#------------------------------------------------------------------------------ #$Date: 2024-07-05 21:01:12 +0300 (Fri, 05 Jul 2024) $ #$Revision: 293280 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/15/99/7159921.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7159921 loop_ _publ_author_name 'Kumar Yadav, Anup' 'Yadav, Dhananjay' 'Kumar, Vipin' 'Ray, Subhasish' 'Singh, Maya Shankar' _publ_section_title ; PIDA-promoted metal-free [3 + 2] heteroannulation of β-ketothioamides with 4-hydroxy coumarins: chemo-/regioselective access to furo[3,2-c]chromen-4-ones at room temperature. ; _journal_issue 21 _journal_name_full 'Organic & biomolecular chemistry' _journal_page_first 4326 _journal_page_last 4331 _journal_paper_doi 10.1039/d4ob00438h _journal_volume 22 _journal_year 2024 _chemical_formula_moiety 'C24 H15 N O4' _chemical_formula_sum 'C24 H15 N O4' _chemical_formula_weight 381.37 _space_group_crystal_system orthorhombic _space_group_IT_number 61 _space_group_name_Hall '-P 2ac 2ab' _space_group_name_H-M_alt 'P b c a' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2023-09-30 _audit_creation_method ; Olex2 1.5 (compiled 2023.08.24 svn.re1ec1418 for OlexSys, GUI svn.r6817) ; _audit_update_record ; 2023-10-02 deposited with the CCDC. 2024-04-29 downloaded from the CCDC. ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 8 _cell_length_a 20.4669(3) _cell_length_b 8.12770(10) _cell_length_c 21.7889(4) _cell_measurement_reflns_used 9902 _cell_measurement_temperature 293(2) _cell_measurement_theta_max 71.6510 _cell_measurement_theta_min 4.0460 _cell_volume 3624.56(10) _computing_cell_refinement 'CrysAlisPro 1.171.42.90a (Rigaku OD, 2023)' _computing_data_collection 'CrysAlisPro 1.171.42.90a (Rigaku OD, 2023)' _computing_data_reduction 'CrysAlisPro 1.171.42.90a (Rigaku OD, 2023)' _computing_molecular_graphics 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 1.5 (Dolomanov et al., 2009)' _computing_structure_refinement 'SHELXL 2018/3 (Sheldrick, 2015)' _computing_structure_solution 'SHELXT (Sheldrick, 2015)' _diffrn_ambient_temperature 293(2) _diffrn_detector 'Hybrid Pixel Array Detector' _diffrn_detector_area_resol_mean 10.0000 _diffrn_detector_type HyPix3000 _diffrn_measured_fraction_theta_full 0.996 _diffrn_measured_fraction_theta_max 0.994 _diffrn_measurement_details ; List of Runs (angles in degrees, time in seconds): # Type Start End Width t~exp~ \w \q \k \f Frames #-------------------------------------------------------------------------- 1 \w -73.00 0.00 0.50 1.74 -- -40.83 104.00 -67.00 146 2 \w -80.00 -55.00 0.50 1.74 -- -40.83 136.00 3.00 50 3 \w -27.00 23.00 0.50 1.74 -- -40.83 20.00 142.00 100 4 \w -113.00 -30.00 0.50 1.74 -- -40.83 -20.00 -23.00 166 5 \w 1.00 26.00 0.50 1.74 -- 40.83 -20.00 -23.00 50 6 \w 41.00 67.00 0.50 1.74 -- 40.83-104.00-168.00 52 7 \w 57.00 102.00 0.50 1.74 -- 40.83 20.00 142.00 90 8 \w 46.00 95.00 0.50 1.74 -- 40.83-133.00 117.00 98 9 \w -65.00 -30.00 0.50 1.74 -- -82.50 104.00 -67.00 70 10 \w -122.00 -96.00 0.50 1.74 -- -82.50 -20.00 -23.00 52 11 \w -148.00 -70.00 0.50 1.74 -- -82.50-136.00 -60.00 156 12 \w -130.00-104.00 0.50 1.74 -- -82.50-104.00-168.00 52 13 \w 88.00 116.00 0.50 1.74 -- 104.00-136.00 -60.00 56 14 \w 106.00 131.00 0.50 1.74 -- 104.00 20.00 142.00 50 15 \w 105.00 130.00 0.50 1.74 -- 104.00 133.00-174.00 50 16 \w 46.00 71.00 0.50 1.74 -- 104.00-104.00-168.00 50 17 \w 78.00 103.00 0.50 1.74 -- 104.00-133.00 117.00 50 18 \w 120.00 145.00 0.50 1.74 -- 104.00 136.00 3.00 50 19 \w 116.00 142.00 0.50 1.74 -- 104.00 104.00 -67.00 52 20 \w -107.00 -14.00 0.50 1.74 -- -40.83 -77.00 -60.00 186 21 \w -6.00 19.00 0.50 1.74 -- -40.83 32.00 -60.00 50 22 \w -5.00 20.00 0.50 1.74 -- 40.83 -11.00 120.00 50 23 \w -46.00 -15.00 0.50 1.74 -- -82.50 42.00 -90.00 62 24 \w -57.00 -21.00 0.50 1.74 -- -82.50 50.00-180.00 72 25 \w 38.00 68.00 0.50 1.74 -- 104.00 -59.00 0.00 60 26 \w 36.00 65.00 0.50 1.74 -- 104.00 -59.00 -60.00 58 27 \w 36.00 64.00 0.50 1.74 -- 104.00 -59.00-120.00 56 28 \w 53.00 79.00 0.50 1.74 -- 104.00-111.00 150.00 52 29 \w 36.00 83.00 0.50 1.74 -- 104.00 -68.00-180.00 94 30 \w 52.00 103.00 0.50 1.74 -- 104.00-111.00 -30.00 102 31 \w 46.00 71.00 0.50 1.74 -- 104.00 -93.00 120.00 50 32 \w 36.00 61.00 0.50 1.74 -- 104.00 -68.00 -90.00 50 33 \w 90.00 115.00 0.50 1.74 -- 104.00 33.00-180.00 50 34 \w 36.00 67.00 0.50 1.74 -- 104.00 -59.00 90.00 62 35 \w 88.00 117.00 0.50 1.74 -- 104.00-133.00 -90.00 58 36 \w 53.00 78.00 0.50 1.74 -- 104.00-133.00 -90.00 50 37 \w 105.00 161.00 0.50 1.74 -- 104.00 93.00 -90.00 112 38 \w 38.00 66.00 0.50 1.74 -- 104.00-133.00 90.00 56 39 \w 79.00 105.00 0.50 1.74 -- 104.00-133.00 90.00 52 40 \w 60.00 108.00 0.50 1.74 -- 104.00-111.00 120.00 96 41 \w 37.00 77.00 0.50 1.74 -- 104.00 -68.00 150.00 80 42 \w 53.00 79.00 0.50 1.74 -- 104.00 -68.00-150.00 52 43 \w 48.00 73.00 0.50 1.74 -- 104.00 -93.00-120.00 50 44 \w 125.00 172.00 0.50 1.74 -- 104.00 33.00-180.00 94 45 \w 80.00 105.00 0.50 1.74 -- 104.00 -93.00 120.00 50 46 \w 79.00 141.00 0.50 1.74 -- 104.00 17.00 30.00 124 47 \w 89.00 138.00 0.50 1.74 -- 104.00 133.00-180.00 98 ; _diffrn_measurement_device 'four-circle diffractometer' _diffrn_measurement_device_type 'XtaLAB Synergy, Dualflex, HyPix3000' _diffrn_measurement_method '\w scans' _diffrn_orient_matrix_type 'CrysAlisPro convention (1999,Acta A55,543-557)' _diffrn_orient_matrix_UB_11 -0.0344018000 _diffrn_orient_matrix_UB_12 -0.0255982000 _diffrn_orient_matrix_UB_13 -0.0621407000 _diffrn_orient_matrix_UB_21 -0.0638851000 _diffrn_orient_matrix_UB_22 -0.0436300000 _diffrn_orient_matrix_UB_23 0.0337126000 _diffrn_orient_matrix_UB_31 -0.0200693000 _diffrn_orient_matrix_UB_32 0.1826497000 _diffrn_orient_matrix_UB_33 -0.0006740000 _diffrn_radiation_monochromator mirror _diffrn_radiation_probe x-ray _diffrn_radiation_type 'Cu K\a' _diffrn_radiation_wavelength 1.54184 _diffrn_reflns_av_R_equivalents 0.0311 _diffrn_reflns_av_unetI/netI 0.0240 _diffrn_reflns_Laue_measured_fraction_full 0.996 _diffrn_reflns_Laue_measured_fraction_max 0.994 _diffrn_reflns_limit_h_max 20 _diffrn_reflns_limit_h_min -25 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_l_max 26 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_number 21846 _diffrn_reflns_point_group_measured_fraction_full 0.996 _diffrn_reflns_point_group_measured_fraction_max 0.994 _diffrn_reflns_theta_full 67.684 _diffrn_reflns_theta_max 72.047 _diffrn_reflns_theta_min 4.058 _diffrn_source 'micro-focus sealed X-ray tube' _diffrn_source_type 'PhotonJet (Cu) X-ray Source' _exptl_absorpt_coefficient_mu 0.785 _exptl_absorpt_correction_T_max 1.00000 _exptl_absorpt_correction_T_min 0.89765 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; CrysAlisPro 1.171.42.90a (Rigaku Oxford Diffraction, 2023) Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm. ; _exptl_crystal_density_diffrn 1.398 _exptl_crystal_description plate _exptl_crystal_F_000 1584 _exptl_crystal_size_max 0.2 _exptl_crystal_size_mid 0.1 _exptl_crystal_size_min 0.05 _refine_diff_density_max 0.118 _refine_diff_density_min -0.215 _refine_diff_density_rms 0.040 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.038 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 262 _refine_ls_number_reflns 3536 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.038 _refine_ls_R_factor_all 0.0538 _refine_ls_R_factor_gt 0.0413 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0662P)^2^+0.2566P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1101 _refine_ls_wR_factor_ref 0.1190 _reflns_Friedel_coverage 0.000 _reflns_number_gt 2701 _reflns_number_total 3536 _reflns_threshold_expression 'I > 2\s(I)' _iucr_refine_instructions_details ; TITL aky-45_autored_a.res in Pbca aky-45_autored.res created by SHELXL-2018/3 at 13:49:09 on 30-Sep-2023 REM Old TITL AKY-45_autored in Pbca REM SHELXT solution in Pbca: R1 0.172, Rweak 0.022, Alpha 0.020 REM 0.344 for 479 systematic absences, Orientation as input REM Formula found by SHELXT: C24 N O4 CELL 1.54184 20.4669 8.1277 21.7889 90 90 90 ZERR 8 0.0003 0.0001 0.0004 0 0 0 LATT 1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 192 120 8 32 L.S. 4 0 0 PLAN 5 SIZE 0.2 0.1 0.05 CONF BOND list 4 MORE -1 BOND $H fmap 2 53 ACTA REM REM REM WGHT 0.066200 0.256600 FVAR 1.83282 O1 4 0.673672 0.818363 0.585283 11.00000 0.04136 0.07224 = 0.05859 0.00789 0.00836 0.00614 O4 4 0.846328 0.670127 0.512393 11.00000 0.04066 0.07713 = 0.07402 0.00548 0.00648 0.00909 O2 4 0.793992 0.522420 0.443011 11.00000 0.05582 0.07428 = 0.08374 -0.00319 0.01105 0.01303 O3 4 0.561870 0.563631 0.460903 11.00000 0.04253 0.13312 = 0.07367 -0.00443 0.00865 -0.00719 N1 3 0.566208 0.765866 0.557868 11.00000 0.03937 0.09139 = 0.06379 -0.00364 0.00597 0.00684 AFIX 43 H1 2 0.540478 0.707252 0.535604 11.00000 -1.20000 AFIX 0 C1 1 0.734256 0.774959 0.562999 11.00000 0.04012 0.06166 = 0.05757 0.01600 0.00886 0.00707 C4 1 0.648026 0.531130 0.391995 11.00000 0.04572 0.05865 = 0.05966 0.00917 0.00483 0.00199 C6 1 0.729138 0.681967 0.511672 11.00000 0.04179 0.05773 = 0.05471 0.01305 0.00743 0.00518 C8 1 0.792725 0.822895 0.592873 11.00000 0.04566 0.06173 = 0.05731 0.01760 0.00379 0.00326 C10 1 0.534890 0.869679 0.600803 11.00000 0.03875 0.06914 = 0.06201 0.00510 0.01030 -0.00062 C12 1 0.660096 0.660911 0.499344 11.00000 0.04288 0.06465 = 0.05477 0.01114 0.00777 0.00515 C14 1 0.788688 0.616887 0.484900 11.00000 0.04420 0.05885 = 0.06497 0.01503 0.00823 0.00772 C16 1 0.629733 0.745434 0.546805 11.00000 0.04175 0.06934 = 0.05815 0.01162 0.00567 0.00576 C18 1 0.849421 0.766947 0.564309 11.00000 0.04634 0.06321 = 0.06717 0.01808 0.00205 0.00670 C20 1 0.476166 0.940722 0.583117 11.00000 0.04051 0.06334 = 0.07315 0.00490 0.00303 -0.00370 AFIX 43 H20 2 0.459770 0.921282 0.543977 11.00000 -1.20000 AFIX 0 C22 1 0.621273 0.583105 0.452178 11.00000 0.04446 0.07268 = 0.06249 0.01149 0.00574 0.00273 C24 1 0.689551 0.628775 0.357640 11.00000 0.06040 0.05791 = 0.06654 0.00245 0.01028 -0.00516 AFIX 43 H24 2 0.706176 0.725840 0.373979 11.00000 -1.20000 AFIX 0 C3 1 0.625538 0.385416 0.367103 11.00000 0.06303 0.06802 = 0.07764 0.01017 0.00573 -0.01325 AFIX 43 H3 2 0.597623 0.319153 0.389977 11.00000 -1.20000 AFIX 0 C13 1 0.798130 0.919805 0.645709 11.00000 0.05980 0.07646 = 0.06232 0.01094 0.00352 0.00306 AFIX 43 H13 2 0.760762 0.957645 0.665470 11.00000 -1.20000 AFIX 0 C7 1 0.442053 1.039645 0.623051 11.00000 0.04572 0.06415 = 0.10463 -0.00218 0.01046 0.00159 AFIX 43 H7 2 0.402592 1.086143 0.610927 11.00000 -1.20000 AFIX 0 C15 1 0.910412 0.807306 0.586553 11.00000 0.04534 0.08230 = 0.09107 0.01562 -0.00206 0.00702 AFIX 43 H15 2 0.947933 0.770419 0.566798 11.00000 -1.20000 AFIX 0 C2 1 0.558726 0.898834 0.658968 11.00000 0.05017 0.11522 = 0.06279 -0.00035 0.00522 0.01064 AFIX 43 H2 2 0.597876 0.851441 0.671491 11.00000 -1.20000 AFIX 0 C17 1 0.706123 0.580829 0.298812 11.00000 0.07710 0.07335 = 0.06841 0.00595 0.02008 -0.01083 AFIX 43 H17 2 0.732803 0.648123 0.275072 11.00000 -1.20000 AFIX 0 C9 1 0.914851 0.903048 0.638454 11.00000 0.05784 0.08752 = 0.09412 0.01232 -0.01763 -0.00165 AFIX 43 H9 2 0.955779 0.930870 0.653817 11.00000 -1.20000 AFIX 0 C19 1 0.643641 0.336601 0.309209 11.00000 0.08720 0.06829 = 0.07894 -0.00865 0.00248 -0.01338 AFIX 43 H19 2 0.628739 0.237158 0.293402 11.00000 -1.20000 AFIX 0 C5 1 0.858949 0.958876 0.668304 11.00000 0.07209 0.08455 = 0.07268 0.00759 -0.01090 -0.00270 AFIX 43 H5 2 0.862722 1.022662 0.703561 11.00000 -1.20000 AFIX 0 C21 1 0.465979 1.069772 0.680469 11.00000 0.05955 0.08392 = 0.10086 -0.01920 0.02538 -0.00787 AFIX 43 H21 2 0.443184 1.137812 0.707286 11.00000 -1.20000 AFIX 0 C11 1 0.683638 0.434873 0.274983 11.00000 0.08518 0.07697 = 0.06722 -0.00482 0.01218 -0.00356 AFIX 43 H11 2 0.695658 0.403057 0.235570 11.00000 -1.20000 AFIX 0 C23 1 0.524081 0.998861 0.698498 11.00000 0.06520 0.12641 = 0.06918 -0.01852 0.01005 -0.00971 AFIX 43 H23 2 0.540121 1.018643 0.737744 11.00000 -1.20000 AFIX 0 HKLF 4 REM aky-45_autored_a.res in Pbca REM wR2 = 0.1190, GooF = S = 1.038, Restrained GooF = 1.038 for all data REM R1 = 0.0413 for 2701 Fo > 4sig(Fo) and 0.0538 for all 3536 data REM 262 parameters refined using 0 restraints END WGHT 0.0656 0.2561 REM Highest difference peak 0.118, deepest hole -0.215, 1-sigma level 0.040 Q1 1 0.5405 0.9410 0.7463 11.00000 0.05 0.12 Q2 1 0.5946 0.7784 0.6822 11.00000 0.05 0.10 Q3 1 0.4461 1.0921 0.7431 11.00000 0.05 0.10 Q4 1 0.5582 0.2638 0.2594 11.00000 0.05 0.10 Q5 1 0.8676 1.1498 0.7356 11.00000 0.05 0.10 REM The information below was added by Olex2. REM REM R1 = 0.0413 for 2701 Fo > 4sig(Fo) and 0.0538 for all 23626 data REM 262 parameters refined using n/a restraints REM Highest difference peak 0.12, deepest hole -0.21 REM Mean Shift 0, Max Shift 0.001. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0538 REM R1_gt = 0.0413 REM wR_ref = 0.1190 REM GOOF = 1.038 REM Shift_max = 0.001 REM Shift_mean = 0 REM Reflections_all = 23626 REM Reflections_gt = 2701 REM Parameters = 262 REM Hole = -0.21 REM Peak = 0.12 REM Flack = n/a ; _cod_data_source_file d4ob00438h2.cif _cod_data_source_block aky-45_autored _cod_depositor_comments 'Adding full bibliography for 7159921--7159922.cif.' _cod_database_code 7159921 _shelx_shelxl_version_number 2018/3 _chemical_oxdiff_formula 'C H N O S' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.962 _shelx_estimated_absorpt_t_min 0.859 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All N(H) groups 2.a Aromatic/amide H refined with riding coordinates: N1(H1), C20(H20), C24(H24), C3(H3), C13(H13), C7(H7), C15(H15), C2(H2), C17(H17), C9(H9), C19(H19), C5(H5), C21(H21), C11(H11), C23(H23) ; _olex2_submission_special_instructions 'No special instructions were received' _oxdiff_exptl_absorpt_empirical_details ; Empirical correction (ABSPACK) includes: - Absorption correction using spherical harmonics - Frame scaling ; _oxdiff_exptl_absorpt_empirical_full_max 1.221 _oxdiff_exptl_absorpt_empirical_full_min 0.794 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' '-x, -y, -z' 'x-1/2, y, -z-1/2' 'x, -y-1/2, z-1/2' '-x-1/2, y-1/2, z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1 O 0.67367(5) 0.81836(13) 0.58528(5) 0.0574(3) Uani 1 1 d . . . . . O4 O 0.84633(5) 0.67013(13) 0.51239(5) 0.0639(3) Uani 1 1 d . . . . . O2 O 0.79399(5) 0.52242(15) 0.44301(6) 0.0713(3) Uani 1 1 d . . . . . O3 O 0.56187(6) 0.56363(18) 0.46090(6) 0.0831(4) Uani 1 1 d . . . . . N1 N 0.56621(6) 0.76587(18) 0.55787(6) 0.0649(4) Uani 1 1 d . . . . . H1 H 0.540478 0.707252 0.535604 0.078 Uiso 1 1 calc R U . . . C1 C 0.73426(7) 0.77496(18) 0.56300(7) 0.0531(3) Uani 1 1 d . . . . . C4 C 0.64803(7) 0.53113(17) 0.39200(7) 0.0547(4) Uani 1 1 d . . . . . C6 C 0.72914(7) 0.68197(16) 0.51167(7) 0.0514(3) Uani 1 1 d . . . . . C8 C 0.79273(7) 0.82289(18) 0.59287(7) 0.0549(4) Uani 1 1 d . . . . . C10 C 0.53489(7) 0.86968(19) 0.60080(7) 0.0566(4) Uani 1 1 d . . . . . C12 C 0.66010(7) 0.66091(18) 0.49934(7) 0.0541(3) Uani 1 1 d . . . . . C14 C 0.78869(7) 0.61689(18) 0.48490(7) 0.0560(4) Uani 1 1 d . . . . . C16 C 0.62973(7) 0.74543(19) 0.54681(7) 0.0564(4) Uani 1 1 d . . . . . C18 C 0.84942(7) 0.76695(19) 0.56431(7) 0.0589(4) Uani 1 1 d . . . . . C20 C 0.47617(7) 0.94072(18) 0.58312(8) 0.0590(4) Uani 1 1 d . . . . . H20 H 0.459770 0.921282 0.543977 0.071 Uiso 1 1 calc R U . . . C22 C 0.62127(7) 0.58310(19) 0.45218(7) 0.0599(4) Uani 1 1 d . . . . . C24 C 0.68955(8) 0.62878(19) 0.35764(7) 0.0616(4) Uani 1 1 d . . . . . H24 H 0.706176 0.725840 0.373979 0.074 Uiso 1 1 calc R U . . . C3 C 0.62554(9) 0.3854(2) 0.36710(8) 0.0696(4) Uani 1 1 d . . . . . H3 H 0.597623 0.319153 0.389977 0.083 Uiso 1 1 calc R U . . . C13 C 0.79813(8) 0.9198(2) 0.64571(8) 0.0662(4) Uani 1 1 d . . . . . H13 H 0.760762 0.957645 0.665470 0.079 Uiso 1 1 calc R U . . . C7 C 0.44205(8) 1.0396(2) 0.62305(9) 0.0715(5) Uani 1 1 d . . . . . H7 H 0.402592 1.086143 0.610927 0.086 Uiso 1 1 calc R U . . . C15 C 0.91041(8) 0.8073(2) 0.58655(9) 0.0729(5) Uani 1 1 d . . . . . H15 H 0.947933 0.770419 0.566798 0.087 Uiso 1 1 calc R U . . . C2 C 0.55873(8) 0.8988(3) 0.65897(8) 0.0761(5) Uani 1 1 d . . . . . H2 H 0.597876 0.851441 0.671491 0.091 Uiso 1 1 calc R U . . . C17 C 0.70612(9) 0.5808(2) 0.29881(8) 0.0730(5) Uani 1 1 d . . . . . H17 H 0.732803 0.648123 0.275072 0.088 Uiso 1 1 calc R U . . . C9 C 0.91485(9) 0.9030(2) 0.63845(10) 0.0798(5) Uani 1 1 d . . . . . H9 H 0.955779 0.930870 0.653817 0.096 Uiso 1 1 calc R U . . . C19 C 0.64364(10) 0.3366(2) 0.30921(9) 0.0781(5) Uani 1 1 d . . . . . H19 H 0.628739 0.237158 0.293402 0.094 Uiso 1 1 calc R U . . . C5 C 0.85895(9) 0.9589(2) 0.66830(9) 0.0764(5) Uani 1 1 d . . . . . H5 H 0.862722 1.022662 0.703561 0.092 Uiso 1 1 calc R U . . . C21 C 0.46598(9) 1.0698(2) 0.68047(10) 0.0814(5) Uani 1 1 d . . . . . H21 H 0.443184 1.137812 0.707286 0.098 Uiso 1 1 calc R U . . . C11 C 0.68364(10) 0.4349(2) 0.27498(9) 0.0765(5) Uani 1 1 d . . . . . H11 H 0.695658 0.403057 0.235570 0.092 Uiso 1 1 calc R U . . . C23 C 0.52408(9) 0.9989(3) 0.69850(9) 0.0869(6) Uani 1 1 d . . . . . H23 H 0.540121 1.018643 0.737744 0.104 Uiso 1 1 calc R U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0414(5) 0.0722(6) 0.0586(6) 0.0079(5) 0.0084(5) 0.0061(4) O4 0.0407(6) 0.0771(7) 0.0740(7) 0.0055(6) 0.0065(5) 0.0091(5) O2 0.0558(7) 0.0743(7) 0.0837(8) -0.0032(6) 0.0110(6) 0.0130(5) O3 0.0425(6) 0.1331(11) 0.0737(7) -0.0044(7) 0.0086(5) -0.0072(6) N1 0.0394(6) 0.0914(9) 0.0638(8) -0.0036(7) 0.0060(6) 0.0068(6) C1 0.0401(7) 0.0617(8) 0.0576(8) 0.0160(7) 0.0089(6) 0.0071(6) C4 0.0457(7) 0.0587(8) 0.0597(8) 0.0092(7) 0.0048(6) 0.0020(6) C6 0.0418(7) 0.0577(7) 0.0547(8) 0.0131(6) 0.0074(6) 0.0052(6) C8 0.0457(8) 0.0617(8) 0.0573(8) 0.0176(7) 0.0038(6) 0.0033(6) C10 0.0388(7) 0.0691(8) 0.0620(9) 0.0051(7) 0.0103(6) -0.0006(6) C12 0.0429(7) 0.0646(8) 0.0548(8) 0.0111(6) 0.0078(6) 0.0051(6) C14 0.0442(8) 0.0589(8) 0.0650(9) 0.0150(7) 0.0082(7) 0.0077(6) C16 0.0417(7) 0.0693(8) 0.0581(8) 0.0116(7) 0.0057(6) 0.0058(7) C18 0.0463(8) 0.0632(8) 0.0672(9) 0.0181(7) 0.0021(7) 0.0067(7) C20 0.0405(7) 0.0633(8) 0.0732(10) 0.0049(7) 0.0030(7) -0.0037(6) C22 0.0445(8) 0.0727(9) 0.0625(9) 0.0115(7) 0.0057(7) 0.0027(7) C24 0.0604(9) 0.0579(8) 0.0665(9) 0.0025(7) 0.0103(8) -0.0052(7) C3 0.0630(10) 0.0680(9) 0.0776(11) 0.0102(9) 0.0057(9) -0.0133(8) C13 0.0598(10) 0.0765(10) 0.0623(9) 0.0109(8) 0.0035(8) 0.0031(8) C7 0.0457(8) 0.0642(9) 0.1046(14) -0.0022(9) 0.0105(9) 0.0016(7) C15 0.0453(8) 0.0823(11) 0.0911(13) 0.0156(10) -0.0021(9) 0.0070(8) C2 0.0502(9) 0.1152(14) 0.0628(10) -0.0004(10) 0.0052(8) 0.0106(9) C17 0.0771(12) 0.0733(10) 0.0684(10) 0.0059(8) 0.0201(9) -0.0108(9) C9 0.0578(10) 0.0875(12) 0.0941(14) 0.0123(11) -0.0176(10) -0.0017(9) C19 0.0872(13) 0.0683(9) 0.0789(12) -0.0086(9) 0.0025(10) -0.0134(9) C5 0.0721(12) 0.0845(11) 0.0727(11) 0.0076(9) -0.0109(9) -0.0027(10) C21 0.0596(11) 0.0839(11) 0.1009(15) -0.0192(11) 0.0254(10) -0.0079(9) C11 0.0852(12) 0.0770(10) 0.0672(10) -0.0048(8) 0.0122(9) -0.0036(9) C23 0.0652(11) 0.1264(16) 0.0692(11) -0.0185(11) 0.0101(9) -0.0097(12) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _diffrn_refln_index_h _diffrn_refln_index_k _diffrn_refln_index_l _diffrn_refln_intensity_net _diffrn_refln_intensity_u _diffrn_refln_scale_group_code 0 0 2 264442 8974.27 20 0 0 2 265940 8975.8 4 0 0 3 8.97942 4.69517 20 0 0 3 3.7846 6.73012 4 0 0 4 31710.9 1088.54 20 0 0 4 32493 1091.95 4 0 0 5 8.64944 6.85093 20 0 0 5 6.53475 10.0383 4 0 0 6 320.741 18.6684 20 0 0 6 345.872 23.6388 4 0 0 7 -2.20319 7.87156 20 0 0 7 -1.91298 12.2574 4 0 0 8 26344.3 910.016 4 0 0 9 -12.9984 13.7378 4 0 0 10 122.199 21.038 4 0 0 11 -3.43842 14.3302 10 0 0 11 3.38776 14.7469 4 0 0 12 236.295 28.9779 10 0 0 12 272.262 30.0293 4 0 0 13 -4.33886 16.0601 10 0 0 13 38.8149 16.8584 4 0 0 14 7583.82 292.145 10 0 0 14 7427.59 291.676 4 0 0 -15 -5.49018 19.9164 14 0 0 15 -5.32608 20.8093 10 0 0 -16 833.503 63.3688 14 0 0 16 738.88 60.0633 10 0 0 -17 -19.4143 24.3962 14 0 0 17 12.5507 21.3545 10 0 0 -18 274.974 41.514 14 0 0 18 259.654 40.2692 10 0 0 -19 -7.1551 28.4333 14 0 0 -24 6.00288 19.9662 12 0 0 24 28.6331 19.5941 46 0 0 25 -3.89519 16.4785 46 0 0 26 13.5396 15.9215 19 0 1 0 4.51172 6.17274 2 0 1 0 0.75543 6.34492 1 0 1 -1 4.87117 6.48588 8 0 1 1 6.2688 5.85058 8 0 1 1 3.63343 4.1331 22 0 -1 1 0.71774 2.72993 4 0 1 1 8.30486 6.57372 2 0 1 -1 3.13636 6.63475 1 0 1 -1 8.28926 6.28211 2 0 1 1 -0.77051 6.44757 1 0 1 1 3.2305 2.77743 4 0 -1 -2 0.98185 4.47754 7 0 1 2 5.55739 6.92904 8 0 1 -2 0.4986 4.59049 7 0 1 -2 7.62347 6.24004 8 0 -1 2 -0.49848 4.54648 4 0 1 2 1.0153 4.74579 4 0 1 -2 10.4274 7.5654 1 0 1 -3 7.48955 5.90865 8 0 1 -3 9.06934 6.67201 7 0 1 3 5.47417 6.04103 8 0 -1 -3 2.98374 6.54052 7 0 -1 3 2.27723 6.10924 4 0 1 3 -0.76934 5.63884 4 0 1 -4 -0.67438 5.81069 8 0 -1 -4 7.06186 8.1509 7 0 1 -4 -9.17311 8.3339 7 0 1 4 4.76859 6.48265 8 0 -1 4 8.86228 8.91406 20 0 1 4 3.78122 3.30669 20 0 1 4 9.34491 8.2527 4 0 -1 4 4.11682 8.11179 4 0 1 -5 15.5419 9.30306 7 0 -1 -5 1.28321 9.54065 7 0 -1 5 8.98677 9.49969 20 0 -1 5 1.30959 9.11425 4 0 1 5 -5.27985 9.48118 4 0 -1 6 13.0689 9.77009 20 0 -1 6 -3.21101 10.0202 4 0 1 6 -1.61555 10.549 4 0 -1 7 -8.1843 10.4891 20 0 -1 7 9.58778 13.3446 4 0 1 7 -7.7074 12.8891 4 0 -1 8 1.83571 10.4019 20 0 1 8 6.77867 11.9344 4 0 -1 8 -2.2513 11.6643 4 0 -1 9 -14.1699 10.8974 20 0 -1 9 -2.60726 13.11 4 0 1 9 -10.4562 14.6946 4 0 1 10 -9.1481 15.4862 10 0 -1 10 -2.21253 10.2784 20 0 -1 10 8.96266 14.0469 4 0 1 10 -2.99248 14.4011 4 0 -1 11 3.40496 16.7571 4 0 1 11 -13.6306 20.5382 4 0 -1 11 -13.8015 18.735 10 0 -1 12 -7.70764 15.3159 4 0 1 12 30.8303 18.1211 4 0 1 12 7.78076 17.8524 10 0 -1 12 3.88764 17.8398 10 0 -1 13 -4.33197 17.5029 4 0 1 13 -8.65759 17.4901 4 0 -1 13 -8.70211 20.7034 10 0 1 13 -21.7551 19.7171 10 0 -1 14 19.344 19.5374 4 0 1 14 43.4648 20.4328 4 0 -1 14 4.82846 18.2053 10 0 1 14 -14.496 21.6125 10 0 1 15 5.31235 21.1106 10 0 -1 15 -5.31878 22.1677 10 0 -1 -15 -5.48491 25.168 14 0 1 -15 -16.4945 24.9114 14 0 -1 16 5.79862 24.9014 10 0 1 16 -5.78891 24.5023 10 0 1 -16 -41.9249 28.1717 14 0 -1 -16 -29.8895 28.1182 14 0 1 17 -6.22623 21.6711 10 0 -1 17 -6.23888 26.008 10 0 -1 -17 -12.8652 26.8152 14 0 1 -17 -38.6476 25.6024 14 0 -1 -18 6.80883 28.8046 14 0 1 -18 6.81452 26.6247 14 0 -1 -21 6.88754 26.4436 33 0 1 -21 -31.4694 27.3758 12 0 -1 -22 -32.3763 30.0839 33 0 1 -22 14.8942 23.5548 12 0 -1 -23 -11.6921 22.8401 33 0 1 -23 13.5688 24.1131 12 0 -1 -24 -5.03727 20.9937 33 0 1 -24 11.8484 20.1594 12 0 -1 -25 8.1849 17.0582 33 0 -1 25 -12.1541 17.3911 46 0 1 25 -16.7374 17.9618 19 0 -1 -26 -39.5165 15.1308 33 0 1 26 -6.48376 14.7003 19 0 -1 26 9.26887 12.8905 46 0 2 0 8730.28 308.285 1 0 2 -1 67918.4 2313.94 8 0 2 -1 67774 2309.57 21 0 2 1 68890.8 2315.02 1 0 2 -1 67612.6 2315.26 1 0 2 -2 128247 4396.4 8 0 2 2 131320 4396.44 8 0 2 -2 129146 4392.64 21 0 2 2 128250 4391.55 22 0 2 2 132184 4398.22 1 0 2 -2 129559 4398.69 1 0 2 -3 201034 6894.11 8 0 2 3 204584 6894.16 8 0 2 3 203376 6891.07 22 0 2 -3 204431 6897.01 1 0 2 4 17515.4 601.416 8 0 2 -4 17290.9 601.358 8 0 -2 4 17439.3 602.985 20 0 2 -4 17436.6 604.941 1 0 2 5 2508.41 96.8916 8 0 2 -5 2515.43 96.8446 8 0 -2 5 2398.75 99.2051 20 0 2 5 2586.27 96.28 4 0 2 -5 2589.64 101.897 1 0 -2 6 16905 588.555 20 0 2 6 16568.1 585.142 4 0 2 -6 17386 591.345 1 0 -2 7 57.805 13.9777 20 0 2 7 38.87 12.0829 4 0 2 -7 58.99 15.879 1 0 -2 8 1291.77 61.5059 20 0 -2 8 1283.08 60.2685 4 0 2 -8 1306.1 64.8892 1 0 2 8 1264.05 60.4693 4 0 -2 9 1830.12 81.1734 20 0 2 9 1766.7 80.685 4 0 -2 9 1785.86 80.5094 4 0 2 -9 1871.03 85.7618 1 0 -2 10 1629.85 75.0413 20 0 -2 10 1468.34 73.8906 4 0 2 -10 1596.26 80.8623 1 0 2 10 1647.29 76.3295 4 0 -2 11 11445.4 420.051 20 0 2 -11 11955.2 429.451 1 0 2 11 11745.5 423.076 4 0 -2 12 11180 402.095 20 0 2 12 11127.1 406.459 4 0 2 -12 10889.2 411.769 1 0 2 -13 30.8258 19.3959 1 0 2 14 4633.29 196.909 10 0 2 -14 4940.35 204.979 1 0 2 15 3052.64 139.813 10 0 2 -15 2906.26 143.718 1 0 2 16 1547.67 87.8256 10 0 2 -16 1503.8 95.8005 12 0 2 -16 1315.65 87.6864 1 0 2 -17 2577.04 135.3 1 0 2 17 2566.78 129.868 22 0 2 -17 2498.04 137.66 12 0 2 -18 15.8812 32.5929 12 0 2 -19 4000.6 192.956 12 0 2 -20 -8.06559 24.1281 12 0 -2 -21 124.528 34.9129 33 0 2 -21 69.9166 28.9066 12 0 -2 -22 70.7371 29.3678 33 0 2 22 139.564 33.7291 19 0 2 -22 130.094 34.9762 12 0 -2 -23 17.239 26.0365 33 0 2 23 -38.0154 23.6416 19 0 2 -23 6.46965 21.511 12 0 -2 -24 14.723 21.6592 33 0 2 -24 16.6594 19.7387 12 0 2 24 -4.65548 19.9835 19 0 -2 -25 -7.91484 16.247 33 0 -2 25 18.6426 15.3079 46 0 2 25 34.0393 18.4118 19 0 -2 -26 128.436 19.3645 33 0 2 26 79.2571 17.8767 19 0 -2 26 99.908 16.8322 46 0 3 0 -4.52579 11.4922 8 0 3 0 -2.28392 11.7167 6 0 3 0 2.47848 14.0439 1 0 3 1 -6.78537 12.061 8 0 3 -1 -15.8888 12.544 8 0 3 1 -4.93275 12.7811 1 0 3 1 4.67533 12.3495 6 0 3 -1 -10.0956 13.4581 1 0 3 -1 -9.09589 12.5669 6 0 3 2 15.8742 12.5326 8 0 3 -2 27.3993 15.1845 8 0 3 -2 -2.62 13.577 1 0 3 2 9.89071 13.7819 1 0 3 2 -2.43965 12.0074 6 0 -3 3 -4.10741 11.6393 20 0 3 3 -4.55444 12.3655 8 0 3 -3 -13.7943 13.7563 8 0 3 -3 -2.7465 14.0916 1 0 -3 4 -6.76476 12.0216 20 0 3 -4 11.588 12.5825 8 0 3 4 -2.29126 10.9004 8 0 3 -4 2.88719 14.8114 1 0 -3 5 7.40178 13.3963 20 0 3 -5 3.00071 14.9259 1 0 -3 6 13.4174 14.046 20 0 3 -6 12.6846 17.0679 1 0 3 -7 -6.85119 14.9124 1 0 -3 7 2.90372 14.7474 20 0 3 -7 -10.7934 15.4429 12 0 3 -8 -7.44497 18.9067 1 0 -3 8 -6.31665 15.7113 20 0 3 -8 -11.7624 17.5371 12 0 3 -9 4.04664 17.6159 1 0 -3 9 3.40071 