#------------------------------------------------------------------------------ #$Date: 2024-07-05 20:57:52 +0300 (Fri, 05 Jul 2024) $ #$Revision: 293261 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/98/7159899.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7159899 loop_ _publ_author_name 'Ohira, Kazuki' 'Kozuka, Kumpei' 'Kaneda, Naoki' 'Yamamoto, Masahiro' 'Imato, Keiichi' 'Ooyama, Yousuke' _publ_section_title ; Photochromism of phenazine-2,3-diol derivatives through excited state intermolecular proton transfer based on keto-enol tautomerization. ; _journal_issue 20 _journal_name_full 'Organic & biomolecular chemistry' _journal_page_first 4077 _journal_page_last 4088 _journal_paper_doi 10.1039/d4ob00387j _journal_volume 22 _journal_year 2024 _chemical_formula_moiety 'C12 H8 N2 O2' _chemical_formula_sum 'C12 H8 N2 O2' _chemical_formula_weight 212.20 _chemical_name_systematic 3-hydroxyphenazin-2(10H)-one _space_group_crystal_system monoclinic _space_group_IT_number 4 _space_group_name_Hall 'P 2yb' _space_group_name_H-M_alt 'P 1 21 1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_block_doi 10.5517/ccdc.csd.cc2j4xvg _audit_creation_date 2023-07-20 _audit_creation_method ; Olex2 1.3-ac4 (compiled 2020.11.27 svn.r5f609507 for Rigaku Oxford Diffraction, GUI svn.r6214) ; _audit_update_record ; 2024-01-26 deposited with the CCDC. 2024-04-11 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 92.843(3) _cell_angle_gamma 90 _cell_formula_units_Z 2 _cell_length_a 3.7249(2) _cell_length_b 9.6327(4) _cell_length_c 12.9466(5) _cell_measurement_reflns_used 4946 _cell_measurement_temperature 100.00(10) _cell_measurement_theta_max 31.7770 _cell_measurement_theta_min 2.6300 _cell_volume 463.96(4) _computing_cell_refinement 'CrysAlisPro 1.171.42.27a (Rigaku OD, 2021)' _computing_data_collection 'CrysAlisPro 1.171.42.27a (Rigaku OD, 2021)' _computing_data_reduction 'CrysAlisPro 1.171.42.27a (Rigaku OD, 2021)' _computing_molecular_graphics 'Olex2 1.3-ac4 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.3-ac4 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' _diffrn_ambient_environment N~2~ _diffrn_ambient_temperature 100.00(10) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix _diffrn_measured_fraction_theta_full 0.999 _diffrn_measured_fraction_theta_max 0.850 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -76.00 6.00 0.50 1.00 -- -5.75 -57.00 90.00 164 2 \w -9.00 35.00 0.50 1.00 -- 7.00 -99.00 120.00 88 3 \w -7.00 37.00 0.50 1.00 -- 7.00 -99.00-120.00 88 4 \w -53.00 1.00 0.50 1.00 -- -5.75 -38.00 -60.00 108 5 \w -57.00 4.00 0.50 1.00 -- -5.75 -57.00-120.00 122 6 \w -9.00 64.00 0.50 1.00 -- -5.75 38.00-120.00 146 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy R, DW system, HyPix' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 0.0297387000 _diffrn_orient_matrix_UB_12 -0.0101234000 _diffrn_orient_matrix_UB_13 -0.0531584000 _diffrn_orient_matrix_UB_21 0.1881966000 _diffrn_orient_matrix_UB_22 -0.0013113000 _diffrn_orient_matrix_UB_23 0.0114531000 _diffrn_orient_matrix_UB_31 -0.0075075000 _diffrn_orient_matrix_UB_32 -0.0729186000 _diffrn_orient_matrix_UB_33 0.0071893000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0186 _diffrn_reflns_av_unetI/netI 0.0221 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.850 _diffrn_reflns_limit_h_max 5 _diffrn_reflns_limit_h_min -5 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -19 _diffrn_reflns_number 6401 _diffrn_reflns_point_group_measured_fraction_full 0.933 _diffrn_reflns_point_group_measured_fraction_max 0.742 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 31.827 _diffrn_reflns_theta_min 2.637 _diffrn_source 'Rotating-anode X-ray tube' _diffrn_source_type 'Rigaku (Mo) X-ray Source' _exptl_absorpt_coefficient_mu 0.107 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.93489 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.27a (Rigaku Oxford Diffraction, 2021) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_colour 'clear dark red' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_modifier dark _exptl_crystal_colour_primary red _exptl_crystal_density_diffrn 1.519 _exptl_crystal_description block _exptl_crystal_F_000 220 _exptl_crystal_size_max 0.217 _exptl_crystal_size_mid 0.109 _exptl_crystal_size_min 0.071 _refine_diff_density_max 0.389 _refine_diff_density_min -0.233 _refine_diff_density_rms 0.050 _refine_ls_abs_structure_details ; Flack x determined using 805 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.3(5) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.110 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 146 _refine_ls_number_reflns 2365 _refine_ls_number_restraints 1 _refine_ls_restrained_S_all 1.110 _refine_ls_R_factor_all 0.0384 _refine_ls_R_factor_gt 0.0349 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0603P)^2^+0.0328P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0981 _refine_ls_wR_factor_ref 0.0999 _reflns_Friedel_coverage 0.658 _reflns_Friedel_fraction_full 0.857 _reflns_Friedel_fraction_max 0.622 _reflns_number_gt 2153 _reflns_number_total 2365 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file d4ob00387j2.cif _cod_data_source_block exp_2549 _cod_depositor_comments 'Adding full bibliography for 7159899--7159902.cif.' _cod_database_code 7159899 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula C12H8N2O2 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.993 _shelx_estimated_absorpt_t_min 0.977 _reflns_odcompleteness_completeness 99.91 _reflns_odcompleteness_iscentric 1 _reflns_odcompleteness_theta 27.82 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups At 1.5 times of: All O(H) groups 2.a Aromatic/amide H refined with riding coordinates: N1(H1), C1(H1A), C4(H4), C5(H5), C6(H6), C7(H7), C8(H8) 2.b Idealised tetrahedral OH refined as rotating group: O2(H2) ; _shelx_res_file ; TITL exp_2549_a.res in P2(1) exp_2549.res created by SHELXL-2018/3 at 11:59:21 on 20-Jul-2023 REM Old TITL exp_2549 in P2(1) REM SHELXT solution in P2(1): R1 0.068, Rweak 0.009, Alpha 0.001 REM 1.254 for 6 systematic absences, Orientation as input REM Flack x = 0.161 ( 0.482 ) from 685 Parsons' quotients REM Formula found by SHELXT: C12 N2 O2 CELL 0.71073 3.7249 9.6327 12.9466 90 92.843 90 ZERR 2 0.0002 0.0004 0.0005 0 0.003 0 LATT -1 SYMM -X,0.5+Y,-Z SFAC C H N O UNIT 24 16 4 4 L.S. 20 PLAN 20 SIZE 0.07 0.11 0.22 TEMP -173 BOND list 4 fmap 2 53 ACTA REM REM REM WGHT 0.060300 0.032800 FVAR 1.15531 O1 4 0.713633 0.202995 0.489044 11.00000 0.02215 0.01596 = 0.01686 -0.00377 0.00604 -0.00142 O2 4 0.448122 0.087564 0.647846 11.00000 0.02576 0.01306 = 0.02026 -0.00093 0.00362 -0.00510 AFIX 147 H2 2 0.466842 0.064291 0.585816 11.00000 -1.50000 AFIX 0 N1 3 0.921619 0.624820 0.675486 11.00000 0.01569 0.01231 = 0.01208 0.00130 0.00274 -0.00125 AFIX 43 H1 2 1.017629 0.664652 0.622261 11.00000 -1.20000 AFIX 0 N2 3 0.634425 0.498379 0.845328 11.00000 0.01452 0.01660 = 0.01261 0.00065 0.00149 -0.00012 C1 1 0.840847 0.417737 0.574987 11.00000 0.01448 0.01286 = 0.01321 0.00192 0.00258 -0.00079 AFIX 43 H1A 2 0.944658 0.459972 0.517248 11.00000 -1.20000 AFIX 0 C2 1 0.715150 0.281264 0.568205 11.00000 0.01148 0.01572 = 0.01443 0.00073 0.00194 0.00255 C3 1 0.565876 0.218476 0.661410 11.00000 0.01315 0.01183 = 0.01802 0.00246 0.00084 -0.00005 C4 1 0.546988 0.288061 0.751646 11.00000 0.01495 0.01492 = 0.01340 0.00381 0.00210 -0.00111 AFIX 43 H4 2 0.455570 0.243552 0.810321 11.00000 -1.20000 AFIX 0 C5 1 0.709162 0.711092 0.941738 11.00000 0.01705 0.02266 = 0.01345 -0.00155 0.00140 0.00200 AFIX 43 H5 2 0.614403 0.667900 1.000470 11.00000 -1.20000 AFIX 0 C6 1 0.810785 0.847051 0.946902 11.00000 0.01923 0.02184 = 0.01978 -0.00626 -0.00054 0.00163 AFIX 43 H6 2 0.786495 0.898053 1.008971 