn.r1) ; _audit_update_record ; 2023-09-14 deposited with the CCDC. 2024-04-15 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 98.298(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 10.7077(8) _cell_length_b 9.2729(7) _cell_length_c 25.954(2) _cell_measurement_reflns_used 9251 _cell_measurement_temperature 298(2) _cell_measurement_theta_max 27.11 _cell_measurement_theta_min 2.34 _cell_volume 2550.0(3) _computing_cell_refinement 'SAINT V8.40B (?, 2016)' _computing_data_reduction 'SAINT V8.40B (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'ShelXL (Sheldrick, 2015)' _computing_structure_solution 'olex2.solve (Bourhis et al., 2015)' _diffrn_ambient_temperature 298.0 _diffrn_measured_fraction_theta_full 1.000 _diffrn_measured_fraction_theta_max 0.998 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0548 _diffrn_reflns_av_unetI/netI 0.0313 _diffrn_reflns_Laue_measured_fraction_full 1.000 _diffrn_reflns_Laue_measured_fraction_max 0.998 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_k_min -12 _diffrn_reflns_limit_l_max 33 _diffrn_reflns_limit_l_min -33 _diffrn_reflns_number 50346 _diffrn_reflns_point_group_measured_fraction_full 1.000 _diffrn_reflns_point_group_measured_fraction_max 0.998 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 27.539 _diffrn_reflns_theta_min 1.586 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.072 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.5022 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.1429 before and 0.0730 after correction. The Ratio of minimum to maximum transmission is 0.6736. The \l/2 correction factor is Not present. ; _exptl_crystal_colour 'clear light colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier light _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.241 _exptl_crystal_description plate _exptl_crystal_F_000 1008 _exptl_crystal_size_max 0.21 _exptl_crystal_size_mid 0.17 _exptl_crystal_size_min 0.11 _refine_diff_density_max 0.276 _refine_diff_density_min -0.200 _refine_diff_density_rms 0.051 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.064 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 337 _refine_ls_number_reflns 5871 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.064 _refine_ls_R_factor_all 0.0667 _refine_ls_R_factor_gt 0.0514 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0703P)^2^+0.6734P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1382 _refine_ls_wR_factor_ref 0.1462 _reflns_Friedel_coverage 0.000 _reflns_number_gt 4500 _reflns_number_total 5871 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ob00421c2.cif _cod_data_source_block ysr032_0m_a _cod_depositor_comments 'Adding full bibliography for 7159896--7159898.cif.' _cod_database_code 7159898 _shelx_shelxl_version_number 2018/3 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.992 _shelx_estimated_absorpt_t_min 0.985 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups At 1.5 times of: All C(H,H,H) groups 2.a Aromatic/amide H refined with riding coordinates: C3(H3), C25(H25), C24(H24), C14(H14), C20(H20), C11(H11), C18(H18), C23(H23), C8(H8), C31(H31), C21(H21), C15(H15), C9(H9), C10(H10), C28(H28), C17(H17), C30(H30), C16(H16), C29(H29) 2.b Idealised Me refined as rotating group: C33(H33A,H33B,H33C), C35(H35A,H35B,H35C), C34(H34A,H34B,H34C) ; _shelx_res_file ; TITL YSR032_0m_a.res in P2(1)/n ysr032_0m_a.res created by SHELXL-2018/3 at 10:49:22 on 14-Sep-2023 CELL 0.71073 10.7077 9.2729 25.9536 90 98.298 90 ZERR 4 0.0008 0.0007 0.002 0 0.003 0 LATT 1 SYMM 0.5-X,0.5+Y,0.5-Z SFAC C H N UNIT 140 112 8 L.S. 10 PLAN 20 SIZE 0.17 0.11 0.21 TEMP 24.85 BOND fmap 2 acta REM REM REM WGHT 0.070300 0.673400 FVAR 0.49325 N1 3 0.634335 0.597763 0.685099 11.00000 0.05187 0.04301 = 0.03662 -0.00869 0.00920 0.00152 N2 3 0.429479 0.314622 0.536229 11.00000 0.03900 0.04824 = 0.03888 -0.00313 0.00907 0.00315 C5 1 0.581720 0.221418 0.492804 11.00000 0.04224 0.03320 = 0.02977 0.00133 0.00508 0.00016 C2 1 0.780374 0.336287 0.562460 11.00000 0.04216 0.03866 = 0.02847 -0.00065 0.00547 0.00036 C6 1 0.559311 0.303334 0.536772 11.00000 0.03936 0.03550 = 0.03215 0.00162 0.00974 0.00276 C27 1 0.595240 0.363202 0.667587 11.00000 0.03982 0.04597 = 0.03345 -0.00545 0.00804 -0.00354 C12 1 0.459582 0.173906 0.467117 11.00000 0.04298 0.03537 = 0.03442 0.00294 0.00365 -0.00195 C1 1 0.657517 0.356934 0.573777 11.00000 0.04321 0.03602 = 0.02872 -0.00088 0.00809 0.00129 C19 1 0.893536 0.387126 0.598009 11.00000 0.03838 0.04168 = 0.03172 -0.00507 0.00776 0.00448 C26 1 0.636244 0.428921 0.623013 11.00000 0.03857 0.04218 = 0.03228 -0.00447 0.00729 0.00149 C32 1 0.595619 0.471932 0.705679 11.00000 0.03604 0.04838 = 0.03413 -0.00538 0.00623 0.00077 C13 1 0.738325 0.128720 0.435303 11.00000 0.04362 0.04056 = 0.03227 -0.00386 0.01032 -0.00227 C4 1 0.706108 0.204551 0.482163 11.00000 0.04436 0.03571 = 0.02965 -0.00002 0.00718 0.00356 C7 1 0.369562 0.238193 0.494118 11.00000 0.04286 0.04356 = 0.03773 0.00505 0.00558 -0.00302 C3 1 0.801747 0.264347 0.517011 11.00000 0.03909 0.04613 = 0.03230 -0.00318 0.00842 0.00268 AFIX 43 H3 2 0.884243 0.256541 0.510008 11.00000 -1.20000 AFIX 0 C25 1 0.659098 0.569797 0.635673 11.00000 0.04622 0.04154 = 0.03523 -0.00152 0.00907 0.00201 AFIX 43 H25 2 0.687637 0.637889 0.613784 11.00000 -1.20000 AFIX 0 C24 1 0.924050 0.332975 0.648074 11.00000 0.05051 0.05516 = 0.03451 0.00221 0.00614 -0.00585 AFIX 43 H24 2 0.869766 0.268209 0.660886 11.00000 -1.20000 AFIX 0 C14 1 0.676549 0.160144 0.385731 11.00000 0.05343 0.05622 = 0.03482 -0.00364 0.00622 0.00484 AFIX 43 H14 2 0.612940 0.229239 0.381456 11.00000 -1.20000 AFIX 0 C20 1 0.976453 0.485140 0.580994 11.00000 0.04337 0.06029 = 0.03636 0.00793 0.00450 -0.00065 AFIX 43 H20 2 0.958681 0.522886 0.547540 11.00000 -1.20000 AFIX 0 C11 1 0.417905 0.080072 0.426001 11.00000 0.05488 0.03976 = 0.04250 -0.00133 0.00191 -0.00647 AFIX 43 H11 2 0.475741 0.031277 0.408889 11.00000 -1.20000 AFIX 0 C18 1 0.835013 0.027546 0.439946 11.00000 0.05130 0.05457 = 0.03812 -0.00368 0.00892 0.00742 AFIX 43 H18 2 0.879514 0.007550 0.472645 11.00000 -1.20000 AFIX 0 C22 1 1.116401 0.472308 0.662174 11.00000 0.03829 0.06647 = 0.03881 -0.00828 0.00567 0.00271 C23 1 1.034079 0.374062 0.679141 11.00000 0.05174 0.07086 = 0.02928 0.00191 0.00322 0.00119 AFIX 43 H23 2 1.053264 0.334666 0.712292 11.00000 -1.20000 AFIX 0 C8 1 0.240486 0.222045 0.478138 11.00000 0.04070 0.06341 = 0.05389 0.00566 0.00854 -0.00584 AFIX 43 H8 2 0.181772 0.269213 0.495268 11.00000 -1.20000 AFIX 0 C31 1 0.560506 0.444967 0.754411 11.00000 0.05037 0.07026 = 0.03531 -0.00825 0.01094 -0.00006 AFIX 43 H31 2 0.560929 0.517952 0.779013 11.00000 -1.20000 AFIX 0 C21 1 1.084693 0.527764 0.612662 11.00000 0.04249 0.06572 = 0.05120 0.00413 0.00816 -0.00833 AFIX 43 H21 2 1.137475 0.595320 0.600406 11.00000 -1.20000 AFIX 0 C15 1 0.709172 0.089207 0.342734 11.00000 0.07014 0.08142 = 0.03237 -0.00887 0.00547 0.00301 AFIX 43 H15 2 0.667094 0.110906 0.309752 11.00000 -1.20000 AFIX 0 C9 1 0.202739 0.133633 0.436006 11.00000 0.04709 0.06738 = 0.06055 0.00788 0.00077 -0.01832 AFIX 43 H9 2 0.117133 0.122639 0.424041 11.00000 -1.20000 AFIX 0 C10 1 0.290402 0.060818 0.411179 11.00000 0.06171 0.05147 = 0.04982 -0.00221 -0.00093 -0.01804 AFIX 43 H10 2 0.262442 -0.002089 0.384047 11.00000 -1.20000 AFIX 0 C28 1 0.558621 0.224171 0.679575 11.00000 0.07783 0.05221 = 0.05126 -0.00851 0.01972 -0.01758 AFIX 43 H28 2 0.557304 0.150282 0.655273 11.00000 -1.20000 AFIX 0 C33 1 0.643603 0.737500 0.710359 11.00000 0.08092 0.05099 = 0.05338 -0.01881 0.01187 0.00107 AFIX 137 H33A 2 0.560507 0.772368 0.713295 11.00000 -1.50000 H33B 2 0.684959 0.804036 0.690062 11.00000 -1.50000 H33C 2 0.691481 0.728671 0.744453 11.00000 -1.50000 AFIX 0 C17 1 0.866254 -0.043927 0.396837 11.00000 0.06515 0.06520 = 0.05640 -0.01313 0.01770 0.01605 AFIX 43 H17 2 0.929995 -0.112874 0.400792 11.00000 -1.20000 AFIX 0 C35 1 0.360702 0.406340 0.567697 11.00000 0.04675 0.07614 = 0.05617 -0.01425 0.01226 0.01276 AFIX 137 H35A 2 0.324131 0.348240 0.592247 11.00000 -1.50000 H35B 2 0.295011 0.456211 0.545579 11.00000 -1.50000 H35C 2 0.417472 0.475239 0.586080 11.00000 -1.50000 AFIX 0 C30 1 0.525316 0.307107 0.764831 11.00000 0.07492 0.08552 = 0.04180 0.00469 0.02186 -0.01331 AFIX 43 H30 2 0.501617 0.286124 0.797098 11.00000 -1.20000 AFIX 0 C16 1 0.803279 -0.013202 0.348224 11.00000 0.07469 0.07914 = 0.04685 -0.02260 0.02022 0.00430 AFIX 43 H16 2 0.824017 -0.061235 0.319164 11.00000 -1.20000 AFIX 0 C34 1 1.236761 0.514621 0.696082 11.00000 0.04969 0.11588 = 0.05370 -0.00366 -0.00260 -0.01210 AFIX 137 H34A 2 1.219956 0.591537 0.718870 11.00000 -1.50000 H34B 2 1.297313 0.546233 0.674597 11.00000 -1.50000 H34C 2 1.269839 0.433100 0.716422 11.00000 -1.50000 AFIX 0 C29 1 0.524432 0.197823 0.727911 11.00000 0.09662 0.06690 = 0.06209 0.00175 0.03033 -0.02705 AFIX 43 H29 2 0.500275 0.105210 0.736057 11.00000 -1.20000 AFIX 0 HKLF 4 REM YSR032_0m_a.res in P2(1)/n REM wR2 = 0.1462, GooF = S = 1.064, Restrained GooF = 1.064 for all data REM R1 = 0.0514 for 4500 Fo > 4sig(Fo) and 0.0667 for all 5871 data REM 337 parameters refined using 0 restraints END WGHT 0.0699 0.6736 REM Highest difference peak 0.276, deepest hole -0.200, 1-sigma level 0.051 Q1 1 1.2377 0.4799 0.7387 11.00000 0.05 0.28 Q2 1 0.6139 0.3953 0.6928 11.00000 0.05 0.25 Q3 1 1.3217 0.4390 0.6852 11.00000 0.05 0.25 Q4 1 0.3987 0.3867 0.6042 11.00000 0.05 0.23 Q5 1 0.9128 0.4826 0.5983 11.00000 0.05 0.22 Q6 1 0.9596 0.3956 0.6686 11.00000 0.05 0.22 Q7 1 0.5273 0.1845 0.4775 11.00000 0.05 0.22 Q8 1 0.7236 -0.0164 0.3533 11.00000 0.05 0.21 Q9 1 0.6078 0.3807 0.6393 11.00000 0.05 0.21 Q10 1 0.6177 0.2870 0.6778 11.00000 0.05 0.20 Q11 1 0.8399 0.3598 0.5807 11.00000 0.05 0.20 Q12 1 0.5475 0.4653 0.7218 11.00000 0.05 0.19 Q13 1 0.6169 0.4335 0.7326 11.00000 0.05 0.19 Q14 1 0.5681 0.2190 0.5234 11.00000 0.05 0.19 Q15 1 0.9550 0.3974 0.5875 11.00000 0.05 0.19 Q16 1 0.7933 0.0828 0.3433 11.00000 0.05 0.19 Q17 1 0.9783 0.5266 0.6105 11.00000 0.05 0.19 Q18 1 1.1045 0.3914 0.6653 11.00000 0.05 0.19 Q19 1 0.9172 0.3320 0.6164 11.00000 0.05 0.19 Q20 1 0.6989 0.1382 0.4113 11.00000 0.05 0.19 ; _shelx_res_checksum 63261 _shelx_hkl_file ; -1 0 0 0.30 0.10 -1 0 0 0.20 0.10 1 0 0 0.40 0.10 -2 0 0 105.39 5.90 2 0 0 103.89 5.90 -2 0 0 109.79 5.90 -3 0 0 0.20 0.30 -3 0 0 -0.20 0.30 3 0 0 -0.20 0.50 4 0 0 718.03 39.10 -4 0 0 692.53 39.10 -4 0 0 718.13 39.10 5 0 0 0.30 0.40 5 0 0 0.70 0.90 -5 0 0 -0.10 0.60 -5 0 0 0.60 0.50 -6 0 0 289.57 15.80 6 0 0 287.27 15.70 6 0 0 267.77 15.70 -6 0 0 292.37 15.80 -7 0 0 0.10 0.70 7 0 0 1.60 0.60 7 0 0 -0.20 0.60 -7 0 0 0.00 0.80 8 0 0 19.10 1.60 8 0 0 21.70 1.60 -8 0 0 18.30 1.70 -8 0 0 22.90 2.00 9 0 0 0.50 0.80 -9 0 0 0.50 1.00 -9 0 0 0.50 1.20 9 0 0 -0.20 1.50 -10 0 0 2.80 1.40 10 0 0 1.80 1.00 10 0 0 3.20 1.00 -10 0 0 1.40 1.10 10 0 0 4.90 1.80 -11 0 0 1.30 1.30 11 0 0 1.00 1.10 11 0 0 1.60 1.00 12 0 0 6.30 1.50 12 0 0 7.40 1.50 13 0 0 1.10 1.70 -13 0 0 2.40 1.90 13 0 0 3.70 1.70 0 -1 0 0.40 0.10 0 -1 0 0.20 0.20 0 -1 0 0.50 0.10 0 -1 0 0.20 0.30 0 -1 0 0.00 0.10 0 -1 0 0.20 0.10 0 -1 0 0.10 0.30 0 1 0 0.00 0.10 0 1 0 0.00 0.10 0 1 0 0.30 0.20 0 1 0 0.00 0.10 0 1 0 0.50 0.20 0 1 0 0.10 0.20 -1 -1 0 21.70 1.20 1 -1 0 20.80 1.20 1 -1 0 19.50 1.20 1 -1 0 21.30 1.20 1 -1 0 21.70 1.20 -1 1 0 21.50 1.20 -1 1 0 21.50 1.20 1 1 0 18.40 1.40 -1 1 0 20.30 1.20 -1 1 0 21.00 1.20 -1 1 0 19.70 1.20 1 1 0 22.80 1.20 2 -1 0 16.00 0.90 2 -1 0 16.10 0.90 2 -1 0 15.30 1.00 2 -1 0 15.80 1.00 2 -1 0 15.80 1.00 2 -1 0 16.50 0.90 -2 -1 0 16.80 1.10 -2 1 0 16.00 1.00 -2 1 0 15.70 0.90 -2 1 0 15.00 1.00 -2 1 0 15.20 1.00 -2 1 0 17.10 1.00 -2 1 0 15.90 1.00 -2 1 0 16.60 0.90 3 -1 0 2057.59 109.99 3 -1 0 1916.41 109.99 3 -1 0 2063.69 109.99 3 -1 0 1863.61 109.99 3 -1 0 2098.99 109.99 -3 1 0 1877.41 109.99 -3 1 0 2137.99 109.99 4 -1 0 56.09 3.10 4 -1 0 60.89 3.20 4 -1 0 55.59 3.20 -4 -1 0 53.79 3.30 4 -1 0 53.79 3.30 4 1 0 50.69 3.40 -4 1 0 55.59 