14.3872 20 0 3 -9 8.58358 17.0553 12 0 3 -10 -8.86331 19.2909 1 0 -3 10 7.32489 14.5535 20 0 3 -10 4.70816 18.7089 12 0 3 -11 14.6066 17.6626 1 0 -3 11 -3.89756 14.4194 20 0 3 -11 10.3327 19.8342 12 0 3 -12 5.33948 17.7519 1 0 3 -12 -11.3188 23.5864 12 0 -3 12 16.6541 17.8703 20 0 3 13 -4.94539 17.9394 34 0 3 -13 5.83317 18.9259 1 0 3 -13 6.17539 21.9486 12 0 -3 13 4.3877 15.2665 20 0 3 14 5.23485 18.6059 34 0 3 -14 -25.3342 24.3144 1 0 -3 14 13.9329 15.4409 20 0 3 -14 6.69596 27.4805 12 0 3 -15 6.81668 20.9832 1 0 3 -15 7.19349 28.5858 12 0 3 -16 -7.25005 22.9289 1 0 3 16 13.1018 24.2354 19 0 3 -16 22.8943 26.5538 12 0 3 -17 -15.9296 25.8444 12 0 3 17 -6.76839 25.041 19 0 3 -18 -8.14466 33.4261 12 0 3 18 13.7296 27.7297 19 0 3 19 -6.80543 25.6578 19 0 3 -19 -16.2472 27.6462 12 0 -3 -20 20.6187 26.3911 33 0 3 -20 15.7563 26.1983 12 0 3 20 13.1367 28.1978 19 0 -3 -21 12.9325 26.1226 33 0 3 21 6.14854 24.8393 19 0 3 -21 14.7916 22.1263 12 0 -3 -22 5.86935 25.1928 33 0 3 22 -16.6846 25.1987 19 0 3 -22 13.3978 20.0396 12 0 3 -22 -10.1557 19.1436 26 0 3 22 -16.7554 18.5699 24 0 3 -23 -11.6497 20.2754 12 0 3 23 19.2641 17.1273 24 0 -3 -23 -5.11596 21.0044 33 0 3 24 -12.047 17.4807 19 0 -3 -24 12.7379 19.2378 33 0 -3 24 -11.5211 15.5134 46 0 -3 -25 6.58032 14.7145 33 0 3 25 -18.6999 13.754 19 0 -3 25 8.85118 13.5378 46 0 4 0 2575.79 114.969 9 0 4 0 2588.61 112.248 6 0 4 0 2525.88 113.016 1 0 4 -1 412.834 35.7064 9 0 4 1 389.231 34.8311 1 0 4 -1 401.665 35.3061 1 0 4 1 404.152 34.0572 6 0 4 -2 2993.92 126.741 9 0 4 2 2735.55 122.828 6 0 4 2 2998.21 125.617 1 0 4 -2 2859.13 125.123 1 0 -4 3 19.1716 13.0316 20 0 4 -3 7.83332 16.0758 9 0 4 3 -3.59978 15.6715 6 0 4 -3 3.81847 16.3909 1 0 -4 4 1099.69 57.9703 20 0 4 -4 1114.82 65.0961 9 0 4 -4 1073.9 64.346 1 0 4 4 1143.72 63.7416 6 0 -4 5 161.874 23.7757 20 0 4 -5 175.017 27.717 9 0 4 -5 146.794 26.7372 1 0 -4 6 26968 942.513 20 0 4 -6 27211.4 951.375 9 0 4 -6 26912.7 950.199 1 0 -4 7 31706 1095.7 20 0 4 -7 32205.4 1105.91 9 0 4 -7 30502.8 1103.7 1 0 4 -8 34552.8 1193.3 1 0 -4 8 33646.1 1184.06 20 0 4 -9 14255.7 531.988 1 0 -4 9 14699.5 524.977 20 0 4 -10 5448 230.542 12 0 -4 10 5810.51 223.718 20 0 4 -10 5370.76 229.928 1 0 -4 11 2351.3 112.417 20 0 4 11 2117.23 116.171 19 0 4 11 2445.03 119.898 37 0 4 -11 2462.36 123.108 12 0 4 11 2273.98 114.941 34 0 4 -11 2386.28 115.474 32 0 4 -11 2367.42 114.097 27 0 4 -11 2428.82 121.243 1 0 4 12 2097.47 112.932 19 0 -4 12 2211.39 107.862 20 0 4 12 2274.9 114.166 37 0 4 -12 2140.73 109.292 32 0 4 12 2220.55 111.419 34 0 4 -12 2152.1 115.564 1 0 4 -12 2082.84 108.702 27 0 4 -12 1980.07 113.94 12 0 4 13 42.246 25.5541 37 0 4 13 86.4452 27.1183 34 0 4 -13 45.0024 21.623 32 0 -4 13 5.2006 16.4825 20 0 4 -13 6.87408 21.1868 1 0 4 -13 42.2562 25.5707 12 0 4 13 56.4577 30.5493 19 0 4 14 475.629 51.3886 37 0 4 -14 473.043 48.1859 32 0 4 14 594.317 53.5918 34 0 -4 14 509.036 46.0133 20 0 4 -14 517.83 54.508 1 0 4 -14 529.359 55.5957 12 0 4 14 576.706 55.1957 19 0 4 -15 41.8843 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130.526 16 1 6 -12 2394.98 128.545 32 -1 6 -12 2517.41 129.423 32 -1 6 -12 2436.67 127.552 30 1 6 -12 2824.3 143.388 9 -1 6 -12 2452.3 136.166 9 -1 6 13 1708.87 97.8815 41 1 6 13 1555.07 96.2337 41 -1 6 13 1463.75 95.6888 16 1 6 13 1568.49 100.009 16 1 6 -13 1638.26 97.1706 32 -1 6 -13 1517.97 94.2416 32 -1 6 -13 1562.28 94.5889 30 1 6 -13 1576.7 95.4531 30 1 6 -13 1522.05 101.838 9 -1 6 -13 1533.69 101.681 9 1 6 14 1831.17 107.54 41 -1 6 14 1806.43 105.653 41 -1 6 14 1970.16 112.069 16 1 6 14 1748.06 108.193 16 1 6 -14 1833.06 105.936 32 -1 6 -14 1861.38 105.178 26 -1 6 -14 2123.73 109.371 30 1 6 -14 1966.71 107.497 30 -1 6 -14 1957.08 115.662 9 1 6 -14 2012.34 117.034 9 1 6 15 106.678 29.9961 41 -1 6 15 92.7292 28.1608 41 1 6 15 99.579 31.3496 16 -1 6 15 39.6842 28.1318 16 1 6 -15 73.5463 27.9215 32 1 6 -15 104.503 28.3572 30 -1 6 -15 78.6678 27.2206 26 -1 6 -15 112.243 28.8988 30 1 6 -15 38.2369 27.3369 9 -1 6 -15 153.361 35.7412 9 -1 6 16 297.936 43.0361 16 1 6 16 430.055 48.5467 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541.227 21 -6 3 -3 14447 508.763 2 -6 3 3 14664.5 508.406 2 -6 3 3 13757.3 506.959 11 -6 3 -3 13555.6 507.242 11 -6 3 -3 13781.7 505.962 8 -6 3 3 14252.4 505.983 8 -6 -3 3 14339.7 499.504 20 6 3 -3 14790.8 507.749 21 -6 3 -4 6164.79 234.615 2 -6 3 4 6343.96 234.496 2 -6 3 -4 5921.94 231.779 8 -6 3 4 6246.65 232.25 8 -6 3 -4 5833.41 233.222 11 -6 3 4 6030.73 233.152 11 -6 -3 4 6334.74 227.883 20 6 3 -4 6130.7 233.854 21 -6 3 4 6205.93 232.157 24 6 3 4 5897.61 233.203 23 -6 3 -5 92.0762 20.6097 2 -6 3 5 132.657 21.4486 2 6 3 5 134.863 23.2368 23 -6 3 5 98.5379 20.4099 24 -6 -3 5 158.618 20.6678 20 6 3 -5 141.983 23.789 21 -6 3 5 89.3078 17.6067 8 -6 3 -5 105.661 20.425 8 6 3 6 8924.12 332.167 23 -6 3 6 8785.77 330.157 24 -6 -3 6 9103.6 326.396 20 6 3 -6 8792.6 330.765 21 6 3 7 4616.77 196.307 23 -6 3 7 5330.93 199.241 24 -6 -3 7 4983.91 192.739 20 6 3 -7 4796.32 196.149 21 -6 -3 8 134.605 22.7296 20 6 3 8 160.56 25.5411 23 6 3 -8 173 28.3853 21 -6 3 8 165.719 26.147 24 6 3 9 230.76 31.5303 23 -6 -3 9 267.688 29.0007 20 -6 3 9 206.34 29.7078 24 -6 -3 10 461.095 39.6419 20 -6 3 10 440.017 41.8505 24 -6 3 11 4427.55 191.792 37 -6 -3 11 4834.31 187.968 20 -6 3 11 4276.55 190.372 24 6 -3 11 4322.35 185.398 20 -6 3 -11 4702.24 192.008 26 -6 3 12 620.625 51.3149 37 -6 3 -12 518.944 47.9632 26 -6 -3 12 492.313 42.6549 20 -6 3 12 518.756 48.7245 24 6 -3 12 523.009 43.9685 20 -6 3 13 2170.04 112.415 37 -6 3 -13 2011.76 107.531 26 -6 -3 13 1905.66 101.985 20 -6 3 13 2071.01 110.766 24 -6 -3 -13 2077.13 109.192 33 -6 3 14 1967.46 108.672 37 -6 3 -14 1965.73 104.982 26 -6 -3 14 1791.48 98.6025 20 -6 3 14 2014.77 109.322 24 -6 3 14 1772.9 101.732 34 -6 -3 -14 1875.99 104.933 33 -6 3 -15 1001.02 70.02 26 -6 -3 15 943.359 65.4587 20 -6 3 15 824.372 69.4708 24 -6 3 15 908.842 68.7393 34 -6 -3 -15 928.608 72.0066 33 -6 3 -16 167.421 36.5273 26 -6 3 16 193.046 38.0486 24 -6 -3 -16 217.176 38.4314 33 -6 3 16 199.825 38.3545 37 -6 3 16 233.048 37.4685 34 -6 3 17 611.949 58.9511 37 -6 3 -17 536.342 53.4838 26 -6 3 17 578.1 57.7216 24 -6 3 17 634.804 55.1431 34 -6 -3 -17 691.602 61.8031 33 -6 3 -18 259.605 39.5721 26 -6 3 18 247.63 38.8861 24 -6 -3 -18 262.092 42.0752 33 -6 3 18 225.909 36.1089 34 -6 3 18 227.163 37.9403 37 -6 3 -19 -6.03024 22.3079 26 -6 -3 -19 6.70538 24.8055 33 -6 3 19 13.2907 25.9629 37 -6 3 19 -13.2191 25.374 24 -6 -3 -20 6.33242 24.744 33 -6 3 20 18.6711 23.466 37 -6 3 20 12.3138 21.4264 24 -6 3 21 -11.2905 23.5304 37 -6 3 21 -11.0805 19.2803 24 -6 3 22 39.3657 20.8459 37 -6 -3 22 31.7077 21.3264 37 -6 3 22 28.6904 18.3905 24 6 -3 -23 43.9755 20.1907 33 -6 3 23 4.08836 17.5623 37 6 -3 -24 375.064 33.9699 33 -6 3 24 423.698 34.1579 37 -6 4 0 708.873 51.7995 2 -6 4 0 730.532 51.133 8 -6 4 0 806.892 54.4975 11 -6 4 -1 4.51229 19.3675 2 -6 4 1 -4.46865 17.459 2 -6 4 1 -4.49082 18.7165 11 -6 4 -1 9.06482 18.6015 11 -6 4 1 -8.36845 17.701 8 -6 4 -1 -12.6599 19.3634 8 -6 4 -2 2263.2 107.212 2 -6 4 2 2116.22 105.597 2 -6 4 -2 2161.61 107.267 11 -6 4 2 2239.33 104.906 8 -6 4 -2 2132.24 104.331 8 -6 4 2 2298.24 107.425 11 -6 4 -3 830.159 56.4853 2 -6 4 3 749.778 54.184 2 -6 4 3 869.199 55.6811 8 -6 4 -3 872.83 56.2582 8 -6 4 3 834.74 55.9445 11 -6 4 -3 718.365 53.7252 11 6 4 3 863.97 55.3471 23 -6 4 -4 605.499 48.3075 2 -6 4 4 768.182 51.6015 2 -6 4 4 586.015 46.0627 8 -6 4 -4 775.821 50.2321 8 -6 4 4 562.417 46.8435 11 -6 4 -4 724.859 51.7947 11 6 4 -4 608.408 45.5666 21 6 4 4 661.071 48.543 23 -6 4 -5 186.176 28.5639 2 -6 4 5 120.711 25.0757 2 6 4 5 130.869 26.1337 23 -6 -4 5 163.977 22.2438 20 6 4 -5 157.739 25.1357 21 -6 4 5 159.403 24.9376 8 -6 4 -5 186.459 27.5953 8 -6 4 5 180.279 26.9087 11 6 4 6 9.46305 18.4858 23 -6 -4 6 10.8418 12.2981 20 6 4 -6 -8.83942 16.9673 21 6 4 7 69.6288 21.1565 23 -6 -4 7 81.7478 19.075 20 6 4 -7 111.001 24.5288 21 -6 4 7 22.8695 18.3106 24 6 4 8 83.7307 23.8272 23 -6 -4 8 62.7289 17.8477 20 -6 4 8 68.6605 20.8808 24 -6 4 9 388.365 39.2246 34 -6 4 9 395.989 42.4739 37 6 4 9 455.346 41.7474 41 6 4 -9 342.164 35.7025 42 -6 4 -9 370.111 38.6632 26 6 4 9 330.222 39.0067 23 -6 -4 9 336.26 35.2159 20 -6 4 9 309.549 38.1361 24 -6 4 10 41.2358 21.8168 37 -6 4 10 21.7048 18.9083 34 6 4 10 32.363 20.7328 41 -6 4 -10 44.2402 20.873 26 6 4 -10 5.14069 17.9165 27 -6 4 10 27.9904 20.3335 24 -6 -4 10 47.8176 18.0562 20 6 -4 10 31.5541 18.7204 20 -6 4 11 74.4395 23.4424 37 -6 4 11 28.6754 21.279 34 6 4 11 33.6489 19.154 41 -6 4 -11 29.2224 20.8369 26 6 4 -11 37.4908 20.2566 27 -6 -4 11 76.2291 21.5606 20 -6 4 11 89.2134 25.9413 24 6 -4 11 43.7953 19.1177 20 -6 4 12 97.4105 29.2062 37 -6 4 12 240.951 35.4124 34 6 4 12 150.94 30.3095 41 -6 -4 12 192.775 30.6149 20 -6 4 12 163.295 33.0238 24 6 -4 12 140.855 27.3892 20 -6 4 -12 171.966 30.0875 26 6 4 -12 205.441 30.6663 27 -6 4 13 13.4904 24.4785 37 -6 4 13 31.3645 25.3488 34 6 -4 13 34.4145 20.8186 20 -6 4 13 6.5774 23.8701 24 -6 -4 13 11.2195 17.2818 20 -6 4 -13 44.8146 26.2841 26 6 4 -13 17.1267 21.9279 27 -6 4 14 527.006 55.0419 37 -6 4 14 452.086 51.1862 34 -6 4 14 463.272 52.0956 24 6 4 -14 446.938 47.3213 27 -6 4 -14 561.184 53.2964 26 -6 4 15 235.765 37.8799 34 -6 4 15 160.069 37.1951 24 -6 4 -15 208.245 36.9347 26 -6 4 16 45.6468 25.6004 34 -6 4 16 105.471 30.2839 37 -6 4 16 76.8718 27.883 24 -6 4 -16 80.5836 32.046 26 -6 4 17 -20.6469 28.2491 37 -6 4 17 57.1297 26.0556 34 -6 4 17 34.3444 28.1941 24 -6 4 -17 19.7147 24.3149 26 -6 4 18 -6.58911 26.1875 37 -6 4 18 -6.01143 22.2432 34 -6 4 18 -46.1277 25.7496 24 -6 4 -18 25.0952 26.1513 26 -6 4 19 71.7116 25.8592 34 -6 4 19 110.551 31.6975 37 -6 4 19 123.108 30.8112 24 -6 4 -19 116.343 29.1403 26 -6 4 20 -5.55408 23.4972 37 -6 4 20 4.8756 17.6883 34 -6 4 20 16.7295 19.4046 24 -6 4 -20 20.8625 20.3789 26 -6 4 21 150.251 28.4828 37 -6 4 -21 148.167 25.8639 26 -6 4 21 214.617 30.3545 24 -6 4 -22 43.9519 17.3101 26 6 -4 -22 72.8512 21.6485 33 -6 4 22 44.5159 19.9902 37 6 -4 -23 -6.37874 13.2932 33 -6 4 23 15.8428 14.1716 37 -6 -4 -23 5.96558 14.1913 44 -6 5 0 1689.73 102.716 2 6 5 0 2168.49 103.708 45 -6 5 0 1966.91 103.875 39 6 5 0 2117.78 104.141 41 -6 5 0 2084.48 97.9113 13 -6 5 0 1936.1 104.5 17 -6 5 0 1925.31 95.8057 35 6 5 0 1912.53 100.732 29 -6 5 0 2086.32 101.645 30 -6 5 0 1977.8 103.681 8 -6 5 0 2097.57 108.361 11 -6 5 -1 58.7688 23.7589 2 -6 5 1 5.82118 20.7124 2 6 5 1 63.38 21.8256 45 -6 5 1 16.2192 19.2399 39 6 5 -1 20.0696 20.6144 41 -6 5 1 37.1625 22.8071 40 6 5 1 40.635 19.5237 41 -6 5 1 33.4428 18.9918 17 -6 5 -1 22.486 18.7146 17 -6 5 1 63.7528 18.7813 13 -6 5 -1 38.1885 17.9763 13 -6 5 -1 29.2217 16.3384 35 -6 5 1 8.21858 15.5216 35 -6 5 1 61.7015 21.526 30 6 5 -1 14.8604 17.6324 29 6 5 1 10.0594 17.9028 29 -6 5 -1 9.65342 17.1825 30 -6 5 1 46.4052 23.8258 11 -6 5 -1 5.41394 19.2667 8 -6 5 -1 35.1369 24.7925 11 -6 5 1 32.2091 19.4972 8 -6 5 2 231.157 33.8244 11 -6 5 -2 329.682 40.0443 11 -6 5 2 283.652 36.202 8 -6 5 -2 261.166 34.1259 8 -6 5 -2 224.559 35.0575 2 -6 5 2 226.218 34.7145 2 6 5 2 333.026 35.0087 45 -6 5 2 291.12 36.4491 39 6 5 2 277.932 34.7112 41 -6 5 2 232.21 35.0041 40 -6 5 2 294.496 37.2759 17 -6 5 -2 344.61 39.3812 17 -6 5 2 285.217 31.0957 13 -6 5 -2 297.026 33.0751 13 -6 5 -2 337.303 34.6827 35 -6 5 2 273.911 30.5604 35 -6 5 -2 288.207 33.4561 30 6 5 -2 282.35 35.3805 29 6 5 2 209.26 31.0956 29 -6 5 2 279.245 36.1151 28 -6 5 2 293.132 33.5379 30 6 5 2 322.381 36.6773 23 -6 5 -3 -5.91765 21.8913 11 -6 5 3 11.52 22.5039 11 -6 5 3 5.3068 16.7821 8 -6 5 -3 5.4337 18.0651 8 -6 5 -3 5.94116 19.2762 2 6 5 3 -19.6875 18.5544 45 -6 5 3 -10.767 20.2946 39 -6 5 3 5.49228 21.0847 40 6 5 3 5.24971 17.0328 41 -6 5 3 11.085 19.6991 17 -6 5 -3 -5.6755 20.1718 17 -6 5 3 17.0385 15.7577 13 -6 5 -3 -12.7195 16.2766 13 -6 5 -3 -8.52862 16.0756 35 -6 5 3 16.2704 16.6935 35 -6 5 3 10.9989 20.7318 31 6 5 -3 -9.96679 17.712 29 6 5 3 -5.19916 19.5997 29 -6 5 -3 -4.97655 16.5453 30 -6 5 3 9.46909 17.1745 30 -6 5 3 -11.5093 20.0224 28 6 5 3 10.068 17.5152 23 -6 5 4 218.233 32.7271 11 -6 5 -4 249.467 36.9495 11 -6 5 4 174.754 28.5373 8 -6 5 -4 130.887 27.975 8 6 5 4 282.522 33.4678 45 6 5 4 220.022 31.8893 41 -6 5 4 190.09 31.3788 40 -6 5 4 193.535 31.3092 17 -6 5 -4 199.336 32.9892 17 -6 5 4 281.427 30.764 13 -6 5 -4 178.05 26.8038 13 -6 5 -4 207.321 27.0957 35 -6 5 4 233.545 33.7616 31 6 5 -4 131.221 28.004 29 6 5 4 255.366 32.5556 29 -6 5 4 189.847 31.4906 28 -6 5 4 199.223 28.159 30 -6 5 -4 197.731 28.8368 30 6 5 4 192.74 29.8248 23 -6 5 5 5.72105 22.3517 11 -6 5 -5 -5.9484 21.5778 11 -6 5 5 -5.25238 18.275 8 -6 5 -5 -5.43131 18.0572 8 6 5 5 4.98864 18.0963 45 -6 5 5 -11.3688 21.4291 40 6 5 5 38.5157 21.4969 41 6 5 -5 5.14303 19.744 29 -6 5 -5 -5.16168 