11.00000 -1.20000 AFIX 0 C7 1 0.952609 0.912198 0.859652 11.00000 0.01877 0.01635 = 0.02568 -0.00364 -0.00124 0.00029 AFIX 43 H7 2 1.020828 1.007138 0.863838 11.00000 -1.20000 AFIX 0 C8 1 0.993367 0.840862 0.769226 11.00000 0.01634 0.01486 = 0.02009 -0.00001 0.00038 -0.00143 AFIX 43 H8 2 1.090663 0.885299 0.711373 11.00000 -1.20000 AFIX 0 C9 1 0.813498 0.491472 0.666467 11.00000 0.01191 0.01421 = 0.01209 0.00218 0.00128 0.00137 C10 1 0.665027 0.428510 0.758158 11.00000 0.01134 0.01480 = 0.01276 0.00293 0.00132 0.00025 C11 1 0.888399 0.700805 0.763856 11.00000 0.01216 0.01618 = 0.01385 0.00079 0.00051 0.00154 C12 1 0.743389 0.633528 0.849693 11.00000 0.01304 0.01643 = 0.01466 0.00010 0.00027 0.00072 HKLF 4 REM exp_2549_a.res in P2(1) REM wR2 = 0.0999, GooF = S = 1.110, Restrained GooF = 1.110 for all data REM R1 = 0.0349 for 2153 Fo > 4sig(Fo) and 0.0384 for all 2365 data REM 146 parameters refined using 1 restraints END WGHT 0.0603 0.0326 REM Highest difference peak 0.389, deepest hole -0.233, 1-sigma level 0.050 Q1 1 0.7576 0.4590 0.7137 11.00000 0.05 0.39 Q2 1 0.6322 0.2528 0.6153 11.00000 0.05 0.37 Q3 1 0.7378 0.6725 0.8989 11.00000 0.05 0.33 Q4 1 0.7939 0.6733 0.8051 11.00000 0.05 0.29 Q5 1 0.8809 0.6651 0.7185 11.00000 0.05 0.28 Q6 1 0.7755 0.4597 0.6189 11.00000 0.05 0.26 Q7 1 0.6141 0.3577 0.7541 11.00000 0.05 0.25 Q8 1 0.9029 0.8720 0.9022 11.00000 0.05 0.24 Q9 1 0.9119 0.7738 0.7648 11.00000 0.05 0.24 Q10 1 0.5595 0.2662 0.7055 11.00000 0.05 0.23 Q11 1 0.8271 0.3454 0.5761 11.00000 0.05 0.22 Q12 1 0.6388 0.4723 0.8001 11.00000 0.05 0.22 Q13 1 0.7666 0.7785 0.9399 11.00000 0.05 0.22 Q14 1 0.6919 0.5674 0.8458 11.00000 0.05 0.21 Q15 1 0.8649 0.5603 0.6754 11.00000 0.05 0.20 Q16 1 0.7617 0.2183 0.4401 11.00000 0.05 0.20 Q17 1 0.9220 0.8768 0.8138 11.00000 0.05 0.19 Q18 1 0.6742 0.1388 0.4883 11.00000 0.05 0.16 Q19 1 0.6611 0.4581 0.8941 11.00000 0.05 0.16 Q20 1 0.6774 0.2575 0.5226 11.00000 0.05 0.16 ; _shelx_res_checksum 11100 _shelx_hkl_file ; 0 -9 14 2.89 1.61 0 -8 9 1.23 1.11 0 -8 10 9.58 1.65 0 -8 11 10.42 1.81 0 -8 12 1.31 1.27 0 -8 13 11.74 1.93 0 -8 14 3.76 1.57 0 -8 15 61.72 3.70 0 -7 7 254.21 6.77 0 -7 8 20.02 1.91 0 -7 9 8.94 1.47 0 -7 10 0.86 1.14 0 -7 -11 1.03 0.70 0 -7 11 0.44 1.13 0 -7 12 18.80 2.07 0 -7 -12 18.49 1.41 0 -7 -13 3.59 0.98 0 -7 13 3.61 1.47 0 -7 14 5.33 1.56 0 -7 15 89.31 4.29 0 -7 16 316.77 8.79 0 -6 5 41.32 2.33 0 -6 6 46.27 2.48 0 -6 7 269.02 6.64 0 -6 8 9.79 1.43 0 -6 -8 10.60 0.88 0 -6 -9 99.58 2.80 0 -6 9 98.78 3.87 0 -6 -10 16.74 1.31 0 -6 10 16.93 1.79 0 -6 -11 41.32 2.05 0 -6 11 39.95 2.67 0 -6 11 35.51 1.26 0 -6 -12 24.17 1.75 0 -6 12 18.49 0.95 0 -6 12 22.73 2.16 0 -6 13 62.47 3.36 0 -6 -13 59.31 2.75 0 -6 14 24.50 2.35 0 -6 -14 33.07 2.24 0 -6 15 0.32 1.25 0 -6 16 23.92 2.48 0 -6 17 55.70 3.63 0 -5 4 11.31 1.19 0 -5 5 6.74 1.02 0 -5 6 22.56 1.64 0 -5 -6 21.98 0.98 0 -5 -7 9.22 0.84 0 -5 7 10.21 1.25 0 -5 8 21.84 1.04 0 -5 8 25.87 1.89 0 -5 -8 22.60 1.32 0 -5 -9 192.27 3.22 0 -5 -9 201.95 4.57 0 -5 9 193.99 3.75 0 -5 -9 183.71 3.13 0 -5 9 197.61 5.41 0 -5 -10 128.58 3.74 0 -5 -10 127.25 2.61 0 -5 10 133.75 4.45 0 -5 10 127.71 2.94 0 -5 11 177.72 3.82 0 -5 11 189.44 5.59 0 -5 -11 189.71 4.96 0 -5 -11 186.85 3.67 0 -5 -12 29.51 1.40 0 -5 12 29.80 2.28 0 -5 -12 33.56 2.15 0 -5 12 31.30 1.47 0 -5 -13 11.77 1.55 0 -5 -13 12.71 1.05 0 -5 13 14.80 1.77 0 -5 13 12.25 1.05 0 -5 14 3.70 1.34 0 -5 -14 2.10 1.24 0 -5 14 2.79 0.75 0 -5 -14 2.70 0.72 0 -5 -15 5.02 0.90 0 -5 -15 9.70 1.56 0 -5 15 7.56 1.63 0 -5 16 26.50 2.51 0 -5 17 6.21 1.66 0 -4 3 433.01 7.91 0 -4 -4 126.91 2.29 0 -4 4 126.52 3.51 0 -4 5 93.53 2.13 0 -4 5 99.90 3.12 0 -4 -5 102.26 2.25 0 -4 6 51.72 2.24 0 -4 -6 51.25 1.73 0 -4 -6 49.62 1.10 0 -4 6 47.27 1.44 0 -4 -6 46.86 1.04 0 -4 -7 3.76 0.73 0 -4 -7 3.58 0.41 0 -4 7 4.69 0.92 0 -4 7 2.76 0.49 0 -4 8 35.59 2.03 0 -4 -8 35.19 1.27 0 -4 -8 38.10 1.82 0 -4 8 35.93 1.39 0 -4 -9 21.39 1.12 0 -4 9 20.97 1.66 0 -4 -9 20.78 1.51 0 -4 9 18.66 1.12 0 -4 -10 5.19 1.03 0 -4 10 8.01 0.85 0 -4 -10 6.11 0.78 0 -4 10 7.34 1.22 0 -4 11 104.81 2.92 0 -4 -11 106.34 3.73 0 -4 -11 104.21 3.00 0 -4 11 104.23 3.89 0 -4 -12 65.77 3.09 0 -4 12 63.58 2.32 0 -4 12 61.85 3.12 0 -4 -12 67.01 2.47 0 -4 -13 7.95 1.07 0 -4 13 8.65 1.06 0 -4 13 6.76 1.46 0 -4 -13 8.15 1.51 0 -4 -14 7.21 1.13 0 -4 14 8.83 1.13 0 -4 14 6.87 1.47 0 -4 -14 7.34 1.45 0 -4 -15 2.27 0.94 0 -4 15 0.59 1.25 0 -4 -15 2.48 1.34 0 -4 15 1.93 0.88 0 -4 16 2.00 1.36 0 -4 -16 0.90 0.91 0 -4 17 -0.80 1.20 0 -4 18 12.92 2.05 0 -3 3 24.73 0.86 0 -3 -3 25.84 0.76 0 -3 3 23.51 1.29 0 -3 4 67.72 1.59 0 -3 4 69.69 2.27 0 -3 -4 69.56 1.72 0 -3 -5 527.05 9.55 0 -3 5 534.54 7.95 0 -3 5 532.49 9.07 0 -3 -5 556.88 8.48 0 -3 6 348.18 5.68 0 -3 6 343.29 6.72 0 -3 -6 350.70 6.31 0 -3 -6 359.17 7.29 0 -3 7 80.23 2.13 0 -3 -7 76.54 3.04 0 -3 7 81.28 2.80 0 -3 -7 77.68 2.57 0 -3 8 90.89 2.48 0 -3 -8 93.62 3.07 0 -3 8 93.39 3.15 0 -3 9 15.25 1.40 0 -3 -9 17.47 1.49 0 -3 -9 14.96 1.12 0 -3 -10 34.89 2.19 0 -3 -10 36.37 1.79 0 -3 -11 11.48 1.49 0 -3 -11 11.05 1.14 0 -3 -12 5.22 1.01 0 -3 -12 5.99 1.31 0 -3 -13 5.55 1.38 0 -3 -13 5.18 1.07 0 -3 14 -0.27 1.15 0 -3 14 1.21 0.84 0 -3 -14 2.23 0.95 0 -3 -14 2.34 1.40 0 -3 -15 10.16 1.85 0 -3 -15 12.40 1.52 0 -3 15 8.88 1.66 0 -3 15 13.46 1.42 0 -3 16 142.77 5.32 0 -3 -16 158.11 4.98 0 -3 -17 97.38 3.92 0 -3 17 89.83 4.30 0 -3 18 30.19 2.77 0 -2 2 260.83 3.91 0 -2 -3 372.29 6.56 0 -2 -3 374.56 5.75 0 -2 3 388.09 5.55 0 -2 -4 1996.24 28.17 0 -2 -4 1986.58 27.31 0 -2 4 2031.94 26.83 0 -2 4 2047.36 27.63 0 -2 -5 334.11 5.95 0 -2 -5 337.05 6.56 0 -2 -6 2034.23 28.61 0 -2 -6 1953.55 27.82 0 -2 -7 590.80 10.66 0 -2 -7 596.13 10.19 0 -2 -8 0.61 0.76 0 -2 -8 1.01 0.71 0 -2 -9 3.66 0.98 0 -2 -9 6.47 1.11 0 -2 -10 8.64 1.33 0 -2 -10 6.83 1.22 0 -2 -11 34.03 2.31 0 -2 -11 33.17 1.96 0 -2 -12 15.03 1.77 0 -2 -12 10.76 1.33 0 -2 -13 9.45 1.34 0 -2 -13 12.47 1.76 0 -2 -14 0.98 0.97 0 -2 -14 -0.16 1.26 0 -2 -15 34.28 2.41 0 -2 -16 100.76 4.17 0 -2 -17 45.83 2.92 0 -2 -18 17.55 2.08 0 -2 19 3.83 1.59 0 -1 -1 1075.91 14.58 0 -1 -2 2590.83 34.43 0 -1 -3 31.15 1.32 0 -1 -4 374.35 6.59 0 -1 4 381.85 6.06 0 -1 5 95.86 2.42 0 -1 -5 95.41 2.75 0 -1 -5 88.11 2.57 0 -1 6 195.59 4.12 0 -1 -6 187.83 4.40 0 -1 -6 190.46 4.48 0 -1 -7 168.95 4.35 0 -1 -7 165.61 4.33 0 -1 7 165.22 3.94 0 -1 8 36.10 1.82 0 -1 -8 36.04 2.03 0 -1 -8 35.35 1.99 0 -1 -9 35.86 2.13 0 -1 -9 39.55 2.27 0 -1 9 34.41 1.92 0 -1 -10 80.06 3.35 0 -1 10 74.86 2.95 0 -1 -10 78.00 3.26 0 -1 11 189.68 5.19 0 -1 -11 190.67 5.53 0 -1 -11 188.98 5.61 0 -1 -12 634.99 12.51 0 -1 12 612.52 11.77 0 -1 -12 634.36 11.81 0 -1 -13 149.37 5.28 0 -1 -13 146.38 4.80 0 -1 13 138.33 4.71 0 -1 -14 11.43 1.57 0 -1 -14 13.14 1.91 0 -1 -15 0.58 1.14 0 -1 -16 2.96 1.26 0 -1 -17 11.65 1.82 0 -1 -18 56.76 3.54 0 -1 -19 26.53 2.67 0 0 -2 880.02 11.81 0 0 -2 830.58 11.92 0 0 -3 0.84 0.48 0 0 -4 0.27 0.32 0 0 -4 0.58 0.56 0 0 -5 37.44 1.17 0 0 -5 38.18 1.58 0 0 6 262.71 5.32 0 0 -6 263.50 5.32 0 0 -6 261.49 4.47 0 0 -7 160.49 3.25 0 0 -7 171.97 4.18 0 0 7 165.85 4.11 0 0 -8 35.01 2.05 0 0 8 35.53 1.88 0 0 -8 32.40 1.29 0 0 -8 35.04 1.85 0 0 -9 91.36 2.35 0 0 -9 82.72 3.13 0 0 -9 91.40 3.52 0 0 9 93.16 3.29 0 0 10 1203.84 19.36 0 0 -10 1216.66 19.97 0 0 -10 1240.37 19.38 0 0 -11 720.45 13.07 0 0 11 712.72 13.06 0 0 -11 738.27 13.74 0 0 12 562.18 11.18 0 0 -12 567.44 11.25 0 0 -12 563.08 11.75 0 0 -13 0.32 1.17 0 0 -13 0.69 0.96 0 0 13 -0.40 0.98 0 0 -14 50.86 3.31 0 0 -14 50.97 3.01 0 0 14 46.51 2.88 0 0 -15 13.72 1.88 0 0 15 16.31 1.91 0 0 -16 5.10 1.48 0 0 -17 1.61 1.42 0 0 -18 10.89 2.01 0 1 0 1.09 0.25 0 1 -1 1081.68 14.60 0 1 1 1073.03 14.66 0 1 -1 1075.45 14.70 0 1 -1 1093.26 14.53 0 1 -2 2571.49 33.57 0 1 2 2558.89 33.75 0 1 2 2583.77 34.22 0 1 -2 2590.80 34.25 0 1 3 31.88 1.29 0 1 -3 