3.20 -4 1 0 59.59 3.20 5 -1 0 143.59 8.20 5 -1 0 144.69 8.40 5 -1 0 150.88 8.30 5 -1 0 149.88 8.20 -5 -1 0 151.18 8.40 5 -1 0 144.39 8.20 -5 1 0 156.58 8.30 5 1 0 144.39 8.50 6 -1 0 347.57 18.20 -6 -1 0 330.87 18.30 6 -1 0 318.57 18.20 -6 -1 0 325.87 18.30 6 -1 0 307.17 18.30 6 -1 0 336.07 18.10 6 -1 0 333.07 18.10 -6 1 0 329.87 18.20 -7 -1 0 303.57 16.50 7 -1 0 307.57 16.40 -7 -1 0 288.87 16.50 7 -1 0 299.27 16.40 7 -1 0 290.37 16.30 7 1 0 271.97 16.50 -7 1 0 298.57 16.50 -7 1 0 307.37 16.60 8 -1 0 0.30 0.70 8 -1 0 -0.30 1.00 -8 -1 0 2.20 0.90 8 -1 0 2.00 0.70 8 -1 0 0.00 0.60 -8 -1 0 0.30 0.90 8 -1 0 -0.30 0.60 8 1 0 0.60 0.80 8 1 0 1.30 1.50 -8 1 0 0.30 1.00 -8 1 0 -0.10 0.80 9 -1 0 83.49 5.00 9 -1 0 84.69 5.00 -9 -1 0 82.39 5.20 9 -1 0 92.09 4.90 -9 -1 0 92.79 5.40 -9 1 0 75.99 5.10 9 1 0 88.99 5.10 -9 1 0 79.89 5.20 9 1 0 91.79 5.10 10 -1 0 1.10 0.80 -10 -1 0 -0.60 1.40 -10 -1 0 1.20 1.10 10 -1 0 3.90 1.60 10 -1 0 -0.10 0.90 10 -1 0 1.20 1.00 10 1 0 1.60 1.00 -10 1 0 0.70 1.10 10 1 0 1.90 1.00 -11 -1 0 0.50 1.70 11 -1 0 0.50 1.10 -11 -1 0 -0.90 1.30 11 -1 0 1.40 1.10 11 1 0 1.20 2.00 11 1 0 0.20 1.20 11 1 0 0.40 1.10 -11 1 0 -0.20 1.40 12 -1 0 1.50 1.40 12 -1 0 1.60 1.30 -12 -1 0 1.50 1.50 -12 1 0 -1.00 1.40 12 1 0 0.70 1.50 12 1 0 0.90 1.40 -13 -1 0 2.20 1.70 13 -1 0 5.10 1.70 13 -1 0 3.30 1.70 -13 1 0 5.40 1.80 13 1 0 1.40 1.80 0 -2 0 3.20 0.30 0 -2 0 1.40 0.60 0 -2 0 1.30 0.60 0 -2 0 2.90 0.30 0 -2 0 3.60 0.40 0 -2 0 2.10 0.30 0 -2 0 2.80 0.30 0 -2 0 3.90 0.80 0 2 0 3.50 0.40 0 2 0 3.20 0.40 0 2 0 2.40 0.50 0 2 0 2.50 0.50 -1 -2 0 122.99 6.60 -1 -2 0 113.59 6.60 1 -2 0 119.89 6.60 1 -2 0 111.49 6.60 -1 -2 0 127.09 6.60 1 -2 0 118.29 6.70 1 -2 0 122.09 6.60 1 -2 0 114.89 6.70 -1 -2 0 124.09 6.60 -1 -2 0 103.99 6.80 -1 2 0 113.89 6.60 1 2 0 130.69 6.60 -1 2 0 129.29 6.60 -1 2 0 122.59 6.60 1 2 0 122.99 6.60 1 2 0 102.59 6.80 1 2 0 112.49 6.60 -1 2 0 127.59 6.60 1 2 0 114.59 6.70 2 -2 0 253.07 13.60 -2 -2 0 237.78 13.50 2 -2 0 246.28 13.50 2 -2 0 238.78 13.50 -2 -2 0 240.18 13.80 -2 -2 0 248.88 13.50 2 -2 0 248.08 13.50 2 -2 0 233.08 13.50 2 2 0 223.58 13.70 -2 2 0 245.38 13.50 -2 2 0 245.08 13.50 2 2 0 254.27 13.50 -2 2 0 259.07 13.50 -2 2 0 246.78 13.50 -2 2 0 242.38 13.50 2 2 0 247.98 13.50 2 2 0 238.58 13.60 -2 2 0 251.17 13.50 3 -2 0 397.16 22.10 -3 -2 0 391.56 22.20 3 -2 0 415.46 22.10 3 -2 0 426.46 22.20 3 -2 0 382.76 22.20 -3 2 0 403.46 22.10 -3 2 0 396.96 22.00 -3 2 0 408.96 22.10 3 2 0 424.66 22.10 3 2 0 369.76 22.20 -3 2 0 397.76 22.10 -3 2 0 414.06 22.10 -3 2 0 385.06 22.20 4 -2 0 345.37 17.90 -4 -2 0 283.17 18.00 4 -2 0 316.47 17.90 4 -2 0 316.97 18.00 4 -2 0 337.07 17.90 4 -2 0 318.37 17.90 -4 2 0 327.27 17.90 -4 2 0 325.07 17.90 4 2 0 306.67 18.00 -4 2 0 348.07 17.90 -4 2 0 337.77 17.90 -5 -2 0 125.29 7.60 5 -2 0 127.59 7.60 5 -2 0 134.49 7.50 -5 -2 0 147.49 7.60 5 -2 0 137.99 7.50 5 -2 0 139.49 7.40 5 -2 0 123.99 7.70 5 -2 0 127.49 7.50 -5 2 0 141.19 7.50 -5 2 0 133.29 7.50 -5 2 0 138.59 7.50 6 -2 0 12.00 0.90 6 -2 0 11.50 0.80 6 -2 0 13.50 1.00 -6 -2 0 8.90 1.20 6 -2 0 12.00 0.90 -6 -2 0 13.50 1.50 6 -2 0 11.90 1.30 6 2 0 8.60 1.50 6 2 0 9.60 2.00 -6 2 0 11.30 1.20 7 -2 0 46.00 2.80 7 -2 0 45.30 2.80 -7 -2 0 47.10 3.10 7 -2 0 42.60 3.70 7 -2 0 46.00 2.80 -7 -2 0 43.20 3.00 7 -2 0 47.50 3.00 7 -2 0 49.99 2.70 -7 2 0 50.09 2.90 7 2 0 48.60 3.50 -7 2 0 47.10 3.00 8 -2 0 66.69 3.80 -8 -2 0 70.29 4.30 -8 -2 0 65.19 4.10 8 -2 0 67.99 3.70 8 -2 0 61.99 3.80 8 -2 0 69.49 3.90 -8 2 0 71.59 4.00 8 2 0 53.09 5.50 -8 2 0 66.09 4.10 8 2 0 56.49 4.60 8 2 0 67.99 4.10 9 -2 0 39.10 2.40 9 -2 0 36.00 2.20 -9 -2 0 37.80 3.10 9 -2 0 37.00 2.50 -9 -2 0 37.70 2.70 9 2 0 38.40 2.80 9 2 0 30.40 3.40 -9 2 0 40.20 2.70 9 2 0 34.10 5.00 -10 -2 0 1.70 1.10 10 -2 0 4.10 0.90 -10 -2 0 1.00 1.40 10 -2 0 2.20 1.00 10 2 0 6.60 3.30 -10 2 0 1.60 1.20 10 2 0 3.50 2.10 10 2 0 4.50 1.20 -11 -2 0 7.30 1.70 11 -2 0 6.00 1.30 11 -2 0 6.60 1.10 -11 -2 0 6.80 1.90 -11 2 0 4.40 1.50 11 2 0 4.90 2.30 11 2 0 7.80 1.50 11 2 0 2.30 3.50 11 2 0 7.70 1.50 -12 -2 0 1.40 1.50 12 -2 0 -1.00 1.20 12 2 0 0.00 1.40 -12 2 0 0.40 1.60 12 2 0 1.20 1.60 13 -2 0 -2.00 1.50 13 -2 0 2.10 1.70 -13 -2 0 0.30 1.70 13 2 0 -0.60 1.70 0 -3 0 -0.20 1.20 0 -3 0 0.10 0.80 0 -3 0 0.20 0.30 0 -3 0 -0.10 0.30 0 -3 0 -0.50 0.90 0 -3 0 0.00 0.40 0 -3 0 -0.20 0.30 0 -3 0 0.30 0.40 0 -3 0 -0.20 0.30 0 3 0 0.00 0.60 0 3 0 0.50 0.40 0 3 0 -0.20 0.50 0 3 0 0.00 0.40 0 3 0 0.30 0.40 0 3 0 0.50 0.50 1 -3 0 141.79 7.80 -1 -3 0 144.29 7.80 -1 -3 0 138.69 7.80 -1 -3 0 139.19 7.80 1 -3 0 143.49 7.80 1 -3 0 120.69 7.90 1 -3 0 150.58 7.80 -1 3 0 140.19 7.80 -1 3 0 144.19 7.90 1 3 0 141.09 7.80 1 3 0 131.19 7.90 1 3 0 141.59 7.80 1 3 0 144.79 7.80 1 3 0 132.79 7.80 1 3 0 135.09 7.90 -1 3 0 148.39 7.80 -2 -3 0 0.60 1.20 -2 -3 0 1.60 2.20 -2 -3 0 0.00 0.40 -2 -3 0 0.50 0.30 2 -3 0 1.10 1.10 2 -3 0 1.00 0.80 2 -3 0 0.80 0.70 -2 -3 0 0.80 0.50 2 -3 0 0.70 0.30 -2 -3 0 0.90 0.40 -2 3 0 0.80 0.40 2 3 0 1.90 1.00 2 3 0 -0.30 0.80 -2 3 0 0.70 0.50 -2 3 0 0.70 0.40 2 3 0 1.80 0.60 2 3 0 -0.10 0.80 -2 3 0 2.00 0.40 3 -3 0 153.08 8.90 3 -3 0 162.38 8.80 -3 -3 0 162.68 8.90 3 -3 0 143.89 9.00 3 -3 0 155.78 8.90 -3 -3 0 168.48 8.90 -3 3 0 161.88 8.90 3 3 0 142.69 9.20 -3 3 0 159.68 8.80 -3 3 0 160.28 8.90 3 3 0 145.19 9.10 -3 3 0 166.28 8.70 3 3 0 162.58 8.90 -3 3 0 160.88 8.80 -3 3 0 159.08 8.80 3 3 0 162.78 8.80 4 -3 0 115.89 6.10 4 -3 0 109.79 6.20 -4 -3 0 93.99 6.20 4 -3 0 100.09 6.30 4 -3 0 104.39 6.00 -4 3 0 113.19 6.10 -4 3 0 114.39 6.10 -4 3 0 110.09 6.00 4 3 0 105.69 6.10 -4 3 0 109.29 6.10 4 3 0 104.39 6.10 5 -3 0 60.49 3.60 5 -3 0 62.59 3.60 5 -3 0 62.59 3.50 -5 -3 0 54.49 3.70 5 -3 0 68.39 3.80 -5 3 0 59.79 3.60 5 3 0 55.99 4.20 5 3 0 58.39 4.70 -5 3 0 63.69 3.50 -5 3 0 64.39 3.60 5 3 0 64.49 3.80 6 -3 0 11.00 0.90 6 -3 0 14.20 1.60 6 -3 0 10.80 1.10 6 -3 0 10.20 1.00 -6 -3 0 10.60 1.30 6 3 0 12.20 1.90 6 3 0 12.60 1.60 6 3 0 13.00 2.70 7 -3 0 17.60 2.20 7 -3 0 18.40 1.30 -7 -3 0 19.60 2.00 -7 -3 0 18.90 1.70 7 -3 0 17.60 1.60 7 3 0 22.10 3.00 7 3 0 21.60 2.50 8 -3 0 -0.10 0.60 8 -3 0 1.10 0.70 -8 -3 0 0.90 1.20 -8 -3 0 1.50 1.00 8 3 0 3.00 2.60 8 3 0 0.60 1.80 9 -3 0 5.20 0.90 -9 -3 0 4.00 1.20 -9 -3 0 6.50 1.70 9 -3 0 4.30 1.00 9 3 0 3.70 3.00 9 3 0 7.20 1.40 9 3 0 5.90 2.10 -10 -3 0 7.50 1.30 10 -3 0 6.90 1.20 -10 -3 0 8.80 1.80 10 -3 0 4.90 1.00 10 3 0 8.30 2.30 10 3 0 8.90 3.20 10 3 0 4.70 1.50 11 -3 0 0.40 1.20 -11 -3 0 -1.30 1.90 -11 -3 0 0.70 1.30 11 -3 0 -0.10 1.00 11 3 0 0.40 2.30 11 3 0 0.00 3.50 11 3 0 0.60 1.40 12 -3 0 1.50 1.20 12 -3 0 2.20 1.40 -12 -3 0 1.60 1.60 12 3 0 2.60 1.60 12 3 0 0.00 2.50 -13 -3 0 2.60 1.70 13 -3 0 1.30 1.60 13 -3 0 5.20 1.80 13 3 0 1.80 1.90 13 3 0 3.50 2.30 0 -4 0 104.79 6.00 0 -4 0 93.19 6.00 0 -4 0 108.79 6.00 0 -4 0 115.19 6.00 0 4 0 108.59 6.20 0 4 0 107.29 6.20 0 4 0 101.89 6.10 0 4 0 107.99 6.00 0 4 0 106.99 6.00 0 4 0 111.69 6.00 -1 -4 0 9.20 0.80 1 -4 0 10.40 1.90 1 -4 0 9.50 0.90 -1 -4 0 9.50 0.90 -1 -4 0 8.20 0.90 -1 -4 0 10.40 1.00 -1 -4 0 8.30 1.00 -1 -4 0 2.90 2.40 1 -4 0 7.70 1.40 -1 -4 0 5.60 1.90 1 -4 0 11.00 0.80 1 -4 0 5.80 1.70 1 -4 0 10.10 0.90 1 4 0 9.30 1.10 -1 4 0 8.90 1.00 -1 4 0 9.80 1.00 1 4 0 10.20 0.90 1 4 0 8.10 1.10 1 4 0 8.20 1.20 1 4 0 9.60 1.20 1 4 0 9.70 1.20 -1 4 0 11.70 1.20 1 4 0 8.00 1.20 -2 -4 0 28.40 2.10 -2 -4 0 33.50 2.00 -2 -4 0 22.70 3.60 2 -4 0 27.90 1.90 -2 -4 0 34.10 2.10 -2 -4 0 35.00 2.00 2 -4 0 30.10 1.90 2 4 0 34.50 2.70 2 4 0 33.10 2.00 -2 4 0 28.50 2.20 2 4 0 38.10 2.70 -2 4 0 32.10 2.10 -2 4 0 29.90 2.00 2 4 0 34.30 2.20 2 4 0 35.70 2.40 3 -4 0 130.29 7.00 -3 -4 0 116.39 7.10 -3 -4 0 135.19 6.90 3 -4 0 109.29 7.30 3 -4 0 124.89 6.90 -3 -4 0 127.99 7.10 -3 4 0 119.49 7.10 3 4 0 128.19 7.10 -3 4 0 121.89 7.10 3 4 0 123.39 7.40 3 4 0 132.39 7.00 -3 4 0 120.59 7.00 4 -4 0 1.90 0.50 4 -4 0 2.40 1.20 4 -4 0 3.10 0.50 -4 -4 0 3.10 0.80 -4 -4 0 2.00 0.80 4 -4 0 1.40 1.40 -4 4 0 4.30 0.80 4 4 0 4.50 0.90 -4 4 0 3.50 0.80 -4 4 0 3.60 0.40 4 4 0 2.90 1.70 4 4 0 2.70 1.40 -4 4 0 4.80 0.60 -4 4 0 2.80 0.70 5 -4 0 51.09 3.10 5 -4 0 52.69 3.00 5 -4 0 47.70 3.80 5 -4 0 45.90 3.40 -5 -4 0 50.39 3.30 5 4 0 45.80 3.80 -5 4 0 57.09 3.20 5 4 0 59.59 4.40 -5 4 0 53.99 3.00 5 4 0 51.59 3.40 -5 4 0 51.09 3.30 6 -4 0 5.10 0.80 6 -4 0 5.30 1.80 6 -4 0 2.60 1.30 -6 -4 0 2.50 0.80 6 -4 0 5.00 0.60 -6 4 0 4.50 0.80 6 4 0 2.60 1.70 -6 4 0 4.00 0.60 6 4 0 3.00 2.10 6 4 0 3.90 1.40 -7 -4 0 6.50 1.30 -7 -4 0 6.40 1.20 7 -4 0 7.10 2.50 7 -4 0 8.40 0.90 7 -4 0 7.50 1.50 7 -4 0 8.20 0.90 7 4 0 6.10 2.50 7 4 0 6.40 2.00 7 4 0 10.00 2.00 8 -4 0 0.30 0.70 -8 -4 0 1.30 1.10 8 -4 0 1.50 0.80 -8 -4 0 0.10 1.00 8 4 0 0.90 2.00 8 4 0 -0.40 2.60 -9 -4 0 59.09 4.00 9 -4 0 63.59 3.80 -9 -4 0 60.39 4.40 9 -4 0 60.29 3.60 9 4 0 56.79 4.90 9 4 0 63.39 6.00 -10 -4 0 3.50 1.60 10 -4 0 2.70 0.90 10 -4 0 4.40 1.20 -10 -4 0 0.90 1.30 10 4 0 1.70 2.40 10 4 0 2.50 1.50 10 4 0 3.50 3.40 11 -4 0 1.30 1.40 -11 -4 0 0.70 1.80 11 -4 0 -0.30 1.00 -11 -4 0 -0.10 1.40 11 4 0 -0.90 1.70 11 4 0 0.90 2.40 11 4 0 0.10 3.60 -12 -4 0 1.40 1.60 12 -4 0 2.10 1.50 12 -4 0 0.40 1.30 12 4 0 3.00 2.90 12 4 0 0.80 2.00 0 -5 0 -0.10 0.60 0 -5 0 0.90 0.60 0 5 0 0.60 1.00 0 5 0 -0.40 0.80 0 5 0 -1.30 0.90 0 5 0 -1.00 0.90 1 -5 0 95.99 5.30 1 -5 0 88.49 5.30 1 -5 0 99.29 5.30 1 -5 0 96.29 5.30 -1 -5 0 90.39 5.30 -1 -5 0 79.89 5.40 -1 -5 0 91.69 5.30 -1 -5 0 100.89 5.30 -1 -5 0 91.39 5.30 1 5 0 82.19 5.50 -1 5 0 98.89 5.50 1 5 0 95.29 5.60 -1 5 0 94.29 5.50 1 5 0 93.39 5.60 -1 5 0 87.49 5.50 -2 -5 0 78.29 4.30 -2 -5 0 69.79 4.40 2 -5 0 84.89 4.40 -2 -5 0 70.69 4.30 2 -5 0 72.49 4.30 -2 -5 0 70.29 4.40 2 -5 0 70.39 4.30 -2 5 0 79.49 4.40 -2 5 0 73.29 4.50 2 5 0 71.99 4.30 2 5 0 77.89 4.90 2 5 0 74.89 4.70 -2 5 0 75.99 4.50 -3 -5 0 69.19 3.90 -3 -5 0 70.69 4.00 3 -5 0 71.09 3.90 3 -5 0 61.19 3.90 -3 -5 0 69.29 4.10 -3 -5 0 69.59 4.10 3 5 0 63.99 4.70 -3 5 0 69.29 4.10 3 5 0 65.29 4.00 -3 5 0 63.69 4.00 3 5 0 76.19 4.50 -3 5 0 60.89 4.10 -4 -5 0 317.97 17.80 -4 -5 0 310.77 17.80 4 -5 0 318.87 17.60 4 -5 0 319.57 17.70 -4 5 0 315.07 17.70 4 5 0 328.47 18.10 4 5 0 303.37 17.60 4 5 0 321.07 18.30 -4 5 0 316.67 17.80 -4 5 0 328.07 17.60 -4 5 0 324.97 17.80 5 -5 0 7.40 0.90 5 -5 0 3.90 2.00 5 -5 0 4.80 0.80 -5 -5 0 5.30 1.10 -5 -5 0 4.70 1.10 -5 5 0 7.40 1.20 -5 5 0 5.20 0.80 5 5 0 6.10 2.20 -5 5 0 6.10 1.00 5 5 0 4.40 1.80 -5 5 0 5.50 0.70 5 5 0 3.90 1.30 6 -5 0 0.10 2.00 6 -5 0 0.40 0.70 -6 -5 0 -0.20 0.90 -6 -5 0 0.40 1.00 6 5 0 0.50 1.70 6 5 0 0.50 2.20 -6 5 0 0.20 0.60 -6 5 0 0.70 0.80 6 5 0 -0.10 2.10 7 -5 0 33.20 2.40 -7 -5 0 37.10 2.90 7 -5 0 34.50 2.20 7 5 0 38.40 3.60 7 5 0 31.50 3.90 -7 5 0 34.10 2.50 -8 -5 0 21.90 2.20 8 -5 0 21.60 1.70 8 -5 0 19.40 1.90 8 5 0 23.50 3.60 8 5 0 25.80 3.30 -9 -5 0 0.30 1.30 9 -5 0 -0.20 1.00 9 -5 0 1.60 0.90 -9 -5 0 -1.50 1.40 9 5 0 2.00 2.40 9 5 0 7.60 3.20 -10 -5 0 4.10 2.10 -10 -5 0 0.50 1.30 10 -5 0 2.80 1.00 10 -5 0 0.10 1.20 10 5 0 2.60 2.50 10 5 0 1.70 1.70 10 5 0 3.20 3.40 11 -5 0 3.90 1.40 11 -5 0 4.60 1.20 -11 -5 0 8.40 1.90 11 5 0 9.30 3.80 11 5 0 4.80 2.80 11 5 0 7.00 2.80 12 -5 0 2.50 1.50 12 -5 0 2.20 1.60 -12 -5 0 2.00 1.70 12 5 0 0.10 4.00 12 5 0 1.80 2.10 12 5 0 1.20 3.00 0 -6 0 0.90 0.70 0 -6 0 2.10 0.90 0 -6 0 0.80 0.70 0 -6 0 -1.50 1.60 0 6 0 -0.50 1.30 0 6 0 0.90 1.10 0 6 0 1.30 1.00 0 6 0 1.50 1.30 1 -6 0 10.20 1.10 1 -6 0 10.10 1.30 -1 -6 0 6.80 1.90 -1 -6 0 12.00 1.30 1 -6 0 10.90 1.20 -1 -6 0 11.00 1.30 1 6 0 7.70 1.80 1 6 0 8.80 1.40 -1 6 0 7.00 1.40 1 6 0 13.40 1.70 -2 -6 0 61.39 3.90 -2 -6 0 54.89 4.50 -2 -6 0 64.09 3.90 2 -6 0 70.09 3.90 2 -6 0 59.29 3.80 -2 -6 0 67.29 3.90 2 -6 0 65.69 3.90 -2 -6 0 56.69 3.90 -2 6 0 70.79 4.20 2 6 0 65.89 4.60 -2 6 0 71.19 4.00 2 6 0 64.59 4.50 2 6 0 66.89 4.30 -2 6 0 65.49 4.10 3 -6 0 19.60 1.70 -3 -6 0 15.60 1.60 -3 -6 0 22.60 1.80 3 -6 0 18.70 1.60 -3 -6 0 16.30 1.90 3 -6 0 19.10 1.80 -3 6 0 24.00 1.90 3 6 0 18.60 1.90 -3 6 0 24.20 2.20 3 6 0 25.50 2.40 3 6 0 20.10 2.30 -3 6 0 21.40 1.70 3 6 0 21.80 2.80 4 -6 0 162.78 8.90 4 -6 0 162.68 8.90 -4 -6 0 