19.8156 30 -6 5 5 6.117 22.1893 28 6 5 5 5.40459 20.7481 23 -6 5 -5 -4.37293 16.7876 35 -6 5 5 -11.7873 21.8026 31 6 5 -6 395.164 41.2534 42 -6 5 6 426.937 44.5328 40 6 5 6 469.259 46.7278 41 6 5 -6 537.334 46.3421 29 -6 5 6 485.311 48.5847 28 -6 5 -6 527.954 46.5897 30 6 5 6 449.287 46.0935 23 -6 5 -6 474.447 40.8219 35 -6 5 6 450.642 47.9399 31 6 5 7 325.7 39.5041 41 6 5 -7 314.662 37.2596 42 -6 5 7 392.757 42.5785 37 -6 5 7 368.689 42.5729 40 -6 5 -7 426.721 42.3936 30 -6 5 7 278.946 40.1986 28 6 5 -7 493.113 46.177 29 6 5 7 373.451 43.912 23 -6 5 7 383.173 43.5725 31 6 5 8 125.638 28.4573 41 6 5 -8 138.189 26.607 42 -6 5 8 180.304 33.1196 37 -6 5 8 118.39 27.5006 40 -6 5 -8 132.134 28.8482 30 6 5 -8 78.5427 24.1206 27 -6 5 8 146.583 32.3523 28 6 5 8 145.542 31.0969 23 6 -5 8 119.552 26.4745 20 -6 5 8 129.272 30.3336 31 6 5 9 159.487 32.2661 41 6 5 -9 167.683 27.9747 42 -6 5 -9 127.86 29.739 26 6 5 -9 144.907 31.3998 27 -6 5 9 170.5 36.4495 28 -6 -5 9 193.673 29.1785 20 6 -5 9 170.969 31.3422 20 -6 5 9 200.687 35.2744 37 -6 5 9 178.934 35.1158 31 -6 5 9 144.354 29.5531 34 6 5 10 43.9686 23.8021 41 6 5 -10 58.8519 24.9714 42 -6 5 -10 115.637 29.0552 26 -6 5 10 34.7357 24.2923 28 6 5 -10 113.292 28.7967 27 -6 -5 10 112.758 24.7557 20 6 -5 10 30.3746 22.6029 20 -6 5 10 67.0727 28.8897 37 -6 5 10 81.1256 27.8504 31 -6 5 10 102.504 30.0875 34 6 5 11 185.246 35.4931 41 6 5 -11 310.946 38.7803 42 6 5 -11 274.533 39.092 27 -6 5 -11 202.557 36.0793 26 -6 5 11 267.126 41.1234 28 6 -5 11 251.953 36.4795 20 -6 5 11 289.327 39.7208 24 -6 -5 11 269.01 36.3101 20 -6 5 11 306.497 40.0306 34 -6 5 11 269.231 41.6419 37 -6 5 11 287.662 40.7277 31 6 5 12 25.8443 24.3593 41 6 5 -12 30.976 24.6203 27 -6 5 -12 -6.52628 26.7862 26 -6 5 12 7.04967 21.7017 28 -6 5 12 26.0058 23.5864 24 -6 5 12 -6.42751 22.8471 34 -6 5 12 -7.04273 25.0335 37 -6 5 12 27.4854 24.4245 31 6 5 13 154.996 33.7199 41 6 5 -13 279.824 40.1015 27 -6 5 -13 212.941 38.207 26 -6 5 13 195.654 37.0411 28 -6 5 13 245.783 39.3421 24 -6 5 13 305.728 43.5576 37 -6 5 13 279.069 39.3554 31 -6 5 13 228.483 38.399 34 6 5 14 89.2199 26.2284 41 -6 5 14 34.117 24.3315 28 6 5 -14 43.0854 24.5376 27 -6 5 -14 80.281 27.5268 26 -6 5 14 40.1521 24.8341 24 -6 5 14 46.4342 25.0842 31 -6 5 14 70.8525 30.0376 37 -6 5 14 52.2902 26.476 34 6 5 -14 83.4995 27.2429 32 6 5 15 6.18856 20.5861 41 6 5 -15 29.9352 22.5803 27 -6 5 -15 6.61357 24.4753 26 -6 5 15 19.8736 25.4405 24 6 5 -15 37.4285 23.9576 32 -6 5 15 41.6827 28.9613 37 -6 5 15 12.8656 25.5713 34 6 5 16 135.29 30.8051 41 -6 5 -16 89.7172 29.7453 26 -6 5 16 135.141 30.2301 24 6 5 -16 112.447 28.1861 32 -6 5 16 124.076 32.7651 34 6 5 17 169.63 30.8335 41 -6 5 17 214.059 36.9698 37 -6 5 -17 224.563 37.5444 26 -6 5 17 299.371 40.7855 24 6 5 -17 147.501 31.0401 32 -6 5 17 303.766 39.0543 34 -6 5 18 23.1381 24.8668 37 -6 5 -18 44.7961 24.4144 26 -6 5 18 50.9077 22.1431 24 -6 5 18 42.8166 23.0139 34 -6 5 19 25.8316 22.4897 37 -6 5 19 -5.08782 18.0841 24 -6 5 -19 -20.0439 20.8848 26 -6 5 -20 147.074 25.0801 26 -6 5 20 107.026 24.5873 37 -6 5 -21 121.012 21.6129 26 -6 5 21 100.572 19.0457 41 6 5 -22 157.744 20.462 26 -6 5 22 117.054 16.9729 41 -6 6 0 2810.23 140.87 40 -6 6 0 3033.98 145.996 39 -6 6 0 3047.81 136.244 13 -6 6 0 2804.48 143.477 17 6 6 0 3032 146.18 18 -6 6 0 2646.66 130.725 35 6 6 0 2780.7 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812.716 62.2087 30 -6 6 2 831.594 68.4866 28 -6 6 2 879.033 63.5056 30 6 6 -2 1015.76 67.7174 29 6 6 2 806.777 63.7113 29 -6 6 2 776.45 62.7902 8 -6 6 -2 770.193 64.3338 8 6 6 3 339.642 40.1697 45 -6 6 3 313.812 40.9693 39 -6 6 -3 329.53 42.0873 39 -6 6 3 300.988 41.2757 40 6 6 -3 380.834 42.7201 43 6 6 3 282.889 40.7681 41 -6 6 3 297.291 37.1628 13 -6 6 -3 312.373 36.1885 13 6 6 -3 258.347 40.0695 18 6 6 3 233.707 36.0724 18 -6 6 3 320.463 41.5144 17 -6 6 -3 287.329 40.4117 17 -6 6 -3 348.238 37.8679 35 -6 6 3 274.228 39.8066 31 -6 6 3 232.789 32.3975 35 6 6 3 221.168 37.1685 36 6 6 -3 203.228 35.5796 29 6 6 3 174.867 33.5882 29 -6 6 3 210.676 32.6812 30 -6 6 3 276.24 40.7757 28 -6 6 -3 236.983 34.7586 30 -6 6 -3 228.661 36.2876 8 -6 6 3 223.157 34.2409 8 6 6 4 -5.96124 21.6259 45 -6 6 4 6.50097 24.0506 39 6 6 -4 16.779 20.2902 42 -6 6 -4 -6.75362 23.4997 39 -6 6 4 -6.61482 23.5118 40 6 6 -4 -6.22117 21.6473 43 6 6 4 19.1264 25.7543 41 -6 6 4 -5.09032 18.0939 13 -6 6 -4 20.3395 19.8679 13 6 6 -4 26.3138 26.5743 18 6 6 4 12.8336 22.8081 18 -6 6 4 -6.61169 26.7085 17 -6 6 -4 6.81621 24.727 17 6 6 4 -6.79823 25.6292 36 -6 6 -4 -15.4033 20.0615 35 -6 6 4 39.2127 19.4792 35 -6 6 4 53.7064 27.1189 31 6 6 4 6.33412 22.5142 29 6 6 -4 6.0038 22.6346 29 -6 6 4 16.5188 18.7391 30 -6 6 4 7.04438 23.4215 28 -6 6 -4 30.0285 22.6417 30 -6 6 4 18.9614 18.9082 8 -6 6 -4 19.547 21.1418 8 6 6 -5 278.669 36.9176 43 -6 6 -5 257.277 40.7858 39 -6 6 5 232.95 38.3414 40 6 6 -5 361.05 39.3088 42 6 6 5 194.055 35.5011 41 6 6 5 290.886 40.0943 18 -6 6 5 261.498 34.4846 13 -6 6 5 234.863 37.6195 17 -6 6 -5 249.95 37.9503 17 6 6 5 192.526 36.2673 36 -6 6 5 171.924 38.276 31 -6 6 -5 287.535 35.5591 35 6 6 5 186.419 34.0379 29 6 6 -5 272.243 37.1628 29 -6 6 5 301.148 42.7784 28 -6 6 -5 231.376 35.5165 30 6 6 5 273.83 37.6032 45 6 6 6 605.151 54.6027 45 6 6 -6 633.112 55.5716 43 -6 6 -6 584.484 49.212 35 -6 6 6 645.611 60.0463 31 6 6 6 623.486 58.7306 36 -6 6 6 739.363 60.3543 40 -6 6 -6 575.09 55.1853 39 6 6 -6 603.253 52.8757 42 6 6 6 570.765 54.8015 41 6 6 6 619.389 56.3291 29 -6 6 -6 696.852 56.9706 30 -6 6 6 698.64 64.4271 28 6 6 -6 555.78 51.0399 27 6 6 -6 696.623 57.0426 29 6 6 6 574.504 53.4192 23 -6 6 7 246.084 40.331 40 6 6 -7 252.716 36.2878 42 6 6 7 252.448 39.4127 41 6 6 -7 183.427 33.6035 27 6 6 7 257.498 39.4724 29 -6 6 -7 248.494 36.6932 30 -6 6 7 257.54 42.1493 28 6 6 7 241.193 38.092 45 -6 6 -7 321.134 36.21 35 -6 6 7 220.995 38.1787 31 6 6 7 187.584 36.5641 36 6 6 8 83.1152 28.4802 36 -6 6 8 57.6234 29.6135 31 6 6 -8 34.654 23.0185 42 -6 6 8 66.0233 26.2949 40 6 6 8 40.1967 29.6173 41 6 6 -8 43.6432 26.4339 27 -6 6 -8 87.2743 27.9352 30 6 6 8 53.3336 23.7603 29 -6 6 8 14.8052 26.3693 28 6 6 9 20.5545 24.8686 36 -6 6 9 7.22907 26.7565 31 6 6 -9 28.9566 22.2493 42 -6 6 9 19.4676 26.2265 40 6 6 9 33.5895 24.8665 41 -6 6 -9 43.6675 22.1885 30 6 6 -9 6.32489 24.2962 27 -6 6 9 36.9996 26.3148 28 6 6 9 26.8089 26.1992 29 -6 6 10 115.112 34.3649 31 -6 6 10 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21.924 21 7 3 7 304.027 32.9176 23 -7 -3 7 287.631 28.6262 20 7 3 -7 282.649 32.0345 21 -7 3 7 316.788 34.6309 24 7 3 8 -4.58852 19.9741 23 -7 -3 8 11.3369 13.7087 20 -7 3 8 13.5791 17.3771 24 7 3 -8 -4.58185 18.2074 21 7 3 9 1902.01 97.0652 23 -7 -3 9 1970.45 93.4297 20 7 3 -9 1648.59 93.4204 21 -7 3 9 1967.22 98.2067 24 7 3 10 538.283 47.1658 23 -7 3 10 484.012 46.5775 24 -7 -3 10 595.317 44.6786 20 -7 3 -10 444.057 42.9315 26 -7 3 11 365.911 42.265 37 -7 -3 11 350.558 35.7666 20 -7 3 -11 305.298 37.8919 26 -7 3 12 2547.91 128.687 37 -7 -3 12 2721.75 124.411 20 -7 3 12 2630.3 130.274 24 -7 3 -12 2486.04 126.249 26 -7 -3 -13 186.374 34.5154 33 -7 3 13 292.961 40.0327 37 -7 3 -13 297.546 37.3132 26 -7 -3 13 232.645 31.5577 20 -7 3 13 238.171 39.2033 24 -7 3 14 2638.67 135.352 34 -7 -3 -14 2808.48 138.929 33 -7 3 14 2689.84 138.38 37 -7 3 -14 2652.89 135.464 26 -7 -3 14 2989.24 135.199 20 -7 3 14 2904.65 142.407 24 -7 3 15 524.338 52.3971 34 -7 -3 -15 630.42 57.0811 33 -7 3 15 752.318 62.1435 37 -7 3 -15 618.86 56.5488 26 -7 3 15 776.153 63.5528 24 -7 3 16 1284.4 83.4648 34 -7 -3 -16 1433.89 89.4509 33 -7 3 16 1358.48 88.2149 37 -7 3 -16 1208.53 82.5718 26 -7 3 16 1207.43 86.1139 24 -7 3 -17 51.3461 27.9501 26 -7 3 17 -13.8863 28.5063 24 -7 -3 -17 27.5818 29.6068 33 -7 3 17 62.5053 28.514 37 -7 3 17 44.2893 23.8652 34 -7 3 -18 124.369 32.6847 26 -7 3 18 40.6768 27.5653 24 -7 -3 -18 74.914 33.6583 33 -7 3 18 115.973 33.3497 37 -7 3 18 121.943 28.8396 34 -7 3 -19 29.2573 22.8774 26 -7 -3 -19 39.3329 25.6262 33 -7 3 19 52.263 25.5379 37 -7 3 19 -6.44484 25.1942 24 -7 3 20 121.372 32.1796 37 -7 3 20 65.3251 23.3772 24 -7 3 21 70.9776 25.6775 37 -7 3 21 -10.5575 19.5368 24 -7 3 22 89.6735 24.3434 37 -7 -3 22 61.7861 22.5547 37 -7 3 23 7.7689 15.9463 37 -7 -3 23 14.2241 15.9078 37 7 -3 -24 19.059 16.4625 33 -7 3 24 -2.96275 13.2562 37 -7 -3 -24 27.5129 14.7168 44 -7 4 0 19.2505 19.7525 11 -7 4 0 -13.4484 16.5849 8 -7 4 0 -14.3863 18.411 2 -7 4 -1 280.693 34.1196 11 -7 4 1 263.451 31.1667 8 -7 4 -1 279.445 32.1085 8 -7 4 1 239.638 31.5942 11 -7 4 -1 250.876 32.5488 2 -7 4 1 267.328 32.9676 2 -7 4 2 2185.13 105.441 8 -7 4 -2 2202.49 105.718 8 -7 4 2 1926.51 104.379 11 -7 4 -2 2362.76 110.022 11 -7 4 -2 2099.21 107.06 2 -7 4 2 2341.83 108.801 2 7 4 3 345.361 35.2105 23 -7 4 3 363.328 37.1354 11 -7 4 -3 299.626 36.5294 11 -7 4 3 360.934 35.7434 8 -7 4 -3 269.825 32.9505 8 -7 4 -3 362.692 38.3177 2 -7 4 3 356.795 37.2916 2 7 4 4 5178.95 209.796 23 -7 4 4 5389.52 210.298 8 -7 4 -4 4990.68 208.629 8 -7 4 4 5335.06 212.395 11 -7 4 -4 4952.16 211.089 11 -7 4 -4 5105.88 211.751 2 -7 4 4 5236.42 211.737 2 7 4 -5 4468.8 189.087 21 7 4 5 4596.73 191.088 23 -7 4 5 4804.9 189.395 8 -7 4 -5 4322.31 187.586 8 -7 4 5 4549.58 190.107 11 -7 4 -5 4616.36 192.081 2 -7 4 5 4548.11 189.903 2 7 4 6 206.174 32.5811 23 -7 -4 6 229.264 26.7678 20 7 4 -6 270.363 32.5121 21 -7 4 6 236.677 30.2289 24 7 4 7 1572.05 86.0872 23 7 4 -7 1311.5 80.2948 21 -7 -4 7 1497.37 77.5682 20 -7 4 7 1450.28 81.6567 24 -7 4 8 103.285 24.617 24 7 4 8 126.555 28.5168 23 -7 -4 8 149.333 24.3964 20 7 4 -8 89.3602 24.4572 21 -7 4 -8 134.031 27.0144 26 -7 4 9 -5.68401 20.2026 37 7 4 9 63.2789 26.064 23 -7 -4 9 18.7458 15.206 20 7 4 -9 -5.51204 20.7798 21 -7 4 9 -16.4839 22.5507 24 -7 4 -9 10.8984 19.3681 26 -7 4 10 -17.9845 22.1779 37 -7 4 10 5.59983 19.9041 34 -7 4 10 -5.82572 22.3658 24 -7 -4 10 24.894 18.4195 20 7 4 -10 10.6 18.8385 27 -7 4 -10 11.4935 21.6651 26 -7 4 11 542.418 51.1357 34 -7 4 11 535.335 53.3264 37 -7 4 11 689.557 58.2558 24 -7 -4 11 618.456 50.7701 20 7 -4 11 507.248 47.8574 20 7 4 -11 707.401 54.453 27 -7 4 -11 591.481 52.1632 26 -7 4 12 92.0105 28.6749 37 -7 4 12 49.3073 25.7609 34 -7 -4 12 49.8916 20.9886 20 -7 4 12 109.774 31.136 24 7 -4 12 52.0648 21.8951 20 7 4 -12 56.415 24.2921 27 -7 4 -12 25.1993 25.1094 26 -7 4 13 6.79832 23.139 37 -7 4 13 19.1518 25.3725 34 7 -4 13 11.6441 17.9271 20 -7 -4 13 17.3505 19.2343 20 -7 4 13 6.71311 27.1213 24 7 4 -13 23.0105 22.4803 27 -7 4 -13 19.5582 27.175 26 -7 4 14 48.6772 26.7113 37 -7 4 14 45.7291 23.2365 34 -7 4 14 6.89931 23.4953 24 -7 4 -14 13.3399 22.7154 26 -7 4 15 85.5806 29.5941 34 -7 4 15 154.5 36.1517 37 -7 4 -15 73.9886 29.8345 26 -7 4 15 62.8223 29.2458 24 -7 4 16 618.021 55.8766 34 -7 4 16 745.158 64.5973 37 -7 4 -16 606.129 59.2209 26 -7 4 16 618.223 59.1069 24 -7 4 17 942.13 71.0509 34 -7 4 17 995.818 74.4586 37 -7 4 17 1028.13 74.3686 24 -7 4 -17 1000.3 72.8753 26 -7 4 18 83.6047 33.1222 37 -7 4 18 82.633 25.8599 34 -7 4 18 109.294 28.523 24 -7 4 -18 73.1555 26.6988 26 -7 4 19 107.378 25.2653 34 -7 4 19 124.917 31.6759 37 -7 4 19 95.1148 27.2344 24 -7 4 -19 167.701 32.442 26 -7 4 20 16.0113 21.5587 37 -7 4 20 -4.69937 18.3601 34 -7 4 20 -5.3254 18.529 24 -7 4 -20 4.9518 18.6673 26 -7 4 21 4.61984 20.6611 37 -7 4 -21 -8.40081 16.4107 26 -7 4 21 9.20187 15.2965 24 7 -4 -22 18.8571 17.9623 33 -7 -4 22 17.248 16.4331 37 -7 -4 -22 28.0208 15.892 44 -7 4 22 38.1802 18.806 37 7 -4 -23 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518.273 3 -8 2 3 14739.8 518.403 3 -8 2 -3 14817 518.277 5 -8 -2 -3 14823.7 518.773 5 8 2 3 15037.4 519.174 4 -8 2 3 14068 520.876 11 -8 2 -3 14140.6 521.701 11 -8 2 3 14524.2 521.408 24 -8 -2 3 14758.7 517.011 20 8 2 -3 14856.5 523.377 21 -8 -2 4 4931.51 189.338 3 -8 2 4 5006.62 188.953 3 -8 2 -4 4820.32 188.583 5 -8 -2 -4 4859.84 189.39 5 8 2 4 5065.72 190.226 4 -8 2 4 4704.26 190.701 11 -8 2 -4 4725.6 191.755 11 -8 -2 4 5010.45 188.41 20 -8 2 4 5043.24 193.065 24 8 2 -4 5139.43 194.893 21 -8 -2 5 5140.28 191.866 3 -8 2 5 4807.26 190.393 3 -8 2 -5 5042.84 191.498 5 -8 -2 -5 5033.45 192.065 5 8 2 5 4720.03 190.603 4 -8 2 5 4929.35 194.416 24 -8 -2 5 5164.29 191.232 20 8 2 -5 4995.75 195.959 21 8 2 5 4713.12 193.147 23 -8 2 -6 1635.58 77.8341 5 -8 -2 6 1659.27 78.3599 3 -8 2 6 1534.78 77.0633 3 -8 -2 -6 1586.37 77.6034 5 8 2 6 1608.17 78.0477 4 8 2 -6 1662.29 77.4833 7 8 -2 -6 1679.19 77.5969 7 -8 2 6 1527.21 79.7447 24 -8 -2 6 1642.33 77.4277 20 8 2 -6 1530.15 80.9277 21 8 2 6 1580.4 80.0569 23 -8 2 7 960.354 56.711 3 -8 -2 7 1111.33 59.042 3 8 2 7 946.878 56.6968 4 8 2 -7 965.472 56.7343 7 8 2 7 1011.62 59.2961 23 -8 -2 7 1073.45 57.668 20 -8 2 7 965.579 60.1205 24 8 2 8 280.515 29.7109 4 8 2 -8 328.995 31.314 7 -8 -2 8 332.77 31.1198 3 -8 2 8 