31.24 1.01 0 1 -3 34.70 1.44 0 1 -4 376.75 6.20 0 1 -4 381.35 6.07 0 1 -4 378.54 6.77 0 1 -5 94.43 2.42 0 1 -5 90.97 2.36 0 1 -5 93.18 2.85 0 1 -6 197.17 4.15 0 1 -6 192.94 3.99 0 1 -7 157.93 3.61 0 1 -7 161.97 3.90 0 1 -8 35.90 1.82 0 1 -8 37.21 1.63 0 1 9 36.51 2.14 0 1 -9 36.35 1.67 0 1 -9 38.38 1.98 0 1 -10 78.50 2.55 0 1 -10 75.67 3.43 0 1 10 79.41 3.31 0 1 -10 73.15 2.95 0 1 11 184.63 5.56 0 1 -11 188.39 4.39 0 1 -11 191.20 5.19 0 1 -11 201.33 6.04 0 1 -12 638.07 12.89 0 1 12 615.88 12.32 0 1 -12 633.32 11.81 0 1 -12 619.94 12.37 0 1 -13 146.52 5.21 0 1 13 151.96 5.22 0 1 -13 147.25 5.48 0 1 -14 10.96 1.73 0 1 14 14.16 1.84 0 1 15 0.50 1.20 0 1 -15 1.55 1.30 0 1 -16 1.83 1.40 0 1 16 5.42 1.57 0 1 -17 11.39 2.01 0 1 -18 53.93 3.71 0 2 0 563.46 8.33 0 2 -1 498.54 7.23 0 2 -1 488.34 6.98 0 2 1 484.39 7.38 0 2 -1 490.69 7.46 0 2 -1 488.44 7.60 0 2 1 491.02 7.20 0 2 2 260.09 4.03 0 2 2 259.67 4.67 0 2 -2 258.44 4.60 0 2 -2 260.30 3.90 0 2 -2 254.42 4.70 0 2 -2 267.79 4.49 0 2 -3 378.62 5.50 0 2 3 390.08 6.60 0 2 3 373.76 5.34 0 2 -3 386.41 6.59 0 2 -4 2028.01 27.64 0 2 4 1995.44 27.57 0 2 -5 341.18 6.19 0 2 -5 328.96 5.51 0 2 -5 328.66 6.57 0 2 5 324.75 6.49 0 2 -6 1998.01 28.62 0 2 -6 1951.29 27.15 0 2 -6 1993.16 27.79 0 2 -7 577.64 9.81 0 2 -7 596.93 10.77 0 2 -7 577.66 9.47 0 2 -8 0.99 0.86 0 2 -8 1.03 0.58 0 2 -8 1.32 0.60 0 2 -9 7.77 0.99 0 2 -9 7.12 0.95 0 2 -10 7.69 1.05 0 2 -10 8.07 1.08 0 2 10 5.35 1.18 0 2 -11 31.27 1.86 0 2 -11 34.32 2.04 0 2 11 37.63 2.52 0 2 -12 15.76 1.80 0 2 12 12.83 1.73 0 2 -12 10.66 1.38 0 2 -12 13.82 1.40 0 2 -13 9.06 1.76 0 2 13 9.78 1.59 0 2 -13 11.77 1.31 0 2 -13 10.17 1.70 0 2 -14 2.08 1.33 0 2 14 1.51 1.36 0 2 -15 29.30 2.66 0 2 15 30.52 2.67 0 2 16 103.72 4.84 0 2 -16 96.77 4.78 0 2 -17 37.92 3.24 0 2 17 39.72 3.14 0 3 0 0.05 0.49 0 3 0 0.08 0.31 0 3 0 -0.15 0.35 0 3 -1 44.07 1.65 0 3 -1 41.72 1.34 0 3 1 46.30 1.53 0 3 1 41.02 1.48 0 3 -1 46.42 1.71 0 3 1 42.37 1.11 0 3 -2 245.05 3.98 0 3 -2 236.82 4.55 0 3 2 242.01 4.24 0 3 -2 233.02 4.83 0 3 -2 240.06 4.63 0 3 2 238.27 4.69 0 3 3 24.36 1.36 0 3 3 24.97 0.95 0 3 -3 24.54 1.34 0 3 -3 23.08 1.20 0 3 -3 24.05 0.85 0 3 4 63.93 2.37 0 3 -4 65.89 1.48 0 3 -4 65.22 2.38 0 3 4 68.94 1.51 0 3 -5 532.90 7.94 0 3 5 548.29 9.60 0 3 -5 557.55 9.64 0 3 -6 350.69 7.26 0 3 6 349.11 7.24 0 3 -6 338.27 5.70 0 3 -6 336.77 6.83 0 3 7 72.36 3.03 0 3 -7 82.15 2.90 0 3 -7 77.23 2.22 0 3 -7 79.56 3.18 0 3 -8 92.97 3.65 0 3 -8 95.51 3.22 0 3 -8 89.92 2.64 0 3 -9 16.42 1.24 0 3 -9 17.56 1.77 0 3 -9 19.36 1.55 0 3 -10 39.98 2.68 0 3 -10 36.14 1.86 0 3 -10 38.03 2.13 0 3 -11 11.89 1.39 0 3 11 9.63 1.58 0 3 -11 10.75 1.19 0 3 -11 9.21 1.66 0 3 -12 4.03 1.25 0 3 -12 3.68 0.99 0 3 12 3.78 1.32 0 3 -13 3.97 1.36 0 3 -13 4.71 1.20 0 3 13 5.07 1.49 0 3 -14 0.76 0.97 0 3 14 1.79 1.22 0 3 -14 0.18 1.29 0 3 15 12.43 1.96 0 3 -15 11.36 1.97 0 3 16 155.05 6.14 0 3 -16 164.96 6.42 0 3 17 102.70 5.08 0 3 -17 110.67 5.36 0 4 0 744.29 10.95 0 4 0 725.95 11.62 0 4 0 725.74 10.37 0 4 0 745.69 10.91 0 4 -1 81.62 2.59 0 4 -1 83.31 2.10 0 4 1 77.71 1.89 0 4 -1 81.95 2.31 0 4 1 79.63 2.41 0 4 1 80.38 2.32 0 4 -1 84.76 2.66 0 4 -2 101.02 2.68 0 4 -2 103.14 3.09 0 4 2 98.97 2.64 0 4 2 102.84 2.92 0 4 -2 100.47 2.93 0 4 -2 101.15 2.37 0 4 2 103.45 1.93 0 4 -3 435.73 8.03 0 4 -3 422.69 7.61 0 4 3 423.53 6.97 0 4 -3 436.19 7.62 0 4 -3 424.03 6.63 0 4 3 431.25 7.80 0 4 -4 125.60 3.53 0 4 4 123.82 2.68 0 4 -4 120.33 2.17 0 4 -4 125.77 3.34 0 4 -4 125.03 2.50 0 4 4 128.43 3.68 0 4 -5 103.06 3.34 0 4 5 99.14 3.37 0 4 -5 98.44 2.00 0 4 5 99.47 2.14 0 4 -6 45.65 1.38 0 4 6 53.06 2.53 0 4 -6 48.15 2.39 0 4 -6 50.95 2.39 0 4 7 3.27 1.01 0 4 -7 3.29 0.55 0 4 -7 4.21 1.08 0 4 -7 2.65 0.89 0 4 8 35.70 2.32 0 4 -8 39.01 2.24 0 4 -8 35.12 1.46 0 4 -8 36.10 2.38 0 4 -9 23.24 1.82 0 4 -9 19.70 1.22 0 4 9 19.68 1.87 0 4 -9 23.37 2.06 0 4 -10 7.33 1.28 0 4 -10 6.57 0.88 0 4 -11 101.79 3.15 0 4 -11 105.33 3.89 0 4 -11 101.70 4.45 0 4 -12 68.51 3.18 0 4 -12 65.58 3.75 0 4 -12 65.54 3.75 0 4 -13 10.19 1.57 0 4 -13 8.29 1.70 0 4 13 7.02 1.66 0 4 14 4.96 1.71 0 4 -14 6.88 1.41 0 4 -14 6.07 1.74 0 4 15 2.79 1.51 0 4 -15 0.62 1.38 0 4 -15 2.15 1.22 0 4 16 0.84 1.38 0 4 -16 2.19 1.57 0 5 0 0.42 0.64 0 5 0 0.52 0.70 0 5 0 0.30 0.53 0 5 0 0.60 0.49 0 5 0 0.54 0.43 0 5 1 1925.30 26.64 0 5 1 1864.41 25.53 0 5 -1 1886.52 27.07 0 5 -1 1857.82 25.68 0 5 1 1858.77 24.58 0 5 -1 1901.50 27.07 0 5 -1 1878.90 26.27 0 5 -1 1849.04 25.58 0 5 1 1858.86 26.28 0 5 2 154.59 3.79 0 5 -2 162.11 4.01 0 5 2 149.71 3.92 0 5 2 155.89 2.92 0 5 -2 162.54 4.22 0 5 -2 156.19 3.45 0 5 -2 160.21 3.67 0 5 -2 156.96 4.25 0 5 3 39.86 1.71 0 5 -3 43.39 2.05 0 5 -3 46.99 2.00 0 5 -3 41.75 1.49 0 5 -3 42.02 2.15 0 5 3 45.47 2.11 0 5 -4 12.00 1.32 0 5 4 12.41 0.93 0 5 -4 10.08 1.13 0 5 -4 10.90 1.10 0 5 -4 12.92 0.78 0 5 4 11.19 1.22 0 5 5 5.47 1.01 0 5 5 6.09 0.65 0 5 -5 5.60 0.40 0 5 -5 7.60 1.00 0 5 -5 7.47 1.11 0 5 -6 20.32 1.70 0 5 -6 21.24 0.79 0 5 6 23.39 1.83 0 5 6 23.12 1.00 0 5 -7 8.24 0.60 0 5 -7 7.97 1.30 0 5 -7 8.33 1.27 0 5 7 11.09 1.39 0 5 -8 20.65 1.01 0 5 -8 26.16 2.03 0 5 8 23.88 2.06 0 5 -8 24.71 2.07 0 5 -9 201.66 6.04 0 5 -9 202.38 6.10 0 5 -9 185.77 3.84 0 5 9 192.08 5.93 0 5 -9 199.26 5.66 0 5 10 136.93 5.08 0 5 -10 137.86 5.07 0 5 -10 126.76 4.98 0 5 -10 131.26 4.61 0 5 -11 192.47 6.38 0 5 11 188.97 6.32 0 5 -11 202.11 5.87 0 5 -12 31.64 2.40 0 5 -13 12.89 1.77 0 5 -14 2.28 1.48 0 5 -14 2.98 1.32 0 5 -15 10.06 2.05 0 5 15 9.71 2.08 0 6 0 9.42 0.70 0 6 0 8.19 1.08 0 6 0 9.24 0.90 0 6 0 8.43 0.87 0 6 0 11.46 1.29 0 6 -1 240.07 4.59 0 6 1 239.68 4.58 0 6 -1 244.58 5.81 0 6 1 243.56 5.51 0 6 1 220.73 3.57 0 6 1 234.32 5.09 0 6 -1 241.06 5.71 0 6 -1 229.46 5.06 0 6 -1 236.43 4.58 0 6 -2 213.97 4.09 0 6 2 219.21 5.12 0 6 2 216.28 3.99 0 6 -2 220.36 5.15 0 6 -2 226.80 4.75 0 6 2 209.39 5.04 0 6 -2 223.22 5.58 0 6 -2 223.95 5.54 0 6 -2 220.89 4.62 0 6 -3 69.02 2.53 0 6 -3 71.91 2.82 0 6 -3 69.36 1.76 0 6 3 74.14 2.58 0 6 3 68.51 2.75 0 6 3 68.81 1.50 0 6 -3 72.22 2.88 0 6 -3 72.23 2.21 0 6 -3 79.47 3.15 0 6 -4 169.80 4.72 0 6 -4 158.80 4.34 0 6 -4 158.27 4.45 0 6 -4 155.47 4.77 0 6 4 162.63 4.62 0 6 -4 158.15 3.42 0 6 4 160.16 3.86 0 6 5 40.02 2.31 0 6 5 41.64 1.69 0 6 -5 41.07 2.33 0 6 -5 38.19 2.20 0 6 -5 33.07 0.83 0 6 -5 39.90 1.41 0 6 -5 40.33 2.14 0 6 6 40.59 2.47 0 6 -6 42.04 2.43 0 6 6 45.54 1.65 0 6 -6 44.39 2.56 0 6 -7 282.07 7.04 0 6 7 269.04 4.69 0 6 -7 270.26 7.09 0 6 7 274.34 7.11 0 6 -7 267.51 6.87 0 6 -8 10.82 1.59 0 6 -8 11.10 1.59 0 6 -8 13.06 1.70 0 6 8 9.60 1.54 0 6 9 103.61 4.40 0 6 -9 103.02 4.13 0 6 -9 96.88 4.27 0 6 -9 96.51 4.18 0 6 -10 13.28 1.88 0 6 -10 20.00 1.99 0 6 10 17.73 2.06 0 6 -10 19.06 2.13 0 6 -11 40.18 2.99 0 6 11 45.63 3.14 0 6 -11 41.78 2.79 0 6 -11 40.13 3.01 0 6 -12 22.15 2.45 0 6 12 23.83 2.51 0 6 -12 21.45 2.16 0 6 13 65.10 4.03 0 7 0 -0.14 0.53 0 7 0 -0.10 0.79 0 7 0 0.07 0.60 0 7 0 0.58 0.82 0 7 0 0.04 0.45 0 7 -1 17.19 1.12 0 7 1 15.73 1.27 0 7 1 12.94 0.53 0 7 -1 16.85 1.29 0 7 1 15.50 1.08 0 7 -1 14.74 1.22 0 7 1 18.22 1.72 0 7 1 18.82 1.59 0 7 -1 16.25 1.07 0 7 -1 17.02 1.57 0 7 -1 17.65 1.57 0 7 -2 48.11 1.97 0 7 2 44.44 2.19 0 7 -2 44.92 2.22 0 7 -2 45.54 2.46 0 7 -2 44.47 1.94 0 7 -2 44.41 1.61 0 7 2 42.89 2.26 0 7 -2 45.50 2.51 0 7 2 44.80 1.59 0 7 -3 20.60 1.82 0 7 3 22.37 1.57 0 7 -3 21.14 0.97 0 7 -3 21.52 1.51 0 7 -3 19.75 1.62 0 7 3 19.71 1.56 0 7 3 19.65 0.83 0 7 -3 24.13 1.82 0 7 -3 21.70 1.32 0 7 -4 118.56 3.00 0 7 -4 111.18 2.19 0 7 4 120.49 4.07 0 7 -4 112.52 4.20 0 7 -4 121.75 4.11 0 7 4 114.99 3.45 0 7 -4 119.73 4.00 0 7 -4 115.88 3.70 0 7 -5 2424.22 35.21 0 7 -5 2391.99 32.90 0 7 -5 2402.20 35.87 0 7 -5 2443.13 35.07 0 7 -5 2377.34 35.59 0 7 5 2470.14 35.64 0 7 5 2457.24 33.82 0 7 -6 127.89 4.64 0 7 6 130.68 3.41 0 7 -6 126.15 4.36 0 7 -7 259.65 6.85 