153.78 9.00 4 -6 0 151.68 8.80 -4 -6 0 147.19 9.00 -4 -6 0 147.09 8.70 -4 6 0 160.78 8.80 -4 6 0 157.38 9.00 4 6 0 167.98 9.70 4 6 0 163.38 9.40 -4 6 0 161.98 8.90 -4 6 0 145.19 9.00 5 -6 0 58.29 3.70 -5 -6 0 55.59 4.00 -5 -6 0 61.19 3.90 5 -6 0 59.59 3.60 -5 6 0 58.59 3.80 5 6 0 68.79 5.90 -5 6 0 62.29 3.70 5 6 0 64.29 5.20 -5 6 0 62.99 4.00 6 -6 0 8.10 1.10 -6 -6 0 8.00 1.30 6 -6 0 10.10 1.10 6 6 0 6.20 2.60 -6 6 0 9.10 1.60 6 6 0 9.10 2.40 -6 6 0 9.20 1.10 -6 6 0 5.80 1.20 7 -6 0 2.70 0.90 7 -6 0 1.70 1.00 -7 -6 0 1.00 1.00 -7 -6 0 1.70 1.50 -7 6 0 -0.50 1.10 7 6 0 1.60 2.20 7 6 0 0.60 2.70 8 -6 0 40.00 2.50 8 -6 0 37.20 2.70 -8 -6 0 28.30 3.50 -8 6 0 34.10 2.50 -8 6 0 37.10 2.80 8 6 0 34.90 4.10 8 6 0 38.00 5.20 -9 -6 0 30.40 3.80 9 -6 0 38.00 2.60 -9 -6 0 32.50 3.00 9 -6 0 35.20 2.80 9 6 0 43.30 4.50 9 6 0 42.60 5.60 -10 -6 0 2.60 1.50 10 -6 0 2.20 1.30 10 -6 0 1.40 1.40 10 6 0 3.00 2.80 10 6 0 2.60 3.40 10 6 0 6.80 2.10 11 -6 0 1.40 1.50 -11 -6 0 1.30 1.60 11 -6 0 0.30 1.60 11 6 0 0.40 3.70 11 6 0 -0.10 2.20 11 6 0 0.30 2.90 0 -7 0 2.10 1.10 0 -7 0 0.10 0.90 0 -7 0 1.60 0.90 0 7 0 -0.20 1.10 0 7 0 -0.50 1.30 0 7 0 -0.50 1.70 0 7 0 -0.40 1.50 -1 -7 0 2.40 1.00 1 -7 0 2.40 0.90 1 -7 0 3.00 1.00 -1 -7 0 2.80 1.20 -1 -7 0 1.50 0.90 1 -7 0 3.60 1.00 -1 -7 0 1.10 2.30 1 7 0 1.60 1.20 -1 7 0 3.80 1.20 -1 7 0 3.30 1.60 -1 7 0 1.80 1.20 1 7 0 2.80 1.80 1 7 0 4.10 1.60 -2 -7 0 82.19 4.80 -2 -7 0 72.29 4.70 2 -7 0 76.89 4.70 2 -7 0 78.19 4.70 2 -7 0 74.19 4.80 2 7 0 84.39 5.50 -2 7 0 77.49 4.90 2 7 0 81.39 5.10 2 7 0 88.89 5.50 -2 7 0 88.19 5.10 -2 7 0 72.39 5.10 3 -7 0 11.90 1.30 -3 -7 0 13.80 1.60 3 -7 0 12.70 1.40 -3 -7 0 14.90 1.60 -3 -7 0 13.30 1.50 3 -7 0 13.00 1.60 3 7 0 19.90 2.50 -3 7 0 13.70 1.80 -3 7 0 17.00 1.70 3 7 0 20.60 2.40 -3 7 0 13.00 2.00 3 7 0 14.00 2.30 -4 -7 0 12.40 1.60 4 -7 0 13.30 1.60 4 -7 0 15.50 1.80 -4 -7 0 17.00 1.80 4 -7 0 14.40 1.50 -4 7 0 18.70 1.90 4 7 0 15.00 2.20 4 7 0 13.00 2.40 4 7 0 20.80 2.80 -4 7 0 13.20 1.90 -5 -7 0 1.30 1.30 5 -7 0 1.20 1.00 5 -7 0 1.10 1.10 -5 -7 0 2.00 1.20 5 -7 0 0.90 1.00 5 7 0 3.40 2.60 -5 7 0 2.60 1.20 5 7 0 4.20 2.10 -5 7 0 1.90 1.40 5 7 0 3.60 2.40 -5 7 0 3.60 1.10 6 -7 0 133.49 7.50 -6 -7 0 127.09 7.80 6 -7 0 127.89 7.60 -6 -7 0 114.19 7.60 6 -7 0 133.19 7.40 -6 7 0 134.09 7.80 -6 7 0 125.19 7.40 -6 7 0 123.99 7.60 6 7 0 143.89 8.80 7 -7 0 40.90 3.30 7 -7 0 47.10 3.20 7 -7 0 46.40 3.50 -7 -7 0 48.30 3.90 -7 -7 0 46.50 3.40 7 7 0 50.89 4.60 -7 7 0 43.40 3.10 -7 7 0 45.50 3.40 7 7 0 51.69 5.50 -8 -7 0 1.70 1.40 8 -7 0 0.80 2.60 8 -7 0 3.80 1.30 -8 -7 0 3.80 1.90 8 -7 0 4.00 1.90 -8 7 0 2.10 1.50 8 7 0 6.10 3.00 8 7 0 6.60 3.20 9 -7 0 -1.80 1.40 9 -7 0 2.60 1.80 9 -7 0 0.20 1.40 -9 -7 0 2.50 1.50 9 7 0 3.90 3.40 9 7 0 3.10 3.00 -10 -7 0 2.20 1.80 10 -7 0 1.50 1.90 10 -7 0 2.40 1.80 10 -7 0 3.20 1.60 10 7 0 0.30 3.20 10 7 0 3.20 3.70 10 7 0 4.10 2.40 11 -7 0 30.40 3.30 11 -7 0 32.60 3.20 11 -7 0 30.40 3.60 -11 -7 0 26.90 3.10 11 7 0 22.50 3.60 11 7 0 38.80 5.10 11 7 0 22.80 4.20 0 -8 0 -0.30 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12 -3 -3 7.40 2.20 12 -3 -3 6.00 1.30 -12 -3 3 4.00 1.60 -12 -3 3 6.50 2.40 12 3 -3 1.00 4.50 12 3 -3 6.90 2.00 12 3 -3 5.70 3.20 11 -3 -3 0.70 1.20 -11 -3 3 1.40 2.10 11 -3 -3 3.30 1.00 -11 -3 3 2.90 1.30 11 3 -3 -1.80 4.10 11 3 -3 4.70 2.90 11 3 -3 0.60 1.50 -10 -3 3 6.40 1.70 10 -3 -3 5.30 0.90 10 -3 -3 5.00 1.10 10 3 -3 10.50 3.80 10 3 -3 0.20 2.60 -10 3 3 4.80 1.50 -10 3 3 5.20 1.40 9 -3 -3 148.49 8.10 9 -3 -3 141.89 8.00 -9 3 3 137.39 8.20 9 3 -3 128.49 9.90 -9 3 3 148.89 8.20 -8 -3 3 12.50 1.60 8 -3 -3 13.00 1.30 -8 -3 3 10.30 1.50 8 3 -3 6.70 2.30 -8 3 3 12.00 1.50 -8 3 3 16.00 1.40 8 3 -3 16.50 2.10 8 3 -3 10.90 3.10 -7 -3 3 79.29 4.90 7 -3 -3 82.29 4.60 7 -3 -3 77.59 4.70 -7 -3 3 82.79 4.80 7 -3 -3 80.79 4.50 7 3 -3 65.99 6.20 7 3 -3 78.09 5.10 6 -3 -3 47.00 2.80 6 -3 -3 45.40 3.40 6 -3 -3 46.40 2.90 -6 -3 3 53.49 3.10 -6 -3 3 55.09 3.30 -6 3 3 48.70 2.90 6 3 -3 43.40 3.10 -6 3 3 53.79 3.00 6 3 -3 38.30 4.50 5 -3 -3 90.19 5.10 5 -3 -3 88.79 5.40 5 -3 -3 94.69 5.30 -5 -3 3 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40.80 2.50 7 5 -4 46.50 5.70 7 5 -4 33.20 4.00 -7 5 4 41.10 2.80 -7 5 4 41.00 2.60 7 5 -4 44.80 6.20 6 -5 -4 40.10 2.90 6 -5 -4 39.90 2.70 -6 -5 4 37.40 2.80 -6 -5 4 44.20 3.20 -6 5 4 42.90 2.60 6 5 -4 35.20 4.50 -6 5 4 44.00 2.80 6 5 -4 39.50 4.00 6 5 -4 51.19 5.60 5 -5 -4 73.39 4.60 -5 -5 4 78.99 4.70 5 -5 -4 77.29 4.60 5 -5 -4 78.99 4.50 -5 -5 4 80.39 4.80 -5 5 4 77.19 4.60 5 5 -4 66.99 5.50 5 5 -4 70.89 6.40 5 5 -4 87.99 7.30 -5 5 4 83.09 4.70 -5 5 4 76.69 4.50 4 -5 -4 8.90 1.00 -4 -5 4 5.50 1.10 -4 -5 4 5.80 1.00 -4 -5 4 8.70 2.00 4 -5 -4 6.90 0.90 4 -5 -4 7.60 0.80 4 5 -4 2.80 2.20 4 5 -4 5.90 1.80 -4 5 4 6.50 1.00 -4 5 4 7.90 1.10 -4 5 4 8.20 1.00 -4 5 4 8.00 0.80 4 5 -4 6.50 2.90 4 5 -4 6.60 1.10 -4 5 4 6.00 0.90 -3 -5 4 24.80 1.90 3 -5 -4 23.70 1.80 -3 -5 4 28.50 2.10 -3 -5 4 26.40 1.80 3 -5 -4 25.50 1.70 -3 -5 4 24.00 2.80 3 -5 -4 25.40 1.90 3 5 -4 22.60 2.80 -3 5 4 26.10 1.70 -3 5 4 28.40 1.80 -3 5 4 23.40 1.90 -3 5 4 25.70 2.00 3 5 -4 22.50 3.10 3 5 -4 28.00 2.00 -3 5 4 23.00 1.80 3 5 -4 29.60 2.80 2 -5 -4 9.50 1.10 2 -5 -4 8.10 0.80 -2 -5 4 8.20 0.90 -2 -5 4 7.10 1.00 2 -5 -4 6.90 1.00 -2 -5 4 8.60 1.00 -2 -5 4 6.10 2.10 2 5 -4 10.90 2.10 -2 5 4 8.30 1.10 2 5 -4 9.30 1.00 2 5 -4 7.80 1.20 2 5 -4 6.60 1.60 -2 5 4 8.50 1.20 2 5 -4 5.30 1.70 -2 5 4 6.20 0.90 -2 5 4 7.10 1.00 -1 -5 4 409.66 22.20 -1 -5 4 423.66 22.20 -1 -5 4 428.16 22.20 -1 -5 4 428.96 22.10 -1 -5 4 422.66 22.20 1 -5 -4 435.76 22.20 1 -5 -4 375.96 22.20 -1 -5 4 372.46 22.30 1 -5 -4 420.86 22.10 -1 5 4 378.16 22.20 1 5 -4 359.16 22.40 -1 5 4 414.16 22.20 1 5 -4 368.16 22.60 -1 5 4 402.66 22.30 1 5 -4 389.26 22.40 1 5 -4 389.76 22.20 -1 5 4 378.76 22.10 0 -5 4 2.60 0.50 0 -5 -4 2.00 0.80 0 -5 -4 2.20 0.60 0 -5 4 1.60 1.60 0 -5 4 2.60 0.70 0 -5 4 2.90 0.70 0 -5 -4 4.30 0.80 0 -5 4 3.80 0.70 0 5 4 0.70 1.00 0 5 -4 2.30 1.40 0 5 4 1.30 1.00 0 5 -4 3.40 1.00 0 5 -4 2.90 1.20 0 5 4 3.10 0.80 0 5 4 2.40 0.80 0 5 4 3.40 1.00 0 5 -4 3.70 1.30 1 -5 4 86.59 4.80 1 -5 4 87.99 4.80 -1 -5 -4 86.29 4.90 -1 -5 -4 86.99 4.90 -1 -5 -4 82.99 4.90 1 5 4 78.59 5.00 -1 5 -4 83.59 5.30 1 5 4 90.29 5.10 1 5 4 87.99 5.00 -1 5 -4 79.59 5.20 -1 5 -4 85.79 5.30 1 5 4 77.39 5.10 1 5 4 79.89 5.10 2 -5 4 0.80 0.50 -2 -5 -4 0.70 0.70 2 -5 4 1.20 0.60 -2 -5 -4 -0.80 2.80 -2 -5 -4 0.80 0.60 -2 -5 -4 1.90 0.80 2 5 4 1.60 1.20 -2 5 -4 3.10 0.90 2 5 4 3.00 1.10 2 5 4 1.60 0.90 2 5 4 0.80 0.90 -2 5 -4 1.40 1.00 -2 5 -4 0.60 1.10 -3 -5 -4 1.50 0.80 3 -5 4 1.10 0.60 -3 -5 -4 1.20 0.70 3 -5 4 0.70 0.50 -3 5 -4 2.30 1.10 -3 5 -4 1.10 1.00 3 5 4 0.30 1.00 -3 5 -4 2.00 0.80 3 5 4 0.10 1.30 3 5 4 1.80 1.10 -3 5 -4 -0.20 0.70 4 -5 4 126.09 7.20 4 -5 4 126.19 7.30 -4 -5 -4 119.49 7.30 -4 -5 -4 129.79 7.40 4 5 4 129.69 7.70 -4 5 -4 134.69 7.50 4 5 4 134.79 7.60 -5 -5 -4 7.70 1.20 5 -5 4 8.00 0.90 5 -5 4 8.90 1.10 5 5 4 8.10 1.40 -5 5 -4 9.70 1.00 5 5 4 10.50 2.60 -5 5 -4 10.90 1.00 -5 5 -4 9.90 1.30 5 5 4 10.90 1.80 -5 5 -4 11.10 1.40 6 -5 4 90.29 5.10 -6 -5 -4 91.39 5.40 6 -5 4 84.69 5.20 -6 5 -4 90.39 5.10 -6 5 -4 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39.50 3.20 -9 -7 4 38.60 3.40 9 -7 -4 47.20 3.50 -9 -7 4 41.10 4.30 9 7 -4 45.20 7.90 9 7 -4 56.69 7.60 -8 -7 4 0.50 1.60 8 -7 -4 0.70 1.30 8 -7 -4 1.80 1.40 8 -7 -4 -1.40 2.60 -8 -7 4 -0.80 1.40 -8 7 4 0.30 1.20 8 7 -4 -1.00 3.70 -8 7 4 0.80 1.50 8 7 -4 1.90 3.20 7 -7 -4 4.70 1.60 -7 -7 4 2.60 1.30 -7 -7 4 3.00 1.50 7 -7 -4 7.70 1.20 7 -7 -4 4.00 1.40 -7 7 4 6.00 1.20 7 7 -4 9.50 5.50 -7 7 4 4.40 1.40 7 7 -4 4.30 3.80 7 7 -4 2.40 3.20 -6 -7 4 63.89 4.70 6 -7 -4 66.99 4.60 6 -7 -4 67.49 4.40 -6 -7 4 60.69 4.40 6 -7 -4 73.99 4.20 6 7 -4 83.29 8.10 6 7 -4 78.99 7.10 6 7 -4 69.69 5.90 -6 7 4 68.79 4.50 -6 7 4 67.89 4.20 5 -7 -4 7.70 1.20 5 -7 -4 6.00 1.30 -5 -7 4 7.70 1.50 5 -7 -4 5.40 1.30 -5 -7 4 8.10 1.60 -5 7 4 10.10 1.30 -5 7 4 8.80 1.00 5 7 -4 7.40 2.70 -5 7 4 5.70 1.20 5 7 -4 2.80 3.20 5 7 -4 11.90 4.00 -4 -7 4 80.99 4.90 -4 -7 4 85.59 5.10 -4 -7 4 76.19 5.00 4 -7 -4 78.19 5.00 4 -7 -4 75.39 5.00 -4 7 4 79.29 4.80 4 7 -4 94.89 7.10 -4 7 4 87.39 4.90 -4 7 4 81.19 5.10 4 7 -4 96.59 6.90 4 7 -4 72.69 6.00 -4 7 4 79.29 5.10 3 -7 -4 93.99 5.90 -3 -7 4 99.29 6.10 -3 -7 4 104.59 6.20 -3 -7 4 102.09 6.00 3 -7 -4 104.99 6.10 3 -7 -4 99.59 6.10 3 7 -4 110.29 7.00 -3 7 4 102.09 6.20 -3 7 4 110.59 6.10 3 7 -4 99.89 7.50 3 7 -4 109.49 7.30 -3 7 4 102.39 6.20 -2 -7 4 1.40 0.90 -2 -7 4 0.10 1.00 -2 -7 4 0.60 1.10 2 -7 -4 2.50 1.00 2 -7 -4 1.00 1.20 2 7 -4 -0.60 1.80 -2 7 4 1.70 1.20 2 7 -4 1.20 2.30 2 7 -4 2.30 2.00 -2 7 4 0.30 1.00 -2 7 4 0.50 1.00 -1 -7 4 163.98 9.40 -1 -7 4 163.38 9.40 1 -7 -4 164.78 9.50 -1 -7 4 162.38 9.50 1 -7 -4 164.18 9.30 1 -7 -4 157.88 9.40 1 7 -4 174.88 10.00 -1 7 4 143.29 9.80 -1 7 4 186.18 9.70 -1 7 4 175.38 9.60 1 7 -4 166.38 9.90 -1 7 4 177.18 9.50 1 7 -4 152.88 10.10 0 -7 -4 26.60 2.00 0 -7 -4 26.00 2.10 0 -7 4 23.50 2.10 0 -7 4 24.10 2.10 0 -7 4 30.80 2.20 0 -7 4 24.30 2.20 0 -7 -4 26.60 2.60 0 -7 4 28.00 2.10 0 7 4 30.40 2.60 0 7 -4 30.30 3.40 0 7 4 27.60 2.30 0 7 -4 27.80 2.90 0 7 -4 30.80 3.40 0 7 4 27.10 2.50 -1 -7 -4 10.50 1.60 1 -7 4 12.70 1.60 -1 -7 -4 12.00 1.60 1 -7 4 14.40 1.40 1 -7 4 13.80 1.40 -1 7 -4 15.20 2.00 1 7 4 11.10 1.60 -1 7 -4 13.30 1.80 1 7 4 15.20 1.80 -1 7 -4 16.30 2.10 1 7 4 14.30 1.80 -2 -7 -4 17.30 1.70 2 -7 4 15.80 1.80 2 -7 4 17.00 1.60 -2 -7 -4 16.80 1.80 2 -7 4 16.20 1.70 -2 -7 -4 14.30 1.70 2 7 4 20.00 2.30 -2 7 -4 18.60 2.40 2 7 4 18.60 2.20 2 7 4 21.60 2.20 -2 7 -4 20.40 2.00 -3 -7 -4 2.00 1.00 -3 -7 -4 3.20 1.00 3 -7 4 2.00 0.90 3 -7 4 3.50 1.00 -3 -7 -4 3.80 1.30 -3 7 -4 4.40 1.70 3 7 4 1.60 1.80 -3 7 -4 3.80 1.20 3 7 4 4.60 2.00 -3 7 -4 5.30 1.40 3 7 4 3.00 1.50 -4 -7 -4 108.49 6.90 -4 -7 -4 113.19 6.80 4 -7 4 108.49 6.80 4 -7 4 118.89 6.90 -4 7 -4 113.69 7.20 4 7 4 131.99 7.50 -4 7 -4 121.69 6.90 4 7 4 128.39 7.50 -4 7 -4 122.19 7.10 5 -7 4 1.80 1.00 5 -7 4 2.50 1.00 -5 -7 -4 1.50 1.20 5 7 4 3.60 2.00 -5 7 -4 0.20 1.20 5 7 4 3.10 2.10 -5 7 -4 4.90 1.70 5 7 4 -0.60 1.70 -5 7 -4 1.50 1.00 6 -7 4 1.20 1.10 -6 -7 -4 0.90 1.30 6 -7 4 0.40 1.10 -6 7 -4 2.60 1.60 6 7 4 3.40 1.50 6 7 4 0.70 2.10 -6 7 -4 1.50 1.30 -6 7 -4 3.10 1.10 6 7 4 7.70 2.40 6 7 4 3.30 2.10 7 -7 4 23.90 2.40 -7 -7 -4 25.10 2.50 7 -7 4 26.50 2.20 7 7 4 24.10 2.90 -7 7 -4 29.00 3.20 7 7 4 22.70 3.00 -7 7 -4 23.40 2.50 7 7 4 27.80 3.70 7 7 4 25.00 3.00 8 -7 4 0.50 1.20 8 -7 4 3.10 1.30 -8 -7 -4 0.10 1.40 8 7 4 2.90 2.70 8 7 4 -0.50 2.10 -8 7 -4 2.20 1.50 8 7 4 0.30 2.30 -9 -7 -4 18.30 2.40 9 -7 4 18.10 1.90 9 -7 4 17.70 2.00 9 7 4 18.80 2.80 9 7 4 18.00 2.90 9 7 4 17.10 3.30 10 -7 4 1.60 1.70 -10 -7 -4 1.10 1.70 10 -7 4 5.70 1.70 10 7 4 2.50 2.70 10 7 4 2.40 2.30 10 7 4 3.00 3.10 -10 -8 4 6.30 1.80 10 -8 -4 14.50 2.90 10 -8 -4 9.90 2.30 -10 -8 4 5.90 2.70 10 8 -4 7.30 5.40 10 8 -4 4.40 4.30 -9 -8 4 1.40 1.60 9 -8 -4 -0.10 1.90 -9 -8 4 -1.10 2.50 9 -8 -4 -0.90 2.30 9 -8 -4 1.40 1.70 9 8 -4 0.30 4.00 9 8 -4 -0.40 4.90 -9 8 4 0.60 2.10 8 -8 -4 11.40 2.30 -8 -8 4 8.50 2.20 8 -8 -4 11.50 2.10 -8 -8 4 9.50 2.00 8 -8 -4 13.40 1.80 8 8 -4 20.90 6.70 8 8 -4 11.40 4.20 8 8 -4 16.10 5.10 -8 8 4 11.10 2.10 -8 8 4 16.80 2.00 7 -8 -4 0.30 1.80 7 -8 -4 2.20 1.40 -7 -8 4 3.00 2.00 -7 -8 4 0.30 1.40 -7 8 4 1.90 1.60 7 8 -4 -0.10 6.00 -7 8 4 -0.70 1.40 7 8 -4 10.80 5.70 7 8 -4 -0.30 4.30 -6 -8 4 -0.20 1.30 6 -8 -4 1.80 1.50 6 -8 -4 0.20 1.20 -6 -8 4 0.30 1.70 6 -8 -4 -0.20 1.60 -6 8 4 2.20 1.40 6 8 -4 3.50 4.50 6 8 -4 -0.10 3.60 -6 8 4 0.20 1.40 6 8 -4 -0.90 2.90 -5 -8 4 1.30 1.30 5 -8 -4 1.20 1.50 -5 -8 4 0.70 1.50 5 -8 -4 0.50 1.50 -5 8 4 1.60 1.30 5 8 -4 2.80 3.40 -5 8 4 3.00 1.80 5 8 -4 0.90 3.50 5 8 -4 -0.90 2.80 -5 8 4 0.20 1.20 -5 8 4 -0.20 1.30 -4 -8 4 58.39 4.30 4 -8 -4 66.49 4.10 -4 -8 4 59.39 4.00 4 -8 -4 63.19 4.20 -4 -8 4 52.59 4.00 -4 8 4 56.99 4.20 4 8 -4 70.39 6.20 -4 8 4 59.49 3.90 -4 8 4 61.79 4.30 4 8 -4 68.39 6.50 4 8 -4 66.09 5.50 -4 8 4 61.69 4.00 3 -8 -4 0.00 1.40 3 -8 -4 -0.30 1.20 -3 -8 4 1.80 1.10 -3 -8 4 0.50 1.20 -3 -8 4 -1.10 1.20 -3 8 4 0.20 1.50 3 8 -4 0.10 2.80 -3 8 4 0.80 1.40 -3 8 4 0.70 1.20 3 8 -4 1.00 2.30 3 8 -4 2.00 2.70 -3 8 4 1.10 1.30 -2 -8 4 185.58 11.50 -2 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2.10 -2 -3 -9 16.60 1.60 2 -3 9 18.70 4.80 2 -3 9 16.00 1.10 2 -3 9 17.60 1.10 -2 -3 -9 17.20 1.30 2 3 9 17.70 1.30 -2 3 -9 16.50 1.90 -2 3 -9 16.00 1.50 -2 3 -9 16.70 1.90 -2 3 -9 14.30 1.60 2 3 9 16.40 1.30 2 3 9 15.10 1.30 -3 -3 -9 272.87 16.80 -3 -3 -9 282.37 16.50 3 -3 9 292.77 16.50 3 -3 9 304.27 17.90 -3 -3 -9 286.47 16.50 3 -3 9 312.17 16.50 3 -3 9 305.57 16.50 -3 -3 -9 323.17 16.60 -3 3 -9 273.77 16.70 3 3 9 293.77 16.60 -3 3 -9 299.67 16.50 3 3 9 282.17 16.70 -3 3 -9 314.07 16.60 3 3 9 316.57 16.60 -3 3 -9 302.97 16.60 4 -3 9 90.59 4.90 -4 -3 -9 84.09 5.00 -4 -3 -9 89.19 5.00 4 -3 9 90.49 4.90 -4 -3 -9 82.89 5.00 4 -3 9 87.59 4.90 4 3 9 83.89 5.00 4 3 9 93.19 5.00 4 3 9 79.59 5.90 -4 3 -9 86.09 5.00 -4 3 -9 89.99 5.10 -4 3 -9 75.69 4.90 4 3 9 80.19 5.00 5 -3 9 76.59 4.50 -5 -3 -9 72.79 4.60 5 -3 9 78.79 4.50 5 -3 9 78.39 4.40 5 3 9 84.29 4.50 5 3 9 70.19 4.60 5 3 9 78.49 4.50 -5 3 -9 80.39 4.70 5 3 9 70.79 6.20 -6 -3 -9 10.20 1.30 6 -3 9 9.50 1.20 6 -3 9 7.60 1.90 6 -3 9 10.80 1.10 6 -3 9 9.00 1.20 6 3 9 14.10 3.40 6 3 9 10.90 1.30 6 3 9 10.20 1.30 6 3 9 9.30 1.20 7 -3 9 50.99 3.00 7 -3 9 50.29 3.10 -7 -3 -9 48.20 3.30 7 -3 9 53.09 3.20 7 3 9 50.49 3.20 7 3 9 49.30 3.30 7 3 9 50.69 3.20 8 -3 9 135.09 7.80 -8 -3 -9 129.99 7.90 8 -3 9 140.89 7.60 8 -3 9 139.59 7.70 8 3 9 129.99 7.80 8 3 9 133.49 7.70 9 -3 9 56.89 3.60 9 -3 9 57.49 3.70 9 -3 9 58.99 3.50 -9 -3 -9 55.69 3.90 9 3 9 56.49 3.80 9 3 9 53.29 3.60 10 -3 9 1.00 1.30 10 -3 9 1.80 1.20 -10 -3 -9 0.10 1.40 10 3 9 -0.40 1.30 10 3 9 1.00 1.20 10 3 9 0.40 1.50 11 -3 9 0.70 1.50 -11 -3 -9 -0.20 1.50 11 -3 9 2.80 1.40 11 3 9 0.50 1.60 11 3 9 0.20 1.60 12 -3 9 11.00 2.00 -12 -3 -9 11.50 2.10 12 -3 9 14.60 2.00 12 3 9 12.20 2.20 12 3 9 13.50 2.20 13 -4 -9 -0.20 2.80 13 -4 -9 0.80 2.10 13 4 -9 -0.70 4.20 12 -4 -9 14.10 2.70 -12 -4 9 10.50 2.10 12 -4 -9 14.00 2.00 -12 -4 9 15.30 3.00 12 4 -9 9.40 4.10 12 4 -9 3.40 5.10 -11 -4 9 -0.40 1.50 11 -4 -9 0.30 1.90 11 -4 -9 0.60 1.40 -11 -4 9 -0.70 2.00 11 4 -9 -0.80 3.90 11 4 -9 -0.60 8.40 -11 4 9 1.10 2.30 11 4 -9 3.20 4.40 -10 -4 9 13.00 2.40 10 -4 -9 9.30 1.50 -10 -4 9 7.30 1.70 10 -4 -9 9.80 1.90 10 4 -9 9.30 3.50 10 4 -9 23.00 7.80 -10 4 9 11.60 2.10 -9 -4 9 7.10 1.50 9 -4 -9 13.30 1.40 9 -4 -9 11.90 1.80 -9 -4 9 8.50 1.90 9 4 -9 17.00 6.20 9 4 -9 7.90 3.10 -9 4 9 12.10 1.80 8 -4 -9 21.70 1.90 -8 -4 9 16.70 2.10 8 -4 -9 18.90 1.40 -8 4 9 16.40 1.80 8 4 -9 10.00 5.70 8 4 -9 17.20 3.10 -7 -4 9 1.70 1.10 7 -4 -9 2.40 1.10 7 -4 -9 4.50 1.00 -7 -4 9 2.90 1.40 7 4 -9 7.20 2.50 7 4 -9 4.60 4.80 -7 4 9 3.10 1.20 6 -4 -9 13.30 1.50 6 -4 -9 11.20 1.40 -6 -4 9 13.30 1.60 -6 -4 9 12.60 1.70 -6 4 9 14.20 1.10 -6 4 9 16.40 1.50 6 4 -9 14.00 4.50 -6 4 9 13.80 1.30 6 4 -9 16.70 1.40 6 4 -9 13.20 2.30 5 -4 -9 224.68 12.50 -5 -4 9 214.38 12.60 5 -4 -9 221.68 12.60 -5 -4 9 231.68 12.70 5 4 -9 245.98 14.00 -5 4 9 226.98 12.50 -5 4 9 220.08 12.40 -5 4 9 220.88 12.40 5 4 -9 232.58 12.80 -5 4 9 215.28 12.60 5 4 -9 218.38 12.40 4 -4 -9 1.10 0.90 -4 -4 9 0.50 0.70 4 -4 -9 2.40 0.70 -4 -4 9 0.70 1.00 -4 -4 9 -0.80 2.90 4 4 -9 -4.80 3.10 -4 4 9 1.80 0.70 -4 4 9 0.30 0.60 -4 4 9 1.30 0.50 4 4 -9 1.60 0.70 4 4 -9 4.10 1.60 -3 -4 9 498.05 27.10 -3 -4 9 472.45 26.70 -3 -4 9 479.65 26.60 -3 -4 9 516.85 26.50 3 -4 -9 473.85 26.60 -3 -4 9 452.35 26.70 3 -4 -9 473.35 26.70 -3 4 9 474.85 26.60 3 4 -9 495.45 26.70 -3 4 9 468.45 26.60 -3 4 9 487.15 26.70 -3 4 9 477.35 26.50 3 4 -9 491.65 27.20 3 4 -9 477.85 26.50 -2 -4 9 136.69 7.90 2 -4 -9 133.19 7.90 -2 -4 9 145.89 7.80 -2 -4 9 144.59 9.20 -2 4 9 139.49 7.90 2 4 -9 139.39 7.80 2 4 -9 146.49 8.90 2 4 -9 141.99 8.10 -2 4 9 145.99 7.90 -2 4 9 140.19 7.90 -2 4 9 132.39 8.00 1 -4 -9 321.67 19.60 -1 -4 9 366.36 19.70 1 -4 -9 345.17 19.70 -1 -4 9 384.26 19.60 -1 -4 9 361.26 19.60 -1 4 9 348.07 19.60 -1 4 9 344.77 19.70 1 4 -9 380.16 19.80 1 4 -9 352.46 20.10 -1 4 9 339.27 19.70 0 -4 -9 713.33 39.40 0 -4 9 764.62 39.30 0 -4 -9 646.34 39.40 0 -4 9 734.13 39.40 0 -4 -9 701.53 39.40 0 -4 -9 747.53 39.40 0 -4 9 744.53 39.40 0 4 -9 668.73 39.60 0 4 -9 739.23 39.40 0 4 9 710.53 39.40 0 4 9 694.03 39.50 0 4 9 674.23 39.40 0 4 -9 745.33 39.50 -1 -4 -9 27.60 1.90 1 -4 9 30.80 1.80 -1 -4 -9 27.70 2.90 1 -4 9 29.40 1.80 -1 -4 -9 31.40 2.00 -1 -4 -9 27.60 2.20 1 4 9 26.50 2.00 1 4 9 30.10 2.00 -1 4 -9 25.70 3.00 -1 4 -9 24.60 3.20 -1 4 -9 30.20 2.30 1 4 9 31.50 2.00 -2 -4 -9 29.90 2.10 -2 -4 -9 31.00 1.90 2 -4 9 28.30 1.80 2 -4 9 26.60 1.80 -2 -4 -9 25.40 2.80 2 4 9 26.80 1.90 2 4 9 28.60 1.90 -2 4 -9 23.60 2.80 2 4 9 29.40 2.00 -2 4 -9 25.00 2.10 -2 4 -9 29.50 2.80 -3 -4 -9 13.20 1.30 3 -4 9 9.10 0.90 3 -4 9 11.30 1.00 -3 -4 -9 13.10 1.40 3 4 9 9.70 1.30 -3 4 -9 11.90 1.60 3 4 9 10.00 1.20 -3 4 -9 14.80 1.50 3 4 9 12.70 1.20 -3 4 -9 10.80 1.40 -3 4 -9 11.60 1.80 -4 -4 -9 52.89 3.30 4 -4 9 52.09 3.10 -4 -4 -9 53.69 3.30 4 -4 9 51.69 3.10 4 -4 9 48.80 3.10 4 4 9 50.89 3.30 -4 4 -9 54.59 3.60 4 4 9 48.20 3.30 -4 4 -9 51.19 3.30 4 4 9 58.09 3.30 5 -4 9 36.90 2.30 5 -4 9 33.60 2.30 5 -4 9 38.20 2.40 -5 -4 -9 37.40 2.60 -5 4 -9 36.50 2.20 5 4 9 36.90 2.50 -5 4 -9 39.70 2.90 5 4 9 36.60 2.50 5 4 9 33.50 2.50 6 -4 9 65.59 3.60 6 -4 9 60.19 3.60 6 -4 9 60.49 3.70 -6 -4 -9 53.99 3.80 6 4 9 58.79 3.80 -6 4 -9 64.09 4.10 6 4 9 63.29 3.80 6 4 9 55.29 3.80 7 -4 9 66.19 4.00 7 -4 9 60.79 4.00 7 4 9 70.99 4.20 7 4 9 70.09 4.20 7 4 9 65.39 4.20 8 -4 9 89.19 5.30 -8 -4 -9 79.99 5.40 8 -4 9 93.39 5.20 8 4 9 89.79 5.30 8 4 9 93.49 5.30 8 4 9 79.99 5.40 9 -4 9 14.20 1.70 9 -4 9 14.90 2.00 -9 -4 -9 9.80 1.60 9 4 9 12.50 1.70 9 4 9 15.30 1.90 9 4 9 10.90 1.60 10 -4 9 -0.40 1.10 10 -4 9 1.80 1.40 -10 -4 -9 0.90 1.60 10 4 9 1.00 1.50 10 4 9 0.20 1.40 11 -4 9 0.80 1.60 -11 -4 -9 1.40 1.40 11 -4 9 0.80 1.40 11 4 9 1.40 1.80 12 -5 -9 1.30 2.60 -12 -5 9 2.60 2.90 12 -5 -9 4.80 2.10 -12 -5 9 0.50 1.60 12 5 -9 3.50 4.30 12 5 -9 2.20 5.60 11 -5 -9 1.30 2.20 -11 -5 9 1.40 2.20 -11 -5 9 0.20 1.70 11 -5 -9 2.80 1.70 11 5 -9 3.90 9.70 11 5 -9 3.80 5.10 10 -5 -9 1.20 1.70 10 -5 -9 -0.20 1.40 -10 -5 9 0.70 1.40 -10 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3.50 0.90 -3 -5 9 3.90 0.90 -3 -5 9 3.70 1.00 3 -5 -9 2.10 1.00 -3 -5 9 2.40 0.80 3 5 -9 3.30 2.70 3 5 -9 2.10 1.20 -3 5 9 3.80 0.90 -3 5 9 2.90 0.80 -3 5 9 3.90 0.60 -3 5 9 4.00 1.00 3 5 -9 3.10 0.80 3 5 -9 3.10 2.90 2 -5 -9 33.40 2.10 -2 -5 9 33.00 2.00 2 -5 -9 26.40 2.40 -2 -5 9 29.70 2.00 -2 -5 9 26.60 2.30 -2 5 9 29.30 2.00 2 5 -9 32.20 2.70 2 5 -9 35.60 3.80 -2 5 9 31.70 2.20 -2 5 9 24.60 2.20 -2 5 9 27.50 1.90 2 5 -9 25.40 3.70 2 5 -9 27.00 2.00 1 -5 -9 3.60 0.80 1 -5 -9 3.40 1.00 -1 -5 9 2.40 0.70 -1 -5 9 1.70 0.70 -1 -5 9 4.50 1.00 1 5 -9 2.50 2.10 -1 5 9 4.10 0.70 1 5 -9 2.70 0.90 1 5 -9 2.90 2.00 -1 5 9 3.10 0.80 0 -5 9 162.78 9.10 0 -5 -9 158.98 9.10 0 -5 -9 164.68 9.00 0 -5 9 167.38 9.00 0 -5 -9 152.58 9.20 0 -5 9 159.68 9.00 0 5 -9 142.19 9.60 0 5 9 158.28 9.20 0 5 9 166.38 9.10 0 5 9 165.28 9.20 0 5 -9 172.78 9.20 1 -5 9 27.60 1.70 -1 -5 -9 18.50 2.10 -1 -5 -9 25.40 1.90 -1 -5 -9 21.00 1.80 1 -5 9 27.90 1.90 1 -5 9 24.40 1.60 -1 -5 -9 23.50 3.00 -1 5 -9 26.10 3.00 1 5 9 19.20 1.80 1 5 9 21.10 1.80 1 5 9 24.30 1.90 -1 5 -9 17.50 2.40 -1 5 -9 24.60 2.10 -2 -5 -9 26.90 2.20 -2 -5 -9 25.30 1.80 -2 -5 -9 22.10 2.40 2 -5 9 25.60 1.70 2 -5 9 25.50 1.70 -2 5 -9 21.30 2.60 -2 5 -9 23.30 2.90 -2 5 -9 25.70 2.10 2 5 9 24.90 1.90 2 5 9 23.10 2.00 2 5 9 26.20 1.90 -2 5 -9 29.00 2.90 3 -5 9 15.70 1.30 -3 -5 -9 15.20 1.50 3 -5 9 16.60 1.30 -3 -5 -9 18.20 1.60 -3 5 -9 14.60 2.10 3 5 9 15.30 1.50 3 5 9 14.70 1.60 3 5 9 14.50 1.60 -3 5 -9 13.90 1.80 -3 5 -9 18.70 2.00 4 -5 9 12.00 1.10 -4 -5 -9 11.10 1.30 4 -5 9 11.50 1.20 -4 5 -9 11.10 1.60 4 5 9 8.30 1.20 4 5 9 8.80 1.30 -4 5 -9 12.00 1.50 4 5 9 10.10 1.30 5 -5 9 23.90 1.70 -5 -5 -9 22.10 1.90 5 -5 9 22.00 1.70 5 5 9 21.70 2.10 -5 5 -9 24.10 2.10 -5 5 -9 26.80 2.60 5 5 9 17.50 2.00 5 5 9 18.00 2.00 -5 5 -9 21.30 1.70 6 -5 9 1.90 0.80 6 -5 9 0.80 0.80 -6 -5 -9 1.30 1.10 6 5 9 5.50 1.30 -6 5 -9 3.00 1.50 6 5 9 3.50 1.30 6 5 9 3.00 1.20 7 -5 9 42.20 2.90 7 -5 9 44.50 2.80 -7 -5 -9 43.60 3.10 7 5 9 41.30 3.20 -7 5 -9 45.50 3.40 7 5 9 37.80 3.10 7 5 9 46.00 3.20 8 -5 9 14.40 1.80 -8 -5 -9 10.40 1.60 8 -5 9 12.30 1.50 -8 5 -9 14.30 2.10 8 5 9 11.20 1.70 8 5 9 13.40 1.80 8 5 9 11.10 1.70 9 -5 9 33.20 2.50 9 -5 9 30.70 2.80 -9 -5 -9 28.20 2.90 9 5 9 33.90 3.00 9 5 9 38.70 3.00 10 -5 9 13.90 1.70 10 -5 9 15.80 1.90 10 5 9 20.60 2.50 10 5 9 12.50 2.20 11 -5 9 0.90 1.50 11 -5 9 -0.70 1.60 -11 -5 -9 1.80 1.70 11 5 9 3.60 2.10 11 -6 -9 1.20 2.60 11 -6 -9 2.50 2.00 -11 -6 9 -0.90 1.60 -11 -6 9 1.00 2.70 11 6 -9 0.70 5.50 11 6 -9 5.40 9.90 11 6 -9 0.80 4.30 10 -6 -9 2.80 2.00 10 -6 -9 2.50 2.20 -10 -6 9 0.40 1.70 -10 -6 9 4.40 2.20 10 6 -9 6.80 9.10 10 6 -9 0.50 3.80 9 -6 -9 2.10 1.50 9 -6 -9 -0.70 1.80 -9 -6 9 0.10 1.80 -9 -6 9 0.30 1.30 9 6 -9 -3.20 7.70 9 6 -9 -1.30 4.70 9 6 -9 0.50 3.50 -8 -6 9 4.70 1.90 8 -6 -9 7.10 1.50 -8 -6 9 4.30 1.60 8 -6 -9 4.30 1.70 8 6 -9 3.20 3.40 8 6 -9 2.40 2.70 8 6 -9 8.90 4.20 8 6 -9 -0.20 6.80 -8 6 9 4.90 1.40 7 -6 -9 47.40 3.40 -7 -6 9 52.39 3.40 -7 -6 9 46.70 4.00 7 6 -9 43.00 5.60 7 6 -9 44.80 4.30 7 6 -9 42.10 5.20 -7 6 9 39.80 3.40 -7 6 9 49.90 3.20 7 6 -9 66.49 7.30 6 -6 -9 4.80 1.20 6 -6 -9 7.70 1.50 -6 -6 9 5.20 1.50 -6 -6 9 8.80 1.70 6 6 -9 9.40 1.90 6 6 -9 5.10 2.70 6 6 -9 3.80 3.40 6 6 -9 8.70 5.40 -6 6 9 8.90 1.40 -5 -6 9 181.48 11.20 -5 -6 9 193.68 11.30 5 -6 -9 197.38 11.20 5 -6 -9 202.28 11.10 -5 6 9 198.28 11.20 -5 6 9 201.58 11.10 -5 6 9 200.38 10.90 5 6 -9 223.28 13.50 5 6 -9 190.28 11.20 5 6 -9 170.08 12.70 4 -6 -9 2.60 1.40 4 -6 -9 6.50 1.10 -4 -6 9 7.00 1.00 -4 -6 9 3.00 1.40 4 6 -9 5.00 2.70 -4 6 9 7.70 1.30 4 6 -9 4.30 2.90 -4 6 9 6.80 0.80 -4 6 9 6.10 1.10 4 6 -9 7.10 4.20 3 -6 -9 4.50 1.30 -3 -6 9 4.30 0.90 -3 -6 9 5.50 1.10 -3 -6 9 6.50 1.30 3 -6 -9 3.40 1.00 -3 6 9 5.20 1.20 3 6 -9 5.40 1.40 -3 6 9 5.60 1.10 3 6 -9 2.60 2.60 3 6 -9 3.80 2.30 -3 6 9 6.10 0.90 3 6 -9 6.90 3.40 -2 -6 9 26.40 1.90 2 -6 -9 25.50 2.50 -2 -6 9 26.90 2.40 -2 -6 9 25.50 2.00 -2 -6 9 25.70 1.90 2 -6 -9 22.20 2.00 -2 6 9 24.10 1.90 2 6 -9 22.00 3.20 2 6 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7 9 3.30 1.40 5 7 -9 0.90 3.30 -5 7 9 0.20 1.10 5 7 -9 0.70 4.00 4 -7 -9 20.10 2.20 -4 -7 9 16.30 2.00 -4 -7 9 18.00 1.80 -4 -7 9 16.60 1.90 4 7 -9 8.30 3.40 -4 7 9 20.20 2.10 4 7 -9 22.00 2.10 4 7 -9 19.50 4.00 4 7 -9 14.80 3.90 -3 -7 9 2.40 1.20 -3 -7 9 4.40 1.00 3 -7 -9 4.10 1.20 3 -7 -9 2.60 1.60 -3 -7 9 3.20 1.40 3 7 -9 2.70 2.80 -3 7 9 2.70 0.90 -3 7 9 5.10 1.20 3 7 -9 4.20 3.40 -3 7 9 1.60 1.00 3 7 -9 0.60 2.30 2 -7 -9 133.79 7.80 -2 -7 9 141.09 7.70 -2 -7 9 130.09 7.80 2 -7 -9 125.99 7.90 -2 -7 9 136.19 7.90 2 7 -9 121.39 9.00 2 7 -9 142.39 8.90 -2 7 9 137.79 7.70 -2 7 9 129.19 7.90 2 7 -9 146.59 7.90 2 7 -9 112.79 8.50 -2 7 9 137.39 7.80 -1 -7 9 2.40 0.90 1 -7 -9 1.40 1.10 -1 -7 9 1.00 1.00 -1 -7 9 3.10 1.00 -1 -7 9 3.60 1.30 1 -7 -9 2.60 1.50 -1 7 9 0.40 1.10 -1 7 9 2.20 1.10 1 7 -9 3.20 2.30 1 7 -9 2.70 1.30 1 7 -9 4.70 2.70 -1 7 9 3.10 1.20 1 7 -9 2.30 2.30 0 -7 -9 2.70 1.50 0 -7 9 3.00 1.00 0 -7 -9 2.80 1.10 0 -7 -9 0.80 1.00 0 -7 9 1.10 1.00 0 7 -9 3.90 2.20 0 7 9 4.50 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7 10 0.40 1.30 -5 7 10 2.10 0.80 -5 7 10 -0.10 1.10 5 7 -10 1.00 1.70 4 -7 -10 -0.20 1.10 -4 -7 10 0.80 0.90 -4 -7 10 0.70 1.20 -4 -7 10 -0.80 1.50 4 -7 -10 1.20 1.50 4 7 -10 1.00 3.60 4 7 -10 -1.10 3.50 -4 7 10 0.20 1.10 4 7 -10 2.40 2.80 4 7 -10 -1.10 1.50 -4 7 10 -0.40 0.80 -4 7 10 2.50 1.30 -3 -7 10 7.00 1.20 3 -7 -10 7.30 1.70 -3 -7 10 11.00 1.40 3 -7 -10 9.90 1.30 -3 -7 10 9.10 1.70 3 7 -10 5.10 3.30 3 7 -10 8.70 2.70 -3 7 10 9.30 1.50 -3 7 10 5.60 1.30 3 7 -10 8.40 1.70 -3 7 10 8.50 1.10 3 