249.143 28.2216 3 8 2 8 299.274 31.6685 23 -8 -2 8 326.47 31.0627 20 -8 2 8 240.225 31.0999 24 -8 2 9 2011.38 97.4381 3 8 2 9 2115.97 99.7436 4 8 2 -9 2081.77 98.2663 7 8 2 9 1820.85 97.0192 23 -8 2 9 2017.09 100.732 24 -8 -2 9 2272.08 99.4224 20 -8 2 10 4022.04 174.669 3 8 2 10 4165.31 176.261 4 -8 -2 10 4529.55 176.273 20 -8 2 10 4118.94 178.685 24 8 2 -10 4302.18 176.356 7 8 2 11 91.8014 23.9477 4 -8 -2 -11 74.0546 23.2044 33 -8 2 11 103.594 25.6487 24 -8 -2 11 70.6237 19.428 20 8 2 -11 95.9118 24.2754 7 -8 2 12 4258.05 178.078 37 8 2 12 3898.47 173.885 46 -8 2 -12 4076.29 174.352 26 -8 -2 12 4012.2 170.451 20 -8 2 12 3774.77 174.742 24 -8 -2 -12 4135.1 178.956 33 8 2 13 27.7894 20.5614 46 -8 2 -13 -5.44193 18.9356 26 -8 -2 -13 -6.06871 24.5148 33 -8 2 13 5.81744 21.5216 37 -8 2 13 11.7324 22.1153 24 -8 -2 13 4.97433 17.681 20 -8 -2 -14 25.7412 26.4146 33 -8 2 14 24.7468 24.5884 37 8 2 14 5.83908 19.875 46 -8 2 14 24.7091 24.551 24 -8 -2 14 5.23305 15.6604 20 -8 -2 -15 1621.25 98.5924 33 -8 2 15 1718.57 98.6049 37 8 2 15 1591.41 93.4813 46 8 -2 15 1482.4 91.2588 46 -8 2 15 1672.51 97.1594 24 8 2 16 6.23797 21.7068 46 8 -2 16 37.6963 25.7867 46 -8 -2 -16 13.99 24.8639 33 -8 2 16 26.916 25.8346 37 8 2 16 -12.888 26.4486 10 -8 2 16 6.59246 22.4359 24 8 -2 17 480.303 51.0861 46 8 2 17 585.068 53.716 46 -8 2 17 534.967 56.2369 37 -8 -2 -17 711.865 62.9731 33 8 2 -17 519.145 55.177 14 8 2 17 608.011 56.1646 10 -8 2 17 563.748 56.4752 24 8 -2 18 89.4434 29.5151 46 8 2 18 99.3995 29.4106 46 8 2 -18 120.892 38.2108 14 -8 -2 -18 120.572 33.9159 33 -8 2 18 95.7567 31.9587 37 8 2 18 103.957 29.637 10 -8 2 18 91.3174 30.1252 24 -8 2 19 1303.32 85.7093 37 8 2 19 1319.78 81.4596 46 8 -2 19 1142.92 80.1243 46 8 2 19 1225.83 80.5572 10 8 2 -19 1349.25 85.493 14 -8 2 20 -12.5572 24.9494 37 8 -2 20 -11.7253 23.6816 46 8 2 20 11.8022 19.6191 10 8 2 -20 42.9379 27.0695 14 -8 2 21 34.4224 22.0564 37 -8 -2 21 39.0524 23.9747 37 8 -2 21 42.8257 21.6564 46 8 2 -21 22.2876 24.2835 14 -8 2 22 -5.06033 20.4415 37 -8 -2 22 19.5487 20.369 37 8 -2 22 14.1141 19.005 46 8 2 -22 -4.85954 20.2538 14 -8 2 23 42.5693 20.5724 37 -8 -2 23 65.3297 21.6478 37 8 -2 23 43.4842 18.2361 46 -8 -2 -23 78.1601 21.9068 44 8 -2 -24 38.4038 18.1387 33 -8 2 24 50.4891 17.661 37 -8 -2 24 54.0836 16.0477 37 -8 -2 -24 48.3458 17.9425 44 8 -2 24 18.7125 13.8291 46 -8 3 0 11808.3 423.937 8 -8 3 0 11427.8 425.417 11 -8 3 1 2450.8 110.255 11 -8 3 1 2543.72 109.577 8 -8 3 -1 2295.19 107.498 8 -8 3 -1 2210.05 108.457 11 -8 3 2 2715.71 119.687 11 -8 3 -2 2543.07 119.026 11 -8 3 2 2718.86 118.224 8 -8 3 -2 2598.47 117.737 8 -8 3 3 5045.52 194.727 8 -8 3 3 4808.49 195.545 11 -8 3 -3 4577.19 195.197 11 -8 3 -3 4808.15 194.51 8 -8 3 3 4834.7 192.788 24 8 3 -3 5169.87 197.206 21 -8 3 -4 460.457 37.4265 8 -8 3 -4 474.841 40.9476 11 -8 3 4 398.12 35.9688 8 -8 3 4 495.182 40.0693 11 -8 3 4 418.485 37.3147 24 -8 -3 4 497.15 34.6892 20 8 3 -4 378.373 36.9362 21 -8 3 5 68.5925 18.3657 8 -8 3 -5 91.4621 21.7887 8 8 3 5 72.076 22.3748 23 8 3 -5 150.631 26.2882 21 -8 -3 5 89.1209 19.0836 20 -8 3 5 76.3959 21.2399 24 -8 -3 6 1515.6 76.3773 20 8 3 -6 1438.26 80.9332 21 -8 3 6 1607.99 81.8955 24 8 3 6 1508.66 81.8322 23 8 3 7 18.5259 20.2253 23 8 3 -7 75.5914 22.0065 21 -8 -3 7 41.9343 14.7237 20 -8 3 7 68.0297 22.3746 24 8 3 8 739.059 54.4508 23 8 3 -8 880.176 58.3114 21 -8 -3 8 731.791 50.9221 20 -8 3 8 744.016 54.8593 24 8 3 9 188.895 30.3964 23 8 3 -9 205.039 31.7068 21 -8 -3 9 284.366 31.5682 20 -8 3 9 242.039 33.8888 24 -8 3 -9 225.864 30.7911 26 -8 3 10 978.451 66.8037 37 8 3 10 1033.86 68.0155 23 -8 3 10 1129.04 70.9956 24 -8 -3 10 998.812 63.6319 20 8 3 -10 936.214 66.9653 21 -8 3 -10 1039.79 67.3074 26 -8 3 11 1473.21 90.3472 37 -8 -3 11 1607.96 87.3584 20 8 3 -11 1745.69 95.8199 21 -8 3 11 1838.59 96.3178 24 -8 3 -11 1437.47 88.7417 26 -8 3 12 108.533 29.1269 37 -8 3 -12 193.742 33.9169 26 -8 3 12 233.655 35.7665 24 8 3 -12 131.685 29.5653 21 -8 -3 12 125.791 26.2805 20 -8 -3 -13 8968.44 348.404 33 -8 3 13 8640.12 346.88 37 -8 3 13 9196.54 350.331 24 -8 -3 13 9236.01 342.997 20 8 3 -13 8410.39 348.112 21 -8 3 -13 8575.19 344.705 26 -8 -3 -14 84.4252 30.5805 33 -8 3 14 59.6061 25.0234 37 -8 3 -14 88.4751 27.9393 26 -8 3 14 -13.4175 28.8436 24 -8 -3 14 45.7946 21.6448 20 8 3 -14 96.8733 28.4475 21 -8 3 15 4142.06 188.417 34 -8 -3 -15 4099.82 189.73 33 -8 3 15 4333.05 191.971 37 -8 3 15 4096.6 190.886 24 -8 3 -15 4230.95 188.52 26 -8 -3 -16 527.204 54.875 33 -8 3 16 535.526 52.5044 34 -8 3 16 601.51 56.9199 37 -8 3 -16 542.179 53.1439 26 -8 3 16 548.778 56.4895 24 -8 3 17 588.565 53.7149 34 -8 3 17 660.744 59.9106 37 -8 3 -17 519.451 52.1643 26 -8 3 17 611.79 57.2954 24 -8 3 -18 412.124 45.4749 26 -8 3 18 404.869 46.9683 24 -8 3 18 435.51 49.5649 37 -8 3 18 471.294 47.8257 34 -8 3 19 74.7894 26.0096 24 -8 3 19 16.7346 19.8717 34 -8 3 19 44.4319 26.4881 37 -8 3 20 50.9895 22.9391 24 -8 3 20 40.8725 25.1105 37 -8 3 21 54.5859 21.3567 24 -8 3 21 36.3724 23.2911 37 -8 3 22 97.737 23.231 37 -8 -3 22 88.5341 21.855 37 -8 -3 -23 220.121 26.8673 44 -8 -3 23 266.111 27.692 37 8 -3 -24 650.279 40.6476 33 -8 -3 -24 626.342 39.0017 44 -8 3 24 612.283 38.8375 37 -8 4 0 2882.38 132.574 11 -8 4 0 2918.64 130.931 8 -8 4 0 2667.61 130.637 2 -8 4 1 1450.41 80.9945 8 -8 4 -1 1547.38 82.7889 8 -8 4 1 1519.36 83.5817 11 -8 4 -1 1363.73 81.9233 11 -8 4 -1 1435.5 82.6664 2 -8 4 1 1414.14 82.5676 2 -8 4 2 301.845 34.823 11 -8 4 -2 260.913 35.2691 11 -8 4 2 205.186 29.563 8 -8 4 -2 326.071 37.309 8 -8 4 -2 250.517 32.745 2 -8 4 2 311.369 36.4821 2 8 4 3 948.544 61.0278 23 -8 4 3 884.712 61.1313 11 -8 4 -3 820.723 60.9355 11 -8 4 3 891.943 59.8642 8 -8 4 -3 902.732 60.4206 8 -8 4 -3 893.778 61.9702 2 -8 4 3 865.804 60.829 2 8 4 4 214.327 32.7311 23 -8 4 4 255.338 35.0792 11 -8 4 -4 306.871 36.6697 11 -8 4 4 271.867 32.7315 8 -8 4 -4 231.975 31.634 8 -8 4 -4 264.732 33.9801 2 -8 4 4 289.813 34.1478 2 8 4 5 371.182 38.7485 23 8 4 -5 336.65 37.1083 21 -8 4 5 352.292 38.4116 11 -8 4 -5 398.763 40.5873 11 -8 4 5 324.051 35.9449 8 -8 4 -5 347.292 37.0855 8 -8 4 -5 431.407 42.7982 2 -8 4 5 315.018 35.6699 2 -8 4 -6 769.523 59.5683 38 8 4 6 940.973 62.9037 23 -8 -4 6 931.361 55.9313 20 -8 4 6 884.366 59.8649 24 8 4 -6 761.979 57.6802 21 -8 4 -6 778.408 57.2046 26 -8 4 -7 1803.98 103.669 38 -8 4 -7 2071.19 105.565 26 8 4 -7 2173.77 104.795 29 8 4 7 2151.15 108.331 23 -8 4 7 1971.17 104.504 24 -8 -4 7 2061.95 99.7901 20 8 4 -7 2052.3 106.934 21 -8 4 -8 16.2675 18.5075 26 8 4 8 28.9122 23.0222 23 -8 -4 8 78.8573 20.2426 20 8 4 -8 33.9651 21.7788 21 -8 4 8 59.957 24.4185 24 -8 4 -9 1196.5 77.459 26 8 4 9 1213.33 79.7963 23 -8 -4 9 1360.19 76.1442 20 -8 4 9 1278.9 80.1525 24 8 4 -9 1292.98 79.7574 21 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35 -8 5 -1 945.391 63.2288 30 -8 5 1 858.736 60.3904 30 8 5 -1 903.281 62.7984 29 8 5 1 924.323 63.7659 29 -8 5 1 786.609 61.7313 8 -8 5 -1 902.771 65.0515 8 -8 5 1 868.855 67.7695 11 -8 5 -1 871.473 67.6979 11 -8 5 -2 651.062 57.6683 2 -8 5 2 681.333 58.6807 2 8 5 2 766.55 59.0898 23 -8 5 2 711.539 57.2873 39 -8 5 2 719.779 58.8257 40 8 5 2 685.42 57.1195 41 -8 5 2 888.061 57.4212 13 -8 5 -2 772.991 53.865 13 -8 5 -2 802.583 54.4064 35 -8 5 2 798.212 53.6698 35 -8 5 2 759.434 56.9368 30 -8 5 -2 852.569 58.7106 30 8 5 -2 810.751 58.29 29 8 5 2 710.42 56.6699 29 -8 5 2 705.703 56.9986 8 -8 5 -2 779.912 60.4867 8 -8 5 2 737.074 60.6216 11 -8 5 -2 791.06 62.7097 11 -8 5 -3 148.877 32.3675 2 -8 5 3 250.978 37.4454 2 8 5 3 165.979 30.5712 23 8 5 3 223.577 34.2557 41 -8 5 3 186.029 29.192 13 -8 5 -3 217.173 29.5911 13 -8 5 -3 297.764 34.065 35 8 5 -3 299.686 37.7756 29 8 5 3 235.355 33.1139 29 -8 5 3 252.828 34.1333 30 -8 5 -3 234.879 32.5603 30 -8 5 3 292.887 39.3018 28 -8 5 3 212.448 32.6103 8 -8 5 -3 182.013 32.5998 8 -8 5 3 202.174 34.1874 11 -8 5 -3 182.135 35.7794 11 -8 5 -4 222.459 36.9796 2 -8 5 4 220.17 35.9089 2 8 5 4 240.589 35.9587 23 8 5 4 255.153 37.382 41 -8 5 4 287.839 33.401 13 -8 5 -4 221.038 29.9617 13 -8 5 -4 278.7 34.6385 35 -8 5 4 280.462 42.4497 31 8 5 -4 264.569 36.9443 29 -8 5 -4 225.761 33.0867 30 8 5 4 194.259 32.7771 29 -8 5 4 239.827 36.3112 28 -8 5 4 157.664 29.4658 8 -8 5 -4 259.939 35.1267 8 -8 5 4 169.49 34.9584 11 -8 5 -4 214.881 38.8742 11 8 5 5 970.889 67.8266 23 -8 5 -5 978.286 62.7805 35 -8 5 5 725.336 63.5746 31 8 5 5 1057.11 69.6075 41 8 5 5 1068.81 69.0654 29 -8 5 -5 880.491 63.8234 30 -8 5 5 892.904 68.2117 28 8 5 -5 854.191 63.32 29 -8 5 5 927.769 68.9885 11 -8 5 -5 870.45 67.8686 11 8 5 6 2906.06 139.01 41 8 5 -6 2658.54 131.372 42 8 5 6 2612.89 135.824 29 -8 5 -6 3121.83 138.465 30 -8 5 6 2882.53 143.177 28 8 5 -6 3048.7 139.757 29 8 5 6 2922.94 140.92 23 -8 5 6 2810.42 141.279 31 8 5 -7 46.9486 21.8223 42 -8 5 7 88.6531 26.8543 40 8 5 7 53.8697 26.4815 41 8 5 7 89.3679 28.6106 23 -8 5 -7 44.2992 21.3414 30 -8 5 7 33.4499 23.8522 31 -8 5 7 55.2622 28.851 28 8 5 -8 295.676 36.2972 42 -8 5 8 299.567 39.8709 40 8 5 8 279.559 38.6592 41 -8 5 -8 344.013 40.8617 26 -8 5 8 370.112 47.074 31 8 5 8 334.118 43.8353 23 -8 5 9 2417.36 124.396 40 8 5 -9 2548.87 120.089 42 8 5 9 2193.3 119.085 41 8 5 -9 2202.97 119.345 27 -8 5 -9 2452.94 123.477 26 8 5 9 2193.68 123.162 23 -8 5 9 2415.38 121.384 34 -8 5 9 2361.87 127.095 31 8 5 10 68.463 28.0159 41 8 5 -10 118.12 27.9988 42 -8 5 -10 76.4095 26.7271 26 8 5 -10 142.042 30.5539 27 -8 5 10 95.0196 31.6669 24 -8 5 10 132.937 33.9053 37 -8 5 10 70.7697 27.3536 31 -8 5 10 74.126 25.9399 34 8 5 11 168.306 33.1419 41 -8 5 -11 150.157 33.0041 26 8 5 -11 205.262 35.736 27 -8 5 11 156.31 33.2647 24 -8 5 11 206.17 39.3856 31 -8 5 11 135.94 35.0198 37 -8 5 11 215.699 36.1374 34 -8 5 12 729.128 65.1212 37 8 5 -12 775.872 63.6283 27 -8 5 -12 980.989 71.2889 26 -8 5 12 868.331 68.3087 24 -8 5 12 793.068 63.581 34 -8 5 12 939.654 72.4163 31 -8 5 -13 305.778 44.4319 26 8 5 -13 464.795 46.3509 27 -8 5 13 366.436 46.5764 24 -8 5 13 380.929 45.3178 31 -8 5 13 302.469 45.0061 37 -8 5 13 433.227 46.5046 34 -8 5 -14 105.086 33.1616 26 8 5 -14 100.849 28.3966 27 -8 5 14 131.733 33.5134 28 -8 5 14 92.3589 30.8068 24 -8 5 14 87.9961 30.435 37 -8 5 14 100.077 30.3909 31 -8 5 14 51.0908 26.8008 34 8 5 -15 -22.5712 22.4254 27 -8 5 -15 82.8733 28.8847 26 -8 5 15 32.8736 23.852 28 -8 5 15 6.41852 24.1988 24 -8 5 15 18.8725 22.3614 31 -8 5 15 13.1025 23.2867 37 8 5 -15 23.9771 24.603 32 -8 5 15 -12.3852 22.9109 34 -8 5 -16 121.23 31.2818 26 -8 5 16 140.133 29.847 28 -8 5 16 67.2562 26.4628 24 8 5 -16 111.476 30.4518 32 -8 5 16 93.9921 29.1058 34 -8 5 16 80.8072 30.4427 37 -8 5 17 63.4305 25.5191 37 -8 5 -17 90.0405 27.4547 26 -8 5 17 39.8856 21.9577 24 8 5 -17 55.3074 21.3558 32 -8 5 17 48.9667 20.9743 34 -8 5 18 -5.21429 22.3826 37 -8 5 -18 20.3272 20.1963 26 -8 5 18 15.516 19.8579 24 -8 5 18 9.79102 19.7776 34 -8 5 19 54.8968 21.1649 37 -8 5 -19 66.6066 22.2511 26 -8 5 19 113.926 24.4454 24 -8 5 19 93.6131 23.2599 34 -8 5 20 11.5939 17.514 37 8 5 21 -5.69093 12.3877 29 -8 6 0 -6.91085 23.5183 39 -8 6 0 52.4538 25.1724 40 -8 6 0 21.6614 22.9102 13 -8 6 0 -14.3533 23.8612 17 -8 6 0 62.8302 24.3243 35 8 6 0 -6.30893 26.2948 29 -8 6 0 6.04996 24.8306 30 -8 6 0 -6.85076 21.6662 8 -8 6 1 1375.94 93.0624 40 -8 6 1 1519.4 95.9006 39 -8 6 -1 1617.44 98.1835 39 -8 6 1 1715.59 91.54 13 -8 6 -1 1708.31 91.3056 13 -8 6 1 1711.8 101.511 17 -8 6 -1 1498.41 97.1775 17 -8 6 -1 1644.61 90.492 35 -8 6 1 1725.76 90.6549 35 8 6 1 1519.27 95.5617 36 -8 6 -1 1453.87 91.2887 30 -8 6 1 1820.04 96.33 30 8 6 -1 1595.82 95.3199 29 8 6 1 1478.69 92.456 29 -8 6 1 1464.12 93.6347 8 -8 6 -1 1444.39 94.1354 8 -8 6 -2 1814.09 107.683 39 -8 6 2 1650.14 103.881 40 8 6 2 2040.92 109.073 41 -8 6 2 1706.4 104.043 39 -8 6 -2 1788.33 107.609 17 -8 6 2 2032.64 101.967 13 -8 6 -2 2060.59 102.578 13 -8 6 2 1952 110.744 17 8 6 -2 1730.73 105.862 18 8 6 2 1687.24 105.05 18 -8 6 -2 2136.6 103.562 35 -8 6 2 1851.26 98.1252 35 8 6 2 1820.16 106.72 36 -8 6 -2 2012.53 106.198 30 -8 6 2 2047.92 110.758 28 -8 6 2 2076.44 107.02 30 8 6 -2 1809.91 103.518 29 8 6 2 1717.81 103.351 29 -8 6 2 1661.99 102.731 8 -8 6 -2 1701.49 104.113 8 8 6 3 69.0501 24.9952 23 -8 6 3 86.9595 27.924 39 -8 6 -3 99.1835 30.8802 39 8 6 -3 38.5573 26.0071 43 8 6 3 77.8549 27.8925 41 -8 6 3 27.4635 25.9322 40 -8 6 3 53.5833 23.0539 13 -8 6 -3 37.3945 22.6552 13 8 6 -3 34.8834 24.3269 18 8 6 3 27.2262 24.7423 18 -8 6 3 13.9848 23.848 17 -8 6 -3 57.5199 29.5511 17 8 6 3 111.471 30.369 36 -8 6 -3 53.6165 24.3447 35 -8 6 3 85.5684 25.3504 35 8 6 -3 24.9082 26.7748 29 -8 6 -3 36.9018 21.4587 30 8 6 3 39.0059 24.1022 29 -8 6 3 17.8831 20.8021 30 -8 6 3 56.2135 28.882 28 -8 6 3 53.4131 23.7838 8 -8 6 -3 27.462 19.9875 8 8 6 -4 116.618 30.9395 42 -8 6 -4 192.324 35.4285 39 8 6 -4 152.204 32.6187 43 -8 