0 7 -7 253.04 7.09 0 7 7 259.04 4.94 0 7 7 268.87 7.16 0 7 -8 16.74 1.96 0 7 -8 17.51 1.98 0 7 -8 16.83 1.87 0 7 8 19.44 2.07 0 7 -9 8.19 1.57 0 7 9 11.90 1.82 0 7 -9 9.67 1.65 0 7 -9 9.49 1.69 0 7 -10 1.48 1.23 0 7 -10 -0.78 1.18 0 7 -10 1.09 1.28 0 7 10 0.53 1.24 0 7 -11 1.35 1.29 0 7 11 1.31 1.34 0 7 12 17.55 2.29 0 7 -12 22.59 2.57 0 7 -13 5.00 1.75 0 7 13 5.06 1.81 0 7 -14 3.66 1.70 0 7 14 1.33 1.62 0 8 0 97.85 3.74 0 8 0 92.61 2.27 0 8 0 94.47 3.02 0 8 0 99.74 3.15 0 8 0 98.44 3.93 0 8 1 34.22 1.91 0 8 -1 36.19 1.69 0 8 -1 39.37 2.45 0 8 -1 36.33 1.99 0 8 1 33.85 2.41 0 8 1 36.14 1.70 0 8 -1 37.20 2.42 0 8 1 40.90 2.35 0 8 -1 36.04 1.99 0 8 -1 37.66 1.62 0 8 -2 21.95 1.21 0 8 2 25.14 2.12 0 8 2 22.60 1.68 0 8 -2 21.79 1.39 0 8 2 22.72 1.84 0 8 -2 24.49 2.02 0 8 -2 22.47 1.92 0 8 2 23.12 1.24 0 8 -2 19.24 1.43 0 8 -2 22.46 1.68 0 8 3 170.88 3.21 0 8 3 179.56 4.87 0 8 -3 174.97 4.27 0 8 -3 183.71 5.15 0 8 3 177.99 5.02 0 8 -3 172.24 5.26 0 8 -3 171.55 3.45 0 8 -3 175.69 4.50 0 8 -3 165.96 5.39 0 8 -4 244.23 6.46 0 8 -4 254.60 6.00 0 8 4 256.20 6.52 0 8 -4 261.56 5.24 0 8 4 258.13 5.92 0 8 -4 251.35 6.86 0 8 -4 234.02 3.97 0 8 -4 261.16 6.63 0 8 5 59.90 2.48 0 8 5 54.62 3.01 0 8 -5 61.35 3.12 0 8 -5 57.60 2.80 0 8 -5 53.39 3.09 0 8 -5 61.76 3.04 0 8 -5 55.38 1.99 0 8 6 360.86 6.97 0 8 -6 352.66 8.14 0 8 -6 345.43 8.05 0 8 -6 345.94 8.68 0 8 6 352.96 8.55 0 8 -6 343.47 8.50 0 8 7 671.53 13.60 0 8 7 693.58 11.06 0 8 -7 665.14 13.73 0 8 -7 704.63 13.28 0 8 8 100.82 4.44 0 8 -8 109.04 4.69 0 8 -8 106.56 4.39 0 8 -8 103.63 4.53 0 8 -9 0.95 1.15 0 8 -9 0.72 1.22 0 8 9 1.06 1.22 0 8 -10 11.16 1.94 0 8 10 9.13 1.84 0 8 11 7.50 1.82 0 8 -11 7.97 1.85 0 8 -12 -0.22 1.57 0 8 12 4.60 1.72 0 8 13 15.01 2.30 0 8 -13 10.94 2.23 0 9 0 0.65 0.71 0 9 0 -0.43 0.79 0 9 0 -0.39 0.96 0 9 0 -0.58 1.08 0 9 0 0.33 0.91 0 9 0 0.22 0.46 0 9 1 192.24 5.60 0 9 -1 197.45 5.89 0 9 -1 184.41 5.02 0 9 -1 193.39 5.11 0 9 -1 185.81 4.40 0 9 1 193.22 4.50 0 9 -1 187.14 4.08 0 9 1 194.45 6.06 0 9 1 191.26 4.97 0 9 -1 185.03 5.86 0 9 -2 86.76 3.39 0 9 -2 77.95 3.67 0 9 -2 83.72 3.06 0 9 2 83.36 2.45 0 9 -2 80.70 2.45 0 9 -2 80.18 2.71 0 9 2 78.87 3.23 0 9 2 82.36 3.45 0 9 2 87.27 4.02 0 9 -2 78.56 3.67 0 9 -3 6.01 1.20 0 9 -3 6.40 1.01 0 9 -3 5.18 0.97 0 9 3 5.81 1.26 0 9 -3 7.90 1.45 0 9 -3 5.73 0.66 0 9 -3 5.16 1.37 0 9 3 5.90 0.57 0 9 3 7.07 1.21 0 9 -4 4.32 0.85 0 9 -4 5.03 1.36 0 9 -4 4.28 1.06 0 9 -4 4.28 0.45 0 9 4 2.81 1.08 0 9 -4 3.88 1.15 0 9 4 4.49 1.08 0 9 -4 5.71 1.35 0 9 5 46.94 2.83 0 9 -5 49.02 1.95 0 9 -5 42.85 2.77 0 9 -5 46.91 2.93 0 9 5 48.17 2.41 0 9 -5 46.19 3.04 0 9 -5 48.81 2.63 0 9 6 10.12 1.56 0 9 6 9.10 1.19 0 9 -6 8.38 1.42 0 9 -6 10.77 1.64 0 9 -6 7.37 1.54 0 9 -6 8.12 0.85 0 9 -7 24.59 2.36 0 9 7 23.91 1.57 0 9 -7 27.40 2.29 0 9 7 24.90 2.34 0 9 -8 4.50 1.36 0 9 -8 5.58 1.52 0 9 8 3.82 1.46 0 9 -9 1.78 1.31 0 9 9 4.61 1.59 0 9 -9 2.11 1.41 0 9 10 34.90 3.01 0 9 -10 33.96 3.05 0 9 11 146.91 6.06 0 9 -11 140.44 6.08 0 9 -12 80.98 4.72 0 9 12 87.06 4.82 0 10 0 361.01 7.28 0 10 0 363.55 7.49 0 10 0 343.93 8.89 0 10 0 357.10 8.05 0 10 0 361.18 8.74 0 10 -1 63.04 2.88 0 10 -1 58.74 1.98 0 10 1 66.72 2.83 0 10 -1 64.96 3.50 0 10 -1 63.62 3.43 0 10 1 61.80 2.44 0 10 1 58.99 3.17 0 10 -1 59.88 2.78 0 10 1 57.79 3.43 0 10 -1 61.27 2.36 0 10 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2.40 1 5 -5 63.12 2.80 1 5 -4 38.68 2.13 1 5 -4 33.83 1.96 1 5 -4 35.42 1.84 -1 5 4 33.29 1.52 -1 5 3 68.91 2.21 1 5 -3 69.13 2.59 -1 5 3 67.85 2.37 1 5 -3 69.82 2.58 1 5 -3 69.44 2.85 1 5 -2 183.48 4.36 -1 5 2 184.39 4.39 1 5 -2 187.50 4.62 1 5 -2 186.87 4.93 1 5 -1 596.51 10.37 -1 5 1 572.65 9.98 1 5 -1 582.02 9.61 1 5 -1 591.87 10.75 -1 5 0 548.61 9.85 1 5 0 564.13 10.11 -1 5 0 562.93 10.08 -1 5 -1 89.13 3.16 -1 5 -1 91.90 3.15 1 5 1 87.74 3.17 1 5 2 1.57 0.73 1 5 2 1.25 0.45 -1 5 -2 2.45 0.83 -1 5 -2 1.50 0.61 1 5 2 2.41 0.67 -1 5 -2 0.86 0.73 -1 5 -3 3.69 0.89 -1 5 -3 4.68 0.95 1 5 3 4.60 1.01 -1 5 -3 4.52 0.76 1 5 3 3.77 0.49 1 5 3 2.52 0.72 -1 5 -4 27.48 1.89 -1 5 -4 25.76 1.93 -1 5 -4 26.78 1.41 1 5 4 24.53 0.85 1 5 4 28.06 1.77 1 5 5 78.12 3.14 -1 5 -5 79.37 3.42 -1 5 -5 80.21 2.45 1 5 6 64.56 2.98 -1 5 -6 65.37 3.23 -1 5 -7 35.07 2.32 1 5 7 34.77 2.35 -1 5 -7 35.62 2.47 -1 5 -8 67.68 3.28 1 5 8 76.05 3.55 -1 5 -8 70.56 2.55 -1 5 -8 70.42 3.61 -1 5 -9 11.94 1.74 -1 5 -9 13.11 1.24 1 5 9 13.41 1.82 -1 5 -9 13.64 1.75 -1 5 -9 11.43 1.65 -1 5 -10 42.30 2.10 1 5 10 41.83 2.83 -1 5 -10 39.82 2.79 1 5 11 23.38 2.38 -1 5 -11 22.59 1.67 -1 5 -11 26.82 2.56 1 5 12 11.76 1.98 -1 5 -12 12.24 1.41 -1 5 -13 11.60 2.02 -1 5 -13 13.24 1.50 1 5 13 7.95 1.89 -1 5 -14 4.00 1.75 -1 5 -15 10.26 2.15 1 6 -11 1.36 1.19 -1 6 11 1.12 1.35 -1 6 10 104.37 4.70 1 6 -10 104.24 4.56 1 6 -10 101.87 4.28 -1 6 9 142.92 5.39 1 6 -9 142.81 5.18 -1 6 9 138.07 3.88 1 6 -9 142.60 5.02 -1 6 8 68.17 3.58 1 6 -8 68.64 3.43 -1 6 8 66.75 2.51 1 6 -8 65.45 3.30 -1 6 7 58.57 3.22 1 6 -7 65.34 3.20 -1 6 7 63.40 2.31 1 6 -7 62.00 3.15 -1 6 6 11.18 1.50 -1 6 6 11.37 0.99 1 6 -6 11.90 1.49 1 6 -6 10.74 1.18 -1 6 5 240.63 6.46 1 6 -5 240.90 6.04 -1 6 5 238.02 4.74 1 6 -5 228.73 5.42 1 6 -4 576.14 10.24 -1 6 4 567.95 9.18 1 6 -4 580.93 10.51 1 6 -4 579.38 11.02 -1 6 3 311.23 5.75 1 6 -3 320.41 6.59 1 6 -3 313.18 7.24 1 6 -3 327.67 6.75 1 6 -2 23.39 1.81 1 6 -2 22.65 1.43 1 6 -2 20.34 1.51 -1 6 2 21.15 1.40 -1 6 1 9.85 1.10 1 6 -1 9.79 0.95 1 6 -1 10.07 1.18 1 6 -1 8.99 1.28 -1 6 1 9.39 1.20 -1 6 0 121.22 3.73 -1 6 0 120.94 3.89 1 6 0 122.75 4.12 1 6 0 118.76 3.85 -1 6 -1 310.12 7.03 1 6 1 307.94 6.11 1 6 1 324.77 7.16 -1 6 -1 308.06 6.89 -1 6 -2 393.57 8.45 1 6 2 389.02 7.67 -1 6 -2 406.47 7.85 1 6 2 403.75 8.50 -1 6 -2 413.62 8.42 1 6 3 257.13 5.92 1 6 3 251.56 4.36 -1 6 -3 267.63 5.76 -1 6 -3 262.74 6.45 -1 6 -3 262.01 6.52 -1 6 -4 10.35 1.10 1 6 4 11.54 1.31 -1 6 -4 10.08 1.43 -1 6 -4 13.70 1.55 -1 6 -5 170.36 4.24 -1 6 -5 161.77 5.27 1 6 5 173.95 5.04 1 6 6 682.75 12.95 -1 6 -6 710.05 13.63 -1 6 -7 597.02 12.06 1 6 7 606.32 12.14 -1 6 -7 615.79 12.61 1 6 8 109.30 4.43 -1 6 -8 103.28 3.11 -1 6 -8 107.89 4.59 -1 6 -8 105.21 4.26 -1 6 -8 100.61 4.19 -1 6 -9 14.17 1.28 -1 6 -9 11.69 1.84 -1 6 -9 14.91 1.85 1 6 9 14.97 1.90 -1 6 -9 13.65 1.83 1 6 9 13.39 0.89 -1 6 -10 4.90 1.44 -1 6 -10 6.37 1.55 1 6 10 6.08 1.50 -1 6 -10 4.19 1.46 -1 6 -10 3.26 0.93 -1 6 -11 2.20 1.40 1 6 11 4.34 1.55 -1 6 -11 3.71 0.95 -1 6 -12 21.29 1.66 1 6 12 21.54 2.51 1 6 13 90.78 4.78 1 6 14 9.40 2.06 -1 7 13 -0.65 1.50 -1 7 12 40.74 3.32 -1 7 11 7.11 1.82 -1 7 10 30.00 2.68 1 7 -10 33.27 2.78 1 7 -9 7.99 1.53 -1 7 9 6.40 1.61 1 7 -9 4.74 1.41 -1 7 8 40.37 2.88 1 7 -8 41.34 2.81 1 7 -8 35.33 2.65 -1 7 7 85.13 4.02 1 7 -7 76.94 3.78 -1 7 7 86.50 2.47 1 7 -7 86.83 3.77 -1 7 6 1314.09 21.62 -1 7 6 1249.36 18.15 1 7 -6 1329.75 20.91 1 7 -6 1265.32 19.62 -1 7 5 280.58 7.35 1 7 -5 290.68 6.85 1 7 -5 278.53 7.12 1 7 -5 281.88 6.29 1 7 -5 270.25 7.21 -1 7 5 285.94 5.17 -1 7 4 199.62 5.83 1 7 -4 202.91 5.80 1 7 -4 205.87 5.27 -1 7 4 192.53 3.94 1 7 -4 196.91 5.05 -1 7 3 49.32 2.12 -1 7 3 51.98 1.80 1 7 -3 51.70 2.36 1 7 -3 52.53 2.82 1 7 -3 50.06 2.43 1 7 -2 51.37 2.50 -1 7 2 50.04 2.21 1 7 -2 49.18 2.14 1 7 -2 47.83 2.72 -1 7 1 51.80 2.35 -1 7 1 55.36 2.68 1 7 -1 55.15 2.88 1 7 -1 60.03 2.73 1 7 -1 54.56 2.09 -1 7 0 17.51 1.51 -1 7 0 15.76 1.55 1 7 0 19.27 1.84 1 7 0 17.73 1.64 -1 7 -1 49.46 2.61 1 7 1 46.52 2.04 1 7 1 47.17 2.73 -1 7 -1 52.10 2.56 1 7 1 53.57 2.73 -1 7 -1 54.34 2.61 -1 7 -2 40.60 2.48 1 7 2 39.07 2.02 -1 7 -2 36.76 2.15 1 7 2 45.31 2.57 -1 7 -2 42.53 2.42 -1 7 -3 122.11 4.41 1 7 3 132.06 3.98 1 7 3 121.49 2.49 -1 7 -3 122.62 3.90 -1 7 -3 118.99 2.68 -1 7 -3 118.68 4.27 1 7 4 57.72 3.11 -1 7 -4 57.60 3.02 -1 7 -4 56.68 2.52 -1 7 -4 58.23 3.03 1 7 4 55.24 2.67 -1 7 -5 302.63 7.70 1 7 5 297.64 7.28 -1 7 -5 305.60 6.58 -1 7 -5 303.53 7.82 1 7 6 424.57 9.51 -1 7 -6 440.71 8.42 -1 7 -6 449.90 10.24 1 7 7 18.05 2.02 -1 7 -7 17.86 2.10 -1 7 -7 16.66 1.89 1 7 7 16.02 1.27 1 7 8 69.84 2.36 -1 7 -8 72.20 3.70 1 7 8 80.22 3.90 -1 7 -8 71.02 2.46 -1 7 -8 67.73 3.78 -1 7 -8 83.99 3.85 -1 7 -9 9.44 1.84 1 7 9 7.83 0.82 -1 7 -9 7.67 1.62 1 7 9 8.97 1.71 -1 7 -9 9.06 1.71 -1 7 -9 8.07 1.02 1 7 10 10.72 0.64 -1 7 -10 14.85 1.28 1 7 10 11.37 1.88 -1 7 -11 6.43 1.01 -1 7 -11 6.55 1.81 1 7 11 4.92 1.64 -1 7 -12 18.92 2.47 1 7 12 15.46 2.22 1 7 13 39.44 3.38 -1 7 -13 42.30 3.53 -1 8 12 11.56 2.21 -1 8 11 11.66 2.08 -1 8 10 8.51 1.79 1 8 -9 31.28 2.61 -1 8 9 27.67 2.62 -1 8 8 1.42 1.24 1 8 -8 5.57 1.52 -1 8 7 25.92 2.42 1 8 -7 28.35 2.30 -1 8 6 20.43 2.13 1 8 -6 22.84 2.00 1 8 -6 23.18 1.72 -1 8 5 381.37 8.93 -1 8 5 346.65 5.56 1 8 -5 366.50 8.88 1 8 -5 370.72 8.07 1 8 -5 359.80 8.64 1 8 -5 359.03 7.58 -1 8 4 872.59 15.71 1 8 -4 852.12 14.43 -1 8 4 838.13 12.17 1 8 -4 855.01 15.63 1 8 -4 859.52 14.44 1 8 -4 875.98 15.83 -1 8 3 237.84 5.39 -1 8 3 245.81 6.63 1 8 -3 254.33 5.80 1 8 -3 246.48 6.81 -1 8 3 241.78 4.52 1 8 -3 257.30 6.19 1 8 -3 241.26 6.73 1 8 -2 0.66 0.90 -1 8 2 2.55 0.98 1 8 -2 2.10 1.20 1 8 -2 0.68 0.72 -1 8 2 1.12 0.74 1 8 -2 0.89 0.85 -1 8 1 7.49 1.14 -1 8 1 10.39 1.46 1 8 -1 7.21 0.89 1 8 -1 6.29 1.44 1 8 -1 9.32 1.36 1 8 0 20.97 1.85 -1 8 0 25.12 1.85 -1 8 0 23.88 1.98 1 8 0 20.86 2.02 -1 8 0 25.06 2.04 -1 8 -1 100.90 4.01 1 8 1 110.94 4.13 1 8 1 97.52 3.17 -1 8 -1 98.77 3.81 1 8 1 103.76 4.24 -1 8 -1 100.06 3.77 -1 8 -2 119.63 4.48 1 8 2 111.71 3.65 -1 8 -2 116.59 4.21 1 8 2 117.19 2.82 1 8 2 123.06 4.50 -1 8 -2 121.68 4.11 -1 8 -3 32.35 2.43 1 8 3 28.98 1.03 -1 8 -3 33.65 2.19 1 8 3 33.28 2.43 -1 8 -3 28.45 1.31 -1 8 -3 33.80 2.35 1 8 3 28.53 1.04 1 8 3 27.19 1.96 -1 8 -4 6.36 1.33 1 8 4 6.44 1.19 1 8 4 6.96 1.15 -1 8 -4 6.11 1.49 -1 8 -4 6.67 0.57 -1 8 -4 4.68 1.11 -1 8 -5 84.97 4.01 1 8 5 93.75 3.83 1 8 5 86.80 4.10 -1 8 -5 90.57 3.65 -1 8 -5 87.75 3.38 -1 8 -5 95.31 4.21 1 8 5 91.14 3.26 1 8 6 521.36 9.68 -1 8 -6 520.25 11.46 1 8 6 510.79 10.98 -1 8 -6 546.93 10.07 -1 8 -6 515.08 11.59 -1 8 -6 516.92 10.79 1 8 7 263.88 7.41 -1 8 -7 269.30 7.28 1 8 7 265.24 5.84 -1 8 -7 259.93 7.76 -1 8 -8 26.45 1.48 1 8 8 25.04 2.39 -1 8 -8 32.72 2.64 -1 8 -8 25.68 2.53 1 8 8 28.20 1.61 1 8 9 7.11 0.87 -1 8 -9 5.41 1.62 1 8 9 7.14 1.67 -1 8 -9 6.49 0.92 1 8 10 12.61 2.02 -1 8 -10 10.15 2.06 -1 8 -11 9.57 2.04 1 8 11 9.48 1.90 1 8 12 53.69 3.77 -1 8 -12 58.80 4.12 -1 9 11 78.22 4.53 -1 9 10 194.49 7.05 -1 9 9 45.69 3.36 -1 9 8 12.74 2.05 1 9 -8 8.85 1.67 -1 9 7 1.24 1.34 1 9 -7 2.66 1.28 -1 9 6 22.61 2.33 1 9 -6 23.74 2.08 1 9 -6 23.98 1.85 -1 9 5 38.97 2.78 1 9 -5 43.38 2.51 1 9 -5 41.44 2.87 1 9 -5 37.60 2.26 -1 9 4 155.81 5.31 1 9 -4 145.94 4.45 1 9 -4 154.47 5.44 1 9 -4 138.00 4.48 1 9 -4 144.75 5.39 -1 9 3 131.80 4.72 1 9 -3 123.44 3.79 -1 9 3 114.00 2.38 1 9 -3 121.76 4.81 1 9 -3 132.22 4.35 1 9 -3 125.18 4.89 -1 9 3 119.14 3.57 -1 9 2 72.76 3.40 -1 9 2 66.19 2.77 -1 9 2 73.02 2.12 1 9 -2 75.27 2.68 1 9 -2 78.70 3.83 1 9 -2 74.61 3.66 1 9 -2 79.27 3.41 -1 9 1 6.30 1.15 -1 9 1 5.17 1.21 1 9 -1 4.78 1.31 -1 9 1 7.38 1.48 1 9 -1 6.74 1.28 1 9 -1 6.94 1.39 -1 9 0 148.66 4.66 1 9 0 154.57 4.12 -1 9 0 149.79 5.11 1 9 0 155.44 5.10 1 9 0 164.37 5.28 -1 9 0 142.81 5.06 1 9 0 147.70 5.42 -1 9 -1 154.69 4.93 -1 9 -1 158.26 5.30 -1 9 -1 153.55 5.09 1 9 1 154.74 5.50 1 9 1 157.54 5.23 1 9 1 145.10 4.97 1 9 1 144.73 3.71 -1 9 -2 55.23 3.19 1 9 2 60.21 2.68 1 9 2 66.25 3.62 -1 9 -2 65.41 3.18 -1 9 -2 54.68 2.46 1 9 2 56.44 1.89 1 9 2 59.35 3.24 1 9 2 56.80 3.01 -1 9 -2 54.39 2.97 1 9 3 12.61 1.50 1 9 3 13.28 1.61 1 9 3 11.26 0.60 -1 9 -3 13.24 1.41 -1 9 -3 12.92 1.70 1 9 3 12.59 1.77 -1 9 -3 11.16 1.76 -1 9 -3 12.80 1.60 1 9 3 9.87 0.58 -1 9 -3 13.61 1.04 1 9 4 11.37 1.47 1 9 4 12.73 1.57 -1 9 -4 9.65 1.75 -1 9 -4 9.34 1.64 -1 9 -4 11.83 1.45 -1 9 -4 12.23 0.78 -1 9 -4 10.05 1.44 1 9 4 13.63 1.84 1 9 5 8.86 1.36 -1 9 -5 10.10 1.44 1 9 5 10.15 1.52 -1 9 -5 9.07 1.62 -1 9 -5 8.83 1.44 1 9 6 27.44 1.90 1 9 6 25.55 2.27 -1 9 -6 27.76 2.07 -1 9 -6 27.00 2.26 -1 9 -6 23.53 2.41 1 9 7 95.10 4.27 -1 9 -7 99.25 4.69 -1 9 -7 91.58 4.11 1 9 7 91.90 3.29 -1 9 -8 277.29 7.74 1 9 8 270.39 7.85 -1 9 -8 273.65 8.43 1 9 9 133.33 5.41 -1 9 -9 128.49 5.72 1 9 10 0.58 1.35 -1 9 -10 0.44 1.46 1 9 11 26.63 2.77 -1 9 -11 22.51 2.85 -1 10 10 94.50 4.93 1 10 -10 79.59 4.50 -1 10 9 24.20 2.63 1 10 -9 19.54 2.44 1 10 -8 3.13 1.39 -1 10 8 5.46 1.67 1 10 -8 2.61 1.37 -1 10 7 27.10 2.58 1 10 -7 23.07 2.22 -1 10 6 3.68 1.43 1 10 -6 3.48 1.25 1 10 -6 4.80 1.14 -1 10 5 1.99 1.27 1 10 -5 3.15 1.19 1 10 -5 1.33 1.04 -1 10 4 2.65 1.24 1 10 -4 2.65 0.97 1 10 -4 2.80 1.07 -1 10 3 5.82 1.41 -1 10 3 3.33 0.89 1 10 -3 3.87 1.04 1 10 -3 4.08 1.07 1 10 -3 4.35 1.24 -1 10 2 -0.41 1.10 1 10 -2 0.49 0.82 -1 10 2 -0.23 0.43 1 10 -2 0.33 0.83 -1 10 2 -0.19 0.91 1 10 -2 -0.92 1.14 -1 10 2 0.38 0.46 -1 10 1 38.17 1.54 -1 10 1 42.45 2.78 -1 10 1 41.62 2.35 1 10 -1 41.75 2.66 -1 10 1 43.67 3.00 1 10 -1 40.19 2.23 1 10 -1 40.43 2.88 -1 10 1 38.87 2.52 -1 10 0 91.40 3.68 -1 10 0 94.35 4.21 -1 10 0 96.63 3.73 -1 10 0 96.09 4.21 1 10 0 98.63 4.13 1 10 0 93.83 4.21 -1 10 0 93.57 2.79 1 10 0 96.54 3.21 -1 10 -1 70.68 3.35 -1 10 -1 58.94 3.41 -1 10 -1 71.24 3.55 -1 10 -1 68.99 2.59 1 10 1 68.99 2.45 -1 10 -1 69.22 3.07 1 10 1 72.54 3.64 1 10 1 63.94 3.44 1 10 2 24.88 1.88 -1 10 -2 26.93 2.33 -1 10 -2 26.47 1.77 -1 10 -2 25.84 1.61 1 10 2 25.33 2.34 1 10 2 24.56 1.25 1 10 2 24.75 2.20 -1 10 -2 28.23 2.27 1 10 3 1.48 0.93 1 10 3 3.46 1.27 -1 10 -3 1.92 0.89 -1 10 -3 0.46 1.07 -1 10 -3 2.19 0.71 -1 10 -3 2.09 1.14 1 10 3 0.17 1.18 -1 10 -4 15.54 2.00 1 10 4 12.79 1.92 1 10 4 10.91 1.60 1 10 4 15.99 1.78 -1 10 -4 12.67 0.86 -1 10 -4 10.01 1.61 -1 10 -4 12.75 1.59 -1 10 -5 8.97 1.47 1 10 5 8.38 1.35 1 10 5 6.97 1.41 -1 10 -5 9.31 1.83 1 10 5 10.72 1.88 -1 10 -5 7.24 1.51 -1 10 -6 4.45 1.57 1 10 6 5.83 1.22 -1 10 -6 5.59 1.39 -1 10 -6 3.77 1.20 1 10 6 3.18 1.32 1 10 7 29.46 2.58 -1 10 -7 29.99 2.54 -1 10 -7 29.09 2.84 1 10 8 4.75 1.53 -1 10 -8 5.21 1.63 1 10 9 15.98 2.15 -1 10 -9 11.40 2.14 -1 10 -10 16.80 2.51 1 10 10 20.36 2.48 -1 11 9 17.60 2.50 1 11 -9 17.66 2.34 -1 11 8 4.65 1.70 1 11 -8 2.11 1.39 -1 11 7 3.26 1.53 1 11 -7 1.08 1.32 -1 11 6 26.14 2.56 1 11 -6 23.46 2.33 1 11 -6 23.73 1.94 -1 11 5 48.63 3.25 1 11 -5 52.32 3.18 1 11 -5 52.98 2.78 -1 11 4 -0.65 1.33 1 11 -4 0.14 0.90 1 11 -4 0.86 1.08 -1 11 3 21.86 2.18 -1 11 3 18.29 1.43 1 11 -3 22.30 2.09 1 11 -3 22.08 1.98 -1 11 2 10.59 1.30 -1 11 2 13.17 1.74 1 11 -2 10.89 1.63 1 11 -2 12.70 1.58 1 11 -1 6.35 1.16 -1 11 1 7.62 1.45 -1 11 1 7.78 1.34 1 11 -1 3.69 1.31 -1 11 0 4.54 1.23 1 11 0 4.43 1.02 -1 11 0 4.23 1.23 1 11 0 4.16 1.31 -1 11 -1 29.04 2.11 -1 11 -1 34.80 2.45 -1 11 -1 28.14 1.90 1 11 1 29.39 1.64 1 11 1 33.89 2.64 -1 11 -2 116.83 4.62 -1 11 -2 112.59 3.87 -1 11 -2 112.05 3.49 -1 11 -3 18.65 2.09 1 11 3 17.95 1.81 -1 11 -3 19.79 1.60 1 11 3 22.24 2.36 1 11 3 18.15 2.01 -1 11 -4 3.57 0.90 1 11 4 4.11 1.37 1 11 4 1.71 1.16 -1 11 -4 3.94 1.51 1 11 4 4.66 1.57 -1 11 -5 51.53 3.42 1 11 5 50.55 3.07 1 11 5 57.74 3.69 1 11 6 101.59 4.44 1 11 6 99.36 5.00 -1 11 -6 92.54 4.74 1 11 7 46.70 3.25 1 11 7 46.15 3.55 -1 11 -7 50.38 3.62 1 11 8 9.43 1.90 -1 11 -8 7.76 1.99 1 11 9 2.32 1.64 1 12 -8 3.16 1.68 -1 12 7 37.95 3.12 1 12 -7 33.64 2.99 -1 12 6 50.55 3.49 1 12 -6 57.30 3.56 -1 12 5 99.35 4.62 1 12 -5 90.25 4.27 1 12 -4 0.89 1.18 -1 12 4 2.14 1.38 1 12 -4 2.70 1.27 1 12 -3 7.79 1.43 -1 12 3 5.91 1.54 1 12 -3 5.85 1.48 1 12 -2 1.93 1.08 -1 12 2 2.02 1.26 1 12 -2 1.90 1.31 -1 12 1 1.47 1.18 1 12 -1 1.85 1.32 -1 12 0 6.51 1.35 -1 12 0 6.48 1.31 -1 12 0 5.78 1.23 1 12 0 9.44 1.80 -1 12 -1 1.38 1.14 -1 12 -1 3.12 1.21 1 12 1 3.26 1.41 