7 -10 7.60 3.20 -2 -7 10 30.50 3.00 2 -7 -10 35.90 3.20 -2 -7 10 27.80 2.40 -2 -7 10 33.00 2.50 -2 -7 10 31.20 2.40 2 -7 -10 30.60 2.50 -2 7 10 32.30 2.60 2 7 -10 27.60 4.30 -2 7 10 30.80 2.30 2 7 -10 31.50 3.00 2 7 -10 30.80 3.90 -2 7 10 33.10 2.50 -1 -7 10 35.90 2.60 1 -7 -10 40.70 3.40 1 -7 -10 33.20 2.50 -1 -7 10 34.00 2.60 -1 -7 10 39.70 3.10 -1 7 10 41.40 2.70 1 7 -10 43.00 4.90 1 7 -10 33.90 3.10 1 7 -10 42.80 4.00 1 7 -10 29.20 4.00 0 -7 10 6.90 1.30 0 -7 -10 5.50 1.60 0 -7 -10 4.80 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246.28 14.10 0 7 11 239.98 13.60 0 7 -11 240.48 13.50 0 7 -11 211.68 14.20 0 7 -11 206.28 13.90 1 -7 11 27.30 2.70 -1 -7 -11 34.80 2.30 -1 -7 -11 31.10 3.20 1 -7 11 29.50 2.30 1 -7 11 31.80 2.40 -1 -7 -11 33.50 2.60 -1 -7 -11 26.70 3.30 1 7 11 31.70 2.60 -1 7 -11 29.20 2.80 -1 7 -11 33.20 3.70 1 7 11 33.60 2.50 -1 7 -11 28.10 3.20 1 7 11 27.50 2.50 2 -7 11 34.60 2.50 -2 -7 -11 34.90 2.50 2 -7 11 32.80 2.50 -2 -7 -11 35.60 3.30 -2 7 -11 36.80 4.00 -2 7 -11 27.20 3.50 2 7 11 37.30 2.80 -2 7 -11 30.20 3.80 2 7 11 30.00 2.70 2 7 11 32.60 2.70 -3 -7 -11 7.70 1.70 -3 -7 -11 9.20 1.40 3 -7 11 9.80 1.30 3 -7 11 12.00 1.40 -3 7 -11 13.60 2.10 -3 7 -11 12.40 2.40 -3 7 -11 9.70 2.10 3 7 11 7.40 1.50 3 7 11 9.30 1.70 4 -7 11 3.20 1.10 -4 -7 -11 5.50 1.30 4 -7 11 7.80 1.20 -4 -7 -11 7.10 1.60 -4 7 -11 4.70 1.60 4 7 11 4.20 1.50 -4 7 -11 6.10 1.90 4 7 11 8.60 1.60 4 7 11 5.50 1.50 -4 7 -11 4.30 2.00 5 -7 11 18.80 2.10 -5 -7 -11 18.70 2.30 5 -7 11 23.40 2.10 5 7 11 15.40 2.10 5 7 11 22.20 2.60 -5 7 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6.90 1.20 -6 3 14 6.80 0.80 -6 3 14 6.70 1.00 6 3 -14 2.10 4.00 6 3 -14 4.10 1.00 6 3 -14 8.70 2.50 5 -3 -14 2.60 1.20 -5 -3 14 0.30 1.00 5 -3 -14 -0.20 1.10 5 -3 -14 1.00 0.70 -5 -3 14 0.50 0.80 5 3 -14 0.90 0.80 -5 3 14 1.90 0.60 5 3 -14 0.10 2.10 5 3 -14 -1.40 3.60 -5 3 14 1.50 0.80 -4 -3 14 0.60 0.90 4 -3 -14 3.70 1.10 -4 -3 14 1.50 0.70 4 -3 -14 2.60 1.80 4 -3 -14 3.00 0.70 -4 -3 14 1.70 1.00 -4 3 14 1.90 0.60 -4 3 14 3.00 0.80 -4 3 14 3.00 0.40 4 3 -14 1.20 1.80 -4 3 14 2.60 0.80 4 3 -14 0.70 3.30 4 3 -14 1.80 0.70 3 -3 -14 97.29 5.90 3 -3 -14 97.19 5.80 -3 -3 14 101.79 5.90 -3 -3 14 106.29 5.60 -3 -3 14 98.69 5.80 3 -3 -14 91.29 6.40 -3 3 14 92.09 5.60 3 3 -14 95.69 7.70 3 3 -14 100.89 6.30 -3 3 14 100.59 5.70 3 3 -14 103.59 5.60 2 -3 -14 1.00 0.60 -2 -3 14 0.60 0.40 -2 -3 14 0.20 1.70 2 -3 -14 -0.10 0.90 2 -3 -14 -0.30 1.80 -2 3 14 0.60 0.60 2 3 -14 -1.20 1.40 2 3 -14 -1.40 2.90 -2 3 14 -0.30 0.60 -1 -3 14 6.30 0.70 1 -3 -14 7.40 2.00 1 -3 -14 6.60 1.10 -1 -3 14 8.50 1.50 1 3 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1.80 4.70 -10 -4 14 17.90 2.50 -10 -4 14 26.90 3.10 10 -4 -14 18.30 2.00 10 -4 -14 20.80 3.10 -10 4 14 20.60 2.60 10 4 -14 13.00 4.40 10 4 -14 32.40 8.30 9 -4 -14 21.90 2.70 -9 -4 14 23.90 2.80 9 -4 -14 20.70 2.60 -9 -4 14 23.50 2.50 9 4 -14 27.20 7.20 9 4 -14 22.20 4.10 -9 4 14 23.20 2.40 -8 -4 14 32.50 3.60 8 -4 -14 33.60 2.70 -8 -4 14 31.40 2.70 8 4 -14 29.40 6.70 8 4 -14 29.20 3.90 -8 4 14 31.10 3.30 7 -4 -14 11.60 2.00 7 -4 -14 14.10 1.80 -7 -4 14 13.40 1.90 -7 4 14 10.40 1.60 7 4 -14 15.60 5.50 7 4 -14 10.30 2.80 -6 -4 14 9.80 1.40 -6 -4 14 10.80 1.70 6 -4 -14 9.80 1.30 6 -4 -14 12.20 1.80 6 4 -14 11.30 2.50 6 4 -14 14.50 4.90 -6 4 14 10.80 1.20 5 -4 -14 0.90 0.90 -5 -4 14 0.90 1.30 -5 -4 14 2.40 1.00 5 -4 -14 3.70 1.50 5 -4 -14 1.50 1.30 -5 4 14 1.50 0.60 -5 4 14 2.20 0.90 5 4 -14 3.30 2.20 5 4 -14 4.20 4.30 4 -4 -14 16.10 1.60 -4 -4 14 17.10 2.10 4 -4 -14 12.00 1.70 -4 -4 14 14.80 1.50 -4 -4 14 17.40 1.50 -4 4 14 17.80 1.30 4 4 -14 17.10 4.30 4 4 -14 16.00 2.30 -3 -4 14 1.90 1.20 3 -4 -14 0.50 1.10 3 -4 -14 3.10 1.90 -3 -4 14 0.80 0.60 -3 -4 14 1.50 1.00 3 -4 -14 0.00 0.70 -3 -4 14 2.20 0.80 -3 4 14 -0.10 0.70 -3 4 14 0.30 1.00 3 4 -14 4.20 3.50 -3 4 14 0.40 0.80 -3 4 14 0.40 0.70 3 4 -14 1.20 1.60 -2 -4 14 3.60 1.00 2 -4 -14 8.00 1.20 -2 -4 14 8.20 1.50 2 -4 -14 5.70 2.00 -2 -4 14 4.70 0.70 2 -4 -14 6.50 0.90 -2 -4 14 5.30 0.90 2 4 -14 5.30 1.50 2 4 -14 5.50 3.50 -2 4 14 5.50 0.80 -2 4 14 5.80 0.90 1 -4 -14 61.59 3.70 -1 -4 14 62.79 3.60 1 -4 -14 60.79 4.90 1 -4 -14 58.89 3.90 -1 -4 14 63.49 4.30 -1 -4 14 66.29 3.80 -1 4 14 66.39 3.70 -1 4 14 55.29 3.70 1 4 -14 53.19 4.10 -1 4 14 60.09 3.60 1 4 -14 55.29 5.90 0 -4 -14 20.90 2.20 0 -4 -14 20.90 2.70 0 -4 14 23.10 1.60 0 -4 14 24.40 1.50 0 4 -14 22.90 3.30 0 4 14 24.80 1.80 0 4 14 20.20 1.60 0 4 14 22.00 1.70 0 4 -14 20.40 2.50 1 -4 14 64.39 3.60 -1 -4 -14 60.99 7.50 1 -4 14 61.89 3.60 -1 -4 -14 62.39 4.00 -1 4 -14 63.49 4.20 1 4 14 66.79 3.80 1 4 14 59.79 3.80 -1 4 -14 56.29 5.10 1 4 14 60.19 3.80 2 -4 14 127.19 7.10 2 -4 14 128.29 7.10 2 -4 14 133.29 7.10 -2 -4 -14 128.69 7.30 -2 -4 -14 114.49 7.70 2 4 14 128.69 7.20 -2 4 -14 122.89 7.40 -2 4 -14 119.69 8.00 2 4 14 126.89 7.20 2 4 14 116.79 7.20 -3 -4 -14 0.70 1.00 3 -4 14 -0.10 0.70 3 -4 14 0.80 0.60 -3 -4 -14 0.10 1.80 3 -4 14 2.60 0.80 3 4 14 0.80 0.80 -3 4 -14 3.10 2.00 -3 4 -14 0.90 2.00 3 4 14 2.50 0.90 3 4 14 1.40 0.90 -3 4 -14 0.30 1.20 4 -4 14 54.49 3.00 -4 -4 -14 42.60 3.30 -4 -4 -14 44.30 3.60 4 -4 14 48.90 3.00 4 -4 14 49.10 3.00 -4 -4 -14 49.10 3.30 4 4 14 48.80 3.10 4 4 14 47.10 3.20 -4 4 -14 48.00 3.90 -4 4 -14 52.69 3.90 -4 4 -14 46.90 3.50 4 4 14 49.20 3.20 5 -4 14 123.99 7.30 5 -4 14 129.09 7.30 5 -4 14 129.49 7.20 5 4 14 121.29 7.40 5 4 14 120.59 7.30 -5 4 -14 140.19 7.70 -5 4 -14 127.69 7.60 5 4 14 126.59 7.40 6 -4 14 90.79 5.20 6 -4 14 87.99 5.20 -6 -4 -14 80.49 5.40 6 -4 14 88.99 5.30 6 4 14 88.19 5.40 6 4 14 90.29 5.30 6 4 14 95.39 5.30 7 -4 14 0.30 1.00 7 -4 14 -0.60 1.00 -7 -4 -14 0.60 1.30 7 -4 14 -0.20 1.00 7 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2.00 2.80 7 5 -14 6.30 6.00 -7 5 14 3.50 1.60 -6 -5 14 5.30 1.70 6 -5 -14 6.10 1.80 6 -5 -14 10.10 1.30 -6 -5 14 5.70 1.30 6 5 -14 4.80 5.30 -6 5 14 7.20 1.30 -6 5 14 8.50 1.00 6 5 -14 5.80 2.50 5 -5 -14 -1.70 1.40 -5 -5 14 0.00 1.30 5 -5 -14 -0.50 0.90 -5 -5 14 3.00 1.00 5 5 -14 1.40 2.00 5 5 -14 1.00 4.80 -5 5 14 -0.40 0.70 -5 5 14 0.60 1.00 4 -5 -14 -0.80 0.90 -4 -5 14 -0.40 1.00 4 -5 -14 0.40 1.50 -4 -5 14 0.00 0.60 -4 -5 14 -1.70 1.20 -4 -5 14 -0.50 0.80 4 5 -14 -1.60 1.80 -4 5 14 0.40 0.70 -4 5 14 -0.60 0.80 -4 5 14 -0.80 0.90 4 5 -14 -2.80 4.20 -3 -5 14 54.99 3.20 -3 -5 14 58.19 3.30 -3 -5 14 57.49 3.80 3 -5 -14 51.29 3.40 3 -5 -14 51.99 3.80 -3 5 14 52.69 3.20 -3 5 14 46.00 3.40 -3 5 14 51.39 3.40 3 5 -14 67.09 6.80 2 -5 -14 114.59 6.80 -2 -5 14 122.39 6.90 -2 -5 14 119.19 6.70 -2 -5 14 119.89 6.90 2 -5 -14 100.49 7.00 -2 -5 14 113.89 6.60 2 -5 -14 124.09 7.60 -2 5 14 124.69 6.80 2 5 -14 114.19 7.10 -2 5 14 112.49 6.60 -2 5 14 115.79 6.80 -1 -5 14 5.10 0.90 1 -5 -14 4.30 1.00 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10.40 1.70 4 -5 14 11.50 1.40 -4 -5 -14 13.80 1.60 4 -5 14 14.20 1.40 4 5 14 14.40 1.70 -4 5 -14 7.20 2.00 4 5 14 12.60 1.50 -4 5 -14 13.40 2.10 4 5 14 13.60 1.70 -4 5 -14 13.60 2.20 -4 5 -14 10.90 1.70 5 -5 14 0.60 0.90 -5 -5 -14 0.10 1.40 5 -5 14 -0.10 0.90 -5 -5 -14 -1.00 1.10 -5 5 -14 0.30 1.50 -5 5 -14 0.50 2.20 5 5 14 0.30 1.00 5 5 14 -0.70 1.10 -5 5 -14 -1.10 1.80 5 5 14 0.50 1.10 6 -5 14 29.80 2.30 6 -5 14 30.90 2.40 -6 -5 -14 30.70 2.60 6 5 14 28.50 2.60 6 5 14 30.70 2.60 6 5 14 34.20 2.60 -6 5 -14 31.60 3.40 -7 -5 -14 0.50 1.20 7 -5 14 1.30 1.30 7 -5 14 -0.40 1.10 7 -5 14 0.90 1.20 7 5 14 0.70 1.20 7 5 14 0.40 1.30 7 5 14 -0.30 1.30 -8 -5 -14 26.20 2.60 8 -5 14 30.10 2.40 8 -5 14 29.30 2.70 8 5 14 26.40 2.80 8 5 14 23.60 2.70 8 5 14 24.80 2.60 9 -5 14 2.70 1.40 9 -5 14 0.60 1.50 -9 -5 -14 -0.60 1.50 9 5 14 1.10 1.60 9 5 14 1.30 1.90 -10 -5 -14 3.80 1.80 10 -5 14 6.50 1.80 10 -5 14 7.60 1.70 10 5 14 6.30 2.20 -11 -6 14 4.00 2.90 11 -6 -14 2.20 2.30 11 -6 -14 5.90 3.10 -11 -6 14 2.80 1.90 11 6 -14 9.40 10.40 11 6 -14 -1.30 6.00 -10 -6 14 2.10 2.60 10 -6 -14 4.30 2.60 -10 -6 14 2.80 1.70 10 -6 -14 3.60 2.00 10 6 -14 -3.50 5.20 10 6 -14 13.50 9.60 -9 -6 14 -0.60 2.40 9 -6 -14 0.50 1.70 9 -6 -14 -1.70 2.30 -9 -6 14 0.40 1.70 9 6 -14 0.50 3.40 9 6 -14 -0.50 5.20 9 6 -14 -1.30 13.70 8 -6 -14 0.10 2.10 -8 -6 14 0.00 1.40 -8 -6 14 -0.20 2.80 8 -6 -14 1.40 1.50 8 6 -14 2.00 2.80 8 6 -14 4.80 7.30 -8 6 14 1.20 1.90 7 -6 -14 21.20 2.60 -7 -6 14 26.50 2.90 7 -6 -14 23.60 2.60 -7 -6 14 21.60 2.30 -7 6 14 16.40 2.30 7 6 -14 26.10 3.20 -7 6 14 26.50 3.10 7 6 -14 19.40 6.80 6 -6 -14 0.00 1.90 -6 -6 14 1.80 1.20 6 -6 -14 1.40 1.20 -6 -6 14 2.50 1.80 6 6 -14 6.50 3.80 -6 6 14 2.30 1.20 6 6 -14 1.30 5.70 6 6 -14 1.40 2.40 -5 -6 14 1.30 1.50 -5 -6 14 0.80 1.10 5 -6 -14 0.60 1.70 5 -6 -14 0.00 1.10 -5 6 14 1.90 1.30 -5 6 14 1.60 0.90 5 6 -14 2.40 5.50 5 6 -14 0.10 2.20 -5 6 14 2.10 1.10 5 6 -14 0.00 3.60 -4 -6 14 2.40 0.90 -4 -6 14 4.20 1.60 4 -6 -14 0.00 1.70 -4 -6 14 1.10 2.10 4 -6 -14 2.50 1.10 -4 6 14 1.70 0.90 -4 6 14 0.50 1.00 4 6 -14 0.60 2.80 4 6 -14 6.20 1.90 4 6 -14 3.30 4.50 -4 6 14 4.90 1.20 3 -6 -14 2.10 1.10 -3 -6 14 0.80 0.90 -3 -6 14 1.00 1.30 3 -6 -14 1.50 1.60 -3 -6 14 1.50 1.10 3 6 -14 -0.20 4.30 3 6 -14 1.30 1.70 -3 6 14 1.50 0.80 -3 6 14 -0.50 1.00 3 6 -14 1.10 3.10 -3 6 14 1.50 1.10 -2 -6 14 19.70 1.80 2 -6 -14 18.80 3.00 2 -6 -14 23.40 2.10 2 -6 -14 20.70 2.00 -2 -6 14 22.90 2.70 -2 -6 14 21.90 1.90 -2 6 14 18.90 1.90 2 6 -14 19.10 2.20 2 6 -14 19.20 3.90 1 -6 -14 1.30 1.50 -1 -6 14 0.90 1.20 -1 -6 14 0.30 0.90 -1 -6 14 0.40 0.90 1 -6 -14 1.70 2.60 1 -6 -14 0.70 1.00 1 6 -14 1.20 1.40 -1 6 14 1.60 1.00 1 6 -14 1.70 2.70 -1 6 14 0.50 1.20 1 6 -14 2.80 2.90 -1 6 14 0.40 0.80 0 -6 -14 16.50 3.00 0 -6 -14 14.60 1.90 0 -6 -14 14.20 1.80 0 -6 14 15.80 1.60 0 -6 14 13.60 1.60 0 6 14 14.30 1.80 0 6 -14 13.40 3.40 0 6 14 15.20 1.60 0 6 14 14.40 1.70 0 6 -14 19.00 3.30 0 6 -14 15.30 1.90 -1 -6 -14 57.79 4.10 1 -6 14 57.29 3.90 1 -6 14 54.39 3.50 1 -6 14 55.09 3.50 -1 -6 -14 55.39 5.60 1 6 14 60.29 3.80 -1 6 -14 54.19 5.50 -1 6 -14 58.89 4.10 1 6 14 61.09 3.70 -1 6 -14 51.79 5.40 1 6 14 58.39 3.70 2 -6 14 79.49 4.60 2 -6 14 72.69 4.80 -2 -6 -14 74.89 5.10 -2 -6 -14 66.69 6.10 2 -6 14 80.79 4.60 -2 6 -14 78.69 5.10 2 6 14 82.19 4.90 2 6 14 82.79 4.80 -2 6 -14 86.79 6.10 2 6 14 79.09 4.80 -2 6 -14 64.49 6.00 -3 -6 -14 32.30 2.90 3 -6 14 29.40 2.10 3 -6 14 29.20 3.30 -3 -6 -14 28.70 2.40 3 -6 14 29.20 2.20 -3 6 -14 24.00 2.80 -3 6 -14 35.60 3.90 3 6 14 28.20 2.50 3 6 14 29.10 2.40 -3 6 -14 27.70 3.10 3 6 14 27.20 2.40 -3 6 -14 27.50 3.00 -4 -6 -14 60.29 4.50 -4 -6 -14 65.69 4.10 4 -6 14 64.79 4.00 4 -6 14 67.69 4.00 -4 6 -14 61.39 4.90 4 6 14 66.79 4.30 4 6 14 66.49 4.20 -4 6 -14 71.19 5.20 4 6 14 62.39 4.20 -4 6 -14 57.39 4.60 5 -6 14 9.20 1.30 -5 -6 -14 12.40 1.80 5 -6 14 10.00 1.30 5 6 14 10.10 1.50 -5 6 -14 8.20 2.20 -5 6 -14 11.10 1.90 5 6 14 8.60 1.50 5 6 14 7.90 1.50 6 -6 14 0.40 1.10 6 -6 14 0.00 1.10 -6 -6 -14 0.90 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15 29.60 2.00 -4 -4 -15 25.10 2.90 -4 4 -15 27.30 3.40 4 4 15 26.80 2.20 -4 4 -15 29.50 2.80 4 4 15 31.80 2.20 -4 4 -15 31.90 3.20 4 4 15 26.90 2.20 5 -4 15 0.20 0.90 5 -4 15 0.00 0.90 -5 -4 -15 -0.50 1.30 5 -4 15 -0.80 0.80 5 4 15 -0.70 0.90 5 4 15 0.50 1.00 -5 4 -15 -0.10 1.20 -5 4 -15 1.50 1.50 5 4 15 -0.20 1.00 -5 4 -15 0.00 1.80 -6 -4 -15 2.60 1.30 6 -4 15 3.70 1.10 6 -4 15 2.20 1.00 -6 -4 -15 2.80 1.20 6 -4 15 3.20 1.00 6 4 15 1.10 1.10 6 4 15 2.60 1.10 6 4 15 6.20 1.20 7 -4 15 3.20 1.10 7 -4 15 1.90 1.20 7 -4 15 3.60 1.10 -7 -4 -15 1.70 1.40 7 4 15 2.60 1.30 7 4 15 2.80 1.20 7 4 15 2.70 1.10 8 -4 15 4.60 1.30 -8 -4 -15 3.20 1.50 8 -4 15 3.90 1.20 8 -4 15 5.20 1.30 8 4 15 2.50 1.40 8 4 15 5.50 1.40 8 4 15 6.20 1.80 9 -4 15 2.00 1.40 -9 -4 -15 1.10 1.70 9 -4 15 1.60 1.40 9 -4 15 0.00 1.40 9 4 15 0.70 1.50 9 4 15 1.20 1.50 9 4 15 0.10 1.50 10 -4 15 0.50 1.60 10 -4 15 -0.20 1.60 10 4 15 1.40 1.70 10 4 15 -0.30 1.80 -11 -5 15 0.60 1.70 11 -5 -15 2.40 2.70 -11 -5 15 2.90 2.90 11 -5 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5 15 101.19 6.00 4 5 -15 96.79 6.70 -4 5 15 105.09 5.90 -4 5 15 105.69 