6 4 110.68 30.9613 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130.915 4 9 -1 7 2874.79 129.29 4 -9 -1 7 3053.3 127.424 20 -9 1 7 2849.41 128.385 24 -9 1 7 2934.08 126.856 20 9 1 -8 11404 412.256 7 9 -1 -8 11423.9 412.57 7 -9 -1 8 11213.2 411.437 3 -9 1 8 11504 412.8 3 9 1 8 10937.9 412.389 4 9 -1 8 11071.2 411.949 4 -9 1 8 10643.7 410.46 24 -9 -1 8 11737.5 409.679 20 -9 1 8 11048.1 407.82 20 9 1 9 198.185 28.7635 4 9 -1 9 179.025 27.6543 4 9 1 -9 214.679 29.2587 7 9 -1 -9 175.767 26.8063 7 -9 -1 9 277.628 32.0682 3 -9 1 9 247.811 30.2216 3 -9 -1 9 166.041 23.4541 20 -9 1 9 199.363 26.2355 20 -9 1 9 229.5 29.4181 24 9 1 -10 5812.99 235.827 7 9 -1 -10 6167.41 237.877 7 -9 -1 10 5829.66 235.621 3 -9 1 10 5857.86 235.927 3 9 1 10 6155.76 238.513 4 9 -1 10 5754.44 236.257 4 -9 -1 10 5749.15 231.293 20 -9 1 10 6040.11 235.666 24 9 1 11 234.075 32.9061 4 9 -1 11 217.33 31.6492 4 -9 -1 11 251.618 33.5229 3 -9 1 11 267.335 32.9935 3 9 1 11 220.646 32.0553 46 9 1 -11 204.367 30.8301 7 9 -1 -11 153.748 29.5477 7 -9 -1 11 231.202 28.7867 20 -9 1 11 256.132 33.5692 24 9 1 12 211.744 33.0897 4 9 -1 12 227.341 32.4372 4 -9 -1 12 167.208 29.8359 3 -9 1 12 210.772 33.0668 3 -9 -1 -12 138.006 28.5626 33 -9 1 12 235.814 34.0596 37 9 1 12 142.126 28.3428 46 9 -1 12 116.569 24.9747 46 9 -1 -12 138.069 29.1788 7 9 1 -12 176.188 30.9531 7 -9 -1 12 152.959 26.2397 20 -9 1 12 190.065 31.48 24 9 1 13 201.094 33.8097 4 9 -1 13 194.254 34.1924 4 -9 -1 13 138.715 29.9987 3 -9 1 13 185.204 33.1087 3 -9 -1 -13 232.693 35.8015 33 -9 1 13 213.803 32.7322 37 9 1 13 197.185 32.0897 46 9 -1 13 198.228 31.3659 46 9 -1 -13 147.74 29.1056 7 9 1 -13 135.509 28.705 7 -9 -1 13 204.503 29.7809 20 9 1 14 158.933 31.2922 46 9 -1 14 222.329 34.8441 46 9 -1 -14 188.185 32.7057 7 9 1 -14 206.388 33.5469 7 9 1 14 223.759 34.8407 4 9 -1 14 247.449 36.1066 4 -9 -1 14 252.256 34.7914 3 -9 1 14 258.548 36.7602 3 -9 1 14 239.968 37.414 37 9 1 15 51.0524 25.8587 46 9 -1 15 75.7625 26.3922 46 9 -1 -15 98.9332 27.1455 7 9 1 -15 111.799 29.0939 7 -9 1 15 50.6329 24.3833 37 9 1 15 58.9186 23.8353 4 9 -1 15 65.1472 23.2448 4 -9 -1 15 19.4645 20.6197 3 -9 1 15 51.8833 24.9812 3 -9 1 16 197.634 36.3363 37 9 1 16 157.831 31.5782 46 9 -1 16 222.371 35.7693 46 -9 1 17 222.39 39.346 37 9 -1 17 186.455 34.4355 46 9 1 17 173.399 34.8236 46 -9 1 18 1747.61 102.401 37 9 -1 -18 1861.73 106.791 14 9 1 -18 1655.97 102.178 14 9 1 18 1705.12 101.132 10 9 -1 18 1440.46 96.1558 10 9 1 18 1641.36 98.4877 46 9 -1 18 1587.34 98.6039 46 9 -1 -19 -13.8778 33.0111 14 9 1 -19 -27.6657 37.5501 14 -9 1 19 6.5886 29.0756 37 -9 -1 19 58.9463 29.2915 37 9 1 19 -6.70287 27.9353 10 9 -1 19 -13.3025 28.5479 10 9 1 19 6.41032 20.7984 46 9 -1 19 6.46202 23.9051 46 -9 -1 20 768.438 64.3173 37 -9 1 20 825.046 65.2487 37 9 -1 -20 872.08 67.9186 14 9 1 -20 706.25 62.5841 14 9 1 20 852.158 66.1042 10 9 -1 20 726.334 61.1022 10 9 1 20 802.221 62.2918 46 9 -1 20 818.435 62.7754 46 9 -1 -21 -5.99221 25.3495 14 9 1 -21 5.98066 27.4424 14 9 1 21 11.5165 19.5953 10 9 -1 21 28.5243 20.6948 10 9 -1 21 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12.089 13.8676 3 -9 2 2 9.05068 13.3137 3 9 2 -3 6368.31 241.603 21 -9 -2 3 6278.97 234.801 20 -9 2 3 6417.44 240.153 11 -9 2 -3 6015.3 239.627 11 -9 -2 3 6234.05 236.136 3 -9 2 3 6380.47 237.025 3 -9 2 -3 6114.19 235.358 5 -9 -2 -3 6227.56 236.634 5 9 2 3 6316.23 236.986 4 -9 -2 4 5066.02 191.912 20 9 2 -4 4978.27 197.274 21 -9 2 4 4758.7 195.056 24 -9 2 -4 4740.36 195.088 11 -9 2 4 4956.72 194.756 11 -9 -2 4 5091.49 193.022 3 -9 2 4 5074.56 193.206 3 -9 2 -4 5057.8 193.115 5 -9 -2 -4 4753.6 192.279 5 9 2 4 4954.49 193.149 4 -9 -2 5 3276.43 137.827 20 -9 2 5 3377.69 142.516 24 9 2 -5 3528.86 144.889 21 9 2 5 3179.88 140.279 23 -9 -2 5 3552.8 139.968 3 -9 2 5 3241.29 137.909 3 -9 2 -5 3343.13 138.545 5 -9 -2 -5 3419.23 140.096 5 9 2 5 3182.99 138.081 4 -9 2 6 3416.81 143.553 24 -9 -2 6 3296.46 138.46 20 9 2 -6 3220.05 143.275 21 9 2 6 2998.71 139.29 23 9 2 -6 3484 139.912 7 -9 -2 6 3188.67 138.223 3 -9 2 6 3281.72 139.306 3 -9 2 -6 3323.32 139.6 5 -9 -2 -6 3516.7 141.59 5 9 2 6 3510.37 142.002 4 9 2 7 16.2158 16.6391 23 9 2 -7 4.43634 15.7692 21 -9 2 7 8.56196 17.0129 24 -9 -2 7 18.3933 14.8613 20 9 2 7 3.94489 14.5951 4 9 2 -7 -3.8177 14.1247 7 -9 2 -7 -3.85719 15.0714 5 -9 -2 -7 3.94064 14.8571 5 -9 -2 7 15.3747 13.663 3 -9 2 7 11.5853 15.3472 3 9 2 8 2368.71 111.162 23 9 2 -8 2503.21 115.747 21 -9 -2 8 2386.3 109.622 20 -9 2 8 2369.23 113.166 24 9 2 -8 2487.02 110.826 7 -9 2 8 2384.41 110.702 3 9 2 8 2194.57 109.229 4 -9 -2 9 2010.13 99.6563 20 -9 2 9 2133.23 105.602 24 9 2 -9 2220.81 102.877 7 -9 2 9 2014.73 101.458 3 9 2 9 2063.44 102.468 4 -9 -2 10 670.556 49.5389 20 -9 2 10 673.84 53.2342 24 9 2 -10 665.933 49.6109 7 9 2 10 653.678 51.0494 4 9 2 11 95.3601 26.1533 46 9 2 11 88.0314 24.7256 4 -9 2 -11 82.4335 22.2138 26 -9 2 11 16.3976 22.5311 24 -9 -2 11 56.9506 20.4788 20 9 2 12 44.6855 21.5191 46 -9 -2 -12 29.8322 22.9759 33 -9 2 12 50.4733 22.3581 37 -9 2 -12 81.0697 24.8645 26 -9 -2 12 45.2431 19.3827 20 -9 2 12 86.7616 26.9303 24 -9 -2 -13 2377.02 120.632 33 -9 2 13 2338.94 118.606 37 9 2 13 2092.03 113.505 46 -9 -2 13 2246.21 112.962 20 -9 2 13 2208.86 117.182 24 9 2 14 -12.202 23.8369 46 -9 -2 14 5.50313 18.7275 20 -9 2 14 -12.6915 23.4757 24 -9 2 14 -6.29846 25.4427 37 9 2 15 333.029 41.7545 46 -9 2 15 300.55 40.3263 24 9 2 16 12.758 23.1397 46 9 -2 16 6.28744 21.8762 46 -9 2 16 -19.8768 24.0342 24 -9 2 16 13.4794 24.4482 37 9 2 17 152.704 31.2991 46 9 -2 17 133.01 31.8306 46 -9 2 17 149.653 35.5372 37 9 2 17 104.897 30.4253 10 -9 2 17 138.201 32.7012 24 -9 2 18 181.216 36.9408 37 9 2 18 155.03 31.1113 46 9 -2 18 237.111 35.8738 46 9 2 18 173.506 35.4124 10 9 2 -18 159.131 35.2151 14 -9 2 19 -6.4521 24.3256 37 9 2 19 -5.89134 19.1178 46 9 -2 19 5.9875 21.2836 46 9 2 19 -24.5425 23.5571 10 9 2 -19 -12.6952 24.3708 14 -9 2 20 84.4855 28.4879 37 9 2 20 59.6705 24.3939 46 9 -2 20 83.6004 24.7272 46 9 2 -20 76.5547 26.8023 14 -9 2 21 27.2408 21.3378 37 -9 -2 21 63.988 26.8439 37 9 -2 21 35.0976 20.6314 46 9 2 -21 63.2147 25.1058 14 -9 2 22 108.921 25.9683 37 -9 -2 22 101.519 24.8702 37 9 -2 22 82.3412 21.4046 46 -9 -2 -22 149.003 28.3498 44 9 2 -22 117.37 26.6552 14 -9 2 23 156.969 24.762 37 -9 -2 23 136.878 23.5392 37 -9 -2 -23 115.496 23.7511 44 9 -2 23 138.98 20.8777 46 -9 2 24 -12.1312 13.5657 37 -9 -2 24 -8.73446 14.788 37 9 -2 -24 -3.0943 13.6575 33 9 -2 24 -2.71553 11.4903 46 -9 -2 -24 -9.23435 13.7684 44 -9 3 0 8.36635 15.4883 8 -9 3 0 35.4893 19.3213 11 -9 3 1 12418.5 456.181 11 -9 3 -1 12294.1 456.026 11 -9 3 1 12708.3 455.101 8 -9 3 -1 12352.1 454.474 8 -9 3 2 319.472 33.2393 8 -9 3 -2 262.982 32.9178 8 -9 3 2 347.878 35.9462 11 -9 3 -2 305.571 33.9086 11 -9 3 3 747.628 51.4873 11 -9 3 -3 614.969 48.2234 11 -9 3 3 622.613 47.1073 8 -9 3 -3 702.68 49.6541 8 9 3 -3 711.629 50.7869 21 -9 3 4 1463.99 80.4418 8 -9 3 -4 1670.94 84.6443 8 -9 3 -4 1463.4 82.5395 11 -9 3 4 1601.89 83.6709 11 9 3 -4 1658.62 85.6352 21 -9 -3 4 1521.25 76.312 20 -9 3 4 1712.38 84.7396 24 -9 3 5 1592.96 89.6121 11 -9 3 -5 1685.38 90.2416 8 -9 3 5 1997.07 93.2591 8 -9 -3 5 1859.1 87.9048 20 9 3 -5 2039.03 97.8521 21 -9 3 5 1814.15 92.9068 24 9 3 5 1918.23 94.9468 23 -9 -3 6 900.416 56.0736 20 -9 3 6 1038.43 63.2715 24 9 3 -6 927.74 62.1322 21 9 3 6 950.048 62.4065 23 9 3 7 2193.48 108.763 23 -9 -3 7 2163.97 103.711 20 -9 3 7 2292.36 109.923 24 9 3 -7 2139.89 109.014 21 9 3 8 5.15189 18.6888 23 9 3 -8 26.9495 19.5521 21 -9 3 8 -20.6542 19.823 24 -9 -3 8 -8.74698 14.5408 20 -9 3 -8 20.2113 17.9591 26 9 3 9 64.4925 24.8633 23 9 3 -9 68.167 24.2393 21 -9 3 9 114.708 26.7724 24 -9 -3 9 107.089 22.6303 20 -9 3 -9 116.849 25.7564 26 9 3 10 374.685 41.8663 23 9 3 -10 222.133 35.8528 21 -9 3 10 236.78 35.8323 24 -9 -3 10 271.72 32.4612 20 -9 3 -10 334.598 38.9142 26 9 3 -11 640.167 56.6387 21 -9 -3 11 727.723 53.4009 20 -9 3 11 614.467 54.8072 24 -9 3 -11 583.604 52.2496 26 -9 3 12 1031.57 72.4494 37 -9 -3 12 1060.22 69.2685 20 9 3 -12 989.732 72.6174 21 -9 3 12 981.957 72.9905 24 -9 3 -12 1142.26 75.0434 26 -9 3 13 109.211 30.0204 37 9 3 -13 75.8937 30.2092 21 -9 3 13 79.5873 29.0533 24 -9 -3 13 126.331 28.1357 20 -9 3 -13 87.8813 27.5181 26 -9 3 14 99.7089 31.3645 37 -9 3 -14 83.419 27.2727 26 -9 3 14 54.6126 27.7006 24 -9 3 15 853.235 66.1815 34 -9 3 15 734.234 64.0745 37 -9 3 -15 724.266 62.5191 26 -9 3 15 713.883 62.9549 24 -9 3 -16 128.065 30.9814 26 -9 3 16 55.297 29.4158 24 -9 3 16 95.525 28.617 37 -9 3 16 103.53 30.2295 34 -9 3 -17 378.388 45.1847 26 -9 3 17 398.56 46.1269 24 -9 3 17 383.364 45.6801 37 -9 3 17 332.768 42.3949 34 -9 3 -18 193.113 34.0571 26 -9 3 18 278.577 40.903 37 -9 3 18 219.261 35.5221 34 -9 3 18 244.488 36.9819 24 -9 3 19 6.07023 23.3035 37 -9 3 19 5.40577 19.2132 34 -9 3 19 -11.913 21.6072 24 -9 3 20 110.408 29.914 37 -9 3 20 101.437 24.4481 24 -9 3 21 63.0873 23.2227 37 -9 -3 -21 86.5471 24.7932 44 -9 -3 22 185.565 27.2131 37 -9 -3 -22 194.849 27.4825 44 -9 3 23 6.50741 14.7443 37 -9 -3 23 27.8349 15.709 37 -9 -3 -23 -3.2294 14.8206 44 -9 4 0 5.5403 19.2769 2 -9 4 0 -5.17619 16.3692 8 -9 4 0 -5.53726 21.6338 11 -9 4 -1 1918.14 99.1257 2 -9 4 1 1746.41 96.4073 2 -9 4 1 1704.78 93.3667 8 -9 4 1 1829.32 97.7329 11 -9 4 -1 1731.77 96.7057 11 -9 4 -1 1738.86 94.4151 8 -9 4 -2 2150.32 111.964 2 -9 4 2 2133.12 110.994 2 -9 4 2 2370.53 114.618 11 -9 4 2 2113.29 108.715 8 -9 4 -2 2126.75 108.846 8 -9 4 -2 2201.29 112.258 11 -9 4 -3 1900.27 106.268 2 -9 4 3 1820.21 102.955 2 9 4 3 2081.15 105.697 23 -9 4 3 2108.75 107.934 11 -9 4 -3 2075.87 108.143 11 -9 4 -3 2213.26 107.614 8 -9 4 3 2208.89 106.734 8 -9 4 -4 17.0637 19.8003 2 -9 4 4 27.2405 21.2946 2 9 4 4 26.7421 22.2993 23 -9 4 4 21.843 19.8188 11 -9 4 -4 11.3308 19.2889 11 -9 4 4 35.7494 19.6159 8 -9 4 -4 5.30354 17.6436 8 -9 4 -4 10.9753 19.9163 38 -9 4 5 1875.37 100.559 11 -9 4 -5 1899.11 102.556 11 -9 4 5 2037.01 100.71 8 -9 4 -5 1723.02 97.6719 8 -9 4 -5 1815.74 101.05 2 -9 4 5 2003.85 102.925 2 -9 4 -5 1828.3 98.8598 47 -9 4 -5 1798.21 100.535 38 -9 4 5 1873.95 97.8092 24 9 4 5 2086.85 104.72 23 -9 4 -5 2012.43 99.9368 26 -9 4 -6 2571.62 129.2 38 9 4 6 2845.77 131.703 23 -9 4 6 2592.8 125.782 24 9 4 -6 2564.52 128.258 21 -9 4 -6 2662.81 126.866 26 -9 4 -7 5.94513 21.5814 38 9 4 7 5.87022 19.9924 23 9 4 -7 23.4926 20.8903 21 -9 -4 7 36.9113 17.7316 20 -9 4 7 21.852 23.7944 24 -9 4 -7 43.6274 18.9921 26 -9 4 -8 1107.69 77.2411 38 -9 4 -8 1311.54 78.4619 26 9 4 8 1243.94 79.7916 23 -9 -4 8 1155.83 71.04 20 -9 4 8 1280.54 79.086 24 9 4 -8 1105.46 75.7311 21 -9 4 -9 -29.7599 22.44 26 9 4 9 -6.2627 25.2995 23 9 4 -9 -6.29193 19.3693 21 -9 -4 9 10.3548 18.4042 20 -9 4 9 12.0569 21.4286 24 -9 4 -10 352.882 42.7626 26 -9 4 10 315.024 42.254 24 9 4 10 386.474 44.6312 23 9 4 -10 339.101 41.5389 21 -9 -4 10 239.566 33.8188 20 9 4 -11 1910.86 103.176 27 -9 4 -11 2075.36 109.909 26 -9 -4 11 1837.07 102.229 20 9 4 -11 1829.23 107.951 21 -9 4 11 1973.63 109.768 24 -9 4 12 1002.54 74.8999 37 -9 4 -12 1065.58 75.8003 26 -9 4 12 1109.37 78.8727 24 -9 4 12 1025.34 73.8435 34 -9 4 -13 73.5527 28.3514 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4.49223 17.2488 4 -11 1 -6 13.462 17.5349 5 -11 -1 -6 13.6051 18.9035 5 -11 -1 6 4.42411 19.7887 3 -11 1 6 -8.84791 18.7179 3 11 1 -7 779.729 53.0999 7 11 -1 -7 701.614 50.8543 7 11 1 -7 583.824 48.0406 21 -11 -1 7 747.185 50.7081 20 -11 1 7 712.638 51.1097 24 -11 -1 7 670.462 50.9781 3 -11 1 7 671.115 51.0171 3 -11 1 -7 642.528 51.1106 5 -11 -1 -7 777.642 53.6698 5 11 1 7 681.009 52.1853 4 11 -1 7 734.668 52.9436 4 11 1 -8 2162.63 107.899 7 11 -1 -8 2076.67 106.841 7 11 1 -8 2115.85 107.159 21 -11 -1 8 2384.38 107.697 20 -11 1 8 2354.77 109.319 24 -11 -1 8 2239.09 109.051 3 -11 1 8 2203.62 108.685 3 -11 1 -8 2121.78 107.979 5 -11 -1 -8 2165.39 108.784 5 11 1 8 2117.63 108.142 4 11 -1 8 2124.81 108.745 4 -11 -1 -9 599.329 52.2528 44 11 1 9 587.376 50.1822 46 11 1 -9 706.52 52.9075 7 11 -1 -9 681.484 52.1553 7 11 1 -9 634.891 50.5597 21 -11 1 9 667.758 51.0617 24 -11 -1 9 606.464 48.1589 20 -11 -1 9 709.063 53.8689 3 -11 1 9 611.094 51.6379 3 -11 1 -9 655.344 51.8607 5 -11 -1 -9 692.143 53.0289 5 11 1 9 641.297 51.7624 4 11 -1 9 560.765 49.8767 4 -11 1 -10 601.355 51.5186 44 11 1 10 624.094 51.9937 46 11 1 -10 667.169 53.519 7 11 -1 -10 546.766 50.0301 7 -11 -1 10 592.765 48.4643 20 -11 1 10 627.607 51.5463 24 -11 -1 10 751.577 55.6804 3 -11 1 10 626.106 52.3694 3 -11 1 -10 597.376 51.1231 5 -11 -1 -10 662.765 52.8132 5 11 1 10 633.37 52.6393 4 11 -1 10 610.566 52.5369 4 11 1 11 883.579 63.0121 46 -11 1 -11 727.037 57.4748 44 11 -1 11 860.451 60.5218 46 11 1 -11 614.72 54.9341 7 11 -1 -11 780.061 59.5945 7 -11 -1 11 837.812 57.6652 20 -11 1 11 770.804 57.0739 