1 12 2 3.43 1.58 -1 12 -2 4.43 1.47 -1 12 -3 17.48 2.12 1 12 3 14.35 2.14 1 12 4 31.44 2.94 -1 12 -4 37.80 2.99 1 12 5 60.57 3.94 -1 12 -5 57.78 3.78 1 12 6 9.22 1.76 -1 12 -6 10.59 2.07 1 12 7 2.40 1.47 -1 12 -7 3.58 1.72 1 12 8 4.59 1.70 -1 13 5 20.87 2.39 -1 13 4 29.10 2.70 1 13 -1 3.69 1.56 1 13 0 29.46 2.69 1 13 1 174.39 6.25 1 13 2 56.95 3.72 1 13 3 8.08 1.91 -1 13 -5 13.44 2.19 -2 -10 8 11.78 2.33 2 -10 -3 26.40 2.44 2 -10 -2 90.10 4.31 2 -10 -1 54.61 3.45 2 -10 0 0.36 1.30 2 -10 1 13.65 2.07 2 -10 2 2.36 1.35 2 -10 3 24.82 2.65 2 -10 4 16.17 2.34 -2 -9 10 8.88 2.18 -2 -9 9 28.55 2.98 2 -9 -8 0.15 0.68 2 -9 -7 3.32 0.91 2 -9 -6 10.70 1.25 2 -9 -6 10.06 1.48 -2 -9 5 48.98 2.93 2 -9 -5 52.37 2.49 2 -9 -5 47.60 2.79 -2 -9 4 195.78 5.71 2 -9 -4 198.39 6.02 2 -9 -4 189.92 5.20 2 -9 -3 413.31 9.75 -2 -9 3 425.43 8.90 2 -9 -3 417.81 8.71 -2 -9 2 226.78 5.68 2 -9 -2 212.62 5.80 2 -9 -2 207.12 6.55 2 -9 -1 16.81 1.75 -2 -9 1 17.92 1.52 2 -9 -1 19.84 2.16 2 -9 0 4.14 1.48 -2 -9 0 6.32 0.97 2 -9 0 6.04 1.32 2 -9 1 11.68 1.93 -2 -9 -1 11.90 1.39 -2 -9 -1 12.04 1.08 2 -9 2 6.72 1.64 -2 -9 -2 6.29 1.17 -2 -9 -2 4.98 0.73 -2 -9 -3 25.66 2.04 -2 -9 -3 20.15 0.94 2 -9 3 23.20 2.52 -2 -9 -4 0.79 0.99 -2 -9 -5 2.42 1.27 2 -9 6 40.51 3.32 2 -9 7 219.15 7.63 2 -9 8 290.06 9.06 -2 -8 12 7.71 2.10 -2 -8 11 5.44 1.85 -2 -8 11 2.88 1.32 -2 -8 10 78.33 4.58 -2 -8 10 77.86 3.67 2 -8 -10 75.51 2.82 -2 -8 9 259.07 8.30 -2 -8 9 252.00 6.81 2 -8 -9 242.35 5.62 -2 -8 8 75.78 4.45 -2 -8 8 78.56 3.57 2 -8 -8 73.00 2.90 2 -8 -8 79.47 2.97 2 -8 -7 0.82 0.83 -2 -8 7 1.92 1.26 2 -8 -7 1.08 0.85 2 -8 -6 7.01 1.28 2 -8 -6 6.99 1.14 -2 -8 6 8.32 1.67 -2 -8 5 147.00 5.87 -2 -8 5 155.17 5.19 2 -8 -5 146.98 4.80 2 -8 -5 145.90 4.40 -2 -8 4 261.62 7.96 -2 -8 4 250.88 6.59 2 -8 -4 246.24 6.07 2 -8 -4 241.03 6.59 2 -8 -3 12.34 1.49 2 -8 -3 10.81 1.60 -2 -8 3 12.36 1.52 -2 -8 2 39.40 1.66 -2 -8 2 43.88 2.39 2 -8 -2 45.00 2.50 2 -8 -2 44.04 2.81 -2 -8 1 21.34 1.41 -2 -8 1 23.74 1.72 2 -8 -1 26.55 2.02 2 -8 -1 20.43 2.10 -2 -8 0 4.29 0.92 2 -8 0 6.17 1.48 -2 -8 0 5.09 0.99 2 -8 0 6.25 1.29 -2 -8 -1 130.38 4.01 -2 -8 -1 130.29 3.60 2 -8 1 136.96 4.68 2 -8 1 128.43 5.09 -2 -8 -2 96.73 3.57 -2 -8 -2 95.00 2.85 2 -8 2 91.77 3.90 2 -8 2 98.73 4.50 -2 -8 -3 58.57 2.87 -2 -8 -3 55.68 2.02 -2 -8 -4 27.78 2.21 -2 -8 -4 30.42 1.41 2 -8 5 12.43 2.05 -2 -8 -5 8.63 1.55 -2 -8 -5 9.66 0.85 -2 -8 -6 30.34 2.48 -2 -8 -6 33.41 1.35 -2 -8 -7 32.63 1.32 -2 -8 -7 34.33 1.38 -2 -8 -8 24.14 1.23 -2 -8 -8 22.57 1.14 2 -8 8 24.72 2.73 2 -8 9 19.48 2.48 -2 -8 -9 20.46 1.14 -2 -8 -9 21.07 1.23 -2 -8 -10 6.66 0.92 -2 -7 13 13.58 2.41 -2 -7 12 4.67 1.84 -2 -7 12 4.41 1.41 2 -7 -11 12.07 1.41 -2 -7 11 16.34 2.37 -2 -7 11 16.68 1.86 -2 -7 10 0.58 1.42 -2 -7 10 3.32 1.58 2 -7 -10 2.27 0.98 -2 -7 10 2.74 1.18 2 -7 -9 62.38 2.75 -2 -7 9 59.12 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12 20.59 2.23 2 -4 13 2.52 1.39 -2 -4 -13 5.18 1.48 -2 -4 -13 3.85 1.15 -2 -4 -14 8.80 1.37 -2 -3 16 46.64 2.57 -2 -3 15 74.63 3.16 -2 -3 15 74.28 4.51 -2 -3 14 6.04 1.93 -2 -3 14 4.78 1.09 -2 -3 14 2.80 1.65 2 -3 -13 2.58 0.44 2 -3 -13 2.38 1.46 2 -3 -13 2.37 0.44 -2 -3 13 5.11 1.04 -2 -3 13 4.70 1.73 -2 -3 13 4.26 1.43 -2 -3 12 14.93 1.40 2 -3 -12 13.83 1.97 -2 -3 12 14.62 2.22 -2 -3 12 12.27 1.71 -2 -3 11 7.42 1.07 2 -3 -11 8.82 1.74 -2 -3 11 6.03 1.75 -2 -3 11 8.77 1.51 -2 -3 10 1.68 0.78 2 -3 -10 3.10 1.14 2 -3 -10 0.85 1.05 -2 -3 10 1.13 1.11 -2 -3 9 41.57 2.00 2 -3 -9 43.68 2.65 -2 -3 9 43.76 2.62 2 -3 -8 14.39 1.65 -2 -3 8 15.95 1.80 -2 -3 8 14.52 1.62 -2 -3 7 7.47 1.37 2 -3 -7 7.00 1.25 -2 -3 7 9.07 1.35 -2 -3 6 36.24 2.19 2 -3 -6 41.29 2.37 -2 -3 6 38.54 2.48 2 -3 -5 110.33 3.84 -2 -3 5 121.66 3.95 -2 -3 5 113.62 4.06 -2 -3 4 133.28 4.41 -2 -3 4 121.34 3.96 -2 -3 4 137.49 4.35 2 -3 -4 133.44 4.19 2 -3 -3 43.32 2.27 -2 -3 3 43.53 2.39 -2 -3 3 43.64 2.34 2 -3 -2 80.65 3.16 -2 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6 -2 171.37 3.80 -2 6 -3 15.48 1.91 2 6 3 16.46 1.32 -2 6 -3 19.40 1.31 2 6 3 17.95 1.79 2 6 3 16.91 1.82 -2 6 -3 13.60 0.88 2 6 4 4.78 1.25 -2 6 -4 4.52 0.74 -2 6 -4 4.34 1.25 -2 6 -4 3.97 0.41 2 6 4 4.33 0.79 2 6 4 5.30 1.31 -2 6 -5 29.47 2.58 2 6 5 36.88 2.41 -2 6 -5 31.12 1.36 2 6 5 32.28 2.51 2 6 5 32.20 1.57 2 6 6 315.20 7.74 2 6 6 319.02 5.85 -2 6 -6 305.07 8.56 2 6 7 332.43 8.02 2 6 7 326.03 5.85 -2 6 -7 341.54 9.21 2 6 8 46.78 2.86 2 6 8 46.46 3.21 -2 6 -9 11.23 1.51 -2 6 -9 12.87 2.11 2 6 9 12.03 1.73 2 6 9 12.81 2.05 -2 6 -10 16.43 2.36 2 6 10 12.00 1.74 -2 6 -10 13.11 1.63 2 6 10 18.49 2.32 -2 6 -11 2.09 1.15 2 6 11 3.74 1.33 2 6 11 0.79 1.38 2 6 12 11.72 2.02 2 6 13 -0.21 1.49 -2 7 12 4.52 1.87 -2 7 12 4.35 1.38 -2 7 11 19.78 2.54 -2 7 11 16.92 1.85 -2 7 10 3.94 1.64 -2 7 10 4.45 1.32 -2 7 9 65.74 4.02 -2 7 9 62.05 2.99 -2 7 8 40.61 3.08 2 7 -8 37.31 2.85 -2 7 8 37.55 2.31 -2 7 7 87.83 3.42 2 7 -7 91.46 4.12 -2 7 6 62.55 2.86 2 7 -6 67.62 3.46 2 7 -6 59.41 3.13 2 7 -5 73.43 3.46 -2 7 5 69.67 2.96 2 7 -5 71.33 3.38 2 7 -4 24.00 2.02 -2 7 4 24.68 1.85 2 7 -4 24.06 2.05 -2 7 3 31.05 2.07 -2 7 3 28.19 2.14 2 7 -3 30.31 2.28 -2 7 2 6.67 1.32 2 7 -2 9.10 1.55 -2 7 1 23.05 2.03 2 7 -1 21.50 2.05 2 7 -1 21.85 2.05 -2 7 0 2.53 1.11 2 7 0 2.04 1.11 2 7 0 5.61 1.36 -2 7 -1 2.77 1.23 2 7 1 3.39 0.93 2 7 1 2.77 1.25 2 7 1 3.41 1.18 -2 7 -2 151.41 5.38 -2 7 -2 154.67 4.34 2 7 2 159.78 4.23 2 7 2 152.60 5.17 2 7 2 158.77 5.43 -2 7 -2 149.78 3.52 -2 7 -3 452.68 10.43 2 7 3 457.23 8.20 -2 7 -3 444.48 8.41 2 7 3 455.68 9.99 2 7 3 466.13 10.46 -2 7 -3 443.94 7.12 2 7 4 30.20 1.54 -2 7 -4 28.67 2.50 2 7 4 28.52 2.30 -2 7 -4 29.73 1.68 2 7 4 28.55 2.46 2 7 5 0.61 0.56 2 7 5 0.57 1.05 -2 7 -5 0.72 1.11 -2 7 -5 -0.13 0.64 2 7 5 -0.34 1.28 2 7 6 0.34 0.48 2 7 6 0.44 1.11 -2 7 -6 0.94 1.26 2 7 6 -0.18 1.23 2 7 7 37.26 2.69 -2 7 -7 38.26 3.12 -2 7 -8 2.48 1.45 2 7 8 1.22 1.27 -2 7 -9 7.97 2.00 2 7 9 6.73 1.55 -2 7 -10 3.07 1.10 -2 7 -10 4.71 1.74 2 7 10 3.47 1.43 -2 7 -11 0.94 1.49 2 7 11 0.85 1.49 2 7 12 3.72 1.71 -2 8 11 4.77 1.71 -2 8 10 78.55 4.64 -2 8 10 77.73 3.20 -2 8 9 266.51 8.36 -2 8 9 257.27 6.25 -2 8 8 88.03 4.59 2 8 -8 89.78 4.30 -2 8 8 78.90 3.13 -2 8 7 0.77 1.25 2 8 -7 -0.63 1.40 -2 8 7 2.32 1.03 2 8 -6 7.31 1.59 -2 8 6 7.96 1.22 2 8 -6 5.46 1.43 2 8 -5 151.65 5.16 -2 8 5 143.95 4.32 2 8 -5 150.76 5.16 2 8 -4 252.88 6.61 -2 8 4 246.55 5.99 2 8 -4 250.32 6.89 -2 8 3 12.20 1.48 -2 8 3 15.54 1.73 2 8 -3 12.56 1.72 -2 8 2 44.44 2.77 2 8 -2 43.83 2.86 -2 8 1 20.60 2.01 2 8 -1 20.93 2.08 -2 8 0 5.89 1.41 2 8 0 4.67 1.45 2 8 0 4.49 1.30 -2 8 -1 124.81 4.84 -2 8 -1 123.42 4.20 2 8 1 129.36 4.97 2 8 1 123.32 3.91 2 8 1 128.93 4.96 -2 8 -2 90.71 4.21 -2 8 -2 94.23 3.49 2 8 2 95.19 3.16 2 8 2 105.78 4.41 2 8 2 94.12 4.28 -2 8 -2 95.77 2.68 -2 8 -3 54.82 3.38 2 8 3 55.24 2.19 -2 8 -3 57.65 2.61 2 8 3 62.23 3.41 2 8 3 55.97 3.37 -2 8 -3 53.30 1.65 2 8 4 32.81 1.50 -2 8 -4 33.60 2.77 2 8 4 29.82 2.54 -2 8 -4 33.22 1.95 2 8 4 34.50 2.79 -2 8 -5 12.47 1.28 2 8 5 8.51 0.74 2 8 5 9.85 1.74 -2 8 -5 12.32 1.97 2 8 5 11.72 1.97 -2 8 -6 31.39 2.91 2 8 6 32.49 2.87 2 8 7 35.89 3.05 -2 8 -7 43.22 3.32 -2 8 -8 23.22 2.68 -2 8 -9 26.38 2.90 -2 8 -10 5.64 1.88 -2 9 10 8.87 2.03 -2 9 9 27.71 2.84 -2 9 8 -0.21 1.46 2 9 -7 2.54 1.24 -2 9 7 4.26 1.49 2 9 -7 3.48 1.53 -2 9 7 3.74 1.01 -2 9 6 10.04 1.90 2 9 -6 11.05 1.77 -2 9 6 11.18 1.30 2 9 -6 11.95 1.74 2 9 -5 49.79 2.94 -2 9 5 47.96 2.30 2 9 -5 44.78 2.91 -2 9 4 184.34 4.90 2 9 -4 197.11 6.12 -2 9 3 416.57 8.46 -2 9 3 414.16 9.27 2 9 -3 430.29 9.86 -2 9 2 209.98 5.49 -2 9 2 197.79 6.04 2 9 -2 207.31 6.44 -2 9 1 18.01 1.97 2 9 -1 19.29 2.14 -2 9 0 5.70 1.57 2 9 0 6.46 1.49 -2 9 -1 13.97 1.88 2 9 1 10.64 1.31 -2 9 -1 9.61 1.48 2 9 1 13.01 1.98 -2 9 -2 6.11 1.57 2 9 2 5.47 0.96 -2 9 -2 5.38 1.18 2 9 2 5.97 1.55 -2 9 -3 22.23 2.34 2 9 3 23.34 