6.10 -3 -5 15 30.20 2.70 3 -5 -15 30.10 3.40 -3 -5 15 29.00 2.20 3 -5 -15 35.70 2.90 3 -5 -15 27.20 2.20 -3 -5 15 27.50 2.00 -3 5 15 27.40 2.10 -3 5 15 28.60 2.00 3 5 -15 26.80 4.40 3 5 -15 29.80 3.30 -3 5 15 25.10 2.20 2 -5 -15 43.90 3.70 2 -5 -15 49.99 3.30 -2 -5 15 50.29 3.10 2 -5 -15 58.29 4.90 -2 -5 15 51.19 3.60 -2 -5 15 50.19 3.10 -2 5 15 57.89 3.40 -2 5 15 51.09 3.10 -2 5 15 46.00 3.20 2 5 -15 40.90 3.80 2 5 -15 52.49 6.70 1 -5 -15 125.59 7.70 1 -5 -15 124.59 8.50 -1 -5 15 127.19 7.40 -1 -5 15 136.19 7.60 1 -5 -15 130.89 7.50 -1 -5 15 138.89 7.40 -1 5 15 125.49 7.50 1 5 -15 127.29 7.70 -1 5 15 140.09 7.50 -1 5 15 123.69 7.40 1 5 -15 113.29 9.20 0 -5 15 6.60 0.80 0 -5 -15 6.00 1.40 0 -5 15 7.70 1.20 0 -5 15 5.00 0.90 0 -5 -15 2.10 2.60 0 5 -15 10.50 3.20 0 5 -15 9.20 1.60 0 5 15 6.50 1.00 0 5 15 6.60 1.00 0 5 15 6.50 1.10 0 5 -15 4.50 2.60 1 -5 15 172.48 9.70 -1 -5 -15 169.78 10.70 -1 -5 -15 173.18 10.00 1 -5 15 170.78 9.70 1 5 15 186.38 9.90 -1 5 -15 169.68 10.70 -1 5 -15 155.58 10.00 1 5 15 177.38 9.90 1 5 15 175.18 9.80 2 -5 15 27.70 2.10 -2 -5 -15 36.70 2.90 2 -5 15 30.20 2.10 2 5 15 28.40 2.40 -2 5 -15 36.20 4.40 2 5 15 32.10 2.30 -2 5 -15 32.20 2.90 2 5 15 32.40 2.30 -2 5 -15 23.80 3.40 3 -5 15 109.09 6.00 3 -5 15 103.49 6.00 -3 -5 -15 97.79 6.70 -3 -5 -15 101.69 6.20 3 5 15 101.39 6.10 3 5 15 105.89 6.10 -3 5 -15 87.49 7.00 -3 5 -15 104.59 7.00 3 5 15 115.79 6.20 -3 5 -15 100.39 6.40 -4 -5 -15 40.60 3.20 4 -5 15 37.00 2.60 -4 -5 -15 38.60 2.90 4 -5 15 38.30 2.60 -4 -5 -15 34.40 3.40 -4 5 -15 34.70 3.30 -4 5 -15 35.80 3.50 4 5 15 39.20 2.80 -4 5 -15 45.80 3.90 4 5 15 43.90 2.80 -4 5 -15 38.20 3.80 4 5 15 41.00 2.90 5 -5 15 30.40 2.30 5 -5 15 26.20 2.30 -5 -5 -15 25.70 3.00 -5 -5 -15 30.10 2.60 5 5 15 33.40 2.50 -5 5 -15 31.40 3.80 5 5 15 37.20 2.60 5 5 15 36.50 2.60 6 -5 15 1.20 1.20 6 -5 15 0.20 1.00 6 -5 15 0.80 1.00 -6 -5 -15 0.70 1.30 6 5 15 -1.10 1.20 -6 5 -15 -0.50 1.90 6 5 15 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7 -6 -15 6.00 2.20 -7 -6 15 3.00 1.40 7 6 -15 6.50 2.70 -7 6 15 5.10 1.90 -7 6 15 6.60 1.60 7 6 -15 7.10 3.90 7 6 -15 5.60 6.70 6 -6 -15 47.60 3.20 -6 -6 15 43.00 4.00 6 -6 -15 47.00 4.20 -6 -6 15 36.90 3.10 6 6 -15 44.10 4.50 6 6 -15 42.20 6.80 -6 6 15 41.30 3.10 -6 6 15 40.50 2.70 5 -6 -15 5.70 2.00 -5 -6 15 9.80 1.40 5 -6 -15 7.10 1.40 -5 -6 15 4.20 1.90 5 6 -15 3.90 3.90 -5 6 15 8.70 1.50 5 6 -15 2.10 5.70 -5 6 15 9.50 1.60 -5 6 15 12.50 1.20 5 6 -15 9.30 2.40 4 -6 -15 18.80 2.10 -4 -6 15 14.90 1.90 4 -6 -15 17.00 2.20 -4 -6 15 24.30 2.80 4 6 -15 15.20 3.70 4 6 -15 20.70 5.50 4 6 -15 19.70 2.50 -4 6 15 18.30 1.90 -4 6 15 19.90 2.10 -4 6 15 20.50 1.70 -3 -6 15 135.69 8.00 3 -6 -15 144.59 8.50 3 -6 -15 141.79 8.20 -3 -6 15 138.99 8.30 -3 -6 15 137.39 8.10 -3 6 15 145.69 8.00 -3 6 15 130.59 8.10 3 6 -15 138.29 8.50 -3 6 15 147.99 8.30 3 6 -15 151.68 10.80 -2 -6 15 8.10 1.30 -2 -6 15 9.90 1.60 -2 -6 15 10.60 1.20 2 -6 -15 11.90 1.80 2 -6 -15 6.70 2.80 2 -6 -15 9.80 1.40 2 6 -15 7.80 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27.30 2.60 -7 -2 22 26.40 2.70 7 -2 -22 21.00 4.00 -7 2 22 27.30 3.50 7 2 -22 27.80 3.20 -7 2 22 28.30 2.60 7 2 -22 19.90 4.40 -6 -2 22 204.28 12.20 -6 -2 22 216.88 12.30 6 -2 -22 222.28 12.30 6 2 -22 210.08 13.30 6 2 -22 209.08 12.00 -6 2 22 218.08 12.00 -6 2 22 196.48 11.90 -5 -2 22 38.60 3.50 -5 -2 22 38.20 2.80 5 -2 -22 46.20 3.70 5 -2 -22 45.90 4.90 5 2 -22 43.30 3.40 -5 2 22 40.00 2.80 5 2 -22 38.60 4.50 -4 -2 22 13.30 1.50 4 -2 -22 11.30 3.50 4 -2 -22 15.60 2.00 4 2 -22 21.60 3.30 -4 2 22 15.70 1.20 -4 2 22 13.40 1.60 4 2 -22 17.60 1.70 4 2 -22 17.60 5.10 -3 -2 22 76.39 4.70 3 -2 -22 68.59 6.70 -3 -2 22 79.39 4.50 3 -2 -22 78.49 5.10 -3 2 22 79.39 4.40 -3 2 22 72.09 4.60 3 2 -22 74.19 6.50 3 2 -22 78.49 4.80 3 2 -22 70.59 8.60 -2 -2 22 11.80 1.50 2 -2 -22 14.30 1.80 2 -2 -22 12.70 3.40 -2 -2 22 13.60 1.40 2 2 -22 11.60 4.70 2 2 -22 17.10 2.90 -2 2 22 16.30 1.40 -2 2 22 10.70 1.30 1 -2 -22 122.29 8.20 -1 -2 22 112.79 6.40 -1 -2 22 113.69 6.30 1 -2 -22 100.19 6.70 -1 2 22 114.59 6.30 -1 2 22 112.59 6.40 1 2 -22 103.59 6.50 1 2 -22 101.39 9.90 1 2 -22 107.79 7.60 0 -2 22 27.70 2.20 0 -2 -22 23.60 3.50 0 -2 -22 33.80 2.90 0 -2 22 29.70 2.10 0 2 22 31.50 2.30 0 2 22 33.20 2.10 0 2 -22 25.30 3.10 0 2 -22 32.70 5.10 1 -2 22 121.29 7.20 -1 -2 -22 114.49 8.30 1 -2 22 131.89 7.30 -1 -2 -22 110.79 7.40 1 2 22 130.89 7.20 -1 2 -22 127.59 8.10 -1 2 -22 129.19 10.10 1 2 22 133.59 7.30 2 -2 22 228.28 12.20 -2 -2 -22 237.38 13.00 2 -2 22 201.98 12.20 -2 -2 -22 203.48 12.40 2 2 22 218.88 12.20 2 2 22 214.98 12.30 -2 2 -22 199.88 14.00 -2 2 -22 230.88 12.80 3 -2 22 27.80 2.30 -3 -2 -22 29.90 3.30 -3 -2 -22 24.00 2.80 3 -2 22 30.80 2.30 3 2 22 27.40 2.40 -3 2 -22 29.80 3.00 3 2 22 29.10 2.30 4 -2 22 28.00 2.30 -4 -2 -22 32.70 3.30 4 -2 22 32.60 2.50 4 2 22 30.70 2.50 4 2 22 28.30 2.60 -4 2 -22 32.00 4.00 5 -2 22 3.90 1.30 5 -2 22 2.40 1.30 -5 -2 -22 5.80 2.20 -5 2 -22 5.60 2.10 5 2 22 3.90 1.30 5 2 22 3.40 1.40 6 -2 22 3.50 1.40 -6 -2 -22 0.40 1.90 6 -2 22 2.00 1.30 6 2 22 2.60 1.30 6 2 22 0.00 1.40 -7 -2 -22 -0.20 2.40 7 -2 22 1.70 1.50 7 -2 22 1.10 1.60 7 2 22 0.20 1.40 7 2 22 1.20 1.60 -7 2 -22 1.90 2.40 8 -2 22 1.30 1.70 8 -2 22 1.00 1.70 8 2 22 -0.50 1.70 8 2 22 0.90 1.70 -11 -3 22 -0.80 2.00 -11 -3 22 1.00 3.20 11 -3 -22 -0.90 3.50 11 -3 -22 4.80 4.60 -11 3 22 0.50 3.20 11 3 -22 1.40 5.90 11 3 -22 0.60 10.50 10 -3 -22 0.10 4.20 -10 -3 22 1.60 1.90 10 -3 -22 -2.20 2.90 -10 -3 22 0.20 2.70 -10 3 22 -1.60 3.40 10 3 -22 2.60 9.60 10 3 -22 1.80 5.20 -9 -3 22 -2.30 2.10 9 -3 -22 1.10 2.80 -9 -3 22 1.90 1.70 9 -3 -22 -1.10 4.40 9 3 -22 -1.10 5.60 -9 3 22 1.00 2.40 9 3 -22 -0.20 8.40 8 -3 -22 3.60 1.70 -8 -3 22 4.60 1.70 -8 -3 22 7.00 2.40 8 -3 -22 6.10 2.40 8 -3 -22 8.70 3.80 8 3 -22 8.30 4.00 8 3 -22 13.40 7.60 -8 3 22 2.40 2.20 7 -3 -22 32.10 2.60 7 -3 -22 26.90 3.00 -7 -3 22 33.30 3.50 7 -3 -22 25.80 4.60 -7 -3 22 36.60 2.90 7 3 -22 31.20 9.00 -7 3 22 29.00 2.50 7 3 -22 29.60 4.50 7 3 -22 32.00 3.30 -6 -3 22 10.10 2.00 6 -3 -22 4.70 2.20 6 -3 -22 6.50 3.70 -6 -3 22 8.90 1.60 6 3 -22 6.60 1.60 6 3 -22 7.00 3.50 6 3 -22 9.60 6.10 -6 3 22 4.10 1.20 5 -3 -22 199.18 11.40 -5 -3 22 203.38 11.40 -5 -3 22 195.18 11.00 5 -3 -22 175.78 12.60 5 3 -22 199.28 12.30 5 3 -22 191.38 14.30 5 3 -22 196.88 11.10 -5 3 22 188.68 11.00 -4 -3 22 4.40 1.50 4 -3 -22 8.70 3.30 -4 -3 22 5.30 1.20 4 -3 -22 5.60 1.80 4 3 -22 1.40 1.40 4 3 -22 6.10 3.00 -4 3 22 4.60 1.00 4 3 -22 6.00 5.40 -4 3 22 4.50 0.80 -3 -3 22 4.20 1.00 3 -3 -22 0.40 1.50 3 -3 -22 1.30 3.20 3 3 -22 1.40 2.80 3 3 -22 2.10 1.20 3 3 -22 -5.10 4.90 -3 3 22 2.60 0.80 -3 3 22 2.60 1.00 -2 -3 22 144.19 7.90 -2 -3 22 145.39 8.00 2 -3 -22 129.49 8.30 2 -3 -22 139.89 9.80 2 3 -22 130.59 11.30 2 3 -22 137.09 9.00 -2 3 22 134.39 8.00 -2 3 22 140.79 7.80 -1 -3 22 1.60 0.90 1 -3 -22 2.60 3.40 -1 -3 22 2.70 1.00 1 -3 -22 2.70 1.60 -1 -3 22 0.60 0.80 -1 3 22 2.00 1.00 1 3 -22 1.60 2.40 -1 3 22 1.90 0.80 1 3 -22 -0.40 5.00 -1 3 22 2.00 1.10 0 -3 22 1.70 0.90 0 -3 -22 1.30 1.40 0 -3 -22 -0.50 3.10 0 -3 22 0.10 0.90 0 -3 22 -1.10 1.00 0 3 22 2.40 1.10 0 3 -22 2.90 4.90 0 3 22 0.70 1.00 0 3 22 0.00 0.80 0 3 -22 -3.60 2.10 -1 -3 -22 2.10 1.50 1 -3 22 3.30 1.00 -1 -3 -22 -0.90 2.60 1 -3 22 0.60 0.90 1 -3 22 0.50 1.00 -1 3 -22 3.70 2.30 -1 3 -22 4.00 4.50 1 3 22 1.10 1.10 1 3 22 0.20 0.90 1 3 22 1.10 1.10 -2 -3 -22 22.10 3.40 2 -3 22 25.90 2.20 2 -3 22 24.00 2.10 -2 -3 -22 23.20 2.70 2 -3 22 26.20 2.00 -2 3 -22 19.40 2.90 2 3 22 27.30 2.20 2 3 22 28.80 2.30 -2 3 -22 24.60 4.80 2 3 22 21.80 2.00 -3 -3 -22 9.30 2.90 -3 -3 -22 13.80 1.90 3 -3 22 13.30 1.60 3 -3 22 12.40 1.60 3 -3 22 10.70 1.50 3 3 22 14.50 1.80 3 3 22 14.50 1.80 -3 3 -22 15.90 2.50 3 3 22 10.60 1.40 -4 -3 -22 2.70 2.40 4 -3 22 3.90 1.30 4 -3 22 4.50 1.30 4 -3 22 5.30 1.30 4 3 22 7.00 1.30 -4 3 -22 3.60 3.50 4 3 22 1.50 1.20 4 3 22 4.30 1.30 -4 3 -22 3.60 2.20 -5 -3 -22 13.00 2.40 5 -3 22 13.10 1.70 5 -3 22 12.60 1.70 5 3 22 14.10 1.60 5 3 22 10.10 1.70 6 -3 22 17.80 2.10 6 -3 22 16.70 2.00 6 -3 22 23.20 2.40 -6 -3 -22 13.20 2.30 6 3 22 15.70 2.10 6 3 22 19.40 2.20 -6 3 -22 17.30 2.70 6 3 22 16.10 1.90 7 -3 22 4.00 1.50 -7 -3 -22 4.30 2.50 7 -3 22 6.60 1.90 7 -3 22 4.10 1.80 7 3 22 3.50 1.70 7 3 22 3.30 1.50 7 3 22 0.80 1.60 8 -3 22 0.50 1.90 8 -3 22 0.70 1.80 8 -3 22 -2.10 1.60 8 3 22 -0.60 1.60 8 3 22 -3.30 1.80 -10 -4 22 -0.90 1.90 -10 -4 22 0.40 3.10 10 -4 -22 1.80 4.60 10 -4 -22 1.70 3.10 10 4 -22 3.70 4.70 10 4 -22 -1.80 10.10 -10 4 22 -1.40 5.00 9 -4 -22 3.00 2.90 -9 -4 22 5.10 2.50 9 -4 -22 -0.70 3.90 -9 -4 22 4.10 1.90 9 4 -22 3.20 6.80 9 4 -22 4.80 9.00 -9 4 22 0.50 2.70 -8 -4 22 3.60 1.70 8 -4 -22 4.50 2.60 8 -4 -22 2.20 4.20 8 -4 -22 0.40 1.50 -8 -4 22 -0.20 2.50 8 4 -22 -1.60 3.90 8 4 -22 6.00 8.20 -8 4 22 2.30 2.40 -7 -4 22 5.10 2.40 7 -4 -22 -1.50 3.80 7 -4 -22 3.30 1.40 -7 -4 22 2.30 1.50 -7 4 22 3.90 1.30 7 4 -22 2.20 7.20 7 4 -22 5.10 3.80 -6 -4 22 -2.00 2.10 6 -4 -22 0.40 3.70 6 -4 -22 -1.80 2.10 6 -4 -22 1.20 1.30 -6 -4 22 1.60 1.30 -6 4 22 0.90 1.10 6 4 -22 1.70 6.90 6 4 -22 3.40 3.60 -5 -4 22 1.00 1.30 5 -4 -22 2.10 3.50 5 -4 -22 1.10 1.20 5 -4 -22 -1.20 1.90 -5 -4 22 1.00 1.80 -5 4 22 -0.20 1.00 5 4 -22 0.10 3.20 5 4 -22 -2.80 6.30 -4 -4 22 6.70 1.40 -4 -4 22 11.40 1.80 4 -4 -22 7.50 2.10 4 -4 -22 6.20 3.90 4 4 -22 4.80 5.90 4 4 -22 6.00 3.00 -4 4 22 8.30 1.30 3 -4 -22 63.19 4.90 -3 -4 22 69.89 4.20 -3 -4 22 73.99 4.80 3 -4 -22 49.50 7.00 -3 4 22 64.59 4.30 -3 4 22 72.79 4.00 3 4 -22 65.59 5.90 -3 4 22 69.29 4.20 3 4 -22 55.49 7.20 2 -4 -22 22.50 2.30 -2 -4 22 21.30 1.90 2 -4 -22 17.50 4.20 2 4 -22 26.20 5.90 2 4 -22 23.10 3.10 -2 4 22 19.00 2.10 -2 4 22 20.20 2.00 -2 4 22 20.00 1.70 1 -4 -22 11.00 4.00 1 -4 -22 13.60 2.00 -1 -4 22 15.50 1.60 -1 -4 22 15.10 1.50 1 4 -22 19.70 2.70 -1 4 22 15.00 1.90 1 4 -22 18.50 5.20 -1 4 22 18.40 1.90 -1 4 22 18.80 1.70 0 -4 22 1.30 1.00 0 -4 -22 1.00 1.60 0 -4 22 2.00 1.30 0 -4 22 2.40 0.90 0 -4 -22 1.20 3.40 0 4 22 2.40 1.00 0 4 22 1.00 1.10 0 4 -22 1.30 2.20 0 4 22 2.50 1.20 0 4 -22 -1.10 4.80 1 -4 22 21.20 1.90 -1 -4 -22 27.90 3.10 1 -4 22 22.70 2.20 -1 -4 -22 13.80 3.40 1 -4 22 23.20 1.90 1 4 22 22.70 2.10 -1 4 -22 26.60 3.10 -1 4 -22 25.60 5.00 1 4 22 26.00 2.30 1 4 22 25.10 2.10 -2 -4 -22 49.80 3.80 2 -4 22 45.20 3.00 2 -4 22 40.70 3.20 2 -4 22 47.70 3.10 -2 -4 -22 44.30 5.20 2 4 22 50.99 3.20 2 4 22 42.50 3.20 -2 4 -22 45.30 4.90 -2 4 -22 49.99 4.70 2 4 22 43.50 3.10 -3 -4 -22 -2.80 2.70 3 -4 22 3.00 1.20 -3 -4 -22 -0.60 1.70 3 -4 22 -0.70 1.20 3 -4 22 -0.90 1.00 -3 4 -22 -0.20 2.20 3 4 22 0.30 1.20 3 4 22 1.10 1.10 -3 4 -22 -1.70 3.40 3 4 22 0.00 1.20 -3 4 -22 0.20 3.30 -4 -4 -22 6.10 2.60 4 -4 22 4.10 1.30 4 -4 22 3.20 1.40 4 -4 22 5.20 1.40 -4 -4 -22 8.00 3.40 4 4 22 5.30 1.30 4 4 22 4.40 1.30 -4 4 -22 9.80 2.60 4 4 22 2.60 1.40 5 -4 22 13.20 1.80 5 -4 22 10.20 1.70 -5 -4 -22 13.40 2.50 5 -4 22 13.00 1.50 5 4 22 10.90 1.80 5 4 22 11.10 1.70 5 4 22 16.70 2.00 -5 4 -22 10.20 2.60 6 -4 22 0.00 1.50 6 -4 22 1.70 1.60 6 -4 22 0.20 1.30 6 4 22 0.20 1.70 6 4 22 2.10 1.50 -6 4 -22 3.00 2.40 6 4 22 0.20 1.40 7 -4 22 14.20 2.10 7 4 22 12.20 2.20 7 4 22 10.80 1.90 7 4 22 12.20 1.80 8 -4 22 4.90 2.10 8 -4 22 3.90 1.70 8 -4 22 -1.00 1.90 8 4 22 0.80 1.70 8 4 22 -1.00 2.00 -10 -5 22 20.40 2.70 10 -5 -22 13.00 5.80 -10 -5 22 19.70 3.80 10 -5 -22 21.40 4.00 10 5 -22 14.80 10.80 -10 5 22 21.20 3.70 10 5 -22 24.80 5.50 9 -5 -22 18.20 4.80 -9 -5 22 13.40 3.30 9 -5 -22 10.40 2.10 -9 -5 22 11.10 2.10 9 -5 -22 18.70 3.60 9 5 -22 22.00 9.80 9 5 -22 20.70 9.90 8 -5 -22 -0.50 4.10 8 -5 -22 3.00 1.60 -8 -5 22 1.10 2.80 -8 -5 22 0.80 1.60 8 -5 -22 3.20 2.90 8 5 -22 4.30 4.30 8 5 -22 5.40 8.40 -8 5 22 -0.90 2.60 7 -5 -22 -1.50 2.40 -7 -5 22 -1.10 2.30 7 -5 -22 0.00 1.40 -7 -5 22 0.20 1.40 7 -5 -22 0.70 3.70 -7 5 22 -0.20 1.60 7 5 -22 -1.60 7.80 7 5 -22 -2.20 3.60 -6 -5 22 4.90 1.60 6 -5 -22 5.90 1.60 6 -5 -22 4.10 2.30 -6 -5 22 4.10 2.20 6 -5 -22 3.90 4.20 6 5 -22 1.60 3.20 -6 5 22 7.40 1.30 6 5 -22 -0.60 7.10 -5 -5 22 -0.60 1.50 -5 -5 22 0.90 2.10 5 -5 -22 0.10 3.60 -5 -5 22 -0.10 1.10 5 -5 -22 -1.30 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5.70 -8 3 28 9.30 3.00 8 3 -28 2.70 9.80 -7 -3 28 0.60 1.80 -7 -3 28 3.20 2.70 7 -3 -28 2.30 2.90 7 -3 -28 1.70 5.30 7 3 -28 2.80 5.00 -7 3 28 3.30 1.90 7 3 -28 10.40 8.90 -6 -3 28 1.40 2.60 6 -3 -28 0.00 2.60 -6 -3 28 -1.40 1.60 6 -3 -28 -3.20 5.40 6 3 -28 -6.00 4.60 6 3 -28 1.10 8.60 -6 3 28 3.00 1.60 6 3 -28 -2.00 2.30 5 -3 -28 2.10 2.40 -5 -3 28 7.20 1.90 -5 -3 28 5.00 2.50 5 -3 -28 5.20 5.20 5 3 -28 3.90 4.30 5 3 -28 8.40 2.20 -5 3 28 4.30 1.60 5 3 -28 12.50 8.30 -4 -3 28 11.50 1.80 4 -3 -28 10.20 5.10 -4 -3 28 9.70 2.40 4 3 -28 13.70 2.30 4 3 -28 -0.10 8.00 4 3 -28 4.20 4.10 -4 3 28 12.30 1.70 3 -3 -28 3.50 4.80 -3 -3 28 1.80 1.40 3 -3 -28 0.40 2.10 3 3 -28 2.20 7.40 3 3 -28 -2.00 3.70 2 -3 -28 2.00 2.10 -2 -3 28 1.60 1.40 2 -3 -28 -1.10 5.10 -2 -3 28 -0.70 1.70 -2 3 28 -1.30 1.20 2 3 -28 -1.60 3.60 -2 3 28 -0.40 1.30 2 3 -28 -1.00 9.60 1 -3 -28 3.50 5.80 -1 -3 28 -0.20 1.50 1 -3 -28 2.50 2.20 -1 -3 28 -0.70 1.30 -1 3 28 -0.10 1.30 -1 3 28 -0.20 1.40 1 3 -28 0.70 7.10 1 3 -28 0.30 3.20 0 -3 28 4.00 1.50 0 -3 -28 1.70 2.30 0 -3 -28 0.90 3.90 0 -3 28 1.00 1.30 0 -3 28 0.30 1.60 0 3 28 1.30 1.60 0 3 -28 3.40 6.60 0 3 28 0.90 1.30 0 3 -28 -0.70 3.10 -1 -3 -28 3.70 2.00 1 -3 28 3.30 1.70 1 -3 28 5.90 1.60 1 -3 28 3.20 1.50 -1 -3 -28 -1.00 3.90 1 3 28 5.50 1.50 -1 3 -28 2.50 6.30 1 3 28 5.30 1.70 -1 3 -28 3.70 3.20 -2 -3 -28 7.60 2.40 -2 -3 -28 10.60 4.00 2 -3 28 3.70 1.40 2 -3 28 7.00 1.80 2 -3 28 5.40 1.80 2 3 28 6.50 1.60 2 3 28 5.00 1.80 -2 3 -28 0.60 3.20 -2 3 -28 7.70 5.70 3 -3 28 36.20 2.80 -3 -3 -28 28.60 3.10 3 -3 28 31.00 3.10 3 -3 28 32.40 3.30 -3 -3 -28 20.40 4.20 3 3 28 24.60 3.20 3 3 28 35.40 2.90 -3 3 -28 28.40 4.00 4 -3 28 0.00 1.90 -4 -3 -28 0.90 3.10 4 -3 28 0.40 2.00 4 -3 28 2.50 1.50 4 3 28 4.00 2.10 4 3 28 1.80 1.70 -4 3 -28 -2.50 3.00 5 -3 28 3.50 2.30 5 -3 28 10.40 1.80 5 -3 28 8.20 2.30 -5 -3 -28 8.50 5.10 -5 3 -28 6.60 3.10 5 3 28 6.50 2.10 5 3 28 5.70 2.00 -7 -4 28 -0.60 2.80 7 -4 -28 0.20 5.40 -7 -4 28 -0.30 1.90 7 -4 -28 -2.90 2.90 -7 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0.20 2.50 3 5 -28 1.30 7.80 3 5 -28 5.00 3.60 -3 5 28 2.60 1.60 2 -5 -28 -1.80 2.30 -2 -5 28 2.10 1.80 2 -5 -28 1.30 5.60 -2 -5 28 0.40 2.30 -2 5 28 -0.30 1.70 2 5 -28 -1.20 3.50 2 5 -28 -1.40 7.70 1 -5 -28 4.10 5.40 1 -5 -28 5.90 2.50 -1 -5 28 7.40 1.80 -1 5 28 9.60 1.70 1 5 -28 5.70 3.60 -1 5 28 6.60 2.10 1 5 -28 6.50 7.70 -1 5 28 6.10 1.90 0 -5 -28 0.30 2.40 0 -5 28 2.40 1.70 0 -5 -28 3.80 6.30 0 5 28 -0.20 1.80 0 5 28 0.40 1.60 0 5 -28 2.60 6.70 0 5 -28 4.00 3.50 0 5 28 1.60 2.00 1 -5 28 1.40 1.70 -1 -5 -28 -1.00 2.30 -1 -5 -28 -1.20 4.40 1 5 28 -0.30 2.00 1 5 28 -0.60 1.70 -1 5 -28 -0.30 5.50 -1 5 -28 1.20 3.20 1 5 28 -1.60 1.90 -2 -5 -28 6.50 4.30 2 -5 28 3.30 1.80 2 -5 28 3.90 1.50 -2 -5 -28 4.20 2.40 2 5 28 6.40 2.30 2 5 28 4.50 1.80 -2 5 -28 1.30 3.10 -2 5 -28 0.30 5.50 2 5 28 3.90 2.00 -2 5 -28 0.80 5.50 -3 -5 -28 2.10 2.70 3 -5 28 1.20 1.70 3 -5 28 0.20 1.80 -3 -5 -28 -2.40 4.20 -3 5 -28 0.00 3.00 3 5 28 -1.10 1.80 3 5 28 1.20 2.20 -3 5 -28 -2.00 4.80 3 5 28 1.90 2.20 5 -6 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5.90 2 4 30 11.90 2.20 4 -5 -30 14.20 3.20 4 -5 -30 8.80 6.80 -4 -5 30 21.20 2.80 -4 -5 30 19.60 3.60 4 5 -30 19.20 4.60 -4 5 30 18.70 2.40 4 5 -30 14.20 9.50 -3 -5 30 15.50 2.40 -3 -5 30 11.50 3.00 3 -5 -30 16.40 6.90 3 -5 -30 9.70 3.00 3 5 -30 5.40 4.20 -3 5 30 14.50 2.20 3 5 -30 12.30 9.40 -2 -5 30 1.40 2.10 2 -5 -30 4.60 6.10 2 -5 -30 0.30 2.80 -2 -5 30 2.80 2.70 2 5 -30 -1.20 8.90 -2 5 30 5.30 2.00 2 5 -30 1.90 4.00 1 -5 -30 22.40 3.50 1 -5 -30 11.40 5.70 -1 -5 30 33.20 3.20 -1 5 30 28.50 3.30 1 5 -30 25.60 4.50 1 5 -30 22.80 8.30 0 -5 30 8.50 2.00 0 -5 -30 2.10 4.90 0 -5 -30 5.10 2.90 0 5 -30 10.90 7.50 0 5 30 8.60 2.20 0 5 -30 0.80 3.80 0 5 30 8.00 2.10 7 0 -31 11.70 3.40 -7 0 31 3.30 2.90 7 0 -31 4.90 5.50 -7 0 31 5.70 2.30 6 0 -31 -0.30 2.90 6 0 -31 2.00 5.50 5 0 -31 -2.00 5.00 -5 0 31 0.90 1.90 5 0 -31 0.10 2.80 -4 0 31 1.20 1.80 4 0 -31 -3.70 2.60 4 0 -31 1.20 4.80 3 0 -31 51.59 6.20 3 0 -31 49.50 4.90 -3 0 31 44.90 3.70 -2 0 31 -1.30 1.30 2 0 -31 2.00 4.50 -2 0 31 2.40 1.70 2 0 -31 -2.30 2.50 -1 0 31 35.70 2.80 1 0 -31 29.00 5.20 -1 0 31 30.80 3.10 1 0 -31 36.10 3.40 1 0 -31 25.00 8.00 0 0 31 3.60 1.80 0 0 -31 2.10 4.10 0 0 -31 -0.40 2.40 0 0 -31 2.90 8.20 0 0 31 0.90 1.40 1 0 31 9.00 1.70 1 0 31 15.60 2.30 -1 0 -31 12.20 4.30 2 0 31 -0.30 1.50 -2 0 -31 0.80 3.90 2 0 31 0.90 1.90 -3 0 -31 17.70 4.10 3 0 31 27.40 3.00 3 0 31 23.80 2.90 7 -1 -31 1.90 3.20 -7 -1 31 2.10 2.80 -7 -1 31 2.80 2.00 7 -1 -31 -3.30 5.50 -7 1 31 4.10 2.40 -7 1 31 4.20 3.00 7 1 -31 -0.40 5.60 6 -1 -31 1.50 5.70 6 -1 -31 0.00 3.10 -6 -1 31 1.90 2.60 -6 1 31 1.10 2.00 6 1 -31 -1.40 5.50 6 1 -31 3.00 3.50 5 -1 -31 4.00 2.80 5 -1 -31 -2.70 5.10 5 1 -31 -6.10 9.30 -5 1 31 1.10 1.90 5 1 -31 0.50 5.10 5 1 -31 -1.00 3.00 -4 -1 31 25.20 3.30 4 -1 -31 17.50 5.60 4 -1 -31 25.00 3.30 4 1 -31 24.80 5.60 4 1 -31 18.20 9.20 -4 1 31 29.90 2.90 4 1 -31 27.80 4.40 3 -1 -31 1.20 2.50 -3 -1 31 2.40 1.60 -3 -1 31 6.00 2.00 3 -1 -31 6.80 5.30 3 1 -31 -0.30 5.10 3 1 -31 2.00 4.30 -3 1 31 2.30 1.70 3 1 -31 1.60 8.20 -2 -1 31 0.70 1.40 -2 -1 31 1.70 1.80 2 -1 -31 1.50 2.30 2 -1 -31 -1.00 4.70 2 1 -31 0.00 2.30 -2 1 31 -0.10 1.30 2 1 -31 2.10 8.10 2 1 -31 -1.60 4.20 -2 1 31 2.00 1.70 -1 -1 31 12.50 1.70 1 -1 -31 10.60 4.70 1 -1 -31 12.80 8.40 -1 -1 31 14.20 2.10 1 -1 -31 10.10 2.60 -1 1 31 13.60 2.00 1 1 -31 9.40 4.20 -1 1 31 15.10 1.70 1 1 -31 9.00 8.40 0 -1 -31 1.70 8.10 0 -1 -31 0.40 4.30 0 -1 -31 2.20 2.30 0 -1 31 -0.60 1.50 0 -1 31 -1.10 1.90 0 1 -31 0.60 4.10 0 1 -31 0.20 8.00 0 1 31 3.40 1.80 0 1 31 0.60 1.40 1 -1 31 2.80 1.90 1 -1 31 1.60 1.40 -1 -1 -31 4.10 2.50 -1 -1 -31 5.40 4.20 -1 1 -31 -2.20 3.80 1 1 31 3.50 1.90 1 1 31 3.60 1.90 2 -1 31 2.50 1.90 -2 -1 -31 9.10 4.20 2 -1 31 5.40 1.70 2 1 31 5.60 1.90 -2 1 -31 3.90 3.70 3 -1 31 2.30 2.00 -3 -1 -31 0.10 3.70 3 -1 31 0.30 1.60 3 1 31 0.90 1.70 -3 1 -31 -2.20 3.60 3 1 31 1.60 1.80 -6 -2 31 4.40 2.70 6 -2 -31 6.30 3.20 6 -2 -31 5.80 5.70 6 2 -31 17.00 5.70 -6 2 31 4.70 2.10 6 2 -31 7.50 10.20 6 2 -31 6.40 3.20 5 -2 -31 15.80 6.10 -5 -2 31 16.20 3.10 5 -2 -31 19.00 3.30 5 2 -31 8.90 9.50 5 2 -31 21.70 3.20 -5 2 31 11.10 2.10 5 2 -31 11.70 5.10 4 -2 -31 20.10 3.20 4 -2 -31 11.10 5.90 4 2 -31 26.70 9.50 -4 2 31 25.30 2.80 4 2 -31 20.80 5.30 -3 -2 31 2.70 2.00 -3 -2 31 2.40 1.60 3 -2 -31 1.90 5.30 3 -2 -31 2.30 2.70 3 2 -31 4.20 2.60 3 2 -31 4.00 4.40 -3 2 31 2.10 1.70 3 2 -31 6.30 9.00 2 -2 -31 14.40 2.90 -2 -2 31 15.90 1.90 -2 -2 31 10.50 2.20 2 -2 -31 5.50 5.20 2 2 -31 11.20 4.60 2 2 -31 5.50 8.50 -2 2 31 14.10 2.20 1 -2 -31 0.90 2.30 -1 -2 31 1.10 1.40 -1 -2 31 -1.10 1.90 1 -2 -31 -3.60 4.70 -1 2 31 0.70 1.70 -1 2 31 1.10 1.40 1 2 -31 0.40 3.60 1 2 -31 -2.30 8.60 0 -2 -31 1.70 2.60 0 -2 -31 3.30 4.70 0 -2 31 6.90 2.10 0 -2 31 3.10 1.50 0 2 -31 2.00 4.00 0 2 31 5.00 1.70 0 2 -31 2.50 10.50 0 2 31 2.00 1.50 -1 -2 -31 2.10 2.40 -1 -2 -31 4.80 4.50 1 -2 31 1.40 1.90 1 -2 31 4.50 1.60 1 2 31 1.60 1.80 1 2 31 2.90 2.00 -1 2 -31 5.60 7.80 -1 2 -31 2.00 3.90 -2 -2 -31 11.90 4.30 2 -2 31 9.10 1.80 2 -2 31 11.40 2.30 2 2 31 7.90 2.10 -2 2 -31 3.90 3.90 2 2 31 10.00 1.90 -3 -2 -31 3.90 3.90 3 -2 31 2.80 2.20 3 -2 31 -0.10 1.60 -3 2 -31 0.90 3.70 3 2 31 -1.10 1.80 3 2 31 -0.40 2.00 -6 -3 31 -0.50 3.10 -6 -3 31 1.80 1.90 6 -3 -31 -0.20 6.50 6 -3 -31 -0.20 3.00 6 3 -31 8.20 10.80 6 3 -31 -2.00 5.20 -6 3 31 2.30 2.00 -5 -3 31 10.90 2.90 5 -3 -31 15.40 6.10 -5 3 31 10.30 2.10 5 3 -31 10.60 10.60 5 3 -31 8.90 5.00 4 -3 -31 4.10 2.70 4 -3 -31 8.50 5.70 -4 -3 31 5.20 2.10 -4 -3 31 4.80 2.60 4 3 -31 8.90 4.90 -4 3 31 0.40 1.80 4 3 -31 0.30 9.70 3 -3 -31 -2.70 2.70 3 -3 -31 2.20 5.60 -3 -3 31 -0.70 1.80 -3 3 31 -0.40 1.70 3 3 -31 3.60 9.20 3 3 -31 -0.40 4.20 2 -3 -31 6.90 5.60 2 -3 -31 0.90 2.80 -2 -3 31 0.80 1.70 2 3 -31 -0.80 3.80 -2 3 31 0.70 1.70 2 3 -31 0.00 8.90 1 -3 -31 10.70 2.70 1 -3 -31 5.70 5.10 -1 -3 31 11.30 2.50 -1 -3 31 14.10 2.00 1 3 -31 17.90 8.20 -1 3 31 13.20 2.00 1 3 -31 9.30 4.00 -1 3 31 15.70 1.90 0 -3 -31 -0.10 4.80 0 -3 31 2.70 2.20 0 -3 31 1.40 1.60 0 -3 -31 0.70 2.50 0 3 -31 5.80 8.00 0 3 31 1.30 1.60 0 3 31 1.30 1.80 0 3 -31 -3.70 3.50 -1 -3 -31 5.50 2.70 1 -3 31 10.20 1.80 1 -3 31 9.20 2.30 -1 -3 -31 9.20 4.80 1 3 31 6.10 2.10 -1 3 -31 7.10 7.80 1 3 31 5.60 1.90 -1 3 -31 8.50 3.90 2 -3 31 0.50 2.20 2 -3 31 0.70 2.20 -2 -3 -31 -0.10 4.50 -2 -3 -31 0.40 2.60 2 -3 31 1.40 1.70 -2 3 -31 -3.20 3.80 2 3 31 2.10 1.80 2 3 31 -2.00 2.00 -2 3 -31 3.80 6.40 -4 -4 31 4.80 2.80 4 -4 -31 9.90 6.40 4 -4 -31 5.70 2.90 -4 -4 31 3.30 2.40 4 4 -31 -0.20 4.60 4 4 -31 2.60 10.20 -4 4 31 1.70 1.90 3 -4 -31 1.20 6.00 3 -4 -31 -1.20 2.90 -3 -4 31 0.50 2.90 -3 -4 31 6.60 2.80 3 4 -31 -3.80 4.00 3 4 -31 1.30 9.40 -3 4 31 4.90 1.90 -2 -4 31 1.50 1.90 2 -4 -31 -0.90 2.80 2 -4 -31 -1.00 6.00 2 4 -31 3.80 8.80 2 4 -31 -1.10 4.00 -2 4 31 0.10 1.80 -1 -4 31 2.10 1.90 1 -4 -31 -2.80 2.70 1 -4 -31 5.90 5.30 -1 4 31 1.80 1.80 1 4 -31 -2.00 8.20 1 4 -31 2.50 3.70 0 -4 -31 18.40 5.50 0 -4 31 28.10 3.10 0 4 -31 25.50 8.30 0 4 -31 28.00 4.60 0 4 31 25.90 3.10 0 4 31 31.30 3.50 1 -4 31 5.40 2.60 1 -4 31 1.60 2.00 -1 -4 -31 1.00 4.80 -1 -4 -31 0.60 2.60 1 4 31 1.40 2.10 -1 4 -31 -1.70 3.90 -1 4 -31 0.20 7.00 1 4 31 0.50 1.80 6 0 -32 -0.90 3.30 6 0 -32 9.00 5.90 5 0 -32 0.20 5.80 -5 0 32 0.40 2.00 5 0 -32 1.80 3.00 -4 0 32 -0.10 2.00 4 0 -32 1.70 5.40 4 0 -32 0.10 2.90 3 0 -32 -5.90 9.20 -3 0 32 4.60 1.90 3 0 -32 -0.90 2.60 3 0 -32 -0.10 4.90 2 0 -32 -0.80 8.60 -2 0 32 0.60 1.40 2 0 -32 -0.50 4.70 2 0 -32 3.20 2.60 -2 0 32 1.70 1.90 1 0 -32 0.90 4.60 -1 0 32 -0.60 1.80 1 0 -32 6.70 2.50 -1 0 32 0.50 1.50 0 0 -32 10.60 4.80 0 0 -32 -1.80 8.70 0 0 32 11.10 2.20 -1 0 -32 -0.10 4.30 1 0 32 0.20 1.80 1 0 32 2.20 1.50 -2 0 -32 15.80 4.60 2 0 32 16.50 2.10 6 -1 -32 5.00 3.30 -6 -1 32 6.60 2.80 6 -1 -32 0.00 5.90 6 1 -32 -0.90 10.50 -6 1 32 0.20 2.30 6 1 -32 7.90 5.80 6 1 -32 0.80 3.30 5 -1 -32 9.30 5.80 5 -1 -32 0.80 3.00 5 1 -32 -1.00 3.10 5 1 -32 -2.00 5.10 -5 1 32 3.10 2.10 5 1 -32 3.50 9.80 4 -1 -32 1.30 2.80 -4 -1 32 1.10 2.10 4 -1 -32 2.00 5.50 4 1 -32 -3.50 5.00 4 1 -32 5.40 9.70 -4 1 32 2.60 1.90 4 1 -32 2.70 2.90 3 -1 -32 2.80 2.80 -3 -1 32 -1.30 2.00 3 -1 -32 -5.30 5.10 3 1 -32 0.90 2.70 3 1 -32 2.50 4.80 3 1 -32 -2.60 8.90 -3 1 32 2.50 1.90 2 -1 -32 1.80 5.10 2 -1 -32 5.20 2.80 -2 -1 32 2.90 2.00 -2 -1 32 1.30 1.50 2 1 -32 7.60 4.80 2 1 -32 2.00 2.60 -2 1 32 1.60 1.90 2 1 -32 -2.40 8.70 1 -1 -32 2.50 2.80 -1 -1 32 2.10 2.00 1 -1 -32 4.10 9.00 -1 -1 32 3.30 1.50 1 -1 -32 2.20 4.80 1 1 -32 2.50 4.30 -1 1 32 0.90 1.70 1 1 -32 -1.00 8.90 -1 1 32 0.30 1.50 0 -1 32 2.90 1.50 0 -1 -32 2.30 4.60 0 -1 -32 5.30 2.60 0 -1 32 2.30 2.00 0 1 -32 -0.80 9.10 0 1 32 3.10 2.00 0 1 32 1.00 1.50 0 1 -32 -3.30 4.10 -1 -1 -32 5.70 4.50 1 -1 32 1.90 1.60 1 -1 32 0.50 1.90 1 1 32 4.40 1.70 -1 1 -32 5.80 4.20 1 1 32 4.00 2.00 -2 -1 -32 13.40 4.70 2 -1 32 16.20 2.00 2 -1 32 13.10 2.50 2 1 32 16.50 2.20 -2 1 -32 9.90 4.30 2 1 32 12.50 2.10 5 -2 -32 15.40 6.50 -5 -2 32 7.40 3.10 5 -2 -32 11.50 3.20 5 2 -32 9.90 3.40 5 2 -32 15.70 10.50 -5 2 32 4.40 2.10 5 2 -32 7.60 5.40 4 -2 -32 8.40 3.00 4 -2 -32 10.90 6.10 -4 2 32 10.50 2.10 4 2 -32 7.40 9.80 4 2 -32 7.10 4.90 -3 -2 32 11.70 2.00 3 -2 -32 3.50 5.70 3 -2 -32 11.10 3.10 3 2 -32 10.10 9.60 -3 2 32 10.60 2.10 3 2 -32 1.60 4.60 2 -2 -32 23.00 3.20 2 -2 -32 15.80 5.90 -2 -2 32 25.10 2.80 -2 -2 32 23.40 3.10 -2 2 32 20.80 2.50 2 2 -32 13.10 8.90 2 2 -32 21.80 4.90 1 -2 -32 23.90 5.60 -1 -2 32 26.60 3.40 1 -2 -32 26.90 3.50 -1 -2 32 32.20 3.30 -1 2 32 26.70 2.70 1 2 -32 12.50 9.30 1 2 -32 30.90 5.00 0 -2 -32 6.50 5.00 0 -2 32 3.10 2.00 0 -2 32 5.90 1.70 0 -2 -32 6.40 2.80 0 2 32 7.10 1.70 0 2 -32 2.90 4.00 0 2 32 7.00 2.00 0 2 -32 0.90 8.10 1 -2 32 12.20 1.90 -1 -2 -32 9.10 4.90 -1 -2 -32 16.60 3.00 1 -2 32 