24 -11 -1 11 630.927 55.654 3 -11 1 11 872.732 61.9081 3 -11 1 -11 632.597 55.6927 5 -11 -1 -11 706.836 58.0191 5 11 1 11 709.981 59.186 4 11 -1 11 756.801 59.8364 4 11 1 12 153.244 31.9664 46 11 -1 12 215.564 32.1478 46 11 1 -12 297.045 37.466 7 11 -1 -12 179.805 32.3217 7 -11 -1 12 173.623 29.2271 20 11 1 12 113.066 29.0336 4 11 -1 12 80.9494 25.8005 4 -11 -1 12 228.239 36.2605 3 -11 1 12 197.861 32.5465 3 11 1 13 1602.19 90.6933 46 11 -1 13 1344.6 84.1654 46 -11 -1 13 1354.09 85.7359 3 -11 1 13 1389.05 87.0043 3 11 1 13 1282.83 84.385 4 11 -1 13 1388.68 86.8603 4 11 -1 -13 1328.72 85.8036 7 11 1 -13 1313.2 84.6417 7 -11 -1 13 1188.32 78.1364 20 11 1 14 323.666 44.4535 4 11 -1 14 528.175 52.182 4 -11 -1 14 463.533 49.8565 3 -11 1 14 432.503 48.6661 3 11 -1 -14 467.011 50.4359 7 11 1 -14 371.574 46.8934 7 11 1 14 474.486 49.2291 46 11 -1 14 558.872 51.8808 46 -11 1 14 469.911 48.393 37 11 1 15 67.2391 27.6417 46 11 -1 15 45.6203 24.1624 46 -11 1 15 32.0295 25.9256 37 11 -1 16 151.398 32.7632 46 11 1 16 148.654 34.6682 46 -11 1 16 137.09 33.5179 37 11 1 17 33.3193 24.1857 46 11 -1 17 26.1013 24.1519 46 -11 1 17 13.0419 25.0458 37 11 1 18 -6.66185 26.9104 10 11 -1 18 -19.7839 27.4847 10 11 1 18 6.43338 21.3894 46 -11 -1 -18 -20.0278 24.2174 44 11 -1 18 44.2252 24.2547 46 -11 1 18 -19.0928 25.2903 37 -11 -1 18 70.1745 26.988 37 11 -1 -19 12.9307 27.7532 14 11 1 -19 -19.3696 29.9965 14 11 1 19 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46 11 -1 23 59.6188 17.7871 46 -11 1 23 48.4761 17.1715 37 -11 -1 23 72.5882 19.8614 37 -11 1 24 23.1283 11.9685 37 -11 -1 24 28.218 13.9534 37 -11 2 0 -4.38867 16.545 11 -11 2 1 97.0815 21.4367 11 -11 2 -1 75.7874 21.4097 11 -11 2 2 954.394 59.8794 11 -11 2 -2 910.758 59.694 11 -11 -2 2 964.057 54.785 20 -11 2 2 915.283 56.86 3 11 2 2 921.019 57.0588 4 -11 2 3 1536.13 82.6168 11 -11 2 -3 1571.45 83.6014 11 -11 -2 3 1545.06 78.0422 20 11 2 -3 1559.43 83.7059 21 -11 -2 -3 1615.62 81.8061 5 -11 2 3 1485.52 79.4023 3 11 2 3 1539.63 80.3211 4 -11 2 4 1975.96 96.3737 11 -11 2 -4 1909.74 96.2685 11 -11 -2 4 1941.01 91.6224 20 11 2 -4 2122.98 99.7296 21 -11 2 4 1949.5 93.7802 3 -11 2 -4 1864.86 92.611 5 -11 -2 -4 1715.27 91.6334 5 11 2 4 1806.99 92.8467 4 -11 2 5 342.203 34.993 11 11 2 5 277.777 32.9279 23 -11 -2 5 324.579 32.7971 20 11 2 -5 397.061 39.2904 21 11 2 5 328.448 33.7904 4 -11 2 -5 277.565 31.8489 5 -11 -2 -5 323.432 33.8793 5 -11 2 5 274.099 30.5415 3 -11 -2 6 4.21646 16.1873 20 11 2 -6 5.04013 18.2834 21 11 2 6 4.58819 16.3078 4 11 2 -6 -22.0698 19.4793 7 -11 2 6 4.47081 17.1637 3 11 2 -7 5608.44 221.211 7 11 2 7 5535.26 222.122 4 -11 -2 7 5662.95 219.689 20 11 2 -7 5204.34 222.953 21 -11 2 7 5294.67 222.362 24 11 2 8 30.3661 17.6335 4 -11 -2 8 56.268 20.147 20 11 2 -8 27.7664 21.716 21 -11 2 8 31.722 23.663 24 11 2 8 53.335 21.564 46 -11 -2 -8 -15.6609 18.9592 44 -11 -2 -9 4967.94 203.613 44 11 2 9 4786.59 202.849 46 -11 -2 9 4654.09 197.122 20 11 2 -9 4513.91 202.122 21 -11 2 9 4816.64 203.214 24 -11 2 -9 4771.3 200.241 26 11 2 10 1037.96 71.3917 46 -11 -2 10 998.664 66.5719 20 11 2 -10 1084.77 72.8636 21 -11 2 10 1060.17 72.6912 24 -11 2 -10 1065.51 70.51 26 11 2 11 663.006 55.8049 46 -11 -2 11 607.365 51.4796 20 -11 2 11 749.559 58.6282 24 11 2 -11 554.998 53.1127 21 -11 2 -11 676.39 55.1648 26 11 2 12 43.7121 22.6528 46 -11 -2 12 28.4587 20.6474 20 11 2 -12 -20.3154 23.0443 21 -11 2 12 18.8253 23.6564 24 -11 2 -12 -11.699 19.9059 26 11 2 13 -6.42502 21.3623 46 -11 -2 13 11.7388 18.0678 20 11 2 -13 14.0996 21.7009 21 -11 2 13 19.3898 24.3664 24 11 2 14 143.893 31.9489 46 -11 2 14 65.8463 29.575 24 -11 2 14 51.0285 25.9104 37 11 2 15 434.6 47.5793 46 -11 2 15 501.33 51.3931 37 11 2 16 130.306 32.5706 46 -11 2 16 104.295 30.8228 24 -11 2 16 58.931 30.9603 37 11 2 17 6.40054 24.1288 10 11 2 17 -6.31858 21.5016 46 -11 2 17 -6.4477 23.3891 37 11 2 -18 269.088 42.5762 14 11 2 18 243.269 36.4319 10 11 2 18 311.508 39.4289 46 -11 -2 -18 259.166 39.2382 44 -11 2 18 254.071 38.9407 37 11 2 -19 127.607 29.7343 14 11 2 19 110.351 26.5601 46 -11 -2 -19 108.594 31.8215 44 11 -2 19 133.425 26.5719 46 -11 2 19 115.92 29.7125 37 11 2 -20 306.929 38.3433 14 -11 -2 -20 283.454 37.8066 44 11 2 20 359.515 38.3625 46 11 -2 20 345.77 37.0056 46 -11 2 20 357.508 40.0082 37 -11 -2 20 389.134 41.9687 37 11 2 -21 295.507 35.7417 14 11 2 21 312.907 33.2064 46 11 -2 21 228.824 29.1868 46 -11 -2 -21 347.056 36.9949 44 -11 2 21 239.432 32.3141 37 -11 -2 21 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40 13 6 -9 49.3708 24.545 27 -13 6 9 18.2261 24.9451 28 -13 6 10 348.099 43.0834 31 -13 6 10 288.27 37.1362 40 13 6 -10 320.97 38.5318 27 -13 6 10 385.186 42.0659 28 13 6 11 63.8195 25.444 36 -13 6 11 125.873 29.5684 31 -13 6 11 64.512 24.566 40 13 6 -11 96.1818 24.5707 27 -13 6 11 60.7159 24.5065 28 13 6 12 169.18 29.1127 36 -13 6 12 127.616 25.8422 40 13 6 -12 192.961 28.9066 27 -13 6 12 169.255 31.4843 28 13 6 -13 15.5785 15.2192 27 -13 6 13 -4.66914 17.6045 28 -13 6 13 9.18595 17.9471 31 13 6 -13 4.30419 15.9257 32 13 6 13 21.3838 17.2783 36 -13 6 14 4.14593 17.2791 28 -13 6 14 24.2965 18.1103 31 13 6 -14 -18.9492 16.7249 32 -13 6 14 3.35385 13.5478 34 13 6 14 14.5741 13.7356 36 -13 6 15 -7.12751 14.8525 28 -13 6 15 3.43854 13.4341 31 13 6 -15 -6.41174 13.7599 32 -13 6 15 11.7155 11.8309 34 -13 6 16 -5.84042 11.7959 28 13 6 -16 2.5418 9.75789 32 13 7 0 9.92704 19.3923 29 -13 7 0 5.76911 21.342 39 13 7 0 -5.46512 20.6026 43 13 7 0 18.1389 24.4236 18 -13 7 0 -12.4481 24.3171 17 13 7 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42 13 8 3 9.70762 15.5806 42 13 8 3 12.8699 14.0148 29 13 8 -4 31.492 15.8739 18 13 8 4 17.0301 14.218 18 -13 8 -4 30.725 18.0756 39 -13 8 4 24.0024 14.5277 40 13 8 4 24.5817 15.0939 43 13 8 -4 56.7967 16.5361 42 13 8 4 18.6506 14.6372 42 13 8 4 37.1503 14.5782 29 13 8 -4 -3.00096 12.5329 27 13 8 5 91.9146 17.9799 36 -13 8 -5 58.5286 16.9523 39 -13 8 5 63.0269 16.1399 40 13 8 5 59.9562 17.5875 43 13 8 -5 72.8132 15.9166 42 13 8 5 85.388 17.1212 42 13 8 5 94.043 17.0894 29 13 8 -5 47.0662 14.6685 27 13 8 6 25.2057 15.8719 36 -13 8 6 25.0477 14.5831 40 13 8 6 12.3757 12.3397 43 13 8 6 43.7864 15.287 42 13 8 6 46.5818 13.8133 29 13 8 -6 39.5998 14.1082 27 13 8 7 20.6442 13.2001 36 13 8 7 32.5791 12.4759 29 13 8 -7 5.3182 11.904 27 -13 8 7 2.88625 12.575 40 13 8 7 14.0005 11.8572 43 13 8 7 19.9158 12.2611 42 13 8 -8 -2.43694 9.8439 27 -13 8 8 2.56872 10.3762 40 13 8 8 -7.33659 11.2213 43 13 8 8 6.59146 9.95484 42 -14 0 0 15789.8 562.82 11 -14 0 0 15067 563.895 44 -14 0 1 14.6785 20.0803 11 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81.3407 25.0813 7 -14 0 -8 109.243 27.7777 5 -14 0 8 88.2297 25.2591 3 14 0 8 131.809 29.3443 46 -14 0 -8 131.23 29.5661 44 14 0 9 -6.62668 22.5499 4 14 0 -9 -6.48677 23.0553 7 -14 0 -9 -6.64446 22.6104 5 -14 0 9 13.0091 22.1342 3 14 0 9 18.5826 23.7794 46 -14 0 -9 19.3266 25.5995 44 -14 0 -10 873.658 68.3913 44 14 0 10 900.284 67.0653 46 -14 0 10 845.99 66.9347 3 -14 0 -10 829.741 67.546 5 14 0 10 846.514 66.9351 4 14 0 -10 871.425 66.8464 7 -14 0 -11 -6.77342 24.074 44 14 0 11 6.55671 22.3117 46 -14 0 -12 956.172 74.2168 44 14 0 12 1048.29 75.1991 46 14 0 13 -6.74207 23.4592 46 -14 0 -13 -6.92214 25.6082 44 14 0 14 6.72365 23.3985 46 -14 0 -14 27.5112 26.8749 44 14 0 15 -26.4131 25.3526 46 -14 0 -15 13.4528 22.8924 44 -14 0 -16 1265.65 83.0551 44 14 0 16 1171.63 80.4794 46 14 0 17 -6.01794 20.4783 46 -14 0 -17 6.05723 22.4076 44 14 0 18 418.624 45.9791 10 14 0 18 465.652 45.7131 46 -14 0 -18 509.494 47.9155 44 -14 0 19 4.62108 19.5511 37 14 0 19 -4.97007 20.0784 46 -14 0 -19 -4.90237 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-1 -6 -42.244 24.7674 5 -14 -1 6 5.91534 21.0245 3 -14 1 6 11.8394 19.2069 3 -14 -1 6 -5.5001 19.5487 20 -14 1 -6 5.82364 20.6986 44 14 1 6 -5.95922 22.4653 46 -14 -1 -6 5.94474 22.4107 44 -14 1 -6 21.999 26.1647 47 14 1 7 343.868 41.9253 4 14 -1 7 252.435 38.0606 4 14 1 -7 337.943 39.605 7 14 -1 -7 324.549 39.9346 7 -14 1 -7 387.996 42.9957 5 -14 -1 -7 292.121 39.6957 5 -14 -1 7 322.023 39.6118 3 -14 1 7 334.696 40.8791 3 -14 -1 7 319.13 38.4611 20 -14 1 -7 226.795 36.2172 44 14 1 7 312.628 40.4313 46 -14 -1 -7 337.473 42.1468 44 -14 -1 8 996.594 71.917 3 -14 1 8 1180.98 76.3747 3 -14 1 -8 1088.61 74.4997 5 -14 -1 -8 1065.49 74.5346 5 14 1 8 1103.46 75.4236 4 14 -1 8 1204.84 76.7991 4 14 1 -8 961.602 70.9946 7 14 -1 -8 902.303 69.2134 7 -14 -1 8 1082.95 72.2862 20 -14 1 -8 1138.82 75.5333 44 -14 -1 -8 1241.65 77.9683 44 14 1 8 952.495 70.7967 46 14 1 9 378.157 45.2025 4 14 -1 9 294.226 41.7275 4 14 1 -9 361.71 43.34 7 14 -1 -9 373.536 44.9564 7 -14 1 -9 322.232 42.488 5 -14 -1 -9 357.643 43.0359 5 -14 -1 9 355.77 43.1441 3 -14 1 9 389.154 45.7391 3 -14 -1 9 351.977 41.3968 20 14 1 9 369.481 44.9828 46 -14 1 -9 376.955 43.9348 44 -14 -1 -9 333.386 42.7841 44 -14 -1 10 1716.44 104.498 3 -14 1 10 1808.18 106.352 3 -14 1 -10 1647.22 103.766 5 -14 -1 -10 2038.87 110.752 5 14 1 10 1842.61 108.124 4 14 -1 10 1863.6 107.137 4 -14 1 -10 1843.19 106.731 44 14 1 10 1928.05 108.604 46 -14 -1 10 2011.77 107.482 20 14 1 -10 1925.24 108.314 7 14 -1 -10 1980.18 108.78 7 -14 -1 -11 123.819 32.648 44 14 1 11 128.782 29.0174 46 -14 1 -11 143.827 33.8328 44 -14 1 -12 1280.03 82.2676 44 -14 -1 -12 1195.04 83.7458 44 14 1 12 1071.4 78.6279 46 14 1 13 179.192 34.642 46 14 -1 13 191.782 35.1152 46 -14 1 -13 263.834 38.3372 44 -14 -1 -13 210.889 37.7959 44 14 1 14 409.833 47.1769 46 14 -1 14 401.329 46.1294 46 -14 1 -14 370.739 44.844 44 -14 -1 -14 328.125 45.9624 44 14 -1 15 99.9326 28.5685 46 -14 1 -15 132.408 32.5825 44 -14 -1 -15 61.4298 30.7765 44 14 1 16 146.946 30.4783 46 14 -1 16 186.226 32.1447 46 -14 -1 -16 124.439 31.9371 44 14 1 17 59.937 27.2673 46 14 -1 17 73.4573 25.7194 46 -14 -1 -17 86.0833 28.67 44 -14 -1 18 55.3474 21.6083 37 14 1 18 16.8774 19.1578 10 14 -1 18 16.6147 20.5006 10 14 1 18 10.9851 19.1245 46 14 -1 18 15.5593 18.0601 46 -14 -1 -18 22.5295 24.8664 44 -14 -1 19 122.188 26.2497 37 14 -1 -19 168.94 30.2881 14 14 1 -19 128.445 29.4661 14 14 1 19 155.154 26.0761 10 14 -1 19 127.964 25.4058 10 14 1 19 132.07 27.1765 46 14 -1 19 120.115 24.133 46 -14 -1 -19 130.176 28.7329 44 -14 1 20 34.636 18.9785 37 -14 -1 20 74.7688 21.2106 37 14 -1 -20 26.3763 20.7077 14 14 1 -20 30.9233 21.5365 14 14 1 20 54.6965 19.3467 46 14 -1 20 39.6733 17.3157 46 -14 -1 -20 8.59423 17.6806 44 -14 1 21 208.616 24.4768 37 -14 -1 21 253.986 27.3709 37 14 1 21 214.274 25.5671 46 14 -1 21 217.223 25.4791 46 -14 -1 -21 228.59 27.198 44 14 -1 -21 258.758 28.35 14 14 1 -21 278.596 29.7098 14 -14 -1 -22 -2.65879 10.3882 44 14 1 22 5.2699 10.982 46 14 -1 -22 -2.70946 11.1202 14 14 1 -22 16.4153 13.016 14 -14 2 0 11.0758 18.4159 47 -14 2 0 16.113 19.0938 25 -14 2 0 6.00519 20.8981 11 -14 2 -1 252.625 33.8292 44 -14 2 1 186.327 30.8245 47 -14 2 -1 297.173 38.3599 47 -14 2 1 286.832 39.6047 11 -14 2 -1 247.284 37.2298 11 -14 2 1 203.96 31.9407 25 -14 2 -1 237.832 33.3263 25 -14 2 -2 -11.2544 21.6027 38 14 2 2 11.8177 20.559 46 -14 2 -2 10.9899 18.2688 44 -14 2 2 -5.40978 21.1356 47 -14 2 -2 -17.023 24.0043 47 -14 2 -2 11.362 19.3319 15 -14 2 2 -5.94366 20.2256 11 -14 2 -2 -6.05178 22.3875 11 -14 2 2 21.5628 18.7562 25 -14 2 -2 10.9279 18.5932 25 -14 2 -3 431.848 46.5871 38 -14 2 -3 449.785 45.9386 15 -14 2 3 432.251 44.6603 15 14 2 3 406.884 43.0812 46 -14 2 3 396.024 42.0617 47 -14 2 -3 511.694 47.8216 47 -14 2 3 408.215 42.8736 25 -14 2 -3 438.265 43.0417 25 -14 2 3 508.113 47.497 11 -14 2 -3 394.076 45.1117 11 -14 2 4 2030.86 105.208 11 -14 2 -4 1895.96 104.65 11 -14 2 -4 1793.72 100.232 15 -14 2 4 1882.9 101.516 15 -14 2 4 1800.32 99.8758 25 -14 -2 4 1897.01 98.6335 20 -14 2 -4 1833.74 102.087 47 14 2 4 1811.74 103.251 46 14 2 5 -6.18813 19.5714 46 -14 2 -5 5.84139 20.7635 47 -14 -2 5 5.36843 16.0613 20 -14 2 5 23.41 20.8031 11 -14 2 -5 24.4129 22.5797 11 -14 -2 6 16.7663 18.581 20 14 2 -6 -6.31556 19.9725 21 14 2 6 6.31487 23.8061 46 -14 -2 -6 -5.95802 20.7305 44 -14 2 -6 5.87216 21.7234 47 14 2 -7 1323.34 85.4359 21 -14 -2 7 1240.39 80.9531 20 -14 -2 -7 1463.4 87.2408 44 14 2 7 1476.83 88.9818 46 -14 -2 8 490.196 49.5256 20 14 2 -8 567.091 53.4126 21 -14 -2 -8 557.907 52.3134 44 14 2 8 598.918 55.7208 46 -14 -2 9 666.269 56.5228 20 -14 -2 -9 678.687 58.6009 44 14 2 9 684.128 59.2332 46 14 2 10 13.6038 22.6229 46 -14 -2 -10 6.68494 27.0107 44 -14 2 -10 56.6673 30.4094 38 14 2 11 13.7312 24.9049 46 -14 -2 -11 -6.8093 28.3788 44 -14 2 -11 -7.09571 24.6885 38 14 2 12 -6.86783 23.3704 46 -14 -2 -12 -6.87732 25.9261 44 -14 2 -12 7.01271 25.9423 38 14 2 13 13.6078 24.6853 46 -14 -2 -13 13.7407 27.7559 44 14 2 14 312.616 42.7509 46 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97.7152 29.1722 25 -14 3 -5 