1.41 -2 9 -3 25.88 1.95 2 9 3 26.09 2.51 -2 9 -3 22.19 1.06 2 9 4 -0.59 0.57 -2 9 -4 -0.40 0.94 2 9 4 1.14 1.39 -2 9 -4 0.38 1.21 -2 9 -5 1.66 0.94 -2 9 -5 0.20 1.43 2 9 5 3.73 1.55 -2 9 -6 45.15 3.45 2 9 6 42.36 3.33 2 9 7 211.88 7.44 -2 9 -7 216.09 7.65 2 9 8 295.46 9.04 -2 9 -8 291.03 9.24 2 9 9 44.69 3.68 -2 9 -9 43.75 3.74 -2 10 8 13.26 2.28 2 10 -7 2.46 1.36 -2 10 7 4.81 1.67 -2 10 6 3.02 1.63 2 10 -6 1.77 1.29 -2 10 5 1.16 1.44 2 10 -5 0.45 1.28 -2 10 4 72.52 2.74 2 10 -4 72.54 3.77 -2 10 3 27.56 1.85 -2 10 3 25.47 2.15 2 10 -3 26.79 2.42 -2 10 2 92.25 3.42 -2 10 2 87.13 3.91 2 10 -2 89.56 4.22 -2 10 1 46.87 3.00 2 10 -1 55.10 3.40 -2 10 0 0.29 1.17 -2 10 0 1.12 1.21 2 10 0 -0.18 1.30 -2 10 -1 12.20 1.88 -2 10 -1 16.25 1.90 2 10 1 11.25 1.93 -2 10 -2 3.54 1.40 -2 10 -2 1.42 1.10 2 10 2 1.50 1.29 -2 10 -3 18.12 2.23 -2 10 -3 19.22 1.89 2 10 3 17.43 2.27 2 10 4 16.25 2.29 -2 10 -4 17.20 2.33 2 10 5 10.18 2.05 -2 10 -5 11.53 2.10 -2 10 -6 43.62 3.49 2 10 6 49.59 3.68 2 10 7 35.27 3.21 -2 10 -7 23.08 2.79 -2 10 -8 125.32 6.06 2 11 -7 10.29 1.77 -2 11 7 8.19 2.08 -2 11 6 64.01 4.09 2 11 -6 54.36 3.29 -2 11 5 27.69 2.84 2 11 -5 26.40 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1.20 -3 -7 10 6.32 1.96 -3 -7 10 6.65 2.03 3 -7 -10 4.58 1.52 3 -7 -9 6.06 1.30 -3 -7 9 9.80 2.09 -3 -7 9 8.72 2.07 3 -7 -9 8.64 1.62 3 -7 -8 425.53 9.39 -3 -7 8 444.15 11.28 -3 -7 8 461.46 11.83 3 -7 -8 442.18 10.10 3 -7 -7 27.02 2.18 -3 -7 7 20.96 0.94 -3 -7 7 28.56 2.77 -3 -7 7 23.09 2.66 3 -7 -7 26.33 2.31 3 -7 -6 24.72 2.25 -3 -7 6 25.57 1.25 -3 -7 6 27.71 2.66 -3 -7 6 27.61 2.74 3 -7 -6 30.25 2.46 -3 -7 5 0.86 0.66 3 -7 -5 1.63 1.15 3 -7 -5 -0.15 1.18 -3 -7 5 1.37 1.33 -3 -7 5 0.20 1.38 3 -7 -4 24.16 2.24 -3 -7 4 20.64 1.44 -3 -7 4 21.48 2.26 -3 -7 4 22.61 2.56 3 -7 -4 24.34 2.22 -3 -7 3 4.59 0.97 3 -7 -3 7.91 1.63 3 -7 -3 7.02 1.55 -3 -7 3 8.26 1.73 -3 -7 3 6.55 1.64 -3 -7 2 13.26 1.36 3 -7 -2 11.07 1.83 3 -7 -2 11.45 1.74 -3 -7 2 13.96 1.85 -3 -7 2 15.58 2.18 3 -7 -1 22.92 2.39 -3 -7 1 22.69 1.77 -3 -7 1 24.37 2.16 3 -7 -1 24.63 2.32 3 -7 0 2.70 1.36 -3 -7 0 2.32 1.08 3 -7 0 3.23 1.44 -3 -7 0 4.01 1.31 3 -7 1 1.78 1.36 -3 -7 -1 1.26 1.03 3 -7 1 0.93 1.26 -3 -7 -1 1.78 1.18 3 -7 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-4 -3 19.37 2.45 4 -4 4 101.59 5.17 -4 -4 -4 109.26 5.13 4 -4 5 245.38 8.16 4 -4 6 55.47 3.92 4 -4 7 28.43 2.98 4 -4 8 143.46 6.34 -4 -3 10 2.19 1.72 -4 -3 9 6.91 1.93 -4 -3 8 318.71 9.89 -4 -3 8 326.47 9.33 -4 -3 7 254.06 8.48 -4 -3 7 245.87 7.77 -4 -3 6 67.72 4.29 -4 -3 6 76.74 4.16 -4 -3 5 37.78 3.21 -4 -3 5 36.76 2.88 -4 -3 4 20.70 2.54 -4 -3 4 19.20 2.19 -4 -3 3 45.00 3.42 -4 -3 3 42.21 2.94 -4 -3 2 39.53 3.28 -4 -3 2 33.28 2.59 -4 -3 1 83.21 4.49 -4 -3 1 86.23 3.88 -4 -3 0 44.95 3.38 -4 -3 0 40.01 2.67 -4 -3 -1 8.70 1.89 -4 -3 -1 4.90 1.27 -4 -3 -2 72.03 4.25 4 -3 5 46.55 3.58 4 -3 6 6.82 1.84 4 -3 7 26.48 2.94 4 -3 8 8.53 1.99 4 -3 9 24.23 2.90 -4 -2 10 1.49 1.86 -4 -2 10 0.85 1.60 -4 -2 9 179.73 6.77 -4 -2 8 1.73 1.55 -4 -2 7 73.53 4.04 -4 -2 6 41.91 3.03 -4 -2 5 7.84 1.68 -4 -2 4 6.25 1.77 -4 -2 4 7.07 1.51 -4 -2 3 1.03 1.50 -4 -2 3 1.03 1.13 -4 -2 2 1.01 1.41 -4 -2 2 1.40 1.16 -4 -2 1 24.52 2.62 -4 -2 1 22.36 2.05 -4 -2 0 60.96 3.93 -4 -2 0 62.18 3.09 -4 -2 -1 21.19 1.89 -4 -2 -1 16.50 2.39 4 -2 7 2.82 1.59 4 -2 8 7.71 1.89 4 -2 9 27.77 2.96 -4 -2 -9 26.60 2.74 4 -2 10 29.80 2.97 -4 -2 -10 28.72 2.88 -4 -2 -11 15.24 2.51 -4 -2 -12 3.11 1.67 -4 -1 13 54.75 3.50 -4 -1 11 47.24 3.70 -4 -1 10 17.86 2.74 -4 -1 10 15.14 2.39 -4 -1 9 5.25 2.09 -4 -1 9 7.18 1.84 -4 -1 8 13.85 2.30 -4 -1 8 9.35 1.95 -4 -1 7 8.80 2.08 -4 -1 7 4.17 1.48 -4 -1 6 7.84 2.04 -4 -1 6 10.42 1.77 -4 -1 5 0.47 1.21 -4 -1 4 11.04 1.66 -4 -1 3 9.38 1.57 -4 -1 2 152.50 4.97 -4 -1 1 119.22 5.47 -4 -1 1 136.96 4.51 -4 -1 0 15.94 1.63 -4 -1 0 17.22 2.40 -4 -1 0 19.54 2.16 -4 -1 -1 14.56 1.50 -4 -1 -1 13.29 2.16 -4 -1 -1 17.02 1.98 -4 -1 -2 10.62 1.72 4 -1 5 8.10 1.52 4 -1 6 12.10 1.68 -4 -1 -6 15.38 2.32 4 -1 7 5.99 1.30 -4 -1 -7 3.77 1.61 4 -1 8 2.35 1.68 -4 -1 -8 3.20 1.68 4 -1 8 2.75 1.16 4 -1 9 37.46 3.30 -4 -1 -9 37.32 3.40 4 -1 9 42.40 2.60 4 -1 10 40.56 3.30 -4 -1 -10 41.40 3.50 4 -1 10 38.95 2.57 4 -1 11 13.09 2.19 -4 -1 -11 7.04 2.02 -4 0 13 42.95 3.33 -4 0 10 1.72 1.63 -4 0 9 3.80 1.89 -4 0 8 13.12 2.33 -4 0 7 21.30 2.73 -4 0 6 2.83 1.57 -4 0 6 -0.32 1.27 -4 0 5 15.42 2.35 -4 0 5 18.06 2.02 -4 0 4 5.90 1.73 -4 0 4 2.35 1.14 -4 0 3 5.23 1.85 -4 0 3 7.95 1.43 -4 0 2 77.36 3.34 -4 0 1 13.49 1.55 -4 0 1 15.55 1.95 -4 0 0 9.44 1.33 -4 0 0 8.34 1.57 -4 0 -1 13.20 1.35 -4 0 -1 12.15 1.85 -4 0 -2 0.08 0.75 -4 0 -2 -0.15 1.18 4 0 3 5.29 1.44 -4 0 -3 6.70 1.46 4 0 4 11.43 1.73 -4 0 -5 -2.34 1.56 4 0 5 -1.00 1.21 -4 0 -6 3.26 1.67 4 0 6 2.98 1.23 -4 0 -7 -0.22 1.46 4 0 7 2.82 1.21 -4 0 -8 2.45 1.53 4 0 8 1.12 1.11 4 0 9 14.42 2.25 -4 0 -9 17.40 2.60 4 0 9 13.56 1.80 4 0 10 3.02 1.77 -4 0 -10 1.15 1.67 4 0 10 1.50 1.23 4 0 11 0.38 1.57 4 0 11 -0.27 1.25 4 0 12 0.94 1.42 -4 1 10 19.55 2.71 -4 1 9 7.51 2.08 -4 1 8 10.06 2.13 -4 1 7 4.00 1.85 -4 1 6 12.61 2.29 -4 1 5 2.37 1.63 -4 1 4 6.99 1.98 -4 1 3 9.98 2.05 -4 1 3 9.19 1.53 -4 1 2 161.46 6.39 -4 1 2 162.49 4.86 -4 1 2 158.03 5.57 -4 1 1 131.85 5.82 -4 1 1 136.18 4.20 -4 1 1 134.02 5.04 -4 1 0 16.96 1.49 -4 1 0 16.77 1.98 4 1 1 15.32 1.97 -4 1 -1 14.87 1.32 -4 1 -1 14.31 1.86 4 1 2 11.48 1.78 -4 1 -2 11.10 1.05 -4 1 -2 11.29 1.70 -4 1 -3 39.57 2.68 -4 1 -3 43.12 3.44 4 1 3 40.25 2.84 -4 1 -4 53.03 3.91 4 1 4 59.67 3.41 -4 1 -5 9.10 2.01 4 1 5 9.13 1.67 4 1 6 14.16 1.93 -4 1 -6 16.89 2.43 -4 1 -7 2.52 1.76 4 1 7 3.87 1.46 -4 1 -8 2.10 1.86 4 1 8 2.02 1.33 -4 1 -9 44.42 3.65 4 1 9 42.78 2.97 4 1 10 37.65 3.08 -4 1 -10 39.51 3.64 4 1 10 38.35 2.82 4 1 11 8.31 1.92 4 1 11 11.99 1.87 4 1 12 1.37 1.34 -4 2 10 0.95 1.75 -4 2 9 187.06 7.30 -4 2 8 0.23 1.60 -4 2 7 77.00 4.51 -4 2 6 52.34 3.71 -4 2 5 7.98 1.91 -4 2 4 8.98 1.98 -4 2 3 0.21 1.36 -4 2 2 2.16 1.57 -4 2 2 1.20 1.32 4 2 -1 20.09 2.31 -4 2 1 21.07 2.62 -4 2 1 22.65 1.73 -4 2 1 25.68 2.29 -4 2 0 58.09 2.45 -4 2 0 61.82 3.30 4 2 0 63.15 3.64 -4 2 -1 17.43 1.33 -4 2 -1 19.72 2.06 4 2 1 18.59 2.21 -4 2 -2 88.25 3.79 4 2 2 88.16 4.25 -4 2 -3 119.77 4.38 4 2 3 105.62 4.68 -4 2 -4 103.78 4.04 4 2 4 89.16 4.27 -4 2 -5 4.37 1.76 4 2 5 8.02 1.72 -4 2 -6 2.34 1.76 4 2 6 1.35 1.41 -4 2 -7 1.19 1.53 4 2 7 2.20 1.36 -4 2 -8 10.36 2.22 4 2 8 8.26 1.68 -4 2 -9 27.20 3.11 4 2 9 22.76 2.48 4 2 10 26.46 2.58 4 2 11 17.27 2.33 4 2 11 23.90 2.42 4 2 12 2.51 1.57 -4 3 10 4.00 1.88 -4 3 9 7.33 2.01 -4 3 8 343.21 10.11 -4 3 7 253.86 8.34 -4 3 6 72.83 4.45 -4 3 5 35.91 3.18 -4 3 4 16.54 2.45 -4 3 3 51.52 3.71 -4 3 2 35.20 3.22 -4 3 2 32.01 2.56 -4 3 1 78.30 4.52 4 3 -1 72.90 4.10 -4 3 0 42.76 2.08 -4 3 0 44.52 2.82 4 3 0 44.83 3.20 -4 3 -1 2.63 1.60 -4 3 -1 4.92 0.83 -4 3 -1 9.01 1.50 4 3 1 6.51 1.74 -4 3 -2 78.09 3.50 -4 3 -2 79.71 4.69 4 3 2 74.84 3.99 -4 3 -3 303.69 7.40 -4 3 -3 296.55 9.43 4 3 3 303.56 8.46 -4 3 -4 152.05 4.83 4 3 4 150.51 5.83 4 3 5 51.45 3.45 -4 3 -6 3.14 1.85 4 3 6 3.24 1.48 -4 3 -7 26.45 3.05 4 3 7 20.73 2.37 -4 3 -8 6.27 2.15 4 3 8 8.34 1.79 4 3 9 28.43 2.76 4 3 10 149.22 5.90 4 3 11 85.79 4.50 -4 4 10 8.30 2.19 -4 4 9 15.34 2.50 -4 4 8 19.36 2.61 -4 4 7 49.99 3.73 -4 4 6 137.17 5.92 -4 4 5 73.46 4.36 -4 4 4 9.70 2.17 -4 4 3 176.58 6.82 4 4 -3 163.39 6.32 -4 4 2 444.22 11.60 -4 4 2 445.05 9.98 -4 4 1 202.94 6.12 -4 4 0 52.11 2.98 -4 4 -1 8.87 2.01 -4 4 -1 3.75 0.80 -4 4 -1 7.67 1.48 4 4 1 5.04 1.58 -4 4 -2 15.13 2.41 -4 4 -2 16.65 1.83 4 4 2 19.06 2.34 -4 4 -3 20.36 2.73 -4 4 -3 17.88 1.80 4 4 3 16.99 2.30 -4 4 -4 105.82 5.58 4 4 4 108.53 5.03 -4 4 -5 221.34 8.30 4 4 5 243.36 7.68 4 4 6 59.52 3.82 4 4 7 19.06 2.49 4 4 8 137.67 5.82 4 4 9 157.73 6.24 -4 5 10 37.98 3.46 -4 5 9 9.26 2.13 -4 5 8 9.84 2.13 -4 5 7 9.44 2.18 -4 5 6 2.14 