Crystallography Open Database

Information card for entry 7159929

Preview

Coordinates	7159929.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H25 N O4
Calculated formula	C24 H25 N O4
Title of publication	Highly enantio- and diastereoselective construction of spirocyclic oxindoles <i>via</i> a palladium-catalyzed decarboxylative asymmetric [4 + 2] annulation strategy.
Authors of publication	You, Pengyuan; Liu, Minjie; Zhang, Ke; Yang, Fan; Tan, Zequn; Chen, Fener
Journal of publication	Organic & biomolecular chemistry
Year of publication	2024
Journal volume	22
Journal issue	22
Pages of publication	4466 - 4471
a	8.0358 ± 0.0003 Å
b	10.9125 ± 0.0004 Å
c	12.2549 ± 0.0005 Å
α	90°
β	90.715 ± 0.001°
γ	90°
Cell volume	1074.56 ± 0.07 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	4
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for all reflections	0.0305
Residual factor for significantly intense reflections	0.0295
Weighted residual factors for significantly intense reflections	0.078
Weighted residual factors for all reflections included in the refinement	0.0793
Goodness-of-fit parameter for all reflections included in the refinement	1.059
Diffraction radiation wavelength	1.34139 Å
Diffraction radiation type	GaKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
293237 (current)	2024-07-05	cif/ Updating files of 7159929 Original log message: Adding full bibliography for 7159929.cif.	7159929.cif
291454	2024-05-02	cif/ Adding structures of 7159929 via cif-deposit CGI script.	7159929.cif