1192.77 81.1827 47 14 3 5 1412.82 87.3884 46 -14 3 5 1260.27 80.7031 15 -14 3 5 1202.97 81.9616 11 -14 3 -5 1286.43 84.6996 11 -14 3 -5 1237.07 83.698 38 14 3 5 1352.01 84.7729 23 -14 3 -6 69.3231 31.8257 38 14 3 6 6.31347 21.9917 23 14 3 6 32.915 23.9026 46 -14 3 -6 38.187 28.1061 47 14 3 7 19.9465 22.6332 46 -14 3 -7 14.163 27.1923 38 14 3 8 60.3265 28.3784 46 -14 3 -8 14.3894 23.9466 38 14 3 9 458.114 49.3794 46 -14 3 -9 319.293 46.2251 38 14 3 10 53.855 24.9285 46 -14 3 -10 14.495 23.5413 38 14 3 11 6.67933 22.743 46 -14 3 -11 57.1971 31.985 38 14 3 12 -19.679 26.5015 46 -14 3 -12 -6.9426 27.1285 38 14 3 13 432.852 46.7655 46 -14 -3 -13 328.444 42.1642 44 14 3 14 30.4194 23.3561 46 -14 -3 -14 -12.2628 25.1637 44 14 3 15 17.1361 21.19 46 -14 -3 -15 93.5487 26.5376 44 -14 3 16 70.362 24.3643 34 14 3 16 94.4052 25.3917 46 -14 -3 -16 81.9699 27.0319 44 -14 3 17 19.5243 19.7302 34 14 3 17 14.0709 18.0208 46 -14 -3 -17 34.8854 21.4027 44 -14 3 18 34.03 19.3593 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158.513 28.4734 39 -14 6 10 208.739 31.1398 40 14 6 -10 201.625 29.8563 27 -14 6 10 186.964 30.4434 28 14 6 11 38.5179 21.5858 36 -14 6 11 34.289 21.0788 31 -14 6 -11 56.8086 22.5725 39 -14 6 11 44.801 20.0931 40 14 6 -11 42.8785 18.4659 27 -14 6 11 53.6039 22.688 28 14 6 12 38.9268 21.0871 36 -14 6 12 49.3711 20.8878 31 -14 6 12 27.4324 17.105 40 14 6 -12 22.9819 17.6199 27 -14 6 12 58.2862 21.3669 28 14 6 -13 39.7721 16.3516 27 -14 6 13 44.3289 19.2086 28 -14 6 13 12.0354 16.2487 31 14 6 -13 41.369 16.8612 32 14 6 13 41.4413 16.8906 36 -14 6 14 70.3258 17.7501 28 -14 6 14 41.6496 17.5224 31 14 6 -14 45.2103 15.2716 32 14 6 14 40.7378 15.1693 36 -14 6 15 152.992 20.0578 28 14 6 -15 118.072 17.4888 32 -14 6 15 125.847 19.5264 31 14 7 0 514.134 47.8555 18 -14 7 0 500.866 46.8286 17 -14 7 0 426.337 43.5193 39 14 7 0 335.871 38.0747 43 14 7 0 446.966 39.7743 42 14 7 -1 11.0407 21.2066 18 14 7 1 16.3995 24.1362 18 -14 7 1 11.2499 23.4558 17 -14 7 -1 28.4315 20.6416 17 14 7 1 50.1982 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40 14 7 -5 337.062 35.873 27 14 7 6 -9.29622 17.5231 36 -14 7 -6 14.908 18.734 39 -14 7 6 4.63793 19.3299 40 14 7 -6 8.6852 17.2569 27 14 7 7 31.2186 19.1555 36 -14 7 -7 32.8436 19.8617 39 -14 7 7 17.5479 18.5725 40 14 7 -7 8.2881 17.0227 27 14 7 8 79.8914 22.2404 36 -14 7 -8 78.0105 23.5472 39 -14 7 8 106.101 22.5908 40 14 7 -8 124.639 23.7 27 14 7 -9 80.5357 18.5829 32 14 7 9 42.7306 18.5694 36 -14 7 -9 54.5254 19.66 39 -14 7 9 40.7325 18.3107 40 14 7 -9 50.2939 17.3831 27 14 7 -10 12.9366 13.2944 32 14 7 10 17.5153 14.3964 36 -14 7 -10 20.1609 16.3705 39 -14 7 10 19.5717 14.4148 40 14 7 -10 45.3492 15.4287 27 14 7 -11 49.3215 14.905 32 14 7 11 76.4033 17.6029 36 -14 7 11 55.0227 15.3665 40 14 7 -11 93.4757 16.8463 27 14 7 -12 11.8352 10.4503 27 14 7 -12 2.49864 10.0977 32 14 7 12 15.2119 11.1926 36 14 8 0 37.8123 16.4036 18 14 8 0 16.8808 12.3138 42 14 8 -1 78.5209 18.992 18 14 8 1 81.2956 19.3206 18 14 8 -1 47.0498 14.9199 42 14 8 1 67.6598 15.7327 42 14 8 1 63.913 15.769 43 14 8 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16.347 18.0382 47 -23 2 -1 8.36478 15.7705 15 -23 2 1 12.5426 16.617 15 -23 2 2 19.5845 18.1964 47 -23 2 -2 -4.21015 18.5801 47 -23 -2 2 -3.77727 15.5027 47 -23 -2 -2 16.2413 17.6751 47 -23 2 -2 12.243 17.5166 15 -23 2 2 -4.08018 15.6644 15 -23 2 -3 197.473 27.6972 47 -23 -2 -3 146.847 25.5103 47 -23 2 -3 218.848 27.4399 15 -23 2 3 246.475 28.4762 15 -23 2 -4 19.7615 15.7087 47 -23 -2 -4 -19.0589 16.1285 47 -23 2 -4 25.6314 14.7944 15 -23 2 4 14.7094 15.3295 15 -23 -2 -5 557.41 40.391 47 -23 -2 5 566.497 39.0957 15 -23 2 -6 67.9771 18.7404 47 -23 -2 -6 59.5556 17.4424 47 -23 -2 -7 5.88774 13.3395 47 -23 2 -7 6.61474 14.1971 38 -23 -2 -8 5.7459 12.506 38 -23 2 -8 -3.11508 12.9828 38 -23 -2 -9 26.5236 13.5021 38 -23 2 -9 28.4944 13.4297 38 -23 3 0 -14.2345 15.7048 47 -23 -3 0 33.9263 18.5832 47 -23 3 1 3.45089 15.4459 47 -23 3 -1 25.1759 16.7192 47 -23 -3 1 22.9928 15.9979 47 -23 -3 -1 23.9764 16.4952 47 -23 3 2 9.81474 14.4408 47 -23 3 -2 7.12952 16.1538 47 -23 -3 2 15.5229 14.4254 47 -23 -3 -2 3.39837 16.1703 47 -23 3 -3 69.2484 18.6572 47 -23 -3 -3 92.7516 20.1461 47 -23 3 -4 3.28717 14.5064 47 -23 -3 -4 -3.15343 16.6554 47 -23 -3 -5 2.93134 13.1101 47 -23 -3 -6 23.7059 13.4007 47 -23 -4 0 7.32716 10.4859 47 -23 -4 -1 82.1065 15.3561 47 -23 -4 -2 36.9401 13.1886 47 -24 0 0 183.756 25.4795 15 -24 0 0 165.852 24.1938 47 -24 0 -1 -3.71052 13.9896 15 -24 0 1 18.6134 15.9796 15 -24 0 1 10.729 15.9958 47 -24 0 -1 3.72622 15.2941 47 -24 0 -2 18.0156 16.114 15 -24 0 2 -14.514 15.1224 15 -24 0 2 -3.4031 14.3963 47 -24 0 -2 11.0982 17.1854 47 -24 0 -3 -3.42528 14.4942 15 -24 0 3 -13.8646 15.092 15 -24 0 -3 -10.8152 16.3373 47 -24 0 -4 50.7761 16.5359 15 -24 0 4 42.0327 15.8335 15 -24 0 -4 65.5379 17.6055 47 -24 0 -5 -3.21502 14.3788 47 -24 0 -6 34.9052 13.8885 47 -24 1 0 7.25427 15.3463 15 -24 -1 0 -3.60775 15.0383 15 -24 1 0 3.58394 15.1636 47 -24 -1 0 -28.1545 16.9385 47 -24 1 -1 3.58902 14.2621 15 -24 1 1 -10.7929 14.2963 15 -24 -1 -1 3.56619 14.1714 15 -24 -1 1 17.912 13.9965 15 -24 1 1 -10.4351 15.1416 47 -24 1 -1 7.24883 15.5567 47 -24 -1 1 20.5115 16.0737 47 -24 -1 -1 -3.5601 16.1301 47 -24 1 -2 13.9247 15.1659 15 -24 1 2 24.5068 13.9254 15 -24 -1 -2 3.45955 13.2953 15 -24 -1 2 38.3923 16.0264 15 -24 1 2 32.9664 14.9488 47 -24 1 -2 17.9824 16.7185 47 -24 -1 2 6.47361 14.1031 47 -24 -1 -2 14.1349 15.1795 47 -24 1 -3 23.1207 13.9934 15 -24 1 3 20.0105 16.0679 15 -24 -1 -3 29.5233 15.2578 15 -24 -1 3 16.6594 14.1156 15 -24 1 -3 31.499 16.6678 47 -24 -1 -3 17.2454 16.2346 47 -24 1 -4 3.04784 11.908 15 -24 1 4 -3.09795 12.5141 15 -24 -1 -4 -6.05529 12.2302 15 -24 -1 4 -6.19988 13.1141 15 -24 1 -4 -6.67452 14.118 47 -24 -1 -4 6.57518 14.5085 47 -24 1 -5 -3.10121 14.0554 47 -24 -1 -5 -18.3738 16.0249 47 -24 1 -6 30.5954 14.5661 47 -24 -1 -6 11.036 12.6766 47 -24 -2 0 16.0215 12.765 15 -24 2 0 44.9076 16.8058 47 -24 -2 0 27.9464 14.6276 47 -24 -2 -1 9.48177 12.3612 15 -24 -2 1 15.9018 12.6506 15 -24 2 1 30.9746 14.7468 47 -24 2 -1 19.4856 15.4605 47 -24 -2 1 23.9401 15.208 47 -24 -2 -1 6.27784 13.8638 47 -24 -2 -2 27.4466 14.652 15 -24 -2 2 98.864 17.7673 15 -24 2 2 78.6137 16.7584 47 -24 2 -2 54.6951 16.6317 47 -24 -2 2 64.6671 16.4465 47 -24 -2 -2 52.9211 16.874 47 -24 -2 -3 22.9267 12.7096 15 -24 -2 3 43.9032 14.9174 15 -24 2 -3 37.3966 15.8765 47 -24 -2 -3 54.5028 17.2034 47 -24 -2 4 220.586 23.131 15 -24 2 -4 264.906 25.484 47 -24 -2 -4 214.929 23.5211 47 -24 2 -5 72.6731 16.2023 47 -24 -2 -5 84.4045 16.783 47 -24 -3 -1 2.45363 10.6809 47 -24 -3 -2 2.42921 11.6906 47 -25 0 0 -8.15087 11.1508 15 -25 0 0 5.29656 12.1518 47 -25 0 -1 5.34596 11.4735 15 -25 0 1 5.3806 10.868 15 -25 0 1 2.52749 11.598 47 -25 0 -1 2.69379 11.7268 47 -25 0 -2 76.693 14.7686 15 -25 0 2 82.9557 15.4338 15 -25 0 -2 98.6801 17.0022 47 -25 0 -3 35.954 12.6952 47 -25 1 0 -12.915 10.4346 15 -25 -1 0 7.72595 10.4036 15 -25 1 0 -5.05329 11.7382 47 -25 -1 0 -4.97911 10.8378 47 -25 1 -1 45.7061 12.9088 15 -25 1 1 63.8689 15.1813 15 -25 -1 -1 70.8267 14.1093 15 -25 -1 1 68.8395 14.3391 15 -25 1 -1 51.4379 14.4621 47 -25 -1 -1 45.5789 14.0038 47 -25 1 2 63.8015 14.265 15 -25 -1 2 80.892 14.6874 15 -25 1 -2 68.6679 15.1088 47 -25 -1 -2 105.289 16.5806 47 loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag C16 O1 C1 105.39(11) . . ? C18 O4 C14 124.69(12) . . ? C10 N1 H1 115.2 . . ? C16 N1 H1 115.2 . . ? C16 N1 C10 129.53(14) . . ? O1 C1 C8 121.86(14) . . ? C6 C1 O1 111.37(13) . . ? C6 C1 C8 126.75(13) . . ? C24 C4 C22 122.84(14) . . ? C3 C4 C22 117.94(14) . . ? C3 C4 C24 118.96(15) . . ? C1 C6 C12 107.14(12) . . ? C1 C6 C14 118.07(14) . . ? C12 C6 C14 134.57(14) . . ? C18 C8 C1 114.11(15) . . ? C18 C8 C13 119.04(15) . . ? C13 C8 C1 126.84(14) . . ? C20 C10 N1 117.21(14) . . ? C2 C10 N1 123.41(14) . . ? C2 C10 C20 119.35(15) . . ? C16 C12 C6 103.89(13) . . ? C16 C12 C22 120.02(14) . . ? C22 C12 C6 136.06(13) . . ? O4 C14 C6 115.18(14) . . ? O2 C14 O4 116.77(13) . . ? O2 C14 C6 128.04(15) . . ? O1 C16 C12 112.18(13) . . ? N1 C16 O1 118.53(13) . . ? N1 C16 C12 129.28(15) . . ? O4 C18 C8 120.95(14) . . ? C15 C18 O4 117.75(15) . . ? C15 C18 C8 121.30(17) . . ? C10 C20 H20 119.8 . . ? C7 C20 C10 120.48(16) . . ? C7 C20 H20 119.8 . . ? O3 C22 C4 117.46(14) . . ? O3 C22 C12 119.06(14) . . ? C12 C22 C4 123.42(13) . . ? C4 C24 H24 120.3 . . ? C17 C24 C4 119.41(15) . . ? C17 C24 H24 120.3 . . ? C4 C3 H3 119.4 . . ? C19 C3 C4 121.22(16) . . ? C19 C3 H3 119.4 . . ? C8 C13 H13 120.1 . . ? C5 C13 C8 119.73(16) . . ? C5 C13 H13 120.1 . . ? C20 C7 H7 119.9 . . ? C21 C7 C20 120.16(16) . . ? C21 C7 H7 119.9 . . ? C18 C15 H15 120.5 . . ? C9 C15 C18 118.90(17) . . ? C9 C15 H15 120.5 . . ? C10 C2 H2 120.2 . . ? C10 C2 C23 119.54(17) . . ? C23 C2 H2 120.2 . . ? C24 C17 H17 119.6 . . ? C11 C17 C24 120.77(16) . . ? C11 C17 H17 119.6 . . ? C15 C9 H9 119.5 . . ? C15 C9 C5 120.94(17) . . ? C5 C9 H9 119.5 . . ? C3 C19 H19 120.2 . . ? C11 C19 C3 119.63(16) . . ? C11 C19 H19 120.2 . . ? C13 C5 C9 120.08(18) . . ? C13 C5 H5 120.0 . . ? C9 C5 H5 120.0 . . ? C7 C21 H21 120.2 . . ? C7 C21 C23 119.69(17) . . ? C23 C21 H21 120.2 . . ? C17 C11 H11 120.0 . . ? C19 C11 C17 119.96(17) . . ? C19 C11 H11 120.0 . . ? C2 C23 H23 119.6 . . ? C21 C23 C2 120.76(18) . . ? C21 C23 H23 119.6 . . ? loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag O1 C1 1.3776(16) . ? O1 C16 1.3649(19) . ? O4 C14 1.3921(19) . ? O4 C18 1.379(2) . ? O2 C14 1.1976(19) . ? O3 C22 1.2407(19) . ? N1 H1 0.8600 . ? N1 C10 1.413(2) . ? N1 C16 1.3327(18) . ? C1 C6 1.354(2) . ? C1 C8 1.417(2) . ? C4 C22 1.483(2) . ? C4 C24 1.383(2) . ? C4 C3 1.382(2) . ? C6 C12 1.449(2) . ? C6 C14 1.4511(19) . ? C8 C18 1.393(2) . ? C8 C13 1.399(2) . ? C10 C20 1.388(2) . ? C10 C2 1.379(2) . ? C12 C16 1.388(2) . ? C12 C22 1.445(2) . ? C18 C15 1.379(2) . ? C20 H20 0.9300 . ? C20 C7 1.375(2) . ? C24 H24 0.9300 . ? C24 C17 1.382(2) . ? C3 H3 0.9300 . ? C3 C19 1.373(2) . ? C13 H13 0.9300 . ? C13 C5 1.376(2) . ? C7 H7 0.9300 . ? C7 C21 1.366(3) . ? C15 H15 0.9300 . ? C15 C9 1.376(3) . ? C2 H2 0.9300 . ? C2 C23 1.380(3) . ? C17 H17 0.9300 . ? C17 C11 1.374(2) . ? C9 H9 0.9300 . ? C9 C5 1.392(3) . ? C19 H19 0.9300 . ? C19 C11 1.365(3) . ? C5 H5 0.9300 . ? C21 H21 0.9300 . ? C21 C23 1.379(3) . ? C11 H11 0.9300 . ? C23 H23 0.9300 . ? loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_2 _geom_torsion_site_symmetry_3 _geom_torsion_site_symmetry_4 _geom_torsion_publ_flag O1 C1 C6 C12 -0.55(15) . . . . ? O1 C1 C6 C14 -175.91(11) . . . . ? O1 C1 C8 C18 179.43(12) . . . . ? O1 C1 C8 C13 -1.7(2) . . . . ? O4 C18 C15 C9 -179.67(15) . . . . ? N1 C10 C20 C7 178.28(14) . . . . ? N1 C10 C2 C23 -178.39(17) . . . . ? C1 O1 C16 N1 179.49(13) . . . . ? C1 O1 C16 C12 -1.94(15) . . . . ? C1 C6 C12 C16 -0.61(15) . . . . ? C1 C6 C12 C22 177.30(16) . . . . ? C1 C6 C14 O4 -5.49(19) . . . . ? C1 C6 C14 O2 173.48(15) . . . . ? C1 C8 C18 O4 -1.53(19) . . . . ? C1 C8 C18 C15 177.95(14) . . . . ? C1 C8 C13 C5 -178.44(15) . . . . ? C4 C24 C17 C11 -2.2(3) . . . . ? C4 C3 C19 C11 -1.2(3) . . . . ? C6 C1 C8 C18 0.7(2) . . . . ? C6 C1 C8 C13 179.59(14) . . . . ? C6 C12 C16 O1 1.60(16) . . . . ? C6 C12 C16 N1 179.97(15) . . . . ? C6 C12 C22 O3 167.80(16) . . . . ? C6 C12 C22 C4 -15.1(3) . . . . ? C8 C1 C6 C12 178.25(13) . . . . ? C8 C1 C6 C14 2.9(2) . . . . ? C8 C18 C15 C9 0.8(2) . . . . ? C8 C13 C5 C9 0.4(3) . . . . ? C10 N1 C16 O1 8.1(2) . . . . ? C10 N1 C16 C12 -170.22(15) . . . . ? C10 C20 C7 C21 0.4(2) . . . . ? C10 C2 C23 C21 0.0(3) . . . . ? C12 C6 C14 O4 -179.26(13) . . . . ? C12 C6 C14 O2 -0.3(3) . . . . ? C14 O4 C18 C8 -1.5(2) . . . . ? C14 O4 C18 C15 178.99(14) . . . . ? C14 C6 C12 C16 173.63(15) . . . . ? C14 C6 C12 C22 -8.5(3) . . . . ? C16 O1 C1 C6 1.51(15) . . . . ? C16 O1 C1 C8 -177.37(12) . . . . ? C16 N1 C10 C20 144.06(17) . . . . ? C16 N1 C10 C2 -37.9(3) . . . . ? C16 C12 C22 O3 -14.5(2) . . . . ? C16 C12 C22 C4 162.60(14) . . . . ? C18 O4 C14 O2 -174.05(13) . . . . ? C18 O4 C14 C6 5.04(19) . . . . ? C18 C8 C13 C5 0.4(2) . . . . ? C18 C15 C9 C5 0.0(3) . . . . ? C20 C10 C2 C23 -0.4(3) . . . . ? C20 C7 C21 C23 -0.8(3) . . . . ? C22 C4 C24 C17 -172.17(15) . . . . ? C22 C4 C3 C19 174.18(16) . . . . ? C22 C12 C16 O1 -176.73(12) . . . . ? C22 C12 C16 N1 1.6(2) . . . . ? C24 C4 C22 O3 132.98(17) . . . . ? C24 C4 C22 C12 -44.2(2) . . . . ? C24 C4 C3 C19 0.0(3) . . . . ? C24 C17 C11 C19 1.0(3) . . . . ? C3 C4 C22 O3 -41.0(2) . . . . ? C3 C4 C22 C12 141.82(15) . . . . ? C3 C4 C24 C17 1.7(2) . . . . ? C3 C19 C11 C17 0.7(3) . . . . ? C13 C8 C18 O4 179.52(13) . . . . ? C13 C8 C18 C15 -1.0(2) . . . . ? C7 C21 C23 C2 0.6(3) . . . . ? C15 C9 C5 C13 -0.6(3) . . . . ? C2 C10 C20 C7 0.2(2) . . . . ?