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Information card for entry 7160206
Preview
| Coordinates | 7160206.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | 1 |
|---|---|
| Formula | C31 H26 O6 |
| Calculated formula | C31 H26 O6 |
| Title of publication | Palladium-Catalyzed [3+2] Cycloaddition of 4-Vinyl-4-Butyro-lactones with Sulfamate-Derived Cyclic Imines: Construction of Sulfamate-Fused Pyrrolidines |
| Authors of publication | Sun, Honghao; Ding, Siyuan; Wang, Bo; Huang, Jiaxing; Guo, Hongchao |
| Journal of publication | Organic & Biomolecular Chemistry |
| Year of publication | 2024 |
| a | 8.6209 ± 0.0001 Å |
| b | 14.4274 ± 0.0002 Å |
| c | 20.7278 ± 0.0003 Å |
| α | 90° |
| β | 91.201 ± 0.002° |
| γ | 90° |
| Cell volume | 2577.5 ± 0.06 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 K |
| Number of distinct elements | 3 |
| Space group number | 14 |
| Hermann-Mauguin space group symbol | P 1 21/n 1 |
| Hall space group symbol | -P 2yn |
| Residual factor for all reflections | 0.0415 |
| Residual factor for significantly intense reflections | 0.0375 |
| Weighted residual factors for significantly intense reflections | 0.1059 |
| Weighted residual factors for all reflections included in the refinement | 0.1095 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.059 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 295814 (current) | 2024-11-07 | cif/ Adding structures of 7160206 via cif-deposit CGI script. |
7160206.cif |
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