1.60 -4 5 5 2.55 1.78 -4 5 4 111.80 5.39 4 5 -3 16.74 2.36 -4 5 3 24.35 2.83 -4 5 2 131.86 5.86 -4 5 2 131.99 4.86 4 5 -2 124.38 5.51 -4 5 1 40.54 2.70 4 5 -1 38.80 3.28 -4 5 0 8.42 1.57 -4 5 0 8.18 2.04 -4 5 -1 2.83 1.72 -4 5 -1 3.18 1.17 -4 5 -2 4.54 1.89 -4 5 -2 6.76 1.39 4 5 2 1.59 1.57 -4 5 -3 19.51 2.72 4 5 3 26.72 2.72 -4 5 -4 31.06 3.26 4 5 4 29.87 2.93 -4 5 -5 68.88 4.63 4 5 5 68.94 4.17 -4 5 -6 7.47 2.23 4 5 6 3.86 1.75 4 5 7 9.08 2.02 -4 6 9 4.28 1.82 -4 6 8 17.68 2.57 -4 6 7 133.03 5.82 -4 6 6 73.74 4.38 -4 6 5 9.89 2.02 4 6 -4 0.62 1.59 -4 6 4 -0.85 1.75 4 6 -3 1.83 1.56 -4 6 3 0.43 1.77 -4 6 2 77.79 4.54 4 6 -2 73.89 4.33 -4 6 1 61.61 3.19 4 6 -1 58.97 3.89 -4 6 0 3.50 1.83 4 6 0 1.84 1.46 -4 6 -1 12.04 2.35 -4 6 -2 5.89 2.05 -4 6 -3 30.79 3.24 4 6 3 26.23 2.94 -4 6 -4 73.75 4.86 4 6 4 74.26 4.41 4 6 5 44.04 3.49 -4 7 9 51.65 3.75 -4 7 8 17.53 2.61 -4 7 7 44.51 3.45 -4 7 6 10.86 2.23 -4 7 5 2.49 1.59 4 7 -4 0.85 1.56 -4 7 4 2.52 1.63 -4 7 3 15.34 2.39 4 7 -3 12.46 2.29 -4 7 2 6.78 1.90 4 7 -2 7.82 2.00 -4 7 1 0.66 1.68 4 7 -1 -1.06 1.70 -4 7 0 5.25 1.89 4 7 0 4.06 1.85 -4 7 -1 1.72 1.78 4 7 1 1.08 1.66 -4 7 -2 11.31 2.51 -4 7 -3 28.25 3.30 -4 8 6 64.90 4.03 -4 8 5 7.67 1.98 -4 8 4 3.47 1.64 -4 8 3 3.35 1.85 -4 8 2 6.69 2.04 -4 8 1 4.56 1.83 -4 8 0 -0.97 1.70 -4 9 3 34.86 3.19 -4 9 2 35.47 3.31 -4 9 1 59.68 4.10 -5 -5 3 2.06 1.67 -5 -5 2 14.57 2.32 -5 -4 4 10.59 2.15 -5 -4 3 42.24 3.37 -5 -4 2 89.03 4.59 -5 -3 5 11.75 2.04 -5 -3 4 14.73 2.23 -5 -3 3 5.89 1.77 -5 -3 2 68.46 3.90 -5 -2 6 1.18 1.56 -5 -2 5 4.52 1.77 -5 -2 4 5.73 1.74 -5 -2 3 1.68 1.52 -5 -2 2 20.11 2.34 -5 -1 7 49.05 3.63 -5 -1 6 19.79 2.46 -5 -1 5 17.83 2.27 -5 -1 4 -0.50 1.37 -5 -1 3 9.81 1.77 -5 0 7 2.66 1.73 -5 0 6 -1.79 1.67 -5 0 5 0.67 1.38 -5 0 4 7.68 1.74 -5 1 7 42.73 3.46 -5 1 6 19.57 2.39 -5 1 5 11.97 2.02 5 1 5 39.92 3.26 -5 2 7 31.40 2.98 -5 2 6 1.82 1.48 0 0 0 0.00 0.00 TITL exp_2549 in P2(1) REM P2(1) (#4 in standard setting) CELL 0.71073 3.724894 9.632681 12.946650 90.0000 92.8429 90.0000 ZERR 2.00 0.000158 0.000366 0.000486 0.0000 0.0034 0.0000 LATT -1 SYMM -x, y+1/2,-z SFAC C H N O UNIT 24.00 16.00 4.00 4.00 REM CrysAlisPro recorded range (K): Min=100.0; max=100.0; aver:100.0 TEMP -173 SIZE 0.07 0.11 0.22 TREF HKLF 4 END _computing_structure_solution 'SHELXT 2018/2 (Sheldrick, 2018)' ; _shelx_hkl_checksum 42033 _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.131 _oxdiff_exptl_absorpt_empirical_full_min 0.894 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.7136(4) 0.20299(14) 0.48904(10) 0.0182(3) Uani 1 1 d . . . . . O2 O 0.4481(4) 0.08756(14) 0.64785(10) 0.0196(3) Uani 1 1 d . . . . . H2 H 0.466842 0.064291 0.585816 0.029 Uiso 1 1 calc R U . . . N1 N 0.9216(4) 0.62482(13) 0.67549(11) 0.0133(3) Uani 1 1 d . . . . . H1 H 1.017629 0.664652 0.622261 0.016 Uiso 1 1 calc R U . . . N2 N 0.6344(4) 0.49838(16) 0.84533(11) 0.0146(3) Uani 1 1 d . . . . . C1 C 0.8408(4) 0.41774(18) 0.57499(13) 0.0135(3) Uani 1 1 d . . . . . H1A H 0.944658 0.459972 0.517248 0.016 Uiso 1 1 calc R U . . . C2 C 0.7152(4) 0.28126(18) 0.56820(12) 0.0138(3) Uani 1 1 d . . . . . C3 C 0.5659(4) 0.21848(18) 0.66141(13) 0.0143(3) Uani 1 1 d . . . . . C4 C 0.5470(5) 0.28806(18) 0.75165(13) 0.0144(3) Uani 1 1 d . . . . . H4 H 0.455570 0.243552 0.810321 0.017 Uiso 1 1 calc R U . . . C5 C 0.7092(5) 0.7111(2) 0.94174(13) 0.0177(4) Uani 1 1 d . . . . . H5 H 0.614403 0.667900 1.000470 0.021 Uiso 1 1 calc R U . . . C6 C 0.8108(5) 0.8471(2) 0.94690(14) 0.0203(4) Uani 1 1 d . . . . . H6 H 0.786495 0.898053 1.008971 0.024 Uiso 1 1 calc R U . . . C7 C 0.9526(5) 0.9122(2) 0.85965(14) 0.0203(4) Uani 1 1 d . . . . . H7 H 1.020828 1.007138 0.863838 0.024 Uiso 1 1 calc R U . . . C8 C 0.9934(5) 0.84086(19) 0.76923(14) 0.0171(4) Uani 1 1 d . . . . . H8 H 1.090663 0.885299 0.711373 0.021 Uiso 1 1 calc R U . . . C9 C 0.8135(4) 0.49147(18) 0.66647(12) 0.0127(3) Uani 1 1 d . . . . . C10 C 0.6650(4) 0.42851(18) 0.75816(12) 0.0129(3) Uani 1 1 d . . . . . C11 C 0.8884(4) 0.70081(17) 0.76386(13) 0.0141(3) Uani 1 1 d . . . . . C12 C 0.7434(5) 0.63353(17) 0.84969(13) 0.0147(4) Uani 1 1 d . . . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0222(6) 0.0160(7) 0.0169(6) -0.0038(5) 0.0060(4) -0.0014(5) O2 0.0258(7) 0.0131(6) 0.0203(6) -0.0009(5) 0.0036(5) -0.0051(5) N1 0.0157(7) 0.0123(7) 0.0121(6) 0.0013(5) 0.0027(5) -0.0012(5) N2 0.0145(7) 0.0166(8) 0.0126(6) 0.0007(6) 0.0015(5) -0.0001(6) C1 0.0145(7) 0.0129(8) 0.0132(7) 0.0019(7) 0.0026(5) -0.0008(6) C2 0.0115(8) 0.0157(9) 0.0144(7) 0.0007(6) 0.0019(5) 0.0025(6) C3 0.0131(8) 0.0118(8) 0.0180(8) 0.0025(7) 0.0008(6) 0.0000(6) C4 0.0149(8) 0.0149(8) 0.0134(7) 0.0038(7) 0.0021(5) -0.0011(6) C5 0.0170(8) 0.0227(10) 0.0134(7) -0.0016(7) 0.0014(6) 0.0020(7) C6 0.0192(9) 0.0218(10) 0.0198(8) -0.0063(7) -0.0005(7) 0.0016(7) C7 0.0188(9) 0.0163(9) 0.0257(9) -0.0036(7) -0.0012(7) 0.0003(7) C8 0.0163(8) 0.0149(9) 0.0201(8) 0.0000(7) 0.0004(6) -0.0014(6) C9 0.0119(7) 0.0142(9) 0.0121(7) 0.0022(6) 0.0013(5) 0.0014(6) C10 0.0113(7) 0.0148(9) 0.0128(7) 0.0029(6) 0.0013(5) 0.0002(6) C11 0.0122(8) 0.0162(9) 0.0139(7) 0.0008(7) 0.0005(6) 0.0015(6) C12 0.0130(8) 0.0164(9) 0.0147(7) 0.0001(6) 0.0003(6) 0.0007(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _exptl_crystal_face_index_h _exptl_crystal_face_index_k _exptl_crystal_face_index_l _exptl_crystal_face_perp_dist -1 0 1 0.0594 0 -1 0 0.1163 -1 0 0 0.0557 1 0 0 0.0612 0 1 0 0.1008 0 0 1 0.0411 0 0 -1 0.0299 0 -1 1 0.0988 1 0 -1 0.0538 -1 0 2 0.0540 -1 -2 2 0.0932 1 2 -2 0.0906 1 -2 0 0.1012 2 0 1 0.0519 1 -1 2 0.0691 -1 2 -2 0.0904 0 -1 2 0.0747 -1 0 -2 0.0519 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C9 N1 C11 122.84(14) . . ? C10 N2 C12 118.85(14) . . ? C9 C1 C2 119.76(15) . . ? O1 C2 C1 126.62(15) . . ? O1 C2 C3 115.28(15) . . ? C1 C2 C3 118.09(14) . . ? O2 C3 C2 114.18(14) . . ? O2 C3 C4 123.20(15) . . ? C4 C3 C2 122.61(16) . . ? C3 C4 C10 119.55(15) . . ? C6 C5 C12 120.73(17) . . ? C5 C6 C7 119.98(17) . . ? C8 C7 C6 121.31(18) . . ? C7 C8 C11 118.72(17) . . ? N1 C9 C1 121.75(15) . . ? N1 C9 C10 116.54(14) . . ? C1 C9 C10 121.71(15) . . ? N2 C10 C4 119.62(14) . . ? N2 C10 C9 122.14(15) . . ? C4 C10 C9 118.23(14) . . ? N1 C11 C8 121.21(15) . . ? N1 C11 C12 117.70(15) . . ? C8 C11 C12 121.09(15) . . ? N2 C12 C5 119.93(15) . . ? N2 C12 C11 121.90(15) . . ? C11 C12 C5 118.17(15) . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C2 1.272(2) . ? O2 C3 1.344(2) . ? N1 C9 1.349(2) . ? N1 C11 1.369(2) . ? N2 C10 1.324(2) . ? N2 C12 1.364(2) . ? C1 C2 1.397(2) . ? C1 C9 1.389(2) . ? C2 C3 1.482(2) . ? C3 C4 1.352(2) . ? C4 C10 1.424(2) . ? C5 C6 1.364(3) . ? C5 C12 1.418(2) . ? C6 C7 1.417(3) . ? C7 C8 1.372(2) . ? C8 C11 1.405(2) . ? C9 C10 1.466(2) . ? C11 C12 1.416(2) . ? loop_ _exptl_oxdiff_crystal_face_indexfrac_h _exptl_oxdiff_crystal_face_indexfrac_k _exptl_oxdiff_crystal_face_indexfrac_l _exptl_oxdiff_crystal_face_x _exptl_oxdiff_crystal_face_y _exptl_oxdiff_crystal_face_z -0.9987 0.0001 1.0003 -0.0829 -0.1765 0.0147 -0.0001 -0.9988 -0.0001 0.0101 0.0013 0.0728 -0.9989 0.0000 0.0011 -0.0298 -0.1880 0.0075 0.9989 -0.0000 -0.0011 0.0298 0.1880 -0.0075 0.0001 0.9988 0.0001 -0.0101 -0.0013 -0.0728 0.0001 0.0001 0.9991 -0.0531 0.0115 0.0072 -0.0001 -0.0001 -0.9991 0.0531 -0.0115 -0.0072 0.0001 -0.9988 0.9990 -0.0430 0.0128 0.0800 0.9987 -0.0001 -1.0003 0.0829 0.1765 -0.0147 -0.9986 0.0001 1.9994 -0.1360 -0.1650 0.0219 -0.9988 -1.9975 1.9991 -0.1158 -0.1624 0.1675 0.9988 1.9975 -1.9991 0.1158 0.1624 -0.1675 0.9987 -1.9977 -0.0014 0.0500 0.1906 0.1382 1.9979 0.0001 0.9969 0.0064 0.3874 -0.0078 0.9991 -0.9987 1.9970 -0.0663 0.2122 0.0797 -0.9990 1.9976 -1.9969 0.0562 -0.2135 -0.1525 0.0002 -0.9987 1.9981 -0.0961 0.0242 0.0872 -0.9992 -0.0001 -1.9971 0.0765 -0.2109 -0.0068