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Information card for entry 7160539
Preview
| Coordinates | 7160539.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C32 H33 N3 O6 |
|---|---|
| Calculated formula | C32 H33 N3 O6 |
| Title of publication | Synthesis of 3-indolyl all-carbon quaternary centers via Rh/Brønsted acid co-catalyzed three-component reactions of azoalkenes with indoles and diazoacetates |
| Authors of publication | Yue, Xiao-Jing; Pei, Li-Ping; Wang, Mincan; Jia, Shi-Kun; Mei, Guang-Jian |
| Journal of publication | Organic & Biomolecular Chemistry |
| Year of publication | 2025 |
| a | 8.75449 ± 0.00018 Å |
| b | 16.6482 ± 0.0004 Å |
| c | 19.5357 ± 0.0004 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 2847.26 ± 0.11 Å3 |
| Cell temperature | 293 ± 2 K |
| Ambient diffraction temperature | 293 ± 2 K |
| Number of distinct elements | 4 |
| Space group number | 19 |
| Hermann-Mauguin space group symbol | P 21 21 21 |
| Hall space group symbol | P 2ac 2ab |
| Residual factor for all reflections | 0.0696 |
| Residual factor for significantly intense reflections | 0.0601 |
| Weighted residual factors for significantly intense reflections | 0.1603 |
| Weighted residual factors for all reflections included in the refinement | 0.1723 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.041 |
| Diffraction radiation probe | x-ray |
| Diffraction radiation wavelength | 1.54184 Å |
| Diffraction radiation type | CuKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 299590 (current) | 2025-05-09 | cif/ Adding structures of 7160539, 7160540 via cif-deposit CGI script. |
7160539.cif |
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Users of the data should acknowledge the original authors of the
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