14.30 2.50 -1 2 -32 11.20 4.10 1 2 32 15.40 2.00 1 2 32 8.40 2.10 4 -3 -32 20.90 6.50 4 -3 -32 26.90 3.40 -4 -3 32 17.10 3.40 4 3 -32 16.90 10.00 -4 3 32 23.40 2.90 -3 -3 32 1.80 2.00 3 -3 -32 1.00 6.10 3 -3 -32 2.40 3.00 3 3 -32 2.90 9.60 3 3 -32 -0.90 4.40 -3 3 32 1.30 1.90 2 -3 -32 10.80 6.00 2 -3 -32 6.20 2.90 -2 -3 32 2.10 2.10 -2 3 32 6.60 2.00 2 3 -32 -1.10 9.30 2 3 -32 2.90 4.20 1 -3 -32 2.40 5.50 1 -3 -32 2.60 2.60 -1 -3 32 2.30 1.90 -1 -3 32 -1.30 2.20 -1 3 32 1.80 1.80 1 3 -32 -7.00 8.40 1 3 -32 -0.30 3.90 0 -3 -32 7.20 2.90 0 -3 -32 4.30 5.10 0 -3 32 1.20 1.70 0 3 32 3.40 2.00 0 3 -32 6.40 8.30 0 3 -32 3.10 3.70 0 3 32 0.30 1.70 4 0 -33 10.30 5.60 -4 0 33 0.30 2.10 4 0 -33 -0.60 3.10 3 0 -33 3.60 5.20 -3 0 33 2.90 2.00 3 0 -33 0.30 2.90 3 0 -33 2.10 9.40 2 0 -33 -0.90 8.90 2 0 -33 1.00 2.90 -2 0 33 -0.70 1.90 2 0 -33 3.10 5.10 1 0 -33 2.10 9.10 1 0 -33 3.40 2.70 -1 0 33 0.60 2.10 -1 0 33 -0.20 1.60 1 0 -33 -2.60 4.80 0 0 33 4.10 2.00 0 0 -33 3.60 4.80 0 0 33 1.20 1.60 4 -1 -33 11.20 6.00 4 -1 -33 10.40 3.20 -4 -1 33 8.10 2.40 -4 1 33 11.90 2.30 4 1 -33 6.60 10.00 4 1 -33 1.70 3.30 4 1 -33 5.60 5.30 3 -1 -33 -1.90 5.60 3 -1 -33 -1.00 3.00 -3 -1 33 1.90 2.20 3 1 -33 -1.40 2.80 3 1 -33 -2.20 10.00 3 1 -33 -2.20 4.90 -3 1 33 -0.20 2.00 -2 -1 33 4.80 1.80 2 -1 -33 -1.80 5.10 2 -1 -33 -0.80 2.80 -2 -1 33 1.70 2.20 2 1 -33 12.50 4.70 -2 1 33 4.70 2.00 2 1 -33 2.50 9.80 2 1 -33 0.90 2.80 1 -1 -33 0.60 2.70 1 -1 -33 4.00 10.00 1 -1 -33 -0.20 5.20 -1 -1 33 -1.00 2.10 1 1 -33 2.60 4.50 -1 1 33 0.50 1.60 -1 1 33 -0.40 1.90 1 1 -33 -2.70 9.10 0 -1 33 7.90 1.80 0 -1 -33 9.60 2.90 0 -1 33 13.30 2.30 0 -1 -33 6.80 5.00 0 1 33 9.10 2.30 0 1 33 13.90 1.90 0 1 -33 9.60 9.90 0 1 -33 11.70 4.70 -3 -2 33 6.40 2.50 3 -2 -33 2.50 2.90 3 -2 -33 5.00 5.80 3 2 -33 2.80 10.20 -3 2 33 4.90 2.10 3 2 -33 3.10 4.90 -2 -2 33 2.40 2.30 2 -2 -33 0.20 5.50 2 -2 -33 7.50 2.80 2 2 -33 11.90 9.50 -2 2 33 5.00 2.10 2 2 -33 6.00 4.50 -1 -2 33 3.30 2.20 1 -2 -33 1.30 2.70 1 -2 -33 -1.90 5.30 -1 -2 33 3.90 1.80 1 2 -33 3.00 4.30 1 2 -33 3.80 9.50 -1 2 33 2.10 2.00 0 0 0 0.00 0.00 _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 76974 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x-1/2, -y-1/2, z-1/2' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group N1 N 0.63433(13) 0.59776(15) 0.68510(5) 0.0436(3) Uani 1 1 d . . . . . N2 N 0.42948(12) 0.31462(15) 0.53623(5) 0.0417(3) Uani 1 1 d . . . . . C5 C 0.58172(14) 0.22142(15) 0.49280(5) 0.0351(3) Uani 1 1 d . . . . . C2 C 0.78037(14) 0.33629(16) 0.56246(5) 0.0364(3) Uani 1 1 d . . . . . C6 C 0.55931(14) 0.30333(16) 0.53677(6) 0.0352(3) Uani 1 1 d . . . . . C27 C 0.59524(14) 0.36320(17) 0.66759(6) 0.0395(3) Uani 1 1 d . . . . . C12 C 0.45958(15) 0.17391(16) 0.46712(6) 0.0378(3) Uani 1 1 d . . . . . C1 C 0.65752(14) 0.35693(16) 0.57378(5) 0.0357(3) Uani 1 1 d . . . . . C19 C 0.89354(14) 0.38713(16) 0.59801(6) 0.0370(3) Uani 1 1 d . . . . . C26 C 0.63624(14) 0.42892(17) 0.62301(6) 0.0375(3) Uani 1 1 d . . . . . C32 C 0.59562(14) 0.47193(18) 0.70568(6) 0.0394(3) Uani 1 1 d . . . . . C13 C 0.73833(15) 0.12872(17) 0.43530(6) 0.0383(3) Uani 1 1 d . . . . . C4 C 0.70611(15) 0.20455(16) 0.48216(5) 0.0364(3) Uani 1 1 d . . . . . C7 C 0.36956(15) 0.23819(17) 0.49412(6) 0.0414(4) Uani 1 1 d . . . . . C3 C 0.80175(15) 0.26435(17) 0.51701(6) 0.0388(3) Uani 1 1 d . . . . . H3 H 0.884243 0.256541 0.510008 0.047 Uiso 1 1 calc R . . . . C25 C 0.65910(15) 0.56980(17) 0.63567(6) 0.0407(3) Uani 1 1 d . . . . . H25 H 0.687637 0.637889 0.613784 0.049 Uiso 1 1 calc R . . . . C24 C 0.92405(17) 0.3330(2) 0.64807(6) 0.0467(4) Uani 1 1 d . . . . . H24 H 0.869766 0.268209 0.660886 0.056 Uiso 1 1 calc R . . . . C14 C 0.67655(17) 0.1601(2) 0.38573(6) 0.0482(4) Uani 1 1 d . . . . . H14 H 0.612940 0.229239 0.381456 0.058 Uiso 1 1 calc R . . . . C20 C 0.97645(16) 0.48514(19) 0.58099(6) 0.0468(4) Uani 1 1 d . . . . . H20 H 0.958681 0.522886 0.547540 0.056 Uiso 1 1 calc R . . . . C11 C 0.41790(17) 0.08007(18) 0.42600(6) 0.0462(4) Uani 1 1 d . . . . . H11 H 0.475741 0.031277 0.408889 0.055 Uiso 1 1 calc R . . . . C18 C 0.83501(17) 0.02755(19) 0.43995(7) 0.0478(4) Uani 1 1 d . . . . . H18 H 0.879514 0.007550 0.472645 0.057 Uiso 1 1 calc R . . . . C22 C 1.11640(15) 0.4723(2) 0.66217(6) 0.0478(4) Uani 1 1 d . . . . . C23 C 1.03408(17) 0.3741(2) 0.67914(6) 0.0509(4) Uani 1 1 d . . . . . H23 H 1.053264 0.334666 0.712292 0.061 Uiso 1 1 calc R . . . . C8 C 0.24049(16) 0.2220(2) 0.47814(7) 0.0525(4) Uani 1 1 d . . . . . H8 H 0.181772 0.269213 0.495268 0.063 Uiso 1 1 calc R . . . . C31 C 0.56051(17) 0.4450(2) 0.75441(6) 0.0515(4) Uani 1 1 d . . . . . H31 H 0.560929 0.517952 0.779013 0.062 Uiso 1 1 calc R . . . . C21 C 1.08469(17) 0.5278(2) 0.61266(7) 0.0530(4) Uani 1 1 d . . . . . H21 H 1.137475 0.595320 0.600406 0.064 Uiso 1 1 calc R . . . . C15 C 0.7092(2) 0.0892(2) 0.34273(7) 0.0615(5) Uani 1 1 d . . . . . H15 H 0.667094 0.110906 0.309752 0.074 Uiso 1 1 calc R . . . . C9 C 0.20274(18) 0.1336(2) 0.43601(8) 0.0590(5) Uani 1 1 d . . . . . H9 H 0.117133 0.122639 0.424041 0.071 Uiso 1 1 calc R . . . . C10 C 0.29040(18) 0.0608(2) 0.41118(7) 0.0552(5) Uani 1 1 d . . . . . H10 H 0.262442 -0.002089 0.384047 0.066 Uiso 1 1 calc R . . . . C28 C 0.5586(2) 0.2242(2) 0.67958(7) 0.0594(5) Uani 1 1 d . . . . . H28 H 0.557304 0.150282 0.655273 0.071 Uiso 1 1 calc R . . . . C33 C 0.6436(2) 0.7375(2) 0.71036(8) 0.0615(5) Uani 1 1 d . . . . . H33A H 0.560507 0.772368 0.713295 0.092 Uiso 1 1 calc GR . . . . H33B H 0.684959 0.804036 0.690062 0.092 Uiso 1 1 calc GR . . . . H33C H 0.691481 0.728671 0.744453 0.092 Uiso 1 1 calc GR . . . . C17 C 0.8663(2) -0.0439(2) 0.39684(8) 0.0614(5) Uani 1 1 d . . . . . H17 H 0.929995 -0.112874 0.400792 0.074 Uiso 1 1 calc R . . . . C35 C 0.36070(18) 0.4063(2) 0.56770(8) 0.0592(5) Uani 1 1 d . . . . . H35A H 0.324131 0.348240 0.592247 0.089 Uiso 1 1 calc GR . . . . H35B H 0.295011 0.456211 0.545579 0.089 Uiso 1 1 calc GR . . . . H35C H 0.417472 0.475239 0.586080 0.089 Uiso 1 1 calc GR . . . . C30 C 0.5253(2) 0.3071(3) 0.76483(8) 0.0661(6) Uani 1 1 d . . . . . H30 H 0.501617 0.286124 0.797098 0.079 Uiso 1 1 calc R . . . . C16 C 0.8033(2) -0.0132(2) 0.34822(8) 0.0658(6) Uani 1 1 d . . . . . H16 H 0.824017 -0.061235 0.319164 0.079 Uiso 1 1 calc R . . . . C34 C 1.23676(19) 0.5146(3) 0.69608(8) 0.0741(7) Uani 1 1 d . . . . . H34A H 1.219956 0.591537 0.718870 0.111 Uiso 1 1 calc GR . . . . H34B H 1.297313 0.546233 0.674597 0.111 Uiso 1 1 calc GR . . . . H34C H 1.269839 0.433100 0.716422 0.111 Uiso 1 1 calc GR . . . . C29 C 0.5244(2) 0.1978(3) 0.72791(8) 0.0733(6) Uani 1 1 d . . . . . H29 H 0.500275 0.105210 0.736057 0.088 Uiso 1 1 calc R . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 N1 0.0519(8) 0.0430(7) 0.0366(7) -0.0087(6) 0.0092(6) 0.0015(6) N2 0.0390(7) 0.0482(7) 0.0389(7) -0.0031(6) 0.0091(5) 0.0032(6) C5 0.0422(8) 0.0332(7) 0.0298(7) 0.0013(6) 0.0051(6) 0.0002(6) C2 0.0422(8) 0.0387(8) 0.0285(7) -0.0007(6) 0.0055(6) 0.0004(6) C6 0.0394(8) 0.0355(7) 0.0322(7) 0.0016(6) 0.0097(6) 0.0028(6) C27 0.0398(8) 0.0460(9) 0.0334(7) -0.0054(6) 0.0080(6) -0.0035(7) C12 0.0430(8) 0.0354(7) 0.0344(7) 0.0029(6) 0.0036(6) -0.0019(6) C1 0.0432(8) 0.0360(7) 0.0287(7) -0.0009(6) 0.0081(6) 0.0013(6) C19 0.0384(8) 0.0417(8) 0.0317(7) -0.0051(6) 0.0078(6) 0.0045(6) C26 0.0386(8) 0.0422(8) 0.0323(7) -0.0045(6) 0.0073(6) 0.0015(6) C32 0.0360(7) 0.0484(9) 0.0341(7) -0.0054(6) 0.0062(6) 0.0008(6) C13 0.0436(8) 0.0406(8) 0.0323(7) -0.0039(6) 0.0103(6) -0.0023(6) C4 0.0444(8) 0.0357(7) 0.0296(7) 0.0000(6) 0.0072(6) 0.0036(6) C7 0.0429(8) 0.0436(8) 0.0377(8) 0.0051(6) 0.0056(6) -0.0030(7) C3 0.0391(8) 0.0461(8) 0.0323(7) -0.0032(6) 0.0084(6) 0.0027(6) C25 0.0462(8) 0.0415(8) 0.0352(8) -0.0015(6) 0.0091(6) 0.0020(7) C24 0.0505(9) 0.0552(10) 0.0345(8) 0.0022(7) 0.0061(7) -0.0059(8) C14 0.0534(10) 0.0562(10) 0.0348(8) -0.0036(7) 0.0062(7) 0.0048(8) C20 0.0434(9) 0.0603(10) 0.0364(8) 0.0079(7) 0.0045(7) -0.0007(8) C11 0.0549(10) 0.0398(8) 0.0425(9) -0.0013(7) 0.0019(7) -0.0065(7) C18 0.0513(9) 0.0546(10) 0.0381(8) -0.0037(7) 0.0089(7) 0.0074(8) C22 0.0383(8) 0.0665(11) 0.0388(8) -0.0083(8) 0.0057(7) 0.0027(8) C23 0.0517(10) 0.0709(12) 0.0293(8) 0.0019(7) 0.0032(7) 0.0012(9) C8 0.0407(9) 0.0634(11) 0.0539(10) 0.0057(9) 0.0085(8) -0.0058(8) C31 0.0504(10) 0.0703(12) 0.0353(8) -0.0083(8) 0.0109(7) -0.0001(9) C21 0.0425(9) 0.0657(12) 0.0512(10) 0.0041(9) 0.0082(8) -0.0083(8) C15 0.0701(12) 0.0814(14) 0.0324(9) -0.0089(9) 0.0055(8) 0.0030(11) C9 0.0471(10) 0.0674(12) 0.0606(12) 0.0079(9) 0.0008(9) -0.0183(9) C10 0.0617(11) 0.0515(10) 0.0498(10) -0.0022(8) -0.0009(8) -0.0180(9) C28 0.0778(13) 0.0522(10) 0.0513(10) -0.0085(8) 0.0197(9) -0.0176(9) C33 0.0809(14) 0.0510(10) 0.0534(11) -0.0188(9) 0.0119(10) 0.0011(10) C17 0.0651(12) 0.0652(12) 0.0564(11) -0.0131(9) 0.0177(9) 0.0160(10) C35 0.0467(10) 0.0761(13) 0.0562(11) -0.0143(10) 0.0123(8) 0.0128(9) C30 0.0749(14) 0.0855(15) 0.0418(10) 0.0047(10) 0.0219(9) -0.0133(11) C16 0.0747(14) 0.0791(14) 0.0469(10) -0.0226(10) 0.0202(10) 0.0043(11) C34 0.0497(11) 0.116(2) 0.0537(11) -0.0037(12) -0.0026(9) -0.0121(12) C29 0.0966(17) 0.0669(13) 0.0621(13) 0.0017(10) 0.0303(12) -0.0270(12) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C32 N1 C33 126.10(14) . . ? C25 N1 C32 108.26(13) . . ? C25 N1 C33 125.61(15) . . ? C6 N2 C35 128.71(14) . . ? C7 N2 C6 108.58(13) . . ? C7 N2 C35 122.06(14) . . ? C6 C5 C12 106.66(13) . . ? C4 C5 C6 119.45(13) . . ? C4 C5 C12 133.88(14) . . ? C1 C2 C19 122.08(13) . . ? C1 C2 C3 120.88(14) . . ? C3 C2 C19 117.04(13) . . ? N2 C6 C5 108.45(13) . . ? N2 C6 C1 128.80(13) . . ? C1 C6 C5 122.73(13) . . ? C32 C27 C26 106.96(14) . . ? C28 C27 C26 134.61(15) . . ? C28 C27 C32 118.43(15) . . ? C7 C12 C5 106.29(13) . . ? C11 C12 C5 135.05(15) . . ? C11 C12 C7 118.58(15) . . ? C2 C1 C6 116.09(13) . . ? C2 C1 C26 120.38(13) . . ? C6 C1 C26 123.51(13) . . ? C24 C19 C2 121.74(14) . . ? C20 C19 C2 120.74(14) . . ? C20 C19 C24 117.42(15) . . ? C27 C26 C1 127.29(14) . . ? C25 C26 C27 106.20(13) . . ? C25 C26 C1 126.41(14) . . ? N1 C32 C27 107.77(13) . . ? N1 C32 C31 129.97(15) . . ? C31 C32 C27 122.26(16) . . ? C14 C13 C4 121.47(14) . . ? C18 C13 C4 120.40(14) . . ? C18 C13 C14 118.09(15) . . ? C5 C4 C13 123.40(13) . . ? C3 C4 C5 117.40(13) . . ? C3 C4 C13 119.18(14) . . ? N2 C7 C12 109.82(14) . . ? N2 C7 C8 128.23(16) . . ? C8 C7 C12 121.95(15) . . ? C4 C3 C2 123.11(14) . . ? C26 C25 N1 110.80(14) . . ? C23 C24 C19 120.83(16) . . ? C15 C14 C13 120.35(17) . . ? C21 C20 C19 121.33(15) . . ? C10 C11 C12 119.24(17) . . ? C17 C18 C13 121.19(16) . . ? C23 C22 C34 121.15(17) . . ? C21 C22 C23 117.35(16) . . ? C21 C22 C34 121.50(18) . . ? C24 C23 C22 121.65(16) . . ? C9 C8 C7 117.68(18) . . ? C30 C31 C32 117.67(17) . . ? C20 C21 C22 121.40(17) . . ? C16 C15 C14 120.72(18) . . ? C8 C9 C10 121.10(17) . . ? C11 C10 C9 121.16(17) . . ? C29 C28 C27 119.12(18) . . ? C16 C17 C18 120.03(18) . . ? C31 C30 C29 121.15(18) . . ? C17 C16 C15 119.58(17) . . ? C28 C29 C30 121.4(2) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag N1 C32 1.372(2) . ? N1 C25 1.372(2) . ? N1 C33 1.449(2) . ? N2 C6 1.3922(19) . ? N2 C7 1.381(2) . ? N2 C35 1.451(2) . ? C5 C6 1.420(2) . ? C5 C12 1.448(2) . ? C5 C4 1.407(2) . ? C2 C1 1.402(2) . ? C2 C19 1.490(2) . ? C2 C3 1.402(2) . ? C6 C1 1.408(2) . ? C27 C26 1.431(2) . ? C27 C32 1.412(2) . ? C27 C28 1.396(2) . ? C12 C7 1.404(2) . ? C12 C11 1.399(2) . ? C1 C26 1.488(2) . ? C19 C24 1.387(2) . ? C19 C20 1.387(2) . ? C26 C25 1.361(2) . ? C32 C31 1.393(2) . ? C13 C4 1.488(2) . ? C13 C14 1.390(2) . ? C13 C18 1.389(2) . ? C4 C3 1.381(2) . ? C7 C8 1.393(2) . ? C24 C23 1.382(2) . ? C14 C15 1.383(2) . ? C20 C21 1.378(2) . ? C11 C10 1.376(3) . ? C18 C17 1.382(2) . ? C22 C23 1.383(3) . ? C22 C21 1.380(2) . ? C22 C34 1.504(2) . ? C8 C9 1.380(3) . ? C31 C30 1.371(3) . ? C15 C16 1.377(3) . ? C9 C10 1.388(3) . ? C28 C29 1.378(3) . ? C17 C16 1.372(3) . ? C30 C29 1.394(3) . ?